NC0000078_Groundwater Monitoring Report July 2023_20230802

GW-59A COMPLIANCE REPORT FORM Permit # i1G4d@p 7e (Submit one each monitoring period with GW--59 forms.)
j Enter date monitoring results were due. Wilt this monitoring report (GW-59 and GW-59A) YES NO
be submitted after tbee stablished due dat
2 Was any required information missing on the GW-59 report forms?
IF the answer to question 1 or 2 is "YES'; list in the space provided below the well
explain the problems encountered in obtaining the required information.
and
YES
3 1 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or m�guidanee.
ng cap, missing YES identification plate, area overgrown, etc.)? If the answer is `"Yes'; contact the Regional Office for
4 Are any monitored constituents equal to or above the established standards? '
If the answer to question 4 is "NO" skip to section B. YES NO
If the answer to question 4 is "YES" list the affected wells individually with constituents) and concentrations)
exceeding standards in the space provided below,•
W1
6
VA
0 -1��
For the constituent identified in question 4 above, have standards been
same constituents, in the same well(s) in the last two years?
If the answer to que tion 5 is "NO", skip to section 8.
If the answer to qu estion 5 is "YES" list in the space provided below, each well with constituent(s) exceeding
standards, concentration'�(s) reported, and sample collection date for each occurrence (for the last two years).
Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES
if the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELYFOR GUIDANCE, if the answer is "NO", monitoring wells maybe improperly
located; contact the Regional Office.
Is the permittee implementing previously approved actions required by the Division involving this YES NO
groundwater quality problem?
If the answer to question 7 is "YES" describe those actions in the space provided below.
If the answer to question 7Is "No-, contact the Realonal office within on
I ne person completing this portion (GW--59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
GW-59A 12f8/2003

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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
July 21, 2023
Mr. Bernie Kelly
Davidson River Village, LLC
P.O. Box 880
Pisgah Forest, NC 28768
RE: Project: MWs July 2023
Pace Project No.: 92676227
Dear Mr. Kelly:
Enclosed are the analytical results for sample(s) received by the laboratory on July 07, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Sara Poulson
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pagel of 21

CERTIFICATIONS
Project: MWs July 2023
Pace Project No.: 92676227
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Drinking Water Cert. #: 99006003
North Carolina Drinking Water Certification #: 37706
Florida/NELAP Certification #: E87627
North Carolina Field Services Certification #: 5342
Kentucky UST Certification #: 84
North Carolina Wastewater Certification #: 12
Louisiana DoH Drinking Water #: LA029
South Carolina Laboratory ID: 99006
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804 South Carolina Laboratory ID: 99030
Florida/NELAP Certification #: E87648 South Carolina Certification #: 99030001
North Carolina Drinking Water Certification #: 37712 Virginia/VELAP Certification #: 460222
North Carolina Wastewater Certification #: 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 21

,I�Face'-3'
Project: MWs July 2023
Pace Project No.: 92676227
Lab ID Sample ID
92676227001 Q88V2
92676227002 ASB-01
92676227003 ASB-02
PAS I -A = Pace Analytical Services -Asheville
PASI-C = Pace Analytical Services - Charlotte
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Method
Analysts
Analytes
Reported
Laboratory
EPA 6010D
DBB1
6
PAS [-A
EPA 6020B
CRW
1
PASI-A
EPA 7470A
NMP
1
PASI-A
SM 2540C-2015
MA82
1
PASI-A
EPA 300.0 Rev 2.1 1993
JCM
1
PASI-A
EPA 350.1 Rev 2.0 1993
ARJ
1
PASI-A
SM 5310B-2014
MJP
1
PASI-A
EPA 6010D
DBB1
6
PASI-A
EPA 60208
CRW
1
PASI-A
EPA 7470A
NMP
1
PASI-A
SM 2540C-2015
MA132
1
PASI-A
EPA 300.0 Rev 2.1 1993
JCM
1
PASI-A
EPA 350.1 Rev 2.0 1993
ARJ
1
PASI-A
SM 5310B-2014
MJP
1
PASI-A
EPA 6010D
DBB1
6
PASI-A
EPA 6020E
CRW
1
PASI-A
EPA 7470A
NMP
1
PASI-A
SM 2540C-2015
MAB2
1
PASI-A
EPA 300.0 Rev 2.1 1993
JCM
1
PASI-A
EPA 350.1 Rev 2.0 1993
ARJ
1
PASI-A
SM 5310B-2014
MJP
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 21

Pace Analytical Services, LLC
2225 Riverside Dr.
aca, Asheville, NC 28804
I [phone]
ANALYTICAL RESULTS
Project: MWs July 2023
Pace Project No.: 92676227
Sample: Q88V2 Lab ID: 92676227001 Collected: 07/07/23 12:25 Received: 07/07/23 12:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
07/21/23 13:29
Collected By
MS
1
07/21/23 13:29
Collected Date
07/07/23
1
07/21/23 13:29
Collected Time
12:25
1
07/21/23 13:29
pH
5.5 Std. Units
1
07/21/23 13:29
Temperature
19.2 deg C
1
07/21/23 13:29
Static Water Level
58.75 feet
1
07/21/23 13:29
Specific Conductance
16.3 umhos/cm
1
07/21/23 13:29
Oxygen, Dissolved
6.15 mg/L
1
07/21/23 13:29
7782-44-7
Total Well Depth
68.50 feet
1
07/21/23 13:29
REDOX
21.5 my
1
07/21/23 13:29
Turbidity
4.99 NTU
1
07/21/23 13:29
Odor
None
1
07/21/23 13:29
Appearance
Clear
1
07/21/23 13:29
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Arsenic
ND ug/L 10.0
1 07/10/2311:37
07/11/2313:51
7440-38-2
Chromium
ND ug/L 5.0
1 07/10/2311:37
07/11/2313:51
7440-47-3
Iron
56.9 ug/L 50.0
1 07/10/2311:37
07/11/2313:51
7439-89-6
Lead
ND ug/L 5.0
1 07/10/2311:37
07/11/2313:51
7439-92-1
Manganese
ND ug/L 5.0
1 07/10/2311:37
07/11/2313:51
7439-96-5
Sodium
15200 ug/L 5000
1 07/10/2311:37
07/11/2313:51
7440-23-5
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Cobalt
ND ug/L 1.0
1 07/10/23 11:37
07/10/23 20:03
7440-48-4
7470 Mercury
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services -Asheville
Mercury
ND ug/L 0.20
1 07/12/23 09:14
07/13/23 11:53
7439-97-6
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
Total Dissolved Solids
85.0 mg/L 25.0
1
07/11/23 11:07
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services - Asheville
Sulfate
4.6 mg/L 1.0
1
07/09/23 00:32
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
Nitrogen, Ammonia
NO mg/L 0.10
1
07/20/23 11:45
7664-41-7
Date: 07/21/2023 04:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 21

(_Vace'�'
Project: MWs July 2023
Pace Project No.: 92676227
Sample: Q88V2
Parameters
53108 TOC
Total Organic Carbon
Date: 07/21/2023 04:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr,
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Lab ID: 92676227001 Collected: 07/07/23 12:25 Received: 07/07/23 12:45 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
ND mg/L 1.0 1 07/12/23 20:23 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 21

(_Vace"�'
Project: MWs July 2023
Pace Project No.: 92676227
Sample: ASB-01
Parameters
Monitoring Well Data
Performed by
Collected By
Collected Date
Collected Time
pH
Temperature
Static Water Level
Specific Conductance
Oxygen, Dissolved
Total Well Depth
REDOX
Turbidity
Odor
Appearance
6010 MET ICP
Arsenic
Chromium
Iron
Lead
Manganese
Sodium
6020 MET ICPMS
Cobalt
7470 Mercury
Mercury
2540C Total Dissolved Solids
Total Dissolved Solids
300.0 IC Anions 28 Days
Sulfate
350.1 Ammonia
Nitrogen, Ammonia
Date: 07/21/2023 04:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Lab ID: 92676227002 Collected: 07/07/23 10:05 Received: 07/07/23 12:45
Matrix: Water
Results Units Report Limit DF Prepared
Analyzed
CAS No.
Analytical Method:
Pace Analytical Services - Charlotte
Pace 1
07/21/23 13:31
MS 1
07/21/23 13:31
07/07/23 1
07/21/23 13:31
10:05 1
07/21/23 13:31
5.91 Std. Units 1
07/21/23 13:31
17.8 deg C 1
07/21/23 13:31
8.65 feet 1
07/21/23 13:31
401.3 umhos/cm 1
07/2112313:31
0.19 mg/L 1
07/2112313:31
7782-44-7
15 feet 1
07/21/23 13:31
76.2 my 1
07/21/23 13:31
7.31 NTU 1
07/21/23 13:31
None 1
07/21/23 13:31
Clear 1
07/21/23 13:31
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
ND ug/L 10.0 1 07/10/2311:37
07/11/2313:53
7440-38-2
ND ug/L 5.0 1 07/10/2311:37
07/11/2313:53
7440-47-3
1550 ug/L 50.0 1 07/10/2311:37
07/11/2313:53
7439-89-6
ND ug/L 5.0 1 07/10/2311:37
07/11/2313:53
7439-92-1
1940 ug/L 5.0 1 07/10/2311:37
07/11/2313:53
7439-96-5
29900 ug/L 5000 1 07/10/2311:37
07/11/2313:53
7440-23-5
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
4.0 ug/L 1.0 1 07/10/23 11:37
07/10/23 20:08
7440-48-4
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
ND ug/L 0.20 1 07/12/23 09:14
07/13/23 11:55
7439-97-6
Analytical Method: SM 2540C-2015
Pace Analytical Services -Asheville
252 mg/L 25.0 1
07/11/2311:07
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
8.0 mg/L 1.0 1
07/09/23 00:47
14808-79-8
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
ND mg/L 0.10 1
07/2012311:47 7664-41-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Qual
Page 6 of 21

%ace"
Project: MWs July 2023
Pace Project No.: 92676227
Sample: ASB-01
Parameters
5310B TOC
Total Organic Carbon
Date: 07/21/2023 04:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Lab ID: 92676227002 Collected: 07/07/23 10:05 Received: 07/07/23 12:45 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
ND mg/L 1.0 1 07/12/23 21:14 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 21

(-Vace-"
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr,
Asheville, NC 28804
[phone]
Project: MWs July 2023
Pace Project No.: 92676227
Sample: ASB-02
Lab ID: 92676227003 Collected: 07/07/23 10:50
Received: 07/07/23 12:45 Matrix: Water
Parameters
Results Units Report Limit
DF
Prepared
Analyzed
CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
07/21/23 13:30
Collected By
MS
1
07/21/23 13:30
Collected Date
07/07/23
1
07/21/23 13:30
Collected Time
10:50
1
07/21/23 13:30
pH
5.78 Std. Units
1
07/21/23 13:30
Temperature
19.7 deg C
1
07/21/23 13:30
Static Water Level
8.98 feet
1
07/21/23 13:30
Specific Conductance
152.1 umhos/cm
1
07/21/23 13:30
Oxygen, Dissolved
2.32 mg/L
1
07/21/23 13:30
7782-44-7
Total Well Depth
12 feet
1
07/21/23 13:30
REDOX
12.9 my
1
07/2112313:30
Turbidity
0.96 NTU
1
07/21/23 13:30
Odor
None
1
07/21/23 13:30
Appearance
Clear
1
07/21/23 13:30
6010 MET ICP
Analytical Method: EPA 601 OD Preparation Method:
EPA 3010A
Pace Analytical Services -Asheville
Arsenic
ND ug/L 10.0
1
07/10/2311:37
07/11/2314:08
7440-38-2
Chromium
5.8 ug/L 5.0
1
07/10/2311:37
07/11/2314:08
7440-47-3
Iron
98.3 ug/L 50.0
1
07/10/2311:37
0711112314:08
7439-89-6
Lead
ND ug/L 5.0
1
07/10/2311:37
07/11/2314:08
7439-92-1
Manganese
8.8 ug/L 5.0
1
07/1012311:37
07/11/2314:08
7439-96-5
Sodium
ND ug/L 5000
1
07/10/2311:37
07/11/2314:08
7440-23-5
6020 MET ICPMS
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services -Asheville
Cobalt
ND ug/L 1.0
1
07/10/23 11:37
07/10/23 20:13
7440-48-4
7470 Mercury
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Asheville
Mercury
ND ug/L 0.20
1
07/12/23 09:14
07/13/23 11:58
7439-97-6
2540C Total Dissolved Solids
Analytical Method: SM 2540C-2015
Pace Analytical Services - Asheville
Total Dissolved Solids
ND mg/L 25.0
1
07/11/23 11:07
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Pace Analytical Services -Asheville
Sulfate
ND mg/L 1.0
1
07/09/23 01:02
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
07/20/23 11:48
7664-41-7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/21/2023 04:09 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 21

�ce
Project: MWs July 2023
Pace Project No.: 92676227
Sample: ASS-02
Parameters
5310B TOC
Total Organic Carbon
Date: 07/21/2023 04:09 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Lab ID: 92676227003 Collected: 07/07/23 10:50 Received: 07/07/23 12:45 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
ND mg/L 1.0 1 07/12/23 21:31 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 21

,� ace,�,
QUALITY CONTROL DATA
Project: MWs July 2023
Pace Project No.: 92676227
QC Batch: 786136
Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A
Analysis Description: 7470 Mercury
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92676227001, 92676227002, 92676227003
METHOD BLANK: 4075898
Matrix: Water
Associated Lab Samples: 92676227001,
92676227002, 92676227003
Blank Reporting
Parameter
Units Result Limit Analyzed Qualifiers
Mercury
ug/L ND 0.20 07/13/2310:59
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 4075899
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.6 102 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4075900 4075901
MS MSD
92674166001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 2.5 2.5 99 97 75-125 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/21/2023 04:09 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 21

(-�Face­
QUALITY CONTROL DATA
Project: MWs July 2023
Pace Project No.: 92676227
QC Batch: 785636
Analysis Method:
EPA 601 OD
QC Batch Method: EPA 3010A
Analysis Description:
6010 MET
Laboratory:
Pace Analytical Services -Asheville
Associated Lab Samples: 92676227001, 92676227002, 92676227003
METHOD BLANK: 4073370
Matrix: Water
Associated Lab Samples: 92676227001,
92676227002, 92676227003
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Arsenic
ug/L
ND
10.0 07/11/2313:18
Chromium
ug/L
ND
5.0 07/11/2313:18
Iron
Lead
ug/L
ND
50.0 0711112313:18
Manganese
ug/L
ND
5.0 07/11/2313:18
Sodium
ug/L
ND
5.0 07/11/2313:18
ug/L
ND
5000 07/11/2313:18
LABORATORY CONTROL SAMPLE: 4073371
Parameter Units
Arsenic ug/L
Chromium ug/L
Iron ug/L
Lead ug/L
Manganese ug/L
Sodium ug/L
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Spike
LCS
LCS
% Rec
Conc.
Result
% Rec
Limits Qualifiers
500
531
106
80-120
500
544
109
80-120
5000
5450
109
80-120
500
533
107
80-120
500
545
109
80-120
5000
5360
107
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
4073372
4073373
MS
MSD
92675538018
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
Arsenic
Chromium
ug/L
ND
500
500
546
535
109
107
75-125
2
Iron
ug/L
ND
500
500
550
537
110
107
75-125
3
ug/L
6820
5000
5000
12400
12200
112
107
75-125
2
Lead
ug/L
ND
500
500
536
523
107
105
75-125
2
Manganese
ug/L
413
500
500
964
934
110
104
75-125
3
Sodium
ug/L
4410J
5000
5000
9790
9590
108
104
75-125
2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/21/2023 04:09 PM without the written consent of Pace Analytical Services, LLC.
Qual
Page 11 of 21

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: MWs July 2023
Pace Project No.: 92676227
QC Batch: 785642
Analysis Method:
EPA 6020B
QC Batch Method: EPA 3010A
Analysis Description:
6020 MET
Laboratory:
Pace Analytical Services -Asheville
Associated Lab Samples: 92676227001, 92676227002, 92676227003
METHOD BLANK: 4073392
Matrix: Water
Associated Lab Samples: 92676227001, 92676227002, 92676227003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Cobalt ug/L
ND 1.0 07/1012319:08
LABORATORY CONTROL SAMPLE: 4073393
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Cobalt ug/L
50 52.1
104 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4073394
4073395
MS MSD
92674921001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qua]
Cobalt ug/L 0.59J
50 50 52.1
52.6 103 104 75-125 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/21/2023 04:09 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 21

Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: MWs July 2023
Pace Project No.: 92676227
QC Batch: 785890
Analysis Method:
SM 2540C-2015
QC Batch Method: SM 2540C-2015
Analysis Description:
2540C Total Dissolved Solids
Laboratory:
Pace Analytical Services -Asheville
Associated Lab Samples: 92676227001,
92676227002, 92676227003
METHOD BLANK: 4074421
Matrix: Water
Associated Lab Samples: 92676227001, 92676227002, 92676227003
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Dissolved Solids
mg/L
ND 25.0
07/11/23 11:03
LABORATORY CONTROL SAMPLE:
4074422
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Total Dissolved Solids
mg/L
250 252
101 90-110
SAMPLE DUPLICATE: 4074423
92676120020 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mg/L 67.0 74.0 10
SAMPLE DUPLICATE: 4074424
92676124008 Dup
Parameter Units Result Result RPD Qualifiers
Total Dissolved Solids mg/L 244 244 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/21 /2023 04:09 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 21

( ace..
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: MWs July 2023
Pace Project No.: 92676227
QC Batch: 785534
Analysis Method:
EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993
Analysis Description:
300.0 IC Anions
Laboratory:
Pace Analytical Services -Asheville
Associated Lab Samples: 92676227001, 92676227002, 92676227003
METHOD BLANK: 4073213
Matrix: Water
Associated Lab Samples: 92676227001, 92676227002, 92676227003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Sulfate mg/L
ND 1.0 07/08/23 20:33
LABORATORY CONTROL SAMPLE: 4073214
Spike LCS
LCS % Rec
Parameter Units
Cone. Result
% Rec Limits Qualifiers
Sulfate mg/L
50 49.8
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4073215
4073216
MS MSD
92676226002
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Cone. Cone. Result
Result % Rec % Rec
Limits RPD Qual
Sulfate mg/L 15.6
50 50 66.1
68.8 101 107
90-110 4
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4073217
4073218
MS MSD
92676082003
Spike Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Cone. Cone. Result
Result % Rec % Rec
Limits RPD Qual
Sulfate mg/L 149
50 50 200
200 103 102
90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/21/2023 04:09 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 21

(�Vace,3,
QUALITY CONTROL DATA
Project: MWs July 2023
Pace Project No.: 92676227
QC Batch: 787659 Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92676227001, 92676227002, 92676227003
METHOD BLANK: 4083294 Matrix: Water
Associated Lab Samples: 92676227001, 92676227002, 92676227003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/L ND 0.10 07/20/23 11:07
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 4083295
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/L 5 5.1 102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4083296 4083297
MS MSD
92676070001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/L 7.5 5 5 12.5 12.4 100 99 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4083298 4083299
MS MSD
92676078001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/L 3.5 5 5 8.3 8.3 96 96 90-110 0
Results presorted on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/21/2023 04:09 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 21

I�Face�-3'
QUALITY CONTROL DATA
Project: MWs July 2023
Pace Project No.: 92676227
QC Batch: 786246
Analysis Method: SM 531 OB-2014
QC Batch Method: SM 531OB-2014
Analysis Description: 5310B TOC
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92676227001, 92676227002, 92676227003
METHOD BLANK: 4076401
Matrix: Water
Associated Lab Samples: 92676227001, 92676227002, 92676227003
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Total Organic Carbon mg/L
ND 1.0 07/12/23 13:50
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 4076402
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Organic Carbon mg/L 25 24.8 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4076403 4076404
MS MSD
92675699001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
Total Organic Carbon mg/L ND 25 25 23.9 23.9 94 94 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4076405 4076406
MS MSD
92675495001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L ND 25 25 23.3 23.5 93 94 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/21/2023 04:09 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 21

I�Face",
QUALIFIERS
Project: MWs July 2023
Pace Project No.: 92676227
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
'Total' may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
Date: 07/21/2023 04:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 21

QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: MWs July 2023
Pace Project No.: 92676227
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92676227001
Q88V2
92676227002
ASB-01
92676227003
ASB-02
92676227001
92676227002
92676227003
92676227001
92676227002
92676227003
92676227001
92676227002
92676227003
Q88V2
ASB-01
ASB-02
Q88V2
ASB-01
ASB-02
Q88V2
ASB-01
ASB-02
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 3010A
EPA 7470A
EPA 7470A
EPA 7470A
785636
785636
785636
785642
785642
785642
786136
786136
786136
EPA
EPA
EPA
EPA
EPA
EPA
EPA
EPA
EPA
6010D
6010D
6010D
6020B
60206
60206
7470A
7470A
7470A
785742
785742
785742
785766
785766
785766
786221
786221
786221
92676227001
92676227002
92676227003
Q88V2
ASB-01
ASB-02
SM 2540C-2015
SM 2540C-2015
SM 2540C-2015
785890
785890
785890
92676227001
92676227002
92676227003
Q88V2
ASB-01
ASB-02
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
EPA 300.0 Rev 2.1 1993
785534
785534
785534
92676227001
92676227002
92676227003
Q88V2
ASB-01
ASB-02
EPA 350.1 Rev 2.0 1993
EPA 350.1 Rev 2.0 1993
EPA 350.1 Rev 2.0 1993
787659
787659
787659
92676227001
92676227002
92676227003
Q88V2
ASB-01
ASB-02
SM 5310B-2014
SM 5310B-2014
SM 5310B-2014
786246
786246
786246
Date: 07/21/2023 04:09 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 18 of 21

' ­ .... . . . ... . ...
���2 DC# —Title: ENV-FRM-HUNI-0083 02—Sample Condition Upon Receipt
Effective Date: 11/14/2022 8:1830 AM
Laboratory receiving samples:
AshevilleO.-I, EdenEl Greenwood Huntersvillen RaleighEl MethanicsvilleO AtlantaEl Kernersvillen
MHEM Client Name: Project #: . WO#t: 92t")76227
P"/L
Courier: i-IFedEx 0 UPS EJLISPS Ocilent
0 Commercial UP-66'e, El Other:
Custody Seat Present? 171 yes
0 N'b" Seals Intact? ❑ Yes
DIN
Packing Material: 171 Bubble Wrap 0,1`ubble Bags E]None 171 other
Thermome
0 '�W15_un ID, 50
Type of Ice: 0-Wiet 08[ue
Correction Factor:
Cooler Temp: Add/Subtract VC)
Cooler Temp Corrected (14",
USDA Regulated Soll ON/A, water sample)
Did samples originate in a quarantine zone within the United States. CA, NY, or 5C
trhprk tnanto riv— nm.
92576227
Date/Initials Person Examining Contents .!I 4
Biological Tissue Fr en?
0Yes EINo 13N/A
ONone
Temp should be above freezing to VC
[hamples out of temp criteria. Sampleson ice,cooling process
has begun
did samples originate from a foreign source (internationally,
Comments/Discrepancy:
-Chain of Custody Present?
ye's
Cto
N/A
1.
-Samples Arrived within Hold TIme7
K-
13 No
0 N/A
2,
-Short Hold rime Analysts (02 hr.)?
121714u,_.
0 N/A
1
-Rush Turn Around Time Requested?
Oyes
EJ'N.
0 N/A
4.
-Sufficient volume?
Xes,
0 N.
0 NIA
S.
Correct Containers Used?
-Pace Containers Used?
f
LIYes�
ONO
ONo
0 N/A
C3 N/A
6.
-Containers Intact?
nYes
ONo
C3 N/A
7:
Dissolved analysis; Samples Field Filtered?
nyes
0 No
N/A
3.
Sample Labels Match COC?
-includes Date/Time/lO/Analysis Matrix:
es 0 No
0 N/A
9.
Headspace in VOA Vials (55-6mm)?
yes
0 No
15N/A
10
Trip Blank Present?
i.Trip Blank Custody Seals Present?
Cities
0 Y'LS
0 � C3 N/A
0 No �;A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUMN
Person contacted:
Project Manager SCURF Review-,
Project ManagerSRF Review:
Date/Time:
Date:
Date,
Field uata Required? UYes UNo
Page 19 of 21
r)tsaor.;3v In. AQA1A P-aelr� 4 of

DC# -Title: ENV-FRM-HUNI-0083 02-Sample^ Condition Upon Receipt ^
Effective Date:11/14/2022 8:18:30 AM'
*Cheek mark tap half of box if pH and/or dechlorination is verified and Project f
WO#:92676227
within the acceptance range for preservation samples. PM: SC Due Date: 07/21/23
Exceptions: VOA, Coliform, TOC, Oil and Grease, RRO/8015 (water) DOt , LLHg CLIENT: 93—D&v14sanR
*Bottom half of box is to list number of bottles
'Check all unpreserved Nitrates for chlorine