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HomeMy WebLinkAboutWQ0002857_Monitoring - 10-2023_20231214Monitoring Report Submittal Permit Number#* Name of Facility:* Month: * October WQ0002857 Piedmont Custom Meats Report Information Type * Revised - NDMR, NDAR-1, NDAR-2, NDMLR Year:* 2023 Upload Document* Revised NDMR Piedmont Custom Meats.pdf PDF Only 1.5MB Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address: * amiecferguson@gmail.com Name of Submitter: * Arnie Ferguson Signature: Date of submittal: 12/14/2023 This will be filled in automatically Initial Review Reviewer: Wanda.Gerald Is the project number correct?* WQ0002857 Is the monitoring report accepted?* Yes No Regional Office* Winston-Salem Reviewer: _anonymous Review Date: 12/18/2023 FORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page of Permit No.: WQ0002857 Facility Name: Piedmont Custom Meats WWTF County: Caswell Month: October Year: 2023 PPI: 001 . Influent Effluent - _ No now generated Parameter Monitoring Point: influent ,- Effluent Groundwater Lowenng Surface water Parameter Code P 50050 50060 31616 00610 00625 00620 00600 00400 00665 00530 00310 00940 70300 ro EP O m 0:0 O a u o ° c lac 12 Z Y .= °Z IL +`9mc� a �m o m Va)_ ° '° mo0 aN 0 24-hr hrs GPD mg1L #1100 mL mg1L mg1L mg1L mg1L su mg1L mg1L m mg1L mg1L 1 1,011 2 1.011 3 1,011 4 0745 025 1,011 <0 01 63 5 1,011 6 1.011 7 982 81 982 9 1 982 101 982 111 1053 0.25 982 <0 01 66 121 1 982 131 1 982 141 1 1,140 151 1 1,140 161 1 1 140 171 1 1,140 181 08-10 1 05 1,140 <0 01 65 191 1 1,140 201 1 1,140 211 1 997 221 1 997 231 1 997 241 1 997 251 1 997 26 12.09 1.25 997 <0.01 2420 54.5 166 1 182 6.5 18.5 1550 581 131 1 640 27 997 28 997 29 995 30 995 311 995 4.5 Average: 1,028 0.00 2,420.00 54.50 166.00 4.50 182.00 18.50 1,550.00 581.00 1 131.00 640.00 Daily Maximum: 1,140 0.01 2,420.00 54.50 166.00 4.50 182.00 6.60 18.50 1,550.00 581.00 131.00 640.00 Daily Minimum: 982 0.01 2,420.00 1 54.50 166.0G 4.50 182.00 6.30 18.50 1,550.00 581.00 131.00 540.00 Sampling Type: Estimate Grab Grab Grab Grab Grab Grab Grab Grab Grab Grab Monthly Avg. Limit: 5,000 Daily Limit: Sample Frequency: Monthly Weekly 3xyr 3xyr I 3xyr 3xyr 3xyr Weekly 3xyr 3xyr 3xyr FORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page of Sampling Person(s) Name: Glenn Price Name Certified Laboratories Name: Pace Analytical Laboratories Name: Does all monitorina data and samnlina freauencies meet the requirements in Attachment A of vour nermit? 17i ompriant Non -compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective taKen. Anacn aaartlonal sheets It necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Glenn Price Permittee: Baron Neal McDuffie (Authorized Agent) Certification No.: 987931/20771 signing official: Baron Neal McDuffie Grade: 11 Phone Number: 336-408-7924 Signing Official's Title: Field Services Director (Pace Analytical Services) Has the ORC changed since the previous NDMR? yes fvo Phone Number. 336-402-9924 Permit Expiration: 3/31/2021 Signature Date SignatwoK Date By this signature I cenify that this report is accurrate and complete to the best of my knowledge I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel property gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or Ihose persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief. true. accurale, and complete. I am aware that there are significant penalties for submitting false information. including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM. NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of Permit No.: WQ0002857 Facility Name: Piedmont Custom Meats WWTF County: Caswell Month: October Year: 2023 Field Name: 1 Field Name: 2 Field Name: 3 Field Name: 4 Did irrigation occur Area (acres): 1 Area (acres): 1 Area (acres): 1 Area (acres): 0.92 at this facility? Cover Crop: P� Fescue Cover P� Fescue Cover P� Fescue Cover P: Fescue YES NO Hourly Rate (in): 0.15 Hourly Rate (in): 0.15 Hourly Rate (in): 0.15 Hourly Rate (in): 0.15 Annual Rate (in): 52 Annual Rate (in): 52 Annual Rate (in): 52 Annual Rate (in): 52 Weather Freeboard Field Irrigated? YES ❑ No Field Irrigated? El YES 0 NO Field Irrigated? O YES ❑ No Field Irrigated? O YES ❑ NO co m r a E m ~ c ° oLo m a V D. w v m o 0 J mm a E M a ? >-Op v�mDD TO a` C E E a I Em m'E T87 _j E m s 00 01 m 2 co C R aom Jt E am64M C E � 0m J 3 'F in ft ft gal min in in gal min in in gal min in in gal min in in 1 2 I 3 41 PC 1 52 0 2 2 5 6 7 8 91 1I 10 ill C 1 72 0 1 2 2 12 13 14 15 16 j 17 18 PC 49 0 2.1 11,160 310 0.41 0.08 11,160 310 0.41 008 1 11,160 310 0.41 0.08 11160 310 1 0.45 0.09 19 20 21 22 23 24 25 261 C 1 71 0 2.8 27 I 28 29 30 31 Monthly Loading: 12 Month Floating Total (in): 11,160 - ' 0.41 2.97 11,160 0.41 2.97 11,160 0.41 2.97 EEJ11 160 0.45 3 13 FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of Did the application rates exceed the limits in Attachment B of your permit? IaCompliant ❑ Non -Compliant Were adequate measures taken to prevent effluent ponding in or runoff from the sites?@'Compliant ❑ Non -Compliant Was a suitable vegetative cover maintained on all sites as specified in your permit? C9Compliant ❑ Non -Compliant Were all setbacks listed in your permit maintained for every application to each permitted site? Compliant ❑ Non -Compliant Were all freeboards maintained in accordance with the specified freeboard heights in your permit? Ci mpliant ❑ Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective dcuunts) rdnrn. nudui duunwndi sneers n IOperator in Responsible Charge (ORC) Certification II Permittee Certification I i ORC: Glenn Price I Certification No.: 987931/20771 I Grade: II Phone Number: 336-408-7924 Has the ORC changed since the previous NDARA? ❑ Yes p No Signature Date By this signature I certify that this report is accurrate and complete to the best of my knowledge Permittee: Baron Neal McDuffie (Authorized Agent) Signing Official: Baron Neal McDuffie Signing Official's Title: Field Service Director (Pace Analytical Services Phone Number: 336-402-9924 Permit Exp.: 3/31/21 nature ►a , Of Date I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel property gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 ��ace November 10, 2023 Larry Moore Piedmont Custom Meats 430 NC Highway 49 South Asheboro, NC 27205 RE. Project. Piedmont Custom Meats- Oct Pace Project No.. 92695435 Dear Larry Moore. 1377 South Park Drive Kernersville NC 27284 Enclosed are the analytical results for sample(s) received by the laboratory on October 26, 2023. The results relate only to the samples Included in this report Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network. • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte • Pace Analytical Services - Eden If you have any questions concerning this report, please feel free to contact me. Sincerely, Stephanie Knott stephanie.knott@pacelabs.com 704-977-0981 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services LLC (704)977-0981 Page 1 of 34 ��ace —"..,y.,....—.,.... , ", 1377 South Park Drive Kernersville, NC 27284 (704)977.0981 CERTIFICATIONS Project Piedmont Custom Meats- Oct Pace Project No 92695435 Pace Analytical Services Charlotte South Carolina Laboratory ID 99006 South Carolina Certification # 99006001 9800 Kincey Ave. Ste 100 Huntersville, NC 28078 South Carolina Drinking Water Cent. # 99006003 North Carolina Drinking Water Certification # 37706 Florida/NELAP Certification # E87627 North Carolina Field Services Certification #: 5342 Kentucky UST Certification # 84 North Carolina Wastewater Certification #: 12 Louisiana DoH Dr nking Water # LA029 South Carolina Laboratory ID: 99006 VirginiaNELAP Certification # 460221 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 South Carolina Laboratory ID 99030 Florida1NELAP Certification #: E87648 South Carolina Certification # 99030001 North Carolina Drinking Water Certification #: 37712 Virginia/VELAP Certification # 460222 North Carolina Wastewater Certification #: 40 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Wastewater Certification #: 633 North Carolina Drinking Water Certification #: 37738 VirginiaNELAP Certificat on #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC Page 2 of 34 ��ace Project P edmont Custom Meats- Oct Pace Project No 92695435 Lab ID Sample ID 92695435001 MW-1 92695435002 MW-4 92695435003 MW-5 92695435004 Effluent PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte PAS I-E = Pace Analytical Services - Eden 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 SAMPLE ANALYTE COUNT Method Analysts Analytes Reported Laboratory SM 2540C-2015 AED 1 PASI-E EPA 350 1 Rev 2 0 1993 SRS 1 PASI-E SM 9222D-2015 DAW 1 PASI-E EPA 8260D JJK 63 PASI-C SM 5310B 2014 MJP 1 PASI-A SM 2540C 2015 AED 1 PASI-E EPA 350 1 Rev 2 0 1993 SRS 1 PASI-E SM 9222D-2015 DAW 1 PASI-E EPA 8260D JJK 63 PASI-C SM 53106-2014 MJP 1 PASI-A SM 254OC-2015 AED 1 PASI-E EPA 350 1 Rev 2 0 1993 SRS 1 PASI-E SM 9222D-2015 DAW 1 PASI-E EPA 8260D JJK 63 PASI-C SM 5310B-2014 MJP 1 PASI-A SM 2540C-2015 AED 1 PASI-E SM 2540D-2015 WE 1 PASI-E SM 521 OB-2016 DAW 1 PASI E Colilert-18 WE 1 PASI E TKN+NO3+NO2 Calculation KDF1 1 PASI-A EPA 300 0 Rev 2 1 1993 JCM 1 PASI-A EPA 350 1 Rev 2 0 1993 NCF 1 PASI-A EPA 351 2 Rev 2 0 1993 MFO 1 PASI-A EPA 353 2 Rev 2 0 1993 NCF 1 PASI A EPA 365 1 Rev 2 0 1993 Zip 1 PASI-A REPORT OF LABORATORY ANALYSIS This report sha I not be reproduced except n full w,thout the written consent of Pace Analytical Services LLC Page 3 of 34 ( I ace ANALYTICAL RESULTS 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Project Piedmont Custom Meats- Oct Pace Project No.: 92695435 Sample: MW-1 Lab ID: 92695435001 Collected: 10/26/23 12:00 Received. 10126/23 14 10 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden Total Dissolved Solids 358 mg/L 50.0 1 10/31/23 09 01 350.1 Ammonia EDN Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Anaiytical Services - Eden Nitrogen Ammonia NO mg/L 0.10 1 11 /03/23 11,33 7664-41-7 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2015 Preparation Method SM 9222D-2015 Pace Analytical Services - Eden Fecal Col -forms; NO CFU/100 mL 1.0 1 10/26/23 19 57 10/27/23 18 02 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone NO ug/L 25.0 1 10/31/23 23:15 67-64-1 Benzene NO ug/L 1.0 1 10/31/23 23:15 71-43-2 Bromobenzene NO ug/L 1.0 1 10/31/23 23:15 108-86-1 Bromochloromethane NO ug/L 1.0 1 10/31/23 23:15 74-97-5 Bromodichloromethane NO ug/L 1.0 1 10/31/23 23:15 75-27-4 Bromoform NO ug/L 1.0 1 10/31/23 23:15 75-25-2 Bromomethane NO ug/L 2.0 1 10/31/23 23:15 74-83-9 IH 2-Butanone (MEK) NO ug/L 5.0 1 10/31/23 23:15 78-93-3 Carbon tetrachloride NO ug/L 1.0 1 10/31/23 23:15 56-23-5 Chlorobenzene NO ug/L 1.0 1 10/31/23 23:15 108-90-7 Chloroethane NO ug/L 1.0 1 10/31/23 23:15 75-00-3 Chloroform NO ug/L 1.0 1 10/31/23 23:15 67-66-3 Chloromethane NO ug/L 1.0 1 10/31/23 23:15 74-87-3 v2 2-Chlorotoluene NO ug/L 1.0 1 10/31/23 23:15 9549-8 4-Chlorotoluene NO ug/L 1.0 1 10/31/23 23:15 106-434 1,2-Dibromo-3-chloropropane NO ug/L 2.0 1 10/31/23 23:15 96-12-8 Dibromochloromethane ND ug/L 1.0 1 10/31/23 23:15 12448-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 10/31/23 23:15 106-93-4 Dibromomethane NO ug/L 1.0 1 10/31/23 23:15 74-95-3 1,2-Dichlorobenzene NO ug1L 1.0 1 10131/23 23:15 95-50-1 1,3-Dichlorobenzene NO ug/L 1.0 1 10/31/23 23:15 541-73-1 1,4-Dichlorobenzene NO ug/L 1.0 1 10/31123 23:15 106-46-7 Dichlorodifluoromethane NO ug/L 1.0 1 10/31/23 23:15 75-71-8 1,1-Dichloroethane NO ug/L 1.0 1 10/31/23 23:15 75-34-3 1,2-Dichloroethane NO ug/L 1.0 1 10/31/23 23:15 107-06-2 1,1-Dichloroethene NO ug/L 1.0 1 10/31/23 23:15 75-35-4 cis-1,2-Dichloroethene NO ug/L 1.0 1 10/31/23 23:15 156-59-2 trans-1,2-Dichloroethene NO ug/L 1.0 1 10/31/2323:15 156-60-5 1,2-Dichloropropane NO ug/L 1.0 1 10/31/23 23:15 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 10/31/23 23:15 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 10/31/23 23:15 594-20-7 1,1-Dichloropropene NO ug/L 1.0 1 10/31/23 23.15 563-58-6 cis- 1,3- Dichloropropene NO ug/L 1.0 1 10/31/23 23.15 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date 1111012023 03 20 PM without the written consent of Pace Analytical Services, LLC Page 4 of 34 ,�ace ANALYTICAL RESULTS 1377 South Park Drive Kernersville, NO 27284 (704)977-0981 Project: Piedmont Custom Meats Oct Pace Project No 92695435 Sample: MW-1 Lab ID: 92695435001 Collected: 10126/23 12 00 Received 10/26/23 14 10 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No Qual 8260D MSV Low Level Analytical Method EPA 8260D Pace Analytical Services - Charlotte trans-1 3-Dichloropropene ND ug/L 1.0 1 10/31/23 23:15 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 10/31/23 23:15 108-20-3 Ethylbenzene ND ug/L 1.0 1 10/31/23 23:15 100-41-4 Hexachloro-1 3-butadiene ND ug/L 2.0 1 10/31/23 23:15 87-68-3 2-Hexanone ND ug/L 5 0 1 10/31/23 23:15 591-78-6 p4sopropyltoluene ND ug/L 1 0 1 10/31/23 23:15 99-87-6 Methylene Chloride ND ug/L 5 0 1 10/31/23 23:15 75-09-2 4-Methyl-2-pentanone (MIRK) ND ug/L 5.0 1 10/31/23 23:15 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 10/31/23 23:15 1634-04-4 Naphthalene ND ug/L 1.0 1 10/31/23 23:15 91-20-3 Styrene ND ug1L 1.0 1 10/31/23 23:15 100-42-5 1.1,1,2-Tetrachloroethane ND u911. 1.0 1 10/31/23 23:15 630-20-6 1.1 2,2-Tetrachloroethane ND ug/L 1.0 1 10/31/23 23:15 79-34-5 Tetrach,oroethene ND ug/L 1.0 1 10/31/23 23:15 127-18-4 Toluene ND ug/L 1.0 1 10/31/23 23:15 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1 0 1 10/31/23 23:15 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 10/31/23 23:15 120-82-1 1, 1, 1 -Trichloroethane ND ug!L 1.0 1 10/31/23 23:15 71-55-6 1,1,2-Trichloroethane ND ug/L 10 1 10/31/23 23:15 79-00-5 Trichloroethene ND ug/L 1.0 1 10/31/23 23:15 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 10/31/23 23:15 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 10/31/23 23:15 96-18-4 Vinyl acetate ND ug/L 2.0 1 10/31/23 23:15 108-05-4 Vinyl chloride ND ug/L 1.0 1 10/31/23 23:15 75-01-4 Xylene (Total) ND ug/L 1.0 1 10/31/23 23:15 1330-20-7 m&p-Xylene ND ug/L 2.0 1 10/31/23 23:15 179601-23-1 o-Xylene ND ug/L 1.0 1 10/31/23 23:15 9547-6 Surrogates 4-Bromofluorobenzene(S) 93 % 70-130 1 10/31/23 23:15 460-004 1,2-Dichloroethane-d4 (S) 93 % 70-130 1 10131/2323:15 17060-07-0 Toluene-d8 (S) 95 % 70-130 1 10/31/23 23:15 2037-26-5 5310B TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon ND mg/L 1.0 1 10/31/23 08:53 7440-44-0 Date 11/10/2023 03 20 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced except in full, without the written consent of Pace Analytical Services. LLC Page 5 of 34 ii`�ace ANALYTICAL RESULTS Project: Piedmont Custom Meats- Oct Pace Project No.: 92695435 , .,. 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Sample: MW4 Parameters Lab ID: 92695435002 Collected: 10/26/23 13:10 Results Units Report Limit OF Received: 10126/23 14:10 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden Total Dissolved Solids 570 mg/L 125 1 10/31/23 09:01 350.1 Ammonia EDN Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Ammonia NO mg/L 0.10 1 11/03/2311:35 7664-41-7 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Eden Fecal Coliforms ND CFU/100 mL 1.0 1 10/26/23 19:57 10/27/23 18:02 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 1 10/31/23 23:34 67-64-1 Benzene NO ug/L 1.0 1 10/31/23 23:34 71-43-2 Bromobenzene NO ug/L 1.0 1 10/31/23 23:34 108-86-1 Bromochloromethane NO ug/L 1.0 1 10/31/23 23:34 74-97-5 Bromodichloromethane NO ug1L 1.0 1 10/31/23 23:34 75-27-4 Bromoform NO ug/L 1.0 1 10/31/23 23:34 75-25-2 Bromomethane NO ug/L 2 0 1 10/31123 23:34 74-83-9 IH 2-Butanone (MEK) NO ug/L 5.0 1 10/31/23 23 34 78-93 3 Carbon tetrachloride NO ug/L 1.0 1 10/31/23 23 34 56-23-5 Chlorobenzene NO ug/L 1.0 1 10/31/23 23 34 108-90-7 Chloroethane NO ug/L 1.0 1 10/31/23 23 34 75-00-3 Chloroform NO ug/L 1.0 1 10/31/23 23 34 67-66-3 Chloromethane ND ug/L 1 0 1 10/31/23 23 34 74-87-3 v2 2-Chlorotoluene NO ug/L 1.0 1 10/31/23 23 34 95-49-8 4-Chlorotoluene NO ug/L 10 1 10/31/23 23 34 10643-4 1,2-Dibromo-3-chloropropane ND ug/L 2 0 1 10/31/23 23 34 96-12-8 Dibromochloromethane NO ug/L 1 0 1 10/31/23 23 34 12448-1 1,2-Dibromoethane (EDB) NO ug/L 1 0 1 10/31/23 23 34 106-93-4 Dibromomethane NO ug/L 1.0 1 10/31/23 23.34 74-95-3 1,2-Dichlorobenzene NO ug1L 1.0 1 10/31/23 23.34 95-50-1 1,3-Dichlorobenzene NO ug/L 1.0 1 10/31/23 23 34 541-73-1 1,4-Dichlorobenzene NO ug/L 1.0 1 10/31/23 23 34 106-46-7 Dichlorodifluoromethane NO ug/L 1.0 1 10/31/23 23 34 75-71-8 1, 1 -Dichloroethane NO ug/L 1.0 1 10/31/23 23 34 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 10/31/23 23 34 107-06-2 1, 1 -Dichloroethene NO ug/L 1.0 1 10/31/23 23 34 75-35-4 cis-1,2-Dichloroethene NO ug/L 1.0 1 10/31/23 23 34 156-59-2 trans- l,2-Dichloroethene ND ug1L 1.0 1 10/31/23 23:34 156-60-5 1,2-Dichloropropane NO ug/L 1.0 1 10131/2323:34 78-87 5 1,3-Dichloropropane NO ug/L 1.0 1 10/31/23 23:34 142 28 9 2,2-Dichloropropane NO ug/L 1.0 1 10/31/23 23:34 594 20 7 1,1-Dichloropropene NO ug/L 1.0 1 10/31/23 23:34 563-58-6 cis- 1, 3-Dichloropropene NO ug/L 1.0 1 10/31/23 23:34 10061-01-5 REPORT OF LABORATORY ANALYSIS This report sha' not be reproduced, except in fu.l Date: 11 /10/2023 03.20 PM without the written consent of Pace Ana ytical Sery ces LLC Page 6 of 34 (--P'ace ANALYTICAL RESULTS Project Piedmont Custom Meats- Oct Pace Project No.: 92695435 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Sample: MWat Parameters Lab ID: 92695435002 Results Units Collected- 10/26/23 13,10 Report Limit DF Received Prepared 10/26/23 14 10 Analyzed Matrix Water CAS No Qual 8260D MSV Low Level trans-1, 3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1, 3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (Ml8K) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1.2 Tetrachloroethane 1,1, 2.2-Tetrachloroethane Tetrachloroethene Toluene 1, 2, 3-Trich lorobenzene 1.2.4-Trichlorobenzene 1 1.1-Trichloroethane 1 1 2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 5310B TOC Total Organic Carbon Date: 11/10/2023 03 20 PM Analytical Method EPA 8260D Pace Analyt-cai Services - Charlotte ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L NO ug/L NO ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L NO ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 101 % 89 % 100 % Analytical Method: SM 531OB-2014 Pace Analytical Services -Asheville ND mg/L 1.0 1 10/31/23 23 34 10061-02-6 1.0 1 10/31/23 23 34 108-20-3 1.0 1 10/31/23 23 34 100-41-4 2.0 1 10/31/23 23 34 87-68-3 5.0 1 10/31/23 23.34 591-78-6 1.0 1 10/31/23 2134 99-87-6 5.0 1 10/31/23 23:34 75-09-2 5.0 1 10/31/23 23:34 108-10-1 1.0 1 10/31/23 23 34 1634 04.4 1.0 1 10/31/23 23 34 91 203 1.0 1 10131 /23 23 34 100-42 5 1.0 1 10/31/23 23 34 630-20-6 1.0 1 10131 /23 23 34 79-34-5 1.0 1 10/31/23 23.34 127-18-4 1.0 1 10/31/23 23 34 108-88-3 1.0 1 10/31/23 23 34 87-61-6 1.0 1 10/31/23 23 34 120-82-1 1.0 1 10/31/23 23 34 71-55-6 1.0 1 10/31/23 23 34 79-00-5 1.0 1 10/31/23 23:34 79-01-6 1.0 1 10/31/23 23:34 75-69-4 1.0 1 10/31/23 23:34 96-18-4 2.0 1 10/31/23 23:34 108-05-4 1.0 1 10/31/23 23:34 75-01-4 1.0 1 10131 /23 23:34 1330-20-7 2.0 1 10131 /23 23:34 179601-23-1 1.0 1 10/31/23 23:34 95-47-6 70-130 1 10/31/23 23:34 460-00-4 70-130 1 10/31/23 23:34 17060-07-0 70-130 1 10/31/23 23:34 2037-26-5 1.0 1 10/31/23 09:13 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full withc,.t the written consent of Pace Analytical Services LLC Page 7 of 34 1377 South Park Drive Kernersville. NC 27284 (704)977-0981 ANALYTICAL RESULTS Project Piedmont Custom Meats- Oct Pace Project No 92695435 Sample: MW-5 Lab ID: 92695435003 Collected 10/26/23 12.40 Received 10/26/23 14:10 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services - Eden Total Dissolved Solids 1860 mg/L 250 1 10/31/23 09 01 350.1 Ammonia EDN Analytical Method: EPA 350 1 Rev 2 0 1993 Pace Ana yticaI Services - Eden Nitrogen Ammonia ND mg/L 010 1 11/03/23 11 36 7664-41-7 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2015 Preparation Method SM 9222D-2015 Pace Analytical Services - Eden Fecal Coliforms ND CFU/100 mL 1 0 1 10/26/23 19 57 10/27/23 18 02 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone NO ug/L 250 1 10/31/23 23:52 67-64-1 Benzene NO ug/L 1.0 1 10/31/23 23:52 71-43-2 Bromobenzene NO ug/L 1.0 1 10/31/23 23:52 108-86-1 Bromochloromethane NO ug1L 1 0 1 10/31/23 23:52 74-97-5 Bromodichloromethane NO ug/L 1 0 1 10/31/23 23:52 75-27-4 Bromoform NO ug/L 1.0 1 10/31/23 23:52 75-25-2 Bromomethane ND ug/L 2.0 1 10/31/23 23:52 74-83-9 Ili 2-Butanone (MEK) ND ug/L 50 1 10/31/23 23:52 78-93-3 Carbon tetrachloride ND ug/L 1 0 1 10/31/23 23:52 56-23-5 Chlorobenzene ND ug/L 1 0 1 10/31/23 23:52 108-90-7 Chloroethane ND ug/L 1 0 1 10/31/23 23:52 75-00-3 Chloroform ND ug/L 1 0 1 10/31/23 23,52 67-66-3 Chloromethane ND ug/L 1 0 1 10/31/23 23:52 74-87-3 v2 2-Chlorotoluene NO ug/L 1 0 1 10/31/23 23:52 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 10/31/23 23:52 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 10/31/23 23:52 96-12-8 Dibromochloromethane ND ug/L 1 0 1 10/31/23 23:52 124-48-1 1,2-Dibromoethane (EDB) NO ug/L 1 0 1 10/31/23 23:52 106-934 Dibromomethane ND ug/L 1 0 1 10/31/23 23:52 74-95-3 1,2-Dichlorobenzene NO ug/L 1 0 1 10/31/23 23:52 95-50-1 1,3-Dichlorobenzene NO ug/L 1.0 1 10/31/23 23:52 541-73-1 1,4-Dichlorobenzene ND ug/L 10 1 10/31/23 23:52 106-46-7 Dichlorodifluoromethane ND ug/L 1 0 1 10/31/23 23:52 75-71-8 1,1-Dichloroethane ND ug/L 1 0 1 10/31/23 23:52 75-34-3 1,2-Dichloroethane ND ug/L 1 0 1 10/31/23 23:52 107-06-2 1,1-Dichloroethene ND ug1L 1 0 1 10/31/23 23:52 75-35-4 cis- 1, 2-Dichloroethene, ND ug/L 1 0 1 10/31/23 23:52 156-59-2 trans- 1,2-Dichloroethene NO ug/L 10 1 10/31/23 23:52 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 10/31/23 23:52 78-87-5 1,3-Dichloropropane ND ug/L 1 0 1 10/31/23 23:52 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 10/31/23 23:52 594-20-7 1,1-Dichloropropene NO ug/L 1 0 1 10/31123 23:52 563-58-6 cis-1,3-Dichloropropene NO ug/L 1.0 1 10/31/23 23:52 10061-01-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced except n full Date 11 /10/2023 03 20 PM without the written consent of Pace Analytical Services LLC Page 8 of 34 (--flace ANALYTICAL RESULTS Project- Piedmont Custom Meats- Oct Pace Project No 92695435 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Sample: MW-5 Lab ID: 92695435003 Coilected: 10/26/23 12 40 Received 10/26/23 14 10 Matrix. Water Parameters Results Un is Report Limit DF Prepared Analyzed CAS No Qual 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte trans-1,3-D chloropropene NO ug/L 1.0 1 10/31/23 23:52 10061 026 Diisopropyl ether NO ug/L 1.0 1 10/31/23 23:52 108-20-3 Ethylbenzene NO ug/L 1.0 1 10/31/23 23 52 100-41-4 Hexachloro-1 3 butadiene NO ug/L 2.0 1 10/31/23 23 52 87-68-3 2-Hexanone NO ug/L 5.0 1 10/31/23 23.52 591-78-6 p-Isopropyltoluene NO ug/L 1.0 1 10/31/23 23 52 99-87-6 Methylene Chloride NO ug/L 5.0 1 10/31/23 23 52 75-09-2 4 Methyl-2-pentanone (MIRK) NO ug/L 5.0 1 10/31/23 23 52 108-10-1 Methyl-tert-butyl ether NO ug/L 1.0 1 10/31/23 23 52 1634-04-4 Naphthalene NO ug/L 1.0 1 10/31/23 23 52 91-20-3 Styrene NO ug/L 1.0 1 10/31/23 23 52 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 10/31123 23 52 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 10 1 10/31123 23 52 79-34-5 Tetrachloroethene NO ug/L 1.0 1 10/31/23 23 52 127-18-4 Toluene NO ug/L 1.0 1 10/31/23 23 52 108-88-3 1,2.3-Trichlorobenzene NO ug1L 1.0 1 10/31/23 23.52 87-61-6 1,2.4-Trichlorobenzene NO ug/L 1.0 1 10/31/23 23:52 120-82-1 1 1 1-Trichloroethane NO ug/L 1.0 1 10/31/23 23:52 71-55-6 1 1 2-Trichloroethane ND ug/L 1.0 1 10/31/23 23:52 79-00-5 Trichloroethene ND ug/L 1.0 1 10/31/23 23:52 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 10/31/23 23:52 75-69-4 1,2,3-Trichloropropane NO ug/L 1.0 1 10/31/23 23.52 96-18-4 Vinyl acetate ND ug/L 2.0 1 10/31/23 23:52 108-05-4 Vinyl chloride NO ug/L 1.0 1 10/31/23 23 52 75-01-4 Xylene (Total) NO ug/L 1.0 1 10/31/23 23 52 1330-20-7 m&p-Xylene NO ug/L 2.0 1 10/31123 23 52 179601-23-1 o-Xylene NO ug/L 1.0 1 10/31/23 23:52 95-47 6 Surrogates 4-Bromofluorobenzene (S) 95 °% 70 130 1 10/31/23 23:52 460-00-4 1,2-Dichloroethane-d4 (S) 93 % 70 130 1 10/31/23 23.52 17060-07-0 Toluene-d8 (S) 96 % 70 130 1 10/31/23 23:52 2037-26-5 5310B TOC Analytical Method. SM 53106-2014 Pace Analytical Services - Asheville Total Organic Carbon NO mg/L 1.0 1 10/31/23 09:33 7440 44-0 Date 11/1012023 03 20 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full without the written consent of Pace Analytical Services LLC Page 9 of 34 (J'ace ANALYTICAL RESULTS 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Project: Piedmont Custom Meats- Oct Pace Project No.: 92695435 Sample: Effluent Lab ID: 92695435004 Collected: 10/26/23 12:15 Received: 10/26/23 14:10 Matrix: Water Parameters 2540C Total Dissolved Solids Total Dissolved Solids 2540D Total Suspended Solids Total Suspended Solids 5210E BOD, 5 day EDN BOD, 5 day Colilert-18 Fecal Coliform EDN Fecal Coliforms Total Nitrogen Calculation Total Nitrogen 300.0 IC Anions 28 Days Chloride 350.1 Ammonia Nitrogen, Ammonia 351.2 Total KJeldahl Nitrogen Nitrogen, Kjeldahl, Total 353.2 Nitrogen, N021NO3 pres. Nitrogen, NO2 plus NO3 365.1 Phosphorus, Total Phosphorus Date 11/10/2023 03 20 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden 640 mg/L 250 1 10131/23 09:02 Analytical Method: SM 2540D-2015 Pace Analytical Services - Eden 1550 mg/L 167 1 10130/2311:07 Analytical Method: SM 52106-2016 Preparation Method: SM 52106-2016 Pace Analytical Services - Eden 581 mg/L 2.0 1 10/2712311:08 11101/2316:23 B1 Analytical Method: Colilert-18 Preparation Method: Colilert-18 Pace Analytical Services - Eden 2420 MPN1100ml- 1.0 1 10/2612318:15 1012712312:35 D6,E1 Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services - Asheville 182 mg/L 0.040 1 11/09/23 08:43 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville 131 mg/L 5.0 5 10/28/23 22:43 16887-00-6 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 54.5 mg/L 1.0 10 11/04/23 05:24 7664-41-7 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 166 mg/L 5.0 1 11/08/23 14:28 11/09/23 06:18 7727-37-9 Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 16.6 mg/L 0.40 10 11 /08123 05:24 Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services - Asheville 18.5 mg/L 0.25 5 11/08/2318:58 11109/2311:36 7723-14-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full without the written consent of Pace Analytical Services, LLC Page 10 of 34 ��ace QUALITY CONTROL DATA Project Piedmont Custom Meats- Oct Pace Project No 92695435 QC Batch: 809891 Analysis Method SM 2540C-2015 QC Batch Method: SM 254OC-2015 Analysis Description. 2540C Total Dissolved Solids Laboratory Pace Analyt cal Services - Eden Associated Lab Samples 92695435001, 92695435002 92695435003 92695435004 METHOD BLANK 4193114 Matrix Water Associated Lab Samples. 92695435001, 92695435002, 92695435003, 92695435004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L ND 25.0 10/31/23 08:59 LABORATORY CONTROL SAMPLE 4193115 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg/L 250 250 100 90-110 SAMPLE DUPLICATE- 4193116 92695131001 Dup Parameter Units Result Result Total Dissolved Solids mg/L 2530 2640 SAMPLE DUPLICATE: 4193117 92695133001 Dup Parameter Units Result Result Total Dissolved Solids mg/L 2500 2510 RPD Qualifiers 4 RPD Qualifiers 0 1377 South Park Drive Kernersville, NC 27284 (704)977.0981 Results presented on th-s page are in the un is .ndicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced except in full Date 11 /10/2023 03.20 PM without the written consent of Pace Analytical Services LLC Page 11 of 34 ,�ace QUALITY CONTROL DATA Project Piedmont Custom Meats- Oct Pace Project No 92695435 QC Batch 809306 Analysis Method: SM 254OD-2015 QC Batch Method SM 2540D-2015 Analysis Description: 25400 Total Suspended Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples. 92695435004 METHOD BLANK 4190717 MatrixWater Associated Lab Samples 92695435004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 10/30/23 11:00 LABORATORY CONTROL SAMPLE 4190718 Spike LCS LCS % Rec. Parameter Units Conc Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 234 94 90-110 SAMPLE DUPLICATE 4190719 92695446003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 1250 1330 6 SAMPLE DUPLICATE 4190720 92695446001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 82A 743 10 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Results presented on this page are In the units Ind cated by the "Units" co umn except where an a ternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced except in ful Date 11/10/2023 03.20 PM without the written consent of Pace Analytical Services, . LC Page 12 of 34 ��ace QUALITY CONTROL DATA Pro)ect Piedmont Custom Meats- Oct Pace Project No.: 92695435 QC Batch 810819 Analysis Method EPA 350.1 Rev 2 0 1993 QC Batch Method. EPA 350 1 Rev 2.0 1993 Analysis Description 350.1 Ammonia, EDN Laboratory Pace Analytical Services - Eden Associated Lab Samples 92695435001, 92695435002. 92695435003 METHOD BLANK 4197792 Matrix Water Associated Lab Samples 92695435001, 92695435002 92695435003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 11/03/23 11:05 LABORATORY CONTROL SAMPLE 4197793 Spike LCS LCS % Rec Parameter Units Conc Result % Rec Limits Qualifiers Nitrogen, Ammonia mg1L 5 4.9 98 90-110 1377 South Park Drive Kernersville. NC 27284 (704)977-0981 MATRIX SPIKE & MATRIX SPIKE DUPLICATE. 4197794 4197795 MS MSD 92696439003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen Ammonia mg/L ND 5 5 5-3 5-4 105 106 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE 4197796 4197797 MS MSD 92696439002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc; Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg1L 0.18 5 5 5.4 53 104 103 90-110 1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in ful', Date 11 /10/2023 03.20 PM without the written consent of Pace Analytical Services, LLC Page 13 of 34 -Pace Project Piedmont Custom Meats- Oct Pace Project No 92695435 QC Batch 809308 QC Batch Method SM 52108-2016 Associated Lab Samples: 92695435004 METHOD BLANK 4190732 ' Associated Lab Samples. 92695435004 Parameter Units BOD, 5 day mg/L QUALITY CONTROL DATA Analysis Method: SM 521 OB-2016 Analysis Description 5210B BOD, 5 day Final EDN Laboratory: Pace Analytical Services Eden Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 11/01/23 13 45 LABORATORY CONTROL SAMPLE. 4190733 Spike LCS Parameter Units Cone. Result BOD. 5 day mg/L 198 199 SAMPLE DUPLICATE: 4190735 92695281002 Dup Parameter Units Result Result BOD, 5 day mg/L 135 169 LCS % Rec % Rec Limits Qualifiers 101 84.6-115 RPD Qualifiers 23 R6 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /10/2023 03:20 PM without the written consent of Pace Analytical Services LLC Page 14 of 34 -Pace QUALITY CONTROL DATA Project P edmont Custom Meats- Oct Pace Project No.. 92695435 QC Batch 809516 Analysis Method: QC Batch Method SM 9222D-2015 Analysis Description Laboratory: Associated Lab Samples 92695435001, 92695435002, 92695435003 METHOD BLANK 4191635 Matrix Water Associated Lab Samples: 92695435001, 92695435002, 92695435003 SM 9222D-2015 9222D Fecal Coliform(MF)-EDN Pace Analytical Services - Eden Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Conforms CFU/100 mL ND 1.0 10/27/23 18,02 METHOD BLANK 4191637 Matrix Water Associated Lab Samples 92695435001. 92695435002, 92695435003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 10/27/23 18:02 SAMPLE DUPLICATE: 4191636 Parameter Fecal Coliforms 92695435002 Dup Units Result Result RPD Qualifiers CFU/100 mL ND ND 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Results presented on th s page are In the units indicated by the "Un is" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS Th s report shall not be reproduced, except n full Date 11 /10/2023 03 20 PM without the written consent of Pace Aralytical Services, LLC Page 15 of 34 ��ace Project Piedmont Custom Meals Oct Pace Project No 92695435 QC Batch 809212 QC Batch Method: Colilert-18 Associated Lab Samples: 92695435004 SAMPLE DUPLICATE: 4190407 ^ Parameter Units Fecal Coliforms MPN1100mL QUALITY CONTROL DATA Analysis Method Colilert-18 Analysis Description Colilert-18 Fecal Coliform EDN Laboratory Pace Analyt cal Services - Eden 92695427003 Dup Result Result RPD Qualifiers 2.0 1.0 67 D6 1377 South Park Dnve Kernersville, NC 27284 (704)977-0981 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS Th s report shall not be reproduced except in full, Date: 11 /10/2023 03:20 PM without the written consent of Pace A-alytical Services, LLC Page 16 of 34 (--Pa'ce QUALITY CONTROL DATA Project: Piedmont Custom Meats- Oct Pace Project No.: 92695435 QC Batch: 810062 Analysis Method EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Laboratory- PaceAnalytcalServices- Charlotte Associated Lab Samples: 92695435001, 92695435002, 92695435003 METHOD BLANK: 4194117 Matrix: Water Associated Lab Samples: 92695435001, 92695435002 92695435003 Blank Reporting Parameter Units Result Limit Analyzed 1,1,1.2-Tetrachloroethane ug/L NO 1 0 10/31/23 14 29 1,1,1-Trichloroethane ug/L NO 1 0 10/31/23 14 29 1,1,2 2-Tetrachloroethane ug/L NO 10 10/31/23 14 29 1,1,2-Trichloroethane ug/L NO 1 0 10/31/23 14 29 1, 1 -Dichloroethane ug/L NO 1.0 10/31/23 14 29 1. 1 -Dichloroethene ug1L ND 1.0 10/31/2314.29 11-Dichloropropene ug/L ND 1.0 10/31/2314:29 1 2.3-Trichlorobenzene ug/L ND 1.0 10/31/23 14 29 1 2.3-Trichloropropane ug/L NO 1.0 10/31/23 14 29 1.2,4 Trichlorobenzene ug/L NO 1.0 10/31/23 14 29 1,2 Dibromo-3-chloropropane ug/L NO 2.0 10/31/23 14 29 1,2 D bromoethane (EDB) ug/L NO 1.0 10/31/23 14 29 1, 2 • D chlorobenzene ug/L NO 1.0 10131 /23 14 29 1,2-Dichloroethane ug/L ND 1.0 10/31/23 14 29 1,2-Dichloropropane ug/L NO 1.0 10/31/23 14 29 1,3-Dichlorobenzene ug/L NO 1 0 10/31/23 14:29 1,3-Dichloropropane ug/L NO 1 0 10131 /23 14.29 1,4-Dichlorobenzene ug/L NO 1 0 10/31/23 14:29 2,2-Dichloropropane ug/L NO 1.0 10/31/23 14:29 2-Butanone (MEK) ug/L NO 50 10/31/23 14:29 2-Chlorotoluene ug/L ND 1.0 10/3112314:29 2-Hexanone ug1L ND 5.0 10/31/23 14:29 4-Chlorotoluene ug/L ND 1.0 10/31/23 14:29 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 10/31/23 14:29 Acetone ug/L ND 25.0 10/31/23 14:29 Benzene ug/L NO 1.0 10/31/23 14:29 Bromobenzene ug/L NO 1.0 10/31/23 14:29 Bromoch loromethane ug/L NO 1.0 10/31/23 14:29 Bromodichloromethane ug/L ND 1.0 10131/2314:29 Bromoform ug/L ND 1.0 10/3112314:29 Bromomethane ug/L NO 2.0 10/31/23 14:29 Carbon tetrachloride ug/L NO 1.0 10/31/23 14:29 Chlorobenzene ug/L NO 1.0 10/31/23 14:29 Chloroethane ug/L NO 1.0 10/31/23 14:29 Chloroform ug/L ND 1.0 10/3112314:29 Chloromethane ug/L ND 1.0 10131/2314:29 cis-1,2-Dich loroethene ug/L NO 1.0 10131/23 14:29 cis-1,3-Dichloropropene ug/L NO 1.0 10/31/23 14:29 Dibromochloromethane ug/L NO 1.0 10/31/23 14:29 Dibromomethane ug/L NO 1.0 10/31/23 14:29 iH v2 Qualifiers 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced except in full. Date 11 /10/2023 03 20 PM without the written consent of Pace Analytical Services, LLC Page 17 of 34 (--Place QUALITY CONTROL DATA Project: Piedmont Custom Meats- Oct Pace Project No: 92695435 METHOD BLANK: 4194117 Matrix: Associated Lab Samples: 92695435001, 92695435002 92695435003 Blank Parameter Units Result Water Reporting Limit Analyzed Dichlorodifluoromethane ug/L ND 1.0 10/31/23 14 29 Diisopropyl ether ug1L ND 1.0 10/31/23 14 29 Ethylbenzene ug/L ND 1.0 10/31/23 14 29 Hexachloro-1 3-butadiene ug/L ND 2.0 10/31/23 1429 m&p-Xylene ug/L ND 2.0 10/31/23 14 29 Methyl-tert-buty ether ug/L ND 1.0 10/31/23 1429 Methylene Chloride ug/L ND 5.0 10/31/23 14 29 Naphthalene ug1L ND 1.0 10131/2314.29 o-Xylene ug/L ND 1.0 10131/2314.29 p-Isopropyltoluene ug1L ND 1.0 10/31/23 14 29 Styrene ug/L NO 1.0 10/31/23 14 29 Tetrachloroethene ug/L ND 1.0 10/31/23 14 29 Toluene ug/L NO, 1.0 10/31/23 14 29 trans 1 2-Dichloroethene ug/L NO, 1.0 10/31/23 1429 trans-1 3-Dichloropropene ug/L ND 1.0 10/31/23 1429 Trichloroethene ug/L ND 1.0 10/31/23 1429 Trichlorofluoromethane ug/L ND 1.0 10/31/23 14 29 Mny acetate ug/L ND 2.0 10/31/23 14 29 Vinyl chloride ug/L ND 1.0 10/31/23 14 29 Xylene (Total) ug/L ND 1.0 10/31/23 14 29 1,2-Dichloroethane-d4 (S) eh 93 70-130 10/31123 14:29 4-Bromofluorobenzene (S) 0 107 70-130 10131/23 1429 Toluene-d8 (S) % 91 70-130 10/31/23 14,29 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 4194118 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1.11,2-Tetrachloroethane ug/L 20 19.5 98 70-130 1.1 A Trichloroethane ug/L 20 19.0 95 70-130 1.1.2,2-Tetrachloroethane ug/L 20 18.6 93 70-130 1.1,2-Trichloroethane ug/L 20 18.0 90 70-130 11-Dichloroethane ug/L 20 17.3 87 70-130 11-Dichloroethene ug/L 20 20.6 103 69-131 1,1-Dichloropropene ug/L 20 190 95 70-132 1,2,3-Trichlorobenzene ug/L 20 198 99 70-132 1,2,3.Trichloropropane ug/L 20 176 88 70-130 1,2,4-Trichlorobenzene ug/L 20 18.8 94 70-130 1,2-Dibromo-3-chloropropane ug/L 20 201 100 70-130 1,2-Dibromoethane (EDB) ug/L 20 192 96 70-130 1,2-Dichlorobenzene ug/L 20 192 96 70-130 1,2-Dichloroethane ug1L 20 16.8 84 70-130 1,2-Dichloropropane ug/l_ 20 176 88 70-130 1,3-Dichlorobenzene ug/L 20 18.7 93 70-130 1,3-Dichloropropane ug/L 20 17.6 88 70-130 Qualifiers 1377 South Park Drive Kernersville, NC 27284 (704)977.0981 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except n fu Date: 11 1012023 03:20 PM without the written consent of Pace Analytical Services LLC Page 18 of 34 (--Place QUALITY CONTROL DATA Project: Piedmont Custom Meats- Oct Pace Project No.. 92695435 LABORATORY CONTROL SAMPLE: 4194118 Spike LCS LCS % Rec Parameter Units Conc Result % Rec Limits Qualifiers 1,4-Dichlorobenzene ug/L 20 190 95 70-130 2.2-Dichloropropane ug/L 20 181 91 69-130 2-Butanone (MEK) ug/L 40 33.5 84 67-133 2 Chlorotoluene ug/L 20 17.4 87 70-130 2 Hexanone ug/L 40 33.8 84 70-133 4-Chlorotoluene ug/L 20 178 89 70-130 4-Methyl-2-pentanone (MIBK) ug/L 40 32.8 82 70-130 Acetone ug/L 40 356 89 67-130 Benzene ug/L 20 173 87 70-130 Bromobenzene ug/L 20 182 91 70-130 Bromochloromethane ug/L 20 191 95 70-130 Bromodichloromethane ug/L 20 167 83 70-130 Bromoform ug/L 20 19 2 96 70-133 Bromomethane ug/L 20 268 134 41-148 IH Carbon tetrachloride ug/L 20 185 92 70-130 Chlorobenzene ug/L 20 187 94 70-130 Chloroethane ug/L 20 214 107 41-157 Chloroform ug/L 20 18.9 95 70-130 Chloromethane ug/L 20 15.9 80 59-141 v3 cis-1,2-Dichloroethene ug/L 20 180 90 70-130 cis-1,3-Dichloropropene ug/L 20 17A 86 70130 Dibromochloromethane ug/L 20 %2 96 70130 Dibromomethane ug/L 20 18.8 94 70-130 Dichlorodifluoromethane ug/L 20 22.3 112 54-147 Diisopropyl ether ug/L 20 164 82 70-130 Ethylbenzene ug/L 20 183 92 70-130 Hexachloro-1,3-butadiene ug/L 20 198 99 70-134 m&p-Xylene ug/L 40 36 8 92 70-130 Methyl-tert-butyl ether ug/L 20 16.6 83 70-130 Methylene Chloride ug/L 20 18.2 91 62-130 Naphthalene ug/L 20 19.4 97 70-135 o-Xylene ug/L 20 18.3 92 70-130 p-IsopropylWuene ug/L 20 19.1 95 70-130 Styrene ug/L 20 18.9 95 70-130 Tetrachloroelhene ug/L 20 19.8 99 70-130 Toluene ug/L 20 181 90 70-130 trans- 1, 2-Dichloroethene ug,L 20 17.9 90 70-130 trans-1,3-Dich oropropene ug/L 20 17.6 88 70-130 Trichloroethene ug/L 20 18.6 93 70-130 Trichlo►ofluoromethane ug/L 20 21.4 107 57-130 Vinyl acetate ug/L 40 34.6 86 70 141 Vinyl ch'oride ug/L 20 16 8 84 fib 140 Xylene (Total) ug/L 60 55.1 92 70-130 1,2-Dichloroethane-d4 (S) % 91 70-130 4-Bromofluorobenzene (S) % 98 70 130 Toluene-d8 (S) % 94 70 130 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fu I. Dale 11 /10/2023 03:20 PM without the written consent of Pace Analytical Services LLC Page 19 of 34 (--Place QUALITY CONTROL DATA Project: Piedmont Custom Meats- Oct Pace Project No.: 92695435 MATRIX SPIKE SAMPLE: 4194119 1377 South Park Drive Kernersville NC 27284 (704)977-0981 92695827001 Spike MS MS % Rec Parameter Un is Result Conc. Result % Rec Limits Qualifiers 11.1,2-Tetrachloroethane ug/L ND 20 210 105 70-146 11,1•Trichloroethane ug/L ND 20 224 112 70-150 1,1,2.2-Tetrachloroethane ug/L ND 20 213 106 66-144 1,1,2 Trichloroethane ug/L ND 20 21.1 106 70 142 1,1•Dichloroethane ug/L NO 20 21.6 108 68-150 1. 1 -Dichloroethene ug/L ND 20 22.4 112 64-162 1, 1 -Dichloropropene ug/L ND 20 242 121 70-160 1,2.3-Trichlorobenzene ug/L ND 20 20.2 101 66-151 1,2.3-Tiichooropropane ug/L ND 20 20A 102 66-144 1, 2 4-Trichlorobenzene ug/L ND 20 20.3 101 69-147 1.2-Dibromo-3-chloropropane ug/L NO 20 19.9 100 62-146 1 2-Dibromoethane (EDB) ug/L ND 20 21.2 106 70-143 1 2-Dichlorobenzene ug/L ND 20 207 104 70-142 1,2-Dichloroethane ug/L NO 20 207 104 68-145 1,2-Dichloropropane ug/L NO 20 225 112 70-144 1,3-Dichlorobenzene ug/L ND 20 208 104 70-142 1,3-Dichloropropane ug/L NO 20 206 103 70-141 1,4-Dichlorobenzene ug/L ND 20 202 101 70-140 2,2-Dichloropropane ug/L NO 20 223 ill 58-160 2-Butanone (MEK) ug/L NO 40 41 8 105 57-156 2-Chlorotoluene ug/L NO 20 202 101 70-148 2-Hexanone ug/L NO 40 45.1 113 62-153 4-Chlorotoluene ug/L ND 20 20.5 103 70-144 4-Methyl-2-pentanone (MIRK) ug/L ND 40 43.8 110 65-144 Acetone ug/L ND 40 42.4 103 49-162 Benzene ug/L ND 20 21.8 109 68-144 Bromobenzene ug/L ND 20 20.3 102 70-144 Bromochloromethane ug/L ND 20 21.7 109 70-148 Bromodichloromethane ug/L NO 20 21.0 105 70-141 Bromoform ug/L ND 20 20.1 101 59-144 Bromomethane ug/L ND 20 18.5 92 23-190 v3 Carbon tetrachloride ug/L ND 20 22.5 113 70-147 Chiorobenzene ug/L ND 20 20.8 104 70-143 Chloroethane ug/L ND 20 22.3 ill 55-190 Chloroform ug/L ND 20 21.4 107 67-148 Chloromethane ug/L NO 20 23.0 115 38-180 cis-1,2-Dichloroethene ug/L ND 20 21.5 107 67-151 cis-1,3-Dichloropropene ug/L ND 20 20.9 104 70-142 Dibromochioromelhane ug/L ND 20 20.7 103 68-140 Dibromomethane ug/L ND 20 20.8 104 70-142 Dichlorodifluoromethane ug/L NO 20 29.5 147 15-200 IH vl Diisopropyl ether ug/L NO 20 20.9 105 62-149 Ethylbenzene ug1L 10 20 22.1 105 70-145 Hexachloro-1,3-butadiene ug/L ND 20 20.6 103 64-164 m&p-Xylene ugiL 4 4 40 47.2 107 70-148 Methyl -left -butyl ether ug/L NO 20 20.2 101 64-146 Methylene Chloride ug/L NO 20 21.4 107 54-149 Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date. 11 /10/2023 03 20 PM without the written consent of Pace Analytical Services, LLC Page 20 of 34 ,�ace QUALITY CONTROL DATA 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Project: Piedmont Custom Meats- Oct Pace Project No.: 92695435 MATRIX SPIKE SAMPLE: 4194119 92695827001 Spike MS MS % Rec Parameter Units Result Conc Result % Rec Limits Qualifiers Naphthalene ug/L NO 20 221 109 62-154 o-Xylene ug/L 24 20 236 106 70-145 p-Isopropyltoluene ug/L NO 20 206 103 70-153 Styrene ug/L NO 20 209 105 70-147 Tetrachloroethene ug/L NO 20 202 101 70-145 Toluene ug/L 3.8 20 25.8 110 65-146 trans- 1,2-Dichloroethene ug/L ND 20 22.4 112 69-155 trans-1,3-Dich oropropene ug/L ND 20 209 105 70-142 Trichloroethene ug/L NO 20 211 106 70-152 Trich orofluoromethane ug/L NO 20 236 118 60-158 Vinyl acetate ug/L NO 40 358 89 56-157 Vinyl chloride ug/L NO 20 21 3 106 51 178 Xylene (Total) ug/L 68 60 708 107 70-146 12-Dichloroethane-0 (S) % 100 70-130 4-Bromofluorobenzene (S) % 101 70-130 Toluene-d8(S) % 100 70-130 SAMPLE DUPLICATE: 4194120 Parameter Units 92695827002 Result Dup Result 1, 1, 1,2-Tetrachloroethane ug/L NO NO 1,1,1-Trichloroethane ug/L NO ND 1, 1,2,2-Tetrach loroethane ug/L NO ND 1,1,2-Trichloroethane ug/L NO ND 1,1-Dichloroethane ug/L NO ND 1,1-Dichloroethene ug/L NO NO 1,1-Dichloropropene ug/L NO NO 1,2,3-Trichlorobenzene ug/L NO NO 1,2,3-Trichooropropane ug/L NO NO 1,2,4-Trichlorobenzene ug/L ND NO 1,2-Dibromo-3-chloropropane ug/L ND NO 1,2-Dibromoethane (EDB) ug/L NO NO 1,2-Dichlorobenzene ug/L NO NO 1,2-Dichloroethane ug/L NO NO 1,2-Dichloropropane ug/L NO ND 1,3-Dichlorobenzene ug/L ND NO 1,3-Dichloropropane ug/L NO NO 1,4-Dichlorobenzene ug/L NO NO 2,2-Dichloropropane ug/L NO NO 2-Butanone (MEK) ug/L NO ND 2-Chlorotoluene ug/L NO NO 2-Hexanone ug/L ND NO 4-Chlorotoluene ug/L ND NO 4-Methyl-2-pentanone (MIRK) ug/L ND NO Acetone ug/L NO NO RPD Qualifiers Results presented on this page are In the units indicated by the 'Units" column except where an alternate unit Is presented to the right or the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date 11110f2023 03 20 PM without the written consent of Pace Analytical Services, LLC Page 21 of 34 ��ace QUALITY CONTROL DATA Project: Piedmont Custom Meats- Oct Pace Project No 92695435 SAMPLE DUPLICATE 4194120 Parameter Units 92695827002 Result Dup Result Benzene ug/L ND ND Bromobenzene ug/L ND ND Bromochloromethane ug/L ND ND Bromodichloromethane ug/L ND ND Bromoform ug/L ND ND Bromomethane ug/L ND ND Carbon tetrachloride ug/L NO ND Chlorobenzene ug/L ND ND Chloroethane ug/L ND NO Chloroform ug/L ND ND Chloromethane ug/L ND ND cis-1,2-Dichloroethene ug/L ND ND cis-1,3-Dichloropropene ug/L ND ND Dibromochloromethane ug/L ND ND Dibromomethane ug/L ND ND Dichlorodifluoromethane ug/L ND ND Diisopropyl ether ug/L ND ND Ethylbenzene ug/L ND 67J Hexachloro-13-butadiene ug/L NO ND m&p-Xylene ug/L 2 9 3 3 Methyl-tert-butyl ether ug/L ND NO Methylene Chloride ug/L ND NO Naphthalene ug/L ND ND o-Xylene ug/L ND 11 p-lsopropyltoluene ug/L ND ND Styrene ug/L ND ND Tetrachloroethene ug/L ND ND Toluene ug L ND 1 2 trans-1.2-Dich oroelhene ug1 ND ND trans-13-Dichloropropene ug/L ND ND Trichloroethene ug/L ND ND Trichlorofluoromethane ug/L NO ND Vinyl acetate ug/L NO ND Vinyl chloride ug/L ND NO Xylene (Total', ug/L 2 9 4 4 1,2-Dichloroethane-d4 (S) 94 99 4-Bromofluorobenzene (S) 95 100 Toluene-d8(S) 94 106 RPD Qualifiers 14 42 v2 1H v1 1377 South Park Drive Kernersvllle NC 27284 (704)977-0981 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced except in full Date 11/10/2023032OPM without the written consent of Pace Ana,ytcal Services LLC Page 22 of 34 (!�Flace QUALITY CONTROL DATA Project Piedmont Custom Meats- Oct Pace Project No.: 92695435 QC Batch 809562 Analys•s Method EPA 300.0 Rev 2.1 1993 QC Batch Method. EPA 300 0 Rev 2 1 1993 Analys s Description. 300.0 IC Anions Laboratory Pace Analytical Services Asheville Associated Lab Samples 92695435004 METHOD BLANK 4191818 Matrix Water Associated Lab Samples 92695435004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg/L ND 1.0 10/28/23 21.09 LABORATORY CONTROL SAMPLE: 4191819 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Chloride mg/L 50 52.0 104 90-110 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 MATRIX SPIKE & MATRIX SPIKE DUPLICATE 4191820 4191821 MS MSD 92695608005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L ND 50 50 54.9 55.5 109 110 90-110 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reprcduced except in full, Date: 11 /10/2023 03:20 PM without the written consent of Pace A•ialytical Services, LLC Page 23 of 34 ,-Pace Project Piedmont Custom Meats- Oct Pace Project No 92695435 QC Batch 811004 QC Batch Method EPA 350 1 Rev 2 0 1993 Assoc ated Lab Samples 92695435004 METHOD BLANK 4199181 Associated Lab Samples 92695435004 Parameter Units Nitrogen, Ammonia mg/L QUALITY CONTROL DATA Analysis Method EPA 350 1 Rev 2.0 1993 Analysis Description 350 1 Ammonia Laboratory Pace Analytical Services - Asheville Matrx: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.10 11/04/23 04 31 LABORATORY CONTROL SAMPLE. 4199182 Spike LCS LCS % Rec Parameter Units Conc Result % Rec Limits Qualifiers Nitrogen Ammonia mg/L 5 5 D 100 90-110 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 MATRIX SPIKE & MATRIX SPIKE DUPLICATE 4199183 4199184 MS MSD 92696579001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L <0.031 5 5 4.8 48 95 95 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE 4199185 4199186 MS MSD 92696579002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 0.97 5 5 58 58 96 96 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shay not be reproduced, except in full Date 11/10/2023 03 20 PM without the written ccnsent of PaceAna ytical Services. LI C Page 24 of 34 -Prate Project Piedmont Custom Meats- Oct Pace Project No 92695435 QC Batch 811781 QC Batch Method EPA 351 2 Rev 2.0 1993 Associated Lab Samples 92695435004 METHOD BLANK: 4202944 Associated Lab Samples 92695435004 Parameter Units Nitrogen Kjeldahl, Total mg1L LABORATORY CONTROL SAMPLE: 4202945 Parameter Units Nitrogen, Kjeldahl, Total mg/L QUALITY CONTROL DATA Analysis Method EPA 351.2 Rev 2.0 1993 Analysis Description 351 2 TKN Laboratory: Pace Analytical Services -Asheville Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0,50 11/09/23 05:55 Spike LCS Cone. Result 10 101 LCS % Rec % Rec Limits Qualifiers 101 90-110 1377 South Park Drive Kernersville NC 27284 (704)977-0981 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4202946 4202947 MS MSD 92695214007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Nitrogen, Kjeldahl, Total mg1L ND 10 10 106 105 105 105 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE 4202948 4202949 MS MSD 92695214008 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone Cone. Result Result % Rec % Rec Limits RPD Nitrogen, Kjeldahl, Total mg1L ND 10 10 106 11 4 102 109 90-110 7 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the r ght of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except .n full Date I V1012023 03 20 PM without the written consent of Pace Analytical Services I.LC Qual Qual Page 25 of 34 ��ace Project: Piedmont Custom Meats- Oct Pace Project No. 92695435 QC Batch: 811642 QC Batch Method EPA 353.2 Rev 2.0 1993 Associated Lab Samples 92695435004 METHOD BLANK 4202376 Associated Lab Samples. 92695435004 Parameter Units Nitrogen, NO2 plus NO3 mg/L LABORATORY CONTROL SAMPLE 4202377 Parameter Units Nitrogen, NO2 plus NO3 mg/L QUALITY CONTROL DATA Analysis Method EPA 353 2 Rev 2 0 1993 Analysis Description 353.2 Nitrate + Nitrite, preserved Laboratory Pace Analytical Services -Asheville Matrix Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.040 11/08/23 05 34 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 2.5 2.5 101 90-110 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 MATRIX SPIKE & MATRIX SPIKE DUPLICATE 4202378 4202379 MS MSD 92695393001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc, Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 270 2.5 2.5 29.9 25.6 115 -56 90-110 15 M1,R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE 4202380 4202381 MS MSD 92695405001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 020 2 5 2 5 27 2.7 100 100 90-110 0 Resu is presented on this page are in the units Indicated by the "Units" cc umn except where an alternate unit is presented to the right or the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fu I, Date 11/10/2023 03.20 PM without the written consent of Pace Analytical Services LLC Page 26 of 34 (-.-Pa'ce Project: Piedmont Custom Meats- Oct Pace Project No: 92695435 QC Batch: 811606 QC Batch Method. EPA 365 1 Rev 2.0 1993 Associated Lab Samples 92695435004 METHOD BLANK 4202168 Associated Lab Samples 92695435004 Parameter Units Phosphorus mg/L LABORATORY CONTROL SAMPLE 4202169 Parameter Units Phosphorus mg/L QUALITY CONTROL DATA Analysis Method EPA 365 1 Rev 2 0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory Pace Analyt cal Services - Asheville Matrix Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.050 11/09/23 10 23 Spike LCS LCS % Rec Conc Result % Rec Limits Qualifiers 2.5 2.5 101 90-110 1377 South Park Drive Kemersville, NC 27284 (704)977.0981 MATRIX SPIKE & MATRIX SPIKE DUPLICATE 4202588 4202589 MS MSD 92696199001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 050 2.5 2 5 3.2 3.1 106 104 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE 4202590 4202591 MS MSD 92696199002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.060 2.5 2 5 2 6 2.6 101 102 90-110 1 Results presented on this page are In the units Indlcated by the "Units- co umn except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced except in ful Date 11/10/2023 03 20 PM without the written consent of Pace Analytica Services, LLC Page 27 of 34 ��Oce QUALITY CONTROL DATA Project Piedmont Custom Meats- Oct Pace Project No 92695435 OC Batch: 809739 Analysis Method SM 531 OB-2014 QC Batch Method SM 531 OB-2014 Analysis Description 5310E TOC Laboratory. Pace Analytical Sery ces - Asheville Associated Lab Samples 92695435001, 92695435002. 92695435003 METHOD BLANK 4192368 Matra Water Associated Lab Samples 92695435001, 92695435002, 92695435003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L NO 1.0 10/31/23 01:28 LABORATORY CONTROL SAMPLE 4192369 Parameter Units Total Organic Carbon mg/L Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 25 23.4 94 90-110 1377 South Park Drive Kernersville, NC 27284 (704)977 0981 MATRIX SPIKE & MATRIX SPIKE DUPLICATE 4192370 4192371 MS MSD 92695045001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L 12.2 25 25 36.6 36.2 98 96 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE 4192372 4192373 MS MSD 92695045002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L ND 25 25 24.7 24.4 97 96 90-110 1 Results presented on this page are in the units Indicated by the "Units" column except where an alternate un t Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report sha.l not be reproduced, except in full, Date 1111012023 03 20 PM without the wr tten consent of Pace Analytical Services. LLC Page 28 of 34 ��ace Project Pace Project No. DEFINITIONS Piedmont Custom Meats- Oct 92695435 1377 South Park Drive Kernersville NC 27284 (704)977 0981 QUALIFIERS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilut on of the sample aliquot ND - Not Detected at or above adjusted reporting limit TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit PQL - Practical Quantitation Limit RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix S - Surrogate 1 2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270 The result for each analyte is a combined concentration. Consistent with EPAguidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U Indicates the compound was analyzed for but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 s recommended n SW846 Chapter 4 for the analysis of Acrolein and Acryiomtnle by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270 The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes TNI - The NELAC Institute. ANALYTE QUALIFIERS B1 Less than 1.0 mg/L DO remained for all dilutions set. The reported value is an estimated greater than value and is calculated for the dilution using the least amount of sample. D6 The precision between the sample and sample duplicate exceeded laboratory control limits El Reported value should be considered a minimum estimate since it is the maximum reportable number for this method based on the sample volume used. The true value is likely greater than the value reported IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be considered an estimated value. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery R1 RPD value was outside control limits. R6 The RPD between valid sample dilutions exceeded 30%. vi The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected In the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report s a l not be reproduced except in full, Date 11/10/2023 0320 PM with_ut the written r, nsent of Pace Analytical Services, LLC Page 29 of 34 ,�ace QUALITY CONTROL DATA CROSS REFERENCE TABLE Project Piedmont Custom Meats- Oct Pace Project No 92695435 Lab ID 92695435001 92695435002 92695435003 92695435004 92695435004 92695435001 92695435002 92695435003 92695435004 92695435001 92695435002 92695435003 92695435004 92695435001 92695435002 92695435003 NYZ4:I.�ir�i�I�L•! 92695435004 92695435004 92695435004 92695435004 92695435004 92695435001 92695435002 92695435003 Sample ID M W-1 MW-4 M W-5 Effluent Effluent MWA MW-4 MW-5 Effluent M W-1 MW-4 MW-5 Effluent M W-1 MWA M W-5 Effluent Effluent Effluent Effluent Effluent Effluent M W-1 MW-4 M W-5 Date 11l1012023 03.20 PM QC Batch Method SM 2540C-2015 SM 2540C-2015 SM 2540C-2015 SM 2540C-2015 SM 254OD-2015 EPA 350.1 Rev 2 0 1993 EPA 350.1 Rev 2 0 1993 EPA 350.1 Rev 2 0 1993 SM 521 OB-2016 SM 9222D-2015 SM 9222D-2015 SM 9222D-2015 Colilert-18 EPA 8260D EPA 8260D EPA 8260D TKN+NO3+NO2 Calculation EPA 300.0 Rev 2 1 1993 EPA 350.1 Rev 2 0 1993 EPA 351.2 Rev 2 0 1993 EPA 353.2 Rev 2 0 1993 EPA 365.1 Rev 2 0 1993 SM 531OB-2014 SM 531OB-2014 SM 531 OB-2014 QC Batch Analytical Method 809891 809891 809891 809891 809306 810819 810819 810819 809308 809516 809516 809516 809212 810062 810062 810062 P.1ii 809562 811004 811781 811642 811606 809739 809739 809739 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced except w full, without the written consent of Pace Analytical Services, .LC SM 521OB-2016 SM 9222D-2015 SM 9222D-2015 SM 9222D-2015 Colilert-18 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Analytical Batch 809663 809517 809517 809517 809213 EPA 351 2 Rev 2 0 1993 811990 EPA 365 1 Rev 2 0 1993 812022 Page 30 of 34 ** 8<8<8<� b� M!1yl�ap a a)Ye1u/01u0) es u0Y YO�Ietiifild a V N x q )Z u n N EE s F Atuo asn gin E o M X b dIMIXHN a NO3 auojw) I-aj dZZZB 018W x X X ~� ►0S!•13/PuoO O X X X > coy— o �• ! E NO3 wJOIIIO3 I?34j 811Lel!I03 x v Si •AUOI43 V / • ` s r< c .2 N h € n 10M1 MOl AS" Q09Z8 X X x x 0 ; 301GOIC9 x x ~ � NQ3 Aop S '008 8o 1 ZS X NQ3 elu0wwy 1 OSC X X X r� 9p110S POPUO&n S R101 OOfSZ X l! � d — o � cr g 3 O r O O O Q Dts t Y `° a C v L R i _ a Y ^ 6A. O QV � 3ccc a _ u z G q w x � s 3 a o ` yyim X Q� Ti C E v In 8 9 1 i ` 34 I� 0 Jvl P N 1-uY El ~ ur • S s ,W 3 m t a ps v a a C h 2 V � ylJ � Z S Y V • ,� M1 w E � < E z W 0 G L 6 DC#_Title: ENV-FRM-HUN1.0084 v01_Tech Spec Sample Condition ce Upon Receipt Effective Date: 0511212022 Laboratory receiving samples: Asheville ❑ Eden ❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersvillecr Sample Condition Upon Client Name: Receipt Project #: �,•e �IMo� Courier: ❑Fed Ex ❑UPS MUSPS []Client C pe f 4-Y /y ❑ Commercial [ace []Other: Carrier Tracking Number: Custody Seal Present? []Yes CNo Seals Intact? ❑Yes ❑No Date/Initials Person Examining Contents:�,� Packing Material: ❑Bubble Wrap ❑Bubble Bags 5None ❑ Other Biological Tissue Fr ten? ❑Yes ❑No [fNN/A Thermometer: ❑ IR Gun 10: t O w� Type of Ice: lJ Wet ❑Blue ❑None Cooler Temp ('C ): 3.1 Correction Factor: Add / Subtract ('C ) T� Temo should be above freezine to 6'C Corrected Cooler Temp {* C 0 ❑Samples out of temp criteria. Samples on ice, cooling process )' 3' has begun USDA Regulated Soil (&N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally, ❑Yes ❑No including Hawaii and Puerto Rico)? ❑Yes []No Comments/Discrepancy: Chain of Custody Present? 16s QN0 N/A 1. Samples Arrived within Hold Time? 16yes No NIA 2. Short Hold Time Analysis (02 hr.)? es ❑No QN/A 3. Rush Turn Around Time Requested? QYes ZJNo N/A 4. Sufficient Volume? Zes oft N/A S. Correct Containers Used? Pace Containers Used? EjrYes 13yes ❑No No ❑N/A N/A 6 Containers Intact? Cyes QN0 N/A 7 Dissolved analysis: Samples Field Filtered? ❑Yes ONo N/A 8. Sample Labels Match COC? Includes Date/Time/ID/Analysis Matrix. Q4es tyT []NO ❑N/A 9. Headspace in VOA Vials (>S-6mm)) OYes JJNo N/A 10, Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes Yes [:]No ONo N/A N/A 11. COMMENTS/SAMPLE DISCREPANCY Temp Log: Temp must be maintained at <6 C during login, record temp every 20 minutes. Time opened: Temp: Time: put in cooler Time: Temp: Person Contacted: Project Manager SCURF Review: Project Manager SRF Review: Lot ID of split containers. CLIENT NOTIFICATION/RESOLUTION Date/Time: Date: Date: Field Data Required? QYes [)No Qualtrax Document ID 70677 Page 1 of 2 Page 33 of 34 Document Name: Document Issued: November 15, 2021 2ceAnaiyhcal Bottle Identification Form (9IFJ Page 1 of 1 Document No.: Issuing Authority: F-CAR-CS-043•Rev.01 Pace Carolinas Quality Office "Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions. VOA, Collform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottles Project A E' C u Q. E N, Z y C 7 J £ � a ` C v J QE d a W p C 6 Y ., _ = O = u J E a d Z Z u J £ r�`v.~. s Z Y N ., J E s N 2 0 z J £ a G q Z5 $ M E: 3 9 L Z a ? Q .r t7 N _ E -X ., 14 t7 V 2 u C E `9rr' M 0 = 171 N S Cq4 Q .r ` l7 N a fV i E J E N r'An l4 u = 2 E Q J E uQ ..:. t7 2 a S O > cQE� Y a t,� 79— �ry Z ¢ > E4 Y ifi 0 4 a 44 c M O > qEq Y a O g S O > E q i�i Q 't O Y k N x < O Z p k N N a _v 4 N .`r. in a A \ M 0. « N N a M n = Y A J r rn a V y> Z ? n > C C oE d J V1 g N t7 Y p a a N2 3 3 I 31 1 31 1 1I 3 Z� 3 + 3 1\N 5 6 7 8 9 M 10 11 \\� I I ]2 N\�\\\� I I pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot p Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ji e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 34 of 34 (-'39'ace November 03, 2023 Larry Moore Piedmont Custom Meats 430 NC Highway 49 South Asheboro, NC 27205 RE: Project: Piedmont Custom Meats -Oct Pace Project No.: 92695966 Dear Larry Moore: Pace Analytical Services, LLC 1377 South Park Drive Kemersville. NC 27284 Enclosed are the analytical results for sample(s) received by the laboratory on October 31, 2023, The results relate only to the samples included in this report. Results reported herein conform to the applicable TNUNELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network • Pace Analytical Services -Asheville • Pace Analytical Services - Eden If you have any questions concerning this report, please feel free to contact me. Sincerely, Stephanie Knott stephanie.knott@pacelabs.com 704-977-0981 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fu'� without the written consent of Pace Analytical Services L_C. (704)977-0981 Page 1 of 17 ace Project Pace Project No. Piedmont Custom Meats -Oct 92695966 Pace Analytical Services, LLC 1377 Soulh Park Drive Kemersville, NC 27284 (704)977-0981 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 Pace Analytical Services Eden 205 East Meadow Road Suite A. Eden, NC 27288 North Carolina Drinking Water Certification # 37738 CERTIFICATIONS South Carolina Laboratory ID 99030 South Carolina Cert fication #: 99030001 Virgin;aNELAP Cert fication #: 460222 North Carolina Wastewater Certification #: 633 Virgin aNELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC Page 2 of 17 ace SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Project: Piedmont Custom Meats -Oct Pace Project No.: 92695966 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92695966001 MW-1 EPA 353.2 Rev 2.0 1993 AED 1 PASI-E EPA 120.1-1982 SMS 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 2 PASI-A 92695966002 MW-4 EPA 353.2 Rev 2.0 1993 AED 1 PASI-E EPA 120.1-1982 SMS 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 2 PASI-A 92695966003 MW-5 EPA 353.2 Rev 2.0 1993 AED 1 PASI-E EPA 120.1-1982 SMS 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 2 PASI-A 92695966004 Effluent EPA 353.2 Rev 2.0 1993 SRS 2 PASI-E PAS I -A - Pace Analytical Services - Asheville PAS I-E = Pace Analytical Services -Eden REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services, LLC Page 3 of 17 ANALYTICAL RESULTS Project: Piedmont Custom Meats -Oct Pace Project No.: 92695966 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: MWA Lab ID: 92695966001 Collected: 10/31/23 11.15 Received: 10/31/23 12:40 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. 353.2 NO2/NO3 unpres EON Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 22.7 mg/L 0.20 5 10/31/23 16:56 14797-55-8 120.1 Specific Conductance Analytical Method: EPA 120.1-1982 Pace Analytical Services - Asheville Specific Conductance 516 umhos/cm 10.0 1 11/02/23 12:08 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 57.5 mg1L 1.0 1 11/02/23 03:00 16887-00-6 Sulfate NO mg1L 1.0 1 11/02/23 03:00 14808-79-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except to fu , Dale: 11/03/2023 05.53 PM without the written consent of Pace Analyt cal Services, LLC. Qual Page 4 of 17 �ce ANALYTICAL RESULTS Project: Piedmont Custom Meats -Oct Pace Project No.: 92695966 Pace Analytical Services, LLC 1377 South Park Drive Kemersvt, e. NC 27284 (704)977-0981 Sample: MW-4 Lab ID: 92695966002 Collected: 10/31/23 11:30 Received: 10/31/23 12:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. 353.2 N021NO3 unpres EON Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 1.6 mg/L 0.040 1 10/31/23 17:14 14797-55-8 120.1 Specific Conductance Analytical Method: EPA 120.1-1982 Pace Analytical Services - Asheville Specific Conductance 1020 umhoslcm 10.0 1 11/02/23 12:10 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 234 mg/L 5.0 5 11/02/23 07:26 16887-00-6 Sulfate 3.3 mg/L 1.0 1 11/02/23 03:15 14808-79-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in fu' , Date: 11/03/2023 05:53 PM without the written consent of Pace Analytical Services, LLC. Qual Page 5 of 17 Pace Analytical Services, LLC 1377 South Park Drive Kemersvdle, NC 27284 (704)977-0981 ANALYTICAL RESULTS Project: Piedmont Custom Meats -Oct Pace Project No.: 92695966 Sample: MW-5 Lab ID: 92695966003 Collected: 10/31/23 11:25 Received: 10/31/23 12:40 Malrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 353.2 N021NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 0.98 mg1L 0.040 1 10/31123 17:02 14797-65-8 120.1 Specific Conductance Analytical Method: EPA 120.1-1982 Pace Analytical Services - Asheville Specific Conductance 1880 umhos/cm 10.0 1 11/02/23 12:12 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville Chloride 502 mg1L 11.0 11 11/02/23 07:40 16887-00-6 Sulfate 1.1 mg1L 1.0 1 11/02/2303:30 14808-79-8 Date: 11l03l2023 05:53 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC Page 6 of 17 ace ANALYTICAL RESULTS Project: Piedmont Custom Meats -Oct Pace Project No. 92695966 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977 0981 Sample: Effluent Lab ID: 92695966004 Collected 10,,31/23 11-20 Received: 10/31/23 12:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 353.2 N021NO3 unpres EDN Analytical Method EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, NO2 plus NO3 43.4 mg L 0.40 10 11/01/23 16:52 Nitrogen. Nitrate 4.5 mg;L 0.80 20 11/01/23 16:53 14797-55-8 Dale: 11/03/2023 05:53 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full without the wntten consent of Pace Analytical Services LI c. Page 7 of 17 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QUALITY CONTROL DATA Project: Piedmont Custom Meats -Oct Pace Project No.: 92695966 QC Batch: 809998 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method EPA 353.2 Rev 2.0 1993 Analysis Description. 353.2 Nitrate + Nitrite, Unpres. EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples 92695966001 METHOD BLANK: 4193815 Matrix: Water Associated Lab Samples: 92695966001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L ND 0.040 10/31/23 16:14 LABORATORY CONTROL SAMPLE: 4193816 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 1.5 1.5 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4193817 4193818 MS MSD 92695939001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L 2.5 1.5 1.5 3.8 3.8 88 87 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4193819 4193820 MS MSD 92695937001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPO Qual Nitrogen, Nitrate mg1L 2.3 1.5 1.5 3.6 3.6 88 88 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/0312023 05 53 PM without the written consent of Pace Analytcal Services, LLC Page 8 of W Pace Analytical Services, LLC 1377 South Park Drive Kemersvde. NC 27284 (704)977-0981 QUALITY CONTROL DATA Protect Piedmont Custom Meats -Oct Pace Project No.: 92695966 QC Batch: 809999 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN Laboratory Pace Analytical Services - Eden Associated Lab Samples: 92695966002, 92695966003 METHOD BLANK: 4193821 Matrix. Water Associated Lab Samples. 92695966002, 92695966003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg1L ND 0.040 10/31/23 17:07 LABORATORY CONTROL SAMPLE 4193822 Spike LCS LCS % Rec Parameter Un is Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mglL 1.5 1.5 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4193823 4193824 MS MSD 92695966003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen. Nitrate mg1L 0,98 1.5 1.5 2.4 2.4 95 94 90-110 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/03/2023 05:53 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 17 QUALITY CONTROL DATA Project: Piedmont Custom Meats -Oct Pace Project No.: 92695966 QC Batch: 810345 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92695966004 METHOD BLANK: 4195500 Associated Lab Samples: 92695966004 Parameter Units Nitrogen, Nitrate mg/L Nitrogen, NO2 plus NO3 mg/L Matrix: Water Blank Reporting Result Limit Analyzed NO 0.040 11/01/2316:46 NO 0.040 11/01/2316:46 Qualifiers Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 4195501 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg1L 1.5 1.5 101 90-110 Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4195502 4195503 MS MSD 92696197001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L 3.2 1.5 1.5 4.5 4.7 89 105 90-110 5 Nitrogen, NO2 plus NO3 mg1L 3.2 2.5 2.5 5.6 5.8 94 102 90-110 3 Results presented on this page are in the units Indicated by the 'Units' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in lull. Date. 11/03/2023 05:53 PM without the written ccnsent of Pace Analytical Services, LLC Page 10 of 17 ace QUALITY CONTROL DATA Project: Piedmont Custom Meats -Oct Pace Project No.: 92695966 QC Batch: 810512 Analysis Method: EPA 120.1-1982 QC Batch Method. EPA 120.1-1982 Analysis Description: 120.1 Specific Conductance Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92695966001, 92695966002, 92695966003 METHOD BLANK: 4196155 Matrix: Water Associated Lab Samples: 92695966001, 92695966002, 92695966003 Blank Reporting Parameter Units Result L mit Analyzed Qualifiers Specific Conductance umhos/cm ND 10.0 11/02/23 11.24 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 4196156 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Specific Conductance umhoslcm 1410 1410 100 90-110 SAMPLE DUPLICATE: 4196157 92695686001 Dup Parameter Units Result Result RPD Qualifiers Specific Conductance umhos/cm 38400 38400 0 SAMPLE DUPLICATE: 4196158 92695686002 Dup Parameter Units Result Result RPD Qualifiers Specific Conductance umhos/cm 34100 34100 0 Results presented an this page are In the units indicated by the 'Units' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/03/2023 05:53 PM without the written consent of Pace Analytical Services, L.0 Page 11 of 17 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977 0981 QUALITY CONTROL DATA Project: Piedmont Custom Meats -Oct Pace Project No.: 92695966 QC Batch: 810436 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92695966001, 92695966002, 92695966003 METHOD BLANK: 4195954 Matrix: Water Associated Lab Samples: 92695966001, 92695966002, 92695966003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg/L ND 1.0 11/01/23 23:48 Sulfate mg/L. ND 1.0 11/01/23 23:48 LABORATORY CONTROL SAMPLE: 4195955 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Chloride mg/L 50 51.8 104 90-110 Sulfate mg/L 50 52.2 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4195956 4195957 MS MSD 92696280001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L. 50 50 66.9 68.6 99 102 W110 2 Sulfate mg/L 249 50 50 299 307 100 117 90-110 3 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4195958 4195959 MS MSD 92696318002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 21.3 50 50 71.8 73.0 101 103 90-110 2 Sulfate mg/L 210 50 50 259 256 97 92 90-110 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 11/03/2023 05:53 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 17 Pace Analytical Services, LLC 1377 South Park Drive Kemersville. NC 27284 (704)977-0981 QUALIFIERS Project: Piedmont Custom Meats -Oct Pace Project No.. 92695966 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilut on of the sample aliquot. ND - Not Detected at or above adjusted report ng limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Pract cal Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Dup Icate RPD - Relative Percent Difference NC - Not Calculable SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethyly nyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. ANALYTE QUALIFIERS M 1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dale: 1110312023 05.53 PM without the written consent of Pace Ana ytical Services. LLC Page 13 of 17 ace QUALITY CONTROL DATA CROSS REFERENCE TABLE Project- Piedmont Custom Meats -Oct Pace Protect No. 92695966 Lab ID Sample ID QC Batch Method QC Batch 92695966001 MWA EPA 353.2 Rev 2.0 1993 809998 92695966002 MW-4 EPA 353.2 Rev 2.0 1993 809999 92695966003 MW-5 EPA 353.2 Rev 2.0 1993 809999 92695966004 Effluent EPA 353.2 Rev 2.0 1993 810345 92695966001 MW-1 EPA120.1-1982 810512 92695966002 MW-4 EPA 120.1-1982 810512 92695966003 MW-5 EPA120 1-1982 810512 92695966001 MW-1 EPA 300.0 Rev 2.1 1993 810436 92695966002 MW-4 EPA 300.0 Rev 2.1 1993 810436 92695966003 MW-5 EPA 300.0 Rev 2.1 1993 810436 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11103/2023 05:53 PM without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Analytical Analytical Method Batch Page 14 of 17 — Jul W rwv. »ununun You ugiHuti�ld a p x L c AuOMAgvi Yo u LO N o� - tz 3 � X CON towpo9/1"UO3 X X X • a $«3 Q � 6 u V o z b O i f I- z o_ « a3 ^' d` a a N n t: C Y L { S $ S �i ST •qR � � � � y a` � D 6 8J� S w jj gal Page 15 of 17 DC#_Title: ENV-FRM-HUN1-0084 v01_Tech Spec Sample Condition ce Upon Receipt 1 �« Effective Date: 05/12J2022 Laboratory receiving samples: Asheville ❑ Eden ❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville[] Atlanta❑ Kernersvillp,6 Sample Condition Upon Client Name: Receipt Project q: t t m b n Courier: E] Fjtd Ex ❑UPS CUSPS ❑Client L ,A � W ❑ Commercial ace ❑Other 0. 1J Carrier Tracking Number: M t Custody Seal Present? ❑Yes ffNo Seals Intact? Dyes ONO Date/Initials Person Examining Contents: Packing Material: ❑Bubble wrap ❑Bubb'eBags &None ❑ Other Biological Tissue Fr en? ? Dyes ❑No ❑�I/A Thermometer: ❑ IR Gun to /<'f'T 0 D 2- r O1 ypeaflce: I%12f fWet ❑Blue ❑None Cooler Temp i'e ): 'L. 1 Correction Factor. Add / Subtract ('C ) temp should be above freezing to 6'C Corrected Cooler Tamp ('C 1:�. 2' d ❑Samptes out of temp crttena. Samples an Ke, roolkng prose, has begun USDA Regulated Soil ( eN/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a fore•gn source (internationally, []Yes ONo Including Hawaii and Puerto Rico)? ❑Yes ❑No commentsJoiscre an : Chain of Custody Present? es No N/A 1. Samples Arrived within Hold Time? Llyes No N/A 2 Short Hold Time Analysis <72 hr.)? Yes No N/A 3 Rush Turn Around Time Requested? Elyes o N/A 4. Sufficient Volume? G6es No N/A 5. Correct Containers Used? Pace Containers Used? C(Yes es (:]No No []N/A N/A 6. Containers Intact? aes QNo CINIA 7. Dissolved analysis: Samples Field filtered? OYes QNO ❑N/A 8. Sample Labels Match COC? -IncludesDate/Time/IO/Analysis Matron 21Yes wr ❑No ❑N/A 9 Heads ace in VOA Vials (�-5.6mm)? 0Yes 0NO N/A 10. Trip Blank Present? Trip Blank Custody Seals Present? []Yes Yet []No 0No N/A /A 11. COMMENTS/SAMPLE DISCREPANCY Field Data Required? ©Yes ❑No Temp tog: Temp must be maintained at <6 C during login, record temp every 20 minutes. Time opened: (LY O Temp; Time:(2 b 0 put in cooler Time: Tamp: Person Contacted: Project Manager SCURF Review: Project Manager SRF Review: Dualtrax Document ID: 70677 Lot ID of split conta ners CLIENT NOTIFICATION/RESOLUTION Date/Time: Date: Date: Page 1 of 2 Page 16 of 17 Document Name Bottle Identification Form (BIF) <1f.EAlJdil'11�c31 Document No F-CAR-CS-043•Rev.01 *Check mark top half of box if pH and/or dechlorination is Project # verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, Wig "Bottom half of box is to list number of bottles Document Issued November 15. 2021 Page 1 of 1 i Issuing Authority: k Pace Carolinas Quality Office u Z V T O v L a u z a R u 4 7.n z �l z > z_ E aj 06 p M o _ V {yyy " C V a Q Z Z �yr ti z 41 Z t Z � ' 4 ayy ck4T 4 W Q Q 2 N fT� Z c ' p u x 60 D N Q Y d Q N y� Ya 4Z l7 M `Ay T > ': n i. n N z d 7 U -:: S r S J ✓ e J V m d _n d 4 J i d 'N _n 4 o £ E Q d J Y Qa V uoi y a: d0 > Z d o } 7 d0 > y d > J[ y w o d d 4K 3 J 10 V, qrr [ -EE tc E E E "tE E v `m i. E `u E a A E "' E E ° -' E E E •� a yF ' e$ > o > m 7 m N m 2 m N ro Kt m u t+ d 't�" 4 l7 d u d l7 4 u d 1q� O 0 > O > \ o a q 1 ` t Z 8 PH Adjustment Log for Preserved Samples -� Sample to Type of preservative pH upon receipt pate preservation adjusted Time preservation Amount of Prese:votive Lot 0 adjusted added —T rvote. whenever there fs a arscrepancy altect ng North Carolina comptance samples, a copy of this lorm will be sent to the Nutth Carolina DLHNR Ceraficaaor, office h.e- Out of hold. incorrect preservative, out of ten+p, incorrect containers. Page 17of17 rvote. whenever there fs a arscrepancy altect ng North Carolina comptance samples, a copy of this lorm will be sent to the Nutth Carolina DLHNR Ceraficaaor, office h.e- Out of hold. incorrect preservative, out of ten+p, incorrect containers. Page 17of17