Loading...
HomeMy WebLinkAboutWQ0007798_GW Monitoring_19981013�I1VDIVISION OF WATER QUALITY - GROUNDWATER SECTION GROUNDWATER QUALITY' MONITORING: forms P.O.GNO 7626- For additional fo[ms RALEIGH, NO 27fi26.0578. COMPLIANCE REPORT FORM please write or call: (919)733-3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name Non -Discharge U 1(�i 6607299 Address tAAJT k1cl, NPDES Z u�G/ 4 LI ee. A). C. County S .6%�A/ D TYPE OF DISPOSAL OPERATION BEING MONITORED �1 (REQUIRED) Well Location LET ��/� c/s r 0�. 7 onA,• /� 7-7 I Lagoon Septic Tank/Drain Field Well Identification Number M tJ -) Well Depth O Ft. spray Field Subsurface Low -Pressure Well Diameters 0 " Sample (Screened) Interval Ft. To a'C 0 Ft. Piping (LPP) Depth to Water Level /9. y.S ft. below measuring point (before sampling) Land Application of Sludge � Measuring point is Z 157 _ ft. above land surface D Rotary Distributor 74 Other Gallons of water pumped/bailed before sampling Field Analysis: pH tp. O fn Specific Conductance uMhos Temp. C Odor Appearance Date Sample Collect d 9• 3 • 98 N Date Lab Sample Analyzed 9 • Z• �_ Laboratory Name WAZ,QAhr! M Certification No. LIS SAMPLES FOR METALS WERE COLLEC ED UNFILTERED AND FIELD ACIDIFIED LV4_YES NO COD Coliform: Coliform: MF Fecal MF Total (Note: Use MPN method for highly turbid samples) _ mg/I /100ml /100ml Dissolved Solids: Total mg/I pH (when analyzed) i . '9 units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/1 Na - Sodium mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. .iS - 9g Sign ture f Permi ee (or Aut orize gent*) Date GW-59 REV. 8/96 kn co O S=n� Ni - Nickel Pb - Lead I�Ig/I — u mg/I Zn - Zinc Pesticides/Herbicides (Specify Compounds) ", mg/I CO_ ug/I ug/I ug/I Other (Specify Compounds and Concentration units) �-. Qf Note: Values should reflec('dissolved and colloidal Ed1YG Qptrz (see #3 on back) FSee back for instructions. mit blue and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. ` 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. ` Sample preparation in the laboratory (extraction and filtration) must be completed w6in72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOTTJHOSE THAT ARE A PART PFF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director,.Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Spepifio Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. ' 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY • GROUNDWATER SECTION 29578 GROUNDWATER QUALITY' MONITORING: P.O.Box For additional forms RALEIGH, NC 27626626- -A578 COMPLIANCE REPORT FORM please write or call: (919) 733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED Facility Name l /AR,S7wJb_�STic_g IA/c Non -Discharge Iw1 O/�n779A Address % .AjT Rd NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED G County —sae : t4.�l,D (REQUIRED) Well Location Ri. Az/° Lem Lagoon Septic Tank/Drain Field Well Identification Number M W - Z Well Depth 30 . 0 Ft. Spray Field Subsurface Low -Pressure Well Diameter l�LSample (Screened)Interval Ft. To;36•O Ft. Piping(LPP) Depth to Water Level /7.3 '9 ft. below measuring point (before sampling) Land Application of Sludge Measuring point is I. goft. above land surface other Gallons of water pumped/bailed before sampling /•S Rotary Distributor Field Analysis: pH Specific Conductance — uMhos Temp. C Odor Appearance Date Sample Collected 1.7 • 4g Date Lab Sample Analyzed_/D • ,S • 99 - w o ca - Laboratory Name c E Certification No$J 2i: SAMPLES FOR METALS WERE COLLEC ED UNFILTERED AND FIELD ACIDIFIED YES NO COD Coliform: Coliform: MF Fecal MF Total (Note: Use MPN method for highly turbid samples) mg/I OOml 00ml Dissolved Solids: Total mg/I pH (when analyzed) 1.. f3 units TOC mg/1 Chloride mg/1 Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN s NM /I Nitrite (NO2) as N Nitrate (NO3) as N Phosphorus: Total Al - Aluminum_ Ba - Barium Ca - Calcium_ Cd - Cadmium_ Chromium: Total Cu - Copper Fe - Iron Hg - Mercury_ K - Potassium Mg - Magnesium Mn - Manganese Na - Sodium as P mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/1 mg/l mg/I mg/I mg/I Ni - Nickel Pb - Lead Zn - Zinc Pesticides/Herbicides (Specify Compounds) .c- : ! CO c Other (Specify Compounds and Concentration units) r%r-.,I, o - /ND�� RIQ s a g ftrnt, CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. 9� Sig at re of P rmit ee (or Authorized Agent*) Date GW-59 REV. 8196 Note: Values s colloidal ug/I ug/I ug/I ;d and #3 on back) * See back for instructions. ** Submit blue and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standatd Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. • - Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. - 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION -QR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1970, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific -Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be.calibrated fn accordance with recommendations by the manufacturer. 9. Samples must be filtered �grough w0 45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 1 O.The sample container' should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATEROUALITY- GROUNDWATERSECTION I GROUNDWATER QUALITY' MONITORING: P.O. BOX 7626- For additional forms RALEIGH, NO 2626.0578 COMPLIANCE REPORT FORM please write or call: (919)733.3221 or Facility Name Address pen ana press PERMIT NUMBER: (REQUIRED) Non -Discharge onn 7'79z NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Well Location I-A-r- Sy' Y7' ]L ` LnA)G i7- Z-1 y i• s Well Identification Number M W - 2 Well Depth 30, O Ft. Well Diameter //, Zs t l Sample (Screened) Interval Ft. To .30. 0 Ft. Depth to Water Level 4'�.7N ft. below measuring point (before sampling) Measuring point is S• Z ft. above land surface Gallons of water pumped/bailed before sampling /•S Field Analysis: pH to Specific Conductance — uMhos Temp. °C Odor Date Sample Collected • Z3 • 9$ Date Lab Sample Analyzed 110.1..99 Certification No. !Viz YES NO Laboratory Name t:2 2 rc, SAMPLES FOR METALS WERE COD _ Coliform: Coliform: MF Fecal MF Total (Note: Use MPN method for highly turbid samples) UNFILTERED AND FIELD ACIDIFIED mg/I OOml OOml Dissolved Solids: Total mg/I pH (when analyzed) units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mq/I Nitrite (NO2) as N _ Nitrate (NO3) as N_ Phosphorus: Total as P Al - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Na - Sodium I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Sig ate of P mitt a (or Authorized Agent') Date GW-59 REV. 8/96 Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge r _..�< Other LO Rotary Distributor Co Appearance N :•u mg/I Ni - Nickel Vmg/I mg/I Pb - Lead mg/I mg/I Zn - Zinc mg/I mg/I Pesticides/Herbicides mg/I (Specify Compounds) mg/I ug/I mg/I ug/I mg/I ug/I mg/I Other (Specify Compounds and mg/I Concentration units) mg/I lL us mg/I rGt(orneiGm.ne_ - 413 y�// mg/I mg/I mg/I o I I; Note: Values s colloidal solved and (see #3 on back) * See back for instructions. •' Submit blue and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. I 2. Metals Analyses: Use "Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD III Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated_ nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection.' 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental, " Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific.Conduotance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. • J, - 8. Field equipment must be calibrated ih accordance with recommendations by the manufacturer. 9. Samples must be filtered.1hro.ug.h;a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY- GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: P.O.GNC276 6- For additional forms RALEIGH, NC.27626.0578 '. COMPLIANCE REPORT FORM please write or call; (916) 733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name Non-Discharge1A)a 7 99 (REQUIRED) Address �,t4L NPDES / aun, SJ G y A)C� County �tn L 4N1� TYPE OF DISPOSAL OPERATION BEING MONITORED Well Location Lagoon Septic Tank/Drain Field Well Identification Number MIAI=`-/ Well Depth 7 /. n Ft. ,r Spray Field Subsurface Low -Pressure Well Diameter ��Sample(Screened)Interval Ft. To_0L90 Ft. Piping(LPP) Depth to Water Level eft. below measuring point (before sampling) Land Application or sludge Measuring point is ft. above land surface Rotary Distributor X Other Gallons of water pumped/bailed before sampling S Field Analysis: pH 79 Specific Conductance uMhos Temp. 7-3. y o C Odor Appearance Date Sample Collected Date Lab Sample Analyzed /D • 7. 95 ? , Laboratory Name OLLECTE17b Certification No. z/g� c SAMPLES FOR METALS WERE CUNFILTERED AND FIELD ACIDIFIED YES NO — - o COD mg/I Nitrite (NO2) as N mg/1 Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I (Note: Use MPN method for highly turbid samples) Al - Aluminum mg/I Dissolved Solids: Total mg/I Ba - Barium mg/I pH (when analyzed) t•sJ units Ca - Calcium mg/1 TOC mg/I Cd - Cadmium mg/I Chloride mg/1 Chromium: Total mg/I Arsenic mg/I Cu - Copper mg/I Grease and Oils mg/I Fe - Iron mg/I Hardness: Total mg/I Hg - Mercury mg/I Phenol mg/I K - Potassium mg/I Sulfate mg/I Mg - Magnesium mg/I Specific Conductance uMhos Mn - Manganese mg/I Total Ammonia mg/I Na - Sodium mg/I TKN as N mg/I Ni - Nickel =mg/I Pb - Lead = N mg/I Zn - Zinc mg/I Pesticides/Herbicides O7 (Specify Compounds) ug/I ug/I ug/I Other (Specify Compounds and Concentration units) 7�.ft/nrr e f%onQ 790v�/i �r;ek(aro e•FD.L2�p - ?30D tr��i Inv 1 CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values shjpMA_r.e&ct dissolved and Sig fur of Pek itt e (or Authorized Agent*) GW-59 REV. 8/96 colloidal (see #3 on back) �G ' 3 / g * See back for instructions. Date I ** Submit blue and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES'IN THE FIELD III Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, Q THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION -AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; - 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least volumes of water in the well.should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, -Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered thrgugh:a ff'.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY GROUNDWATER SECTION GROUNDWATER QUALITY' MONITORING: P.O. NG 2 626- For additional forms RALEIGH, NC 27626.0578 COMPLIANCE REPORT FORM please write or call. (919) 733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name 11P '— Non -Discharge 1nJ61^nQp '>'z9 Address„- ofT NPDES / A, ,e1A)LiU2C Al. P.. CDUnty �,r�%L/}AI a PE OF REQUIRED DISPOSAL OPERATION BEING MONITORED Well Location t-f}T' qq" VX r Di;. gib A2 *79* Z% ' go. g (REQUIRED) ) Lagoon Septic Tank/Drain Field Well Identification Number M/Aj —S Well Depth ZN. O Ft. Well Diameter /.25"' Sample (Screened) Interval Ft. To ZN D Ft. —Spray Field Subsurface Low -Pressure p ( Piping (LPP) Depth to Water Level /0 , Sfo ft. below measuring point (before sampling) Land Application of Sludge Measuring point is 3 - ZO ft. above land surface other Rotary Distributor , Gallons of water pumped/bailed before sampling S Field Analysis: pH Specific Conductance - uMhos Temp. ZC• °C Odor — Appearance — co T Date Sample Collected C/ — $ —Date Lab Sample Analyzed //� • ] 9R `o m Laboratory Name �ile 4a r� �4 IUA -)IT-t o- 4L / ,4Ro e_-4raavFs Certification No. `191 c SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED t4l_YES NO V Tri COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) -Sr 78 units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/1 Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N ma/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Signatul of Pe lee (or Authorized Agent*) Date GW-59 REV. 8/96 Ni - Nickel Pb - Lead Zn -Zinc Pesticides/Herbicides (Specify Compounds) Other (Specify Compounds and Concentration units) Note: Values mg/I mg/I ug/I ug/I ug/I and (see #3 on back) * See back for instructions. ** Submit blue and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Siandard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD m Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION _QR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. - 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director,. Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49,.No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH,.Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in•accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY- GROUNDWATER SECTION GROUNDWATER QUALITY' MONITORING:For P.O., NO 7626- COMPLIANCE 'REPORT FORM please rite additional forms RALE`GH'N027626 0578 pleasewrlteorcalL• 9i9 733-3221 or Facility pen and press PERMIT NUMBER: (REQUIRED) Non -Discharge MQ OQp 7795 NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED rRF:nl IlArnl Well Location LA-i -<LID N/ SS.y"" �jAX a' Z1 YG.7-' Lagoon Septic Tank/Drain Field Well Identification Number & W— G Sample Screened Interval Well Diameter Sam p (Screened) Well Depth 36" o Ft. Ft. To - Ft. —spray Field Subsurface Low -Pressure Piping (LPP) Depth to Water Level 1(c• /t•1 ft. below measuring point (before sampling) Land Application of Sludge Measuring point is 4y, 20 ft. above land surface Z— Rotary Distributor Other Gallons of water pumped/bailed before sampling /O. O Field Analysis: pH y.9 ( Specific Conductance — uMhos Temp. Zo. to C Odor Appearance — LO Date Sample Collec�t yd % Z ` Y4a1FO %q R�� Date Lab Sample Analyzed /v • 7' 9$ MAI_ /a9An Pao TaQi ES Certification No. //8/ co o c,n Laboratory Name IC nPAL SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel =' �'rlg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Pb - Lead = rlg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc mg/I (Note: Use MPN method for highly turbid samples) Al - Aluminum mg/I Pesticides/Herbicides o Dissolved Solids: Total mg/I Ba - Barium mg/1 (Specify Compounds) pH (when analyzed) 1/. 9 /o units Ca - Calcium mg/1 ug/1 TOC mg/I Cd - Cadmium mg/I ug/I Chloride mg/I Chromium: Total mg/I ug/I Arsenic mg/I Cu - Copper mg/l Other (Specify Compounds and Grease and Oils mg/I Fe - Iron mg/1 concentration units) Hardness: Total mg/I Hg - Mercury mg/1 s- / 2-�; �{� (ora a na - 336 09/. Phenol mg/I K - Potassium mg/1 %�,'e_h(cro r4,e .-e_e. - /s ,o ,, / j Sulfate mg/I Mg - Magnesium mg/I Specific Conductance uMhos Mn - Manganese mg/I Total Ammonia mg/I Na - Sodium mg/I�� TKN as N mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values sh uld rAMOdissolved and colloidaFAc a t�lions. (see #3 on back) tLr-� ,y/��, _ 3 o rs. �'1 `� `- � �Q / 9g See back for instructions. Si !t�e of er ittee (or Authorized Agent`) Date •* Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD W Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT -THOSE THAT RE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental. Management: (a) Standard Methods for the Examination of Waterand Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition,1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific•;Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0:45,micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY -GROUNDWATER SECTION P.O.BOX 27628 GROUNDWATER QUALITY MONITORING: For additional forms RALEIGH, NC 27626-0578 COMPLIANCE REPORT FORM please write or call: (919) 733.3221 Type or Use a ball-point pen ana press firmly. PERMIT NUMBER: (REQUIRED) Facility Namev� 4p•FS Non -Discharge— _ 1A) A Gad •77 99 Address F/arf NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED RoR1tA)1Z )eG A&r Well Location AT &y0 W rf LO/Lf6 Count .Srn2- -AA) y (REQUIRED) Lagoon Septic Tank/Drain Field , �� W0 Z7 N7• Z Well Identification Number /YI(j - 7 Well Depth 45'. b Ft. Spray Field Subsurface Low -Pressure Well Diameter •Do Sample (Screened) Interval � Ft. To 3S0 Ft. Piping (LPP) Depth to Water Level /5• ID ft. below measuring point (before sampling) Land Application of Sludge Measuring point is �/_- ZO ft. above land surface K Rotary Distributor Other is r� Gallons of water pumped/bailed before sampling � 3• �-- Field Analysis: PH ,S 37 Specific Conductance - uMhos Temp. 70 • Z-oC Odor — Appearance o � Mn Date Sample Collected Date Lab Sample Analyzed /D • 7 • Laboratory Name aa...m AA; A•G / nA.47-6RdeF5 Certification No. `t8/ ND SAMPLES FOR METALS WERE COLLECT D UNFILTERED AND FIELD ACIDIFIED �W_YES NO COD mg/I Nitrite (NO2) as N mg/I Ni - Nickeling/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Pb - Lead mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc = mg/I (Note: Use MPN method for highly turbid samples) Al -Aluminum mg/I Pesticides/Herbicides Dissolved Solids: Total mg/I Ba - Barium mg/I (Specify Compounds) pH (when analyzed) S.a H units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I mnll Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. /0 • l3 " 9� Sign ur of Perm•tte (or uthori ed Agent*) Date GW-59 REV. 8/96 ug/I ug/I ug/I Other (Specify Compounds and Concentration units) c� Ip., 2 ne - IaBD c J/ ' E Note: Values 2 f issolved and colloid-00 '� - s. (see #3 on back) Fee back for instructions. ubmit blue and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!r Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. - Sample preparation in the laboratory (extraction and filtration) must be completed within72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART 9F SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION 2 SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical. procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition,1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for,PH Sped!f C Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered throug!r=a.0.45'rnicron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY - GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: P.O. sox zs57a For additional farms RALEIGH, NC 27626-0578 COMPLIANCE REPORT FORM please write or call; (919)733-3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name S'r Non -Discharge L.cJQ Ooa 7798 AddressN NPDES I�-r/Q1A)39AG Ale, County Srn>t.an/D TYPEDISPOSAL OPERATION BEING MONITORED rr / (REQUIRED) Well Location G/FT i� e NS f Q'�!. `/ �n/t)L %0o Z % Ste. /o Lagoon Septic Tank/Drain Field Well Identification Number M W ` q Well Depth' Z-S-• O Ft. Spray Field Subsurface Low -Pressure Well Diameter �Sample (Screened) Interval Ft. To 7-S OO Ft. Piping (LPP) Depth to Water Level It—ft. below measuring point (before sampling) Land Application of Sludge - —i.p Measuring point is—ft. above land surface o Other Distributor co r Gallons of water pumped/bailed before sampling S Field Analysis: pH 5'-0 7 Specific Conductance — uMhos Temp.1$_i °C Odor — Appearance — Date Sample Collect e Z3 • 9 Date Lab Sample Analyzed /0 • 7 • i 1? Laboratory Name A r n 14WAIL1-r.r.m!- Z,&L?7A.4 7d _:5 Certification No. ye6 N "' SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED AVq—YES NO COD mg/I Nitrite (NO2) as N mg/I — Ni - Nickel s- t mg/I Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb - Lead `a mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc mg/I (Note: Use MPN method for highly turbid samples) Al - Aluminum mg/I Pesticides/Herbicides Dissolved Solids: Total mg/I Ba - Barium mg/I (Specify Compounds) pH (when analyzed) S . z 3 units Ca - Calcium mg/I ug/I TOC mg/I Cd - Cadmium mg/I ug/I Chloride mg/I Chromium: Total mg/I ug/I Arsenic mg/I Cu - Copper mg/I Other (Specify Compounds and Grease and Oils mg/I Fe - Iron mg/I Concentration units) Hardness: Total mg/I Hg - Mercury mg/1 C.j]5- 4 Z - 71tome-t4v y2e - 4/ A Phenol mg/I K - Potassium mg/I Sulfate mg/I Mg - Magnesium mg/I T, Specific Conductance uMhos Mn - Manganese mg/I P a r." ME ` Total Ammonia mg/I Na - Sodium mg/I TKN as N mg/I — W, I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values shotlicl"01Wi�[Welved and 0, d colloidal corfa9W QFcFd&1 see #3 on back) /ram � /' 9g See back for instructions. Sign .tut a of Pe(mitt e (o/ r Authorized Agent") Da a� F Submit blue and yellow copies only to address above. GW-59 FfEV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD Ilt Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 Hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION .QR SAMPLING CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: ` (a) Standard Methods for the Examination of Water, and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing, any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific`Coriddctance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. �- 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered,throuyh a.0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container shddid be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY- GROUNDWATER SECTION: ' P.O. BOX 29578 GROUNDWATER QUALITY MONITORING: 6- For additional forms RALEIGH, NC.27626-.U578 COMPLIANCE REPORT FORM. please write or call: (919) 733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name <Q 17-M#STe.2 /J,/C Non -Discharge r-J+&-Ono 774g /71r'/- �• NPDES Address TYPE OF DISPOSAL OPERATION BEING MONITORED /.�ur:e aura N.G. County—Sf�T�-� /a (REQUIRED) Well Location Lagoon Septic Tank/Drain Field Well Identification Number M W - /O Well Depth ZS. 6 Ft. Well Diameter Lt. oc"Sam le Screened Interval Ft. Tob52Ft. Spray Field SubsurfaceLow-Pressure p (Screened) Piping (LPP) Depth to Water Level _//. 1.2 ft. below measuring point (before sampling) Land Application of Sludge Measuring point is a. ZS it. above land surface _ Other !3 S t \ Rotary Distributor Gallons of water pumped/bailed before sampling drJTJ1 _ Field Analysis: pH S• $S Specific Conductance - uMhos Temp. 8-7 oC Odor Appearance Date Sample Collected 9 • Z R • �g Date Lab Sample Analyzed /n • 7. 98 Laboratory Name 2426b eC.M �}/Uw77eAt Z_4,Q6,eq-m e.f c5 Certification No. 4/5r/ SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) 5'• oZ units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N Nitrate (NO3) as N_ Phosphorus: Total as AI - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Na - Sodium 0 < V r. r-, mg/I Ni - Nickel mg/I mg/I Pb - Lead mg/I Zn - Zinc mg/I mg/I Pesticides/Herbicides mg/I (Specify Compounds) mg/I ug/I mg/I ug/I mg/I ug/I mg/I Other (Specify Compounds and mg/I Concentration units) ' $ mg/I • - - - v5 / mg/I % '?- pme44-nm. -IW ug/b mg/I if mg/I mg/I 7- J1 % 1 CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal eFAY&t d$6hstE{see #3 on back) I ,. See back for instructions. Signature of Pe mitt e or Authorized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. ` Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental , Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes. of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY • GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: P.O. eox For additional forms RALEIGH, NO 276267626- �0678 COMPLIANCE REPORT FORM please write or call: (919)733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name 0�%M •rF� /�/� Non -Discharge Ma 41667229 Address P%,r'f- �U NPDES /A+JQrAI ,rr2G /t/� County SceTGSFu D TYPE OF DISPOSAL OPERATION BEING MONITORED Well Locations 3'f ° YS' 00• L' �Nb 72' 7- 7' Y.Y. Z (REQUIRED) Lagoon Septic Tank Drain Field Well Identification Number A114 - // Well Depth ZS. D Ft. Well Diameter •oo '� Sample (Screened) Interval Ft. TO Ft. Depth to Water Level / 7,116 K ft. below measuring point (before sampling) Measuring point is : f S ft. above land surface Gallons of water pumped/bailed before sampling 3 7 . O Field Analysis: pH .t. Z6 Specific Conductance — uMhos Temp.C Odor Date Sample Collected 9 • Z3. 91 Date Lab Sample Analyzed /D • 7. 99 Laboratory Name F" 4.01,,m Z4rVA4kr1e1 V' LARA Pw rn2iE5 Certification No. SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIEDg#D,,—YES Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge _ - Other Rotary Distributor VD Appearance — NO COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel �mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Pb - Lead mg/l Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc _mg/I (Note: Use MPN method for highly turbid samples) Al - Aluminum mg/I Pesticides/Herbicides Dissolved Solids: Total mg/I Ba - Barium mg/I (Specify Compounds) pH (when analyzed) S. S 1 units Ca - Calcium mg/I ug/I TOC mg/I Cd - Cadmium mg/I ug/I Chloride mg/I Chromium: Total mg/I ug/I Arsenic mg/I Cu - Copper mg/I Other (Specify Compounds and Grease and Oils mg/I Fe - Iron mg/I Concentration units) Hardness: Total mg/I Hg - Mercury mg/I C 'S - 1, z - ; nhl rn e inP Phenol mg/I K - Potassium mg/I Sulfate mg/I Mg - Magnesium mg/I Specific Conductance uMhos Mn - Manganese mg/I Total Ammonia mg/I Na - Sodium mg/I r-j lff7Qz: jj� = TKN as N mg/I "- I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Si na re ofVerittee(or Au orized Agent*) Date GW- REV.8/ Note: Values should reflect dissolved and colloidal QOpRVWTaWW IIsee #3 on back) See back for instructions. •` Submit blue and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OFF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 161h Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through,a, 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY`- GROUNDWATER SECTION GROUNDWATER QUALITY' MONITORING: PO 29578- For additional Corms RALEIGH, NO :27626;0575 COMPLIANCE REPORT FORM please write or call: (919) 733.3221 Type or Use a ball-point pen and press Facility Name Address County Gf a TL AAJ/-.) Well PERMIT NUMBER: (REQUIRED) Non -Discharge & 0d0 7 719 NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Well Identification Number lou) - /Z Well Depth?S. 0 Ft. Well Diameter " Sample (Screened) Interval Ft. To %S.O Ft. spray Field Septic Tank/Drain Field Subsurface Low -Pressure Piping (LPP) Depth to Water Level /l. fo3 ft. below measuring point (before sampling) Land Application of Sludge Measuring point is Z . S ft. above land surface other Gallons of water pumped/bailed before sampling g !� Rotary Distributor Field Analysis: pH .5--. / 0 Specific Conductance — uMhos Temp.`/ C Odor � Appearance Date Sample Collected 9. 2 3 • Date Lab Sample Analyzed-16 • 7 • 98 Laboratory Name LsFGro.2 Rrr=s Certification No. h 9/ SAMPLES FOR METALS WERE COLLECTED'UNFILTERED AND FIELD ACIDIFIED 4 YES NO COD Coliform: Coliform: MF Fecal MF Total mg/I 00ml OOml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) o .. )'� units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N Nitrate (NO3) as N_ Phosphorus: Total as P Al - Aluminum Ba - Barium. - Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Na - Sodium CJ �0 0 O o mg/I Ni - Nickel T ;= mg/I mg/I Pb - Lead mg/1 mg/I Zn - Zinc — r'lmg/I mg/I Pesticides/Herbicides t-O mg/I (Specify Compounds) o mg/I ug/I mg/I ug/I mg/I ug/I mg/I Other (Specify Compounds and mg/I Concentration units) mg/I T_, rh in, 6 eWik" e? mg/I mg/I mg/I mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and . .R #3 on back) 45_ � �/ lb • 1-3 9 * See back for instructions. S na re of er ittee (or Authorized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1: Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED As WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT.THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION DR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title'15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must fie calibrated in accordance with recommendations by the manufacturer. 9. Samples must be f!Itered.through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY - GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: P.O. sox For additional forms RALEIGH, NO 27626- 7626.0578 COMPLIANCE 'REPORT FORM please write or call: (919) 733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name I c Non -Discharge bL Gnp�?'726 Address Pn.,a AodNPDES / �rrst3! 1t.�lU �. CountOy y c.eT�.onje TYPE OF DISPOSAL OPERATION BEING MONITORED 9(REQUIRED) Well Location Ll1T RV0 %g n OY. 9 rr 40ALI[. 70 27 r -/9• 3 rr Lagoon Septic Tank/Drain Field Well Identification Number Al AJ - 13 Well Depth •!0. O Ft. Well Diameter -06" Sample (Screened) Interval Ft. ToSQ-0 Ft. Depth to Water Level Z_Z _L6 ft. below measuring point (before sampling) Measuring point is 3 Z ft. above land surface Gallons of water pumped/bailed before sampling /D. �t= Field Analysis: pH C. Hho O Specific Conductance uMs Temp./$-5C Odor Date Sample Collected 9 - 2 2 - 95? Date Lab Sample Analyzed AQ- 3 - 99 Laboratory Name Z:cCertification No. SAMPLES FOR METALS WERE COLLECT UNFILTERED AND FIELD ACIDIFIED zZZ YES COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) .S.NIo units TOC mg/I Chloride mg/1 Arsenic mg/1 Grease and Oils mg/1 Hardness: Total mg/l Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/1 TKN as N mg/I Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge _ c Other c Rotary Distributor Appearance — n NO v Nitrite (NO2) as N mg/I Ni - Nickel = R mg/I Nitrate (NO3) as N mg/I Pb - Lead rn mg/I Phosphorus: Total as P mg/I Zn - Zinc o " mg/I Al - Aluminum mg/I Pesticides/Herbicides Ba - Barium mg/I (Specify Compounds) Ca - Calcium mg/I ug/I Cd - Cadmium mg/I ug/I Chromium: Total mg/I ug/I Cu - Copper mg/I Other (Specify Compounds and Fe - Iron mg/I Concentration units)// Hg - Mercury mg/I els K - Potassium mg/I Tr-, cA(a1-o e4Ae_*Le Mg - Magnesium mg/I Mn - Manganese mg/I Na -Sodium mg/I - � KiaR� A S rF 4 I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. lb - L :R - 15! 6 igna ure of erm'ttee (or Authorized Agent*) Date GW-59 REV. 8/96 Note: Values shodRefUtV&olved and colloidal copgq(ZtI I F_M4see #3 on back) ni_u. ur-i" Rai_ * See back for instructions. ** Submit blue and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES'IN THE FIELD !11 Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within.72`hours of'collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE, GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION t R SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director,.Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be lahel2d'at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. IGROUNDWATER QUALITY MONITORING: For additional forms COMPLIANCE REPORT FORM please write or pap, Type or Use a ball-point pen and press firmly. Facility Name .�6 7-M4-,TTrW_, //VC. Address/r+ ✓t •F 2�) . DIVISION OF WATER QUALITY• GROUNDWATER SECTION.> P.O.. BOX.29578 RALEIGH, NC 27626.0578 (919) 7333221. PERMIT NUMBER: (REQUIRED) Non -Discharge tJd eOo 7749 NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Well Location /_A-T &Y° '78 O%. ,S - /_ON.- /7- [ / -17.(= Lagoon Septic Tank/Drain Field Well Identification Number /YAW - /'-/ Well Depth. 30.60 Ft. Well Diameter !V.0 " Sample (Screened) Interval Ft. To Jin .eo Ft. Depth to Water Level 13 - G57 ft. below measuring point (before sampling) Measuring point is i4. 7_0 ft. above land surface Gallons of water pumped/bailed before sampling 33 Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge Other Rotary Distributor Field Analysis: pH �i.7 i Specific Conductance — uMhos Temp. /RTi oC Odor Appearance Date Sample Collected ?A Date Lab Sample Analyzed /0 7 9il Laboratory Name A•-2i-yrc " AIVALV7 ceAC Laao/l aTr /y c 5 Certification No. Z-/ SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED COD mg/1 Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) S. wo units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Prel Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. - /S . (3• 911K Si re of r ittee (or Authorized Agent*) Date GW-59 REV. 8/96 Ni - Nickel t mg/I Pb - Lead = «}Ig/1 Zn - Zinc 's -img/I Pesticides/Herbicides (Specify Compounds) ug/I ug/I ug/I Other (Specify Compounds and Concentration units) / Z - .r li Gi/) era P'ti1Ch� ' trc/I Note: Values shd(00 rofje"ossolved and colloidal concentrations. (see #3 on back) v_ if, * See back for insPnFMQ0a' _;L"° _ ** Submit blue and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN -THE FIELD err Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection: 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION _R SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209,, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 1 O.The sample container should be labeled at the time of collection with, the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY - GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: P.O. BOX 29578 For additional forms RALEIGH, INC 27626-0578 COMPLIANCE REPORT FORM please write or call: (919) 733.3221 J Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name D /V Non -Discharge WQndo77c%R Address W �v + )ZP NPDES Lrrl2! U�j C� Sc TYPE OF DISPOSAL OPERATION BEING MONITORED Ni3 G ^! County oTtAa (REQUIRED) Well Location Lagoon Septic Tank/Drain Field Well Identification Number gLL3 — I Well Depth ,!d.06 Ft. Well Diameter Sample (Screened) Interval Ft. To 5a dyFt. spray Field Subsurface Low -Pressure Piping (LPP) Depth to Water Level 26', 64.ft. below measuring point (before sampling) Land Application of Sludge Measuring point is1,0 ft. above land surface )C other Gallons of water pumped/bailed before sampling Rotary Distributor Field Analysis: pH O Specific Conductance _ uMhos Temp. 11 4 oC Odor Appearance Date Sample Collected 9 Z A • I Date Lab Sample Analyzed c0 - 7 - W Laboratory Name FA" D l�, A n, A l �.TlP #6 L nn1z,& S Certification No. `j R J `CD SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED A.0 YES NO COD mg/I Coliform: MF Fecal /loom) Coliform: MFTotal /loom[ (Note: Use MPN method for highly turbid Samples) Dissolved Solids: Total mg/I pH (when analyzed) 47, yit, units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NOp) as N mg/I Ni -Nickel (1 Nitrate (NO3) as N mg/I Pb - Lead ^mg/I Phosphorus: Total as P mg/I Zn - Zinc C� mg/I AI -Aluminum mg/I Pesticides/Herbicides o Ba - Barium mg/I (Specify Compounds) Ca - Calcium mg/I ug/I Cd - Cadmium mg/I ug/I Chromium: Total mg/I ug/I Cu - Copper mg/I Other (Specify Compounds and Fe - Iron mg/I Concentration units) Hg - Mercury mg/I —880 vaI t K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na -Sodium mg/I 'P a I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. O rl Signat reo.f Permit (or Authorized Agent*) Date GW-59 R 8/96 Note: Values should reflbct'dYssolved and colloidal cprjperAr8k�ft!Ls.(see #3 on back) • See back for instructions. ** Submit blue and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. - . . Sample preparation in the laboratory (extraction and filtration) must be completed within 72,hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE 9 PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the method§ described in one of the following publications, or by other methods approved beforehand by the Director, Division c.tEnvironmental Management: " (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample containef'should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. IGROUNDWATER QUALITY MONITORING: For additional forms COMPLIANCE REPORT FORM please write or call: Type or Use a ball-point pen and press firmly. Facility Name 1 nftt i Nt14STr-2_ //U O Address pT1"T (A-ug�iAr13u/LG A1L county SccTe_4AJb Well Location Well Identification Number gj'W — Z Well Depth a- 60 Ft. Well Diameter i140 Sample (Screened) Interval Ft. To_SZ_&�t. Depth to Water Level _IS . Zq ft. below measuring point (before sampling) Measuring point is 2, 10 ft. above land surface Gallons of water pumped/bailed before sampling Field Analysis: pH 5. 10 Specific Conductance — uMhos Temp. L9 `� C Date Sample Collected 9 • 7_ 3 ' 9A Date Lab Sample ADalyzed /h • 7 • 2 Laboratory Name <&A Arne SAMPLES FOR METALS WERE AND FIELD ACIDIFIED DIVISION OF WATER QUALITY - GROUNDWATER SECTION P.O. BOX 29578 RALEIGH, NC 27626.0578 (919) 733-3221 PERMIT NUMBER: (REQUIRED Non -Discharge W 666 '> 7 4f NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge )C Other Rotary Distributor Odor x Appearances— co O di Certification No. !�4 ;71 YES NO — COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel i^ rri;, ^ r•mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Pb - Lead _ �= -mg/I Coliform: MF Total /100mI Phosphorus: Total as P mg/I Zn - Zinc "' mg/I (Note: Use MPN method for highly turbid samples) Al - Aluminum mg/I Pesticides/Herbicides -- Dissolved Solids: Total mg/I Ba - Barium mg/I (Specify Compounds) pH (when analyzed) Z�I units Ca - Calcium mg/I ug/I TOC mg/I Cd - Cadmium mg/I ug/1 Chloride mg/I Chromium: Total mg/I ug/I Arsenic mg/I Cu - Copper mg/I Other (Specify Compounds and Grease and Oils mg/I Fe - Iron mg/I con ntrafi units) Hardness: Total mg/I Hg -Mercury mg/I c klom >z+EtevtlL — /loy Phenol mg/I K - Potassium mg/I Sulfate mg/I Mg - Magnesium mg/I Specific Conductance uMhos Mn - Manganese mg/I Total Ammonia mg/I Na - Sodium mg/I TKN as N mg/I Ki I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal coifie n'fiatlohtsCAPQ OFFICE (see #3 on back) See back for instructions. Signat re f Permitt e ( r Authorized Agent") Date •• Submit blue and yellow copies only to address above. GW-59 RE . 8196 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD tII Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. r 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION QR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical, procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition,1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be cali6ratdd'in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0,45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should. 30%labeledat the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY • GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: IG NG2626- For additional forms RALEIGH, NC 27628�0578 COMPLIANCE REPORT FORM please write or call: (919) 733.3221 or Use a Facility Name Well Location K W — pen and press County Sri dan Well Identificati n Number 4!,A) _3 Well Depth NA.O0 Ft. Well Diameter . u Sample (Screened) Interval Ft. ToL16 -00Ft. Depth to Water Level ZZ 5 9ft. below measuring point (before sampling) Measuring point ism 60 ft. above land surface Gallons of water pumped/bailed before sampling L— Field Analysis: pH _Specific Conductance — uMhos Temp.ZO. 7, oC Odor Date Sample Collecte Z Date Lab Sample Analyzed 99 Laboratory Name filar i '4211 �r—t�A-li Certification No. yg� SAMPLES FOR METALS WERE COLLECTED UNFILTERED AJ�YES NO PERMIT NUMBER: (REQUIRE 7 7 }$ Non -Discharge NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field AND FIELD ACIDIFIED Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge Other Rotary Distributor Appearance cr t-0 COD mg/I Nitrite (NOp) as N mgll Ni -Nickel "' = =,Jngll Coliform: MF Fecal /100m1 Nitrate (NO3) as N mg/I Pb -Lead — ri-7ng/I Coliform: MF Total /100m1 Phosphorus: Total as P mg/I Zn -Zinc = ='�mg/I (Note: Use MPN method for highly turbid samples) Al -Aluminum mg/I Pesticides/Herbicides Dissolved Solids: Total mg/I Ba -Barium mg/I (Specify Compounds) o � pH (when analyzed) _t�. S3 units Ca - Calcium mg/I - ug/1 TOC mg/I Cd -Cadmium mg/I ug/I Chloride mg/I Chromium: Total mg/I ug/I Arsenic mg/I Cu -Copper mg/I Other (Specify Compounds and Grease and Oils mg/I Fe -Iran mg/I co9�ntratioP units) Hardness: Total mg/I Hg -Mercury mg/I 1 n2.ti lcrb ern inn Phenol mg/I K -Potassium mg/I Sulfate mg/I Mg -Magnesium mg/I Specific Conductance uMhos Mn -Manganese mg/I Total Ammonia mg/I Na -Sodium mg/I TKN as N mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values shlovvuld relldiftissolved and cQlloidal;�'p�cegltC�tlons. (see #3 on back) I f PI_R /D • /3 • 8 9 See back for instructions. Sig at re of Per it ee (or Authorized Agent') Date •* Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD III Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental,_ Management: ' (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; - 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY - GROUNDWATER SECTION' GROUNDWATER QUALITY MONITORING: P.O.GNO 7626- :For additional forms RALEIGH, NO 27626.0575 , COMPLIANCE REPORT FORM please write or call: (919)733.3221 or Facility Well pen and press PERMIT NUMBER: (REQUIRED) Non -Discharge j_)Q Gbo 2-7TS NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) _ Lagoon Septic Tank/Drain Field Well Identification Number 1A)rLu—c'l 7— Well Depth Ft. Well Diameter —Sample Screened Interval Ft. To Ft. Spray Field Subsurface Low -Pressure (Screened) Piping (LPP) Depth to Water Level ft. below measuring point (before sampling) Land Application of Sludge Measuringpoint is ft. above land surface _7 Other of Rotary Distributor co Gallons of water pumped/bailed before sampling Field Analysis: pH y Specific Conductance — uMhos Temp./9-0 C Odor — Appearance Date Sample Collect Date Lab Sample Analyzed 612 • *7 93 _ Laboratory Name, A70 rGM as!rr,nAt /-A3oeRira,eLFs Certification No. yev SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED AVA YES NO COD _ Coliform: Coliform: MF Fecal MF Total (Note: Use MPN method for highly turbid samples) _ mg/I /100ml /100ml Dissolved Solids: Total mg/I pH (when analyzed) f. z 8 units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N _ Nitrate (NO3) as N_ Phosphorus: Total as Al - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Na - Sodium 0 I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. 0- 13 9� na ure of Pe m ttee (of=uthorize_cT_Agent*) Date GW-59 REV. 8/96 mg/I Ni - Nickel .. n cn = mg/I mg/I Pb - Lead " =' mg/I mg/I Zn - Zinc mg/I mg/I Pesticides/Herbicides mg/I (Specify Compounds) mg/I ug/I mg/I ug/I mg/I ug/I mg/I Other (Specify Compounds and mg/I Concentration units) mg/I '%r; rh torne_4-" - / /Onya,/ mg/I mg/I mg/I mg/I Note: Values should reflect dissolved and colloidal condeh r-s I OVii(ke #3 on back) nos= u= * See back for instructions. ** Submit blue and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 1. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD Ilt Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated'in accordance with recommendations by the manufacturer. 9. Samples must be filtered through'a`D:45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should,be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY'= GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: P.O. BOX 29578 For. additional forms RALEIGH,.NO 27626.0578 COMPLIANCE REPORT FORM please wrlteorcall; (919)733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name /Ylf}STc� ��t1� Non -Discharge uJ/� nl5c) :> 7 Address a/ -A'- kd- NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED k'�(Zf aQs.QG nrC� COUnty���T/-h'A�� (REQUIRED) Well Location Lagoon Septic Tank/Drain Field Well Identification Number 12Enlc-N &;tLuenJi Well Depth Ft. Spray Field Subsurface Low -Pressure (Screened) Well Diameter —Sample Screened Interval Ft. To Ft. Piping (LPP) Depth to Water Level ft. below measuring point (before sampling) Land Application of sludge Measuring point is—ft. above land surface _-e Other Rotary Distributor Gallons of water pumped/bailed before sampling Field Analysis: pH Specific Conductance uMhos Temp. /9. Z/ DC Odor — Appearance _ co 7 y • 98 Date Sample Collect Date Lab Sample Analyzed /O • 7. 98 T 0 Laboratory Name rr/Zybvt AnrAa�,nu90 //dam/L47a2 ors Certification No. e/A/ SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO GJ ra , COD mg/I Nitrite (NO2) as N �= me mg/I Ni - Nickel =_ '- mg/I Coliform: MF Fecal /100m1 Nitrate (NO3) as N rr mg/I Pb -Lead mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc = mg/I (Note: Use MPN method for highly turbid samples) AI - Aluminum mg/I Pesticides/Herbicides =- Dissolved Solids: Total mg/I Ba - Barium mg/I (Specify Compounds) pH (when analyzed) 6, • R R units Ca - Calcium mg/I ug/I TOC mg/I Cd - Cadmium mg/I ug/I Chloride mg/I Chromium: Total mg/I Ug/I Arsenic mg/I Cu - Copper mg/I Other (Specify Compounds and Grease and Oils mg/I Fe - Iron mg/I Concentration units) Hardness: Total mg/I Hg - Mercury mg/I Phenol mg/I K - Potassium mg/I Sulfate mg/I Mg - Magnesium mg/I Specific Conductance uMhos Mn - Manganese mg/I Total Ammonia mg/I Na -Sodium mg/I TKN as N mg/I s I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values fh'W, I1c dissolved and colloidaR l0s. (see #3 on back) i /D - /3 See back for instructions. Slgnatuof P mitt e r Authorized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59-REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1: Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. . 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION "_R SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the, Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition,1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; ` (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No.209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volum "are°removed; samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45, micron -filler immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection_with the.facility-name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. I DIVISION OF WATER QUALITY • GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: P.O. Box 29578 For additional forms RALEIGH, NO 27626.0578 COMPLIANCE REPORT FORM please write or call: (919)733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name nAa_Si Qe Non -Discharge V 16 6_08 : C�k Address'P\4,.' V NPDES County Sr_ ni tr<.n. & TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Well Location Lagoon Septic Tank/Drain Field Well Identification Number r--t F 10n-..,,TT Well Depth Ft. Well Diameter -Sample Screened Interval Ft. To Ft. Spray Field Subsurface Low -Pressure (Screened) Piping (LPP) Depth to Water Level ft. below measuring point (before sampling) Land Application of Sludge Measuring point is ft. above land surface Other Gallons of water pumped/bailed before sampling Rotary Distributor Field Analysis: pH E,`'15? Specific Conductance uMhosTemp?\,O °C Odor Appearance Date Sample Collected 'n ,20 cI 9 Date Lab Sample Analyzed 6 1119 Laboratory Name �nen c� inn. A..,'�-1 , �, r,n l L"en. �a2 cS _ Certification No. �� I SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED ti11)r_YES NO COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel o - mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Pb - Lead co n—,mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc C= 89;mg/I (Note: Use MPN method for highly turbid samples) AI - Aluminum mg/I Pesticides/Herbicides o< Dissolved Solids: Total mg/I Ba - Barium mg/I (Specify Compounds) cn no pH (when analyzed) 5, 119 units Ca - Calcium mg/I oug/I ug/I TOC mg/I Cd - Cadmium mg/I �' Chloride mg/I Chromium: Total mg/I — 2-1 g/I Arsenic mg/I Cu - Copper mg/I Other (Specify Compounds and Grease and Oils mg/1 Fe - Iron mg/I Concentration units) z Hardness: Total mg/I Hg - Mercury mg/I iz: c l \cDzc�p. 4.� �, - — 'tcC L7 0311­ Phenol mg/I K - Potassium mg/I Sulfate mg/I Mg - Magnesium mg/I Specific Conductance uMhos Mn - Manganese mg/I Total Ammonia mg/I Na - Sodium mg/I TKN as N mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) Y' tty See back for instructions. Signat a Of rm t e (or uthorized Agent`) tom,_ Date _.,�'' " Submit blue and yellow copies only to address above. GW-59 REV. 8/96 w COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART QF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure -and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY - GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: 1 P.O. BOX 29578 For additional forms RALEIGH, NC 27626.0578 COMPLIANCE REPORT FORM please write or call: (919)733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name�flRSTM ns i e0 k ntC Non -Discharge c'`c9c3't'i CA 4 Address ti • NPDES Lk r ns \nt�P wC County cn'�\IN TYPE OF DISPOSAL OPERATION BEING MONITORED Well Location %Q r t lr\.. — S tl�1 octi 1 (REQUIRED) Lagoon Septic Tank/Drain Field Well Identification Number Well Depth Ft. Well Diameter —Sample Screened Interval Ft. To Ft. (Screened) spray Field Subsurface Low -Pressure Piping (LPP) Depth to Water Level ft. below measuring point (before sampling) Land Application of Sludge / Measuring point is—ft. above land surface — other Gallons of water pumped/bailed before sampling Rotary Distributor Field Analysis: pH — Specific Conductance uMhos Temp. — oC Odor — Appearance Date Sample Collected `�_ `a9 `5 y Date Lab Sample Analyzed r 1 9 '1 Laboratory Name A�.t?\�`r'.ckl I- .A\,c,-TIP,%`L:rt Certification No. u SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED LL YES NO COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I Ni - Nickel Pb - Lead mg/I mg/I Zn - Zinc Pesticides/Herbicides (Specify Compounds) —a rqC3 N sug/I C-) ug/1 ug/I Other (Specify Compounds and Concentration units) ` I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and _ I colloidal concentrations. (see #3 on back) L�t c©t �� See back for instructions. Sign ure o Per Ittee Authorized Agent') Date *` Submit blue and yellow copies only to address above. GW-59 REV. 8/96 1�` COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. GROUNDWATER QUALITY MONITORING: For additional forms COMPLIANCE REPORT FORM please write or call: or Facility Name pen and press Well Location _LJ4T 34 ° 449 ' 67r3'r L b C, '79` Well Identification Number 0" LJ -%XA Well Depth 30,6i Well Diameter Lk. O" Sample (Screened) Interval Ft. To3oC Depth to Water Level 10. %0 ft. below measuring point (before sampling) Measuring point is 3N rAC> ft. above land surface Gallons of water pumped/bailed before sampling 4C). n Field Analysis: pH ti. S 61 Specific Conductance — uMhos Temp. Date Sample Collec ed �� 'AO,�! Date Lab Sample Analyzed_ DIVISION OF WATER QUALITY -,GROUNDWATER SECTION P.O. BOX 29578. RALEIGH, NC 27626.0578 (919)733-3221. PERMIT NUMBER: (REQUIRED) WWQ ���,� Non -Discharge NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Slue Other Rotary Distributor °C Odor — Appearance Laboratory Name �f <ILRC� ��r.1 Avr \ ��� r. Al 9 Asa rL�i � -, P r _ Certification No. LA 82 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED ,NLA-`YES NO COD _ Coliform Coliform MF Fecal MF Total (Note: Use MPN method for highly turbid samples) mg/I OOml OOml Dissolved Solids: Total mg/I pH (when analyzed)h , S t units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N Nitrate (NO3) as N Phosphorus: Total AI - Aluminum Ba - Barium Ca - Calcium_ Cd - Cadmium_ Chromium: Total Cu - Copper Fe - Iron Hg - Mercury_ K - Potassium Mg - Magnesium Mn - Manganese _ Na - Sodium as P. mg/I Ni - Nickel mg/I mg/I Pb - Lead mg/I mg/I Zn - Zinc mg/I mg/I Pesticides/Herbicides °D C'= mg/I (Specify Compounds) C �n mg/I ?r= ug/I mg/I %n -ug/I mg/I -*+ r:'ioug/I mg/I Other (Specify Compounds and mg/I Concentration units) mg/I",,�`�a``dto�.``4i cG,(�d��� mg/I J�ir.fi ,-�GN VnGJQ. Ct — t� ��L mg/I l e L mg/I mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and � 9 colloidal concentrations. (see #3 on back) L `0 See back for instructions. Signa ure o er ttee Authorized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 r COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, Q THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; r 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At leastavolumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. S. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY - GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: P.O. BOX 29578 For additional forms RALEIGH, NO 27626.0578 COMPLIANCE REPORT FORM please Write or oath (919) 733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name I Oti<TO-^ �z�9— r 1:'.'C_ Non -Discharge i�.S c` L '2�06-7 -?CA Address •Q(R^�t `Q�-�- NPDES ( 11JP. J .Nl1�}4 �.1C - County _<C ) I1' ., f TYPE OF DISPOSAL OPERATION BEING MONITORED Well Location / f1 T .3 4° \� r c? < 1.3 ` Lt 7nl �iq ° `vlo -1 f L-(�(, Z �' (REQUIRED) Lagoon Septic Tank/Drain Field Well Identification Number M\.s —lZ Well Depth '76.0 Ft. Well Diameter "1 Oc�' Sample Screened Interval Ft. To D O Ft. Spray Field Subsurface Low -Pressure p (Screened) :�+-�— Piping (LPP) Depth to Water Level ft. below measuring point (before sampling) Land Application of Sle Measuring point is 's, 1 ft. above land surface Other Gallons of water pumped/bailed before sampling h L�d�rtdl Rotary Distributor Field Analysis: pH 5. 6LA Specific Conductance uMhos Temp. 2a DC Odor Appearance Date Sample Collected aJ.q�' Date Lab Sample Analyzed Laboratory Name PPr2rL� �r_ ns }\ �:cA \ � ��r»pr�t�t i r 5 Certification No. LA 2 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED A/t /} YES NO COD _ Coliform Coliform MF Fecal MF Total (Note: Use MPN method for highly turbid samples) mg/I /1 ooml /1 ooml Dissolved Solids: Total mg/I pH (when analyzed) units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N Nitrate (NO3) as N_ Phosphorus: Total as AI - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Na - Sodium 0 mg/I Ni - Nickel g/I mg/I Pb - Lead-uig/I mg/I Zn - Zinc Cn :;7_ mg/I Pesticides/Herbicides ,ig/I -0 z m mg/I (Specify Compounds) cn 2 mg/I ug/I mg/I t �l Ig/I mg/I 'Dg/I mg/I Other (Specify Compounds and mg/I Concentration units) mg/I C:s- t,a-- eT-'eiat mg/I TtT , c.V1 r,%e, e1-1• r_ — 'All y c I. L mg/I mg/I mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) \ t� See back for instructions. Signature o er • tee ( r Authorized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE 94. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART QF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number t EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. S. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to'sign official documents. DIVISION OF WATER QUALITY - GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: P.O. BOX 29578 For additional forms RALEIGH, NC 27626-0578 COMPLIANCE REPORT FORM please write or call: (919) 733-3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name 1 HRG7nMl`G�l l TT"[e Non -Discharge- __ l/'Ja 000 iiG� Address NPDES ( r),l9;�1\nJ2a. nsf_ County Sr'n-�-\na` TYPE OF DISPOSAL OPERATION BEING MONITORED - (REQUIRED) Well Location Lagoon Septic Tank/Drain Field Well Identification Number Mkt - trl- Well Depth Ft. Well Diameter's r`_ Sample Screened Interval Ft. To �S�� Ft. spray Field PipingSubsulace Low -Pressure P (Screened) Piping (LPP) Depth to Water Level 10, Oq ft. below measuring point (before sampling) Land Application of Sludge Measuring point is '1,9 ft. above land surface other Gallons of water pumped/bailed before sampling Z�g Rotary Distributor Field Analysis: pH _Specific Conductance r uMhos Temp. C Odor — Appearance Date Sample Collected a Date Lab Sample Analyzed F •2 'et8 Laboratory Name Prst rA et Z. . R U �l-k:c.w1 Certification No. y gt SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED niI�YES NO COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/1 Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Pb - LeadCo �n mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc mg/I (Note: Use MPN method for highly turbid samples) Al - Aluminum mg/I Pesticides/Herbicides cm Dissolved Solids: Total mg/I Ba - Barium mg/I (Specify Compounds) _ o< pH (when analyzed) A7. I units Ca - Calcium mg/I ug/I TOC mg/I Cd - Cadmium mg/I -'� ug/I Chloride mg/I Chromium: Total mg/I > ug/I Arsenic mg/I Cu - Copper mg/1 Other (Specify Compounds and - c, Grease and Oils mg/I Fe - Iron mg/I Concentration units) r o Hardness: Total mg/I Hg - Mercury mg/I Mp+l .. \.� N� cQ \�n_'�\p - � .)6% li- Phenol mg/I K- Potassium mg/I Sulfate mg/I Mg - Magnesium mg/I Specific Conductance uMhos Mn - Manganese mg/I Total Ammonia mg/I Na - Sodium mg/I TKN as N mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) EDS (O t * See back for instructions. Sign re of Per i ee (bf uthorized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION QR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; r, (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW 846; r (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, r October 26, 1984; 5. Measure*and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumpedibailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. GROUNDWATER QUALITY MONITORING: for additional forms COMPLIANCE REPORT FORM please write or call: Type or Use a ball-point pen and press firmly. Facility Name Address Well Location &Ar 3 LI 0 C1-g ` coo 3 " 1 ntj o '?q o '7 ' t t3 Well Identification Number /�?W -I I Well Depth 'IS, b Ft. Well DiameterLk,W"Sample (Screened) Interval Ft. To kq.0 Ft. Depth to Water Level 1�`Zft. below measuring point (before sampling) Measuring point is I tC ft. above land surface Gallons of water pumped/bailed before sampling -0 Field Analysis: pH 5 � 412 Specific Conductance "' uMhos Temp. k �1' Date Sample Collected '; ,ab —Date Lab Sae Analyzed 6 •a'`t Laboratory Name 2f\P-A01',, . ANr4\�},Glt-t mpplAL1 ,-)o-tk�njIc4 SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED COD _ Coliform: Coliform: MF Fecal MF Total (Note: Use MPN method for highly turbid samples) mg/I 00ml 00ml Dissolved Solids: Total mg/I pH (when analyzed) units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N Nitrate (NO3) as N Phosphorus: Total Al - Aluminum_ Ba - Barium Ca - Calcium_ Cd - Cadmium_ Chromium: Total _ Cu - Copper Fe - Iron Hg - Mercury_ K - Potassium Mg - Magnesium _ Mn - Manganese _ Na - Sodium as P. I DIVISION OF WATER QUALITY - GROUNDWATER SECTION P.O. BOX 29578 RALEIGH, NO 27626.0578 (919)733-3221 PERMIT NUMBER: (REQUIRED)b Non -Discharge �. 000-'11111(I> NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of SI e Other Rotary Distributor Odor Appearance Certification No. bD NIA' YES NO mg/I Ni - Nickel mg/1 mg/1 Pb - Lead c mg/1 mg/1 Zn - Zinc ca mg/I mg/I Pesticides/Herbicides o mg/I (Specify Compounds) sr mg/I om ug/I mg/I va ug/I mg/I ug/I mg/I Other (Specify Compounds and - m� mg/I Concentration units) —" mg/I i?:C\'\t�0.�� eHir_ v� C1UT- L mg/I mg/I mg/I mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and %r 9 colloidal concentrations. (see #3 on back) See back for instructions. Signat2o`fperrrfit e (or uthorized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART QF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; - (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; r (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure -and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least TVolumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. GROUNDWATER QUALITY MONITORING: For additional forms COMPLIANCE REPORT FORM please write or call: Type or Use a ball-point pen and press firmly. Facility Name T�v,s�mnsir3 t T ice. Address (-'1Art� `c. GA, o,,-3ta�,Pr,.)C County GGc�tlnnc� Well Location Well Identification Number /14LJ -10 Well Depth Ft. Well Diameters "r Sample (Screened) Interval Ft. Tor`�c-D' Ft. Depth to Water Level Vt5t72 ft. below measuring point (before sampling) Measuring point is III; ft. above land surface Gallons of water pumped/bailed before sampling 3C Field Analysis: pH !n r t Specific Conductance — uMhos Temp. II t,r+-1 00C DIVISION OF WATER QUALITY - GROUNDWATER SECTION P.O. BOX29578 RALEIGH, NC 27626-0578 (919) 733-3221 PERMIT NUMBER: (REQUIRED) Non -Discharge W bZ NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge Other Rotary Distributor Odor '- Appearance Date Sample Collected 10 ' afa K b Date Lab Sample Anzed In ` t °WS' Laboratory Name ?PsgMNZ�t.. A,,)k ;�s�t ZA.,,alyC—qe (\Q, i c< Certification No. �( � SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED AJ�L_YES NO COD Coliform: Coliform: MF Fecal MF Total (Note: Use MPN method for highly turbid samples) _ mg/I /100ml /100ml Dissolved Solids: Total mg/I pH (when analyzed) LA,q units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/1 Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Signa re o Per rD r Authorized Agent`) GW-59 REV. 8/96 Ni - Nickel mg/1 Pb - Lead o mg/I Zn - Zinc o o mg/I Pesticides/Herbicides ` A� (Specify Compounds) m ug/I ug/I v m` ug/I Other (Specify Compounds and cn� Concentration units) _ Crn c;s-1 t�- A ,Jy1L- 11A.,2,%t� t Y.Ai� �.LJiI � aY � 5y e k)_ Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) Sto, (V See back for instructions. Date •` Submit blue and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART -OFF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION 911 SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number r . EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3.volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY - GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: P.O. BOX 29578 For additional forms RALEIGH, NO 27626.0578 COMPLIANCE REPORT FORM please write or call: (919)733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name 1STmnspr, 0!aSTe_. -,,4C Non -Discharge Z"C1 (Doc)-1 S Address G\A-3QI (_n.�n:y��_ QL_ County Sr.ni•1fvs� NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED Well Location �-l�i 2�' �-1S ` l3 U 4 r� f-O•.1G Zd`'' 'air 4� t. �'r (REQUIRED) Lagoon Septic Tank/Drain Field Well Identification Number Ml z-q Well Depth aErL2 Ft. Well Diameter s"Sam le Screened Interval P (Screened) Ft. To 36�_Ft. spray Field Subsurface Low -Pressure Piping (LPP) Depth to Water Level ft. below measuring point (before sampling) Land Application of Sludge Measuring point is—ft. above land surface 1 other Rotary Distributor Gallons of water pumped/bailed before sampling rL7 Field Analysis: pH h • W? Specific Conductance _ uMhos Temp. t 6,ct °C Odor Appearance — Date Sample Collected (n ao c� S? Date Lab Sample Analyzed 6, �L `A q Laboratory Name Phhq A fs r� A FZck. t /t- p, y n-Fnn.; •e c _ Certification No. SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED A!3-YES NO COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Pb - Lead o mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc o mg/I (Note: Use MPN method for highly turbid samples) Al - Aluminum mg/I Pesticides/Herbicides �� Dissolved Solids: Total mg/I Ba - Barium mg/I (Specify Compounds) _ om pH (when analyzed) h , a3 units Ca - Calcium mg/I u — g/I TOC mg/I Cd - Cadmium mg/I n ug/I Chloride mg/I Chromium: Total mg/I Arsenic mg/I Cu - Copper mg/I Other (Specify Compounds and ,nz Grease and Oils mg/I Fe - Iron mg/I Concentration units) Hardness: Total mg/I Hg - Mercury mg/I r Cs - Ilk - �:<.l �otgc�ih� - uS1L Phenol mg/I K- Potassium mg/I Sulfate mg/I Mg - Magnesium mg/I Specific Conductance uMhos Mn - Manganese mg/I Total Ammonia mg/I Na - Sodium mg/I TKN as N mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) eq * See back for instructions. Sig atur f P ittee or Authorized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW 846; (d) Test Procedures for the Analysis of Po!luants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, r' October 26, 1984; r 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well voluines are removed; samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY - GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: P.O. eox 29578 For additional forms RALEIGH, NC 27626-0578 COMPLIANCE REPORT FORM please write or call: (919) 733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name t 04c \ r nhe.Ae2- ; PJ C. Non -Discharge IN Cc c,30 c1 Address Pta,-,T 2 ,. NPDES Lt - t )nos r )C - County <c-i \ a << TYPE ODISPOSAL OPERATION BEING MONITORED Well Location i by Zy� t-tq� Lv.aG -7c)o �i td`I.aii (REQUIRED) Lagoon Septic Tank/Drain Field Well Identification Number Well Depth Ft. s Field subsurface Low -Pressure Well Diameter 21.00" Sample (Screened) Interval Ft. To Ft. Spray Piping (LPP) Depth to Water Level 12,2A� ft. below measuring point (before sampling) Land Application of Slue Measuring point is L-A1i ft. above land surface Other Gallons of water pumped/bailed before sampling Rotary Distributor Field Analysis: pH h . M o Specific Conductance - uMhos Temp. 00,4 °C Odor Appearance Date Sample Collected ti Date Lab Sam le Analyzed 6t3ltt4? s Laboratory Name Patz(��;� ti Ak\ k-,aN\ I.rt� 2rrtoe:Ls _CertificationNo. L; l SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED A-L _YES NO COD Coliform Coliform MF Fecal MF Total (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/1 Sulfate mg/l Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N Nitrate (NO3) as N_ Phosphorus: Total as P Al -Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Na - Sodium mg/I mg/I mg/1 mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I Ni - Nickel mg/I Pb - Lead mg/1 Zn - Zinc mg/I Pesticides/Herbicides co CD (Specify Compounds) C_ om — �;�Jg/I glg/I Other (Specify Compounds and =9 70,�n Concentration units) N� LDS - i, a - �:c1, Q6IL I eT2t3G\n1no,jtL 7z:c1 \.>:Lcearl.aaG - 11ODo L I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and q colloidal concentrations. (see #3 on back) See back for instructions. Si� f Plirittee Dr Authorized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At Ieasf 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well vo(uim6s'are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. GROUNDWATER QUALITY MONITORING: For additional forms COMPLIANCE REPORT FORM please write or call: Type or Facility pen ana press Well Location LA-C 2LO A_? ' \ 40 , b" `?C(o 'dl l U4 Well Identification Number AA w -(6 Well Depth .; F.O Ft. Well Diameter IND " Sample (Screened) Interval Ft. To 3b ,J Ft. Depth to Water Level 14 5.0 ft. below measuring point (before sampling) Measuring point is G.AO ft. above land surface Gallons of water pumped/bailed before sampling I O. (1) Field Analysis: pH b N6 Specific Conductance r uMhos Temp. C DIVISION OF WATER QUALITY • GROUNDWATER SECTION P.O. BOX 29578. RALEIGH, NC 27626.0578 (919) 733.3221. PERMIT NUMBER: (REQUIRED Non -Discharge NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge `^'— Other Rotary Distributor Odor — Appearance - Date Sample Collected F ?; ,u Q Date Lab Sample Analyzed f_. 3 Ufi Laboratory Name 4ntua;l.�a�,nnl�4nr��c< _ Certification No. SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED '�12YES NO COD _ Coliform: Coliform: MF Fecal MF Total (Note: Use MPN method for highly turbid samples) _ mg/I /loom[ /loom[ Dissolved Solids: Total mg/I pH (when analyzed) h �3 units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I a Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/[ Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. A, Signat re of er i ee (ol Authorized Agent') GW-59 REV. 8/96 Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc r o 7; mg/I Pesticides/Herbicides CIO (Specify Compounds) z om - = ug/I Ln = rn ug/I .+ m� ug/I Other (Specify Compounds and t( r" Concentration units) - CiS-\*1-_")'CN'N\SK)c'-eh-e_ -gip vs\L 1n 0"\kNna r' N.at _ \hok1 Zc\L Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) `_ w .% * See back for instructions. Date ** Submit blue and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART 2F SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION _R SAMPLING PROCEDURES, CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, r October 26, 1984; C 5. Measurorand record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least a volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. S. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM or Facility Name I nasl'mft�l�n_ �L, c, Address o%o.--Nk �• DIVISION OF WATER QUALITY - GROUNDWATER SECTION P.O. BOX.29578 For additional forms RALEIGH, NC 27626.0578 please write or call: (919) 733.3221Y PERMIT NUMBER: (REQUIRED) Non -Discharge W Q Q W''1'7gY NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED Well Location ! AT _3 (I' L)9(?4 t9" C.O 1C3 G° a"fr LAO. "' (REQUIRED) Lagoon Septic Tank/Drain Field Well Identification Number /" w h Well Depth riLt.0 Ft. Well Diameter1. 16 " Sample (Screened) Interval Ft. To 1�k. L) Ft. spray Field SubsuurfaccePiping P' ow -Pressure Depth to Water Level ft. below measuring point (before sampling) Land Application of Slud ie Measuring point is 3 , o ft. above land surface !� other Gallons of water pumped/bailed before sampling t cl7 Rotary Distributor Field Analysis: pH & v 3 3 Specific Conductance — uMhos Temp. C Odor — Appearance — Date Sample Collected G 'AO •4c2 Date Lab Sample Analyzed CkQ Laboratory Name LNzAc -rn �"r0s�1-;c.nl �n�rzasoR��s Certification No. L02( SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED .v YES NO pen and press COD mg/1 Nitrite (NO2) as N mg/I Ni - Nickel mg/1 Coliform: MF Fecal /100ml Nitrate (Nog) as N mg/I Pb - Lead mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc , o mg/I (Note: Use MPN method for highly turbid samples) Al - Aluminum mg/I Pesticides/Herbicides Dissolved Solids: Total mg/I Ba - Barium mg/I (Specify Compounds) rn pH (when analyzed) C. to units Ca - Calcium mg/I g 1Ug/l TOC mg/I Cd - Cadmium mg/1 cn F r ug/I Chloride mg/I Chromium: Total mg/l ,a g/l Arsenic mg/I Cu - Copper mg/I Other (Specify Compounds and �= �� Grease and Oils mg/I Fe - Iron mg/I Concentration units) Hardness: Total mg/I Hg - Mercury mg/I -&o aS(L Phenol mg/I K- Potassium mg/I vrz:Cvlrar�efil.e�e — 4Zhc lL Sulfate mg/I Mg - Magnesium mg/I Specific Conductance uMhos Mn - Manganese mg/I Total Ammonia mg/I Na - Sodium mg/I TKN as N mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) �1� S- P., See back for instructions. Sig ture o Pelfiittee Authorized Agent`) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION QR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; _ (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, r October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. ,; 6. At lbasP volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. GROUNDWATER QUALITY MONITORING: For additional forms COMPLIANCE REPORT FORM please write or call: or Facility Name nAcTrwhcif- e.V y i Nc . Address Q,"• t NO2. mtt ",k, P6 C_ County Well Location Well Identification Number Anw-H Well Depth I . 0 Ft. Well Diameter1,15 " Sample (Screened) Interval Ft. To'N 1, ZFt. Depth to Water Level 13 %5 5 ft. below measuring point (before sampling) Measuring point is ft. above land surface Gallons of water pumped/bailed before sampling i , O Field Analysis: pH IN %' 3 Specific Conductance — uMhos Temp. Date Sample Collected a .au •r\q Date Lab Sample Analyzed `3 Laboratory Name_ 9A.n-A&a rn A"�r\!:g F: r r'l jinn.:-_ SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIE pen and press COD _ Coliform: Coliform: mn/I MF Fecal /loom[ MF Total /loom[ (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) tnunits TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total _ mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I DIVISION OF WATER QUALITY- GROUNDWATER SECTION P.O. BOX 29578 RALEIGH, NO 27626-0578 (919)733-3221 PERMIT NUMBER: (REQUIRED) Non -Discharge \w1Q C'QO%ZCA. {� NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge Other Rotary Distributor D °C Odor — Appearance G8 Certification No. L1(21 n:iJi YES NO Nitrite (NO2) as N DIVISION OF WATER QUALITY- GROUNDWATER SECTION P.O. BOX 29578 RALEIGH, NO 27626-0578 (919)733-3221 PERMIT NUMBER: (REQUIRED) Non -Discharge \w1Q C'QO%ZCA. {� NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge Other Rotary Distributor D °C Odor — Appearance G8 Certification No. L1(21 n:iJi YES NO Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I Ni - Nickel = mg/I Pb - Lead rr, mg/I Zn - Zinc mg/I Pesticides/Herbicides zm (Specify Compounds)cil :r:m Other (Specify Compounds and ,� � Concentration units) o 0 C lS - l t a - a % r_kn1020 e tk7e.a ` 970 QtIL I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and c� Q colloidal concentrations. (see #3 on back) See back for instructions. Sign ture o Permi ee (or uthorized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; r; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measurs'and record the depth of water in the well prior to pumping or bailing any water from the well. c• 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. GROUNDWATER QUALITY MONITORING: For additional forms COMPLIANCE REPORT FORM please write or call: Type or Use a ball-point pen and press firmly. Facility Name Ton4�n�rtSTeD_ kiN�. Address P\nNT R2 DIVISION OF WATER QUALITY - GROUNDWATER SECTION P.O. BOX,29578 RALEIGH, INC 27626-0578 (919)'733-3221 PERMIT NUMBER: (REQUIRED)) Non -Discharge. vJ a ewf 0ii c1'� NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED REQUIRED Well Location Lrit �Lic q-y .�6.(�r` 1_n�,,(, �1" ;ry 4�­I.3tr ( ) Lagoon Septic Tank/Drain Field Well Identification Number I'A W -3 Well Depth 30.o Ft. Well Diameter!,. Sample (Screened) Interval Ft. To 3c7,O Ft. spray Field Piping P 9( Subsurface LPPLow-Pressure ) Depth to Water Level \ ] .3O ft. below measuring point (before sampling) Land Application or Sludge Measuring point is ft. above land surface other Gallons of water pumped/bailed before sampling I ro Rotary Distributor Field Analysis: pH r. , (� L4 Specific Conductance — uMhos Temp. C Odor — Appearance _ Date Sample Collected Date Lab Sample Analyzed 6 ` \ r\,g t t Q Laboratory Name Pnnac�'.$m A %r r, 1 � tzco-,\ La-1�,o2wton_;r— Certification No. SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED N 1 A YES NO COD _ Coliform: Coliform: mn/I MF Fecal /100ml MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) 6.'t 3 units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total _ mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/1 Nitrite (NO2) as N mg/1 Nitrate (Nog) as N mg/1 Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/1 K - Potassium mg/1 Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Si ature f Per ittee or Authorized Agent`) GW-59 REV. 8/96 Ni - Nickel mg/I Pb - Lead mg/1 Zn - Zinc m mg/1 Pesticides/Herbicides �= (Specify Compounds) cc' rn .. Other (Specify Compounds and rn to � Concentration units) cis - l,l - J:c�loear.fhr Icy CTao IL 61'e11- i-aZo.a.c P+I.eNc - au u,I,L Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) See back for instructions. Date •* Submit blue and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At leasf 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4, above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY - GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: P.O. 2 For additional Corms NC 626- RALEIGH, NC 27626.0578 COMPLIANCE REPORT FORM please write or caul (919) 733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Facility Name 1n`js Mlle I eV_ Non -Discharge 060 Address NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED "III 1+' �C.C1'tf}Jc� o County Well Location LAT 340 �F�r ] ,3 LDraG �(�� ai yf,(��rr (REQUIRED) Lagoon Septic Tank Drain Field Well Identification Number M(N- a Well Depth —Ft. rr Well Diameter k � 3 5 Sample (Screened) Interval Ft. To 30, 0 Ft. Spray Field Subsurface Low -Pressure Piping Depth to Water Level 1 S, 6`� ft. below measuring point (before sampling) (LPP) Land Application of Stud Measuring point is i . 10 ft. above land surface Other Distributor Gallons of water pum ed/bailed before sampling IC)Rotary Field Analysis: pH 64 Specific Conductance uMhos Temp. °C Odor — Appearance Date Sample Colle led 1E'aO' q Date Lab Sample Analyzed l •qq ANPr�.;�N:Gfx( uy� Laboratory Name �R�*� �n1 (cS Certification No. SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED N14 YES NO o COD Coliform: Coliform: ma/I MF Fecal /100ml MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) 4 '38 units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Ni - Nickel tng/I Nitrate (NO3) as N mg/I Pb - Lead r#ig/I Phosphorus: Total as P mg/1 Zn - Zinc — ". g/I Al - Aluminum mg/I Pesticides/Herbicides Ba - Barium mg/I (Specify Compounds) y 11-1 C:3. Ca -Calcium mg/I g/I Cd - Cadmium mg/I ` l Ig/I Chromium: Total mg/I o dug/I Cu - Copper mg/I Other (Specify Compounds and Fe - Iron Hg - Mercury mg/I mg/I Concentration units) M�t\..P. ' r. C\ — IO1 ug)L K - Potassium mg/I ``e ia; Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) See back for instructions. Sign to f ermitte (or Authorized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8196 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. - Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of -Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition,1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be.collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official docurnents. DIVISION OF WATER QUALITY - GROUNDWATER SECTION P.O. BOX 29578 GROUNDWATER QUALITY MONITORING: 626- For additional forms RALEIGR, NC 27fi28.0578 COMPLIANCE REPORT FORM please write or call: (919) 733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED Facility Name T',A,S q<TrQ T 0C Non -Discharge � Address AtoRA,.tr QNPDES (_n.,2:,ati.,9 � 1�C County SCttlRad TYPEDISPOSAL OPERATION BEING MONITORED n�e� (REQUIRED) Well Location i r cx2"7 ' f-c7N& 79.O 7�Zf Lagoon Septic Tank/Drain Field Well Identification Number m W" I Well Depth ab ,0 Ft. Well Diameter ')-,0" Sample (Screened) Interval Ft. To ah ,b Ft. Depth to Water Level 1 a • 1 `I ft. below measuring point (before sampling) Measuring point is 0 ,b ft. above land surface Gallons of water pumped/bailed before sampling '1 •0 Field Analysis: pH (,%L tLt Specific Conductance uMhos Temp.:O• °C Date Sample Collected a • OO ^1 Date Lab Sample Analyzed 6 • A "kS Laboratory Name QAcb- iprn A. aLg+;rAi Spray Field Subsurface Low -Pressure Piping (LPP) Land. Application of Sludge 7� Other Rotary Distributor Odor r Appearance — Certification No. NS SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED NIA YES NO COD Coliform: Coliform: MF Fecal /10om[ MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) r,.S'? units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N Nitrate (NO3) as N Phosphorus: Total AI - Aluminum_ Ba - Barium Ca - Calcium_ Cd - Cadmium_ Chromium: Total _ Cu - Copper Fe - Iron Hg - Mercury_ K - Potassium Mg - Magnesium _ Mn - Manganese _ Na - Sodium as P mg/I Ni - Nickel r 7 mg/I Pb - Lead w ` mg/I Zn - Zinc �— mg/I Pesticides/Herbicides == 5 mg/I (Specify Compounds) cs1 mg/I 1 mg/I - mg/I mg/I Other (Specify Compounds and - F ` mg/I Concentration units) mg/I T2\try\D L 7 Qt\1C Nt" - CC Z mg/I mg/I mg/I mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) � qS c - Io - See back for instructions. Signs ure q PPe?n­tee r Authorized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE 94. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD III Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED A5 WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT AREA PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION QR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Directors Division of Environmental _ . Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. c. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign off icial'documents. DIVISION OF WATER QUALITY - GROUNDWATER SECTION 29578 GROUNDWATER QUALITY MONITORING: �RO P.Q. NC For additional forms RALEIGH,.NC 27626.7626- 0578 COMPLIANCE REPORT FORM please write or call: (919)733-3221 _ Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIR e Facility Name Non -Discharge Address NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED Uri Ur C CDUnty (REQUIRED) Well Location Well Identification Number Well Depth Ft. Well Diameter Sample (Screened) Interval Ft. To Ft. Depth to Water Level ft. below measuring point (before sampling) Measuring point is-ft. above land surface Gallons of water pumped/baailed before sampling Field Analysis: . Co .7_ Specd'fic Conductance — uMhos Temp. ° Date Sample Collected ' a D Date Lab Sample Analyzed I • P 1 ' g Laboratory Na t rh CAI k ruiSntS SAMPLES FOR METALS WERE COLLEdTED UNFILTERED AND FIELD ACIDIFIED h COD Coliform: MF Fecal Coliform: MF Total _ mg/I /100ml /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) 5. units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N Nitrate (NO3) as N_ Phosphorus: Total as P Al - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Na - Sodium Lagoon Septic TanWDrain Field Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Slud e Other Rotary Distributor Odor — Appearance Certification No. 491 `0 �' YES NO mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I mg/I Ni - Nickel Pb - Lead Zn - Zinc Pesticides/Herbicides (Specify Compounds) mg/I —c m9 /I —r mg/I ug/I ug/I ug/I Other (Specify Compounds and Concentration units L Cam�C) IIa-b"1arD2 end-q�,9 fri D 2n� IL I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values shREi6&lk1Fl®d and , (� colloidal concentrations. (see #3 on back) / 77 l�2 / "t FSee back for instructions. Signat re Permittee (or ut rized Agent*) Date ubmit blue and ye#AcyV_1gLw address above. GW-59 REV. 8/96 nr_%j. OFFICE COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 30300 for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES-IN"THE FIELD !!t Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. ." ":... . _ "_.. . Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, N T THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title ) 5„ North Carolina Administrative Code, Subchapter 2L, analytical -procedures shall be in accordance with the methods described in one of the following publications, or by other methods', approved beforehand by the Director, Division of Environmental. Management:_ `.:. _ .. " . " 1 ........ (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; Y; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition,1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3-volumes of" Water,!n the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes_are:re_mQved, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH?SeCiffc6r�ituctanGe, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrai2din accordance with recommendations by the manufacturer. 9. Samples must be #filtered; tfirougll~at, 0:95 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample containef should be labeidd a#rt;(1e time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent"is_aay�Cp erase* officer or public official authorized by the company, corporation, or governmental body to sign official'documents. ,.., . GROUNDWATER QUALITY MONITORING: For atlditional forms COMPLIANCE REPORT FORM please write or call: DIVISION OF WATER QUALITY • GROUNDWATER SECTION P.O.Box 626- RALEIGH, NC 27626-0678 (919)733-3221 Type or sea ball-point pen and press firmly. PERMIT NUMBER: (REQUIR -�ir h Facility Name Non -Discharge �%%9$ Address Gf,d NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED ,1AY r n Well Location LAT ?i4D `iA 0o'% LONG ^Cniinty�l5�4 ! 1 a% r (REQUIRED) Lagoon Septic Tank Drain Field Well Identification Number M LA-) — I Well Diameters ,D Sam le (Screened) Interval Well Depth , D Ft. Ft. To 45, 0 Ft. Spray Field Subsurface Low -Pressure Piping (LPP) Depth to Water Level 7,91 ft. below measuring point (before sampling) Land Application of Sludgg �_ Other T7: Measuring point is a r ft. above land surface 12,0 �O Rotary Distributor CO _? Gallons of water pumped/ ailed before sampling Field Analysis: pH 9 Specific Conductance LiMhos Temp. °C Odor — Appearance Co r„ r Date Sample Coll ted 1 a7 98 Date Lap Sample Analyzed I' ' 9% Analu+i eL+ort No. N 70 C— cam Laboratory Name RY7X�;!Ipn al ahoy- .S SAMPLES FOR METALS IERE CO f __TEA UNFILTERED AND FIELD ACIDIFIED R Certification YES —NO `�" COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel w"mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/1 Pb - Lead == mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc mg/I (Note: Use MPN method for highly turbid samples) Al - Aluminum mg/I Pesticides/Herbicides Dissolved Solids: Total mg/I Ba - Barium mg/I (Specify Compounds) pH (when analyzed) •a�units Ca - Calcium mg/I ug/I TOC mg/1 Cd - Cadmium mg/I ug/I Chloride mg/I Chromium: Total mg/I ug/I Arsenic mg/I Cu - Copper mg/I Other (Specify Compounds and Grease and Oils mg/I Fe - Iron mg/1 Concentration units) Hardness: Total mg/I Hg - Mercury mg/1 Phenol mg/I K - Potassium mg/I Sulfate mg/I Mg - Magnesium mg/I Specific Conductance uMhos Mn - Manganese mg/I Total Ammonia mg/I Na - Sodium mg/I TKN as N mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values shoL&KQ1{" Ived and Colloidal cor796kr4)Aft9ee #3 on back) See back for instructions. Si atur of ermittee or thorized Agent*) Date •* Submit blue and yellow copies only to address above. GW-59 REV. 8/96 " COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection: 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS� WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART gFF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION QR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 11 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division,of Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition,1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for PH Pecif Cori ictartct't�"r.dtu[e;jodor and appearance must be made in the field on unfiltered samples when the sample is collected. "... 7:4 3� 8. Field equipment must be calibrated in accordance with.recommendations by the manufacturer. .,r 9. Samples must be filtered _fltJd6d 0.45 micron filtq; imFti'Mately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the:time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. - DIVISION OF WATER QUALITY- GROUNDWATER SECTION QUALITY MONITORING: P.OGROUNDWATER 7626- For additional forms IG NO RALEIGH, NC27626�0578 COMPLIANCE REPORT FORM please write orcallr (919)733-3221 - Type or usea ball-point pen and press firmly. I PERMIT NUMBER: (REQU`R•�D], 6 MQ % %� Facility Name 'r•u 1►7C • Non -Discharge W NPDES Address�lan} (Z TYPE OF DISPOSAL OPERATION BEING MONITORED C- County n a r q Well Location) ATAT r S$' 3 NG 79 01 -� LI�(0'IO(O (REQUIRED) Lagoon Septic Tank/Drain Field Well Identification Number MIA) Well Depth -0 Ft. Spray Field Subsurface Low -Pressure 11 Well Diameter�i9 (Screened) Interval Ft. To,��Ft. Piping (LPPA gSample Depth to Water Level ft. below measuring point (before sampling) Land Application of Sludge co �C _C:; V Measuring point is 1,30 ft. above land surface Other Rotary Distributor � , _ Qt— Gallons of water pum ed/bailed before sampling c71.O — II oC — _ of Field Analysis: pH �4Specific Conductance uMhos Temp. -D Odor Appearance ro M, Date Sample Colle ted 1 ' a'1 9 `6 Date Lab Sampl�1 Anal zed I' Al- `)1A Laboratory Name rad�ar.r. flrA%A� i I styiri tt n vs Certification No. T$I SAMPLES FOR METALS WdRE COLLE&ED UNFILTERED AND FIELD ACIDIFIED YES NO COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel P, mg/1 Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Pb - Lead mg/1 Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn -Zinc mg/I (Note: Use MPN method for highly turbid samples) Al - Aluminum mg/I Pesticides/Herbicides Dissolved Solids: Total mg/I Ba - Barium mg/I (Specify Compounds) pH (when analyzed) , oR units Ca - Calcium mg/I ug/1 TOC mg/I Cd - Cadmium mg/I ug/I Chloride mg/I Chromium: Total mg/I ug/1 Arsenic mg/I Cu - Copper mg/I Other (Specify Compounds and Grease and Oils mg/I Fe - Iron mg/I Concentration nits) TrtGhjoro -13 u9I Hardness: Total mg/I Hg - Mercury mg/I aAena- L Phenol mg/I K - Potassium mg/I Sulfate mg/I Mg - Magnesium mg/I Specific Conductance uMhos Mn - Manganese mg/I Total Ammonia mg/I Na - Sodium mg/IRECEn-,,;=n TKN as N mg/I 7' 9 I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Z- Z ,Q@ Sig at f Permittee (o Aut orized Agent*) Date GW-59 REV. 8/96 Note: Values s colloidal solved and (see #3 on back) * See back for instructions. ** Submit blue and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDINGTIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPL•ESJN"THE FIELD 111 Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT -THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION PR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative. Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Diviston of Environmental Management: - (a) Standard Methods for the Examination of Water'and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR' Part 136, October 26, 1984; • - 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water_ in the well shouldpe pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well Volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. y dwz._ 7. Determination for pH, Specify QQnductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. �' % , • ' '' S 8. Field equipment must be calibrated in accordance with recom pidations by the manufacturer. 9. Samples must be filtered. throagh.q 045 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container�"hould`b'e labeled at the time of collection with -the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. GROUNDWATER QUALITY MONITORING- For additional forms COMPLIANCE REPORT FORM please write or call: or Facility pen and press Well Location I RI 6!t- 9 / ` ,-AP t9 IJIr`L-e /- a r. `t r- Z Well Identification Number fK1W 3 Well Depth 30.4 Ft. It Well Diameter I101Sam,(�le (Screened) interval Ft. To 30, 0 Ft. Depth to Water Level �3 ft. below measuring point (before sampling) Measuring point is 5, ft. above land surface Gallons of water pumped/b iled before sampling of r D Field Analysis: pHSpecific Conductance — uMhos Temp. I�^ Date Sample Collected Laboratory Name C-Ir SAMPLES FOR METALS DIVISION OF WATER QUALITY- GROUNDWATER SECTION P.O. BOX29578 RALEIGH, NC 27626-0578 (919)733.3221 PERMIT NUMBER:(REQUlgyb OOD,77`l8, Non -Discharge WW NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Spray Field Subsurface Low -Pressure Piping (LP� Land Application of Slud Other f-1 f^ Rotary Distributor t7J _Jc� y oC Odor Appearance— ca I LAWr'CA_T*Vr% Certification No. UNFILTERED AND FIELD ACIDIFIED A YES COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed)units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I NO Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. 2 -2co -9R '/ — C' LALL�� — Sig ture f Permittee (or A thorized Agent*) Date GW-59 REV. 8/96 L4 8 I Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Pesticides/Herbicides (Specify Compounds) ug/I ug/I ug/I Other (Specify Compounds and Co centration units) / ct-1,g-DichloV-Qe ter Suy L TrT� orpe ens 5fn� u4 /►. Note: Values s colloidal �d and #3 on back) * See back for instructions. ** Submit blue and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE ##4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES'INTHE FIELD !i! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. �- Sample preparation in the laboratory (extraction and filtration) must be completed within- 727hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION_QR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, pivision of Environmental_ , Management: F - (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes. of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes.aee.Yemoved, samples,can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered through a f 45•micron filter immediately after collection when a dissolved analysis is required. (See #4. above) pu •„e ;`�. a i;.':>t 1 O.The sample containe iafioiil&bapow at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY - GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: P.O. 13Ox 29s7$ For additional forms RALEIGH, NO 27626.0578 COMPLIANCE REPORT FORM please write or call: (919)733-3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIR Facility Name lT_t_ G• Non -Discharge M 007-29W Address NPDES N C— County f� (REQUIRED) TYPE OF DISPOSAL OPERATION BEING MONITORED Well Location Lagoon Septic Tank/Drain Field Well Identification Nun)0er MLV- 4 Well Depth d1-U Well Diameters. as Sample (Screened) Interval Ft. To�211 Depth to Water Level 940 ft. below measuring point (before sampling) Measuring point is—ft. above land surface Gallons of water pumped/b@iled before sampling a•O Field Analysis: pH �7' 3 1 —Specific Conductance — uMhos Temp. Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of SI e Other Rotary Distributor Odor Appearance — Date Sample Collected I • of 1 "I�5 Date Lab Sample Analyzed 1' ac f • r a Laboratory Name �Arp�Igwl ono Iujlt'CAI Laboro�iyri e5 Certification No. SAMPLES FOR METALS WY=RE COLLE. .IED UNFILTERED TERED AND FIELD ACIDIFIED �Y YES NO try ^' co _. COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/1 pH (when analyzed) 5.(o3 units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/1 TKN as N mg/I Nitrite (NO2) as N mg/I Ni - Nickel mg/l Nitrate (NO3) as N mg/1 Pb - Lead --ing/I Phosphorus: Total as P mg/1 Zn -Zinc Al - Aluminum mg/I Pesticides/Herbicides Ba - Barium mg/I (Specify Compounds) - �= Ca - Calcium mg/I w ug/I Cd - Cadmium mg/I ug/I Chromium: Total mg/1 ug/I Cu - Copper mg/1 Other (Specify Compounds and Fe - Iron Hg - Mercury mg/I mg/I Concentration units) dT, a Dic1 dorDtlklOu_- Sao uy L K- Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/1 I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and Sign ure)f Permittee (r Au orized Agent*) GW-59 REV. 8/96 colloidal (see #3 on back) r r"%a. t See back for instructions. Date ** Submit blue and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES - Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be'submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION _QR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the, methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental , Management: _ .. (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition,1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; = 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least,3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes. are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. i 8. Field equipment must be calibratgd in accordance with recommendations by the manufacturer. 9. Samples must be filtered through.,; Q.J5 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 1 O.The sample container slsdiNEel •Iape#I'ed &t;the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY GROUNDWATER SECTION P.O. BOX2 GROUNDWATER QUALITY MONITORING: 26- For additional forms RALEIGH, NO 27626-0678 COMPLIANCE REPORT FORM please write or call: (919)733-3221 or Facility Name Address pen ano press PERMIT NUMBER: (REQUIRtUb )0779 d Non -Discharge ((��GGII u.[! 0 NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Well Location G f 0 q u r ' g ,r Lagoon Septic Tan1-0Drair{_ield Well Identification Nugiber M W -S )'a7 Well Depth oZ - 0 Ft. To�SLFt. Spray Field �= Subsurfaces ow -Pressure E-j Well Diameter Sample (Screened) Interval Ft. Piping (LAP.}t F:7 Depth to Water Level (e05 ft. below measuring point (before sampling) Land Application of Sludy� � other c r,'. Measuring point is 3, DO ft. above land surface !- Rotary Distributor � Gallons of water pumped/bailed before sampling ark _1 Field Analysis: pH oZ Specific Conductance uMhos Temp. 15• °C Odor Appearance Date Sample Collected Date Lap Sample Analyzed I ' oth' 78 Laboratory Name ?try i M ftc born i Certification No. SAMPLES FOR METALS WERE COLLb",TED UNFILTERED AND FIELD ACIDIFIED n AYES NO vI '" COD mg/I Coliform: MF Fecal /loom[ Coliform: MFTotal /loom) (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/1 pH (when analyzed) units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils Hardness: Total Phenol mg/I mg/I mg/I Sulfate mg/I Specific Conductance uMhos Nitrite (NO2) as N Nitrate (NO3) as N Phosphorus: Total Al - Aluminum_ Ba - Barium Ca - Calcium_ Cd - Cadmium_ Chromium: Total Cu - Copper Fe - Iron Hg - Mercury_ K - Potassium Mg - Magnesium _ Mn - Manganese _ as P. mg/I Ni - Nickel mg/I mg/I Pb - Lead mg/I mg/I Zn - Zinc mg/I mg/I Pesticides/Herbicides mg/I (Specify Compounds) mg/I ug/I mg/I ug/I mg/I ug/I mg/I Other (Specify Compounds and mg/I Concentration units mg/I C-111 o1- D; c� o ro i e- qCD mg/I TrloroeA_- (P= J%L. I_ mg/1 mg/I Total Ammonia mg/I Na - Sodium mg/I TKN as N mg/1 t yea I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values sh6Uld refle dissolved and (�Q colloidal=9?"iid . (see #3 on back) 2 2 CD "lC FTSeeb ack for InstructionsVV1)Sig of Permittee or thorized Agent`) Date Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.. ,, 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be'subrrlitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection.' 3. ANALYSES ARE TO BE MADEOF THE MOBILE.CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT AREA PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION,QR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods cJescribed in one of the following publications, or by other methods approved beforehand by the Director, Division of EnvironmentalC. _... " Management: (a) Standard Methods for the Examination of Water,and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition,1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least.3youlumes of water in_ the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes ,are1..removed, samp1.lQsc1.an.be.coll@cted as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance,,temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered tlirou 'h a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container shoyldb,,glaf3elo;1 of the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent" is any corpolte,:officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY - GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: P.O. BOX NIC 29673 :For additional forms RALEIGH, NC 2762&0578 COMPLIANCE REPORT FORM please write or call: (919) 733-3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIggEEpp gyp Facility Name ^ Q T.C. • Non -Discharge W� 00775M Address NPDES Y U G Count a n TYPE OF DISPOSAL OPERATION BEING MONITORED LOJAc f v , (REQUIRED) Well Location T 5. � G Lagoon Septic Tank//Drairf Field Well Identification Nur ber f.U" Well Depth70'ti, Ft. rSpray Field Subsurfacx w-Pressure Well Diameter�Sample (Screened) Interval Ft. To�Ft. Piping (LgR)I j :; Depth to Water Level lb Qq ft. below measuring point (before sampling) Land Application of sludg ua - M Measuring point is q, Ro ft. above land surface^ other ry `v,; id O Rotary Distributor �. Gallons of water pum ed/b sled before sampling Field Analysis: pH �' $ S ecific Conductance " uMhos Temp. °C Odor Appearance Date Sample Collected Date La Simple Analyzed /p I = Ti=`: f� LIE Laboratory Name �a 'IiM �R u artt rl e. Certification No. W u, SAMPLES FOR METALS WIRE GOLLEC. dD UNFILTERED TERED AND FIELD ACIDIFIED r? LX YES NO cn c-! COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) lam I units TOC mg/I Chloride mg/1 Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al -Aluminum mg/1 Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/1 Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. )UM %> � -2& 'fie Sign ure f Pe mittee (o(Au orized Agent') Date GW-59 REV. 8/96 Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Pesticides/Herbicides (Specify Compounds) ug/I ug/I Ug/I Other (Specify Compounds and Concentration units CA I , a- D�cl,ioroe. Fl,Pr--I qo fcg)L -19-cW Drop 2nL - ! -DDT 0� IFa G� Note: Values shQjujd reflect dissolved and colloidal N(N ► EE(see #3 on back) ' See back for instructions. " Submit blue and yellow copies only to address above. COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1.. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use StandardMethod 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD if' Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and shb fd lie submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection: 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT _ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per TitI6.15, North Carolina Administrative Code, Subchapter 2L, analytical -procedures shall be in accordance with the methods. described in one of the following publications, or by other methods approved beforehand by the Director, _Division of Environmental __ r Management: - (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can.b.e collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conduc%ance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 'r 8. Field equipment must be eali6rated in accordance with recommendations by the manufacturer. 9. Samples must be filtered throe jh 3,0,�15 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) ::1✓.. t .ti .� 10.The sample containersfiould' be9aksered'at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official•documents. GROUNDWATER QUALITY MONITORING: For additional forms COMPLIANCE REPORT FORM please Write or oaM DIVISION OF WATER QUALITY - GROUNDWATER SECTION. P.O. BOX 29578 RALEIGH, NO 27626-0578 (919) 733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIF}Ep �M r�r Non -Discharge W & OX77 % a Facility Name r NPDES Address A C- TYPE OF DISPOSAL OPERATION BEING MONITORED n Y Count n I not Y r f Well Location 4 UrV� 0 7' (REQUIRED) Lagoon Septic Tank/Drain Field Well Identification Number W --7 Well Depth 35•0 Ft. Interval Ft. To �Ft. spray Field Subsurface Low -Pressure Well Diameter0� Sample (Screened) Piping (LPP) Depth to Water Level S•43 ft. below measuring point (before sampling) Land Application of Slu Other Measuring point is • aD ft. above land surfac g p w Fotary Distributor M Gallons of water pumped/bailed before sampling a(o ' ivr °� - _ ri =M1 Field Analysis: pH Specific Conductance uMhos Temp. I' g Odor Appearance ,ni Date Sample Colle ed of - 98 pate L b S mple A alyzed . ✓ yg I J �' Laboratory Name AY I Certification No. SAMPLES FOR METALS RE COLLE ED UNFILTERED AND FIELD ACIDIFIED a'�YES NO COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) S�units TOC mg/1 Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/1 Phenol mg/1 Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I '!A; i Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/1 Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/1 K - Potassium mg/1 Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I ri Ni - Nickel = Pb - Lead E—� Zn - Zinc Pesticides/Herbicides (Specify Compounds) Other (Specify Compounds and ,in ntration un t,$) IIrir�lorD��f\4-nf?�— MD aAIL mg/I mg/I ug/I ug/1 ug/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Nate: Values s NN�`��k#ssolved and Colloidal FMA3. (see #3 on back) 98 See back for instructions. Sig(ature f Permittee horized Agent') Date *• Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD 11, Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Diyision.of Environmental _ Management: (a) Standard Methods for the Examination of Water'and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number ` EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; _ 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of -water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for M,.'.SpeCi ie bndu�Gtaripe, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrtited iii accordance with recommendations by the manufacturer. 9. Samples must be filte,74 hrc}{ghaLf,5.micron lifter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11. "Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. GROUNDWATER QUALITY MONITORING: For additional forms COMPLIANCE REPORT FORM please write or call: DIVISION OF WATER QUALITY -GROUNDWATER SECTION PX 29578 26- RALEIGH, N NC 27628.0578 (919) 733.3221 1 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRE Non -Discharge I0h 00077c?d Facility Name 1'P" 0 2c NPDES Address Ar •� r N Co t cb a TYPE OF DISPOSAL OPERATION BEING MONITORED n Well Location � � 0L• -r M (REQUIRED) 7f 55, _ Lagoon Septic Tank/Drain Field Well Identification Nupber MLA) — 9 Well Diameters Sample (Screened) Interval Well Depth 5' a Ft. 0 Ft. To 5 Ft. Spray Field Subsurfacece Low-P `ensure Piping (LPPCO Depth to Water Level 10 r� ft. below measuring point (before sampling) Land Application of SI d e co Other Measuring point is—ft. above land surface 7r aField f_q Rotary Distributor Tl Gallons of water pu�mped/b iled before sampling Temp.15, S oC Odor — AppearanceDate Analysis: pH Specific Conductance q Date Lap uMhos Sample Analyzedgg Sample Colle� Laboratory Name ckr-aol;wr+rn Ana, N' l f pt�rct�DricS Certification No. ' / L19 1 SAMPLES FOR METALS V:IoC w1LLCC• tD UNFILTERED 11 TFPFfI AND FIELD ACIDIFIED yES NO COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel ci mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Pb - Lead mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc mg/I (Note: Use MPN method for highly turbid samples) Al - Aluminum mg/I Pesticides/Herbicides Dissolved Solids: Total mg/1 Ba - Barium mg/I (Specify Compounds) pH (when analyzed) r 1 units Ca - Calcium mg/I ug/I TOC mg/I Cd - Cadmium mg/I ug/I Chloride mg/I Chromium: Total mg/I ug/I Arsenic mg/I Cu - Copper mg/I Other (Specify Compounds and Grease and Oils mg/I Fe - Iron mg/I Concentration units) Hardness: Total mg/I Hg - Mercury mg/I Phenol mg/I K - Potassium mg/I _- Sulfate mg/I Mg - Magnesium mg/I Specific Conductance uMhos Mn - Manganese mg/I,Tlgr�� Total Ammonia mg/I Na - Sodium mg/I TKN as N mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see#3 on back) See back for instructions. Sign ture f Per ittee (oK&utbAbrized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD III Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. ' Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours ofcollection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NDT..•THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods.approved beforehand by the Director,"Division of Environmental- Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removbd S—W� s''ca'R&c lfected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH„Specifictbrlductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. •• s a! E �r 't 8. Field equipment must ba lera&t ?(rn,pyccordancetyith recommendations by the manufacturer 9. Samples must be filtered:1hr6bh 3 g-4t r icron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents: DIVISION OF WATER QUALITY - GROUNDWATERSECTION GROUNDWATER QUALITY MONITORING: P.O. BOX 29578 For additional forms RALEIGH, NC 27626.0578 COMPLIANCE REPORT FORM please write or call; (919)733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED ,�/ Facility Name Non -Discharge I'�77�25 Address �'�I NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED r-U/' C CDUnty Q (REQUIRED) Well Location Lagoon Septic Tank/Drain Field Well Identification Number f•Yt W' f U Well Depth a5 • D Ft. r Well Diameter Q a'mj�le (Screened) Interval Ft. To �O —Ft. Depth to Water Level eft. below measuring point (before sampling) Measuring point is Ioff 5 ft. above land surfaco Gallons of water pumped/bailed before sampling Field Analysis: pH � Spgoific Conductance r uMhos Temp.. Date Sample CoIlec yd f a I Date Lab sample Analyzed f r Laboratory Name Ta✓txL ��t * 1 r1o� U ' 1 L9 b0KtfDn �S SAMPLES FOR METALS VV91RE COLLEC D UNFILTERED AND FIELD ACIDIFIED COD mg/I Coliform: MF Fecal /100m1 Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) rJT R units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge, X. Other Rotary Distributor r Odor Appearance Certification No. 4901 �YES NO Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/1 Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I co co n rV v Ni - Nickel e mg/I Pb - Lead mg/I Zn - Zinc ' mg/I Pesticides/Herbicides s (Specify Compounds) ug/I ug/I ug/I Other (Specify Compounds and Concentration units) /lic-1 - is r I en -0 ] aS�L Tp:j�2 joroe.,tkpbj. - 77 ul' L M1')� I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values s Alsolved and Colloidal co d arts. (see #3 on back) Z,2(,.q UQ See back for instructions. Signa re Permittee (oLAOorized Agent') Date •' Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use`Stan der d Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD III Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. - - Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION ,OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental.-, Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the well should' be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are_ removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for H,'Sp c'i a pnd t`c32ni;e, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. °` F 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filteedd-thpg6 4� 5 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 1 O.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY • GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: P.O. sox29578 For additional forms ,RALEIGH, NC 27626- 7626.0578 COMPLIANCEREPORT FORM please write or call: (919)733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED Facility Name l Q )-tf"' Non -Discharge WU W01-7gK Address NPDES tLrt of Count c-0 0.n TYPE OF DISPOSAL OPERATION BEING MONITORED Well Location T e r 00, 2 n LD E 9 y 7 r 3.0 n (REQUIRED) Lagoon Septic Tank/Drain Field Well Identification Number iY)W— II Well Depth ,0 Ft. Ir Spray Field Subsurface Low -Pressure Well Diameter Sample (Screened) Interval Ft. To a5Ft. Piping (LPP) Depth to Water Level 61 - ft. below measuring point (before sampling) Land Application of Sludge Measuring point is 3_3,1-5 ft. above land surface other Gallons of water pumped/bailed before samplinq 37.0 Rotary Distributor Field Analysis: pH J *1 Appearance Date Sample CoIle ted � Ck a a>r uate Lao asr le Hn I zea r � 6 , m� ��Y� u 1 �i borQ tOn e 5 o No. o c.: Laboratory Name t a Certification SAMPLES FOR METAL�OLLEC D UNFILTERED AND FIELD ACIDIFIED 9Lr YES NO c COD mg/I Nitrite (NO2) as N mg/I Ni - Nickel ; _=mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I Pb - Lead 'Mmg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Zn - Zinc -;mg/I (Note: Use MPN method for highly turbid samples) AI - Aluminum mg/1 Pesticides/Herbicides _ n? Dissolved Solids: Total mg/I Ba - Barium mg/I (Specify Compounds) w pH (when analyzed) units Ca - Calcium mg/I 47, ug/I TOC mg/I Cd - Cadmium mg/1 ug/I Chloride mg/I Chromium: Total mg/1 ug/I Arsenic mg/I Cu - Copper mg/1 Other (Specify Compounds and Grease and Oils mg/I Fe - Iron mg/1 �oAnc ntration unit ) Hardness: Total mg/I Hg - Mercury mg/I Jri� oro v end — I t'i D Phenol mg/I K - Potassium mg/I Sulfate mg/I Mg - Magnesium mg/I 11 Ir-ems, Specific Conductance uMhos Mn - Manganese mg/I Total Ammonia mg/1 Na - Sodium mg/I 1�141998 TKN as N mg/1 I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values s11351j,.q§ solved and Q ff colloidal concentratio s. (see #3 on back) See back for instructions. Sighatuib of Permittee(&thorized Agent') Date Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES'IN THE'FIELD II! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT -THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical.procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, -Division of_ Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; _ 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least3 volumes of water in the well should. be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination fo[ pH; .Spe�feGgfidu`dtahce, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must tie callbrated in accordance with recommendations by the manufacturer. 9. Samples must be filter t 10` hdb% micron filter immediately after collection when a dissolved analysis is required. See #4. above 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. IGROUNDWATER QUALITY MONITORING: For additional forms COMPLIANCE REPORT FORM please write or call: Type or Use a ball-point pen and press firmly. Facility Name . asIm =rG• Well Location Well Identification Number MUJ— Id, Well Depth 615. O'U Ft. Well Diameter a,pi! Sample (Screened) Interval Ft. To •07 Ft. Depth to Water Level 7• 4 ft. below measuring point (before sampling) Measuring point isc�r L_ft. above land surface, Gallons of water pumped/bailed before sampling / DIVISION OF WATER QUALITY • GROUNDWATER SECTION P.O. BOX29578 RALEIGH, NC 27626-0578 (919) 733.3221 PERMIT NUMBE aUIWh OW7798� Non -Discharge rge ((�,((JJ NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED (REQUIRED) Lagoon Septic Tank/Drain Field Spray Field Subsurfacg Low Piessure Piping ( ) - Land Application of Sludge :, Other• M rr; D Rotary Distributor CCr Field Analysis: pH r a S ec'fic Conductance uMhos Temp.y15. 7 0 Odor Appearance c� Date Sample Coll '� Date a Sample A )alyzed�► � t � =_ Laboratory Name I I n Certification No. 9 = SAMPLES FOR METALS WERE COLLE ED UNFILTERED AND FIELD ACIDIFIED n !X YES NO �! COD Coliform: Coliform: mn/I MF Fecal /100ml MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) 5 0 units TOC mg/I Chloride mg/1 Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N Nitrate (NO3) as N_ Phosphorus: Total as P Al -Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Na - Sodium I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Signa ure Permittee ( r Aut orized Agent*) Date GW-59 REV. 8196 mg/I mg/I mg/I mg/I mg/I mg/I mg/1 mg/1 mg/I mg/I mg/I mg/I mg/I mg/I mg/I Ni - Nickel mg/1 Pb - Lead mg/I Zn - Zinc mg/I Pesticides/Herbicides (Specify Compounds) Other (Specify Compounds and ug/I ug/I ug/I L Note: Values shoulil reflect dissolved and colloid=f&s. (see #3 on back) * See back for instructions. ** Submit blue and yellow copies only to address above. 11 -''\\ COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN'THE FIELD 111 Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. ' . - • Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division, of Environmental Management:. (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; - 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of water in the. well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are rer idved,.sample's can fie collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be calibrated in'accbrdance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 ri1(oron filter immediately after collection when a dissolved analysis is required. (See #4. above) IV 10.The sample container slioyc,Ii&Nb&Q& the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY - GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: P.O.t30X29576 For additional forms RALEIGH, NC27626-0578 COMPLIANCE REPORT FORK please write or call: (919)733-3221 Type or Use as ball-point pen and press firmly. PERMIT NUMBER: (REQUIR D d Facility Name r rr7C. Non -Discharge JAM W�7%9n Address NPDES Ur'if1 r' County TYPE OF DISPOSAL OPERATION BEING MONITORED Well Location 3 0 % I (REQUIRED) Lagoon Septic Tank/Drain Field Well Identification Number YY)W '! S Well Depth .712.60 Ft. Well Diameters -0 to Sam le (Screened) Interval Ft. To 50. OO Ft. Depth to Water Level ft. below measuring point (before sampling) Measuring point is 3 ft. above land surface Gallons of water pumpedI�/bailed before sampling 17.0 Field Analysis: ' �.L Specific Conductance — uMhos Temp. ' Date Sample Colle.QWd -LAS 9Z. Date Lal) Sample Analyzed l c Laboratory Name SAMPLES FOR METALS COD Coliform: MF Fecal Coliform: MF Total UNFILTERED AND FIELD ACIDIFIED mg/I /1 ooml /1 ooml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) S. units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils Hardness: Total Phenol mg/I mg/I mg/I Sulfate mg/I Specific Conductance Total Ammonia uMhos mg/I Spray Field Subsurface Low -Pressure Piping (LPP) Land Application of Sludge _lli� Other Rotary Distributor Odor Appearance r-� _ m Certification No. YES NO rn n Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I Ni - Nickel —' Gam' mg/I Pb - Lead- `- mg/I Zn - Zinc — mg/I Pesticides/Herbicide (Specify Compounds) Y ug/I ug/I ug/I Other (Specify Compounds and Concentration units r - - D ick DY'Qe n[,-5 IA /L o C —Vj IL o� e TKN as N mg/I I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values s6�d�l /l±�r/��fl�Z�slt,r'�iCfisolved and FMB Colloidal FIdr;rf Offf1Q&. (see #3 on back) 2� v * See back for instructions. Signat re o er ittee or uthor ed Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be "submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within_72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THO E THAT ARE OF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION � AMPLIN PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. Asper Title 15, North Carolina Administrative Code, Subchapter 2L, analytical- procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of Environmental ... - Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition,1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3-volumes of water in the.well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pHJ S ec$ dncjudf e, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. " "x ` 8. Field equipment must be calibrated in accordance with recommendations by the manufacturer. 9. Samples must be filtered tW &hh- V-4_t micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY -GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: P.O.ox For additional forms RALEIGH, NO 2762fi,0578 626- COMPLIANCE REPORT FORM please write or call: (919)733-32211 Ty a or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIR�E� Facility Name me . Non -Discharge OR CX77RK Address '�' NPDES • C- County C _t h TYPE OF DISPOSAL OPERATION BEING MONITORED l7 t O p f r Well Location '3 Ltrn a (REQUIRED) Lagoon Septic Tank/Drain Field Well Identification Number Well Depth • OD Ft. n Well Diameter �i 0 S pie (Screened) Interval Ft. To 0• W Ft. Spray Field Subsurface Low -Pressure Piping (LPG ' ft. below measuring point before Depth to Water Level rJ g p (sampling) Land Application of Slud e c)o Other r Measuring point is 3•a0 ft. above land surfacp5 -'rt ,^ Gallons of water pumped /b^ fled before sampling ``tt Rotary Distributor Field Analysis: pH )' S e ifto Conductance uMhos Temp. 15 I oC g'�� )'o •F8 Odor Appearance t t Date Sample Collected Date Lab Sample Analyzed � 1/ Laboratory Name Yrn LR Q Certification No. " t g I m SAMPLES FOR METALS RE COLLEC ED UNFILTERED AND FIELD ACIDIFIED 1-ILL-YES NO — r•i� COD Coliform Coliform mn/I MF Fecal /100ml MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed)units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils Hardness: Total Phenol mg/I mg/I mg/I Sulfate mg/I Specific Conductance Total Ammonia uMhos mg/I Nitrite (NO2) as N _ Nitrate (NO3) as N_ Phosphorus: Total as AI - Aluminum Ba - Barium Ca - Calcium Cd - Cadmium Chromium: Total Cu - Copper Fe - Iron Hg - Mercury K - Potassium Mg - Magnesium Mn - Manganese Na - Sodium 0 mg/I Ni - Nickel mg/I mg/I Pb - Lead mg/I mg/I Zn - Zinc mg/I mg/I Pesticides/Herbicides mg/I (Specify Compounds) mg/I ug/I mg/I ug/I mg/I ug/I mg/I Other (Specify Compounds and mg/I mg/I Concentration unitg) Gi 1-I, a-DIXlorneRene-- a u91L mg/I fir; DrDe here. - 13 !2q L mg/I mg/I M-r.FINIFM, mg/I TKN as N mg/I 1 CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values sFrp��&�ssolved and Q colloidal COff9el* egs. (see #3 on back) l * See back for instructions. Sig Lure f ermittee or A horized Agent*) Date ** Submit blue and yellow copies only to address above. GW-59 REV. 8/96 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES IN THE FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be submitted to the lab within 24 hours. Sample preparation in the laboratory (extraction and filtration) must be completed within 72 Hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NOT THOSE THAT ARE A PART (QF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION OR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical, procedures shall be in accordance with the methods described in one of the following publications, or by other methods approved beforehand by the Director, Division of_ Environmental Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least-3 volumes of water in the, well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are'removed; samples can, be cQflected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pHt Secf'ndO'Y e, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be'cafibrdted in accordance with recommendations by the manufacturer. 9. Samples must be filtered-tlii a4�5 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents. DIVISION OF WATER QUALITY - GROUNDWATER SECTION GROUNDWATER QUALITY MONITORING: 9578 P.O.GNC2626- For additional forms RALEIGH, NC 27626�0578 COMPLIANCE REPORT FORM please write or call; (919)733.3221 Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED) Wa ccn7-%Address Facility Name Non -Discharge tvri NPDES TYPE OF DISPOSAL OPERATION BEING MONITORED CDUnfy (REQUIRED) Well Location Lagoon Septic Tank/Drain Field _ Well Identification Number Well Depth Ft. Spray Field Subsurface Low -Pressure Well Diameter Sample (Screened) Interval Ft. To Ft. Piping (LPP2 Depth to Water Level ft. below measuring point (before sampling) Land Application of Slu "^ Measuring point is-ft. above land surface Rotary Distributor (M Omer n c, C-� Gallons of water pumped/bailed before sampling , Field Analysis: Ic Conductance uMhos Temp. C a ' 9 9 Odor Appearance n er Date Sample Coll ted Date Lab S m le/jrtal ed 1 ' p )pt'1 �r$� Laboratory Name d '� COL Certification No. _ T SAMPLES FOR METALS VI) RE COLLE D UNFILTERED AND FIELD ACIDIFIED A. YES NO : _ rq :;;- COD mg/I Coliform: MF Fecal /100ml Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total mg/I pH (when analyzed) units TOC mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Hardness: Total mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia mg/I TKN as N mg/I Nitrite (NO2) as N mg/I Nitrate (NO3) as N mg/I Phosphorus: Total as P mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I Na - Sodium mg/I Ni - Nickel " mg/I Pb - Lead mg/I Zn - Zinc mg/I Pesticides/Herbicides (Specify Compounds) ug/I ug/I ug/I Other (Specify Compounds and Concentration units) RPrTIVED yA.4' 7 1099 I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and colloidal concentrations. (see #3 on back) Z . 2tD A v See back for instructions. Signekure,bf Permitte (or Authorized Agent*) Date •* Submit blue and yellow copies only to address above. GW-59 REV. 8/96 •• 1 COLLECTION AND ANALYSIS OF GROUNDWATER SAMPLES 1. Samples should be analyzed as soon as possible after collection. SAMPLES WHICH ARE NOT ANALYSED WITHIN THE HOLDING TIME SPECI- FIED FOR THE METHOD USED (SEE #4. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED. 2. Metals Analyses: Use Standard Method 3030C for sample preparation (mercury excluded). DO NOT FILTER METALS SAMPLES'IN T14E FIELD !!! Unfiltered samples must be collected for metals, then field acidified with 5 ml concentrated nitric acid per liter of sample,;and should be s�bfnitted to the lab within 24 hours. ' .. - . � - Sample preparation in the laboratory (extraction and filtration) must be completed within 72 hours of collection. 3. ANALYSES ARE TO BE MADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE GROUNDWATER, NQTNTHO E THAT ARE A PART QF SEDIMENT ASSOCIATED WITH WELL CONSTRUCTION 9RR SAMPLING PROCEDURES. CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION. 4. As per Title 15, North Carolina Administrative Code, Subchapter 2L, analytical procedures shall be in accordance with the, methods od_ s described in one of the following publications, or by other methods approved beforehand by the Director_, Division of Environmental. Management: (a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by ` American Public Health Association, American Water Works Association and Water Pollution Control Federation; (b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number EPA-600/4-79-020, as revised March 1983; (c) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency publication number SW-846; (d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136, October 26, 1984; 5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well. 6. At least 3 volumes of.Wgter.in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/bailed dry before 3 well volumes are removed, sa6nptp ea IJ6 * of(lected as soon as the well recovers to the point where enough water is available to collect your sample. 7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is collected. 8. Field equipment must be ili6r4�Ltedn£1lccordance with recommendations by the manufacturer. 9. Samples must be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above) 10.The sample container should be labeled at the time of collection with the facility name, well identification number and date and time collected. 11."Authorized agent' is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents: