HomeMy WebLinkAboutWQ0007798_Trimester Monitoring_19971031. LF N �. `f READ ENVIRONMENTAL, INC.
CONTRACTORS AND CONSULTANTS
CIVIL • GEOTECHNICAL • ENVIRONMENTAL
RESULTS OF 3m TRIMESTER GROUND WATER SAMPLING
(1997)
PERMIT No. WQ0007798
TOASTMASTER, INC. — INGRAHAM TIME PRODUCTS FACILITY
GROUND WATER INFILTRATION GALLERY
SCOTLAND COUNTY
LAURINBURG9 NORTH CAROLINA p r
HLL;Ld V tLU)
PREPARED FOR:
f,:ry 0 5 1997
I -AYE i € VI LE
IT -Ha. OrFIGE
NORTH CAROLINA DEPARTMENT OF ENVIRONMENT,
HEALTH, & NATURAL RESOURCES
DIVISION OF WATER QUALITY
RALEIGH, NORTH CAROLINA
PREPARED BY:
GULFSTREAM ENVIRONMENTAL, INC.
CONTRACTORS & CONSULTANTS
WILDIINGTON and CHARLOTTE
V ULFSTREAM ENVIRONMENTAL, INC.
--f CONTRACTORS AND CONSULTANTS
{ CIVIL • GEOTECHNICAL • ENVIRONMENTAL
October 31, 1997
North Carolina Department of Environment, Health,
and Natural Resources
Division of Water Quality
_ P.O. Box 29578
Raleigh, North Carolina 27626-0535
Re: Results of 3rd Trimester Ground Water Sampling (1997)
Permit No. W00007798
Toastmaster, Inc.- Ingraham Time Products Facility
Ground Water Infiltration Gallery
Laurinburg, Scotland County, North Carolina
Dear Sir or Madam:
Please find enclosed the monitoring report outlining the results of the Yd Trimester
Ground Water Sampling event conducted on September 11, 1997 at Toastmaster,
Incorporated's Ingraham Time Products Facility. Within this report, you will find:
• Ground Water Pump & Treat Remediation Site Data Sheet, Part A
• Table 1 -- Ground Water Level Data
• Table 2 -- Laboratory Analytical Results for Trichloroethene -- Ground Water
• Table 3 -- pH and Temperature Data — Ground Water
• Table 4A — Ground Water Remediation System Pressure Readings
Table 4B — Ground Water Remediation System Volume Readings
• Graphs 1-18 depicting Ground Water Monitoring data trends for all sampling
events 1/16/96 through 9/11/97
• GW-59 forms for 7/97 through 9/97
• Laboratory Analytical Results
• Drawings 1 and 2 depicting Trichloroethene Isocontours and Ground Water
Contours respectively
P.O. BOX 592 WRIGHTSVILLE BEACH, NC 28480 (910) 686-4493 OFFICEIFAX
1
I
,ir
G,
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October 31, 1997
Page 2
If you have any questions, or if we may be of assistance, please do not hesitate to contact
us at 910.686.4493.
Sincerely,
'P-J, a
Rudy A. Smithwick, P.G.
President
Enclosures
cc: Mr. Larry Clark, Toastmaster, Inc.
Jon K Jester
Vice President
GW-79 GROUND WATER PUMP & TREAT
REMEDIATION SITE DATA SHEET
Ll
NORTH,CAROLINA DEPARTMENT OF ENVIRONMENT, HEALTH AND NATURAL RESOURCES
Division of Environmental Management, Groundwater Section
(To be
each submission)
Background
Site Name: �IQASTMA9fF2�SilL. IXWGRAWA A DIV. Incident No: Date:
Location: r
Region: 1: 1VEM&V
Responsible Party:
SC aR.AN Q Date Release Identified:
1:1►jC_ Date CAP Completed:
PART R
(To be completed for initial report or to update information previously provided)
Hydrogeology
Description of Aquifer Lithology:
Is bedrock aquifer/fractured saprolite impacted? Describe.
Average Hydraulic Conductivity (ft./day): Average Groundwater Gradient
How were above determined?
Major Pumping Influences Which may Affect GW Flow:
Distance from Site: Pumping Rate:
Location and Distance from Site of Nearest Supply Well(s): _
Description of Release ,
Type of Product: Estimated Volume Released:
Average Plume Dimensions(ft.)--Width: Length: Depth Interval:
Ranges of Concentrations from CSA:
Emergency Response/Initial Remedial Actions
Date Source Removed/Repaired: Free Product Recovered (gal.):
Soil Excavation (tons): Average Contaminant Concentration (mg/kg):
Type of Treatment or Disposal:
Remediation
Goals of Remediation:
Description of Treatment System:
Pilot test conducted? (Type) Date:
Method of System Effluent Disposal:
No. of Monitoring Wells: Monitoring Schedule:
Date GW System Started: No. of.Recovery Wells:
Recovery Well Flowrate Drawdown Radius of • .Pump Type/
GPM (ft.) Influence(ft.) Capacity
Are any other remediation systems used in conjunction with Pump & Treat? Describe.
PART C
SYSTEM PERFORMANCE MONITORING
(To be completed with each submission)
PERIOD OF OPERATION
Report for: _/_/_ to —/_/— Days of Operation this Period:
SYSTEM DOWNTIME SUMMARY (current reporting period only)
DATE
From/To
FREE PRODUCT RECOVERY
Total Gallons Recovered Since Last Report:
Total Gallons Recovered to Date:
Well Z.D.:
Reason
Date
Screened interval*
FP Thickness (in.)
Avg. GW Level*
Recovery Method
*Depth in Feet from Top of Casing
Provide similar table for each well containing free product by attaching additional sheet(sJ
INFLUENT & EFFLUENT CONCENTRATION DATA - TREATMENT SYSTEM
Gallons Treated Since Last Report:
Total Gallons Treated To Date: _
Parameter/Units:
Date
Influent
Effluent
Attach additional sheet(s) as needed.
COMMENTS:
Parameter/units:
Note: Attach a current map showing location of all monitoring/recovery wells,
remediation system components, and the extent of the contaminant plume.,
4
trenches,
GW-79/5-94
TABLES
TABLE 1(Page 1 of 4)
Ground Water Table Data
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, North Carolina
Well ID
Date
Top of Casing
Elevation
Depth to
Ground Water
Ground Water
Table
Elevation
Monitoring
Wells
MW-1
1/16/96
116.41
11.73
104.68
5/23/96 _
116.41
11.15
105.26
9/16/96
116.41
15.66
100.75
1/31/97
116.41
8.75
107.66
4/28/97
116.41
12.82
103.59
9/11/97
116.41
15.70
100.71
1%M-2
1/16/96/
113.76
15.57
98.19
5/23/96
113.76
15.72
98.04
9/16/96
113.76
17.82
95.94
1/31/97
113.76
13.26
100.50
4/28/97
113.76
15.82
97.94
9/11/97
113.76
17.93
95.83
MW-3
1/16/96
112.34
12.41
99.93
5/23/96
112.34
9/16/96
112.34
1/31/97
112.34
4/28/97
112.34
12.11
100.23
9/11/97
112.34
14.82
97.52
MW-4
1/16/96
115.12
14.08
101.04
5/23/96
115.12
13.64
101.48
9/16/96
115.12
16.58
98.54
1/31/97
115.12
11.89
103.23
4/28/97
115.12
13.60
101.52
9/11/97
115.12
16.65
98.47
MW-5
1/16/96
119.78
9.00
110.78
5/23/96
119.78
8.73
111.05
9/16/96
119.78
10.32
109.46
1/31/97
119.78
7.15
112.63
4/28/97
119.78
8.10
111.68
9/11/97
119.78
11.94
107.84
Note: * - No Data Available
BQL -Below Quantitation Limit
All monitoring wells with the prefix GT/T have been reassigned the designation/prefix MW
r -
I
�J
TABLE 1(Page 2 of 4)
Ground Water Level Data
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, North Carolina
Well ID
Date
Top of Casing
Elevation
Depth to
Ground Water
Ground Water
Table
Elevation
NM-6
1/16/96
112.94
14.52
98.42
5/23/96
112.94
14.51
98.43
9/16/96
112.94
16.82
96.12
1/31/97
112.94
12.65
100.29
4/28/97
112.94
14.64
98.30
9/11/97
112.94
16.77
96.17
MW-7
1/16/96
120.81
14.41
106.40
5/23/96
120.81
13.88
106.93
9/16/96
120.81
16.52
104.29
1/31/97
120.81
11.44
109.37
4/28/97
120.81
13.14 '
107.67
9/11/97
120.81
16.93
103.88
NIW-8
1/16/96
114.82
0.40
114.42
5/23/96
114.82
1.21
113.61
9/16/96
114.82
0.00
114.82
1/31/97
114.82
0.00
114.82
4/28/97
114.82
0.07
114.75
9/11/97
114.82
2.58
112.24
NIW-9
1116/96
117.15
15.20
101.95
5/23/96
117.15
14.96
102.19
9/16/96
117.15
17.81
99.34
1/31/97
117.15
13.45
103.70
4/28/97
111.15
14.51
102.64
9/11/97
117.15
17.70
99.45
NM-10
1/16/96
110.83
10.48
100.35
5/23/96
110.83
9.17
101.66
9/16/96
110.83
13.55
97.28
1/31/91
110.83
7.41
103.42
4/28/97
110.83
8.60
102.23
9/11/97
110.83
13.25
97.58
MW-11
1/16/96
117.57
'11.82
105.75
5/23/96
117.57
11.52
106.05_
Note: " - No Data Available
BQL - Below Quantitation Limit
All monitoring wells with the prefix GT/T have been reassigned the designation/prefix MW
'LI)
TABLE 1(Page 3 of 4)
Ground Water Level Data
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, North Carolina
Well ID
Date
Top of Casing
Elevation
Depth to
Ground Water
Ground Water
Table
Elevation
MW-11 cont'd
9/16/96
117.57
11.65
105.92
1/31/97
117.57
9.14
108.43
4/28/97
117.57
10.70
106.87
9/11/97
117.57
14.26
10331
AM-12
1/16/96
109.25
8.77
100.48
5/23/96
109.25
7.93
101.32
9/16/96
109.25
12.85
96.40
1/31/97
109.25
4/28/97
109.25
9/11/97
109.25
9.85
99.40
NM-13
1/16/96
120.35
23.50
96.85
5/23/96
120.35
21.73
98.62
9/16/96
120.35
21.55
98.80
1/31197
120.35
19.28
101.07
4/28/97
120.35
27.41
92.94
9/11/97
120.35
20.86
99.49
MW-14
1/16/96
119.03
12.02
107.01
5/23/96
119.03
11.12
107.91
9/16/96
119.03
15.82
103.21
1/31/97
119.03
6.07
112.96
4/28/97
119.03
10.85
108.18
9/11/97
119.03
15.39
103.64
RC-15
1/16/96
121.15
17.29
103.86
5/23/96
121.15
19.80
101.35
9/16/96
121.15
19.74
101.41
1131 /97
121.15
15.82
105.33
4/28/97
121.15
16.41
104.74
9/11/97
121.15
20.00
101.15
Recovery
Wells
RW-1
1/16/96
112.38
18.14
94.24
5/23/96
112.38
15.42
96.96
Note: * -No Data Available
BQL -Below Quantitation Limit
All monitoring wells with the prefix GT/T have been reassigned the designation/prefix MW
TABLE 1(Page 4 of 4)
Ground Water Level Data
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, North Car6lina
Well ID
Date
Top of Casing
Elevation
Depth to
Ground Water
Ground Water
Table
Elevation
RW-1 cont'd
9/16/96
112.38
19.92
92.46
1/31/97
1.12.38
18.71
93.67
4/28/97
112.38
24.90
87.48
9/11/97
112.38
22.40
89.98
RW-2
1/16/96
117.48
22.99
94.49
5/23/96
117.48
18.61
98.87
9/16/96
117.48
34.78
82.70
1/31/97
117.48
24.51
92.97
4/28/97
117.48
32.74
84.74
9/11/97
117.48
35.42
82.06
RW-3
1/16/96
117.09
19.93
97.16
5/23/96
117.09
16.31
100.78
9/16/96
117.09
34.30
82.79
1/31/97
117.09
28.97
88.12
4/28/97
117.09
11.54
1 105.55
9/11/97
117.09
31.94
1 85.15
Note:. -No Data Available
BQL -Below Quantitation Limit
All monitoring wells with the prefix GT/T have been reassigned the designationtprefix MW
TABLE 2 (Page 1 of 4) ,
Laboratory Analytical Results for Trichloroethene— Ground Water
EPA Method 624
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, North Carolina
Well ID
Date
Trichloroethene (ppb)
NC Standard — 2.8
Monitoring Wells
MW-1
1/16/96
930
5/23/96
96
9/16/96
510
1/31/97
730
4/28/97
130
9/11/97
560
MW-2
1/16/96
1100
5/23/96
29
y
9/16/96
8.0
1/31/97
14.0
4/28/97
11.0
9/11/97
1400
MW-3
1/16/96
5/23/96
9/16/96
1/31/97
4/28/97
110
9/11/97
150
MW-4
1/16/96
6100
5/23/96
3100
9/16/96
1600
1/31/97
5000.
4/28/97
3600
9/11/97
5500
MW-5
1/16/96
13000
5/23/96
14000
9/16/96
9000
1/31/97
8400
4/28/97
6400
9/11/97
1600
Note: * - No Data Available
BQL — Below Quantitafion Limit
All monitoring wells with the prefix GT/T have been reassigned the designation/prefix MW
TABLE 2 (Page 2 of 4)
Laboratory Analytical Results for Trichloroethene— Ground Water
EPA Method 624
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, North Carolina
WellID
Date
Trichloroethene (ppb)
C Standard — 2.8
MW-6
1/16/96
2500
5/23/96
1800
9/16/96
1000
1/31/97
1800
4/28/97
1900
9/11/97
720
MW-7
1/16/96
1200
5/23/96
14000
9/16/96
1600
1/31/97
12000
4/28/97
4700
9/11/97
1100
MW-8
1/16/96
15
5/23/96
20
9/16/96
<5.0
1/31/97
<5.0
4/28/97
<5.0
9/11/97
16
MW 9
1/16/96
16
5/23/96
49
9/16/96
54
1/31/97
23
4/28/97
37
9/11/97
17
NM-10
1/16/96
17
5/23/96
<5.0
9/16/96
1700
1/31/97
<5.0
4/28/97
<5.0
9111/97
580
MW-11
1/16/96
280
5/23/96
240
Note: * - No Data Available
BQL —Below Quantitation Limit
All monitoring wells with the prefix GT/T have been reassigned the designation/prefix MW
I�
TABLE 2 (Page 3 of 4)
Laboratory Analytical Results for Trichloroethene— Ground Water
EPA Method 624
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinbur , North Carolina
Well ID
Date
Trichloroethene (ppb)
NC Standard — 2.8
MW-11 cont'd
9/16/96
230
1/31/97
94
4/28/97
130
9/11/97
410
NM-12
1/16/96
90
5/23/96
41
9/16/96
110
1131/97
14
4/28/97
9/11/97
3
MW-13
1/16/96
340
5/23/96
230
9/16/96
160
1/31/97
62
4/28/97
280
9/11/97
66
NM-14
1/16/96
28
5/23/96
87
9/16/96
460
1/31/97
60
4/28/97
120
9/11/97
22
RC-15
1/16/96
<5.0
5/23/96
<5.0
9/16/96
<5.0
1/31/97
<5.0
4/28/97
<5.0
9/11/97
<1.0
Recovery Wells
RW-1
1/16/96
1600
5/23/96
1800
9/16/96
1 1500
Note: * -No Data Available
BQL — Below Quantitation Limit
All monitoring wells with the prefix GUT have been reassigned the designation/prefix MW
TABLE 2 (Page 4 of 4)
Laboratory Analytical Results for Trichloroethene— Ground Water
EPA Method 624
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, North Carolina
Welly
Date
Trichloroethene (ppb)
C Standard —2.8
RW-1 cont'd
1/31/97
1400
4/28/97
1200
9/11/97
1200
RW-2
1/16/96
2300
5/23/96
2900
9/16/96
2000
1/31/97
2000
4/28/97
1500
9/11/97
1600
RW-3
1/16/96
410
5/23/96
1700
9/16/96
310
1/31/97
460
4/28/97
420
9/11/97
1300
Influent
9/11/97
1100
Effluent (System)
9/11/97
100
Effluent Trench
10/6/97
B L
Note: * -No Data Available
BQL —Below Quantitation Limit L6
All monitoring wells with the prefix GT/T have been reassigned the designation/prefix MW
Table 3
pH and Temperature Data - Ground Water
3rd Trimester Sampling Event - 9/11/97
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinbur NC
Well ID
pH - Laboratory
Measurement
pH - Field
Measurement
Temperature
(Celsius)
Wells
-Monitoring
MW-1
6.51
6.45
28.5
MW-2
5.82
6.62
24.1
MW-3
5.98
6.42
23.4
MW-4
5.67
6.59
23.9
MW-5
5.80
6.72
20.5
MW-6
5.42
6.87
28.3
MW-7
5.32
6.65
24.5
MW-8
5.44
6.91
27.0
MW-9
5.20
6.83
25.8
AM-10
4.75
6.45
24.0
MW-11
5.80
6.35
21.9
AM-12
5.50
6.63
22.5
AM-13
6.39
6.36
23.5
MW-14
5.28
6.47
20.3
RC-15
5.47
6.59
23.8
Recovery Wells
RW-1
5.72
6.90
24.7
RW-2
5.33
6.62
26.7
RW-3
5.66
6.90
24.9
EFFLUENT
6.26
6.83
18.7
INFLUENT
5.54
6.59
27.8
EFFLUENT
10/6/97
6.39
Note: * - No Data Available
BQL -Below Quantitation Limit
All monitoring wells with the prefix GT/T have been reassigned the designation/prefix MW
Table 4A
Ground Water Remediation System Pressure Readings
3'd Trimester Sampling Event — 9/11/97
Toastmaster, Inc.
Ingraham Time Products Facility
Laurin bur , NC
Location
Reading
Bag Filter (Right)
29
psi
Bag Filter Left
32
psi
Blower Pressure
47 psi
G
Carbon Bank 1
22
psi
Carbon Bank 2
20
psi
Carbon Bank 3
19
psi
Table 4B
Ground Water Remediation System Volume Readings
3rd Trimester Sampling Event— 9/11/97
Toastmaster, Inc.
Ingraham Time Products Facility
Laurin bur , NC
Location
Reading
Influent RW-1
426818.0 gal.
Influent RW-2
672091.7 gal.
Influent RW-3
710456.8 gal.
Effluent Totalizer
414882.0 gal.
Note: * -No Data Available
BQL — Below Quantitation Limit
All monitoring wells with the prefix GT/T have been reassigned the designation/prefix MW
[!!:Z\ is f.`+
i
L;
0
1000
900
800
700
a
a 600
W
C
O
500
c
d
c 400
0
U
300
200
100
0
Graph 1
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, NC
MWA Monitoring Data -- Trichloroethene
1/16196 5/23/96 9/16/96 1/31/97 - 4/28/97 9/11/97
Date Sampled
tMW-1
Graph 2
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, NC
MW-2 Monitoring Data -- Trichloroethene
tMW-2
Graph 3
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, NC
MW-3 Monitoring Data -- Trichloroethene
Date Sampled
No data was collected during 1996 and during the first trimester of 1997 because MW-3 had been damaged.
Graph 4
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, NC
MW-4 Monitoring Data -- Trichloroethene
16000
14000
12000
n 10000
a
N
C
O
8000
c
d
n
c
U 6000
�za�r
0
Graph 5
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, NC
MW-5 Monitoring Data -- Trichloroethene
Date Sampled
Graph 6
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, NC
MW-6 Monitoring Data -- Trichloroethene
Graph 7
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, NC
MW-7 Monitoring Data -- Trichloroethene
tMW-7
Graph 8
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, NC
MW-8 Monitoring Data -- Trichloroethene
`A
20
29
Z=
16;
;..
a
15
4
C
O
M
V
M
d
c
10
_.
o
gg
k
5
l
0 I r i •9 i �9 r G9 r
1 /16/96 5/23/96 9/16/96 1 /31 /97 4/28/97 9111 /97
Date Sampled
Concentrations of Trichloroethene for the sampling periods of 9/16196, 1/31/97, and 4/28/97 were not detected above the quantitation limit of 5.0 ppb.
Graph 9
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, NC
MW-9 Monitoring Data -- Trichloroethene
Date Sampled
1800
1600
1400
1200
C
a
a
No . 11
me
200
0
Graph 10
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, NC
MW-10 Monitoring Data -- Trichloroethene
1 /16196 5/23/96 9/16/96 1 /31 /97 4/28/97 9/11 /97
Date Sampled
Concentrations of Trichloroethene for the sampling periods 5/23/96, 1 /31197, and 4128/97 were not detected above the quantitation limit of 5.0 ppb.
450
400
350
300
a
a
o.
250
0
A
d 200
u
0
0
U
150
100
50
C
Graph 11
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, NC
MW-11 Monitoring Data -- Trichloroethene
1116/96 5/23/96 9116/96 1 /31 /97 4/28/97 9/11 /97
Date Sampled
120
100
T;
20
A
Graph 12
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, NC
MW-12 Monitoring Data -- Trichloroethene
1/16/96 5/23/96 9/16/96 1/31/97 4/28/97 9/11/97
Date Sampled
No data was available for the sampling period of 4/28/97.
M
350
300
a 250
a
0
C
O
riy 200
C
d
V
C
V 150
100
50
i)
Graph 13
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, NC
MW-13 Monitoring Data -- Trichloroethene
Date Sampled
i
Graph 14
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, NG
MW-14 Monitoring Data -- Trichloroethene
Graph 15
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, NC
RC-15 Monitoring Data -- Trichloroethene
Concentrations of Trichloroethene for all sampling periods in 1996 and 1997 were not detected above the respective quantitation limits.
2000
1800
1600
1400
C
a 1200
Ol
C
O
1000
C
d
c 800
O
U
600
400
200
0
Graph 16
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, NC
RW-1 Monitoring Data -- Trichloroethene
Date Sampled
-�-- RW-1
3500
3000
2500
a
a
a
N 2000
e
0
R
1500
c
0
U
1000
500
7
Graph 17
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, NC
RW-2 Monitoring Data -- Trichloroethene
Date Sampled
:i•
1600
1400
1200
a
a
a
e 1000
0
m 800
c
0
A
IlP
400
200
Graph 18
Toastmaster, Inc.
Ingraham Time Products Facility
Laurinburg, NC
RW-3 Monitoring Data -- Trichloroethene
1700
1300
_424_--
0.
1/16/96 5/23196 9/16/96 1/31/97 4/28/97 9/11/97
Date Sampled
GW-59 GROUND WATER QUALITY MONITORING
COMPLIANCE REPORT FORMS
I
U
DIVISION OF WATER QUALITY -GROUNDWATER SEOTION
GROUNDWATER QUALITY MONITORING ; °�PQ Boxzs57a _, a
z - For additional forms RALEIGN, NC 27626 057f
COMPLIANCE REPORT FORM „s please,writeoreall r (gi9)733p3227 a `s
Type or Use a ball-point pen and press firmly.
PERMIT NUMBER: (REQUIRED,1,
-�P'�
Non -Discharge %Q'x7i'i�}g
Facility Name
Address I
NP.DES
TYPE OF DISPOSAL OPERATION BEING MONITORED
t County I
Well Location /� ° L I o�7
(REQUIRED) Lagoon Septic TanWDrain Field
Well Identification Number MW —1 Well Depth z�. s Ft.
Well Diameter. I • ZS Sample (Screened) Interval Ft. To /.SFt.
Spray Field Subsurface Low -Pressure
Piping (LPP)
Depth to Water Level t5,10 ft. below measuring point (before sampling)
Land application of.Sedgge,
�S— Other
Measuring point is I . 7-0 ft. above land surface
Gallons of water pumped/bailed betoresampling 2� ..
Rotary Distributor
Field Analysis: pH (17 • u'S Specific Conductance uMhos Temp. C
Odor Appearance
Date Sample Collected q- I I . Q r7 Date Lab Sample Analyzed cf 115-L `i 7
Laboratory Name '�� q y A)aby'f -- C� I ( iIDO ids rC'S _ Certification No. �01
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED UL6�YES NO
COD mg/1
Coliform: MF Fecal /100ml
Coliform: MF Total /100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed) Co. tl
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P
mg/1
Al -Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/1
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
Ni - Nickel'
mg/I
Pb - Lead
mg/I
Zn - Zinc
mg/I
Pesticides/Herbicides
(Specify Compounds)
ug/I
ug/I
ug/I
Other (Specify Compounds and
Concentration units)
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
2 �] colloidal concentrations. (see #3 on back)
See back for instructions.
nature f ermi e (or Authorized Agent*) Date ** Submit blue and yellow copies only to address above.
GW-59 REV. 8/96
UIVISIUN
GROUNDWATER QUALITY MONITORING: For'a'dd Tonal rorma,
COMPLIANCE REPORT FORM � °''' please write or call
_ Type or Use a ball-point pen and press firmly.
Facility Name-
Address-aSi�VlGsa��,�
Ont
Wcxrinb nil Count ry4l ond
Well Location LA_T 'Ito LIT' 5?r.-S L.4ln.folo 11
Well Identification Number it Q Well Depth 3 O.o Ft.
Well Diameter I+Z5__Sample (Screened) Interval Ft. T0':90.0 Ft.
Depth to Water Level Irl, q3 ft. below measuring point (before sampling)
Measuring point is I +30 ft. above land surface
Gallons of water pumped/bailed before sampling 2, 32
Field Analysis: pH � lvZ Specific Conductance uMhos Temp._
Date Sample Collec d a' i I , L'A2 Date Lab Sample Analyzed q +'t
oC
Laboratory Name Pr CQ64M A-12W+; cC l L4[QDrGto✓i LS _
SAMPLES FOR METALS WY=RE COLLECTED UNFILTERED AND FIELD ACIDIFIED
COD
mg/I
Coliform: MF Fecal
/100m]
Coliform: MF Total
/100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/1
pH (when analyzed)
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/1
TKN as N
mg/1
PERMIT NUMBE charge(REQUIR_Epa, �7%-Pg
Non -Discharge ht�� "
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED)
. ,Lagoon Septic tank/Drain Field
Spray Field Subsurface Low -Pressure
Piping (LPP)
Land Application of Sludg9e
!2L Other
Rotary Distributor
Odor Appearance
Certification No. uCJ
YES NO
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
_ mg/I
Phosphorus: Total as P
mg/I
AI - Aluminum
mg/I
Ba - Barium
mg/1
Ca - Calcium
mg/I
Coll - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/1
Mn - Manganese
mg/1
Na - Sodium
mg/1
Ni - Nickel
mg/I
Pb - Lead
mg/I
Zn - Zinc
mg/I
Pesticides/Herbicides
(Specify Compounds)
ug/I
ug/I
ug/I
Other (Specify Compounds and
Concentration units)
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
q colloidal concentrations. (see #3 on back)
See back for instructions.
Signatu of Permi ee (or Authorized Agent') Date t* Submit blue and yellow copies only to address above.
GW-59 REV. 8/96
Well Location T " V UY Ib ' . U
Well Identification Number Well Depth 3D.r
Well Diameter l - Sample (Screened) Interval Ft. To
Depth to Water Level ILI' �ft. below measuring point (before sampling)
Measuring point is T_j ft. above landsurface.D
Gallons of water pumped/bailed before sampling
Field Analysis: pH Z Specific Conductance uMhos Temp.
Date Sample ColleAted Date Lab Sample Analyzed —
Laboratory Nam
Lagoon
Septic Tank/Drain Field
Spray Field Subsurface Low -Pressure
Piping (LPP)
Land Application of SI d e
V Other
Rotary Distributor
Appearance
Certification No. �U
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED LJ I YES NO
COD
Coliform
Coliform
MF Fecal
MF Total
mg/I
/1 o0ml
/100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total mg/I
pH (when analyzed) Em units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/l
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
Nitrite (NO2) as N
Nitrate (NO3) as N
Phosphorus: Total
AI - Aluminum_
Ba - Barium
Ca - Calcium_
Cd - Cadmium_
Chromium: Total _
Cu - Copper
.Fe - Iron
Hg - Mercury_
K - Potassium
Mg - Magnesium
Mn - Manganese _
Na - Sodium
as P.
mg/I
Ni - Nickel
mg/I
mg/I
Pb - Lead
mg/I
mg/I
Zn - Zinc
mg/I
mg/I
Pesticides/Herbicides
mg/I
(Specify Compounds)
mg/I
ugh
mg/l
ugh
mg/I
ugh
mg/1
Other (Specify Compounds and
mg/I
mg/I
Coentration units)
I�tGhlfky�t1Y�2'�
mg/I
mg/I
mg/I
mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
`^` f (� �/ colloidal concentrations. (see #3 on back)
\ 10 , 3 L ,9! See back for instructions.
9lgnatLtr� of Per a (or Authorized Agent-) Date •* Submit blue and yellow copies only to address above.
GW-59 REV. 8/96
GROUNDWATER ,QU
COMPLIANCE REPO
Facility Name
Address
PERMIT NUMBER: (REQUIRED) .
Non-Discharge�7
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED
Well Location (REQUIRED)
Well Identification Number V4 'L4 Well Depth Ft.
Well Diameter �Sample (Screened) Interval Ft. To Ft.
Depth to Water Level Ro,L0 L below measuring point (before sampling)
Measuring point is ft. above land surface
Gallons of water pumped/bailed before sampling I , O
Type or Use a ball-point pen and press firmly.
Lagoon
Septic Tank/Drain Field
Subsurface Low -Pressure
_ Piping (LPP)
Land Application of Sludge
Rotary Distributor
)C- Other
Spray Field
Field Analysis: pH (D.Sq Specific Conductance uMhosTemp. ?31t °C Odor — Appearance
Date Sample Colle�(ed Q - It •ate Date Lab Sample Analyzed a ' 22 •612
Laboratory Name IJ��Ck(AM t�.CG,• ( (C oprcrloriG-S _ Certification No. UP3 I
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO
COD
mg/I
Coliform: MF Fecal
/100m1
Coliform: MF Total
/100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed) • to units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P
mg/I
Al - Aluminum
mg/1
Ba - Barium
mg/1
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
- mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
Ni - Nickel
mg/I
Pb - Lead
mg/I
Zn - Zinc
mg/I
Pesticides/Herbicides
(Specify Compounds)
Ug/I
Ug/I
ug/I
Other (Specify Compounds and
I�centration units)
�; Mtn l[arcYylr-nne — 55 (X� u9� t
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
I i colloidal concentrations. (see #3 on back)
-. )` "� See back for instructions.
Si nature f P mittee or Authorized Agent`) Date •• Submit blue and yellow copies only to address above.
GW-59 REV. 8/96
GROUNDWATER QUALITY MO
COMPLIANCE REPORT FORM,
Type or
Facility Name
DIVI:
Por.additional forms
pen and press firmly. PERMIT NUMBER: (REQUIRED)
Non-DischargeG�Oi%��i
NODES
TYPE OF DISPOSAL OPERATION BEING MONITORED
— County_ . (REQUIRED)
Well Location t A -I 34- uo` n l " t a VI -1 I`l—t. I �iv. o
Well Identification NuMber fwlt,JfS Well Depth —Ft.
Well Diameter s%'Sample (Screened) Interval Ft. To -ZLI,C Ft.
Depth to Water Level ( ( 3LA ft. below measuring point (before sampling)
Measuring point is'3 - '2,0 ft. above land surface
Gallons of water pumped/bailed before sampling �3' f`7
Field Analysis: pH to -qf?N Specific Conductance uMhos Temp. C
Date Sample Colle d G' , It (' CC-7DateLab Sample Analyzed Q , 1 Co R _7
Laboratory Name( nQt� 1 Qly tiCQ l �afJD✓Gl (fXteS
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIEDOL
COD
mg/I
Coliform: MF Fecal
/100ml
Coliform: MF Total
/100mI
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed) - 43D
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
Lagoon Septic Tank/Drain Field
Spray Field Subsurface. Low -Pressure
Piping (LPP)
Land Application of Sludge
Other
Rotary Distributor
Odor Appearance ' -
Certification No. uP)l
YES NO
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P
mg/I
Al - Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
Ni - Nickel
Pb - Lead
mg/I
mg/I
Zn -Zinc
Pesticides/Herbicides
(Specify Compounds)
mg/I
ug/I
ug/I
ug/I
Other (Specify Compounds and
Qancentration units)
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
1o,3/�97 See back for instructions.
S naturdi of ermi e (or Authorized Agent*) Date ** Submit blue and yellow copies only to address above.
GW-59 REV. 8/95
GROUNDWATER QUALITY MONITORING.
COMPLIANCE REPORT FORM
For additional forms' '
please write or call:
1 �T�y�p, a or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED)
Facility Name ,:O L'`� � 1�� ' Non -Discharge
Address 0 nt NPDES
! 1:L+lii)KjllY�L.1.t'G� rCounty �11G TYPE OF.DISPOSAL OPERATION BEING MONITORED
YY (REQUIRED)
Well Location L-A� 21 1° f I� rj'(o " I rw( --?q - 7,7 r
Well Identification Number ''(-9 Well Depth I
Well Diameter 2, CD Sample (Screened) Interval Ft. To _4J5, t
Depth to Water Level (to.-I-7 ft. below measuring point (before sampling)
Measuring point is 0,7,0 ft. above land surface Q
Gallons of water pumped/bailed before sampling
Field Analysis: pH —Specific Conductance uMhos Temp.
Date Sample Colle�(ed 11• t l .G'7 Date Lab Sample Analyzed—
LaboratoryName1(CA(roQ A N l�U IiCGLI (�10cXGi 1CS
. Lagoon Septic Tank/Drain Field
Spray Field Subsurface Low -Pressure
Piping (LPP)
Land Application of Sludge
X Other
Rotary Distributor
CCl Odor Appearance
'��-- Certification No.
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED n _YES NO
COD —
Coliform
Coliform
mo/I
MF Fecal /100ml
MF Total /100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total mg/I
pH (when analyzed) —units
TOC
mg/I
Chloride
mg/1
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
LiMhos
Total Ammonia
mg/I
TKN as N
mg/I
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P
mg/I
AI - Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Pesticides/Herbicides
(Specify Compounds)
mg/I
mg/I
mg/I
ug/I
Ug/I
ug/I
Other (Specify Compounds and
C cantr tion unit )
`Ch�lOtrMV,e.f — -7ZOc
c9/ I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
Q �% colloidal concentrations. (see #3 on back) 10,31 ` ` See back for instructions.
S natur of ermitt (or Authorized Agent*) Date •* Submit blue and yellow copies only to address above.
GW-59 REV. 8196
Well Location I
- Loii " f '
Well Identification Number Well Depth _31S t
Well Diameter 2. DDT Sample (Screened) Interval Ft. To
Depth to Water Level _ ft. below measuring point (before sampling)
Measuring point is W ft. above land surface ()C7
Gallons of water pumped/b before sampling
Field Analysis: pH Specific Conductance uMhos Temp.
Date Sample Colleted ` ( I Ig iz Date., Lab Sample Analyzed , t
Laboratory Name w y its 'I'
SAMPLES FOR METALS WE E COLLECTED UNFILTERED AND FIELD ACIDIFIED
COD mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total /100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed)
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
Lagoon Septic TanWDrain Field
Spray Field Subsurface Low -Pressure
Piping (LPP)
Land Application of Slu g
Other
Rotary Distributor
Odor � Appearance
Certification No. LIP,
YES NO
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P
mg/I
Al - Aluminum
mg/I
Be - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE.
/aQ&ab=::
Sig lure P rhittee r Authorized Agent`)
Ni - Nickel
mg/I
Pb - Lead
mg/I
Zn - Zinc
mg/I
Pesticides/Herbicides
(Specify Compounds)
ug/I
ug/I
ug/I
Other (Specify Compounds and
_,6encentr lion units) 1
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
_I n- ' I ` l ( See back for instructions.
Date '• Submit blue and yellow copies only to address above.
GW-59 REV. 8/96
GROUNDWATER Q
COMPLIANCE REP
or
Facility Name
nt pen and press
. nor addiLonal farm
s
Well Location
Well Identification Numper Well Depth ZCo.O
Well Diameter �0Sample (Screened) Interval Ft. To
Depth to Water Level ft. below measuring point (before sampling)
Measuring point is D ft. above land surface
Gallons of water pumPed/bailed before sampling 2•00
Field Analysis: pH (a Specific Conductance uMhos Temp.
Date Sample Collet;�d q; I i •g r7 n Da(e. Lab Sample Analyzed!
Laboratory Name y L_ tRED - '
LLECTED NFIL SAMPLES FOR METAL S WER COTEAND FIELD ACIDIFIED
COD
mg/1
Coliform: MF Fecal
/100ml
Coliform: MF Total
/100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/1
pH (when analyzed)
�- �I—units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/1
Grease and Oils
mg/1
Hardness: Total
mg/1
Phenol
mg/1
Sulfate
mg/1
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
.. PERMIT NUMBER: (REQUIR,
_ Non -Discharge
NPDES
— TYPE OF DISPOSAL OPERATION BEING MONITORED
— (REQUIRED)
Lagoon Septic Tank/Drain Field
Spray Field Subsurface Low -Pressure
Piping (LPP)
Land Application of
Slud e
Other
Rotary Distributor
Odor Appearance
Certification No. ua (
YES NO
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P
mg/I
Al - Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I.
Mg - Magnesium
mg/I
Mn - Manganese
mg/1
Na - Sodium
mg/1
Ni - Nickel
Pb - Lead
Zn - Zinc
Pesticides/Herbicides
(Specify Compounds)
Other (Specify Compounds and
l
C�llRentratidn unds
i t -tn bd•
mg/1
mg/I
mg/I
ug/I
ug/I
ug/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
f �% colloidal concentrations. (see #3 on back)
/
/ o .3 ` 5 ` See back for instructions.
Si natur o ermi e (or Authorized Agent*) Date ** Submit blue and yellow copies only to address above.
GW-59 REV. 8/96
Well Location LA+ :500 LAB` OLI • q r L04° '7
Well Identification Number Mt.Well Depth 00
Well Diameter JOi, Sample (Screened) Interval Ft. To 2D
Depth to Water Level '11 ,'7 [7 ft. below measuring paint (before sampling)
Measuring point is Z ft. above land surface
Gallons of water pum e bt�lied before sampling a,0y
Field Analysis: . mr Specific Conductance IuMhos Temp.
Lagoon Septic Tank/Drain Field
Spray Field Subsurface Low -Pressure
Piping (LPP)
Land Application of Slud
Other
Rotary Distributor
°C _ Odor — Appearance -
Date Sample Coll ted " 1 l t • " r Date Lab ample analyzed�_r r � rg I
Laboratory Name ��'o M An(l�r�( �10FXC� l�10 Certification No. `—t
SAMPLES FOR METALS WW�OLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO
COD mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total /100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed)
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/1
Phosphorus: Total as P
mg/I
AI - Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/1
Cu - Copper
- mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
Ni - Nickel
mg/I
Pb - Lead
mg/I
Zn - Zinc
mg/I
Pesticides/Herbicides
(Specify Compounds)
ug/I
ug/I
ug/I
Other (Specify Compounds and
Co entration units)
i C�1lDt�0�l�Pt11e— iattg I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
�^ colloidal concentrations. (see #3 on back)
/0 -3 / !G� �/ ( FSS
ee back for instructions.
S nat ee (or Authorized Agent*) Date ubmit blue and yellow copies only to address above.
GW-59 REV. 8/96
DIVISION OF WATER QUALITY - GRGUNDWATER'SECTION
GROUNDWATER QUALITY MONITORING: P.O. BOX29578
For additional forms RALEIGH; No27626.0578
COMPLIANCE REPORT FORM please write or call: (9119)733-3221
Tiny nr I lep a hnn.nnlnT npn Anil nrpSS Tlrn v- -
Facili
Well
Well
Well
Deptl
Measuring point is 3 .'Z ft. above land surface
Gallons of water pumped/bailed before sampling
Field Analysis: pH (o U:5-- Spgpidq, Conductance uMhos Temp.
Date Sample Coll Date Lab Sample Analyzeed C.A • t �_c,
Laboratory Na1�no it 11 IPC
SAMPLES FOR METALS VVERt COLLECTED UNFILTERED AND FIELD ACIDIFIED
COD
mg/I
Coliform: MF Fecal
/100ml
Coliform: MF Total
/100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed) % units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
PERMIT NUMBER: (REQUIRE ) n
Non -Discharge („ )a
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED)
Lagoon Septic Tank/Drain Field
Spray Field Subsurface Low -Pressure
Piping (LPP)
Land Application of SI dge
Other
Rotary Distributor
Odor Appearance
Certification No.
YES —NO
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P
mg/I
Al - Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE.
A •;fir• - • ' •
..
Ni - Nickel
Pb - Lead
mg/I
mg/I
Zn - Zinc
Pesticides/Herbicides
(Specify Compounds)
mg/I
ug/I
ug/I
ug/I
Other (Specify Compounds and
C I nitration units
-f In two -1
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
O, 3 r ` See back for instructions.
Date •* Submit blue and yellow copies only to address above-
GW-59 REV. 8/96
GROUNDWATER QU
COMPLIANCE REPO
Facility Name
Addressy I
Ln
Well Location I0i
Well Identification I
Well Diameter
Depth to Water Let
Measuring point is.
Gallons of water pL
Field Analysis: pH
or Use a
ONITORINC
r` -For additional
please write o
press
before sampling 2Z•0r7
Specific Conductance � uMhos Temp.
^-5 P.o.•BOX ;29578� P <.
)ns RALEIGH; NO 27628 057B.' q
dl ..,'•„ , '. (9t9)733,-3221
PERMIT NUMBER:(REQUSRF,f)] �����
Non -Discharge LaYY��
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED) - .
.Lagoon Septic Tank/Drain Field
Spray Field Subsurface Low -Pressure
Piping (LPP)
Land Application of Slu e
Other
Rotary Distributor
Odor �— Appearance I —
Date Sample ColleS�d ` ` `t' Date Lab Sa ple Analyzed r
Laboratory Name l,C 06pyn (1'ilyhen� �hfirQlfX1PS Certification No.
SAMPLES FOR METALS WEFT COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO
COD
mg/I
Coliform: MF Fecal
/100ml
Coliform: MF Total
/100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed)�
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P
mg/I
AI - Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
Ni - Nickel
Pb - Lead
mg/I
mg/I
Zn -Zinc
Pesticides/Herbicides
(Specify Compounds)
mg/I
ug/I
ug/I
ug/I
Other (Specify Compounds and
Concentration units)
1�� r � lo�r�c3f-hrzne -
1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
) r� colloidal concentrations. (see #3 on back)
r
Seeback for instructions.
Si nature f ermitt (or Authorized Agent*) Date Submit blue and yellow copies only to address above.
GW-59 REV. 8/96
Facili
Well
Well
Well
Deptl
Measuring point is—ft. above land surface
Gallons of water pumped/b tied before sampling —
Field Analysis: Specific Conductance uMhos Temp.
PERMIT NUMBER: (REQu1RE[�, �,���n� ,
Non -Discharge I' 'I
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED)
Lagoon Septic Tank/Draih Field
Spray Field Subsurface Low -Pressure
Piping (LPP)
Land Application of SI d e
Other
Rotary Distributor
Odor Appearance
Date Sample Colle d I I e Lab ample Anay etl t• tn, -t f u�y
Laboratory Name - I r1��ril (y�+� �te5 Certification No. z)
SAMPLES FOR METALS W_. •E COLLECTED UNFILTERED AND FIELD ACIDIFIEE�- YES NO
COD
Coliform
Coliform
MF Fecal
MF Total
(Note: Use MPN method for highly turbid samples)
_ mg/I
/100m]
/100m1
Dissolved Solids: Total
mg/I
pH (when analyzed)
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
Nitrite (NO2) as N
Nitrate (N08) as N_
Phosphorus: Total as P
AI - Aluminum
Ba,- Barium
Ca - Calcium
Cd - Cadmium
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury
K - Potassium
Mg - Magnesium
Mn - Manganese
Na - Sodium
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
Ni - Nickel mg/I
Pb - Lead mg/I
Zn - Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
ug/I
ug/I
ug/I
Other (Specify Compounds and
CoijQentration units)
�11i �i1 7-t�s7
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
1 ✓ \ (v �( C f� See back for instructions.
igriatu f erm• tee (or Authorized Agent*) Date ** Submit blue and yellow copies only to address above.
GW-59 REV. 8/96
V"
DIVISION OF WATER QUALITY, -;;GROUNDWATER SECTION
"
GROUNDWATER QUALITY MONITORINGFor '�onal s
addirite
Po eox?ss7a
RALE(GH, INC 7826 0578 ^
COMPLIANCE REPORT. FORMplease6 or ea l
z 19) 733 3zzt ;
e ;
y
Type or Use a ball-point pen and press firmly. - , .
PERMIT NUMBER: (REQUIF�Ep
Non
Facility Name S
-Discharge
Address
t1
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED
r County o n yr
Well Location
(REQUIRED)
Lagoon Septic Tank/Drain
Field
Well Identification Number ell Depth �,� . Ft.
tt
Spray Field Subsurlace. Low -Pressure
Well DiameterSample (Screened) Interval Ft. To 47) Ft.
Piping (LPP)
Depth to Water Level 902 M(o ft. below measuring point (before sampling)
Land Application of slu�gg
other
Measuring point is ft. above land surface
�
—
' Rotary Distributor
Gallons of water pumped bailed before sampling
� oC —
Field Analysis: pH S ecific Conductance uMhos Temp. - S Odor
Appearance
Dale Sample Coll d (.I '� Date Lab Sa pie Analyzed
l
Laboratory Name ._ Certification No.
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES
NO
COD mg/I Nitrite (NO2) as N
mg/I Ni - Nickel
mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N
mg/I Pb - Lead
mg/I
Coliform: MF Total /100ml Phosphorus: Total as P
mg/I Zn - Zinc
mg/I
(Note: Use MPN method for highly turbid samples) Al - Aluminum
mg/I Pesticides/Herbicides
Dissolved Solids: Total mg/I Ba - Barium
mg/I (Specify Compounds)
pH (when analyzed) (o, ` 9 - units Ca - Calcium
mg/I
ug/I
TOC mg/I Cd - Cadmium
mg/I
ug/I
Chloride mg/I Chromium: Total
mg/I
ug/I
Arsenic mg/I Cu - Copper
mg/I Other (Specify Compounds and.
Grease and Oils mg/I Fe - Iron
mg/I central units
�rCVt IMEC — (QaU(�
/1
Hardness: Total mg/I Hg - Mercury
mg/I l
Phenol mg/I K- Potassium
mg/I
•J
Sulfate mg/I Mg - Magnesium
mg/I
Specific Conductance uMhos Mn - Manganese
mg/1
Total Ammonia mg/I Na - Sodium
mg/I
TKN as N mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE.
Note: Values should reflect dissolved and
concentrations. (see #3 on back)
1��(\colloidal
I o.31
q�
Zf}^V
t v \ ,
* See back for instructions.
Si ature f ermitt (or Authorized Agent*) Date
** Submit blue and yellow copies only to address above.
GW-59 REV. 8/96
GROUNDWATER QUALITY MONITORING-.,
COMPLIANCE REPORT FORM
For additional forms ,.
please write or call:
Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIR
li__n � Y1Ci5� 1 Non -Discharge �Q`�r7�96
Facility Name ��
Address IGicr NPDES -
L.n, 01 n n
i2 C C. Counn� C: �C(l C( TYPE OF DISPOSAL OPERATION BEING MONITORED
—--a .. (REQUIRED) -
Well Location t K v' o i"I f t
Well Identification Number AA — IU Well Depth Q,00 F.
Well Diameter U-00Sample (Screened) Interval Ft. To _ja.L1_2Ft.
Depth to Water Level 16-.'?>q ft. below measuring point (before sampling)
Measuring point is"�;_7_.t`Zft. above land surface
Gallons of water pumped/bailed before sampling �S
Field Analysis: pH (,9�0�7 Specific Conductance uMhos Temp.
Date Sample Colle ed Ct Date Lab Sample Analyzed I,
Laboratory Name - 1 rn
SAMPLES FOR METALS WE14E COLLECTED UNFILTERED AND FIELD ACIDIFIED
COD
Coliform
Coliform
MF Fecal
MF Total
mg/I
/100ml
/100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total mg/I
pH (when analyzed) units
TOC
mg/1
Chloride
mg/1
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
Lagoon Septic Tank/Drain Field
Spray Field Subsurface Low -Pressure
Piping (LPP)
Land Application of Sludge
Other
Rotary Distributor
Odor — Appearance
Certification No. WeI (
YES —NO
Nitrite (NO2) as N
mg/1
Nitrate (NO3) as N
mg/1
Phosphorus: Total as P
mg/I
Al - Aluminum
mg/I
Ba - Barium
mg/I
Ca- Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu.- Copper
mg/I
Fe - Iron
mg/1
Hg - Mercury
mg/1
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/1
Ni - Nickel
Pb - Lead
mg/I
mg/I
Zn - Zinc
Pesticides/Herbicides
(Specify Compounds)
mg/I
ug/I
ug/I
ug/I
Other (Specify Compounds and
�Cc centrat'IIon units)
v'i C h ID�y.�FY�P�1Q —
Z2uq 1 I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
—�V I O `� .�' / • ' See back for instructions.
S gnatur of ermitte (or Authorized Agent') Date ** Submit blue and yellow copies only to address above.
GW-59 REV. 8/96
GROUNDWATER
or
Facility
pen and press
Well Location w-t_ - t / ' r )Ll- SIT? Ulf.0 ""!4 - ' - � '
Well Identification Number t2C-ts Well Depth 70 • S Ft.
Well Diameter •00"'Sample (Screened) Interval Ft. To Z-SFt.
Depth to Water Level eft. below measuring point (before sampling)
Measuring point is Z- ft. above land surface
Gallons of water pumped/b ' ed before sampling Lo, OLD
Field Analysis: pH Specific Conductance _ uMhos Temp.
Date Sample Collecjed Date Lab Sample Analyzed G
Laboratory Name t'/ar L
SAMPLES FOR METALS
COD
Coliform: MF Fecal
Coliform: MF Total
(Note: Use MPN method for highly turbid samples)
_ mg/I
/100ml
/100ml
Dissolved Solids: Total
mg/I
pH (when analyzed) ri .LI2
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
PERMIT NUMBER: (REQUIR�E�l
Non -Discharge C-u, 0:02"1Q8
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED
4� 3r, (REQUIRED)
Lagoon Septic Ta k/Drain Field
Spray Field Subsurface Low -Pressure
Piping (LPP)
Land Application of SI d e
Y_ Other
Rotary Distributor
Nitrite (NO2) as N —
Nitrate (NO3) as N_
Phosphorus: Total as P
Al - Aluminum
Ba - Barium
Ca - Calcium
Cd - Cadmium
Chromium: Total
Cu - Copper
Fe - Iron _
Hg - Mercury
K - Potassium
Mg - Magnesium
Mn - Manganese
Na - Sodium
Appearance —
Certification No. UH (
YES — NO
mg/I
mg/I
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
mg/I
mg/I
mg/I
mg/I
Pesticides/Herbicides
mg/I
mg/I
(Specify Compounds)
Ug/I
mg/I
ug/I
mg/I
ug/I
mg/I
Other (Specify Compounds and
mg/I
Concentration units)
mg/I
mg/I
mg/I
mg/I
mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
/(� colloidal concentrations. (see #3 on back)
zEX U 10 .J 1 �" See back for instructions.
Sigbatur,f ermitte (or Authorized Agent') Date •• Submit blue and yellow copies only to address above.
GW-59 REV. 8/96
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility
A(
For additional forms
please write or call:
Type or Use a ball-point pen and press firmly.
Well Location
Well Identification Number Well Depth SD,00 Ft.
Well Diameter- L d2Sample (Screened) Interval Ft. To5D.60 Ft.
Depth to Water Level Z&LAD ft. below measuring point (before sampling)
Measuring point is 1. G ft. above land surface 6-5-1Gallons of water pum ed/ ailed before sampling CIO
Field Analysis: pH I Specific Conductance 11uMhos TempzO ,'7 oC
Date Sample Colles(ecl Date Lab Sample Analyzed G ' (t
Laboratory Name ✓ '( I L c-ci it
SAMPLES FOR METALS Wl E COLLECTED UNFILTERED AND FIELD ACIDIFIED
COD
mg/I
Coliform: MF Fecal
/100m1
Coliform: MF Total
/100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed) units
TOG
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/1
TKN as N
mg/1
Nitrite (NO2) as N
Nitrate (NO3) as N
Phosphorus: Total
Al -Aluminum_
Ba - Barium
Ca - Calcium_
Cd - Cadmium_
Chromium: Total _
Cu - Copper
Fe - Iron
Hg - Mercury_
K - Potassium _
Mg - Magnesium _
Mn - Manganese _
Na - Sodium
PERMIT NUMBER: ( MI � MOP)
Non -Discharge
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED
IREOUIREDI
Lagoon Septic TanMDrain Field
Spray Field Subsurface Low -Pressure
Piping (LPP)
Land Application of SI dge
Other
Rotary Distributor
Odor Appearance '—
Certification No. 48
YES NO
mg/I
mg/I
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
mg/1
mg/I
mg/I
mg/I
Pesticides/Herbicides
mg/I
mg/I
(Specify Compounds)
ug/I
mg/I
ug/I
mg/I
ug/I
mg/I
Other (Specify Compounds and
mg/I
mg/I
Coffin entration units)
l �i( Vl IW✓Yl — IZUO
L Q I
mg/I
mg/I
mg/I
mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
ZM A I O ` St 19 See back for instructions.
Ka ur of ermitt e or Authorized Agent') Date " Submit blue and yellow copies only to address above.
GW-59 REV. 8/96
GROUNDWATER QUALITY MONITORING
COMPLIANCE REPORTTORM
Facil
Well
Well
Well
Dept]
Measuring point is 2 , lO ft. above land surface
Gallons of water pumped/bailed before sampling 4�2� • C)C)
Field Analysis: pH Specific Conductance uMhos Temp,
Date Sample Collept4�d Date Lab Sa)nple Analyzed —
DIVISION OF W
For additional forms
_ please write or call:
Tvpe or Use a ball-point pen and press firmly.
Laboratory Name c a � r � > r f
SAMPLES FOR METALS W E COLLECTED UNFILTERED AND FIELD ACIDIFIED
COD mg/I
Coliform: MF Fecal /loom]
Coliform: MFTotal /loom]
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total mg/I
pH (when analyzed) S-3units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
PERMIT NUMBER: (REQUIREC1hCM��98
Non -Discharge ��1�11
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED . .
(REQUIRED)
Lagoon Septic Tank/Drain, Field
Spray Field _ Subsurface Low -Pressure
Piping (LPP)
Land Application of Sludge
-!>d— Other
Rotary Distributor
Odor Appearance
Certification No.�
YES NO
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P
mg/I
Al - Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
Ni - Nickel
Pb - Lead
Zn - Zinc
Pesticides/Herbicides
(Specify Compounds)
mg/I
mg/I
mg/I
ug/I
ug/I
ug/I
Other (Specify Compounds and
Con entration units) %
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
r �% colloidal concentrations. (see #3 on back)
O`� f '� r See back for instructions.
Siqtatur bf �rmitte (or Authorized Agent') Date •• Submit blue and yellow copies only to address above.
GW-59 REV. 8/96
GROUNDWATER'
COMPLIANCE RE
Facility Name TC
Address—P
t;
ai DI
For.additional forms
or Use a ball-point pen and press firmly.
LQS -�n_G -
Well Location
Well Identification Number Well Depth 110-1
Well Diameteramplp (Screened) Interval Ft. To QC
Depth to Water Level ft. below measuring point (before sampling)
Measuring point is 1, Q0 ft. above land surface
�,-)
Gallons of wat
Field Analysis:
Date Sample (
Laboratory Name_l-LUf
SAMPLES FOR METALS
COD
Coliform:
Coliform:
mn/I
MF Fecal /loom[
MF Total /loom[
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total mg/I
pH (when analyzed) S.foLo units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
PERMIT NUMBER: (REQUIRED
Non -Discharge I Cr'-)n�9a
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED)
Lagoon Septic Tank/Drain Field
Spray Field Subsurface Low -Pressure
Piping (LPP)
Land Application of Sludge -
Other
Rotary Distributor
Appearance —
Certification No.
YES NO
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P
mg/I
Al - Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
- mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
Ni - Nickel
mg/I
Pb - Lead
mg/I
Zn - Zinc
mg/I
Pesticides/Herbicides
(Specify Compounds)
ug/I
ug/I
ug/I
Other (Specify Compounds and
Con entratioq units)_ 1, �,,�/-�
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
q colloidal concentrations. (see #3 on back)
o/ See back for instructions.
Si atur of P rmitte (or Authorized Agent`) Date *' Submit blue and yellow copies only to address above.
GW-59 REV. 8/96
nal
GROUNDWATER QUALITY MONITORING For nAdiha...to .. a'.
Type or
Facility Name
pen
Well Location
Well Identification Number Well Depth Ft.
Well Diameter — Sample (Screened) Interval — Ft. To — Ft.
Depth to Water Level ft. below measuring point (before sampling)
Measuring point is ft. above land surface
Gallons of water pumped/bailed before sampling �p rI
Field Analysis: pH ZSpe if' Conductance uMhos Temp. � , I ,
Date Sample Collecte -1 -t ) -1 Date Lab Sample Analyzed Gj -lI O I
Laboratory Name alit QM Gbs of I obax-ni"o Ifi?S
SAMPLES FOR METALS WE COLLECTED UNFILTERED AND FIELD ACIDIFIED !, I
COD
Coliform:
Coliform:
mn/l
MF Fecal /loom[
MF Total /l ooml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed) (P r 2CP
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
%mg/I
Hardness: Total
mg/I
Phenol
mg/1
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
PERMIT NUMBER: (REQUIREDIL� -
'Non -Discharge 1r.1(�2(�D'77�)8
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED)
Lagoon
Septic TanWDraih Field
Spray'Field ``
Subsurface Low -Pressure
Piping (LPP)
Land Application of Sludge
X
Other
_
Rotary Distributor
Odor _ Appearance
Certification No. a fS
YES NO
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P
mg/I
Al - Aluminum
mg/1
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
Ni - Nickel
Pb - Lead
mg/1
mg/I
Zn - Zinc
Pesticides/Herbicides
(Specify Compounds)
mg/I
ug/I
ug/I
ug/I
Other (Specify Compounds and
Concentration units)
''��icl�lor-o2-the✓IQ� � IC�»�r�l
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
See back for instructions.
i na e oftermi ee'(or Authorized Agent*) Date **'Submit blue and yellow copies only to address above.
GW-59 REV. 8/96
GROUNDWATER QUALITY MONITORING:,, For atlditfbnel forms
COMPLIANCE REPORT FORM please write or call:
a ball-point pen
Facility Name A4 IL
Address A� d
Well Location
Well Identification N
press
DIVISION OFWATER QUALITY -GROUNDWATER SECTION
'P.O. BOX.29578
RALEIGH; NC 27626.0518
•(919) M-3221
PERMIT NUMBER: (REQUIgE 6) 0r 1��
Non -Discharge WWiCa�
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED)
Lagoon Septic Tank/Drain Field
Well Diameter Sample (Screened) Interval — Ft. To Ft. Spray Field
e?�r-, 3e N ^ FxrLUF1J1- Well Depth — Ft.
Subsurface Low -Pressure
Piping (LPP)
Depth to Water Level ft. below measuring point (before sampling) Land Application or sludge
Measuring point is r ft. above land surface Z Rotary Distributor Other
Gallons of water pumped/bailed before sampling
Field Analysis: pH Specific Conductance --uMhos Temp. — oC Odor — Appearance
Date Sample CoIlec d , 10-6 -Cc' Date Lab Sample Analyzed In -D --4Z
Laboratory Name ��QCI'M�) Lc(� fCb�C� Certification No. I8
SAMPLES FOR METALS VVLAE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO
COD
Coliform: MF Fecal
Coliform: MF Total
_ mg/I
/100ml
/100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total mg/I
pH (when analyzed) G�units
TOC
mg/I
Chloride
mg/1
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P
mg/I
Al - Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
Ni - Nickel mg/I
Pb - Lead mg/I
Zn - Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
ug/I
ug/I
ug/I
Other (Specify Compounds and
Concentration units)
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
i�/ `Y� )�� See back for instructions.
gnatur of ermit ee (Or Authorized Agent') Date •• Submit blue and yellow copies only to address above.
GW-59 REV. 8/96
LABORATORY ANALYTICAL RESULTS
PARADIGM ANALYTICAL LABORATORIES, INC.
2627 Northchase Parkway S.E.
Wilmington, North Carolina 28405
(910) 350-1903
fax (910) 350-1557
Mr. John Jester Date 09-29-97
Gulfstream Environmental
PO Box 592
Wrightsville Beach, NC 28480
Report Number: G216-1
Client Project ID : 01-0997
Dear Mr. Jester:
Enclosed are the results of the analytical services performed under the
referenced project. Copies of this report and supporting data will be retained in
our files for a period of five years in the event they are required for future
reference. Any samples submitted to our laboratory will be retained for a
maximum of thirty (30) days from date of this report unless other arrangements
are requested.
If there are any questions about the report or the services performed during this
project, please call for assistance. We will be happy to answer any questions or
concerns which you may have.
JThank you for using Paradigm Analytical Labs for your analytical service
projects. We look forward to working with you again on any additional needs
which you may have.
Sincerely,
Paradigm Analytical Laboratories
Laboratory Director
Mark Randall
North Carolina Wastewater Certification #481
PARADIGM ANALYTICAL LABORATORIES,
INC.
Results for Volatiles
by GCMS 624
Client Sample ID: MW-1
Date Analyzed:
9/15/97
Client Project ID: 01-0997
Analyzed By:
WML
Lab Sample ID: 29597
Date Collected:
9/11/97
Lab Project JD: G216-1
Date Received:
9/12/97
Matrix: Water
Dilution:
40.0
Compound
Quantitatlon
Result
Limit (ug/L)
(ug/L)
Benzene
40
BQL
Bromochloromethane
40
BQL
Bromoform
40
BQL
Bromomethane
40
BQL
Carbon tetrachloride
40
BQL
Chlorobenzene
40
BQL
Chloroethane
40
BQL
2-Chloroethyl vinyl ether
200
BQL
Chloroform
40
BQL
Chloromethane
40
BQL
- Dibromochloromethane
40
BQL
1,2-Dichlorobenzene
40
BQL
1,3-Dichlorobenzene
40
BQL
1,4-Dichlorobenzene
40
BQL
1,1-Dichloroethane
40
BQL
1,1-Dichloroethene
40
BQ L
1,2-Dichloroethane
40
BQL
_ trans-1,2-Dichloroethene
40
BQL
1,2-Dichloropropane
40
BQL
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
40
40
BQL
BQL
Dilsopropyl ether (DIPE)
40
BQL
Ethylbenzene
40
BQL
Methylene chloride
200
BQL
Methyl-tert-butyl ether (MTBE)
40
BOL
1,1,2,2-Tetrachloroethane
40
BQL
Tetrachloroethene
40
BQL
Toluene
40
BQL
— Trichloroethene
40
560
1,1,1-Trichloroethane
40
BQL
1,1,2-Trichloroethane
40
BQL
Trichlorofluoromethane
40
BQL
Vinyl chloride
40
BQL
m-,p-Xylene
80
BQL
o-Xylene
40
BQL
Surrogate Standards
Surrogate
Surrogate
Percent
Added
Result
Recovery
Compound
(ug/L)
(ug/L)
1,2-Dichloroethane-d4
10.0
10.0
100
Toluene -dB
i0,0
9.9
gg
Bromorluorobenzene
10.0
9.3
93
Comments:
All results are corrected for dilution.
Flags:
BQL = Below Quantltatlon Limit
Reviewed By: 1JA�-
Pego 1 of 1
PARADIGM ANALYTICAL LABORATORIES,
INC.
Results for Volatiles
by GCMS 624
Client Sample ID: MW-2
Date Analyzed:
9115/97
Client Project ID: 01-0997
Analyzed By:
WML
Lab Sample ID: 29598
Date Collected:
9/11/97
Lab Project ID: G216-1
Date Received:
9/12/97
Matrix: Water
Dilution:
80.0
Compound
Quantltatlon
Result
Lim It (ug/L)
(ug/L)
Benzene
80
BQL
Bromochloromethane
80
BQL
Bromoform
80
BQL
Bromomethane
80
BQL
Carbon tetrachloride
Chlorobenzene
80
80
BQL
BQL
Chloroethane
80
BQL
2-Chloroethyl vinyl ether
400
BQL
Chloroform
80
BQL
'
Chloromethane
80
BQL
Dlbromochloromethane
80
BQL
1,2-Dichlorobenzene
80
BQL
1,3-Dichlorobenzene
80
BQL
1,4-Dichlorobenzene
80
BQL
1,1-Dichloroethane
80
BQL
—.
1,1-Dichloroethene
80
BQL
1,2-Dichloroethane
80
BQL
'J
trans-1,2-Dichloroethene
80
BQL
1,2-Dichloropropane
80
BQL
cis-1,3-Dlchloropropene
80
BQL
trans-1,3-Dichloropropene
80
BQL
'-
Dilsopropyl ether (DIPE)
80
BQL
_
Ethylbenzene
80
BQL
Methylene chloride
400
BOL
Methyl-tert-butyl ether (MTBE)
80
BQL
1,1,2,2-Tetrachloroethane
80
BQL
t
Tetrachloroethene
80
BQL
Toluene
80
BQL
Trichloroethene
80
1400
1,1,1-Trichloroethane
80
BQL
1,1,2-Trichloroethane
80
BQL
Trlchlorolluoromethane
80
BQL
Vinyl chloride
80
BQL
m-,p-Xylene
160
BQL
o-Xylene
80
BQL
Surrogate Standards
Surrogate
Surrogate
Percent
"
Added
Result
Recovery
Compound
(ug/L)
(ug/L)
1,2-Dichloroethane-d4
10.0
9.8
98
Toluene-d8
10.0
9,9
99
Bromofluorobenzene
10.0
9.4
94
Comments:
All results are corrected for dilution.
Flags:
BQL = Below Quantltatlon Limit
Reviewed By: k-
Page 1 of 1
PARADIGM ANALYTICAL LABORATORIES,
INC.
.I
Results for Volatiles
.-
by GCMS 624
Client Sample ID: MW-3
Date Analyzed:
9/15/97
Client Project ID: 01-0997
Analyzed By:
WML
Lab Sample ID: 29599
Date Collected:
9/11/97
Lab Project ID: G216-1
Date Received:
9/12/97
Matrix: Water
Dilution:
10.0
Compound
Quantitatlon
Result
�-
Limit (ug/L)
(ug/L)
Benzene
10
BQL
Bromochloromethane
10
BQL
Bromoform
10
BQL
Bromomethane
10
BQL
Carbon tetrachloride
10
BQL
Chlorobenzene
10
BQL
Chloroethane
10
BQL
2-Chloroethyl vinyl ether
50
BQL
- Chloroform
10
BQL
Chloromethane
10
BQL
Dibromochloromethane
10
BQL
1,2-Dichlorobenzene
10
BQL
1,3-Dichlorobenzene
10
BQL
1,4-Dichlorobenzene
10
BQL
` 1,1-Dichloroethane
10
BQL
1,1-Dichloroethene
10
BQL
1,2-Dichloroethane
10
BQL
trans-1,2-Dichloroethene
10
BQL
1,2-Dlchloropropane
10
BQL
' cis-1,3-Dlchloropropene
10
BQL
f ttans-1,3-Dlchloropropene
10
BQL
Diisopropyl ether (DIPE)
10
BQL
Ethylbenzene
10
BQL
Methylene chloride
50
BQL
Methyl-tert-butyl ether (MTBE)
10
BQL
1,1,2,2-Tetrachloroethane
10
BQL
Tetrachloroethene
10
BQL
Toluene
10
BQL
—' Trichloroethane
10
150
1,1,1-Trichloroethane
10
BQL
1,1,2-Trichloroethane
10
BQL
Trichlorofluoromethane
10
BQL
Vinyl chloride
10
BQL
m-,p-Xylene
20
BQL
o-Xylene
10
BQL
Surrogate Standards
Surrogate
Surrogate
Percent
Added
Result
Recovery
— Compound
(ug/L)
(ug/L)
1,2-Dichloroethane-d4
10.0
10.3
103
Toluene-d6
10.0
10.0
100
Bromofluorobenzene
10.0
9.4
94
Comments:
All results are corrected for dilution.
- Flags:
_ BQL =.Below Quantitatlon Limit
Reviewed By: K*.
Pape 1 of 1
PARADIGM
.I
ANALYTICAL LABORATORIES,
INC.
J
Results for Volatiles
by GCMS 624
Client Sample ID:
MW4
Date Analyzed:
9/22/97
Client Project ID:
01-0997
Analyzed By:
WML
Lab Sample ID:
29600
Date Collected:
9/11197
Lab Project ID:
G216-1
Date Received:
9/12/97
Matrix:
Water
Dilution:
400.0
Compound
Benzene
Bromochloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroelhyl vinyl ether
Chloroform
Chloromethane
D Ib romoch to ro methane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,1-Dichloroelhene
1,2-Dichloroethane
trans-1,2-Dichloroethene
1,2-Dichloropropane
cis-1,3-Dichloropropene
trans-1, 3-Dichloropropene
Dlisopropyl ether (DIPE)
Ethylbenzene
Methylene chloride
Methyl-tert-butyl ether (MTBE)
1,1,2,2-Tetrachloroethane
Tetrachloroethane
Toluene
Trichloroethene
1,1,1-Trichloroetha ne
1,1, 2-Trichloroethane
Trichlorolluorometha ne
Vinyl chloride
m-,p-Xylene
o-Xylene
Surrogate Standards
Compound
1,2-Dichloroethane-d4
Toluene-d8
_ Bromolluorobenzene
Comments:
All results are corrected for dilution.
Flags:
BQL = Below Quantltatlon Limit
Quantitatlon
Limit(ug/L)
400
400
400
400
400
400
400
2000
400
400
400
400
400
400
400
400
400
400
400
400
400
400
400
2000
400
400
400
400
400
400
400
400
400
800
400
Surrogate
Added
(ug/L)
10.0
10.0
10.0
Surrogate
Result
(ug/L)
9.5
10.3
10.1
Result
(ug/L)
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
5500
BQL
BQL
BQL
BQL
BQL
BQL
Percent
Recovery
95
103
101
Reviewed By: AAn—
Pap 1 of 1
PARADIGM
I
ANALYTICAL LABORATORIES,
INC.
Results for Volatiles
-
by GCMS 624
Client Sample ID: MW-5
Date Analyzed:
9/16/97
Client Project ID: 01-0997
Analyzed By:
WML
Lab Sample ID: 29601
Date Collected:
9111/97
Lab Project ID: G216-1
Date Received:
9112/97
Matrix: Water
Dilution:
100.0
• Compound
Quantitatlon
Result
Limit (ug/L)
(ug/L)
Benzene
100
BQL
Bromochloromethane
100
BQL
'Bromoform
100
BQL
Bromomethane
100
BQL
Carbon tetrachloride
100
BQL
Chlorobenzene
100
BQL
Chloroethane
`
100
BQL
2-Chloroethyl vinyl ether
Soo
BQL
Chloroform
100
BQL
1 Chloromethane
100
BQL
Dibromochloromethane
100
BQL
1,2-Dichlorobenzene
100
BQL
+ 1,3-Dichlorobenzene
100
BQL
J 1,4-Dichlorobenzene
100
BQL
1,1-Dichloroethane
100
BQL
_ 1,1-Dichloroethene
100
BQL
1,2-Dichloroethane
100
BQL
trans-1,2-Dichloroethene
100
BQL
1,2-Dichloropropane
100
BQL
cis-1,3-Dichloropropene
100
BQL
trans-1,3-Dichloropropene
100
BQL
Dilsopropyl ether (DIPE)
100
BQL
Ethyibenzene
100.
BQL
Methylene chloride
500
BQL
Methyl-tert-butyl ether (MTBE)
100
BQL
1,1,2, 2-Tetrachloroethane
100
BQL
Telrachloroethene
100
BQL
Toluene
100
BQL
Trichloroelhene
100
1600
1,1,1-Trichloroethane
100
BQ L
1,1, 2-Trichloroethane
100
BQL
Trichlorofluoromethane
100
BQL
Vinyl chloride
100
BQL
- • m-,p-Xylene
200
BQL
o-Xylene
100
BQL
Surrogate Standards
Surrogate
Surrogate
Percent
Added
Result
Recovery
Compound
(ug/L)
(ug/L)
1,2-Dichloroethane-d4
10.0
9.8
96
Toluene-d6
1,0,0
9,6
98
Bromoliuorobenzene
10.0
9.3
93
Comments:
All results are corrected for dilution.
Flags:
BQL = Below Quantitatlon Limit
Reviewed By: Z^i�_
Pago 1 of 1
- PARADIGM ANALYTICAL LABORATORIES,
INC.
Results for Volatiles
--
by GCMS 624
Client Sample ID: MW-6
Date Analyzed:
9122197
Client Project ID: 01-0997
Analyzed By:
WML
Lab Sample ID: 29602
Date Collected:
9111/97
Lab Project ID: G216-1
Date Received:
9/12/97
Matrix: Water
Dilution:
80.0
Compound
Quantltatlon
Result
Llmlt (ug/L)
(ug/L)
Benzene
80
BQL
Bromochloromethane
80
BQL
Bromoform
80
BQL
Bromomethane
80
BQL
Carbon tetrachloride
80
BQL
— Chlorobenzene
80
BQL
Chloroethane
80
BQL
2-Chloroethyl vinyl ether
400
BQL
Chloroform
80
BQL
Chioromethane
80
BQL
_ Dibromochloromethane
80
BQL
1,2-Dichlorobenzene
80
BQL
1,3-Dichlorobenzene
80
BQL
1,4-Dichlorobenzene
80
BQL
1,1-Dichloroethane
80
BQL
M-Dichloroethene
80
BQL
1,2-Dichloroethane
80
BQL
trans-1,2-Dichloroethene
80
BQL
1,2-Dlchloropropane
80
BQL
cis-1,3-Dlchloropropene
80
BQL
trans-1,3-Dlchloropropene
80
BQL
Dlisopropyl ether (DIPE)
80
BQL
Ethylbenzene
J
80
BQL
Methylene chloride
400
BQL
Methyl -tart -butyl ether (MTBE)
80
BQL
1,1,2,2-Tetrach loroelhane
80
BQL
- Tetrachloroelhene
80
BQL
( Toluene
80
BQL
_ Trichloroethane
80
720
1,1,1-Trichloroethane
80
BQL
1,1, 2-Trichloroethane
80
BQL
Trichlorolluoromethane
80
BQL
Vinyl chloride
80
BQL
_ m-,p-Xylene
160
BQL
o-Xylene
80
BQL
Surrogate Standards
Surrogate
Surrogate
Percent
Added
Result
Recovery
— Compound
(ug/L)
(ug/L)
1,2-Dichloroethane-d4
10.0
10.1
101
Toluone-d8
10.0
10.4
104
Bromofluorobenzene
10.0
10.5
105
Comments:
All results are corrected for dilution.
Flogs:
BQL = Below Quantilallon Limit
Reviewed By: /)--
Pepe 1 of 1
PARADIGM ANALYTICAL LABORATORIES, INC.
L_
Results for Volatiles
by GCMS 624
_
Client Sample ID: MW-7
Date Analyzed:
9/22/97
Client Project ID: 01-0997
Analyzed By:
WML
Lab Sample ID: 29603
Date Collected:
9/11/97
Lab Project,ID: G216-1
Date Received:
9/12/97
Matrix: Water
Dilution:
100.0
Compound
Quantitatlon
Result
_
Lim It (ug/L)
(ug/L)
Benzene
100
BQL
Bromochloromethane
100
BQL
Bromoform
100
BQL
Bromomelhane
100
BQL
Carbon tetrachloride
100
BQL
Chlorobenzene
100
BQL
Chloroethane
100
BQL
2-Chloroelhyl vinyl ether
500
BQL
Chloroform
100
BQL
i
Chloromethane
100
BQL
Dibromochloromethane
100
BQL
1,2-Dlchlorobenzene
100
BQL
1,3-Dlchlorobenzene
100
BQL
1,4-Dlchlorobenzene
100
BQL
1,1-Dichloroethane
100
BQL
1,1-Dlchloroethene
100
BQL
1,2-Dichloroethane
100
BQL
trans-1,2-Dichloroethene
100
BQL
1,2-Dichloropropane
100
BQL
cis-1,3-Dichloropropene
100
BQL
trans-1,3-Dichloropropene
100
BQL
-
Diisopropyl ether (DIPE)
100
BQL
Ethylbenzene
100
BQL
Methylene chloride
500
BQL
Methyl-tert-butyl ether (MTBE)
100
BQL
1,1,2,2-Tetrachloroethane
100
BQL
Tetrachloroethene
100
BQL
Toluene
100
BQL
_
Trichloroethene
100
1100
1,1,1-Trichloroethane
100
BQL
1,1, 2-Trichloroethane
100
BQL
Trichlorolluoromethane
100
BQL
Vinyl chloride
100
BQL
m-, p-Xylene
200
BQL
o-Xylene
100
BQL
Surrogate Standards
Surrogate
Surrogate
Percent
Added
Result
Recovery
Compound P
(ug/L)
(ug/L)
1,2-Dichloroethane-d4
10.0
10.1
101
Toluene-d0
10.0
10.5
105
Bromoflucrobenzene
10.0
10.1
101
Comments:
All results are corrected for dilution.
Flags:
BQL = Below Quantltation Limit
Reviewed By: 4N..
Page 1 or 1
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GGMS 624
Client Sample ID: MW-8 Date Analyzed: 9/15/97
Client Project ID: 01-0997 Analyzed By: CKC
Lab Sample ID: 29604 Date Collected: 9111/97
Lab Project ID: G216-1 Date Received: 9/12/97
Matrix: Water Dilution: 1.0
Compound
Quantitatlon
Result
Limit (ug/L)
(ug/L)
Benzene
1
BQL
Bromochloromethane
1
BQL
Bromoform
1
BQL
Bromomethane
1
BQL
Carbon tetrachloride
1
BQL
Chlorobenzene
1
BQL
Chloroethane
1
BQL
2-Chloroethyl vinyl ether
5
BQL
Chloroform
1
BQL
Chloromethane
1
BQL
Dibromochloromethane
1
BQL
1,2-Dichlorobenzene
1
BQL
1,3-Dichlorobenzene
1
BQL
1,4-Dichlorobenzene
1
BQL
1,1-Dichloroethane
1
BQL
1,1-Dichloroethene
1
BQ L
1,2-Dichloroethane
1
BQL
trans-1,2-Dichloroethene
1
BQL
1,2-Dichloroprdpane
1
BQL
cis-1,3-Dichloropropene
1
BQL
trans-1,3-Dichloropropene
1
BQL
Dlisopropyl ether (DIPE)
1
BQL
Ethylbenzene
1
BQL
Methylene chloride
5
BQL
Methyl -tart -butyl ether (MTBE)
1
BQL
1,1,2,2-Tetrachloroethane
1
BQL
Tetrachloroethene
1
BQL
Toluene
1
BQL
Trichloroethene
1
18
1,1,1-Trichloroelhane
1
BQL
1,1,2-Tiichloroethane
1
BQL
Trichlorofluoromethane
1
BQL
Vinyl chloride
1
BQL
m-,p-Xylene
2
BQL
o-Xylene
1
BQL
Surrogate Standards
Surrogate
Surrogate
Percent
Added
Result
Recovery
Compound
(ug/L)
(ug/L)
1,2-Dichloroethane-d4
10.0
9.4
94
Toluene-d8
10.0
9.7
97
Bromolluorobenzene
10.0
9.7
97
Comments:
All results are corrected for dilution.
Flags:
BQL = Below Quantitatlon Limit
Reviewed By: tw+
Page 1 of 1
PARADIGM ANALYTICAL LABORATORIES,
INC.
J
Results for Volatiles
._
by GCMS 624
Client Sample ID: MW-9
Date Analyzed:
9115/97
Client Project ID: 01-0997
Analyzed By:
CKC
Lab Sample ID: 29605
Date Collected:
9111197
Lab Project ID: G216-1
Date Received:
9/12/97
Matrix: Water
Dilution:
1.0
Compound
Quantltatlon
Result
Limit (ug/L)
(ug/L)
Benzene
1
BQL
Bromochloromethane
1
BQL
Bromoform
1
BQL
Bromomethane
1
BQL
Carbon tetrachloride
1
BQL
Chlorobenzene
1
BQL
Chloroethane
1
BQL
2-Chloroethyl vinyl ether
5
BQL
Chloroform
1
BQL
Chloromethane
1
BQL
Dibromochloromethane
1
BQL
1,2-Dichlorobenzene
1
BQL
1,3-Dichlorobenzene
1
BQL
J 1,4-Dichlorobenzene
1
BQL
1,1-Dichloroelhane
1
BQL
_ 1,1-Dichloroethene
1
BQL
1,2-Dichloroethane
1
BQL
trans-1,2-Dichloroethene
1
BQL
1,2-Dichloropropane
1
BQL
-I cis-1,3-Dichloropropene
1
BQL
trans-1,3-Dichloropropene
1
BQL
_ Dilsopropyl ether (DIPE)
1
BQL
Ethylbenzene
1
BQL
Methylene chloride
5
BQL
Methyl-tert-butyl ether (MTBE)
1
BQL
—" 1,1,2,2-Tetrachloroethane
1
BQL
Tetrachloroelhene
1
BQL
Toluene
1
BQL
_ Trichloroethene
1
17
1,1,1-Trichloroethane
1
BQL
1,1,2-Trichloroethane
1
'BQL
Trichlorofluoromelhane
1
BQL
Vinyl chloride
1
BQL
_ m-,p-Xylene
2
BQL
o-Xylene
1
BQL
Surrogate Standards
Surrogate
Surrogate
Percent
Added
Result
Recovery
Compound
(ug/L)
(ug/L)
1,2-Dichloroelhane-d4
10.0
9.5
95
Toluene-d6
10.0
9.3
93
Bromofluorobenzene
10.0
9.9
99
Comments:
All results are corrected for dilution.
Flags:
BQL = Below Quantltatlon Limit
Reviewed By: (a=_
Pape 1 of 1
PARADIGM ANALYTICAL LABORATORIES,
INC.
Results for Volatiles
by GCMS 624
Client Sample ID: MW-10
Date Analyzed:
9/16/97
Client Project ID: 01-0997
Analyzed By:
WML
Lab Sample ID: 29606
Date Collected:
9/11/97
Lab Project ID: G216-1
Date Received:
9/12/97
Matrix: Water
Dilution:
50.0
Compound
Quantitatlon
Result
Limit (ug/L)
(ug/L)
Benzene
50
BQL
Bromochloromethane
50
BQL
Bromoform
5o
BQL
Bromomethane
50
BQL
Carbon tetrachloride
50
BQL
Chlorobenzene
50
BQL
Chloroethane
50
BQL
2-Chloroethyl vinyl ether
250
BQL
_
Chloroform
50
BQL
Chloromethane
50
BQL
Dibromochloromethane
50
BQL
1,2-Dichlorobenzene
50
BQL
1,3-Dichlorobenzene
50
BQL
IJI
1,4-Dichlorobenzene
50
BQL
1,1-Dichloroethane
50
BQL
_
1,1-Dichloroethene
50
BQL
1,2-Dichloroethane
50
BQL
trans-1.2-Dichloroethene
50
BQL
1,2-Dichloropropane
50
BQL
-I
cls-1,3-Dlchloropropene
50
BQL
trans-1,3-Dlchloropropene
5o
BQL
Dlisopropyl ether (DIPE)
50
BQL
Ethylbenzene
50
BQL
Methylene chloride
250
BQL
Methyl-tert-butyl ether (MTBE)
50
BQL
1,1, 2,2-Tetrachloroethane
50
BQL
Tetrachloroethene
Toluene
50
50
BQL
BQL
Trichloroelhene •
50
580
1,1,1-Trichloroethane
50
BQ L
1,1,2-Trichloroethane
so
BQL
Trichlorofluoromethane
50
BQL
Vinyl chloride
50
BQL
m-,p-Xylene
100
BQL
o-Xylene
50
BQL
I
Surrogate Standards
Surrogate
Surrogate
Percent
Added
Result
Recovery
IJ
Compound
(ug/L)
(ug/L)
1,2-Dichioroethane-d4
10.0
10.3
103
Toluene-d8
10.0
10.1
101
Bromofluorobenzene
10.0
9.3
93
Comments:
All results are corrected for dilution.
Flags:
BQL = Below Quantitatlon Limit
Reviewed By: n _
Page 1 of 1
a
PARADIGM ANALYTICAL LABORATORIES,
INC.
J
Results for Volatiles
-
by GCMS 624
Client Sample ID: MW-11
Date Analyzed:
9/16/97
Client Project ID: 01-0997
Analyzed By:
WML
Lab Sample ID: 29607
Date Collected:
9/11/97
Lab Project ID: G216-1
Date Received:
9/12/97
Matrix: Water
Dilution:
20.0
Compound
Quantltation
Result
Limit (ug/L)
(ug/L)
Benzene
20
BQL
Bromochloromethane
20
BQL
Bromoform
20
BQL
Bromomethane
20
BQL
Carbon tetrachloride
20
BQL
Chlorobenzene
20
BQL
Chloroethane
20
BQL
2-Chloroethyl vinyl ether
100
BQL
Chloroform
20
BQL
Chloromethane
20
BQL
Dibromochloromethane
20
BQL
1,2-Dichlorobenzene
20
BQL
1 1,3-Dichlorobenzene
20
BQL
1,4-Dichlorobenzene
20
BQL
'— 1,1-Dichloroethane
20
BQL
_ 1,1-Dichloroethene
20
BQL
1,2-Dichloroethane
20
BQL
-._ trans-1,2-Dichloroethene
20
BQL
1,2-Dichloropropane
20
BQL
cis-1,3-Dichloropropene
20
BQL
trans-1,3-Dichloropropene
20
BQL
-- Dllsopropyl ether (DIPE)
20
BQL
Ethyibenzene
20
BQL
Methylene chloride
100
BQL
Methyl-tert-butyl ether (MTBE)
20
BQL
1,1,2,2-Tetrachloroethane
20
BQL
Tetrachioroethene
20
BQL
Toluene
20
BQL
-- Trcchloroethene
20
410
1,1,1-Trlchloroethane
20
BQL
1,1,2-Trlchloroethane
20
BQL
Trlchlorofluoromethane
20
BQL
Vinyl chloride
20
BQL
m-,p-Xylene
40
BQL
o-Xylene
20
BQL
Surrogate Standards
Surrogate
Surrogate
Percent
Added
Result
Recovery
Compound
(ug/L)
(ug/L)
1,2-Dichloroethane-d4
10.0
9.9
99
Toluene -de
10.0
10.1
101
Bromofluorobenzene
10.0
9.2
92
Comments:
All results are corrected for dilutlon.
Flags:
BQL = Below Quantitatlon Llmit
Revlewed By: hag,`
Page 1 of 1
PARADIGM
ANALYTICAL LABORATORIES, INC.
y
Results for Volatiles
by GCMS 624
Client Sample ID: MW-12
Date Analyzed:
9/18/97
Client Project ID: 01-0997
Analyzed By:
WML
Lab Sample ID: 29608
Date Collected:
9/11/97
Lab Project ID: G216-1
Date Received:
9/12/97
Matrix: Water
Dilution:
1.0
Compound
Quantitatlon
Result
Limit (ug/L)
(ug/L)
Benzene
1
BQL
Bromochloromethane
1
BQL
Bromoform
1
BQL
Bromomethane
1
BQL
Carbon tetrachloride
1
BQL
Chlorobenzene
1
BQL
Chloroethane'
1
BQL
2-Chloroethyl vinyl ether
5 .
BQL
Chloroform
1
BQL
Chloromethane
1
BQL
Dibromochloromethane
1
BQL
1,2-Dichlorobenzene
1
BQL
1,3-Dichlorobenzene
1
BQL
1,4-Dichlorobenzene
1
BQL
1,1-Dichloroethane
1
BQL
1,1-Dichloroethene
1
BQL
1,2-Dichloroethane
1
BQL
trans-1,2-Dichloroethene
1
BQL
1,2-Dichloropropane
1
BQL
cis-1,3-Dichloropropene
1
BQL
trans-1,3-Dichloropropene
1
BQL
Diisopropyl ether (DIPE)
1
BQL
Ethylbenzene
1
BQL
Methylene chloride
5
BQL
Methyl-tert-butyl ether (MTBE)
1
BQL
1,1,2,2-Tetrachloroethane
1
BQL
Tetrachloroelhene
Toluene
1
1
BQL
6
Trichloroelhene •
1
3
y
1,1,1-Trichloroelhane
1
BQL
1,1, 2-Trichloroethane
1
BQL
Trichlorofluoromethane
1
BQL
Vinyl chloride
1
BQL
m-,p-Xylene
2
BQL
o-Xylene
1
BQL
Surrogate Standards
Surrogate
Surrogate
Percent
Added
Result
Recovery
Compound
(ug/L)
(ug/L)
1,2-Dichloroethane-d4
10.0
10.4
104
Toluene-d8
10.0
7.4
74
Bromofluorobenzene
10.0
8.9
89
Comments:
All results are corrected for dilution.
Flags:
BQL = Below Quantitation Limit
Reviewed By: v ,
Page 1 of 1
i
.-J
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GGMS 624
Client Sample ID: MW-13 Date Analyzed: 9116/97
Client Project ID: 01-0997 Analyzed By: WML
Lab Sample ID: 29609 Date Collected: 9/11/97
Lab Project ID: G216-1 Date Received: 9/12/97
Matrix: Water Dilution: 4.0
Compound
Quantitation
Result
Limit (ug/L)
(ug/L)
Benzene
4
BQL
Bromochloromethane
4
BQL
Bromoform
4
BQL
Bromomethane
4
BQL
Carbon tetrachloride
4
BQL
Chlorobenzene
4
BQL
Chloroethane
4
BQL
2-Chloroethyl vinyl ether
20
BQL
Chloroform
4
BQL
Chlbromethane
4
BQL
Dibromochloromethane
4
BQL
1,2-Dichlorobenzene
4
BQL
1,3-Dichlorobenzene
4
BQL
1,4-Dichlorobenzene
4
BQL
1,1-Dichloroethane
4
BQL
1,1-Dichloroethene
4
BQL
1,2-Dichloroethane
4
BQL
trans-1,2-Dichloroethene
4
BQL
1,2-Dichloropropane
4
BQL
cis-1,3-Dichloropropene
4
BQL
trans-1,3-Dichloropropene
4
BQL
Dlisopropyl ether (DIPE)
4
BQL
Ethylbenzene
4
BQL
Methylene chloride
20
BQL
Methyl-tert-butyl ether (MTBE)
4
BQL
1,1,2,2-Tetrachloroethane
4
BQL
Tetrachloroethene
4
BQL
Toluene
4
BQL
Trichloroethene
4
66
1,1,1-Trlchloroethane
4
BQL
1,1,2-Trichloroethane
4
BQL
Trichlorofluoromethane
4
BQL
Vinyl chloride
4
BQL
m-,p-Xylene
8
BQL
o-Xylene
4
BQL
Surrogate Standards
Surrogate
Surrogate
Percent
Added
Result
Recovery
Compound
(ug/L)
(ug/L)
1,2-Dichloroethane-d4
10.0
10.3
103
Toluene-d8
10.0
9.3
93
Bromofluorobenzene
10.0
8.8
88
Comments:
All results are corrected for dilution.
Flags:
BQL = Below Quanlltatlon Limit
Page 1 of 1
Reviewed By: hv�
PARADIGM ANALYTICAL LABORATORIES,
INC.
Results for Volatiles
by GCMS 624
Client Sample ID:
MW-14
Date Analyzed:
9/15197
Client Project ID:
01-0997
Analyzed By:
CKC
Lab Sample ID:
29610
Date Collected:
9/11197
Lab Project ID:
G216-1
Date Received:
9112/97
Matrix:
Water
Dilution:
1.0
Compound
Benzene
Bromochloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
D Ib romochloro methane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,1-Dichloroethene
1,2-Dichloroethane
trans-1,2-Dlchloroethene
1,2-Dichloropropane
cis-1, 3-Dichloropropene
trans-1,3-Dichloropropene
Diisopropyl ether (DIPE)
Ethylbenzene
Methylene chloride
Methyl-lert-butyl ether (MTBE)
1,1,2.2-Tetrachloroethane
Tetrachloroethane
Toluene
Trichloroethene
1,1,1-Ticchloroethane
1,1,2-Trlch loroethane
Tri chlo roll uorom et h a n e
Vinyl chloride
m-,p-Xylene
o-Xylene
Quantitatlon
Limit (ug/L)
Surrogate Standards
Surrogate
Added
Compound
(ug/L)
1,2-Dichloroethane-d4
10.0
Toluene -do
10.0
Bromolluorobenzene
10.0
Comments:
All results are corrected for dilution.
Flags:
SOL = Below Quantitatlon Limit
Result
(ug/L)
SOL
SOL
BQL
SOL
SOL
BQL
BQL
SOL
SOL
SOL
SOL
SOL
SOL
BQL
SOL
SOL
SOL
BQL
SOL:
SOL
BQL
SOL
SOL
BQL
SOL
BQL
BQL
SOL
22
SOL
BQL
SOL
BQL
SOL
SOL
Surrogate
Percent
Result
Recovery
(ug/L)
9.9
99
7.7
77
9.6
96
Pago 1 of 1
Reviewed By: 6,1y_
j PARADIGM ANALYtICAL LABORATORIES,
INC.
Results for Volatiles
-
by GCMS 624
Client Sample ID: RC-15
Date Analyzed:
9/15/97
Client Project ID: 01-0997
Analyzed By:
CKC
Lab Sample ID: 29611
Date Collected:
9111197
Lab Project ID: G216-1
Date Received:
9/12197
Matrix: Water
Dilution:
1.0
Compound
Quantltatlon
Result
Limit(ug/L)
(ug/L)
Benzene
1
BQL
Bromochloromethane
1
BQL
Bromoform
1
BQL
Bromomethane
1
BQL
Carbon tetrachloride
1
BQL
Chlorobenzene
1
BQL
Chloroethane
1
BQL
2-Chloroethyl vinyl ether
5
BQL
Chloroform
1
BQL
Chloromethane
1
BQL
Dibromochloromethane
1
BQL
1,2-Dlchlorobenzene
1
BQL
1,3-Dlchlorobenzene
1
BQL
1,4-Dlchlorobenzene
1
BQL
1,1-Dichloroelhane
1
BQL
1,1-Dichloroethene
1
BQL
1,2-Dichloroelhane
1
BQL
trans-1,2-Dichloroethene
1
BQL
1,2-Dlchloropropane
1
BQL
cis-1,3-Dichloropropene
1
BQL
trans-1,3-Dichloropropene
1
BQL
Dlisopropyl ether (DIPE)
1
BQL
Ethylbenzene
1
BQL
Methylene chloride
5
BQL
J Methyl-tert-butyl ether (MTBE)
1
BQL
1,1,2,2-Telrachloroethane
1
BQL
Tetrachloroethene
1
BQL
Toluene
1
BQL
- Trichloroethene •
1
BQL
1,1,1-Trlchloroethane
1
BQL
1,1,2-Trlchloroethane
1
BQL
Trichloro0uoromelhane
1
BQL
Vinyl chloride
1
BQL
-� m-,p-Xylene
2
BQL
o-Xylene
J
1
BQL
Surrogate Standards
Surrogate
Surrogate
Percent
Added
Result
Recovery
Compound
(ug/L)
(ug/L)
1,2-Dlchloroethane-d4
10.0
9.7
97
Toluene-d8
10.0
8.7
87
Bromofluorobenzene
10.0
9.8
98
Commonts:
All results are corrected for dilution.
Flags:
BQL =Below Quantltatlon Limit
Reviewed By: r%
Pape 1 of 1
j PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 624
Client Sample ID: RW-1
Date Analyzed:
9/16/97
Client Project ID: 01-0997
Analyzed By:
WML
Lab Sample ID: 29612
Date Collected:
9/11/97
Lab Project ID: G216-1
Date Received:
9/12/97
Matrix: Water
Dilution:
50.0
Compound
Quantitatlon
Result
Limit (ug/L)
(ug/L)
Benzene
50
BQL
Bromochloromethane
50
BQL
Bromoform
5o
BQL
- Bromomelhane
50
BQL
Carbon tetrachloride
50
BQL
Chlorobenzene
50
BQL
Chloroethane
50
BQL
2-Chloroethyl vinyl ether
250
BQL
Chloroform
50
BQL
Chloromelhane
50
BQL
Dibromochloromethane
50
BQL
1,2-Dichlorobenzene
50
BQL
1,3-Dichlorobenzene
50
BQL
1,4-Dichlorobenzene
50
BQL
1,1-Dichloroethane
50
BQL
_ 1,1-Dichloroethene
50
BQL
1,2-Dichloroethane
50
BQL
trans-1,2-Dichloroethene
50
BQL
1,2-Dichloropropane
50
BQL
cis-1,3-Dichloropropene
50
BQL
trans-1,3-Dichloropropene
50
BQL
-- Dlisopropyl ether (DIPE)
50
BQL
Ethylbenzene
50
BQL
Methylene chloride
250
BQL
Methyl-tert-butyl ether (MTBE)
50
BQL
1,1,2,2-Tetrachloroethane
50
BQL
Tetrachloroelhene
5o
BQL
Toluene
50
BQL
Trichloroethene
50
1200
1,1,1-Trichloroethane
50
BQL
1,1, 2-Trichloroethane
50
BQL
Trichlorofluoromethane
50
BQL
Vinyl chloride
50
BQL
m-,p-Xylene
100
BQL
o-Xylene
50
BQL
Surrogate Standards
Surrogate
Surrogate
Percent
Added
Result
Recovery
Compound
(ug/L)
(ug/L)
1,2-Dichloroethane-d4
10.0
9.9
99
Toluene-d8
10.0
10.0
100
Bromofluorobenzene
10.0
9.5
95
Comments:
All results are corrected for dilution.
Flags:
BQL = Below Quantitatlon Limit
Reviewed By: km`
Papa 1 of f
PARADIGM
ANALYTICAL LABORATORIES,
INC.
Results for Volatiles
by GCMS 624
Client Sample ID:
RW-2
Date Analyzed:
9/16/97
Client Project ID:
01-0997
Analyzed By:
WML
Lab Sample ID:
29613
Date Collected:
9/11/97
Lab Project ID:
G216-1
Date Received:
9/12/97
Matrix:
Water
Dilution:
100.0
Compound
Benzene
Bromochloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
2-Chloroethyl vinyl ether
Chloroform
Chloromethane
D i b ro m o c h l o ro m et h a n e
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1,1-Dichloroethane
1,1-Dichloroethene
1,2-Dichloroethane
trans-1, 2-Dichloroethene
1,2-Dichloropropane
cis-1, 3-Dlch to roprop a ne
trans-1,3-Dlchloropropene
Dlisopropyl ether (DIPE)
Ethylbenzene
Methylene chloride
Methyl-tert-butyl ether (MTBE)
1,1,2, 2-Tetrachloroethane
Tetrachloroethene
Toluene
Trichloroethene
1,1,1-Trichloroelhane
1,1, 2-Trichloroethane
Trichlorofluorom ethane
Vinyl chloride
m-,p-Xylene
o-Xylene
Surrogate Standards
Compound
1, 2-Dichloroethane-d4
Toluene-d0
Bromofluorobenzene
Comments:
All results are corrected for dilution.
Flags:
BQL = Below Quantitatlon Limit
Quantitatlon
Limit (ug/L)
100
100
100
100
100
100
100
500
100
100
100
100
100
100
100
100
100
100
100
100
100
100
100
500
100
100
100
100
100
100
100
100
100
200
100
Surrogate
Added
(ug/L)
10.0
10.0
10.0
Surrogate
Result
(ug/L)
10.1
10.0
9.1
Result
(ug/L)
BQL
BQL
BQL
BQL
BQL
BOIL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
1600
BQL
BQL
BQL
BQL
BQL
BQL
Percent
Recovery
101
100
91
Reviewed By:
Page 1 of 1
J
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 624
Client Sample ID: RW-3 Date Analyzed: 9/18197
Client Project ID: 01-0997 Analyzed By: WML
Lab Sample ID: 29614 Date Collected: 9111/97
Lab ProjectlD: G216-1 Date Received: 9/12/97
Matrix: Water Dilution: 80.0
Compound
Quantltatlon
Result
Limit (ug/L)
(ug/L)
Benzene
80
BQL
Bromochloromethane
80
BQL
Bromoform
80
BQL
Bromomethane
80
BQL
Carbon tetrachloride
80
BQL
Chlorobenzene
80
BQL
Chloroethane
80
BQL
2-Chloroethyl vinyl ether
400
BQL
Chloroform
80
BQL
Chloromethane
80
BQL
Dibromochloromethane
80
BQL
1,2-Dichlorobenzene
80
BQL
1,3-Dichlorobenzene
80
BQL
1,4-Dichlorobenzene
80
BQL
1,1-Dichloroethane
80
BQL
1,1-Dichloroelhene
80
BQL
1,2-Dichloroethane
80
BQL
trans-1,2-Dichloroethene
80
BQL
1,2-Dlchloropropane
80
BQL
cis-1,3-Dlchloropropene
80
BQL
trans-1,3-Dlchloropropene
80
BQL
Dllsopropyl ether (DIPE)
80
BQL
Ethylbenzene
80
BQL
Methylene chloride
400
BQL
Methyl-tert-butyl ether (MTBE)
80
BQL
1,1,2,2-Tetrachloroethane
80
BQL
Tetrachloroethene
80
BQL
Toluene
80
BQL
Trichloroethene
80
1300
1,1,1-Trichloroethane
80
BQL
1,1,2-Trichloroethane
80
BQL
Trichlorofiuoromethane
80
BQL
Vinyl chloride
80
BQL
m-,p-Xylene
160
BQL
o-Xylene
80
BQL
Surrogate Standards
Surrogate
Surrogate
Percent
Added
Result
Recovery
Compound
(ug/L)
(ug/L)
1,2-Dichloroethane-d4
10.0
10.2
102
Toluene-d8
10.0
10.2
102
Bromofluorobenzene
10.0
9.8
98
Comments:
All results are corrected for dilution.
Flags:
BQL = Below Quantltatlon Limit
Pago I of 1
Reviewed By: M ,
PARADIGM
ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GCMS 624
Client Sample ID: Influent
Date Analyzed:
9119/97
Client Project ID: 01-0997
Analyzed By:
WML
Lab Sample ID: 29615
Date Collected:
9/11197
Lab Project ID: G216-1
Date Received:
9/12/97
Matrix: Water
Dilution:
80.0
Compound
Quantitatlon
Result
Limit (ug/L)
(ug/L)
Benzene
80
BQL
Bromochloromethane
80
BQL
Bromoform
80
BQL
Bromomethane
80
BQL
Carbon tetrachloride
80
BQL
Chlorobenzene
80
BQL
Chloroethane
80
BQL
2-Chloroethyl vinyl ether
400
BQL
Chloroform
80
BQL
Chloromethane
80
BQL
Dibromochloromethane
80
BQL
1,2-Dichlorobenzene
80
BQL
1,3-Dichlorobenzene
80
BQL
1,4-Dichlorobenzene
80
BQL
1,1-Dichloroethane
80
BQL
1,1-Dichloroethene
80
BQL
1,2-Dichloroethane
80
BQL
trans-1,2-Dichloroethene
80
BQL
1,2-Dichloropropane
80
BQL
cis-1,3-Dichloropropene
80
BQL
trans-1,3-Dichloropropene
80
BQL
Dilsopropyl ether (DIPE)
80
BQL
Elhylbenzene
80
BQL
Methylene chloride
400
BQL
Methyl-tert-butyl ether (MTBE)
80
BQL
1,1,2,2-Tetrachloroethane
80
BQL
Telrachloroethene
80
BQL
Toluene
80
BQL
Trichloroethene
80
1100
1. 1, 1-Trichloroethane
80
BQL
1,1,2-Trichloroethane
80
BQL
Trichlorofluoromethane
80
BQL
Vinyl chloride
80
BQL
m-,p-Xylene
160
BQL
o-Xylene
80
BQL
Surrogate Standards
Surrogate
Surrogate
Percent
Added
Result
Recovery
Compound
(ug/L)
(ug/L)
1,2-Dichloroethane-d4
10.0
10.2
102
Toluene-d8
10.0
10.2
102
Bromofluorobenzene
10.0
10.1
101
Comments:
All results are corrected for dilution.
Flags:
BQL = Below Quantitatlon Limit
Reviewed By: JNd�
Pape 1 of 1
PARADIGM
ANALYTICAL LABORATORIES,
INC.
Results for Volatiles
by GCMS 624
Client Sample ID: Effluent
Date Analyzed:
9/19/97
Client Project ID: 01-0997
Analyzed By:
WML
Lab Sample ID: 29616
Date Collected:
9/11/97
Lab Project ID: G216-1
Date Received:
9112/97
Matrix: Water
Dilution:
5.0
Compound
Quantitation
Result
Limit (ug/L)
(ug/L)
Benzene
5
BQL
Bromochioromethane
5
BQL
Bromoform
5
BQL
Bromomethane
5
BQL
Carbon tetrachloride
5
BQL
Chlorobenzene
5
BQL
Chloroelhane
6
BQL
2-Chloroethyl vinyl ether
25
BQL
Chloroform
5
BQL
Chloromethane
5
BQL
Dibromochloromethane
5
BQL
1,2-Dichlorobenzene
5
BQL
1,3-Dichlorobenzene
5
BQL
1,4-Dichlorobenzene
5
BQL
1,1-Dichloroethane
5
BQL
1,1-Dichloroethene
5
BQL
1,2-Dichloroethane
5
BQL
trans-1,2-Dichloroethene
5
BQL
1,2-Dichloropropane
5
BQL
cis-1,3-Dichloropropene
5
BQL
trans-1,3-Dichloropropene
5
BQL
Dlisopropyl ether (DIPE)
5
BQL
Elhylbenzene
5
BQL
Methylene chloride
25
BQL
Methyl-tert-butyl ether (MTBE)
5
BQL
1,1,2,2-Telrachloroethane
5
BQL
Telrachloroelhene
5
BQL
Toluene
5
BQL
Trichloroelhene
5
100
1,1,1-trichloroethane
5
BQL
1,1,2-Trichloroethane
5
BQL
Trichlorolluoromethane
5
BQL
Vinyl chloride
5
BQL
m-,p-Xylene
10
BQL
o-Xylene
5
BQL
Surrogate Standards
Surrogate
Surrogate
Percent
Added
Result
Recovery
Compound
(ug/L)
(ug/L)
1,2-Dichloroethane-d4
10.0
10.0
100
Toluene -dB
10.0
10.2
102
Bromolluorobenzene
10.0
9.6
96
Comments:
All results are corrected for dilution.
Flags:
BQL = Below Quantitation Limit
Reviewed By: h e
Pago 1 of 1
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MWA
Client Project ID:
01-0997
Lab Sample ID:
29597
Lab Project ID:
G216-1
Matrix:
Water
Parameter
'pH
Date Collected:
9111/97
Date Received:
9/12197
Analyzed By:
MAG
Result Date
Analyzed
6.61 9/23/97
'NCDEM requires that pH be analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
Reviewed By: yn=�-
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-2
Date Collected: 9/11/97
Client Project ID:
01-0997
Date Received: 9/12/97
Lab Sample ID:
29598
Analyzed By: MAG
Lab Project ID:
G216-1
Matrix:
Water
Parameter Result Date
Analyzed
'pH 5.82 9/23/97
'NCDEM requires that pH be,analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
Reviewed By: }.T,
PARADIGNI ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-3
Client Project ID:
01-0997
Lab Sample ID:
29599
Lab Project ID:
G216-1
Matrix:
Water
Parameter
.pH
Date Collected: 9/11197
Date Received: 9112/97
Analyzed By: MAG
Result Date
Analyzed
5.98 9/23/97
'NCDEM requires that pH.be analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
Reviewed By: M.
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-4
Date Collected:
9/11197
Client Project ID:
01-0997
Date Received:
9/12/97
Lab Sample ID:
29600
Analyzed By:
MAG
Lab Project ID:
G216-1
Matrix:
Water
Parameter
Result
Date
Analyzed
'pH
5.67
9/23197
'NCDEM requires that pH be analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
Reviewed By: Ampy
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-5
Client Project ID:
01-0997
Lab Sample ID:
29601
Lab Project ID:
G216-1
Matrix:
Water
Parameter
'pH
Date Collected: 9/11/97
Date Received: 9112/97
Analyzed By: MAG
Result Date
Analyzed
5.80 9/23/97
'NCDEM requires that pH be analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
Reviewed By: fwi
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
f,
Client Sample ID:
MW-6
Client Project ID:
01-0997
Lab Sample ID:
29602
Lab Project ID:
G216-1
Matrix:
Water
Parameter
'pH
Dale Collected:
9111/97
Date Received:
9/12/97
Analyzed By:
MAG
Result Date
Analyzed
5.42 9/23/97
'NCDEM requires that pH be analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
Reviewed By: Ma,
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-7
Date Collected: 9/11/97
Client Project ID:
01-0997
Date Received: 9112/97
Lab Sample ID:
29603
Analyzed By: MAG
Lab Project ID:
G216-1
Matrix:
Water
Parameter
Result Date
Analyzed
'pH
5.32 9/23/97
'NCDEM requires that pH be analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
Reviewed By: nv
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-8
Date Collected:
9111197
Client Project ID:
01-0997
Date Received:
9/12/97
Lab Sample ID:
29604
Analyzed By:
MAG
Lab Project ID:
G216-1
Matrix:
Water
Parameter
Result
Date
Analyzed
'pH
5.44
9/23/97
'NCDEM requires that pH be analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
Reviewed By: j,
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-9
Client Project ID:
01-0997
Lab Sample ID:
29605
Lab Project ID:
G216-1
Matrix:
Water
Parameter
'pH
Date Collected:
9/11197
Date Received:
9/12197
Analyzed By:
MAG
Result Date
Analyzed
5.20 9/23/97
'NCDEM requires that pH be analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
Reviewed By:Y-?—
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-10
Date Collected: 9/11/97
Client Project ID:
01-0997
Date Received: 9/12/97
Lab Sample ID:
29606
Analyzed By: MAG
Lab Project ID:
G216-1.
Matrix:
Water
Parameter
Result Date
Analyzed
'pH
4.75 9/23/97
'NCDEM requires that pH be analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
Reviewed By: U..-
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-11
Date Collected: 9/11/97
Client Project ID:
01-0997
Date Received: 9112/97
Lab Sample ID:
29607
Analyzed By: MAG
Lab Project ID:
G216-1
Matrix:
Water
Parameter
Result Date
Analyzed
'pH
5.80 9/23/97
'NCDEM requires that pH be analyzed within 15 minutes of sampling.,
This analysis was performed outside this specified holding time.
Reviewed By: by
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-12
Date Collected:
9/11/97
Client Project ID:
01-0997
Date Received:
9/12197
Lab Sample ID:
29608
Analyzed By:
MAG
Lab Project ID:
6216-1
Matrix:
Water
Parameter
Result
Date
Analyzed
'pH
5.50
9/23/97
'NCDEM requires that pH be analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
Reviewed By: 1sw-_
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-13
Date Collected: 9/11/97
Client Project ID:
01-0997
Date Received: 9/12197
Lab Sample ID:
29609
Analyzed By: MAG
Lab Project ID:
G216-1
Matrix:
Water
Parameter
Result Date
Analyzed
'pH
6.39 9/23/97
'NCDEM requires that pH be analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
Reviewed By: psc,,
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-14
Date Collected:
9/11/97
Client Project ID:
01-0997
Date Received:
9/12/97
Lab Sample ID:
29610
Analyzed By:
MAG
Lab Project ID:
G216-1
Matrix:
Water
" Parameter
Result
Date
Analyzed
— 'pH
5.28
9123/97
'NCDEM requires that pH be analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
Reviewed By: hn
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
RC-15
Client Project ID:
01-0997
Lab'Sample ID:
29611
Lab Project ID:
G216-1
Matrix:
Water
Parameter
'pH
Date Collected: 9/11/97
Date Received: 9112/97
Analyzed By: MAG
Result Date
Analyzed
5.47 9/23/97
'NCDEM requires that pH be analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
Reviewed By: b&,,
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
RW-1
Client Project ID:
01-0997
Lab Sample ID:
29612
Lab Project ID:
G216-1
Matrix:
Water
Parameter
'pH
Date Collected:
9/11/97
Date Received:
9112/97
Analyzed By:
MAG
Result Date
Analyzed
5.72 9/23/97
'NCDEM requires that pH be analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
Reviewed By: un
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
RW-2
Date Collected: 9111197
Client Project ID:
01-0997
Date Received: 9/12/97
Lab Sample ID:
29613
Analyzed By: MAG
Lab Project ID:
G216-1
Matrix:
Water
Parameter Result . Date
Analyzed
'pH 5.33 9123/97
'NCDEM requires that pH be analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
_J
Reviewed By: ue,
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
RW-3
Client Project ID:
01-0997
Lab Sample ID:
29614
Lab Project ID:
G216-1
Matrix:
Water
Parameter
'pH
Date Collected:
9/11/97
Date Received:
9/12197
Analyzed By:
MAG
Result Date
Analyzed
5.66 9/23/97
•NCDEM requires that pH be analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
J
I
Reviewed By:
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
Influent
Client Project ID:
01-0997
Lab Sample ID:
29615
Lab Project ID:
G216-1
Matrix:
Water
Parameter
'pH
Date Collected:
9/11/97
Date Received:
9/12/97
Analyzed By:
MAG
Result Date
Analyzed
5.54 9/23/97
'NCDEM requires that pH be analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
I
1
I
J
Reviewed By: tom_
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
Effluent
Client Project ID:
01-0997
Lab Sample ID:
29616
Lab Project ID:
G216-1
Matrix:
Water
Parameter
'pH
Date Collected:
9/11/97
Date Received:
9/12197
Analyzed By;
MAG
Result Date
Analyzed
6.26 9/23/97
'NCDEM requires that pH be analyzed within 15 minutes of sampling.
This analysis was performed outside this specified holding time.
Reviewed By: Vows
PARADIGM ANALYTICAL LABORATORIES, INC.
2627 Northchase Parkway SE, Wilmington, NC 28405
Phone: (910)-350-1903 FAX: (910)-350-1557
'-lient: loysrMC4 1ac •'p
Wdress: taM1:,
kddress:
quote #: Sec Mart Pawl
Chain -of Custody Record & Analytical Request
Project ID: O� -
P.O. Number:
Contact: ,SGS iic'
Phone: 2SG.-o�S7
Date:
Turnaround:
Job Number:
COC#
Page _�— of 2-
ReportTo:
PV 8 S ti 2
Nc
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Invoice To:
r
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Preservatives
Analyses
Comments:
a`
Please specify any special reporting
requirements
`S", Siffi Ie ID
Date
Tune
Marrir
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W-
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5-1,42
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Relinquished By
Date
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Date
Time
Temperature
Sampled By
Airbill #
(11111, 1 0',I
PARADIGM ANALYTICAL LABORATORIES, INC.
2627 Northchase Parkway SE, Wilmington, NC 28405
Phone: (910)-350-1903 FAX: (910)-350-1557
Chain -of Custody Record & Analytical Request
'-Iient: Coop Project ID: Q 911
kddress: Uv--,, P.O. Number:
liddress: yDD Contact: -)'VVJ
ItiMP it- '.It- M4.7-r ^e%xf Phone: 2576 --0352
Date: 1-// - 47 ') —
Turnaround: 5mcfs-e4
Job Number:
COC#
Page _a Of '?
Report
P0 vy -717-
Invoice To: !;4-,t,
"W. ;N"W
W 2 S;ir
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!�t'iPmKo'Mn
'Date
Time
Matra
Aimlyses
r. -
Comments:
e specify any special reporting
Pleas requirements
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Date
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Temperature
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Airbill #
ontowAl
PARADIGM ANALYTICAL LABORATORIES, INC.
2627 Northchase Parkway S.E.
Wilmington, North Carolina 28405
(910) 350-1903
Fax (910) 350-1557
Mr. John Jester
Gulfstream Environmental, Inc Date 09-08-97
PO Box 592
Wrightsville Beach, NC
Report Number: G212-2
Client Project Name : Toastmaster
Dear Mr. Jester:
Enclosed are the results of the analytical services performed under the
referenced project. Copies of this report and supporting data will be retained in
our files for a period of five years in the event they are required for future
_! reference. Any samples submitted to our laboratory will be retained for a
maximum of thirty (30) days from date of this report unless other arrangements
are requested.
If there are any questions about the report or the services performed during this
project, please call for assistance. We will be happy to answer any questions or
concerns which you may have.
Thank you for using Paradigm Analytical Labs for your analytical service
projects. We look forward to working with you again on any additional needs
which you may have.
Sincerely,
Paradigm Analytical
Laboratories
Laboratory Director
Mark Randall
North Carolina Wastewater Certification #481
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for inorganics
Client Sample ID:
Trench Date Collected: 10/6/97
Client Project ID:
Toastmaster Date Received: 10/6/97
Lab Sample ID:
30722 Analyzed By: ELP
Lab Project ID:
G216-2
Matrix:
Water
Parameter Result Date
Analyzed
'pH . 6.39 10/8/97
'NCDEM requires that pH be analyzed within 15 minutes of sampling. a
This analysis was performed outside this specified holding time.
Reviewed By: �
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatlles
by GCMS 624
Client Sample ID: Trench Date Analyzed: 1OM97
Client Project ID: Toastmaster Analyzed By: CKC
Lab Sample ID: 30722 Date Collected: 10/6197
Lab Project ID: G216-2 Date Received: 10/6/97
Matrix: Water Dilution: 1.0
Compound
Quantitatlon
Result
Limit (ug/L)
(ug/L)
Benzene
1
BQL
Bromochloromethane
1
BQL
Bromoform
1
BQL
Bromomethane
1
BQL
Carbon tetrachloride
1
BQL
Chlorobenzene
1
BQL
Chloroethane
1
BQL
2-Chloroethyl vinyl ether
5
BQL
Chloroform
1
BQL
Chloromethane
1
BQL
Dlbromochloromethane
1
BQL
1,2-Dichlorobenzene
1
BQL
1,3-Dichlorobenzene
1
BQL
1,4-Dichlorobenzene
1
BQL
1,1-Dlchloroethane
1
BQL .
1,1-Dlchloroethane
1
BQL
1,2-Dlchloroethane
1
BQL
trans-1,2-Dichloroethene
1
BQL
1,2-Dlchloropropane
1
BQL
cis-1,3-Dlchloropropene
1
BQL
trans-1,3-Dlchloropropene
1
BQL
Dlisopropyl ether (DIPE)
1
BQL
Ethylbenzene
1
BQL
Methylene chloride
5
BQL
Methyl-tert-butyl ether (MTBE)
1
BQL
1,1,2;2-Tetrachloroethane
1
BQL
Tetrachloroethene
1
BQL
Toluene
1
BQL
Trichloroethane
1
BQL
1,1,1-Trichloroethane
1
BQL
1,1,2-Trichloroethane
1
BQL
Trichloro0uoromethane
1
BQL
Vinyl chloride
1
BQL
m-,p-Xylene
2
BQL
o-Xylene
1
BQL
Surrogate Standards
Surrogate
Surrogate
Percent
Added
Result
Recovery
Compound
(ug/L)
(ug/L)
1,2-Dlchloroethane-d4
10.0
9.7
97
Toluene-d6
10.0
9.9
99
Bromofluorobenzene
10.0
110.2
102
Comments:
All results are corrected for dilution.
Flags:
BQL = Below Quantitatlon Limit
1.
Pape 1 or 1
Reviewed By:
'ARADIGII ANALYTICAL LABORATORIES, INC. COC#
?627 Nonhchase Parkway SE, Wilmington, NC 28405 Chain -of Custody Record & Analytical Request
'hone: (910)-350-1903 FAX: (910)-350-1557 Page of
'lient: nuif(_A N`
Adress: is 54Z
Adress: Wa ?—bgb0
juote #:
Project ID: It�twlQS
P.O. Number:
Contact: JM aSkV_
Phone: (0 ICI - C09 11
Date: l0 to Ct�
Turnaround:
Job Number:
Report To: � 6A
Invoice To:
Sample ID
Date
J
Time
v
Manr'r
Preservatives _ .
Analyses
Comments:
Please specify any special reporting
requirements
Wo
G-Vt ttketAA
Relinquished By
Date
Time
. . Received By ',..•
Date"
Time
Temperature
Sampled By
Airbill #
D-6-F
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