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HomeMy WebLinkAboutWQ0007798_Trimester Monitoring_19971031. LF N �. `f READ ENVIRONMENTAL, INC. CONTRACTORS AND CONSULTANTS CIVIL • GEOTECHNICAL • ENVIRONMENTAL RESULTS OF 3m TRIMESTER GROUND WATER SAMPLING (1997) PERMIT No. WQ0007798 TOASTMASTER, INC. — INGRAHAM TIME PRODUCTS FACILITY GROUND WATER INFILTRATION GALLERY SCOTLAND COUNTY LAURINBURG9 NORTH CAROLINA p r HLL;Ld V tLU) PREPARED FOR: f,:ry 0 5 1997 I -AYE i € VI LE IT -Ha. OrFIGE NORTH CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH, & NATURAL RESOURCES DIVISION OF WATER QUALITY RALEIGH, NORTH CAROLINA PREPARED BY: GULFSTREAM ENVIRONMENTAL, INC. CONTRACTORS & CONSULTANTS WILDIINGTON and CHARLOTTE V ULFSTREAM ENVIRONMENTAL, INC. --f CONTRACTORS AND CONSULTANTS { CIVIL • GEOTECHNICAL • ENVIRONMENTAL October 31, 1997 North Carolina Department of Environment, Health, and Natural Resources Division of Water Quality _ P.O. Box 29578 Raleigh, North Carolina 27626-0535 Re: Results of 3rd Trimester Ground Water Sampling (1997) Permit No. W00007798 Toastmaster, Inc.- Ingraham Time Products Facility Ground Water Infiltration Gallery Laurinburg, Scotland County, North Carolina Dear Sir or Madam: Please find enclosed the monitoring report outlining the results of the Yd Trimester Ground Water Sampling event conducted on September 11, 1997 at Toastmaster, Incorporated's Ingraham Time Products Facility. Within this report, you will find: • Ground Water Pump & Treat Remediation Site Data Sheet, Part A • Table 1 -- Ground Water Level Data • Table 2 -- Laboratory Analytical Results for Trichloroethene -- Ground Water • Table 3 -- pH and Temperature Data — Ground Water • Table 4A — Ground Water Remediation System Pressure Readings Table 4B — Ground Water Remediation System Volume Readings • Graphs 1-18 depicting Ground Water Monitoring data trends for all sampling events 1/16/96 through 9/11/97 • GW-59 forms for 7/97 through 9/97 • Laboratory Analytical Results • Drawings 1 and 2 depicting Trichloroethene Isocontours and Ground Water Contours respectively P.O. BOX 592 WRIGHTSVILLE BEACH, NC 28480 (910) 686-4493 OFFICEIFAX 1 I ,ir G, I` October 31, 1997 Page 2 If you have any questions, or if we may be of assistance, please do not hesitate to contact us at 910.686.4493. Sincerely, 'P-J, a Rudy A. Smithwick, P.G. President Enclosures cc: Mr. Larry Clark, Toastmaster, Inc. Jon K Jester Vice President GW-79 GROUND WATER PUMP & TREAT REMEDIATION SITE DATA SHEET Ll NORTH,CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES Division of Environmental Management, Groundwater Section (To be each submission) Background Site Name: �IQASTMA9fF2�SilL. IXWGRAWA A DIV. Incident No: Date: Location: r Region: 1: 1VEM&V Responsible Party: SC aR.AN Q Date Release Identified: 1:1►jC_ Date CAP Completed: PART R (To be completed for initial report or to update information previously provided) Hydrogeology Description of Aquifer Lithology: Is bedrock aquifer/fractured saprolite impacted? Describe. Average Hydraulic Conductivity (ft./day): Average Groundwater Gradient How were above determined? Major Pumping Influences Which may Affect GW Flow: Distance from Site: Pumping Rate: Location and Distance from Site of Nearest Supply Well(s): _ Description of Release , Type of Product: Estimated Volume Released: Average Plume Dimensions(ft.)--Width: Length: Depth Interval: Ranges of Concentrations from CSA: Emergency Response/Initial Remedial Actions Date Source Removed/Repaired: Free Product Recovered (gal.): Soil Excavation (tons): Average Contaminant Concentration (mg/kg): Type of Treatment or Disposal: Remediation Goals of Remediation: Description of Treatment System: Pilot test conducted? (Type) Date: Method of System Effluent Disposal: No. of Monitoring Wells: Monitoring Schedule: Date GW System Started: No. of.Recovery Wells: Recovery Well Flowrate Drawdown Radius of • .Pump Type/ GPM (ft.) Influence(ft.) Capacity Are any other remediation systems used in conjunction with Pump & Treat? Describe. PART C SYSTEM PERFORMANCE MONITORING (To be completed with each submission) PERIOD OF OPERATION Report for: _/_/_ to —/_/— Days of Operation this Period: SYSTEM DOWNTIME SUMMARY (current reporting period only) DATE From/To FREE PRODUCT RECOVERY Total Gallons Recovered Since Last Report: Total Gallons Recovered to Date: Well Z.D.: Reason Date Screened interval* FP Thickness (in.) Avg. GW Level* Recovery Method *Depth in Feet from Top of Casing Provide similar table for each well containing free product by attaching additional sheet(sJ INFLUENT & EFFLUENT CONCENTRATION DATA - TREATMENT SYSTEM Gallons Treated Since Last Report: Total Gallons Treated To Date: _ Parameter/Units: Date Influent Effluent Attach additional sheet(s) as needed. COMMENTS: Parameter/units: Note: Attach a current map showing location of all monitoring/recovery wells, remediation system components, and the extent of the contaminant plume., 4 trenches, GW-79/5-94 TABLES TABLE 1(Page 1 of 4) Ground Water Table Data Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, North Carolina Well ID Date Top of Casing Elevation Depth to Ground Water Ground Water Table Elevation Monitoring Wells MW-1 1/16/96 116.41 11.73 104.68 5/23/96 _ 116.41 11.15 105.26 9/16/96 116.41 15.66 100.75 1/31/97 116.41 8.75 107.66 4/28/97 116.41 12.82 103.59 9/11/97 116.41 15.70 100.71 1%M-2 1/16/96/ 113.76 15.57 98.19 5/23/96 113.76 15.72 98.04 9/16/96 113.76 17.82 95.94 1/31/97 113.76 13.26 100.50 4/28/97 113.76 15.82 97.94 9/11/97 113.76 17.93 95.83 MW-3 1/16/96 112.34 12.41 99.93 5/23/96 112.34 9/16/96 112.34 1/31/97 112.34 4/28/97 112.34 12.11 100.23 9/11/97 112.34 14.82 97.52 MW-4 1/16/96 115.12 14.08 101.04 5/23/96 115.12 13.64 101.48 9/16/96 115.12 16.58 98.54 1/31/97 115.12 11.89 103.23 4/28/97 115.12 13.60 101.52 9/11/97 115.12 16.65 98.47 MW-5 1/16/96 119.78 9.00 110.78 5/23/96 119.78 8.73 111.05 9/16/96 119.78 10.32 109.46 1/31/97 119.78 7.15 112.63 4/28/97 119.78 8.10 111.68 9/11/97 119.78 11.94 107.84 Note: * - No Data Available BQL -Below Quantitation Limit All monitoring wells with the prefix GT/T have been reassigned the designation/prefix MW r - I �J TABLE 1(Page 2 of 4) Ground Water Level Data Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, North Carolina Well ID Date Top of Casing Elevation Depth to Ground Water Ground Water Table Elevation NM-6 1/16/96 112.94 14.52 98.42 5/23/96 112.94 14.51 98.43 9/16/96 112.94 16.82 96.12 1/31/97 112.94 12.65 100.29 4/28/97 112.94 14.64 98.30 9/11/97 112.94 16.77 96.17 MW-7 1/16/96 120.81 14.41 106.40 5/23/96 120.81 13.88 106.93 9/16/96 120.81 16.52 104.29 1/31/97 120.81 11.44 109.37 4/28/97 120.81 13.14 ' 107.67 9/11/97 120.81 16.93 103.88 NIW-8 1/16/96 114.82 0.40 114.42 5/23/96 114.82 1.21 113.61 9/16/96 114.82 0.00 114.82 1/31/97 114.82 0.00 114.82 4/28/97 114.82 0.07 114.75 9/11/97 114.82 2.58 112.24 NIW-9 1116/96 117.15 15.20 101.95 5/23/96 117.15 14.96 102.19 9/16/96 117.15 17.81 99.34 1/31/97 117.15 13.45 103.70 4/28/97 111.15 14.51 102.64 9/11/97 117.15 17.70 99.45 NM-10 1/16/96 110.83 10.48 100.35 5/23/96 110.83 9.17 101.66 9/16/96 110.83 13.55 97.28 1/31/91 110.83 7.41 103.42 4/28/97 110.83 8.60 102.23 9/11/97 110.83 13.25 97.58 MW-11 1/16/96 117.57 '11.82 105.75 5/23/96 117.57 11.52 106.05_ Note: " - No Data Available BQL - Below Quantitation Limit All monitoring wells with the prefix GT/T have been reassigned the designation/prefix MW 'LI) TABLE 1(Page 3 of 4) Ground Water Level Data Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, North Carolina Well ID Date Top of Casing Elevation Depth to Ground Water Ground Water Table Elevation MW-11 cont'd 9/16/96 117.57 11.65 105.92 1/31/97 117.57 9.14 108.43 4/28/97 117.57 10.70 106.87 9/11/97 117.57 14.26 10331 AM-12 1/16/96 109.25 8.77 100.48 5/23/96 109.25 7.93 101.32 9/16/96 109.25 12.85 96.40 1/31/97 109.25 4/28/97 109.25 9/11/97 109.25 9.85 99.40 NM-13 1/16/96 120.35 23.50 96.85 5/23/96 120.35 21.73 98.62 9/16/96 120.35 21.55 98.80 1/31197 120.35 19.28 101.07 4/28/97 120.35 27.41 92.94 9/11/97 120.35 20.86 99.49 MW-14 1/16/96 119.03 12.02 107.01 5/23/96 119.03 11.12 107.91 9/16/96 119.03 15.82 103.21 1/31/97 119.03 6.07 112.96 4/28/97 119.03 10.85 108.18 9/11/97 119.03 15.39 103.64 RC-15 1/16/96 121.15 17.29 103.86 5/23/96 121.15 19.80 101.35 9/16/96 121.15 19.74 101.41 1131 /97 121.15 15.82 105.33 4/28/97 121.15 16.41 104.74 9/11/97 121.15 20.00 101.15 Recovery Wells RW-1 1/16/96 112.38 18.14 94.24 5/23/96 112.38 15.42 96.96 Note: * -No Data Available BQL -Below Quantitation Limit All monitoring wells with the prefix GT/T have been reassigned the designation/prefix MW TABLE 1(Page 4 of 4) Ground Water Level Data Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, North Car6lina Well ID Date Top of Casing Elevation Depth to Ground Water Ground Water Table Elevation RW-1 cont'd 9/16/96 112.38 19.92 92.46 1/31/97 1.12.38 18.71 93.67 4/28/97 112.38 24.90 87.48 9/11/97 112.38 22.40 89.98 RW-2 1/16/96 117.48 22.99 94.49 5/23/96 117.48 18.61 98.87 9/16/96 117.48 34.78 82.70 1/31/97 117.48 24.51 92.97 4/28/97 117.48 32.74 84.74 9/11/97 117.48 35.42 82.06 RW-3 1/16/96 117.09 19.93 97.16 5/23/96 117.09 16.31 100.78 9/16/96 117.09 34.30 82.79 1/31/97 117.09 28.97 88.12 4/28/97 117.09 11.54 1 105.55 9/11/97 117.09 31.94 1 85.15 Note:. -No Data Available BQL -Below Quantitation Limit All monitoring wells with the prefix GT/T have been reassigned the designationtprefix MW TABLE 2 (Page 1 of 4) , Laboratory Analytical Results for Trichloroethene— Ground Water EPA Method 624 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, North Carolina Well ID Date Trichloroethene (ppb) NC Standard — 2.8 Monitoring Wells MW-1 1/16/96 930 5/23/96 96 9/16/96 510 1/31/97 730 4/28/97 130 9/11/97 560 MW-2 1/16/96 1100 5/23/96 29 y 9/16/96 8.0 1/31/97 14.0 4/28/97 11.0 9/11/97 1400 MW-3 1/16/96 5/23/96 9/16/96 1/31/97 4/28/97 110 9/11/97 150 MW-4 1/16/96 6100 5/23/96 3100 9/16/96 1600 1/31/97 5000. 4/28/97 3600 9/11/97 5500 MW-5 1/16/96 13000 5/23/96 14000 9/16/96 9000 1/31/97 8400 4/28/97 6400 9/11/97 1600 Note: * - No Data Available BQL — Below Quantitafion Limit All monitoring wells with the prefix GT/T have been reassigned the designation/prefix MW TABLE 2 (Page 2 of 4) Laboratory Analytical Results for Trichloroethene— Ground Water EPA Method 624 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, North Carolina WellID Date Trichloroethene (ppb) C Standard — 2.8 MW-6 1/16/96 2500 5/23/96 1800 9/16/96 1000 1/31/97 1800 4/28/97 1900 9/11/97 720 MW-7 1/16/96 1200 5/23/96 14000 9/16/96 1600 1/31/97 12000 4/28/97 4700 9/11/97 1100 MW-8 1/16/96 15 5/23/96 20 9/16/96 <5.0 1/31/97 <5.0 4/28/97 <5.0 9/11/97 16 MW 9 1/16/96 16 5/23/96 49 9/16/96 54 1/31/97 23 4/28/97 37 9/11/97 17 NM-10 1/16/96 17 5/23/96 <5.0 9/16/96 1700 1/31/97 <5.0 4/28/97 <5.0 9111/97 580 MW-11 1/16/96 280 5/23/96 240 Note: * - No Data Available BQL —Below Quantitation Limit All monitoring wells with the prefix GT/T have been reassigned the designation/prefix MW I� TABLE 2 (Page 3 of 4) Laboratory Analytical Results for Trichloroethene— Ground Water EPA Method 624 Toastmaster, Inc. Ingraham Time Products Facility Laurinbur , North Carolina Well ID Date Trichloroethene (ppb) NC Standard — 2.8 MW-11 cont'd 9/16/96 230 1/31/97 94 4/28/97 130 9/11/97 410 NM-12 1/16/96 90 5/23/96 41 9/16/96 110 1131/97 14 4/28/97 9/11/97 3 MW-13 1/16/96 340 5/23/96 230 9/16/96 160 1/31/97 62 4/28/97 280 9/11/97 66 NM-14 1/16/96 28 5/23/96 87 9/16/96 460 1/31/97 60 4/28/97 120 9/11/97 22 RC-15 1/16/96 <5.0 5/23/96 <5.0 9/16/96 <5.0 1/31/97 <5.0 4/28/97 <5.0 9/11/97 <1.0 Recovery Wells RW-1 1/16/96 1600 5/23/96 1800 9/16/96 1 1500 Note: * -No Data Available BQL — Below Quantitation Limit All monitoring wells with the prefix GUT have been reassigned the designation/prefix MW TABLE 2 (Page 4 of 4) Laboratory Analytical Results for Trichloroethene— Ground Water EPA Method 624 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, North Carolina Welly Date Trichloroethene (ppb) C Standard —2.8 RW-1 cont'd 1/31/97 1400 4/28/97 1200 9/11/97 1200 RW-2 1/16/96 2300 5/23/96 2900 9/16/96 2000 1/31/97 2000 4/28/97 1500 9/11/97 1600 RW-3 1/16/96 410 5/23/96 1700 9/16/96 310 1/31/97 460 4/28/97 420 9/11/97 1300 Influent 9/11/97 1100 Effluent (System) 9/11/97 100 Effluent Trench 10/6/97 B L Note: * -No Data Available BQL —Below Quantitation Limit L6 All monitoring wells with the prefix GT/T have been reassigned the designation/prefix MW Table 3 pH and Temperature Data - Ground Water 3rd Trimester Sampling Event - 9/11/97 Toastmaster, Inc. Ingraham Time Products Facility Laurinbur NC Well ID pH - Laboratory Measurement pH - Field Measurement Temperature (Celsius) Wells -Monitoring MW-1 6.51 6.45 28.5 MW-2 5.82 6.62 24.1 MW-3 5.98 6.42 23.4 MW-4 5.67 6.59 23.9 MW-5 5.80 6.72 20.5 MW-6 5.42 6.87 28.3 MW-7 5.32 6.65 24.5 MW-8 5.44 6.91 27.0 MW-9 5.20 6.83 25.8 AM-10 4.75 6.45 24.0 MW-11 5.80 6.35 21.9 AM-12 5.50 6.63 22.5 AM-13 6.39 6.36 23.5 MW-14 5.28 6.47 20.3 RC-15 5.47 6.59 23.8 Recovery Wells RW-1 5.72 6.90 24.7 RW-2 5.33 6.62 26.7 RW-3 5.66 6.90 24.9 EFFLUENT 6.26 6.83 18.7 INFLUENT 5.54 6.59 27.8 EFFLUENT 10/6/97 6.39 Note: * - No Data Available BQL -Below Quantitation Limit All monitoring wells with the prefix GT/T have been reassigned the designation/prefix MW Table 4A Ground Water Remediation System Pressure Readings 3'd Trimester Sampling Event — 9/11/97 Toastmaster, Inc. Ingraham Time Products Facility Laurin bur , NC Location Reading Bag Filter (Right) 29 psi Bag Filter Left 32 psi Blower Pressure 47 psi G Carbon Bank 1 22 psi Carbon Bank 2 20 psi Carbon Bank 3 19 psi Table 4B Ground Water Remediation System Volume Readings 3rd Trimester Sampling Event— 9/11/97 Toastmaster, Inc. Ingraham Time Products Facility Laurin bur , NC Location Reading Influent RW-1 426818.0 gal. Influent RW-2 672091.7 gal. Influent RW-3 710456.8 gal. Effluent Totalizer 414882.0 gal. Note: * -No Data Available BQL — Below Quantitation Limit All monitoring wells with the prefix GT/T have been reassigned the designation/prefix MW [!!:Z\ is f.`+ i L; 0 1000 900 800 700 a a 600 W C O 500 c d c 400 0 U 300 200 100 0 Graph 1 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MWA Monitoring Data -- Trichloroethene 1/16196 5/23/96 9/16/96 1/31/97 - 4/28/97 9/11/97 Date Sampled tMW-1 Graph 2 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-2 Monitoring Data -- Trichloroethene tMW-2 Graph 3 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-3 Monitoring Data -- Trichloroethene Date Sampled No data was collected during 1996 and during the first trimester of 1997 because MW-3 had been damaged. Graph 4 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-4 Monitoring Data -- Trichloroethene 16000 14000 12000 n 10000 a N C O 8000 c d n c U 6000 �za�r 0 Graph 5 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-5 Monitoring Data -- Trichloroethene Date Sampled Graph 6 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-6 Monitoring Data -- Trichloroethene Graph 7 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-7 Monitoring Data -- Trichloroethene tMW-7 Graph 8 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-8 Monitoring Data -- Trichloroethene `A 20 29 Z= 16; ;.. a 15 4 C O M V M d c 10 _. o gg k 5 l 0 I r i •9 i �9 r G9 r 1 /16/96 5/23/96 9/16/96 1 /31 /97 4/28/97 9111 /97 Date Sampled Concentrations of Trichloroethene for the sampling periods of 9/16196, 1/31/97, and 4/28/97 were not detected above the quantitation limit of 5.0 ppb. Graph 9 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-9 Monitoring Data -- Trichloroethene Date Sampled 1800 1600 1400 1200 C a a No . 11 me 200 0 Graph 10 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-10 Monitoring Data -- Trichloroethene 1 /16196 5/23/96 9/16/96 1 /31 /97 4/28/97 9/11 /97 Date Sampled Concentrations of Trichloroethene for the sampling periods 5/23/96, 1 /31197, and 4128/97 were not detected above the quantitation limit of 5.0 ppb. 450 400 350 300 a a o. 250 0 A d 200 u 0 0 U 150 100 50 C Graph 11 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-11 Monitoring Data -- Trichloroethene 1116/96 5/23/96 9116/96 1 /31 /97 4/28/97 9/11 /97 Date Sampled 120 100 T; 20 A Graph 12 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-12 Monitoring Data -- Trichloroethene 1/16/96 5/23/96 9/16/96 1/31/97 4/28/97 9/11/97 Date Sampled No data was available for the sampling period of 4/28/97. M 350 300 a 250 a 0 C O riy 200 C d V C V 150 100 50 i) Graph 13 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC MW-13 Monitoring Data -- Trichloroethene Date Sampled i Graph 14 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NG MW-14 Monitoring Data -- Trichloroethene Graph 15 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC RC-15 Monitoring Data -- Trichloroethene Concentrations of Trichloroethene for all sampling periods in 1996 and 1997 were not detected above the respective quantitation limits. 2000 1800 1600 1400 C a 1200 Ol C O 1000 C d c 800 O U 600 400 200 0 Graph 16 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC RW-1 Monitoring Data -- Trichloroethene Date Sampled -�-- RW-1 3500 3000 2500 a a a N 2000 e 0 R 1500 c 0 U 1000 500 7 Graph 17 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC RW-2 Monitoring Data -- Trichloroethene Date Sampled :i• 1600 1400 1200 a a a e 1000 0 m 800 c 0 A IlP 400 200 Graph 18 Toastmaster, Inc. Ingraham Time Products Facility Laurinburg, NC RW-3 Monitoring Data -- Trichloroethene 1700 1300 _424_-- 0. 1/16/96 5/23196 9/16/96 1/31/97 4/28/97 9/11/97 Date Sampled GW-59 GROUND WATER QUALITY MONITORING COMPLIANCE REPORT FORMS I U DIVISION OF WATER QUALITY -GROUNDWATER SEOTION GROUNDWATER QUALITY MONITORING ; °�PQ Boxzs57a _, a z - For additional forms RALEIGN, NC 27626 057f COMPLIANCE REPORT FORM „s please,writeoreall r (gi9)733p3227 a `s Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED,1, -�P'� Non -Discharge %Q'x7i'i�}g Facility Name Address I NP.DES TYPE OF DISPOSAL OPERATION BEING MONITORED t County I Well Location /� ° L I o�7 (REQUIRED) Lagoon Septic TanWDrain Field Well Identification Number MW —1 Well Depth z�. s Ft. Well Diameter. I • ZS Sample (Screened) Interval Ft. To /.SFt. Spray Field Subsurface Low -Pressure Piping (LPP) Depth to Water Level t5,10 ft. below measuring point (before sampling) Land application of.Sedgge, �S— Other Measuring point is I . 7-0 ft. above land surface Gallons of water pumped/bailed betoresampling 2� .. Rotary Distributor Field Analysis: pH (17 • u'S Specific Conductance uMhos Temp. C Odor Appearance Date Sample Collected q- I I . Q r7 Date Lab Sample Analyzed cf 115-L `i 7 Laboratory Name '�� q y A)aby'f -- C� I ( iIDO ids rC'S _ Certification No. �01 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED UL6�YES NO COD mg/1 Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) Co. tl units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/1 Al -Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/1 Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I Ni - Nickel' mg/I Pb - Lead mg/I Zn - Zinc mg/I Pesticides/Herbicides (Specify Compounds) ug/I ug/I ug/I Other (Specify Compounds and Concentration units) I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and 2 �] colloidal concentrations. (see #3 on back) See back for instructions. nature f ermi e (or Authorized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 UIVISIUN GROUNDWATER QUALITY MONITORING: For'a'dd Tonal rorma, COMPLIANCE REPORT FORM � °''' please write or call _ Type or Use a ball-point pen and press firmly. Facility Name- Address-aSi�VlGsa��,� Ont Wcxrinb nil Count ry4l ond Well Location LA_T­ 'Ito LIT' 5?r.-S L.4ln.folo 11 Well Identification Number it Q Well Depth 3 O.o Ft. Well Diameter I+Z5__Sample (Screened) Interval Ft. T0':90.0 Ft. Depth to Water Level Irl, q3 ft. below measuring point (before sampling) Measuring point is I +30 ft. above land surface Gallons of water pumped/bailed before sampling 2, 32 Field Analysis: pH � lvZ Specific Conductance uMhos Temp._ Date Sample Collec d a' i I , L'A2 Date Lab Sample Analyzed q +'t oC Laboratory Name Pr CQ64M A-12W+; cC l L4[QDrGto✓i LS _ SAMPLES FOR METALS WY=RE COLLECTED UNFILTERED AND FIELD ACIDIFIED COD mg/I Coliform: MF Fecal /100m] Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/1 pH (when analyzed) units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/1 TKN as N mg/1 PERMIT NUMBE charge(REQUIR_Epa, �7%-Pg Non -Discharge ht�� " NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) . ,Lagoon Septic tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludg9e !2L Other Rotary Distributor Odor Appearance Certification No. uCJ YES NO Nitrite (NO2) as N mg/I Nitrate (NO3) as N _ mg/I Phosphorus: Total as P mg/I AI - Aluminum mg/I Ba - Barium mg/1 Ca - Calcium mg/I Coll - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/1 Mn - Manganese mg/1 Na - Sodium mg/1 Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Pesticides/Herbicides (Specify Compounds) ug/I ug/I ug/I Other (Specify Compounds and Concentration units) I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and q colloidal concentrations. (see #3 on back) See back for instructions. Signatu of Permi ee (or Authorized Agent') Date t* Submit blue and yellow copies only to address above. GW-59 REV. 8/96 Well Location T " V UY Ib ' . U Well Identification Number Well Depth 3D.r Well Diameter l - Sample (Screened) Interval Ft. To Depth to Water Level ILI' �ft. below measuring point (before sampling) Measuring point is T_j ft. above landsurface.D Gallons of water pumped/bailed before sampling Field Analysis: pH Z Specific Conductance uMhos Temp. Date Sample ColleAted Date Lab Sample Analyzed — Laboratory Nam Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of SI d e V Other Rotary Distributor Appearance Certification No. �U SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED LJ I YES NO COD Coliform Coliform MF Fecal MF Total mg/I /1 o0ml /100m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) Em units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/l Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N Nitrate (NO3) as N Phosphorus: Total AI - Aluminum_ Ba - Barium Ca - Calcium_ Cd - Cadmium_ Chromium: Total _ Cu - Copper .Fe - Iron Hg - Mercury_ K - Potassium Mg - Magnesium Mn - Manganese _ Na - Sodium as P. mg/I Ni - Nickel mg/I mg/I Pb - Lead mg/I mg/I Zn - Zinc mg/I mg/I Pesticides/Herbicides mg/I (Specify Compounds) mg/I ugh mg/l ugh mg/I ugh mg/1 Other (Specify Compounds and mg/I mg/I Coentration units) I�tGhlfky�t1Y�2'� mg/I mg/I mg/I mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and `^` f (� �/ colloidal concentrations. (see #3 on back) \ 10 , 3 L ,9! See back for instructions. 9lgnatLtr� of Per a (or Authorized Agent-) Date •* Submit blue and yellow copies only to address above. GW-59 REV. 8/96 GROUNDWATER ,QU COMPLIANCE REPO Facility Name Address PERMIT NUMBER: (REQUIRED) . Non-Discharge�7 NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED Well Location (REQUIRED) Well Identification Number V4 'L4 Well Depth Ft. Well Diameter �Sample (Screened) Interval Ft. To Ft. Depth to Water Level Ro,L0 L below measuring point (before sampling) Measuring point is ft. above land surface Gallons of water pumped/bailed before sampling I , O Type or Use a ball-point pen and press firmly. Lagoon Septic Tank/Drain Field Subsurface Low -Pressure _ Piping (LPP) Land Application of Sludge Rotary Distributor )C- Other Spray Field Field Analysis: pH (D.Sq Specific Conductance uMhosTemp. ?31t °C Odor — Appearance Date Sample Colle�(ed Q - It •ate Date Lab Sample Analyzed a ' 22 •612 Laboratory Name IJ��Ck(AM t�.CG,• ( (C oprcrloriG-S _ Certification No. UP3 I SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) • to units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/1 Ba - Barium mg/1 Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper - mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Pesticides/Herbicides (Specify Compounds) Ug/I Ug/I ug/I Other (Specify Compounds and I�centration units) �; Mtn l[arcYylr-nne — 55 (X� u9� t I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and I i colloidal concentrations. (see #3 on back) -. )` "� See back for instructions. Si nature f P mittee or Authorized Agent`) Date •• Submit blue and yellow copies only to address above. GW-59 REV. 8/96 GROUNDWATER QUALITY MO COMPLIANCE REPORT FORM, Type or Facility Name DIVI: Por.additional forms pen and press firmly. PERMIT NUMBER: (REQUIRED) Non-DischargeG�Oi%��i NODES TYPE OF DISPOSAL OPERATION BEING MONITORED — County_ . (REQUIRED) Well Location t A -I 34- uo` n l " t a VI -1 I`l—t. I �iv. o Well Identification NuMber fwlt,JfS Well Depth —Ft. Well Diameter s%'Sample (Screened) Interval Ft. To -ZLI,C Ft. Depth to Water Level ( ( 3LA ft. below measuring point (before sampling) Measuring point is'3 - '2,0 ft. above land surface Gallons of water pumped/bailed before sampling �3' f`7 Field Analysis: pH to -qf?N Specific Conductance uMhos Temp. C Date Sample Colle d G' , It (' CC-7DateLab Sample Analyzed Q , 1 Co R _7 Laboratory Name( nQt� 1 Qly tiCQ l �afJD✓Gl (fXteS SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIEDOL COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100mI (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) - 43D units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Lagoon Septic Tank/Drain Field Spray Field Subsurface. Low -Pressure Piping (LPP) Land Application of Sludge Other Rotary Distributor Odor Appearance ' - Certification No. uP)l YES NO Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I Ni - Nickel Pb - Lead mg/I mg/I Zn -Zinc Pesticides/Herbicides (Specify Compounds) mg/I ug/I ug/I ug/I Other (Specify Compounds and Qancentration units) I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) 1o,3/�97 See back for instructions. S naturdi of ermi e (or Authorized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/95 GROUNDWATER QUALITY MONITORING. COMPLIANCE REPORT FORM For additional forms' ' please write or call: 1 �T�y�p, a or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name ,:O L'`� � 1�� ' Non -Discharge Address 0 nt NPDES ! 1:L+lii)KjllY�L.1.t'G� rCounty �11G TYPE OF.DISPOSAL OPERATION BEING MONITORED YY (REQUIRED) Well Location L-A� 21 1° f I� rj'(o " I rw( --?q - 7,7 r Well Identification Number ''(-9 Well Depth I Well Diameter 2, CD Sample (Screened) Interval Ft. To _4J5, t Depth to Water Level (to.-I-7 ft. below measuring point (before sampling) Measuring point is 0,7,0 ft. above land surface Q Gallons of water pumped/bailed before sampling Field Analysis: pH —Specific Conductance uMhos Temp. Date Sample Colle�(ed 11• t l .G'7 Date Lab Sample Analyzed— LaboratoryName1(CA(roQ A N l�U IiCGLI (�10cXGi 1CS . Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge X Other Rotary Distributor CCl Odor Appearance '��-- Certification No. SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED n _YES NO COD — Coliform Coliform mo/I MF Fecal /100ml MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) —units TOC mg/I Chloride mg/1 Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance LiMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I AI - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I Ni - Nickel Pb - Lead Zn - Zinc Pesticides/Herbicides (Specify Compounds) mg/I mg/I mg/I ug/I Ug/I ug/I Other (Specify Compounds and C cantr tion unit ) `Ch�lOtrMV,e.f — -7ZOc c9/ I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and Q �% colloidal concentrations. (see #3 on back) 10,31 ` ` See back for instructions. S natur of ermitt (or Authorized Agent*) Date •* Submit blue and yellow copies only to address above. GW-59 REV. 8196 Well Location I - Loii " f ' Well Identification Number Well Depth _31S t Well Diameter 2. DDT Sample (Screened) Interval Ft. To Depth to Water Level _ ft. below measuring point (before sampling) Measuring point is W ft. above land surface ()C7 Gallons of water pumped/b before sampling Field Analysis: pH Specific Conductance uMhos Temp. Date Sample Colleted ` ( I Ig iz Date., Lab Sample Analyzed , t Laboratory Name w y its 'I' SAMPLES FOR METALS WE E COLLECTED UNFILTERED AND FIELD ACIDIFIED COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Lagoon Septic TanWDrain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Slu g Other Rotary Distributor Odor � Appearance Certification No. LIP, YES NO Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Be - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. /aQ&ab=:: Sig lure P rhittee r Authorized Agent`) Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Pesticides/Herbicides (Specify Compounds) ug/I ug/I ug/I Other (Specify Compounds and _,6encentr lion units) 1 Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) _I n- ' I ` l ( See back for instructions. Date '• Submit blue and yellow copies only to address above. GW-59 REV. 8/96 GROUNDWATER Q COMPLIANCE REP or Facility Name nt pen and press . nor addiLonal farm s Well Location Well Identification Numper Well Depth ZCo.O Well Diameter �0Sample (Screened) Interval Ft. To Depth to Water Level ft. below measuring point (before sampling) Measuring point is D ft. above land surface Gallons of water pumPed/bailed before sampling 2•00 Field Analysis: pH (a Specific Conductance uMhos Temp. Date Sample Collet;�d q; I i •g r7 n Da(e. Lab Sample Analyzed! Laboratory Name y L_ tRED - ' LLECTED NFIL SAMPLES FOR METAL S WER COTEAND FIELD ACIDIFIED COD mg/1 Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/1 pH (when analyzed) �- �I—units TOC mg/I Chloride mg/I Arsenic mg/1 Grease and Oils mg/1 Hardness: Total mg/1 Phenol mg/1 Sulfate mg/1 Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I .. PERMIT NUMBER: (REQUIR, _ Non -Discharge NPDES — TYPE OF DISPOSAL OPERATION BEING MONITORED — (REQUIRED) Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Slud e Other Rotary Distributor Odor Appearance Certification No. ua ( YES NO Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I. Mg - Magnesium mg/I Mn - Manganese mg/1 Na - Sodium mg/1 Ni - Nickel Pb - Lead Zn - Zinc Pesticides/Herbicides (Specify Compounds) Other (Specify Compounds and l C�llRentratidn unds i t -tn bd• mg/1 mg/I mg/I ug/I ug/I ug/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and f �% colloidal concentrations. (see #3 on back) / / o .3 ` 5 ` See back for instructions. Si natur o ermi e (or Authorized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 Well Location LA+ :500 LAB` OLI • q r L04° '7 Well Identification Number Mt.Well Depth 00 Well Diameter JOi, Sample (Screened) Interval Ft. To 2D Depth to Water Level '11 ,'7 [7 ft. below measuring paint (before sampling) Measuring point is Z ft. above land surface Gallons of water pum e bt�lied before sampling a,0y Field Analysis: . mr Specific Conductance IuMhos Temp. Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Slud Other Rotary Distributor °C _ Odor — Appearance - Date Sample Coll ted " 1 l t • " r Date Lab ample analyzed�_r r � rg I Laboratory Name ��'o M An(l�r�( �10FXC� l�10 Certification No. `—t SAMPLES FOR METALS WW�OLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/1 Phosphorus: Total as P mg/I AI - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/1 Cu - Copper - mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Pesticides/Herbicides (Specify Compounds) ug/I ug/I ug/I Other (Specify Compounds and Co entration units) i C�1lDt�0�l�Pt11e— iattg I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and �^ colloidal concentrations. (see #3 on back) /0 -3 / !G� �/ ( FSS ee back for instructions. S nat ee (or Authorized Agent*) Date ubmit blue and yellow copies only to address above. GW-59 REV. 8/96 DIVISION OF WATER QUALITY - GRGUNDWATER'SECTION GROUNDWATER QUALITY MONITORING: P.O. BOX29578 For additional forms RALEIGH; No27626.0578 COMPLIANCE REPORT FORM please write or call: (9119)733-3221 Tiny nr I lep a hnn.nnlnT npn Anil nrpSS Tlrn v- - Facili Well Well Well Deptl Measuring point is 3 .'Z ft. above land surface Gallons of water pumped/bailed before sampling Field Analysis: pH (o U:5-- Spgpidq, Conductance uMhos Temp. Date Sample Coll Date Lab Sample Analyzeed C.A • t �_c, Laboratory Na1�no it 11 IPC SAMPLES FOR METALS VVERt COLLECTED UNFILTERED AND FIELD ACIDIFIED COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) % units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I PERMIT NUMBER: (REQUIRE ) n Non -Discharge („ )a NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of SI dge Other Rotary Distributor Odor Appearance Certification No. YES —NO Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. A •;fir• - • ' • .. Ni - Nickel Pb - Lead mg/I mg/I Zn - Zinc Pesticides/Herbicides (Specify Compounds) mg/I ug/I ug/I ug/I Other (Specify Compounds and C I nitration units -f In two -1 Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) O, 3 r ` See back for instructions. Date •* Submit blue and yellow copies only to address above- GW-59 REV. 8/96 GROUNDWATER QU COMPLIANCE REPO Facility Name Addressy I Ln Well Location I0i Well Identification I Well Diameter Depth to Water Let Measuring point is. Gallons of water pL Field Analysis: pH or Use a ONITORINC r` -For additional please write o press before sampling 2Z•0r7 Specific Conductance � uMhos Temp. ^-5 P.o.•BOX ;29578� P <. )ns RALEIGH; NO 27628 057B.' q dl ..,'•„ , '. (9t9)733,-3221 PERMIT NUMBER:(REQUSRF,f)] ����� Non -Discharge LaYY�� NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) - . .Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Slu e Other Rotary Distributor Odor �— Appearance I — Date Sample ColleS�d ` ` `t' Date Lab Sa ple Analyzed r Laboratory Name l,C 06pyn (1'ilyhen� �hfirQlfX1PS Certification No. SAMPLES FOR METALS WEFT COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed)� units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I AI - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I Ni - Nickel Pb - Lead mg/I mg/I Zn -Zinc Pesticides/Herbicides (Specify Compounds) mg/I ug/I ug/I ug/I Other (Specify Compounds and Concentration units) 1�� r � lo�r�c3f-hrzne - 1 I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and ) r� colloidal concentrations. (see #3 on back) r Seeback for instructions. Si nature f ermitt (or Authorized Agent*) Date Submit blue and yellow copies only to address above. GW-59 REV. 8/96 Facili Well Well Well Deptl Measuring point is—ft. above land surface Gallons of water pumped/b tied before sampling — Field Analysis: Specific Conductance uMhos Temp. PERMIT NUMBER: (REQu1RE[�, �,���n� , Non -Discharge I' 'I NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Draih Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of SI d e Other Rotary Distributor Odor Appearance Date Sample Colle d I I e Lab ample Anay etl t• tn, -t f u�y Laboratory Name - I r1��ril (y�+� �te5 Certification No. z) SAMPLES FOR METALS W_. •E COLLECTED UNFILTERED AND FIELD ACIDIFIEE�- YES NO COD Coliform Coliform MF Fecal MF Total (Note: Use MPN method for highly turbid samples) _ mg/I /100m] /100m1 Dissolved Solids: Total mg/I pH (when analyzed) units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N Nitrate (N08) as N_ Phosphorus: Total as P AI - Aluminum Ba,- Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Na - Sodium mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Pesticides/Herbicides (Specify Compounds) ug/I ug/I ug/I Other (Specify Compounds and CoijQentration units) �11i �i1 7-t�s7 I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) 1 ✓ \ (v �( C f� See back for instructions. igriatu f erm• tee (or Authorized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 V" DIVISION OF WATER QUALITY, -;;GROUNDWATER SECTION " GROUNDWATER QUALITY MONITORINGFor '�onal s addirite Po eox?ss7a RALE(GH, INC 7826 0578 ^ COMPLIANCE REPORT. FORMplease6 or ea l z 19) 733 3zzt ; e ; y Type or Use a ball-point pen and press firmly. - , . PERMIT NUMBER: (REQUIF�Ep Non Facility Name S -Discharge Address t1 NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED r County o n yr Well Location (REQUIRED) Lagoon Septic Tank/Drain Field Well Identification Number ell Depth �,� . Ft. tt Spray Field Subsurlace. Low -Pressure Well DiameterSample (Screened) Interval Ft. To 47) Ft. Piping (LPP) Depth to Water Level 902 M(o ft. below measuring point (before sampling) Land Application of slu�gg other Measuring point is ft. above land surface � — ' Rotary Distributor Gallons of water pumped bailed before sampling � oC — Field Analysis: pH S ecific Conductance uMhos Temp. - S Odor Appearance Dale Sample Coll d (.I '� Date Lab Sa pie Analyzed l Laboratory Name ._ Certification No. SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/I Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc mg/I (Note: Use MPN method for highly turbid samples) Al - Aluminum mg/I Pesticides/Herbicides Dissolved Solids: Total mg/I Ba - Barium mg/I (Specify Compounds) pH (when analyzed) (o, ` 9 - units Ca - Calcium mg/I ug/I TOC mg/I Cd - Cadmium mg/I ug/I Chloride mg/I Chromium: Total mg/I ug/I Arsenic mg/I Cu - Copper mg/I Other (Specify Compounds and. Grease and Oils mg/I Fe - Iron mg/I central units �rCVt IMEC — (QaU(� /1 Hardness: Total mg/I Hg - Mercury mg/I l Phenol mg/I K- Potassium mg/I •J Sulfate mg/I Mg - Magnesium mg/I Specific Conductance uMhos Mn - Manganese mg/1 Total Ammonia mg/I Na - Sodium mg/I TKN as N mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and concentrations. (see #3 on back) 1��(\colloidal I o.31 q� Zf}^V t v \ , * See back for instructions. Si ature f ermitt (or Authorized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 GROUNDWATER QUALITY MONITORING-., COMPLIANCE REPORT FORM For additional forms ,. please write or call: Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIR li__n � Y1Ci5� 1 Non -Discharge �Q`�r7�96 Facility Name �� Address IGicr NPDES - L.n, 01 n n i2 C C. Counn� C: �C(l C( TYPE OF DISPOSAL OPERATION BEING MONITORED —--a .. (REQUIRED) - Well Location t K v' o i"I f t Well Identification Number AA — IU Well Depth Q,00 F. Well Diameter U-00Sample (Screened) Interval Ft. To _ja.L1_2Ft. Depth to Water Level 16-.'?>q ft. below measuring point (before sampling) Measuring point is"�;_7_.t`Zft. above land surface Gallons of water pumped/bailed before sampling �S Field Analysis: pH (,9�0�7 Specific Conductance uMhos Temp. Date Sample Colle ed Ct Date Lab Sample Analyzed I, Laboratory Name - 1 rn SAMPLES FOR METALS WE14E COLLECTED UNFILTERED AND FIELD ACIDIFIED COD Coliform Coliform MF Fecal MF Total mg/I /100ml /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) units TOC mg/1 Chloride mg/1 Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge Other Rotary Distributor Odor — Appearance Certification No. WeI ( YES —NO Nitrite (NO2) as N mg/1 Nitrate (NO3) as N mg/1 Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca- Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu.- Copper mg/I Fe - Iron mg/1 Hg - Mercury mg/1 K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/1 Ni - Nickel Pb - Lead mg/I mg/I Zn - Zinc Pesticides/Herbicides (Specify Compounds) mg/I ug/I ug/I ug/I Other (Specify Compounds and �Cc centrat'IIon units) v'i C h ID�y.�FY�P�1Q — Z2uq 1 I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) —�V I O `� .�' / • ' See back for instructions. S gnatur of ermitte (or Authorized Agent') Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 GROUNDWATER or Facility pen and press Well Location w-t_ - t / ' r )Ll- SIT? Ulf.0 ""!4 - ' - � ' Well Identification Number t2C-ts Well Depth 70 • S Ft. Well Diameter •00"'Sample (Screened) Interval Ft. To Z-SFt. Depth to Water Level eft. below measuring point (before sampling) Measuring point is Z- ft. above land surface Gallons of water pumped/b ' ed before sampling Lo, OLD Field Analysis: pH Specific Conductance _ uMhos Temp. Date Sample Collecjed Date Lab Sample Analyzed G Laboratory Name t'/ar L SAMPLES FOR METALS COD Coliform: MF Fecal Coliform: MF Total (Note: Use MPN method for highly turbid samples) _ mg/I /100ml /100ml Dissolved Solids: Total mg/I pH (when analyzed) ri .LI2 units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I PERMIT NUMBER: (REQUIR�E�l Non -Discharge C-u, 0:02"1Q8 NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED 4� 3r, (REQUIRED) Lagoon Septic Ta k/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of SI d e Y_ Other Rotary Distributor Nitrite (NO2) as N — Nitrate (NO3) as N_ Phosphorus: Total as P Al - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron _ Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Na - Sodium Appearance — Certification No. UH ( YES — NO mg/I mg/I mg/I Ni - Nickel Pb - Lead Zn - Zinc mg/I mg/I mg/I mg/I Pesticides/Herbicides mg/I mg/I (Specify Compounds) Ug/I mg/I ug/I mg/I ug/I mg/I Other (Specify Compounds and mg/I Concentration units) mg/I mg/I mg/I mg/I mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and /(� colloidal concentrations. (see #3 on back) zEX U 10 .J 1 �" See back for instructions. Sigbatur,f ermitte (or Authorized Agent') Date •• Submit blue and yellow copies only to address above. GW-59 REV. 8/96 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility A( For additional forms please write or call: Type or Use a ball-point pen and press firmly. Well Location Well Identification Number Well Depth SD,00 Ft. Well Diameter- L d2Sample (Screened) Interval Ft. To5D.60 Ft. Depth to Water Level Z&LAD ft. below measuring point (before sampling) Measuring point is 1. G ft. above land surface 6-5-1Gallons of water pum ed/ ailed before sampling CIO Field Analysis: pH I Specific Conductance 11uMhos TempzO ,'7 oC Date Sample Colles(ecl Date Lab Sample Analyzed G ' (t Laboratory Name ✓ '( I L c-ci it SAMPLES FOR METALS Wl E COLLECTED UNFILTERED AND FIELD ACIDIFIED COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total /100m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) units TOG mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/1 TKN as N mg/1 Nitrite (NO2) as N Nitrate (NO3) as N Phosphorus: Total Al -Aluminum_ Ba - Barium Ca - Calcium_ Cd - Cadmium_ Chromium: Total _ Cu - Copper Fe - Iron Hg - Mercury_ K - Potassium _ Mg - Magnesium _ Mn - Manganese _ Na - Sodium PERMIT NUMBER: ( MI � MOP) Non -Discharge NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED IREOUIREDI Lagoon Septic TanMDrain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of SI dge Other Rotary Distributor Odor Appearance '— Certification No. 48 YES NO mg/I mg/I mg/I Ni - Nickel Pb - Lead Zn - Zinc mg/1 mg/I mg/I mg/I Pesticides/Herbicides mg/I mg/I (Specify Compounds) ug/I mg/I ug/I mg/I ug/I mg/I Other (Specify Compounds and mg/I mg/I Coffin entration units) l �i( Vl IW✓Yl — IZUO L Q I mg/I mg/I mg/I mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) ZM A I O ` St 19 See back for instructions. Ka ur of ermitt e or Authorized Agent') Date " Submit blue and yellow copies only to address above. GW-59 REV. 8/96 GROUNDWATER QUALITY MONITORING COMPLIANCE REPORTTORM Facil Well Well Well Dept] Measuring point is 2 , lO ft. above land surface Gallons of water pumped/bailed before sampling 4�2� • C)C) Field Analysis: pH Specific Conductance uMhos Temp, Date Sample Collept4�d Date Lab Sa)nple Analyzed — DIVISION OF W For additional forms _ please write or call: Tvpe or Use a ball-point pen and press firmly. Laboratory Name c a � r � > r f SAMPLES FOR METALS W E COLLECTED UNFILTERED AND FIELD ACIDIFIED COD mg/I Coliform: MF Fecal /loom] Coliform: MFTotal /loom] (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) S-3units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I PERMIT NUMBER: (REQUIREC1hCM��98 Non -Discharge ��1�11 NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED . . (REQUIRED) Lagoon Septic Tank/Drain, Field Spray Field _ Subsurface Low -Pressure Piping (LPP) Land Application of Sludge -!>d— Other Rotary Distributor Odor Appearance Certification No.� YES NO Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I Ni - Nickel Pb - Lead Zn - Zinc Pesticides/Herbicides (Specify Compounds) mg/I mg/I mg/I ug/I ug/I ug/I Other (Specify Compounds and Con entration units) % I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and r �% colloidal concentrations. (see #3 on back) O`� f '� r See back for instructions. Siqtatur bf �rmitte (or Authorized Agent') Date •• Submit blue and yellow copies only to address above. GW-59 REV. 8/96 GROUNDWATER' COMPLIANCE RE Facility Name TC Address—P t; ai DI For.additional forms or Use a ball-point pen and press firmly. LQS -�n_G - Well Location Well Identification Number Well Depth 110-1 Well Diameteramplp (Screened) Interval Ft. To QC Depth to Water Level ft. below measuring point (before sampling) Measuring point is 1, Q0 ft. above land surface �,-) Gallons of wat Field Analysis: Date Sample ( Laboratory Name_l-LUf SAMPLES FOR METALS COD Coliform: Coliform: mn/I MF Fecal /loom[ MF Total /loom[ (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) S.foLo units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I PERMIT NUMBER: (REQUIRED Non -Discharge I Cr'-)n�9a NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge - Other Rotary Distributor Appearance — Certification No. YES NO Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper - mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Pesticides/Herbicides (Specify Compounds) ug/I ug/I ug/I Other (Specify Compounds and Con entratioq units)_ 1, �,,�/-� I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and q colloidal concentrations. (see #3 on back) o/ See back for instructions. Si atur of P rmitte (or Authorized Agent`) Date *' Submit blue and yellow copies only to address above. GW-59 REV. 8/96 nal GROUNDWATER QUALITY MONITORING For nAdiha...to .. a'. Type or Facility Name pen Well Location Well Identification Number Well Depth Ft. Well Diameter — Sample (Screened) Interval — Ft. To — Ft. Depth to Water Level ft. below measuring point (before sampling) Measuring point is ft. above land surface Gallons of water pumped/bailed before sampling �p rI Field Analysis: pH ZSpe if' Conductance uMhos Temp. � , I , Date Sample Collecte -1 -t ) -1 Date Lab Sample Analyzed Gj -lI O I Laboratory Name alit QM Gbs of I obax-ni"o Ifi?S SAMPLES FOR METALS WE COLLECTED UNFILTERED AND FIELD ACIDIFIED !, I COD Coliform: Coliform: mn/l MF Fecal /loom[ MF Total /l ooml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) (P r 2CP units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils %mg/I Hardness: Total mg/I Phenol mg/1 Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I PERMIT NUMBER: (REQUIREDIL� - 'Non -Discharge 1r.1(�2(�D'77�)8 NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic TanWDraih Field Spray'Field `` Subsurface Low -Pressure Piping (LPP) Land Application of Sludge X Other _ Rotary Distributor Odor _ Appearance Certification No. a fS YES NO Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/1 Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I Ni - Nickel Pb - Lead mg/1 mg/I Zn - Zinc Pesticides/Herbicides (Specify Compounds) mg/I ug/I ug/I ug/I Other (Specify Compounds and Concentration units) ''��icl�lor-o2-the✓IQ� � IC�»�r�l I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) See back for instructions. i na e oftermi ee'(or Authorized Agent*) Date **'Submit blue and yellow copies only to address above. GW-59 REV. 8/96 GROUNDWATER QUALITY MONITORING:,, For atlditfbnel forms COMPLIANCE REPORT FORM please write or call: a ball-point pen Facility Name A4 IL Address A� d Well Location Well Identification N press DIVISION OFWATER QUALITY -GROUNDWATER SECTION 'P.O. BOX.29578 RALEIGH; NC 27626.0518 •(919) M-3221 PERMIT NUMBER: (REQUIgE 6) 0r 1�� Non -Discharge WWiCa� NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Well Diameter Sample (Screened) Interval — Ft. To Ft. Spray Field e?�r-, 3e N ^ FxrLUF1J1- Well Depth — Ft. Subsurface Low -Pressure Piping (LPP) Depth to Water Level ft. below measuring point (before sampling) Land Application or sludge Measuring point is r ft. above land surface Z Rotary Distributor Other Gallons of water pumped/bailed before sampling Field Analysis: pH Specific Conductance --uMhos Temp. — oC Odor — Appearance Date Sample CoIlec d , 10-6 -Cc' Date Lab Sample Analyzed In -D --4Z Laboratory Name ��QCI'M�) Lc(� fCb�C� Certification No. I8 SAMPLES FOR METALS VVLAE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD Coliform: MF Fecal Coliform: MF Total _ mg/I /100ml /100m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) G�units TOC mg/I Chloride mg/1 Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Pesticides/Herbicides (Specify Compounds) ug/I ug/I ug/I Other (Specify Compounds and Concentration units) I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) i�/ `Y� )�� See back for instructions. gnatur of ermit ee (Or Authorized Agent') Date •• Submit blue and yellow copies only to address above. GW-59 REV. 8/96 LABORATORY ANALYTICAL RESULTS PARADIGM ANALYTICAL LABORATORIES, INC. 2627 Northchase Parkway S.E. Wilmington, North Carolina 28405 (910) 350-1903 fax (910) 350-1557 Mr. John Jester Date 09-29-97 Gulfstream Environmental PO Box 592 Wrightsville Beach, NC 28480 Report Number: G216-1 Client Project ID : 01-0997 Dear Mr. Jester: Enclosed are the results of the analytical services performed under the referenced project. Copies of this report and supporting data will be retained in our files for a period of five years in the event they are required for future reference. Any samples submitted to our laboratory will be retained for a maximum of thirty (30) days from date of this report unless other arrangements are requested. If there are any questions about the report or the services performed during this project, please call for assistance. We will be happy to answer any questions or concerns which you may have. JThank you for using Paradigm Analytical Labs for your analytical service projects. We look forward to working with you again on any additional needs which you may have. Sincerely, Paradigm Analytical Laboratories Laboratory Director Mark Randall North Carolina Wastewater Certification #481 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GCMS 624 Client Sample ID: MW-1 Date Analyzed: 9/15/97 Client Project ID: 01-0997 Analyzed By: WML Lab Sample ID: 29597 Date Collected: 9/11/97 Lab Project JD: G216-1 Date Received: 9/12/97 Matrix: Water Dilution: 40.0 Compound Quantitatlon Result Limit (ug/L) (ug/L) Benzene 40 BQL Bromochloromethane 40 BQL Bromoform 40 BQL Bromomethane 40 BQL Carbon tetrachloride 40 BQL Chlorobenzene 40 BQL Chloroethane 40 BQL 2-Chloroethyl vinyl ether 200 BQL Chloroform 40 BQL Chloromethane 40 BQL - Dibromochloromethane 40 BQL 1,2-Dichlorobenzene 40 BQL 1,3-Dichlorobenzene 40 BQL 1,4-Dichlorobenzene 40 BQL 1,1-Dichloroethane 40 BQL 1,1-Dichloroethene 40 BQ L 1,2-Dichloroethane 40 BQL _ trans-1,2-Dichloroethene 40 BQL 1,2-Dichloropropane 40 BQL cis-1,3-Dichloropropene trans-1,3-Dichloropropene 40 40 BQL BQL Dilsopropyl ether (DIPE) 40 BQL Ethylbenzene 40 BQL Methylene chloride 200 BQL Methyl-tert-butyl ether (MTBE) 40 BOL 1,1,2,2-Tetrachloroethane 40 BQL Tetrachloroethene 40 BQL Toluene 40 BQL — Trichloroethene 40 560 1,1,1-Trichloroethane 40 BQL 1,1,2-Trichloroethane 40 BQL Trichlorofluoromethane 40 BQL Vinyl chloride 40 BQL m-,p-Xylene 80 BQL o-Xylene 40 BQL Surrogate Standards Surrogate Surrogate Percent Added Result Recovery Compound (ug/L) (ug/L) 1,2-Dichloroethane-d4 10.0 10.0 100 Toluene -dB i0,0 9.9 gg Bromorluorobenzene 10.0 9.3 93 Comments: All results are corrected for dilution. Flags: BQL = Below Quantltatlon Limit Reviewed By: 1JA�- Pego 1 of 1 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GCMS 624 Client Sample ID: MW-2 Date Analyzed: 9115/97 Client Project ID: 01-0997 Analyzed By: WML Lab Sample ID: 29598 Date Collected: 9/11/97 Lab Project ID: G216-1 Date Received: 9/12/97 Matrix: Water Dilution: 80.0 Compound Quantltatlon Result Lim It (ug/L) (ug/L) Benzene 80 BQL Bromochloromethane 80 BQL Bromoform 80 BQL Bromomethane 80 BQL Carbon tetrachloride Chlorobenzene 80 80 BQL BQL Chloroethane 80 BQL 2-Chloroethyl vinyl ether 400 BQL Chloroform 80 BQL ' Chloromethane 80 BQL Dlbromochloromethane 80 BQL 1,2-Dichlorobenzene 80 BQL 1,3-Dichlorobenzene 80 BQL 1,4-Dichlorobenzene 80 BQL 1,1-Dichloroethane 80 BQL —. 1,1-Dichloroethene 80 BQL 1,2-Dichloroethane 80 BQL 'J trans-1,2-Dichloroethene 80 BQL 1,2-Dichloropropane 80 BQL cis-1,3-Dlchloropropene 80 BQL trans-1,3-Dichloropropene 80 BQL '- Dilsopropyl ether (DIPE) 80 BQL _ Ethylbenzene 80 BQL Methylene chloride 400 BOL Methyl-tert-butyl ether (MTBE) 80 BQL 1,1,2,2-Tetrachloroethane 80 BQL t Tetrachloroethene 80 BQL Toluene 80 BQL Trichloroethene 80 1400 1,1,1-Trichloroethane 80 BQL 1,1,2-Trichloroethane 80 BQL Trlchlorolluoromethane 80 BQL Vinyl chloride 80 BQL m-,p-Xylene 160 BQL o-Xylene 80 BQL Surrogate Standards Surrogate Surrogate Percent " Added Result Recovery Compound (ug/L) (ug/L) 1,2-Dichloroethane-d4 10.0 9.8 98 Toluene-d8 10.0 9,9 99 Bromofluorobenzene 10.0 9.4 94 Comments: All results are corrected for dilution. Flags: BQL = Below Quantltatlon Limit Reviewed By: k- Page 1 of 1 PARADIGM ANALYTICAL LABORATORIES, INC. .I Results for Volatiles .- by GCMS 624 Client Sample ID: MW-3 Date Analyzed: 9/15/97 Client Project ID: 01-0997 Analyzed By: WML Lab Sample ID: 29599 Date Collected: 9/11/97 Lab Project ID: G216-1 Date Received: 9/12/97 Matrix: Water Dilution: 10.0 Compound Quantitatlon Result �- Limit (ug/L) (ug/L) Benzene 10 BQL Bromochloromethane 10 BQL Bromoform 10 BQL Bromomethane 10 BQL Carbon tetrachloride 10 BQL Chlorobenzene 10 BQL Chloroethane 10 BQL 2-Chloroethyl vinyl ether 50 BQL - Chloroform 10 BQL Chloromethane 10 BQL Dibromochloromethane 10 BQL 1,2-Dichlorobenzene 10 BQL 1,3-Dichlorobenzene 10 BQL 1,4-Dichlorobenzene 10 BQL ` 1,1-Dichloroethane 10 BQL 1,1-Dichloroethene 10 BQL 1,2-Dichloroethane 10 BQL trans-1,2-Dichloroethene 10 BQL 1,2-Dlchloropropane 10 BQL ' cis-1,3-Dlchloropropene 10 BQL f ttans-1,3-Dlchloropropene 10 BQL Diisopropyl ether (DIPE) 10 BQL Ethylbenzene 10 BQL Methylene chloride 50 BQL Methyl-tert-butyl ether (MTBE) 10 BQL 1,1,2,2-Tetrachloroethane 10 BQL Tetrachloroethene 10 BQL Toluene 10 BQL —' Trichloroethane 10 150 1,1,1-Trichloroethane 10 BQL 1,1,2-Trichloroethane 10 BQL Trichlorofluoromethane 10 BQL Vinyl chloride 10 BQL m-,p-Xylene 20 BQL o-Xylene 10 BQL Surrogate Standards Surrogate Surrogate Percent Added Result Recovery — Compound (ug/L) (ug/L) 1,2-Dichloroethane-d4 10.0 10.3 103 Toluene-d6 10.0 10.0 100 Bromofluorobenzene 10.0 9.4 94 Comments: All results are corrected for dilution. - Flags: _ BQL =.Below Quantitatlon Limit Reviewed By: K*. Pape 1 of 1 PARADIGM .I ANALYTICAL LABORATORIES, INC. J Results for Volatiles by GCMS 624 Client Sample ID: MW4 Date Analyzed: 9/22/97 Client Project ID: 01-0997 Analyzed By: WML Lab Sample ID: 29600 Date Collected: 9/11197 Lab Project ID: G216-1 Date Received: 9/12/97 Matrix: Water Dilution: 400.0 Compound Benzene Bromochloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroelhyl vinyl ether Chloroform Chloromethane D Ib romoch to ro methane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,1-Dichloroethane 1,1-Dichloroelhene 1,2-Dichloroethane trans-1,2-Dichloroethene 1,2-Dichloropropane cis-1,3-Dichloropropene trans-1, 3-Dichloropropene Dlisopropyl ether (DIPE) Ethylbenzene Methylene chloride Methyl-tert-butyl ether (MTBE) 1,1,2,2-Tetrachloroethane Tetrachloroethane Toluene Trichloroethene 1,1,1-Trichloroetha ne 1,1, 2-Trichloroethane Trichlorolluorometha ne Vinyl chloride m-,p-Xylene o-Xylene Surrogate Standards Compound 1,2-Dichloroethane-d4 Toluene-d8 _ Bromolluorobenzene Comments: All results are corrected for dilution. Flags: BQL = Below Quantltatlon Limit Quantitatlon Limit(ug/L) 400 400 400 400 400 400 400 2000 400 400 400 400 400 400 400 400 400 400 400 400 400 400 400 2000 400 400 400 400 400 400 400 400 400 800 400 Surrogate Added (ug/L) 10.0 10.0 10.0 Surrogate Result (ug/L) 9.5 10.3 10.1 Result (ug/L) BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL 5500 BQL BQL BQL BQL BQL BQL Percent Recovery 95 103 101 Reviewed By: AAn— Pap 1 of 1 PARADIGM I ANALYTICAL LABORATORIES, INC. Results for Volatiles - by GCMS 624 Client Sample ID: MW-5 Date Analyzed: 9/16/97 Client Project ID: 01-0997 Analyzed By: WML Lab Sample ID: 29601 Date Collected: 9111/97 Lab Project ID: G216-1 Date Received: 9112/97 Matrix: Water Dilution: 100.0 • Compound Quantitatlon Result Limit (ug/L) (ug/L) Benzene 100 BQL Bromochloromethane 100 BQL 'Bromoform 100 BQL Bromomethane 100 BQL Carbon tetrachloride 100 BQL Chlorobenzene 100 BQL Chloroethane ` 100 BQL 2-Chloroethyl vinyl ether Soo BQL Chloroform 100 BQL 1 Chloromethane 100 BQL Dibromochloromethane 100 BQL 1,2-Dichlorobenzene 100 BQL + 1,3-Dichlorobenzene 100 BQL J 1,4-Dichlorobenzene 100 BQL 1,1-Dichloroethane 100 BQL _ 1,1-Dichloroethene 100 BQL 1,2-Dichloroethane 100 BQL trans-1,2-Dichloroethene 100 BQL 1,2-Dichloropropane 100 BQL cis-1,3-Dichloropropene 100 BQL trans-1,3-Dichloropropene 100 BQL Dilsopropyl ether (DIPE) 100 BQL Ethyibenzene 100. BQL Methylene chloride 500 BQL Methyl-tert-butyl ether (MTBE) 100 BQL 1,1,2, 2-Tetrachloroethane 100 BQL Telrachloroethene 100 BQL Toluene 100 BQL Trichloroelhene 100 1600 1,1,1-Trichloroethane 100 BQ L 1,1, 2-Trichloroethane 100 BQL Trichlorofluoromethane 100 BQL Vinyl chloride 100 BQL - • m-,p-Xylene 200 BQL o-Xylene 100 BQL Surrogate Standards Surrogate Surrogate Percent Added Result Recovery Compound (ug/L) (ug/L) 1,2-Dichloroethane-d4 10.0 9.8 96 Toluene-d6 1,0,0 9,6 98 Bromoliuorobenzene 10.0 9.3 93 Comments: All results are corrected for dilution. Flags: BQL = Below Quantitatlon Limit Reviewed By: Z^i�_ Pago 1 of 1 - PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles -- by GCMS 624 Client Sample ID: MW-6 Date Analyzed: 9122197 Client Project ID: 01-0997 Analyzed By: WML Lab Sample ID: 29602 Date Collected: 9111/97 Lab Project ID: G216-1 Date Received: 9/12/97 Matrix: Water Dilution: 80.0 Compound Quantltatlon Result Llmlt (ug/L) (ug/L) Benzene 80 BQL Bromochloromethane 80 BQL Bromoform 80 BQL Bromomethane 80 BQL Carbon tetrachloride 80 BQL — Chlorobenzene 80 BQL Chloroethane 80 BQL 2-Chloroethyl vinyl ether 400 BQL Chloroform 80 BQL Chioromethane 80 BQL _ Dibromochloromethane 80 BQL 1,2-Dichlorobenzene 80 BQL 1,3-Dichlorobenzene 80 BQL 1,4-Dichlorobenzene 80 BQL 1,1-Dichloroethane 80 BQL M-Dichloroethene 80 BQL 1,2-Dichloroethane 80 BQL trans-1,2-Dichloroethene 80 BQL 1,2-Dlchloropropane 80 BQL cis-1,3-Dlchloropropene 80 BQL trans-1,3-Dlchloropropene 80 BQL Dlisopropyl ether (DIPE) 80 BQL Ethylbenzene J 80 BQL Methylene chloride 400 BQL Methyl -tart -butyl ether (MTBE) 80 BQL 1,1,2,2-Tetrach loroelhane 80 BQL - Tetrachloroelhene 80 BQL ( Toluene 80 BQL _ Trichloroethane 80 720 1,1,1-Trichloroethane 80 BQL 1,1, 2-Trichloroethane 80 BQL Trichlorolluoromethane 80 BQL Vinyl chloride 80 BQL _ m-,p-Xylene 160 BQL o-Xylene 80 BQL Surrogate Standards Surrogate Surrogate Percent Added Result Recovery — Compound (ug/L) (ug/L) 1,2-Dichloroethane-d4 10.0 10.1 101 Toluone-d8 10.0 10.4 104 Bromofluorobenzene 10.0 10.5 105 Comments: All results are corrected for dilution. Flogs: BQL = Below Quantilallon Limit Reviewed By: /)-- Pepe 1 of 1 PARADIGM ANALYTICAL LABORATORIES, INC. L_ Results for Volatiles by GCMS 624 _ Client Sample ID: MW-7 Date Analyzed: 9/22/97 Client Project ID: 01-0997 Analyzed By: WML Lab Sample ID: 29603 Date Collected: 9/11/97 Lab Project,ID: G216-1 Date Received: 9/12/97 Matrix: Water Dilution: 100.0 Compound Quantitatlon Result _ Lim It (ug/L) (ug/L) Benzene 100 BQL Bromochloromethane 100 BQL Bromoform 100 BQL Bromomelhane 100 BQL Carbon tetrachloride 100 BQL Chlorobenzene 100 BQL Chloroethane 100 BQL 2-Chloroelhyl vinyl ether 500 BQL Chloroform 100 BQL i Chloromethane 100 BQL Dibromochloromethane 100 BQL 1,2-Dlchlorobenzene 100 BQL 1,3-Dlchlorobenzene 100 BQL 1,4-Dlchlorobenzene 100 BQL 1,1-Dichloroethane 100 BQL 1,1-Dlchloroethene 100 BQL 1,2-Dichloroethane 100 BQL trans-1,2-Dichloroethene 100 BQL 1,2-Dichloropropane 100 BQL cis-1,3-Dichloropropene 100 BQL trans-1,3-Dichloropropene 100 BQL - Diisopropyl ether (DIPE) 100 BQL Ethylbenzene 100 BQL Methylene chloride 500 BQL Methyl-tert-butyl ether (MTBE) 100 BQL 1,1,2,2-Tetrachloroethane 100 BQL Tetrachloroethene 100 BQL Toluene 100 BQL _ Trichloroethene 100 1100 1,1,1-Trichloroethane 100 BQL 1,1, 2-Trichloroethane 100 BQL Trichlorolluoromethane 100 BQL Vinyl chloride 100 BQL m-, p-Xylene 200 BQL o-Xylene 100 BQL Surrogate Standards Surrogate Surrogate Percent Added Result Recovery Compound P (ug/L) (ug/L) 1,2-Dichloroethane-d4 10.0 10.1 101 Toluene-d0 10.0 10.5 105 Bromoflucrobenzene 10.0 10.1 101 Comments: All results are corrected for dilution. Flags: BQL = Below Quantltation Limit Reviewed By: 4N.. Page 1 or 1 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GGMS 624 Client Sample ID: MW-8 Date Analyzed: 9/15/97 Client Project ID: 01-0997 Analyzed By: CKC Lab Sample ID: 29604 Date Collected: 9111/97 Lab Project ID: G216-1 Date Received: 9/12/97 Matrix: Water Dilution: 1.0 Compound Quantitatlon Result Limit (ug/L) (ug/L) Benzene 1 BQL Bromochloromethane 1 BQL Bromoform 1 BQL Bromomethane 1 BQL Carbon tetrachloride 1 BQL Chlorobenzene 1 BQL Chloroethane 1 BQL 2-Chloroethyl vinyl ether 5 BQL Chloroform 1 BQL Chloromethane 1 BQL Dibromochloromethane 1 BQL 1,2-Dichlorobenzene 1 BQL 1,3-Dichlorobenzene 1 BQL 1,4-Dichlorobenzene 1 BQL 1,1-Dichloroethane 1 BQL 1,1-Dichloroethene 1 BQ L 1,2-Dichloroethane 1 BQL trans-1,2-Dichloroethene 1 BQL 1,2-Dichloroprdpane 1 BQL cis-1,3-Dichloropropene 1 BQL trans-1,3-Dichloropropene 1 BQL Dlisopropyl ether (DIPE) 1 BQL Ethylbenzene 1 BQL Methylene chloride 5 BQL Methyl -tart -butyl ether (MTBE) 1 BQL 1,1,2,2-Tetrachloroethane 1 BQL Tetrachloroethene 1 BQL Toluene 1 BQL Trichloroethene 1 18 1,1,1-Trichloroelhane 1 BQL 1,1,2-Tiichloroethane 1 BQL Trichlorofluoromethane 1 BQL Vinyl chloride 1 BQL m-,p-Xylene 2 BQL o-Xylene 1 BQL Surrogate Standards Surrogate Surrogate Percent Added Result Recovery Compound (ug/L) (ug/L) 1,2-Dichloroethane-d4 10.0 9.4 94 Toluene-d8 10.0 9.7 97 Bromolluorobenzene 10.0 9.7 97 Comments: All results are corrected for dilution. Flags: BQL = Below Quantitatlon Limit Reviewed By: tw+ Page 1 of 1 PARADIGM ANALYTICAL LABORATORIES, INC. J Results for Volatiles ._ by GCMS 624 Client Sample ID: MW-9 Date Analyzed: 9115/97 Client Project ID: 01-0997 Analyzed By: CKC Lab Sample ID: 29605 Date Collected: 9111197 Lab Project ID: G216-1 Date Received: 9/12/97 Matrix: Water Dilution: 1.0 Compound Quantltatlon Result Limit (ug/L) (ug/L) Benzene 1 BQL Bromochloromethane 1 BQL Bromoform 1 BQL Bromomethane 1 BQL Carbon tetrachloride 1 BQL Chlorobenzene 1 BQL Chloroethane 1 BQL 2-Chloroethyl vinyl ether 5 BQL Chloroform 1 BQL Chloromethane 1 BQL Dibromochloromethane 1 BQL 1,2-Dichlorobenzene 1 BQL 1,3-Dichlorobenzene 1 BQL J 1,4-Dichlorobenzene 1 BQL 1,1-Dichloroelhane 1 BQL _ 1,1-Dichloroethene 1 BQL 1,2-Dichloroethane 1 BQL trans-1,2-Dichloroethene 1 BQL 1,2-Dichloropropane 1 BQL -I cis-1,3-Dichloropropene 1 BQL trans-1,3-Dichloropropene 1 BQL _ Dilsopropyl ether (DIPE) 1 BQL Ethylbenzene 1 BQL Methylene chloride 5 BQL Methyl-tert-butyl ether (MTBE) 1 BQL —" 1,1,2,2-Tetrachloroethane 1 BQL Tetrachloroelhene 1 BQL Toluene 1 BQL _ Trichloroethene 1 17 1,1,1-Trichloroethane 1 BQL 1,1,2-Trichloroethane 1 'BQL Trichlorofluoromelhane 1 BQL Vinyl chloride 1 BQL _ m-,p-Xylene 2 BQL o-Xylene 1 BQL Surrogate Standards Surrogate Surrogate Percent Added Result Recovery Compound (ug/L) (ug/L) 1,2-Dichloroelhane-d4 10.0 9.5 95 Toluene-d6 10.0 9.3 93 Bromofluorobenzene 10.0 9.9 99 Comments: All results are corrected for dilution. Flags: BQL = Below Quantltatlon Limit Reviewed By: (a=_ Pape 1 of 1 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GCMS 624 Client Sample ID: MW-10 Date Analyzed: 9/16/97 Client Project ID: 01-0997 Analyzed By: WML Lab Sample ID: 29606 Date Collected: 9/11/97 Lab Project ID: G216-1 Date Received: 9/12/97 Matrix: Water Dilution: 50.0 Compound Quantitatlon Result Limit (ug/L) (ug/L) Benzene 50 BQL Bromochloromethane 50 BQL Bromoform 5o BQL Bromomethane 50 BQL Carbon tetrachloride 50 BQL Chlorobenzene 50 BQL Chloroethane 50 BQL 2-Chloroethyl vinyl ether 250 BQL _ Chloroform 50 BQL Chloromethane 50 BQL Dibromochloromethane 50 BQL 1,2-Dichlorobenzene 50 BQL 1,3-Dichlorobenzene 50 BQL IJI 1,4-Dichlorobenzene 50 BQL 1,1-Dichloroethane 50 BQL _ 1,1-Dichloroethene 50 BQL 1,2-Dichloroethane 50 BQL trans-1.2-Dichloroethene 50 BQL 1,2-Dichloropropane 50 BQL -I cls-1,3-Dlchloropropene 50 BQL trans-1,3-Dlchloropropene 5o BQL Dlisopropyl ether (DIPE) 50 BQL Ethylbenzene 50 BQL Methylene chloride 250 BQL Methyl-tert-butyl ether (MTBE) 50 BQL 1,1, 2,2-Tetrachloroethane 50 BQL Tetrachloroethene Toluene 50 50 BQL BQL Trichloroelhene • 50 580 1,1,1-Trichloroethane 50 BQ L 1,1,2-Trichloroethane so BQL Trichlorofluoromethane 50 BQL Vinyl chloride 50 BQL m-,p-Xylene 100 BQL o-Xylene 50 BQL I Surrogate Standards Surrogate Surrogate Percent Added Result Recovery IJ Compound (ug/L) (ug/L) 1,2-Dichioroethane-d4 10.0 10.3 103 Toluene-d8 10.0 10.1 101 Bromofluorobenzene 10.0 9.3 93 Comments: All results are corrected for dilution. Flags: BQL = Below Quantitatlon Limit Reviewed By: n _ Page 1 of 1 a PARADIGM ANALYTICAL LABORATORIES, INC. J Results for Volatiles - by GCMS 624 Client Sample ID: MW-11 Date Analyzed: 9/16/97 Client Project ID: 01-0997 Analyzed By: WML Lab Sample ID: 29607 Date Collected: 9/11/97 Lab Project ID: G216-1 Date Received: 9/12/97 Matrix: Water Dilution: 20.0 Compound Quantltation Result Limit (ug/L) (ug/L) Benzene 20 BQL Bromochloromethane 20 BQL Bromoform 20 BQL Bromomethane 20 BQL Carbon tetrachloride 20 BQL Chlorobenzene 20 BQL Chloroethane 20 BQL 2-Chloroethyl vinyl ether 100 BQL Chloroform 20 BQL Chloromethane 20 BQL Dibromochloromethane 20 BQL 1,2-Dichlorobenzene 20 BQL 1 1,3-Dichlorobenzene 20 BQL 1,4-Dichlorobenzene 20 BQL '— 1,1-Dichloroethane 20 BQL _ 1,1-Dichloroethene 20 BQL 1,2-Dichloroethane 20 BQL -._ trans-1,2-Dichloroethene 20 BQL 1,2-Dichloropropane 20 BQL cis-1,3-Dichloropropene 20 BQL trans-1,3-Dichloropropene 20 BQL -- Dllsopropyl ether (DIPE) 20 BQL Ethyibenzene 20 BQL Methylene chloride 100 BQL Methyl-tert-butyl ether (MTBE) 20 BQL 1,1,2,2-Tetrachloroethane 20 BQL Tetrachioroethene 20 BQL Toluene 20 BQL -- Trcchloroethene 20 410 1,1,1-Trlchloroethane 20 BQL 1,1,2-Trlchloroethane 20 BQL Trlchlorofluoromethane 20 BQL Vinyl chloride 20 BQL m-,p-Xylene 40 BQL o-Xylene 20 BQL Surrogate Standards Surrogate Surrogate Percent Added Result Recovery Compound (ug/L) (ug/L) 1,2-Dichloroethane-d4 10.0 9.9 99 Toluene -de 10.0 10.1 101 Bromofluorobenzene 10.0 9.2 92 Comments: All results are corrected for dilutlon. Flags: BQL = Below Quantitatlon Llmit Revlewed By: hag,` Page 1 of 1 PARADIGM ANALYTICAL LABORATORIES, INC. y Results for Volatiles by GCMS 624 Client Sample ID: MW-12 Date Analyzed: 9/18/97 Client Project ID: 01-0997 Analyzed By: WML Lab Sample ID: 29608 Date Collected: 9/11/97 Lab Project ID: G216-1 Date Received: 9/12/97 Matrix: Water Dilution: 1.0 Compound Quantitatlon Result Limit (ug/L) (ug/L) Benzene 1 BQL Bromochloromethane 1 BQL Bromoform 1 BQL Bromomethane 1 BQL Carbon tetrachloride 1 BQL Chlorobenzene 1 BQL Chloroethane' 1 BQL 2-Chloroethyl vinyl ether 5 . BQL Chloroform 1 BQL Chloromethane 1 BQL Dibromochloromethane 1 BQL 1,2-Dichlorobenzene 1 BQL 1,3-Dichlorobenzene 1 BQL 1,4-Dichlorobenzene 1 BQL 1,1-Dichloroethane 1 BQL 1,1-Dichloroethene 1 BQL 1,2-Dichloroethane 1 BQL trans-1,2-Dichloroethene 1 BQL 1,2-Dichloropropane 1 BQL cis-1,3-Dichloropropene 1 BQL trans-1,3-Dichloropropene 1 BQL Diisopropyl ether (DIPE) 1 BQL Ethylbenzene 1 BQL Methylene chloride 5 BQL Methyl-tert-butyl ether (MTBE) 1 BQL 1,1,2,2-Tetrachloroethane 1 BQL Tetrachloroelhene Toluene 1 1 BQL 6 Trichloroelhene • 1 3 y 1,1,1-Trichloroelhane 1 BQL 1,1, 2-Trichloroethane 1 BQL Trichlorofluoromethane 1 BQL Vinyl chloride 1 BQL m-,p-Xylene 2 BQL o-Xylene 1 BQL Surrogate Standards Surrogate Surrogate Percent Added Result Recovery Compound (ug/L) (ug/L) 1,2-Dichloroethane-d4 10.0 10.4 104 Toluene-d8 10.0 7.4 74 Bromofluorobenzene 10.0 8.9 89 Comments: All results are corrected for dilution. Flags: BQL = Below Quantitation Limit Reviewed By: v , Page 1 of 1 i .-J PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GGMS 624 Client Sample ID: MW-13 Date Analyzed: 9116/97 Client Project ID: 01-0997 Analyzed By: WML Lab Sample ID: 29609 Date Collected: 9/11/97 Lab Project ID: G216-1 Date Received: 9/12/97 Matrix: Water Dilution: 4.0 Compound Quantitation Result Limit (ug/L) (ug/L) Benzene 4 BQL Bromochloromethane 4 BQL Bromoform 4 BQL Bromomethane 4 BQL Carbon tetrachloride 4 BQL Chlorobenzene 4 BQL Chloroethane 4 BQL 2-Chloroethyl vinyl ether 20 BQL Chloroform 4 BQL Chlbromethane 4 BQL Dibromochloromethane 4 BQL 1,2-Dichlorobenzene 4 BQL 1,3-Dichlorobenzene 4 BQL 1,4-Dichlorobenzene 4 BQL 1,1-Dichloroethane 4 BQL 1,1-Dichloroethene 4 BQL 1,2-Dichloroethane 4 BQL trans-1,2-Dichloroethene 4 BQL 1,2-Dichloropropane 4 BQL cis-1,3-Dichloropropene 4 BQL trans-1,3-Dichloropropene 4 BQL Dlisopropyl ether (DIPE) 4 BQL Ethylbenzene 4 BQL Methylene chloride 20 BQL Methyl-tert-butyl ether (MTBE) 4 BQL 1,1,2,2-Tetrachloroethane 4 BQL Tetrachloroethene 4 BQL Toluene 4 BQL Trichloroethene 4 66 1,1,1-Trlchloroethane 4 BQL 1,1,2-Trichloroethane 4 BQL Trichlorofluoromethane 4 BQL Vinyl chloride 4 BQL m-,p-Xylene 8 BQL o-Xylene 4 BQL Surrogate Standards Surrogate Surrogate Percent Added Result Recovery Compound (ug/L) (ug/L) 1,2-Dichloroethane-d4 10.0 10.3 103 Toluene-d8 10.0 9.3 93 Bromofluorobenzene 10.0 8.8 88 Comments: All results are corrected for dilution. Flags: BQL = Below Quanlltatlon Limit Page 1 of 1 Reviewed By: hv� PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GCMS 624 Client Sample ID: MW-14 Date Analyzed: 9/15197 Client Project ID: 01-0997 Analyzed By: CKC Lab Sample ID: 29610 Date Collected: 9/11197 Lab Project ID: G216-1 Date Received: 9112/97 Matrix: Water Dilution: 1.0 Compound Benzene Bromochloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane D Ib romochloro methane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,1-Dichloroethane 1,1-Dichloroethene 1,2-Dichloroethane trans-1,2-Dlchloroethene 1,2-Dichloropropane cis-1, 3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether (DIPE) Ethylbenzene Methylene chloride Methyl-lert-butyl ether (MTBE) 1,1,2.2-Tetrachloroethane Tetrachloroethane Toluene Trichloroethene 1,1,1-Ticchloroethane 1,1,2-Trlch loroethane Tri chlo roll uorom et h a n e Vinyl chloride m-,p-Xylene o-Xylene Quantitatlon Limit (ug/L) Surrogate Standards Surrogate Added Compound (ug/L) 1,2-Dichloroethane-d4 10.0 Toluene -do 10.0 Bromolluorobenzene 10.0 Comments: All results are corrected for dilution. Flags: SOL = Below Quantitatlon Limit Result (ug/L) SOL SOL BQL SOL SOL BQL BQL SOL SOL SOL SOL SOL SOL BQL SOL SOL SOL BQL SOL: SOL BQL SOL SOL BQL SOL BQL BQL SOL 22 SOL BQL SOL BQL SOL SOL Surrogate Percent Result Recovery (ug/L) 9.9 99 7.7 77 9.6 96 Pago 1 of 1 Reviewed By: 6,1y_ j PARADIGM ANALYtICAL LABORATORIES, INC. Results for Volatiles - by GCMS 624 Client Sample ID: RC-15 Date Analyzed: 9/15/97 Client Project ID: 01-0997 Analyzed By: CKC Lab Sample ID: 29611 Date Collected: 9111197 Lab Project ID: G216-1 Date Received: 9/12197 Matrix: Water Dilution: 1.0 Compound Quantltatlon Result Limit(ug/L) (ug/L) Benzene 1 BQL Bromochloromethane 1 BQL Bromoform 1 BQL Bromomethane 1 BQL Carbon tetrachloride 1 BQL Chlorobenzene 1 BQL Chloroethane 1 BQL 2-Chloroethyl vinyl ether 5 BQL Chloroform 1 BQL Chloromethane 1 BQL Dibromochloromethane 1 BQL 1,2-Dlchlorobenzene 1 BQL 1,3-Dlchlorobenzene 1 BQL 1,4-Dlchlorobenzene 1 BQL 1,1-Dichloroelhane 1 BQL 1,1-Dichloroethene 1 BQL 1,2-Dichloroelhane 1 BQL trans-1,2-Dichloroethene 1 BQL 1,2-Dlchloropropane 1 BQL cis-1,3-Dichloropropene 1 BQL trans-1,3-Dichloropropene 1 BQL Dlisopropyl ether (DIPE) 1 BQL Ethylbenzene 1 BQL Methylene chloride 5 BQL J Methyl-tert-butyl ether (MTBE) 1 BQL 1,1,2,2-Telrachloroethane 1 BQL Tetrachloroethene 1 BQL Toluene 1 BQL - Trichloroethene • 1 BQL 1,1,1-Trlchloroethane 1 BQL 1,1,2-Trlchloroethane 1 BQL Trichloro0uoromelhane 1 BQL Vinyl chloride 1 BQL -� m-,p-Xylene 2 BQL o-Xylene J 1 BQL Surrogate Standards Surrogate Surrogate Percent Added Result Recovery Compound (ug/L) (ug/L) 1,2-Dlchloroethane-d4 10.0 9.7 97 Toluene-d8 10.0 8.7 87 Bromofluorobenzene 10.0 9.8 98 Commonts: All results are corrected for dilution. Flags: BQL =Below Quantltatlon Limit Reviewed By: r% Pape 1 of 1 j PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GCMS 624 Client Sample ID: RW-1 Date Analyzed: 9/16/97 Client Project ID: 01-0997 Analyzed By: WML Lab Sample ID: 29612 Date Collected: 9/11/97 Lab Project ID: G216-1 Date Received: 9/12/97 Matrix: Water Dilution: 50.0 Compound Quantitatlon Result Limit (ug/L) (ug/L) Benzene 50 BQL Bromochloromethane 50 BQL Bromoform 5o BQL - Bromomelhane 50 BQL Carbon tetrachloride 50 BQL Chlorobenzene 50 BQL Chloroethane 50 BQL 2-Chloroethyl vinyl ether 250 BQL Chloroform 50 BQL Chloromelhane 50 BQL Dibromochloromethane 50 BQL 1,2-Dichlorobenzene 50 BQL 1,3-Dichlorobenzene 50 BQL 1,4-Dichlorobenzene 50 BQL 1,1-Dichloroethane 50 BQL _ 1,1-Dichloroethene 50 BQL 1,2-Dichloroethane 50 BQL trans-1,2-Dichloroethene 50 BQL 1,2-Dichloropropane 50 BQL cis-1,3-Dichloropropene 50 BQL trans-1,3-Dichloropropene 50 BQL -- Dlisopropyl ether (DIPE) 50 BQL Ethylbenzene 50 BQL Methylene chloride 250 BQL Methyl-tert-butyl ether (MTBE) 50 BQL 1,1,2,2-Tetrachloroethane 50 BQL Tetrachloroelhene 5o BQL Toluene 50 BQL Trichloroethene 50 1200 1,1,1-Trichloroethane 50 BQL 1,1, 2-Trichloroethane 50 BQL Trichlorofluoromethane 50 BQL Vinyl chloride 50 BQL m-,p-Xylene 100 BQL o-Xylene 50 BQL Surrogate Standards Surrogate Surrogate Percent Added Result Recovery Compound (ug/L) (ug/L) 1,2-Dichloroethane-d4 10.0 9.9 99 Toluene-d8 10.0 10.0 100 Bromofluorobenzene 10.0 9.5 95 Comments: All results are corrected for dilution. Flags: BQL = Below Quantitatlon Limit Reviewed By: km` Papa 1 of f PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GCMS 624 Client Sample ID: RW-2 Date Analyzed: 9/16/97 Client Project ID: 01-0997 Analyzed By: WML Lab Sample ID: 29613 Date Collected: 9/11/97 Lab Project ID: G216-1 Date Received: 9/12/97 Matrix: Water Dilution: 100.0 Compound Benzene Bromochloromethane Bromoform Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane 2-Chloroethyl vinyl ether Chloroform Chloromethane D i b ro m o c h l o ro m et h a n e 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,1-Dichloroethane 1,1-Dichloroethene 1,2-Dichloroethane trans-1, 2-Dichloroethene 1,2-Dichloropropane cis-1, 3-Dlch to roprop a ne trans-1,3-Dlchloropropene Dlisopropyl ether (DIPE) Ethylbenzene Methylene chloride Methyl-tert-butyl ether (MTBE) 1,1,2, 2-Tetrachloroethane Tetrachloroethene Toluene Trichloroethene 1,1,1-Trichloroelhane 1,1, 2-Trichloroethane Trichlorofluorom ethane Vinyl chloride m-,p-Xylene o-Xylene Surrogate Standards Compound 1, 2-Dichloroethane-d4 Toluene-d0 Bromofluorobenzene Comments: All results are corrected for dilution. Flags: BQL = Below Quantitatlon Limit Quantitatlon Limit (ug/L) 100 100 100 100 100 100 100 500 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 500 100 100 100 100 100 100 100 100 100 200 100 Surrogate Added (ug/L) 10.0 10.0 10.0 Surrogate Result (ug/L) 10.1 10.0 9.1 Result (ug/L) BQL BQL BQL BQL BQL BOIL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL BQL 1600 BQL BQL BQL BQL BQL BQL Percent Recovery 101 100 91 Reviewed By: Page 1 of 1 J PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GCMS 624 Client Sample ID: RW-3 Date Analyzed: 9/18197 Client Project ID: 01-0997 Analyzed By: WML Lab Sample ID: 29614 Date Collected: 9111/97 Lab ProjectlD: G216-1 Date Received: 9/12/97 Matrix: Water Dilution: 80.0 Compound Quantltatlon Result Limit (ug/L) (ug/L) Benzene 80 BQL Bromochloromethane 80 BQL Bromoform 80 BQL Bromomethane 80 BQL Carbon tetrachloride 80 BQL Chlorobenzene 80 BQL Chloroethane 80 BQL 2-Chloroethyl vinyl ether 400 BQL Chloroform 80 BQL Chloromethane 80 BQL Dibromochloromethane 80 BQL 1,2-Dichlorobenzene 80 BQL 1,3-Dichlorobenzene 80 BQL 1,4-Dichlorobenzene 80 BQL 1,1-Dichloroethane 80 BQL 1,1-Dichloroelhene 80 BQL 1,2-Dichloroethane 80 BQL trans-1,2-Dichloroethene 80 BQL 1,2-Dlchloropropane 80 BQL cis-1,3-Dlchloropropene 80 BQL trans-1,3-Dlchloropropene 80 BQL Dllsopropyl ether (DIPE) 80 BQL Ethylbenzene 80 BQL Methylene chloride 400 BQL Methyl-tert-butyl ether (MTBE) 80 BQL 1,1,2,2-Tetrachloroethane 80 BQL Tetrachloroethene 80 BQL Toluene 80 BQL Trichloroethene 80 1300 1,1,1-Trichloroethane 80 BQL 1,1,2-Trichloroethane 80 BQL Trichlorofiuoromethane 80 BQL Vinyl chloride 80 BQL m-,p-Xylene 160 BQL o-Xylene 80 BQL Surrogate Standards Surrogate Surrogate Percent Added Result Recovery Compound (ug/L) (ug/L) 1,2-Dichloroethane-d4 10.0 10.2 102 Toluene-d8 10.0 10.2 102 Bromofluorobenzene 10.0 9.8 98 Comments: All results are corrected for dilution. Flags: BQL = Below Quantltatlon Limit Pago I of 1 Reviewed By: M , PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GCMS 624 Client Sample ID: Influent Date Analyzed: 9119/97 Client Project ID: 01-0997 Analyzed By: WML Lab Sample ID: 29615 Date Collected: 9/11197 Lab Project ID: G216-1 Date Received: 9/12/97 Matrix: Water Dilution: 80.0 Compound Quantitatlon Result Limit (ug/L) (ug/L) Benzene 80 BQL Bromochloromethane 80 BQL Bromoform 80 BQL Bromomethane 80 BQL Carbon tetrachloride 80 BQL Chlorobenzene 80 BQL Chloroethane 80 BQL 2-Chloroethyl vinyl ether 400 BQL Chloroform 80 BQL Chloromethane 80 BQL Dibromochloromethane 80 BQL 1,2-Dichlorobenzene 80 BQL 1,3-Dichlorobenzene 80 BQL 1,4-Dichlorobenzene 80 BQL 1,1-Dichloroethane 80 BQL 1,1-Dichloroethene 80 BQL 1,2-Dichloroethane 80 BQL trans-1,2-Dichloroethene 80 BQL 1,2-Dichloropropane 80 BQL cis-1,3-Dichloropropene 80 BQL trans-1,3-Dichloropropene 80 BQL Dilsopropyl ether (DIPE) 80 BQL Elhylbenzene 80 BQL Methylene chloride 400 BQL Methyl-tert-butyl ether (MTBE) 80 BQL 1,1,2,2-Tetrachloroethane 80 BQL Telrachloroethene 80 BQL Toluene 80 BQL Trichloroethene 80 1100 1. 1, 1-Trichloroethane 80 BQL 1,1,2-Trichloroethane 80 BQL Trichlorofluoromethane 80 BQL Vinyl chloride 80 BQL m-,p-Xylene 160 BQL o-Xylene 80 BQL Surrogate Standards Surrogate Surrogate Percent Added Result Recovery Compound (ug/L) (ug/L) 1,2-Dichloroethane-d4 10.0 10.2 102 Toluene-d8 10.0 10.2 102 Bromofluorobenzene 10.0 10.1 101 Comments: All results are corrected for dilution. Flags: BQL = Below Quantitatlon Limit Reviewed By: JNd� Pape 1 of 1 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatiles by GCMS 624 Client Sample ID: Effluent Date Analyzed: 9/19/97 Client Project ID: 01-0997 Analyzed By: WML Lab Sample ID: 29616 Date Collected: 9/11/97 Lab Project ID: G216-1 Date Received: 9112/97 Matrix: Water Dilution: 5.0 Compound Quantitation Result Limit (ug/L) (ug/L) Benzene 5 BQL Bromochioromethane 5 BQL Bromoform 5 BQL Bromomethane 5 BQL Carbon tetrachloride 5 BQL Chlorobenzene 5 BQL Chloroelhane 6 BQL 2-Chloroethyl vinyl ether 25 BQL Chloroform 5 BQL Chloromethane 5 BQL Dibromochloromethane 5 BQL 1,2-Dichlorobenzene 5 BQL 1,3-Dichlorobenzene 5 BQL 1,4-Dichlorobenzene 5 BQL 1,1-Dichloroethane 5 BQL 1,1-Dichloroethene 5 BQL 1,2-Dichloroethane 5 BQL trans-1,2-Dichloroethene 5 BQL 1,2-Dichloropropane 5 BQL cis-1,3-Dichloropropene 5 BQL trans-1,3-Dichloropropene 5 BQL Dlisopropyl ether (DIPE) 5 BQL Elhylbenzene 5 BQL Methylene chloride 25 BQL Methyl-tert-butyl ether (MTBE) 5 BQL 1,1,2,2-Telrachloroethane 5 BQL Telrachloroelhene 5 BQL Toluene 5 BQL Trichloroelhene 5 100 1,1,1-trichloroethane 5 BQL 1,1,2-Trichloroethane 5 BQL Trichlorolluoromethane 5 BQL Vinyl chloride 5 BQL m-,p-Xylene 10 BQL o-Xylene 5 BQL Surrogate Standards Surrogate Surrogate Percent Added Result Recovery Compound (ug/L) (ug/L) 1,2-Dichloroethane-d4 10.0 10.0 100 Toluene -dB 10.0 10.2 102 Bromolluorobenzene 10.0 9.6 96 Comments: All results are corrected for dilution. Flags: BQL = Below Quantitation Limit Reviewed By: h e Pago 1 of 1 PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MWA Client Project ID: 01-0997 Lab Sample ID: 29597 Lab Project ID: G216-1 Matrix: Water Parameter 'pH Date Collected: 9111/97 Date Received: 9/12197 Analyzed By: MAG Result Date Analyzed 6.61 9/23/97 'NCDEM requires that pH be analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. Reviewed By: yn=�- PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-2 Date Collected: 9/11/97 Client Project ID: 01-0997 Date Received: 9/12/97 Lab Sample ID: 29598 Analyzed By: MAG Lab Project ID: G216-1 Matrix: Water Parameter Result Date Analyzed 'pH 5.82 9/23/97 'NCDEM requires that pH be,analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. Reviewed By: }.T, PARADIGNI ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-3 Client Project ID: 01-0997 Lab Sample ID: 29599 Lab Project ID: G216-1 Matrix: Water Parameter .pH Date Collected: 9/11197 Date Received: 9112/97 Analyzed By: MAG Result Date Analyzed 5.98 9/23/97 'NCDEM requires that pH.be analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. Reviewed By: M. PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-4 Date Collected: 9/11197 Client Project ID: 01-0997 Date Received: 9/12/97 Lab Sample ID: 29600 Analyzed By: MAG Lab Project ID: G216-1 Matrix: Water Parameter Result Date Analyzed 'pH 5.67 9/23197 'NCDEM requires that pH be analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. Reviewed By: Ampy PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-5 Client Project ID: 01-0997 Lab Sample ID: 29601 Lab Project ID: G216-1 Matrix: Water Parameter 'pH Date Collected: 9/11/97 Date Received: 9112/97 Analyzed By: MAG Result Date Analyzed 5.80 9/23/97 'NCDEM requires that pH be analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. Reviewed By: fwi PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics f, Client Sample ID: MW-6 Client Project ID: 01-0997 Lab Sample ID: 29602 Lab Project ID: G216-1 Matrix: Water Parameter 'pH Dale Collected: 9111/97 Date Received: 9/12/97 Analyzed By: MAG Result Date Analyzed 5.42 9/23/97 'NCDEM requires that pH be analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. Reviewed By: Ma, PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-7 Date Collected: 9/11/97 Client Project ID: 01-0997 Date Received: 9112/97 Lab Sample ID: 29603 Analyzed By: MAG Lab Project ID: G216-1 Matrix: Water Parameter Result Date Analyzed 'pH 5.32 9/23/97 'NCDEM requires that pH be analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. Reviewed By: nv PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-8 Date Collected: 9111197 Client Project ID: 01-0997 Date Received: 9/12/97 Lab Sample ID: 29604 Analyzed By: MAG Lab Project ID: G216-1 Matrix: Water Parameter Result Date Analyzed 'pH 5.44 9/23/97 'NCDEM requires that pH be analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. Reviewed By: j, PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-9 Client Project ID: 01-0997 Lab Sample ID: 29605 Lab Project ID: G216-1 Matrix: Water Parameter 'pH Date Collected: 9/11197 Date Received: 9/12197 Analyzed By: MAG Result Date Analyzed 5.20 9/23/97 'NCDEM requires that pH be analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. Reviewed By:Y-?— PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-10 Date Collected: 9/11/97 Client Project ID: 01-0997 Date Received: 9/12/97 Lab Sample ID: 29606 Analyzed By: MAG Lab Project ID: G216-1. Matrix: Water Parameter Result Date Analyzed 'pH 4.75 9/23/97 'NCDEM requires that pH be analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. Reviewed By: U..- PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-11 Date Collected: 9/11/97 Client Project ID: 01-0997 Date Received: 9112/97 Lab Sample ID: 29607 Analyzed By: MAG Lab Project ID: G216-1 Matrix: Water Parameter Result Date Analyzed 'pH 5.80 9/23/97 'NCDEM requires that pH be analyzed within 15 minutes of sampling., This analysis was performed outside this specified holding time. Reviewed By: by PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-12 Date Collected: 9/11/97 Client Project ID: 01-0997 Date Received: 9/12197 Lab Sample ID: 29608 Analyzed By: MAG Lab Project ID: 6216-1 Matrix: Water Parameter Result Date Analyzed 'pH 5.50 9/23/97 'NCDEM requires that pH be analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. Reviewed By: 1sw-_ PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-13 Date Collected: 9/11/97 Client Project ID: 01-0997 Date Received: 9/12197 Lab Sample ID: 29609 Analyzed By: MAG Lab Project ID: G216-1 Matrix: Water Parameter Result Date Analyzed 'pH 6.39 9/23/97 'NCDEM requires that pH be analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. Reviewed By: psc,, PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: MW-14 Date Collected: 9/11/97 Client Project ID: 01-0997 Date Received: 9/12/97 Lab Sample ID: 29610 Analyzed By: MAG Lab Project ID: G216-1 Matrix: Water " Parameter Result Date Analyzed — 'pH 5.28 9123/97 'NCDEM requires that pH be analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. Reviewed By: hn PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: RC-15 Client Project ID: 01-0997 Lab'Sample ID: 29611 Lab Project ID: G216-1 Matrix: Water Parameter 'pH Date Collected: 9/11/97 Date Received: 9112/97 Analyzed By: MAG Result Date Analyzed 5.47 9/23/97 'NCDEM requires that pH be analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. Reviewed By: b&,, PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: RW-1 Client Project ID: 01-0997 Lab Sample ID: 29612 Lab Project ID: G216-1 Matrix: Water Parameter 'pH Date Collected: 9/11/97 Date Received: 9112/97 Analyzed By: MAG Result Date Analyzed 5.72 9/23/97 'NCDEM requires that pH be analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. Reviewed By: un PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: RW-2 Date Collected: 9111197 Client Project ID: 01-0997 Date Received: 9/12/97 Lab Sample ID: 29613 Analyzed By: MAG Lab Project ID: G216-1 Matrix: Water Parameter Result . Date Analyzed 'pH 5.33 9123/97 'NCDEM requires that pH be analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. _J Reviewed By: ue, PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: RW-3 Client Project ID: 01-0997 Lab Sample ID: 29614 Lab Project ID: G216-1 Matrix: Water Parameter 'pH Date Collected: 9/11/97 Date Received: 9/12197 Analyzed By: MAG Result Date Analyzed 5.66 9/23/97 •NCDEM requires that pH be analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. J I Reviewed By: PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: Influent Client Project ID: 01-0997 Lab Sample ID: 29615 Lab Project ID: G216-1 Matrix: Water Parameter 'pH Date Collected: 9/11/97 Date Received: 9/12/97 Analyzed By: MAG Result Date Analyzed 5.54 9/23/97 'NCDEM requires that pH be analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. I 1 I J Reviewed By: tom_ PARADIGM ANALYTICAL LABORATORIES, INC. Results for Inorganics Client Sample ID: Effluent Client Project ID: 01-0997 Lab Sample ID: 29616 Lab Project ID: G216-1 Matrix: Water Parameter 'pH Date Collected: 9/11/97 Date Received: 9/12197 Analyzed By; MAG Result Date Analyzed 6.26 9/23/97 'NCDEM requires that pH be analyzed within 15 minutes of sampling. This analysis was performed outside this specified holding time. Reviewed By: Vows PARADIGM ANALYTICAL LABORATORIES, INC. 2627 Northchase Parkway SE, Wilmington, NC 28405 Phone: (910)-350-1903 FAX: (910)-350-1557 '-lient: loysrMC4 1ac •'p Wdress: taM1:, kddress: quote #: Sec Mart Pawl Chain -of Custody Record & Analytical Request Project ID: O� - P.O. Number: Contact: ,SGS iic' Phone: 2SG.-o�S7 Date: Turnaround: Job Number: COC# Page _�— of 2- ReportTo: PV 8 S ti 2 Nc �yV9v Invoice To: r aG» f r E • Preservatives Analyses Comments: a` Please specify any special reporting requirements `S", Siffi Ie ID Date Tune Marrir C1 1 L mil' W- Aso % X In - S 5-1,42 n,% w - '7 -21 Relinquished By Date Time Received By Date Time Temperature Sampled By Airbill # (11111, 1 0',I PARADIGM ANALYTICAL LABORATORIES, INC. 2627 Northchase Parkway SE, Wilmington, NC 28405 Phone: (910)-350-1903 FAX: (910)-350-1557 Chain -of Custody Record & Analytical Request '-Iient: Coop Project ID: Q 911 kddress: Uv--,, P.O. Number: liddress: yDD Contact: -)'VVJ ItiMP it- '.It- M4.7-r ^e%xf Phone: 2576 --0352 Date: 1-// - 47 ') — Turnaround: 5mcfs-e4 Job Number: COC# Page _a Of '? Report P0 vy -717- Invoice To: !;4-,t, "W. ;N"W W 2 S;ir ':4,- S641 il D,33;l !�t'iPmKo'Mn 'Date Time Matra Aimlyses r. - Comments: e specify any special reporting Pleas requirements w 2- 1 Co Mv— Ix -Ile /2 C, - 1am f1w- I y r- Relinquished By Date Time Received By Date Time Temperature Sampled By Airbill # ontowAl PARADIGM ANALYTICAL LABORATORIES, INC. 2627 Northchase Parkway S.E. Wilmington, North Carolina 28405 (910) 350-1903 Fax (910) 350-1557 Mr. John Jester Gulfstream Environmental, Inc Date 09-08-97 PO Box 592 Wrightsville Beach, NC Report Number: G212-2 Client Project Name : Toastmaster Dear Mr. Jester: Enclosed are the results of the analytical services performed under the referenced project. Copies of this report and supporting data will be retained in our files for a period of five years in the event they are required for future _! reference. Any samples submitted to our laboratory will be retained for a maximum of thirty (30) days from date of this report unless other arrangements are requested. If there are any questions about the report or the services performed during this project, please call for assistance. We will be happy to answer any questions or concerns which you may have. Thank you for using Paradigm Analytical Labs for your analytical service projects. We look forward to working with you again on any additional needs which you may have. Sincerely, Paradigm Analytical Laboratories Laboratory Director Mark Randall North Carolina Wastewater Certification #481 PARADIGM ANALYTICAL LABORATORIES, INC. Results for inorganics Client Sample ID: Trench Date Collected: 10/6/97 Client Project ID: Toastmaster Date Received: 10/6/97 Lab Sample ID: 30722 Analyzed By: ELP Lab Project ID: G216-2 Matrix: Water Parameter Result Date Analyzed 'pH . 6.39 10/8/97 'NCDEM requires that pH be analyzed within 15 minutes of sampling. a This analysis was performed outside this specified holding time. Reviewed By: � PARADIGM ANALYTICAL LABORATORIES, INC. Results for Volatlles by GCMS 624 Client Sample ID: Trench Date Analyzed: 1OM97 Client Project ID: Toastmaster Analyzed By: CKC Lab Sample ID: 30722 Date Collected: 10/6197 Lab Project ID: G216-2 Date Received: 10/6/97 Matrix: Water Dilution: 1.0 Compound Quantitatlon Result Limit (ug/L) (ug/L) Benzene 1 BQL Bromochloromethane 1 BQL Bromoform 1 BQL Bromomethane 1 BQL Carbon tetrachloride 1 BQL Chlorobenzene 1 BQL Chloroethane 1 BQL 2-Chloroethyl vinyl ether 5 BQL Chloroform 1 BQL Chloromethane 1 BQL Dlbromochloromethane 1 BQL 1,2-Dichlorobenzene 1 BQL 1,3-Dichlorobenzene 1 BQL 1,4-Dichlorobenzene 1 BQL 1,1-Dlchloroethane 1 BQL . 1,1-Dlchloroethane 1 BQL 1,2-Dlchloroethane 1 BQL trans-1,2-Dichloroethene 1 BQL 1,2-Dlchloropropane 1 BQL cis-1,3-Dlchloropropene 1 BQL trans-1,3-Dlchloropropene 1 BQL Dlisopropyl ether (DIPE) 1 BQL Ethylbenzene 1 BQL Methylene chloride 5 BQL Methyl-tert-butyl ether (MTBE) 1 BQL 1,1,2;2-Tetrachloroethane 1 BQL Tetrachloroethene 1 BQL Toluene 1 BQL Trichloroethane 1 BQL 1,1,1-Trichloroethane 1 BQL 1,1,2-Trichloroethane 1 BQL Trichloro0uoromethane 1 BQL Vinyl chloride 1 BQL m-,p-Xylene 2 BQL o-Xylene 1 BQL Surrogate Standards Surrogate Surrogate Percent Added Result Recovery Compound (ug/L) (ug/L) 1,2-Dlchloroethane-d4 10.0 9.7 97 Toluene-d6 10.0 9.9 99 Bromofluorobenzene 10.0 110.2 102 Comments: All results are corrected for dilution. Flags: BQL = Below Quantitatlon Limit 1. Pape 1 or 1 Reviewed By: 'ARADIGII ANALYTICAL LABORATORIES, INC. COC# ?627 Nonhchase Parkway SE, Wilmington, NC 28405 Chain -of Custody Record & Analytical Request 'hone: (910)-350-1903 FAX: (910)-350-1557 Page of 'lient: nuif(_A N` Adress: is 54Z Adress: Wa ?—bgb0 juote #: Project ID: It�twlQS P.O. Number: Contact: JM aSkV_ Phone: (0 ICI - C09 11 Date: l0 to Ct� Turnaround: Job Number: Report To: � 6A Invoice To: Sample ID Date J Time v Manr'r Preservatives _ . Analyses Comments: Please specify any special reporting requirements Wo G-Vt ttketAA Relinquished By Date Time . . Received By ',..• Date" Time Temperature Sampled By Airbill # D-6-F i 125�r r-vv