WQ0007798_GW Monitoring_20001010

PARADIGM ANALYTICAL LABORATORIES, INC.
2627 Northchase Parkway S.E.
Wilmington, North Carolina 28405
[phone]
Fax [phone]
Mr. Rudy Smithwick October 10, 2000
Gulfstream Environmental
6509 Old Fort Road
Wilmington, NC 28411
Report Number: G216-82
Client Project ID: Toastmaster
Dear Mr. Smithwick,
Enclosed are the results of the analytical services performed under the
referenced project. Copies of this report and supporting data will be retained
in our files for a period of five years in the event they are required for future
r� reference. Any samples submitted to our laboratory will be retained for a
maximum of thirty (30) days from the date of this report unless other
arrangements are requested.
If there are any questions about the report or the services performed during this
project, please call for assistance. We will be happy to answer any questions or
concerns which you may have.
Thank you for using Paradigm Analytical Labs for your analytical services.
We look forward to working with you again on any additional analytical needs
which you may have.
Sincerely,
Paradigm Analytical Laboratories, Inc.
Laboratory Director
Mark Randall
I North Carolina Wastewater Certification #481
l _'

PARADIGM ANALYTICAL LABORATORIES, INC.
Results
for Volatiles
-
by
GC 601
f
Client Sample ID: MW-1
Analyzed By:
RNP
Client Project ID: Toastmaster
Date Collected:
09/26/00
Lab Sample ID: 96157
Date Received:
09/27/00
Lab Project ID: G216-82
Matrix:
Water
l; Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
10/2100
10
10
BQL
Bromoform
10/2/00
10
20
BQL
Bromomethane
10/2/00
10
20
BQL
Carbon tetrachloride
10/2100
10
10
BQL
Chlorobenzene
10/2/00
10
10
BQL
Chloroethane
1012/00
10
10
BQL
-- Chloroform
10/2/00
10
10
BQL
Chloromethane
10/2/00
10
10
BQL
Dibromochloromethane
1012100
10
10
BQL
1,2-Dibromoethane (EDB)
10/2/00
10
10
BQL
1,2-Dichlorobenzene
10/2/00
10
10
BQL
1,3-Dichlorobenzene
10/2/00
10
10
BQL
1,4-Dichlorobenzene
r
10/2/00
10
10
BQL
M-Dichloroethane
10/2/00
10
10
BQL
J_.' 1,2-Dichloroethane
10/2/00
10
10
BQL
M-Dichloroethene
10/2100
10
10
BQL
i l cis-1,2-Dichloroethene
10/2/00
10
10
BQL
trans-1,2-Dichloroethene
10/2/00
10
10
BQL
1,2-Dichloropropane
10/2100
10
10
BQL
- cis-1,3-Dichloropropene
10/2/00
10
10
BQL
trans-1,3-Dichloropropene
10/2/00
10
10
BQL
Methylene Chloride
10/2/00
10
50
BQL
— 1,1,2,2-Tetrachloroethane
10/2/00
10
10
Tetrachloroethene
10/2100
10
10
BQL
BQL
1,1,1-Trichloroethane
10/2/00
10
10
BQL
_ 1,1,2-Trichloroethane
10/2/00
10
10
BQL
Trichloroethene
10/2/00
10
10
140
Trichlorofluoromethane
10/2/00
10
10
BQL
Vinyl Chloride
10/2/00
10
10
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
_
Added
Result
Recovered
1,4-Dichlorobutane
40
36
89
Comments:
J All values corrected for dilution.
L Fl: gs:
BQL = Below quantitation limit.
_ Reviewed By:
Page 1 of 1
UN.C. Certification #481 S.C. Certification #99029

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Client Sample ID: MW-2
Analyzed By: RNP
Client Project ID: Toastmaster
Date Collected: 09/26/00
Lab Sample ID: 96158
Date Received: 09/27/00
Lab Project ID: G216-82
Matrix: Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
10/2/00
25
25
BQL
Bromoform
10/2/00
25
50
BQL
Bromomethane
10/2/00
25
50
BQL
Carbon tetrachloride
10/2/00
25
25
BQL
j Chlorobenzene
10/2/00
25
25
BQL
Chloroethane
10/2/00
25
25
BQL
Chloroform
10/2/00
25
25
BQL
Chloromethane
L
10/2100
25
25
BQL
Dibromochloromethane
10/2/00
25
25
BQL
1,2-Dibromoethane (EDB)
10/2/00
25
25
BQL
1,2-Dichlorobenzene
10/2/00
25
25
BQL
1,3-Dichlorobenzene
10/2/00
25
25
BQL
1,4-Dichlorobenzene
10/2/00
25
25
BQL
1,1-Dichloroethane
10/2/00
25
25
BQL
1,2-Dichloroethane
10/2/00
25
25
BQL
1,1-Dichloroethene
10/2/00
25
25
BQL
cis-1,2-Dichloroethene
10/2100
25
25
BQL
_. trans-1,2-Dichloroethene
10/2/00
25
25
1,2-Dichloropropane
10/2/00
25
25
BQL
BQL
— cis-1,3-Dichloropropene
10/2/00
25
25
BQL
trans-1,3-Dichloropropene
10/2/00
25
25
Methylene Chloride
10/2/00
25
125
BQL
1,1,2,2-Tetrachloroethane
10/2/00
25
25
BQL
Tetrachloroethene
10/2/00
25
25
BQL
1,1,1-Trichloroethane
10/2100
25
25
BQL
1,1,2-Trichloroethane
10/2/00
25
25
BQL
Trichloroethene
10/2/00
25
25
BQL
Trichlorofluoromethane
10/2/00
25
25
610
Vinyl Chloride
10/2/00
25
25
BQL
BQL
Surrogate Spike Recoveries
Spike P�
Spike
Percent
Added
Result
Recovered
_ 1,4-Dichlorobutane
40
41
102
ii
Comments:
— All values corrected for dilution.
Flags:
BQL = Below quantitation limit.
Reviewed By:
Page 1
of 1
r;
�` ! N.C. Certification #481
S.C. Certification #99029

PARADIGM ANALYTICAL LABORATORIES, INC.
Results
for Volatiles
by
GC 601
Client Sample ID: MW-3
Analyzed By:
RNP
Client Project ID: Toastmaster
Date Collected:
09/26/00
-- Lab Sample ID: 96159
Date Received:
09/27/00
Lab Project ID: G216-82
Matrix:
Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
10/5/00
2
2
BQL
Bromoform
10/5/00
2
4
BQL
Bromomethane
10/5/00
2
4
BQL
Carbon tetrachloride
10/5/00
2
2
BQL
l Chlorobenzene
10/5/00
2
2
BQL
Chloroethane
10/5/00
2
2
BQL
Chloroform
10/5/00
2
2
BQL
Chloromethane
10/5/00
2
2
BQL
Dibromochloromethane
10/5/00
2
2
1,2-Dibromoethane (EDB)
10/5/00
2
2
BQL
1,2-Dichlorobenzene
10/5/00
2
2
BQL
1,3-Dichlorobenzene
10/5/00
2
2
BQL
1,4-Dichlorobenzene
10/5/00
2
2
BQL
1,1-Dichloroethane
10/5/00
2
2
BQL
1,2-Dichloroethane
10/5/00
2
2
BQL
1,1-Dichloroethene
10/5/00
2
2
BQL
cis-1,2-Dichloroethene
10/5/00
2
2
BQL
- trans-1,2-Dichloroethene
10/5/00
2
2
4
1,2-Dichloropropane
10/5/00
2
2
BQL
cis-1,3-Dichloropropene
10/5/00
2
2
BQL
trans-1,3-Dichloropropene
10/5/00
2
2
BQL
Methylene Chloride
10/5/00
2
10
BQL
1,1,2,2-Tetrachloroethane
10/5/00
2
BQL
Tetrachloroethene
10/5/00
2
2
2
BQL
1,1,1-Trichloroethane
10/5/00
2
2
BQL
1,1,2-Trichloroethane
10/5/00
2
2
BQL
' Trichloroethene
10/5/00
2
2
BQL
Trichlorofluoromethane
10/5/00
2
2
29
Vinyl Chloride
10/5/00
2
2
BQL
BQL
- Surrogate Spike Recoveries
Spike
Spike
Percent
•
Added
Result
Recovered
1,4-Dichlorobutane
40
39
97
Comments:
1 All values corrected for dilution.
Flags:
BQL = Below quantitation limit.
Page 1 of 1 Reviewed By: —
�?
L_i N.C. Certification #481 S.C. Certification #99029

PARADIGM ANALYTICAL LABORATORIES, INC.
-
Results for Volatiles
by GC 601
f'
Client Sample ID: MW-4
Analyzed By:
RNP
Client Project ID: Toastmaster
Date Collected:
09/26/00
Lab Sample ID: 96160
Date Received:
09/27/00
Lab Project ID: G216-82
Matrix:
Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
I -I
Bromodichloromethane
10/2/00
50
50
BQL
Bromoform
10l2/00
50
100
BQL
Bromomethane
10/2/00
50
100
BQL
ri
Carbon tetrachloride
10/2/00
50
50
BQL
Chlorobenzene
10/2/00
50
50
BQL
Chloroethane
10/2/00
50
50
BQL
Chloroform
10/2/00
50
50
BQL
Chloromethane
10/2/00
50
50
BQL
Dibromochloromethane
10/2/00
50
50
BQL
1,2-Dibromoethane (EDB)
10/2/00
50
50
BQL
1,2-Dichlorobenzene
10/2/00
50
50
BQL
1,3-Dichlorobenzene
10l2l00
50
50
BQL
1,4-Dichlorobenzene
10/2/00
50
50
BQL
r
1,1-Dichloroethane
10/2/00
50
50
BQL
1,2-Dichloroethane
10/2/00
50
50
BQL
1,1-Dichloroethene
10/2100
50
50
BQL
`
cis-1,2-Dichloroethene
10/2/00
50
50
trans-1,2-Dichloroethene
10/2/00
50
50
260
BQL
1,2-Dichloropropane
10/2/00
50
50
BQL
cis-1,3-Dichloropropene
10/2/00
50
50
BQL
trans-1,3-Dichloropropene
10/2/00
50
50
BQL
Methylene Chloride
10/2/00
50
250
gQL
- -
1,1,2,2-Tetrachloroethane
10/2/00
50
50
BQL
Tetrachloroethene
10/2100
50
50
gQL
1,1,1-Trichloroethane
10/2/00
50
50
BQL
-.
1,1,2-Trichloroethane
10/2/00
50
50
BQL
Trichloroethene
10/2/00
50
50
1000
Trichlorofluoromethane
10/2100
50
50
BQL
_
Vinyl Chloride
10/2/00
50
50
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
—
Added
Result
Recovered
1,4-Dichlorobutane
40
41
103
Comments:
All values corrected for dilution.
I Flags:
r,
BQL = Below quantitation limit.
i
Reviewed By:
Page 1 of 1
CN.C.
Certification #481
S.C. Certification
#99029

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Client Sample ID: MW-5
Analyzed By:
RNP
Client Project ID: Toastmaster
Date Collected:
09/26/00
Lab Sample ID: 96161
Date Received:
09/27/00
Lab Project ID: G216-82
Matrix:
Water
j l Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
i Bromodichloromethane
10/2/00
10
10
BQL
_ Bromoform
10/2/00
10
20
BQL
Bromomethane
10/2/00
10
20
BQL
7 Carbon tetrachloride
10/2/00
10
10
BQL
Chlorobenzene
10/2/00
10
10
BQL
Chloroethane
1012/00
10
10
BQL
i Chloroform
10/2/00
10
10
BQL
Chloromethane
10/2/00
10
10
BQL
Dibromochloromethane
10/2/00
10
10
BQL
_ 1,2-Dibromoethane (EDB)
1012100
10
10
BQL
+ 1,2-Dichlorobenzene
10/2/00
10
10
BQL
1,3-Dichlorobenzene
10/2100
10
10
BQL
1,4-Dichlorobenzene
10/2/00
10
10
BQL
M-Dichloroethane
10/2/00
10
10
BQL
1,2-Dichloroethane
10/2/00
10
10
BQL
1,1-Dichloroethene
�I
1012100
10
10
BQL
cis-1,2-Dichloroethene
10/2/00
10
10
BQL
trans-1,2-Dichloroethene
10/2/00
10
10
BQL
1,2-Dichloropropane
10/2/00
10
10
BQL
cis-1,3-Dichloropropene
10/2/00
10
10
BQL
trans-1,3-Dichloropropene
10/2/00
10
10
BQL
Methylene Chloride
10/2/00
10
50
BQL
- - 1,1,2,2-Tetrachloroethane
10/2/00
10
10
Tetrachloroethene
10/2l00
10
10
BQL
1,1,1-Trichloroethane
10/2l00
10
10
BQL
_ 1,1,2-Trichloroethane
10/2/00
10
10
BQL
Trichloroethene
10/2/00
10
10
BQL
TrichloroFluoromethane
10/2l00
10
10
200
Vinyl Chloride
10/2/00
10
10
BQL
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
_ 1,4-Dichlorobutane
40
39
98
Comments:
All values corrected for dilution.
e_ Flags:
BQL = Below quantitation limit.
Reviewed By:
Page 1 of 1
N.C. Certification #481
S.C. Certification
#99029

PARADIGM ANALYTICAL LABORATORIES, INC.
-
Results for Volatiles
by GC 601
Client Sample ID: MW-6
Analyzed By:
RNP
Client Project ID: Toastmaster
Date Collected:
09/26/00
Lab Sample ID: 96162
Date Received:
09/27/00
Lab Project ID: G216-82
Matrix:
Water
Compound
Date
Quantitation
Result
-
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
10/2100
40
40
BQL
Bromoform
10/2/00
40
80
BQL
Bromomethane
10/2/00
40
80
BQL
Carbon tetrachloride
10/2/00
40
40
BQL
Chlorobenzene
10/2/00
40
40
BQL
Chloroethane
10/2/00
40
40
BQL
Chloroform
10/2/00
40
40
BQL
Chloromethane
10/2/00
40
40
BQL
-
Dibromochloromethane
10/2/00
40
40
BQL
1,2-Dibromoethane (EDB)
1012100
40
40
?
1,2-Dichlorobenzene
10/2/00
40
40
BQL
l
1,3-Dichlorobenzene
10/2/00
40
40
BQL
BQL
1,4-Dichlorobenzene
10/2/00
40
40
BQL
1,1-Dichloroethane
10/2/00
40
40
BQL
1,2-Dichloroethane
10/2/00
40
40
BQL
1,1-Dichloroethene
10/2/00
40
40
BQL
cis-1,2-Dichloroethene
10/2/00
40
40
trans-1,2-Dichloroethene
10/2/00
40
40
78
1,2-Dichloro ro ane
P P
10/2/00
40
40
BQL
cis-1,3-Dichloropropene
10/2/00
40
40
BQL
trans-1,3-Dichloropropene
10/2/00
40
40
BQL
Methylene Chloride
1012100
40
200
BQL
1,1,2,2-Tetrachloroethane
10/2/00
40
40
BQL
Tetrachloroethene
10/2/00
40
40
BQL
1,1,1-Trichloroethane
10/2/00
40
40
BQL
"
1,1,2-Trichloroethane
10/2/00
40
40
BQL
Trichloroethene
10/2/00
40
40
BQL
Trichlorofluoromethane
10/2/00
40
40
720
Vinyl Chloride
10/2/00
40
40
BQL
BQL
__
Surrogate Spike Recoveries
Spike P
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
I
40
101
Comments:
All values corrected for dilution.
li
Flags:
BQL = Below quantitation limit.
Reviewed
By:
Page 1 of 1
r
14
N.C. Certification
#481
S.C. Certification #99029

--
PARADIGM ANALYTICAL LABORATORIES, INC.
_
Results for Volatiles
by GC 601
Client Sample ID: MW-7
Analyzed By: RNP
Client Project ID: Toastmaster
Date Collected: 09/26/00
Lab Sample ID: 96163
Date Received: 09/27/00
Lab Project ID: G216-82
Matrix: Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
- t
Bromodichloromethane
10/2/00
250
250
BQL
Bromoform
10/2100
250
500
BQL
Bromomethane
10/2/00
250
500
BQL
Carbon tetrachloride
10/2/00
250
250
BQL
Chlorobenzene
10/2/00
250
250
BQL
Chloroethane
10/2/00
250
250
BQL
i
Chloroform
10/2/00
250
250
BQL
Chloromethane
10/2100
250
250
BQL
--
Dibromochloromethane
10/2/00
250
250
BQL
1,2-Dibromoethane (EDB)
10/2/00
250
250
BQL
r
I_
1,2-Dichlorobenzene
10/2/00
250
250
BQL
1,3-Dichlorobenzene
10/2/00
250
250
BQL
1,4-Dichlorobenzene
10/2/00
250
250
BQL
1,1-Dichloroethane
10/2/00
250
250
BQL
1_
1,2-Dichloroethane
10/2/00
250
280
BQL
^;
1,1-Dichloroethene
10/2/00
250
250
BQL
cis-1,2-Dichloroethene
10/2/00
250
250
trans-1,2-Dichloroethene
10/2/00
250
250
BQL
1,2-Dichloropropane
10/2/00
250
250
BQL
-
cis-1,3-Dichloropropene
10/2/00
250
250
BQL
'
trans-1,3-Dichloropropene
10/2/00
250
250
BQL
Methylene Chloride
10/2/00
250
1250
BQL
_
1,1,2,2-Tetrachloroethane
10/2/00
250
250
BQL
Tetrachloroethene
10/2/00
250
250
BQL
1,1,1-Trichloroethane
10/2/00
250
250
520
1,1,2-Trichloroethane
10/2/00
250
250
BQL
Trichloroethene
10/2/00
250
250
BQL
Trichlorofluoromethane
10/2/00
250
250
4100
Vinyl Chloride
10/2/00
250
250
BQL
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
41
104
Comments:
All values corrected for dilution.
Flags:
BQL =Below quantitation limit.
l
Reviewed By:
Page 1
of 1
N.C. Certification
#481
S.C. Certification
#99029

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Client Sample ID: MW-9
Client Project ID: Toastmaster
Lab Sample ID: 96164
Lab Project ID: G216-82
Analyzed By: RNP
Date Collected: 09/26/00
Date Received: 09/27/00
Matrix: Water
Compound
Date
Quantitation
Result
Analyzed
Dilution Limit (ug/L)
(ug/L)
Bromodichloromethane
10/2/00
1
1
BQL
Bromoform
10/2/00
1
2
BQL
Bromomethane
10/2/00
1
2
BQL
r"
Carbon tetrachloride
10/2/00
1
1
BQL
Chlorobenzene
10/2/00
1
1
BQL
Chloroethane
10/2100
1
1
BQL
Chloroform
10/2/00
1
1
BQL
Chloromethane
10/2/00
1
1
BQL
Dibromochloromethane
10/2/00
1
1
1,2-Dibromoethane (EDB)
10/2/00
1
1
BQL
1,2-Dichlorobenzene
10/2/00
1
1
BQL
1,3-Dichlorobenzene
10/2/00
1
1
BQL
1,4-Dichlorobenzene
10/2/00
1
1
BQL
1,1-Dichloroethane
10/2/00
1
1
BQL
1,2-Dichloroethane
10/2/00
1
BQL
1,1-Dichloroethene
10/2/00
1
1
1
BQL
(�
cis-1,2-Dichloroethene
10/2/00
1
BQL
trans-1,2-Dichloroethene
10/2/00
1
1
1
f
1,2-Dichloropropane
10/2/00
1
1
BQL
cis-1,3-Dichloropropene
10/2/00
1
BQL
trans-1,3-Dichloropropene
10/2100
1
1
BQL
Methylene Chloride
10/2/00
1
1
BQL
—,
1,1,2,2-Tetrachlorcethane
10/2/00
1
5
BQL
Tetrachloroethene
10/2/00
1
1
BQL
1,1,1-Trichloroethane
10/2/00
1
1
BQL
-.
1,1,2-Trichloroethane
10/2/00
1
1
BQL
Trichloroethene
10/2/00
1
1
BQL
Trichlorofluoromethane
10/2/00
1
1
25
Vinyl Chloride
10/2/00
1
1
BQL
1
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
r—
Added
Result
Recovered
1,4-Dichlorobutane
40
41
102
Comments:
All values corrected for dilution.
I` Flags:
r
BQL = Below quantitation limit.
L
Reviewed By:
Page 1
of 1
N.C. Certification
#481
S.C.
Certification #99029

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Client Sample ID: MW-10
Analyzed By: RNP
Client Project ID: Toastmaster
Date Collected: 09/26/00
_
Lab Sample ID: 96165
Date Received: 09/27/00
Lab Project ID: G216-82
Matrix: Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
�—
Bromodichloromethane
10/2/00
100
100
BQL
Bromoform
10/2100
100
200
BQL
Bromomethane
1012/00
100
200
BQL
Carbon tetrachloride
10/2/00
100
100
BQL
Chlorobenzene
10/2/00
100
100
BQL
Chloroethane
10/2/00
100
100
BQL
Chloroform
10/2/00
100
100
BQL
`
Chloromethane
10/2/00
100
100
BQL
Dibromochloromethane
10/2/00
100
100
BQL
1,2-Dibromoethane (EDB)
10/2/00
100
100
BQL
1,2-Dichlorobenzene
10/2/00
100
100
BQL
1,3-Dichlorobenzene
10/2/00
100
100
BQL
(
1,4-Dichlorobenzene
1,1-Dichloroethane
10/2/00
100
100
BQL
10/2/00
100
100
BQL
1t.
1,2-Dichloroethane
10/2/00
100
100
BQL
1,1-Dichloroethene
10/2/00
100
100
BQL
cis-1,2-Dichloroethene
10/2/00
100
100
490
trans-1,2-Dichloroethene
10/2100
100
100
BQL
1,2-Dichloropropane
10/2/00
100
100
BQL
cis-1,3-Dichloropropene
10/2/00
100
100
BQL
trans-1,3-Dichloropropene
10/2/00
100
100
BQL
Methylene Chloride
1012100
100
500
BQL
1,1,2,2-Tetrachloroethane
10/2/00
100
100
BQL
Tetrachloroethene
10/2/00
100
100
BQL
1,1,1-Trichioroethane
10/2/00
100
100
BQL
1,1,2-Trichloroethane
10/2/00
100
100
BQL
Trichloroethene
10/2/00
100
100
1700
--
Trichlorofluoromethane
10/2/00
100
100
BQL
Vinyl Chloride
10/2/00
100
100
J
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
40
41
r1,4-Dichlorobutane
104
Comments:
All values corrected for dilution.
Flags:
_
BQL = Below quantitation limit.
�J
Reviewed By:
Page 1 of 1
��
N.C. Certification #481
S.C. Certification
#99029

i
PARADIGM ANALYTICAL LABORATORIES, INC.
—
Results for Volatiles
by GC 601
I
Client Sample ID: MW-11
Analyzed By: RNP
Client Project ID: Toastmaster
Date Collected:
09/26/00
Lab Sample ID: 96166
Date Received:
09/27/00
Lab Project ID: G216-82
Matrix:
Water
{
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
10/3/00
10
10
BQL
Bromoform
10/3l00
10
20
BQL
Bromomethane
10l3/00
10
20
BQL
Carbon tetrachloride
10/3/00
10
10
BQL
Chlorobenzene
10/3/00
10
10
BQL
Chloroethane
10/3/00
10
10
BQL
Chloroform
10/3/00
10
10
BQL
Chloromethane
10/3/00
10
10
BQL
Dibromochloromethane
10/3/00
10
10
1,2-Dibromoethane (EDB)
10/3/00
10
10
BQL
i
1,2-Dichlorobenzene
10l3/00
10
10
BQL
-'
1,3-Dichlorobenzene
10/3/00
10
10
BQL
1,4-Dichlorobenzene
10/3100
10
10
BQL
F1,1-Dichloroethane
10/3/00
10
10
BQL
—
1,2-Dichloroethane
10/3/00
10
10
BQL
1,1-Dichloroethene
10/3l00
10
10
BQL
cis-1,2-Dichloroethene
10/3/00
10
BQL
trans-1,2-Dichloroethene
10/3/00
10
10
10
BQL
1,2-Dichloro ro ane
P P
10/3100
10
10
BQL
cis-1,3-Dichloropropene
10/3/00
10
10
BQL
trans-1,3-Dichloropropene
10/3/00
10
10
BQL
Methylene Chloride
10/3/00
10
50
BQL
1,1,2,2-Tetrachloroethane
10/3/00
10
BQL
Tetrachloroethene
10/3/00
10
10
BQL
1,1,1-Trichooroethane
10/3/00
10
10
BQL
1,1,2-Trichooroethane
10l3/00
10
10
BQL
Trichloroethene
10/3/00
10
10
BQL
-
TrichloroFluoromethane
10/3l00
10
10
240
Vinyl Chloride
10/3/00
10
10
BQL
110
BQL
-
Surrogate Spike Recoveries
Spike P
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
40
101
Comments:
All values corrected for dilution.
L` Flags:
FBQL =Below quantitation limit. I
Page 1 of 1
Reviewed By: Mom,
�! N.C. Certification #481 S.C. Certification #99029

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
-'
by GC 601
�
Client Sample ID: MW-12
P
Analyzed By: RNP
Client Project ID: Toastmaster
Date Collected: 09/26/00
Lab Sample ID: 96167
Date Received: 09/27/00
Lab Project ID: G216-82
Matrix: Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
(
Bromodichloromethane
10/3/00
1
1
BQL
Bromoform
10/3/00
1
2
BQL
Bromomethane
10/3/00
1
2
BQL
Carbon tetrachloride
10/3/00
1
1
BQL
Chlorobenzene
10/3/00
1
1
BQL
Chloroethane
10/3/00
1
1
BQL
Chloroform
10/3/00
1
1
BQL
Chloromethane
10/3/00
1
1
BQL
-!
Dibromochloromethane
10/3/00
1
1
BQL
1,2-Dibromoethane (EDB)
10/3/00
1
1
BQL
1,2-Dichlorobenzene
10/3/00
1
1
BQL
1,3-Dichlorobenzene
10/3/00
1
1
BQL
�
1,4-Dichlorobenzene
10/3/00
1
1
BQL
11-Dic hloroethane
10/3/00
1
1
BQL
1,2-Dichloroethane
10/3/00
1
1
BQL
1,1-Dichloroethene
10/3/00
1
1
BQL
rl
cis-1,2-Dichloroethene
10/3/00
1
1
BQL
I I
trans-1,2-Dichloroethene
10/3/00
1
1
BQL
1,2-Dichloropropane
10/3/00
1
1
BQL
--
cis-1,3-Dichloropropene
10/3/00
1
1
BQL
trans-1,3-Dichloropropene
10/3/00
1
1
BQL
-
Methylene Chloride
10/3/00
1
5
BQL
1,1,2,2-Tetrachloroethane
10/3/00
1
1
s
Tetrachloroethene
10/3/00
1
1
BQL
1,1,1-Trichloroethane
10/3/00
1
1
BQL
_
1,1,2-Trichloroethane
10/3/00
1
1
BQL
Trichloroethene
10/3/00
1
1
BQL
Trichlorofluoromethane
10/3/00
1
1
9
Vinyl Chloride
10/3/00
1
1
BQL
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
41
101
Comments:
r-
All values corrected for dilution.
Flags:
BQL = Below quantitation limit.
Reviewed
By:
Page 1 of 1
i
N.C. Certification #481
S.C. Certification
#99029

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Client Sample ID: MW-13 Analyzed By: RNP
Client Project ID: Toastmaster Date Collected: 09/26/00
Lab Sample ID: 96168 Date Received: 09/27/00
Lab Project ID: G216-82 Matrix: Water
Compound P
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
10/3/00
5
5
BQL
t_J
Bromoform
10/3/00
5
10
BQL
-.
Bromomethane
10/3/00
5
10
BQL
Carbon tetrachloride
10/3/00
5
5
BQL
Chlorobenzene
10/3/00
5
5
BQL
Chloroethane
10/3/00
5
5
BQL
Chloroform
10/3/00
5
5
BQL
Chloromethane
10/3/00
5
5
BQL
Dibromochloromethane
10/3/00
5
5
BQL
1,2-Dibromoethane (EDB)
10/3/00
5
5
BQL
1,2-Dichlorobenzene
10/3/00
5
5
BQL
1,3-Dichlorobenzene
10/3/00
5
5
BQL
1,4-Dichlorobenzene
10/3/00
5
5
BQL
M-Dichloroethane
10/3/00
5
5
BQL
1,2-Dichloroethane
10/3/00
5
5
BQL
M-Dichloroethene
10/3/00
5
5
BQL
cis-1,2-Dichloroethene
10/3/00
5
5
trans-1,2-Dichloroethene
10/3/00
5
5
8
1,2-Dichloropropane
10/3/00
5
5
BQL
cis-1,3-Dichloropropene
10/3/00
5
5
BQL
j,
trans-1,3-Dichloropropene
10/3/00
5
5
BQL
Methylene Chloride
10/3/00
5
25
BQL
—
1,1,2,2-Tetrachloroethane
10/3/00
5
5
BQL
Tetrachloroethene
10/3/00
5
5
BQL
1,1,1-Trichloroethane
10/3/00
5
5
BQL
-.
1,1,2-Trichloroethane
10/3/00
5
5
BQL
J
Trichloroethene
10/3/00
5
5
BQL
Trichlorofluoromethane
10/3/00
5
5
170
_
Vinyl Chloride
10/3/00
5
5
BQL
BQL
--
Surrogate Spike Recoveries
Spike
Spike P�
Percent
- ,
Added
Result
Recovered
1,4-Dichlorobutane
40
41
103
Comments:
r I
LI
- Flags:
All values corrected for dilution.
BQL = Below quantitation limit.
Reviewed By:
Page 1 of 1
�����
N.C. Certification
#481
S.C. Certification #99029

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Client Sample ID: MW-14
p Analyzed By: RNP
Client Project ID: Toastmaster Date Collected: 09/26/00
Lab Sample ID: 96169 Date Received: 09/27/00
d,
Lab Project ID: G216-82 Matrix: Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
-
Bromodichloromethane
10/3100
4
4
BQL
Bromoform
10/3/00
4
8
BQL
Bromomethane
10/3/00
4
8
BQL
1r l
Carbon tetrachloride
10/3/00
4
4
BQL
Chlorobenzene
10/3/00
4
4
BQL
Chloroethane
10/3/00
4
4
BQL
Chloroform
10/3/00
4
4
BQL
Chloromethane
10/3100
4
4
BQL
Dibromochloromethane
10/3/00
4
4
BQL
1,2-Dibromoethane (EDB)
1013/00
4
4
BQL
1,2-Dichlorobenzene
10/3/00
4
4
BQL
-
1,3-Dichlorobenzene
10/3/00
4
4
BQL
1,4-Dichlorobenzene
10/3/00
4
4
BQL
1,1-Dichloroethane
10/3/00
4
4
BQL
U
1,2-Dichloroethane
1013/00
4
4
BQL
1,1-Dichloroethene
10/3/00
4
4
BQL
cis-1,2-Dichloroethene
10/3/00
4
4
trans-1,2-Dichloroethene
10/3/00
4
4
6
1,2-Dichloropropane
10/3/00
4
4
BQL
cis-1,3-Dichloropropene
10/3/00
4
4
BQL
L
trans-1,3-Dichloropropene
10/3/00
4
4
BQL
Methylene Chloride
10/3/00
4
20
BQL
—
1,1,2,2-Tetrachloroethane
10/3/00
4
4
BQL
Tetrachloroethene
10/3/00
4
4
BQL
1,1,1-Trichloroethane
10/3/00
4
4
BQL
_
1,1,2-Trichloroethane
10/3/00
4
4
BQL
Trichloroethene
10/3/00
4
4
BQL
Trichlorofluoromethane
10/3/00
4
4
82
Vinyl Chloride
10/3/00
4
4
BQL
BQL
_
Surrogate Spike Recoveries
Spike
Spike P
Percent
--.
Added
Result
Recovered
1,4-Dichlorobutane
40
43
108
Comments:
All values corrected for dilution.
L� Flags:
BQL = Below quantitation limit.
F1
_
Reviewed By:
Page 1
of 1
N.C. Certification
#481
S.C. Certification #99029

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Client Sample ID: Influent
Analyzed By:
RNP
Client Project ID: Toastmaster
Date Collected:
09/26/00
Lab Sample ID: 96173
Date Received:
09/27/00
.,
Lab Project ID: G216-82
I
Matrix:
Water
(
Compound
Date
Quantitation
Result
--
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
10/3/00
25
25
BQL
t
Bromoform
10/3/00
25
50
BQL
Bromomethane
10/3/00
25
50
BQL
Carbon tetrachloride
10/3/00
25
25
BQL
Chlorobenzene
10/3/00
25
25
BQL
Chloroethane
10/3/00
25
25
BQL
Chloroform
10/3/00
25
25
BQL
`
Chloromethane
10/3/00
25
25
BQL
L
Dibromochloromethane
10/3/00
25
25
BQL
1,2-Dibromoethane (EDB)
10/3/00
25
25
BQL
1,2-Dichlorobenzene
10/3/00
25
25
BQL
Lk
1,3-Dichlorobenzene
10/3/00
25
25
BQL
1,4-Dichlorobenzene
10/3/00
25
25
BQL
(j
(_
M-Dichloroethane
10/3/00
25
25
BQL
!
1,2-Dichloroethane
10/3/00
25
25
BQL
1,1-Dichloroethene
10/3/00
25
25
BQL
j
cis-1,2-Dichloroethene
10/3/00
25
25
BQL
1
trans-1,2-Dichloroethene
10/3/00
25
25
BQL
1,2-Dichloropropane
10/3/00
25
25
BQL
cis-1,3-Dichloropropene
10/3/00
25
25
BQL
trans-1,3-Dichloropropene
10/3/00
25
25
BQL
Methylene Chloride
10/3/00
25
125
BQL
1,1,2,2-Tetrachloroethane
10/3/00
25
25
BQL
Tetrachloroethene
10/3/00
25
25
BQL
1.1,1-Trichloroethane
10/3/00
25
25
BQL
1,1,2-Trichloroethane
10/3100
25
25
BQL
jr
Trichloroethene
10/3/00
25
25
630
--
Trichlorofluoromethane
10/3/00
25
25
BQL
Vinyl Chloride
10/3/00
25
125
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
i
Added
Result
Recovered
1,4-Dichlorobutane
40
41
102
i
Comments:
All values corrected for dilution.
Flags:
t I
BQL = Below quantitation limit.
{_
Reviewed By:
Page 1 of 1
1
i
N.C. Certification #481
S.C. Certification
#99029

PARADIGM ANALYTICAL LABORATORIES, INC.
Results
for Volatiles
by
GC 601
•
Client Sample ID: Effluent Trench
Analyzed By:
RNP
`
Client Project ID: Toastmaster
Date Collected:
09/26/00
Lab Sample ID: 96174
Date Received:
09/27/00
Lab Project ID: G216-82
Matrix:
Water
,-I
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
10/3/00
1
1
BQL
Bromoform
10/3/00
1
2
BQL
Bromomethane
10/3/00
1
2
BQL
Carbon tetrachloride
1013/00
1
1
BQL
Chlorobenzene
10/3100
1
1
BQL
Chloroethane
10/3/00
1
1
BQL
Chloroform
10/3/00
1
1
BQL
Chloromethane
10/3/00
1
1
BQL
—'
Dibromochloromethane
10/3/00
1
1
BQL
1,2-Dibromoethane (EDB)
10/3/00
1
1
1,2-Dichlorobenzene
10/3/00
1
1
BQL
1,3-Dichlorobenzene
10/3/00
1
1
BQL
1,4-Dichlorobenzene
10/3/00
1
1
BQL
1,1-Dichloroethane
10/3/00
1
1
BQL
1,2-Dichloroethane
10/3100
1
1
BQL
1,1-Dichloroethene
10/3/00
1
1
BQL
cis-1,2-Dichloroethene
10/3/00
1
1
BQL
trans-1,2-Dichloroethene
10/3/00
1
1
BQL
1,2-Dichloropropane
10/3/00
1
1
BQL
cis-1,3-Dichloropropene
10/3/00
1
1
BQL
trans-1,3-Dichloropropene
10/3/00
1
1
BQL
Methylene Chloride
10/3/00
1
BQL
1,1,2,2-Tetrachloroethane
10/3/00
1
5
1
BQL
Tetrachloroethene
10/3/00
1
1
BQL
1,1,1-Trichloroethane
10/3100
1
1
BQL
1,1,2-Trichloroethane
10/3/00
1
BQL
Trichloroethene
10/3/00
1
1
BQL
—
Trichlorofluoromethane
10/3/00
1
1
BQL
Vinyl Chloride
10/3/00
1
1
1
BQL
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
40
100
Comments:
( Ail values corrected for dilution.
Flags:
f BQL = Below quantitation limit.
I Page 1 of 1 Reviewed By:
1 N.C. Certification #481 S.C. Certification #99029

PARADIGM ANALYTICAL LABORATORIES, INC.
-J
Results
for Volatiles
by GC 601
1 yl
Client Sample ID: Cooling Tower
Analyzed By: RNP
Client Project ID: Toastmaster
Date Collected: 09/26/00
-;
Lab Sample ID: 96175
Date Received: 09/27/00
Lab Project ID: G216-82
Matrix: Water
r-
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
+�+
Bromodichloromethane
10/3/00
1
1
BQL
I_
Bromoform
10/3/00
1
2
BQL
Bromomethane
10/3/00
1
2
BQL
Carbon tetrachloride
Chlorobenzene
10/3100
1
1
BQL
10/3/00
1
1
BQL
Chloroethane
10/3/00
1
1
BQL
Chloroform
10/3/00
1
1
BQL
Chloromethane
10/3/00
1
1
BQL
Dibromochloromethane
10/3/00
1
1
BQL
1,2-Dibromoethane (EDB)
10/3/00
1
1
'
1,2-Dichlorobenzene
10/3/00
1
1
BQL
1,3-Dichlorobenzene
10/3/00
1
1
BQL
_
1,4-Dichlorobenzene
10/3/00
1
1
BQL
r
1,1-Dichloroethane
10/3/00
1
1
BQL
1,2-Dichloroethane
10/3/00
1
1
BQL
1,1-Dichloroethene
10/3/00
1
1
BQL
cis-1,2-Dichloroethene
10/3/00
1
1
BQL
trans-1,2-Dichloroethene
10/3/00
1
1
3
1,2-Dichloropropane
10/3/00
1
1
BQL
cis-1,3-Dichloropropene
10/3/00
1
1
BQL
trans-1,3-Dichloropropene
10/3/00
1
1
BQL
Methylene Chloride
10/3/00
1
5
BQL
-
1,1,2,2-Tetrachloroethane
10/3/00
1
1
BQL
Tetrachloroethene
10/3/00
1
1
BQL
'
1,1,1-Trichloroethane
10/3/00
1
1
BQL
-,
1,1,2-Trichloroethane
10/3/00
1
1
BQL
Trichloroethene
10/3/00
1
1
BQL
Trichlorofluoromethane
10/3/00
1
1
BQL
Vinyl Chloride
10/3/00
1
1
BQL
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
40
99
Comments:
n
All values corrected for dilution.
—
Flags:
F
BQL = Below quantitation limit.
'
Reviewed By:
Page 1 of 1
_If
N.C. Certification
#481
S.C. Certification #99029

PARADIGM ANALYTICAL LABORATORIES, INC.
Results
for Volatiles
by
GC 601
Client Sample ID: RW-1
Analyzed By:
RNP
Client Project ID: Toastmaster
Date Collected:
09/26/00
Lab Sample ID: 96170
Date Received:
09/27/00
Lab Project ID: G216-82
Matrix:
Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
(J
Bromodichloromethane
10/3/00
50
50
BQL
Bromoform
10/3/00
50
100
BQL
Bromomethane
10/3/00
50
100
BQL
Carbon tetrachloride
10/3/00
50
50
BQL
L)
Chlorobenzene
10/3/00
50
50
BQL
Chloroethane
10/3100
50
50
BQL
r
Chloroform
10/3/00
50
50
BQL
Chloromethane
10/3100
50
50
BQL
Dibromochioromethane
10/3/00
50
50
BQL
1,2-Dibromoethane (EDB)
10/3/00
50
50
BQL
L'
1,2-Dichlorobenzene
10/3/00
50
50
BQL
1,3-Dichlorobenzene
10/3/00
50
50
BQL
1,4-Dichlorobenzene
10/3/00
50
50
BQL
1,1-Dichloroethane
10/3/00
50
50
BQL
1,2-Dichloroethane
10/3/00
50
50
BQL
1,1-Dichloroethene
10/3/00
50
50
BQL
cis-1,2-Dichloroethene
10/3/00
50
50
BQL
trans-1,2-Dichloroethene
10/3/00
50
50
1,2-Dichloropropane
10/3/00
50
50
BQL
cis-1,3-Dichloropropene
10/3/00
50
50
BQL
trans-1,3-Dichloropropene
10/3/00
50
50
BQL
Methylene Chloride
10/3/00
50
280
BQL
-
1,1,2,2-Tetrachloroethane
1013/00
50
50
BQL
Tetrachloroethene
10/3/00
50
50
BQL
1,1,1-Trichloroethane
10/3/00
50
50
BQL
_
1,1,2-Trichloroethane
10/3/00
50
50
BQL
Trichloroethene
10/3/00
50
50
BQL
Trichlorofluoromethane
10/3/00
50
50
900
Vinyl Chloride
10/3/OD
50
50
BQL
i
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
--,
Added
Result
Recovered
1,4-Dichlorobutane
40
41
103
Comments:
LFlags: All values corrected for dilution.
BQL = Below quantitation limit.
I I
Page 1 of 1
Reviewed By: M ",
N.C. Certification #481 S.C. Certification #99029

1, -4 PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Client Sample ID: RW-2 Analyzed By: RNP
Client Project ID: Toastmaster Date Collected: 09/26/00
Lab Sample ID: 96171 Date Received: 09/27/00
Lab Project ID: G216-82 Matrix: Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
10/3/00
50
50
BQL
L,
Bromoform
10/3/00
50
100
BQL
Bromomethane
10/3/00
50
100
BQL
Carbon tetrachloride
10/3/00
50
50
BQL
Chlorobenzene
10/3100
50
50
BQL
J
Chloroethane
10/3/00
50
50
BQL
Chloroform
10/3/00
50
50
BQL
L'
Chloromethane
10/3/00
50
50
BQL
Dibromochloromethane
10/3/00
50
50
BQL
1,2-Dibromoethane (EDB)
10/3/00
50
50
BQL
L
1,2-Dichlorobenzene
10/3/00
50
50
BQL
1,3-Dichlorobenzene
10/3/00
50
50
BQL
1,4-Dichlorobenzene
10/3/00
50
50
BQL
1,1-Dichloroethane
10/3/00
50
50
BQL
1,2-Dichloroethane
10/3/00
50
50
BQL
1,1-Dichloroethene
10/3/00
50
50
BQL
cis-1,2-Dichloroethene
10/3/00
50
50
BQL
trans-1,2-Dichloroethene
10/3/00
50
50
BQL
1,2-Dichloropropane
10/3/00
50
50
BQL
-
cis-1,3-Dichloropropene
10/3/00
50
50
BQL
J
trans-1,3-Dichloropropene
10/3/00
50
50
BQL
Methylene Chloride
10/3/00
50
250
BQL
1,1,2,2-Tetrachloroethane
10/3/00
50
50
Tetrachloroethene
10/3/00
50
50
BQL
--
1,1,1-Trichloroethane
10/3/00
50
50
BQL
__.
1,1,2-Trichloroethane
10/3/00
50
50
BQL
Trichloroethene
10/3/00
50
50
BQL
Trichlorofluoromethane
10/3/00
50
50
1000
—•
Vinyl Chloride
10/3/00
50
50
BQL
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
39
98
— Comments:
All values corrected for dilution.
jl.
Flags:
BQL = Below quantitation limit.
Reviewed By:
Page 1 of 1
N.C. Certification #481
S.C. Certification #99029

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Client Sample ID: RW-3 Analyzed By: RNP
Client Project ID: Toastmaster Date Collected: 09/26/00
Lab Sample ID: 96172 Date Received: 09/27/00
Lab Project ID: G216-82 Matrix: Water
Compound
Date
Quantitation
Result
{—'
Analyzed
Dilution
Limit (ug/L)
(ug/L)
i
Bromodichloromethane
10/3/00
10
10
BQL
Bromoform
10/3/00
10
20
BQL
Bromomethane
10/3/00
10
20
BQL
Carbon tetrachloride
10/3/00
10
10
BQL
I�
Chlorobenzene
10/3/00
10
10
BQL
Chloroethane
10/3/00
10
10
BQL
Chloroform
10/3/00
10
10
BQL
Chloromethane
10/3/00
10
10
BQL
Dibromochloromethane
10/3/00
10
10
BQL
C'
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
10/3/00
10/3/00
10
10
10
BQL
10
BQL
1,3-Dichlorobenzene
10/3/00
10
10
BQL
1,4-Dichlorobenzene
10/3/00
10
10
BQL
1,1-Dichloroethane
10/3/00
10
10
BQL
1,2-Dichloroethane
10/3/00
10
10
BQL
1,1-Dichloroethene
10/3/00
10
10
BQL
cis-1,2-Dichloroethene
10/3/00
10
10
BQL
trans-1,2-Dichloroethene
10/3/00
10
10
BQL
1,2-Dichloropropane
10/3/00
10
10
BQL
cis-1,3-Dichloropropene
10/3/00
10
10
BQL
trans-1,3-Dichloropropene
10/3/00
10
10
BQL
Methylene Chloride
10/3/00
10
50
BQL
1,1,2,2-Tetrachloroethane
10/3/00
10
10
BQL
Tetrachloroethene
10/3/00
10
10
BQL
—
1,1,1-Trichloroethane
10/3/00
10
10
BQL
1,1,2-Trichloroethane
10/3/00
10
10
BQL
Trichloroethene
10/3100
10
10
100
Trichlorofluoromethane
10/3/00
10
10
BQL
Vinyl Chloride
10/3/00
10
10
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
_-
Added
Result
Recovered
1,4-Dichlorobutane
40
40
99
Comments:
All values corrected for dilution.
Flags:
BQL =Below quantitation limit.
_•
Page 1 of 1
1
Reviewed By:
N.C. Certification #481
S.C. Certification #99029

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
r.
LI
Client Sample ID:
MW-1
Date Collected: 9/26/00
Client Project ID:
Toastmaster
Date Received: 9/27/00
Lab Sample ID:
96157
Analyzed By: EES
Lab Project ID:
G216-82
Matrix:
Water
Parameter
Result
Date
Analyzed
pH
6.02
9/29/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
N.C. Certification #481 S.C. Certification #99029
Reviewed By: 1 e

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-2
Date Collected:
9/26/00
Client Project ID:
Toastmaster
Date Received:
9/27/00
Lab Sample ID:
96158
Analyzed By:
EES
Lab Project ID:
G216-82
Matrix:
Water
Parameter
Result
Date
Analyzed
pH
6.11
9/29/00
Comments: ,
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
N.C. Certification #481 S.C. Certification #99029
Reviewed By: �„_

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-3
Date Collected: 9/26/00
Client Project ID:
Toastmaster
Date Received: 9/27/00
Lab Sample ID:
96159
Analyzed By: EES
Lab Project ID:
G216-82
Matrix:
Water
Parameter
Result
Date
Analyzed
pH
5.79
9/29100
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
N.C. Certification #481 S.C. Certification #99029
Reviewed By:

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-4
Client Project ID:
Toastmaster
Lab Sample ID:
96160
Lab Project ID:
G216-82
Matrix:
Water
Parameter
Result
pH
5.59
Date Collected: 9/26/00
Date Received: 9/27/00
Analyzed By: EES
Date
Analyzed
9/29/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
N.C. Certification #481 S.C. Certification #99029
Reviewed By: fv-

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-5
Date Collected: 9/26/00
Client Project ID:
Toastmaster
Date Received: 9/27/00
Lab Sample ID:
96161
Analyzed By: EES
Lab Project ID:
G216-82
Matrix:
Water
Parameter
Result
Date
Analyzed
pH
5.65
9/29/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
N.C. Certification #481 S.C. Certification #99029 Reviewed By:

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID: MW-6
Date Collected: 9/26/00
Client Project ID:
Toastmaster
Date Received: 9/27/00
Lab Sample ID:
96162
Analyzed By: EES
Lab Project ID:
G216-82
Matrix:
Water
Parameter
Result
Date
Analyzed
PH
5.18
9/29/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
N.C. Certification #481 S.C. Certification #99029 Reviewed By: �J_

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-7
Date Collected:
9/26/00
Client Project ID:
Toastmaster
Date Received:
9127/00
Lab Sample ID:
96163
Analyzed By:
EES
Lab Project ID:
G216-62
Matrix:
Water
Parameter
Result
Date
Analyzed
pH
5.33
9129/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
N.C. Certification #481 S.C. Certification #99029 Reviewed By: .i

PARADIGM ANALYTICAL LABORATORIES, INC.
-
Results for Inorganics
'
Client Sample ID:
MW-9 Date Collected:
9/26/00
Client Project ID:
Toastmaster Date Received:
9/27/00
Lab Sample ID:
96164 Analyzed By:
EES
Lab Project ID:
G216-82
- Matrix:
Water
Parameter
Result
Date
r7
Analyzed
' pH
4.92
9/29/00
I�
< Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for IVPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
LE
i�
N.C. Certification #481 S.C. Certification #99029
Reviewed By:

PARADIGM ANALYTICAL LABORATORIES, INC.
Results For Inorganics
1
Client Sample ID:
MW-10
Client Project ID:
Toastmaster
Lab Sample ID:
96165
Lab Project ID:
G216-82
Matrix:
Water
Parameter
Result
pH
4.92
Date Collected: 9/26/00
Date Received: 9/27/00
Analyzed By: EES
Date
Analyzed
9/29/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
N.C. Certification #481 S.C. Certification #99029
Reviewed By: j� �J

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-11
Client Project ID:
Toastmaster
Lab Sample ID:
96166
Lab Project ID:
G216-82
Matrix:
Water
Parameter
Result
pH
Comments:
5.06
Date Collected: 9/26/00
Date Received: 9/27/00
Analyzed By: EES
Date
Analyzed
9129100
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
N.C. Certification #481 S.C. Certification #99029
Reviewed By: 1� I

PARADIGM ANALYTICAL LABORATORIES, INC.
- -
Results for Inorganics
n
Client Sample ID:
MW-12 Date Collected:
9/26/00
Client Project ID:
Toastmaster Date Received:
9127100
Lab Sample ID:
96167 Analyzed By:
EES
Lab Project ID:
G216-82
Matrix:
Water
Parameter
Result
Date
,
Analyzed
5
pH
I
5.25
9/29/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Ii
�, N.C. Certification #481 S.C. Certification #99029 Reviewed By:

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-13
Date Collected: 9/26/00
Client Project ID:
Toastmaster
Date Received: 9/27/00
Lab Sample ID:
96168
Analyzed By: EES
Lab Project ID:
G216-82
Matrix:
Water
Parameter
Result
Date
Analyzed
pH
5.08
9/29/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
N.C. Certification #481 S.C. Certification #99029
Reviewed By: -—J -

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-14
Date Collected: 9/26100
Client Project ID:
Toastmaster
Date Received: 9/27/00
Lab Sample ID:
96169
Analyzed By: EES
Lab Project ID:
G216-82
Matrix:
Water
Parameter
Result
Date
Analyzed
pH
5.26
9/29/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
N.C. Certification #481 S.C. Certification #99029
Reviewed By:

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
Influent
Date Collected:
9/26/00
Client Project ID:
Toastmaster
Date Received:
9/27/00
Lab Sample ID:
96173
Analyzed By:
EES
Lab Project ID:
G216-82
Matrix:
Water
Parameter
Result
Date
Analyzed
pH
5.57
9/29/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
N.C. Certification #481 S.C. Certification #99029 Reviewed By: Y'�—

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
Effluent Trench
Client Project ID:
Toastmaster
Lab Sample ID:
96174
Lab Project ID:
G216-82
Matrix:
Water
Parameter
Result
pH
7.02
Date Collected: 9/26100
Date Received: 9/27100
Analyzed By: EES
Date
Analyzed
9/29/00
Comments: ,
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By:V(cation
N.C. Certification #481 S.C. Certifi#99029 "---

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID: Cooling Tower
Date Collected:
9/26/00
Client Project ID: Toastmaster
Date Received:
9/27100
Lab Sample ID: 96175
Analyzed By:
EES
Lab Project ID: G216-82
Matrix: Water
Parameter Result
Date
Analyzed
pH 6.65
9/29/00
Comments: ,
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
N.C. Certification #481 S.C. Certification #99029
Reviewed By:

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
RW-1
Client Project ID:
Toastmaster
Lab Sample ID:
96170
Lab Project ID:
G216-82
Matrix:
Water
Parameter
Result
BE
5.29
Date Collected: 9/26/00
Date Received: 9/27100
Analyzed By: EES
Date
Analyzed
9/29/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
N.C. Certification #481 S.C. Certification #99029
Reviewed By: Its -

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
RW-2
Date Collected: 9126/00
Client Project ID:
Toastmaster
Date Received: 9/27/00
Lab Sample ID:
96171
Analyzed By: EES
Lab Project ID:
G216-82
Matrix:
Water
Parameter
Result
Date
Analyzed
pH
4.95
9/29/00
Comments: ,
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
N.C. Certification #481 S.C. Certification #99029
[Reviewed By:-

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
RW-3
Client Project ID:
Toastmaster
Lab Sample ID:
96172
Lab Project ID:
G216-82
Matrix:
Water
Parameter
Result
pH
5.20
Date Collected: 9/26100
Date Received: 9127/00
Analyzed By: EES
Date
Analyzed
9/29!00
Comments: ,
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By:V6'J__
N.C. Certification #481 S.C. Certification #99029

;e write or call:
Type or Use a ball-point pen and press firmly. ( PERMIT NUMBER: (REQUIRED) . `'" � ` M"
Facility Name-lOQ5t-MQ-5,le r$nL / ngrUYvAm li PCO[)uC'i`� To Gk Itty� Non -Discharge V\r�� DOU-"I -I cif
Address P I cL n+ 2 on�l NPDES
SC(yt-1QnC� € TYPE OF DISPOSAL OPERATION BEING MONITORED
n �' 3 County (REQUIRED)'
Well Location fat ay- y I..,
Lu�� �n A,' Lagoon _Septic TanklDrain Field
Well Identification Number MY 1-t _ Well Depth Q i • Ft.
Spray Field _ Subsurface L"-Presgure
Well Diameter -,2 • U Sample (Screened) Interval 15.0 Ft. To 2 5D Ft. Piping (LPP)--
Depth to Water Level l a.• a ft. below measuring point (before sampling) j _ Land Application of Sludge =o
Other
Measuring point is J .5 ft. above land surface T Rotary Distributor
'!
Gallons of water pumped/balled before sampling ;
16—
Field Analysis: pH S. ,A I Specific Conductance uMhos Temp. °C Odor
, � Appearance
Date Sample Collected Date Lab Sample Analyzed
Laboratory Name
r"
An a.t Certification No. "I 1 O r' .J
SAMPLES FOR METALS WtRE COLLECTED UNFILTERED AND FIELD ACIDIFIED ✓ YES NO —
COD
mg/I
Coliform: MF Fecal
/100ml
Coliform: MF Total
/100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed) t, • o-
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/1
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/l
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P r,
mg/I
AI - Aluminum )
mg/I
Ba - Barium
mg/1
Ca - Calcium
mg/1
Cd - Cadmium
mg/I
Chromium: Total i
mg/I
Cu - Copper mg/I
Fe - Iron mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/1
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE.
A Ifloo �oj co I
Signature of Permittee (or Authorized Agent") Date 11
GW-59 REV. 8/96
Ni - Nickel
mg/I
Pb - Lead
mg/I
Zn - Zinc
mg/I
Pesticides/Herbicides
(Specify Compounds)
ug/I
ug/I
ug/1
Other (Specify Compounds and
Concentration units)
Trichloroc+h n� - tyL)u51L
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
F
Seeback for Instructions.
Submit blue and yellow copies only to address above.

write ordall:- '.-
Type or Use a ball-point pen and press firmly. I PERMIT NUMBER: (REQUIRED)
Facility Name Ti�QsYn/lQ YaY Sr�C.ISnQf lw.m IIti� PrrctUCV� fctGllliL(_ NPDESNon-Discharge 4,ItJ oO� i9�lu
Address P Inn-(- VQaCt TYPE OF DISPOSAL OPERATION BEING MONITORED
I nvrinhii'rn nr� ?x35a't- County �c�-1-1r.�r�d racnntaFm'
Well Location za - 14' 1 r sL.3 L02 - "I m
Well Identification Number Mw'�- Well Depth 30• U Ft.
Well Diameter I -J 5 Sample (Screened) Interval Ft. To 12 11 Ft.
Depth to Water Level kLIJ it. below measuring point (before sampling)
Measuring point is I. 3,) ft. above land surface
Gallons of water pumped/bailed before sampling
Field Analysis: pH 5 -99 Specific Conductance uMhos Temp. oC Odor
C,!a t, Do Date Lab Sample Analyzed
Lagoon _ bepuc ianWurain rieia
Spray Field Subsurface Low -Pressure
Piping (LPP) o
Land Application of Sludge o
_ A Omer
Rotary Distributor
Appearance
Date Sample Collected —/
LaboratoryName brad,ii3nnl Certification No.
SAMPLES FOR METALS WtRE COLLECTED UNFILTERED AND FIELD ACIDIFIED —,LYES _NO
COD
mg/I
Coliform: MF Fecal
/100ml
Coliform: MF Total
/100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed) I I
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance -uMhos
Total Ammonia
mg/I
TKN as N
mg/I
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/1
Phosphorus: Total as P
mg/I
Al - Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/1
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
;-y
Ni - Nickel `' :'mg/I
Pb - Lead mg/I
Zn - Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
ug/I
ug/I
ug/I
Other (Specify Compounds and
Concentration units)
Tit�hlofitPt�ene 100411.
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
Uil't�)atnrI n•�i ic-, t'I.Q i ( IG IOA Do See back for Instructions.
Signature of Permittee (or Authorized Agent`) Date `� Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

GRUulvuvvH?r Gn VFv�+r. x < k
s e...., r lease wrlle or call
P ,.
w a
COMPLIANCE�REpOC�T£FORM
Type or Use a ball point pen and press firmly
PERMIT NUMBER: (REDUIRQ1
-ri ° Prt.6UCi S �0.0 h%
Non-Discharge...--
acility Name Si Sn c �n c r ^�
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED
Address S C��
d13 . - 3- County
(REQUIRED)' Lagoon — Septic Tank/Drain Field
19 ' �').3
c Li L I d-I
Jell Location n Well Depth >r� •o Ft.
Spray Field — (ace Low -Pressure
r
Veil Identification Number Ft. To is C) Ft.
i 15 Sample (Screened) Interval
pipingSubsu
Piping(LPP)
Land Application of Sludge o
Veil Diameter -
Water Level I1- 3 it. below measuring point (before sampling)
< Other
Distributor
)epth to
point is ft. above land surface
Rotary
-
�Aeasuring a
3allons of water pumped/bailed before sampling oC
uMhos Temp.
Odor Appearance t
:ield Analysis: pH I • A u Specific Conductance
12t let, _Date Lab Sample Analyzed
No. LA
Date Sample Collected L a +
Certification
Laboratory Name - r .
UNFILTERED AND FIELD ACIDIFIED ✓
YES NO o
SAMPLES FOR METALS RE COLLECTED
COD
Coliform: MF Fecal
mgll
/100m1
Coliform: MF Total
/100ml
(Note: Use MPN method for highly turbid samples)
m9
Dissolved Solids: Total �
-79
units
pH (when analyzed) ,
mg/l
TOO
mg/I
Chloride
mg/I
Arsenic
Grease and Oils
mgll
mg/1
Hardness: Total
mg/I
Phenol
mg/l
Sulfate
Specific Conductance
Alhos
mg/I
Total Ammonia
mg/I
TKN as N
Nitrite (NO2) as N
mg/I
mg/I
Nitrate (NO3) as N
m9/1
Phosphorus: Total as P�
mg/I
Al - Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/1
Cd - Cadmium
mg/1
Chromium: Total
mg/1
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/1
Mn - Manganese
mg/I
Na - Sodium
CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE.
Io13olno
)!�Q 1 I i1On f7 1 fr ti P r' r Date
Signature of Permlttee (or Authorized Agent*)
GW-59 REV. 8/96
Ni - Nickel
mg/I
mg/1
Pb - Lead
mg/I
Zn - Zinc
Pesticides/Herbicides
(Specify Compounds)
Ug/1
ug/1
Ug/1
Other (Specify Compounds and
.Concentration units)
r r, I L
I C,"oroe c r.n
-�i iL1�l ocfz-ole r, C_ - 2ci r�
n�t-_
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
=back =yellow
es only to address above.

Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED)
Non -Discharge MAID o0u1-19S
Facility Name Tor4Skm0,5Fe r 1-0c) n Y' 1 trae Pr rlur l5 Faulk u— NPDES
Address 0-I TYPE OF DISPOSAL OPERATION BEING MONITORED
1 n 1 y i nhU ra , n .2a 351 County SC oY)n Ind (REQUIRED)'
-�-------�- Se tic TanWDrain Field
Well Location I. U Ft.
Well Identification Number M W - `( Well Depth
Weil Diameter o 15_Sample (Screened) Interval Ft. To :21. Z' Ft.
Depth to Water Level I A 1—ft. below measuring point (before sampling)
Measuring point is ft. above land surface
Gallons of water pumpedthailed before sampling LA
Field Analysis: pH U A O Specific Conductance uMhos Temp. °C Odor
L b Sam le Anal zed
Lagoon
P
Spray Field _ Subsurface Low -Pressure
Piping (LPP)
Land Application of Sludge
X Other o -
Rotary Distributor —
Appearance
Date Sample Collected J` I Z U 1011 Date a a p y
Laboratory Name a 1 r t o Certification No.
-SAMPLES FOR METALS W RE COLLECTED UNFILTERED AND FIELD ACIDIFIED AYES NO
COD
mg/I
Coliform: MF Fecal
/100ml
Coliform: MF Total
/100m1
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed) 5.5 9
units
TO.0
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P
mg/I
AI - Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
s7
Ni - Nickel — fmcl/I
Pb - Lead r mg/I
Zn - Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
ug/l
ug/I
ug/I
Other (Specify Compounds and
Concentration units)
r i5-1 -7 cA�lac e-Fhene - Alpou.31L
TYi(_Hor '+y)e e - lc°ouoll
TKN as
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
19 �O u ." See back for instructions.
Signature of Permittee (or Authorized Agent) Date Submit blue and yellow copies only to address above.
GW-59 REV. 8196

k(aFiUU1VUYVH'1Crtl+lUHtLlI`r,IYlvtYllvntt��a For etldittonel'forma
.:r�. x xy a ,
I E`�,,: please write or ealL•- .
�COMPLJ�A° P REPORT FORMu �
�... d. '•�.11 .... kra .S .ST^• n`L5. rF <P .Y..1.. .�
RALEIGH;,N=7,628.0578r.;
, :.
2 .f ld »i p
- + ' _ ' �' ^[phone]ti"�
VIM-
Type or Use a ball-point pen and press firmly.
PERMIT NUMBER: (REQUIRED)
'VJ 9
'kMCS1e( - nL- 1Inyo ,_Lrn TtM4? Prodtrrl-S FOCII,I+L)
Non -Discharge �cX�11G j
Facility NameT�(X
Address P In n+ Ro rl
SC CUM\-
TYPE OF DISPOSAL OPERATION BEING MONITORED
L� I i v u h L 2 R.b59 County --+I
(REQUIRED)'
( )
Well Location L3 l0'TL.`1 Lon-'lq"�t�'4o.�'•
Lagoon _ Septic TanklDrainField
Well Identification Number M l-S Well Depth ?`I• a Ft.
Spray Field Subsurface Low-Pressdse
Well Diameter I • a `> Sample (Screened) Interval Ft. To 't_J- o Ft.
Piping (LPP) 0 4
Depth to Water Level o—ft. below measuring point (before sampling)
Land Application of Sludge
'_ Other
Measuring point is } o ft. above land surface
Rotary Distributor = u
Gallons of water pumped/bailed before sampling t
;
Field Analysis: pH � 9 1 Specific Conductance uMhos Temp. oC
Odor Appearance ry ;
Date Sample Collected 912J, 1 ou -Date Lab Sample Analyzed
Laboratory Name c. r T i e s
Certification No. t
SAMPLES FOR METALS W E COLLECTED UNFILTERED AND FIELD ACIDIFIED ✓
YES NO U
COD
mg/I
Coliform: MF Fecal
/100ml
Coliform: MF Total
/100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed) 5. f, 5
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/1
Specific Conductance
uMhos
Total Ammonia
mg/1
TKN as N
mg/I
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/1
Phosphorus: Total as P
mg/I
Al - Aluminum
mg/I
Ba -.Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
ri
Ni - Nickel Zmg/I
Pb - Lead mg/I
Zn - Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
ug/I
ug/I
ug/1
Other (Specify Compounds and
Concentration units)
TrlclnlorceNnene ago LtaIL
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values'should reflect dissolved and
colloidal concentrations. (see #3 on back)
�r
IG ! 1/lnn ?)O I ou See back for Instructions.
Signature of Permittee (or Authorized Agent') Date •• Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

� please writaorcall <_
�C0IIAPLIANCEREFORT FORM -
r ,'� , 919 733+3!'Ll .� r it .,3 „�,,•�,?:.
�i..su�. .,w 6.,+t y. <�.. •,-'yI ,ro,(a. ,. a
4se-. .. s... ,, .<. xs, ,.. ,xa ,..fps,
Type or Use a ball-point pen and press firmly.
PERMIT NUMBER: (REQUIRED)
t� 000 1 19 S
TOO i r Gl� c f T�r� �n m Ti nn r Fyort a r 1 s Fact (t
Non-Discharge^1
Facility Name S RnC�S+c
NPDES
Address 1216 13t e Q d ,
TYPE OF DISPOSAL OPERATION BEING MONITORED
1.ptivt,3bi'IrQrt� 2835 County Rrc'�lnrx�l
(REQUIRED)'
Lagoon Septic Tank/Drain Field
t o .H , S� 4 „ n ��, .I
Well Location Sri
•
Well Identification Number ^^ `N-1 D Well Depth _ Ft.
Spray Field Subsurface Low -Pressure
Well Diameter s • O Sample (Screened) Interval '.7• U Ft. To - `; o Ft.
Piping (LPP)
Land Application of Sludge
Depth to Water Level ' • O ft. below measuring point (before sampling)
K other
Measuring point is f 0 ft. above land surface
Rotary Distributor o
Gallons of water pumped[bailed before sampling y
oC
Odor Appearance -
Field Analysis: pH 5 • S I Specific Conductance uMhos Temp.
Field
Date Sample Collected '1 1 zl, 1 nu Date Lab Sample Analyzed
i
a g l
l a r e
Certification No.
Laboratory Name r
UNFILTERED AND FIELD ACIDIFIED AYES
NO -
SAMPLES FOR METALS W E COLLECTED
COD mg/I
Coliform: MF Fecal /loom]
Coliform: MF Total /100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total mg/l
pH (when analyzed) 5. I F units
TOC mg/I
Chloride mg/I
Arsenic mg/I
Grease and Oils mg/I
Hardness: Total mg/I
Phenol mg/I
Sulfate mg/I
Specific Conductance uMhos
Total Ammonia mg/I
TKN as N mg
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P.
m9/1
Al - Aluminum
mg/1
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/1
K - Potassium
mg/I
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE.
N 11 i]nn M r +n lu n I t
Signature of Permittee (or Authorized Agent')
Ni - Nickel �hYg/l
Pb - Lead -;mg/I
Zn -Zinc
Pesticides/Herbicides
(Specify Compounds)
ug/I
ug/I
ug/I
Other (specify Compounds and
Concentration units)
Ci5-t U rh\oroeihPnC-'IAtL�jL
L
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
See back for instructions.
Date Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

Type or Use a ball-point pen and press firmly.
PERMIT NUMBER:
(REQUIRED)
8
r �! Zvi Nur Produc l S FaGlt 1
tA)O 000�1G
Facility Nameon
0(kS'MaS-t
—I J�rnhorr\
NPDEScliarge
Address P Ian'
2006l
I 2 County fir' i( O C
TYPE OF DISPOSAL
OPERATION BEING MONITORED
Lq
1
3 ` `I ' L- r -jq- AI' 11 "I •.1-'
(REQUIRED)
Lagoon Septic TanWDrain Field
Well Location a - 4
Well Identification Number N\W - Well Depth 3"546 Ft.
Spray Field Subsurface Low -Pressure
0
S le (Screened) Interval lei • ° Ft. To = ' • f? Ft.
Piping (LPP)
Well Diameter amp Land Application of Slud e
Depth to Water Level l a. le ft. below measuring point (before sampling) fa other
Measuring point is `I . -2 ft. above land surface
Rotary Distributor
o
Gallons of water pumped/bailed before sampling
Field Analysis: pH 5. 9 3 Specific Conductance
uMhos Temp. °C Odor
Appearance —
_
Date Sample Collected 9 66101) Date Lab Sample Analyzed
' Lo' Certification
No.
Laboratory Name r .bo•
.SAMPLES FOR METALS ERE COLLECTED UNFILTERED AND FIELD ACIDIFIED .YES
NO
r�
COD mg/I
Nitrite (NO2) as N
mg/I
Ni - Nickel
s ,;mg/1
/I
Coliform: MF Fecal /100ml
/100m1
Nitrate (NO3) as N
Phosphorus: Total as P
mg/I
mg/I
Pb- Lead
Zn - Zinc
�tTtg/I
Coliform: MF Total
AI - Aluminum
mg/I
Pesticides/Herbicides
(Note: Use MPN method for highly turbid samples)
D' I d Solids• Total mg/I
Ba - Barium
mg/I
(Specify Compounds)
ISso ve
pH (when analyzed) S• a �
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/l
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
ug!
, r\,N as
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
(o ( 3 010 U See back for instructions.
Signature of Permittee (or Authorized Agent) Date Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

or
pen ana press
Facility Name nn ca Mn ai2r Yn c 4 sngr c harm 1 Im e. Pror\u c-ys Fn r i I li ,6=
-County Scs-Hrl ;-d
Well
PERMIT NUMBER: (REQUIRED)
Non -Discharge W6� nen T99
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED)'
Lagoon
Septic Tank/Drain Field
Well Identification Number N, N- �l ' Well Depth -2 5 • U Ft. Spray Field _ Subsurface Low -Pressure
Well Diameter )- K- Sample (Screened) Interval D• 5 Ft. To .'29 • J Ft. Piping (LPP)
Depth to Water Level Jot'—ft. below measuring point (before sampling) Land Application of Sludge
y
Measuring point is-ft. above land surface Rotary Distributor
Other o J
Gallons of water pumped/bailed before sampling
Field Analysis: pH 5 . t 5 Specific Conductance uMhos Temp. oC Odor Appearance __j ='
Date Sample Collected `t 1Z,IA o L Date Lab Sample Analyzed t _
Laboratory Name rc r ..( cr P s Certification No. L(S l ^'
SAMPLES FOR METALS W E COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO '--�
COD
mg/I
Coliform: MF Fecal
/100ml
Coliform: MF Total
/100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed) 4.9 a-
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P
mg/I
Al - Aluminum
mg/I
Ba - Barium
mg/I
CaCalcium Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE.
Signature of Permittee (or Authorized Agent*)
Ni - Nickel
Pb - Lead
-' ivig/I
-`_mg/I
Zn - Zinc
Pesticides/Herbicides
(Specify Compounds)
mg/I
ug/I
ug/I
ug/I
Other (Specify Compounds and
Concentration units)
Ct5-I D �h\oroe�hc.rt2 - 1 LLnI L
"t"rt�L,lori>etytev�e a�;rr
IL.
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
101 �O I Co See back for Instructions.
Date •• Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

wril9
Type or Use a ball-point pen and press firmly.
Facility Name ILOS+1111Cl5 •LZnprnYtnm tl tvoclur+•i Fa(-l«
Address P'"'-)f- 2rr4c(
Imo; ..�, t [; sI n r. County i-�
PERMIT NUMBER: (REQUIRED)
Non -Discharge \&J-Q t 11Ct a -
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED)'
Well Location I - 1
Well Identification Number na W -10 Well Depth .9 • t' Ft.
Well Diameter �J- 0 Sample (Screened) Interval 2-'i Ft. To .9 , V Ft.
Depth to Water Level to • G ft. below measuring point (before sampling)
Measuring point is ). •t `> ft. above land surface
Gallons of water pumped/bailed before sampling
Field Analysis: pH H-R0 Specific Conductance uMhos Temp.— oC Odor
`Ila bfoo Date Lab Sample Analyzed
Lagoon _ Septic Tank/Drain Field
Spray Feld _ Subsurface Low -Pressure
Piping (LPP)
Land Application or Sludge ZZ
ci
- Other
Rotary Distributor �
Appearance
Date Sample Collected P
Laboratory Name Po- v act r c� Iv aver I y+ La L La lzro-t-crl e s Certification No. LA S l
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED ✓ YES NO
COD
mg/I
Coliform: MF Fecal
/100m1
Coliform: MF Total
/100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed) y • 9 a-
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance —uMhos
Total Ammonia
mg/I
TKN as N
mg/I
Nitrite (NO2) as h
Nitrate (NO3) as I
Phosphorus: Totc
Al - Aluminum_
Ba - Barium
Ca - Calcium
Cd - Cadmium_
Chromium: Total
Cu - Copper
Fe - Iron
Hg - Mercury_
K - Potassium _
Mg - Magnesium
Mn - Manganese
Na - Sodium
mg/I
mg/I
mg/I
mg/I
mg/1
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/I
mg/l
Ni - Nickel
Pb - Lead
Zn - Zinc
Pesticides/Herbicides
(Specify Compounds)
I
ry
i*-
0
ug/I
ug/I
ug/I
Other (Specify Compounds and
Concentration units)
is _t R - Drchlo,-0CA -Ile
le- 4clorLs3lU
TV, C,k l c e-yi e v) c- I-roo l l- L
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
i' ((1 P11')nn ('1-C Vl P l ( to 1,31 � 01.) • See back for instructions.
Signature of Permittee (or Authorized Agent`) Date •• Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

Type or Use a ball-point pen and press tirmiy. PERMIT NUMBER: (REQUIRED)
Facility Name Y'`S-t"rnG';;;�1 St1[ /.innrnhnm Ts Me, Produ(+S Fa(ktl+Non-Discharge VI� COU11GS
Address 20r)+ Ron rt NPDES
LnI vinh r ✓1[ rtf3;[52 Count Srl>i-LCLr i TYPEUI DISPOSAL OPERATION BEING MONITORED
4—t Y (REQUIREDI
Well
oo. a-"
Well Identification Number MVV L L ' Well Depth 2 5 ' L) Ft.
Well Diameter `I-0 Sample (Screened) Interval (, • 0 Ft. To a`5• 0 Ft.
Depth to Water Level ft. below measuring point (before sampling)
Measuring point is I `i ft. above land surface
Gallons of water pumped/bailed before sampling y
Lagoon _
Septic Tank/Drain Field
Spray Field _
Subsurface LoS31'resii6re
Piping (LPP) '--
Land Application of Sludge
X
•
Other —� f
Rotary Distributor
I .:
Field Analysis: pH 939 Specific Conductance uMhos Temp. °C Odor Appearance
Date Sample Collected `I 0_ o 1 0o Date Lab Sample Analyzed
Laboratory Name 5 Certification No. ti$ 1 E3
SAMPLES FOR METALS - RE COLLECTED UNFILTERED AND FIELD ACIDIFIED z YES NO
COD
Coliform: MF Fecal
Coliform: MF Total
(Note: Use MPN method for highly turbid samples)
mg/I
00ml
00m]
Dissolved Solids: Total
mg/I
pH (when analyzed) S. o L�
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P
mg/I
AI - Aluminum
mg/I
Ba -.Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
Ni - Nickel mg/I
Pb - Lead mg/I
Zn - Zinc mg/I
Pesticides/Herbicides
(Specify Compounds)
Other (Specify Compounds and
Concentration units)
TrtGhtovicei-Vlene - .1NntJ�L
ug/I
ug/I
ug/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
t colloidal concentrations. (see #3 on back)
10�� l lO(� ) • See back for instructions.
Signature of Permittee (or Authorized,Agent*Date •• Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

a orEall::. .
Type or Use a ball-point pen and press firmly. PERMIT NUMBER: (REQUIRED)
Facility Name TO 05 -mrt at r =n C �rnr rn Inn m T M L LUCI U (I-S FG Li I4q Non -Discharge \-I G cOO-1-Ici Y)
Address 210. 1f )'LaCL NPDES
R r ti In nC� TYPE OF DISPOSAL OPERATION BEING MONITORED
I nurinhi.trn,12 A9,bri� County REQUIRED'
Well Location -� ( ) _ Lagoon _ Septic TanIdDraln Field
Well Identification Number M W - I P- Well Depth 2 • o' Ft.
J; O Spray Field _ Subsurface Low -Pressure
Well Diameter �� • D Sample (Screened) Interval 15.0Ft. To Ft. Piping (LPP)
Depth to Water Level (i 75- ft. below measuring point (before sampling) — Land Application of sludge —
X Other C:3
Measuring point is �1 • 5 ft. above land surface
Gallons of water pumped/bailed before sampling LA
Field Analysis: pH 5• A 1 Specific Conductance uMhos Temp. oC
Date Sample Collected 912le 100 Date Lab Sample Analyzed
Laboratory Name PrI r . es
SAMPLES FOR METALS W E COLLECTED UNFILTERED AND FIELD ACIDIFIED
Rotary Distributor
Odor Appearance —
certification No. LIS I
YES —NO ti
=
COD
mg/I
Nitrite (NO2) as N
mg/I
Ni - Nickel r
c�
mg/I
Coliform: MF Fecal
/loom[
Nitrate (NO3) as N
mg/I
Pb - Lead
== mg/I
mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
Zn - Zinc
(Note: Use MPN method for highly
turbid samples)
Al - Aluminum
mg/I
Pesticides/Herbicides
Dissolved Solids: Total
mg/I
Ba -.Barium
-
mg/I
(Specify Compounds)
ug/I
pH (when analyzed)5.05
units
Ca Calcium
mg/I
ug/I
TOC
mg/I
Cd - Cadmium
mg/I
ug/I
Chloride
mg/I
Chromium: Total
mg/I
Arsenic
mg/I
Cu - Copper
mg/I
Other (Specify Compounds and
Grease and Oils
mg/I
Fe - Iron
mg/I
. Concentration units)
cl I l-
Hardness: Total
mg/I
Hg - Mercury
mg/I
Tv 1 r Ior :e t Vwn r - un
Phenol
mg/I
K - Potassium
mg/I
Sulfate
mg/I
Mg - Magnesium
mg/I
Specific Conductance
uMhos
Mn - Manganese
mg/I
Total Ammonia
mg/I
Na - Sodium
mg/I
TKN as N
mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
" See back for instructions.
Signature of Permittee (or Authorized Agent*) ate F.
Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

Type or Use a ball-point pen and press firmly.
Facility Name Tons-MnasiPrsln( �Znarn.irornTnne Protiu�tS fau_I
Address n I.. n+ IZ on al
t of Luni'lcirq J.nc 1Z°5315�L County SCcri'UnCL
Well Location Lai 34' It !a c l b" Lonq 19 2.-1 tri 3"
PERMIT NUMBER: (REQUIRED)
Non -Discharge U 16
'1 �-i-t"IG g
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED)
Lagoon _Septic Tank/Drain Field
Well Identification Number MW -1 3 Well Depth 0 Ft.
Well Diameter � • D Sample (Screened) Interval -1' • D Ft. To `1) ^ Ft.
Depth to Water Level 4. a ft. below measuring point (before sampling)
Measuring point is -;Lft. above land surface
Gallons of water pumeed/bailed before sampling
Field Analysis: pH h - U S Specific Conductance uMhos Temp. oC Odor
D t S m le Collected I1JL6 100 Date Lab Sample Analyzed
Spray Field Subsurface Low -Pressure
Piping (LPP) o
Land Application of Sludge O o
X Other
Rotary Distributor
r'v
Appearance
ae a p
Laboratory Name P Yn. d.Lr i i L. hu n_-hor I e 5 Certification No. Ll51
COLLECTED UNFILTERED AND FIELD ACIDIFIED YES NO
SAMPLES FOR METALS WE E
COD
mg/I
Nitrite (NO2) as N
mg/I
Ni - Nickel r
ti
6mg/I
mg/I
Coliform: MF Fecal
/100m1
Nitrate (NO3) as N
mg/I
Pb - Lead
mg/I
Coliform: MF Total
/10oml
Phosphorus: Total as P
mg/I
Zn - Zinc
(Note: Use MPN method for highly turbid samples)
Al - Aluminum
mg/I
Pesticides/Herbicides
Dissolved Solids: Total
mg/I
Ba -.Barium
-Calcium
mg/I
(Specify Compounds)
ug/
pH (when analyzed) 5.o>;
units
Ca
mg/I
ug/I
TOC
mg/I
Cd - Cadmium
Total
mg/I
mg/I
ug/I
Chloride
mg/I
Chromium:
Arsenic
mg/I
Cu - Copper
mg/I
Other (specify compounds and
Grease and Oils
mg/I
Fe - Iron
mg/I
Concentration units)
B«31u
Hardness: Total
mg/I
Hg - Mercury
mg/I
ci> - 1. ;L -'DchtoYoel-t1Pn0
Phenol
mg/I
K - Potassium
mg/l
iy r f.hlnr,•. r FV Pn e — 11 u u I
L
Sulfate
mg/I
Mg - Magnesium
mg/I
Specific Conductance
uMhos
Mn - Manganese
mg/I
Total Ammonia
mg/I
Na - Sodium
mg/I
TKN as N
mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE.
Note:
Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
/� hC111 �11 I Y1 t fTh f l C
10.131 co
See back for instructions.
Signature of Permittee (or Authorized
Agent')
Date
•• Submit
blue and yellow copies only to address above.
GW-59 REV. 8/96

Type or Use a ball-point pen and press tirmly.
Facility Name TOO-0-1,46Stec-Inr. / 14osra-ham-Ttmc.Rfxiv(+-5 l=Gcilt-W
Address P 10 04- Poct d
PERMIT NUMBER: (REQUIRED)
Nan -Discharge •\A) t9 0( 1211
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED)•
Well Location La 4 - 3 4 " `t b' o _1 3 " Lonc- - -19 ` ' `♦ 9 • lr '• Lagoon _Septic Tank/D n Field_
Well Identification Number MW - t u Well Depth '-9 O Ft. — `7j
Spray Field _ Subsurface Loay-Pressure
Well Diameter y . Sample (Screened) Interval!- . Ft. To 'i11 a Ft. Piping (LPP) "O
Land Application o1 Sludge
Depth to Water Level 1)_y —ft. below measuring point (before sampling) _ other
Measuring point is -/- a ft. above land surface Rotary Distributor v
Gallons of water pumped/bailed before sampling y b
Field Analysis: pH t, •I S Specific Conductance uMhos Temp. oC Odor Appearance —
Date Sample Collected J P y
I ato I on Date Lab Sample Anal zed r-,
Laboratory Name vies Certification No. 4P, I
SAMPLES FOR METALS WEhE COLLECTED UNFILTERED AND FIELD ACIDIFIED ✓ YES NO
r
COD
mg/I
Coliform: MF Fecal
/100ml
Coliform: MF Total
/100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed) S • a to
units
TOC
mg/1
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P
mg/1
Al - Aluminum
mg/1
Ba - Barium
mg/I
Ca - Calcium
mg�
Cd - Cadmium
mg/I
Chromium: Total
mg/l
Cu - Copper
mg/I
Fe - Iron
mg/I .
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg- Magnesium
mg/I
Mn - Manganese
mg/1
Na - Sodium
mg/I
Ni - Nickel
mg/1
Pb - Lead
mg/I
Zn - Zinc
Pesticides/Herbicides
(Specify Compounds)
mg/1
ug/I
ug/I
ug/I
Other (Specify Compounds and
Concentration units)
-Dt(hlY kt)eriai
(ou91�
Ty l c ki oroe 4"t'I eo L' PiAun1L
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
A hen on YVl t 1 c 12C u L 31 (clo See back for Instructions.
Signature of Permittee (or Authorized Agent') Date •� Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

Type or Use a ball-point pen and press firmly.
Facility Name Tha5-1-Maet-er_�nr Farm alkam­T1nn-c l3r'raucl-s tcdlt�
Address "'" Pon cl_
C I,�a6 75 a- County Sr 'TLtCLI'Q
PERMIT NUMBER: (REQUIRED)
Non -Discharge W r (",A_1015
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED)'
Well Location Li — L
Well Identification Number I IN 1 Well Depth Ft.
Well Diameter Sample (Screened) Interval Ft. To Ft.
Depth to Water Level ft. below measuring point (before sampling)
Measuring point is-ft. above land surface
Gallons of water pumped/bailed before sampling
Field Analysis: pH -Specific Conductance uMhos Temp. °C Odor
d (at I(0u Date Lab Sample Analyzed
Lagoon
Spray Field
Septic Tank/Drain Field
Subsurface Low-Pre�sgre
Piping (LPP) O
Land Application of Sludge — `3
Other
Rotary Distributor
Appearance
Date Sample Collected o LAO i
Laboratory Name YLUc',
SAMPLES FOR METALS
I ntZrCLt0(Ies Certification No.
UNFILTERED AND FIELD ACIDIFIED —/ YES NO
COD
mg/I
Coliform: MF Fecal
/100ml
Coliform: MF Total
/100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed) 5. zCl
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
rng/I
Nitrite (NO2) as N
mg/I
Ni - Nickel
� o
Nitrate (NO3) as N
mg/I
Pb - Lead
mg/I
mg/I
Phosphorus: Total as P
mg/I
Zn - Zinc
Al - Aluminum
mg/I
Pesticides/Herbicides
Ba - Barium
mg/I
(Specify Compounds)
ug/I
Ca -. Calcium
mg/I
ug/I
Cd - Cadmium
mg/I
ug/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Other (specify Compounds and
Fe - Iron
mg/I .
Concentration units)
Hg - Mercury
mg/I
Tv r nl ran .v+t2r rn e - Q OU U
A I L.
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
See back for Instructions.
Signature of Permittee (or Authorized Agent*) Date Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

Type or Use a ball-point pen and press firmly.
Facility Name -Tbrl 5+ry)o,l'e r -,T-nc . 1-1riy n imam i 1 NA Lod u (+5 f Qc' dlk
Address 91 " " 1' c r rl
L'u-r_`nUL�� nt 2,?5 F? S County Jr c+ln ncl
PERMIT NUMBER: (REQUIRED)
Non -Discharge WC
l 11�9
NPDES
TYPE OF DISPOSAL OPERATION BEINGMONITORED
(REQUIRED)'
Well Location
Well Identification Number Q\i - a- Well Depth Ft.
Well Diameter Sample (Screened) Interval Ft. To —Ft -
Depth to Water Level ft. below measuring point (before sampling)
Measuring point is—ft. above land surface `k
Gallons of water pumped/balled before sampling
Field Analysis: pH Specific Conductance uMhos Temp. oC Odor
I D L b S I Anal zed
Lagoon
Septic Tank/Draln Field
Spray Field _ Subsurface Low -Pressure
Piping (LPP)
Land Application of Sludge
x Other
Rotary Distributor
Appearance
Date Sample Collected :1 �-ate a amp e
LaboratoryName jkr-"f n I I alx:ra or Certification No. CIS i
SAMPLES FOR METALS WE E COLLECTED UNFILTERED AND FIELD ACIDIFIED _YES _ NO
COD
mg/I
Nitrite (NO2) as N
mg/I
Ni - Nickel
r —
mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
mg/I
Pb - Lead
�mg/I
Coliform: MF Total
/100mi .
Phosphorus: Total as P
mg/I
Zn - Zinc
(Note: Use MPN method for highly turbid samples)
Al - Aluminum
mg/I
Pesticides/Herbicides
Dissolved Solids: Total
mg/I
Ba -.Barium
mg/I
(Specify Compounds)
ug/I
pH (when analyzed) H . s c
units
Ca - Calcium
mg/I
ug/I
TOC
mg/I
'
Cd - Cadmium
mg/I
mg/I
ug/I
Chloride
mg/I
Chromium: Total
Arsenic
mg/I
Cu - Copper
mg/I
Other (Specify Compounds and
Grease and Oils
mg/I
Fe : Iron
mg/I .
Concentration units)
Hardness: Total
mg/I
Hg - Mercury
mg/I
e. - Loou
t� �
Phenol
mg/I
K - Potassium
mg/I
Sulfate
mg/(
Mg - Magnesium
mg/I
Specific Conductance
uMhos
Mn - Manganese
mg/I
Total Ammonia
mg/I
Na - Sodium
mg/I
TKN as N
mg/I
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations.. (see #3 on back)
Cn -L L(- I D 31 1 00 See back for instructions.
ignature of Permittee (or Authorized Agent') Date •• Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

Facility Name
Address
Type or Use a ball-point pen and press firmly.
0.uy(n VmLr S,V1L qP,��.`}
PERMIT NUMBER: (REQUIRED)
Non -Discharge WQ Ol 1�gi�
NPDES
TYPE OF DISPOSAL OPERATION BEING MONITORED
(REQUIRED)'
Well Location "e "
Well Identification Number �tn)-'�', Well Depth Ft. Spray Field
Well Diameter Sample (Screened) Interval Ft. To Ft.
Septic TanktDraln Field
Subsurface Low -Pressure
Piping (LPP)
Depth to Water Level ft. below measuring point (before sampling) Land Application of Sludge
x Other n
Measuring point is—ft. above land surface Rotary Distributor o
Gallons of water pumped/bailed before sampling ti
Field Analysis: pH Specific Conductance uMhos Temp. °C Odor Appearance —
Date Sample Collected 9Ia_L, I Do Date Lab Sample Analyzed
LaboratoryName ftylkcLu ry) fkna ly+t r a,l I C0.1x2(Lti-ortf 5 Certification No. `f a 1
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED —YES NO a _
`o
COD
mg/I
Coliform: MF Fecal
/loom[
Coliform: MF Total
/100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed) 5.2.0
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Hardness: Total
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P
mg/I
AI - Aluminum
mg/I
Ba - Barium
mg/I
Ca -'Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Na - Sodium
mg/I
Ni - Nickel `,,mg/I
Pb - Lead = mg/I
Zn - Zinc = mg/I
Pesticides/Herbicides
(Specify Compounds)
ug/1
ug/I
ug/I
Other (Specify Compounds and
Concentration units)
'Ty1ct)lornP+l,je0e - IPuua J 1�
I CERTIFY THAT THIS REPORT IS TRUE AND ACCURATE. Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
InnInnan M�lC t LIL �SeebackforInstructions.
Signature of Permittee (or Authorized Agent') Date Submit blue and yellow copies only to address above.
GW-59 REV. 8/96

APPENDIX V
LABORATORY ANALYTICAL RESULTS

�r � o Afid'Ml�'L�� � w C,�.ostfl� tits
SUBMIT FORM ON YELLOW PAPER ONLY SGoal kp 0 `� l ZFj �O p
FACILITY -INFORMATION Please Print Clearly or Type )
Facility Name: Ton5+rna2+e r _Lne, 1nQraham T5m e R°o_&Y i-7 FQC i I i-tv
Permit Name (if different): t`
Well Location/ Site
Telephone #: (5 -r
No. of Wells to be
Well Identification Number (from Permit): MW 1 For Groundwater Treatment systems
Well Depth: • t= ft. Well Diameter: •_� in. Check One:
Screened Interval: 15.0 ft. to 25.1) ft. I ❑ Influent . (98)
Depth to Water Level:_ft. below measuring point ❑ 'Effluent (99)1
Measuring Point is _9. 5 ft. above land surface.
Gallons of water pumped/bailed before sampling: y
Field analysis: pH 5"-*7 / , Specific Conductance uMhos `
Temp. A-3. 9 OC, Odor Appearance
PERMIT M EXPIRATION DATE: 0.3 b - o a -
Non -Discharge W O CW II9 8 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITOREDf-'
Lagoon Remedialiom lnfiltralloE8aliel-y
Spray Field Remediation:
Rotary Distributor Land Application of SIU40
Other.
na
NOTE: Values should reflect dissolved and
colloidal concentrations.
O r�.a
Date sample collected: i ^ Date sample lyz
Laboratory Name: Poxagtam Cl- c . hint L4 ivrlEs
Certification No.
for metals were collected un111teredIL/A—YES I NO
and field acldifled
PARAMETERS (Samples
COD
mg/I
Nitrite (NO2) as N
mg/I
Coliform: MF Fecal
Coliform: MF Total
/100ml
/100rill
Nitrate (NO3) as N
Phosphorus: Total as P
mg/I
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
f
mg/I
mg/I
Dissolved Solids: Total
mg/I;
Al -Aluminum
mg/I
pH (when analyzed) L, . I S6
units
Ba - Barium
mg/I
TOC
mg/I
mg/I
Ca - Calcium
Cd - Cadmium
mg/I
Chloride
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
mgll
Phenol
Sulfate
mg/I
mg/I
Fe - Iron
Hg -.Mercury
.
mgll
Specific Conductance
uMhos
K - Potassium '
mg/I
mg/I
Total Ammonia
mg/I
Mg'- Magnesium
I
mg/I
TKN as N
mg/I
Mn - Manganese
GW-59 Rev. 4198
✓ YES _ NO)
`
Ni - Nickel
mg/I
Pb - Lead
mg/I
Zn -Zinc
mg/I
Ammonia Nitrogen
mg/I
Other (Specify Compounds and Concentration Units)
Triahlorue-lfi ne -2u�IL
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
ReportAttached7 Yes X (1) No_(0)
VOC C, method # - tao 1
method #_
method #
r'.

SUBMIT FORM ON YELLOW PAPER ONLY
Facility Name:_
Permit Name (if
. Well Location/ Site
Print Clearly or Type
County Seui-lan(,L
Telephone #: (513) ` q5
No. of Wells to be Sampled:
Well Identification Number (fr6l Permit): MW-C For Groundwater Treatment Systems
Well Depth: • 10•0 ft. Well Diameter: - `in.
Check One:
Screened Interval: ft. to 10 - 0 ft.
❑ Influent
Depth to Water Level: !l S ft. below measuring point.
❑ Effluent
Measuring Point is I • 10" ft. above land surface.
Gallons of water pumped/balled before sampling: Li
Field analysis: pH 5 • `t b , Specific Conductance
uMhos
Temp. i l `I -C, Odor Appearance
PERMIT EXPIRATION DATE: 11-30-o3
Non -Discharge V40 0DO-119 8 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED:
Lagoon Rernediatlon:lnfillrat&Gelreiy
Spray Field Remediatlon:
Rotary Distributor Land Application of S=ge
X Other: t r
(98) NOTE: Values should reflect dissolved and L:
(99) colloidal concentrations. E5 ?,
Date sample collected: 5/aG/a4 I Du Date sampliaana�ied:
Laboratory Name' Parrtid iern annl F+�cit Cabca Ftir tz'z__
Certification No. 91 k 0
pARAMETgRS (Samples for metals were collected unlilterec[B� .YES _NO
and field acidified
mg/I
COD
mg/l
/100ml
Nitrite (NO2) as N
Nitrate (NO3) as N
mg/l
Coliform: MF Fecal
Coliform: MF Total
/100ml
Phosphorus: Total as P.
mg/l
mg/I
(Note: Use MPN method for highly turbid samplesy
mg/I
Orthophosphate
Al - Aluminum
Dissolved Solids: Total
pH (when analyzed) 5. • o
_units
Be - Barium
mg/I
mg/I
TOC
mg/l
mg/ l
Ca - Calcium
Cd - Cadmium
mg/I
Chloride
Arsenic
mg/l
Chromium: Total
mg/l
Grease and Oils
mg/l
mg/I
Cu -Copper
Fe - Iron
mg/I
Phenol
Sulfate
mg/I
Hg -.Mercury
mg/I
Specific Conductance
UA
mg/I
K - Potassium
Mg,- Magnesium
mg/I
Total Ammonia
TKN as N
mg/I
Mn - Manganese
mg/I
GW-59 Rev. 4/98
_YES _ NO)
Ni - Nickel mg/I
Pb - Lead mg/I
Zn -Zinc mg/I
-Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
Trir hiorce--thane. - Aby un ) L
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
ReportAttached? Yes__X__0) No _ (0)
VOC GC method#- loot
method # _
method # _
Permitlee (or Authorized Agem) Name and Title - Please print or type I I

SUBMIT FORM ON YELLOW PAPER ONLY
Facility Name:_
Permit Name (if
Well Location/ Site Name:
Print
or
County IJUUrr ru is L
Telephone #: (5,73) 4`i5-
No. of Wells to be Sampled:
Well Identification Number (from Permit): 4AW- 3 For Groundwater Treatment Systems
Well Depth: 343•0 ft. Well Diameter:t•? In. Check One:
Screened Interval: - ft. to loo ft. ❑ Influent (98)
Depth to Water Level: 13. a ft. below measuring point. ❑ Effluent (99)
Measuring Point Is y , ? ft. above land surface.
Gallons of water pumpedibailed before sampling: y
Field analysis: pH—L.L 6E , Specific Conductance . uMhos
Temp. Q, 0 • �2 °C, Odor Appearance
PARAMETERS (Samples for metals were collected I
COD
mg/I
Coliform: MF Fecal
/100ml
Coliform: MF Total
1100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (When analyzed) In 017
units
TOC
mg/I
Chloride
mg/I
Arsenic,
Grease and Oils
m9;l
Phenol
mg/l
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
PERMIT #:
DATE:
NPDES
TYPE OF PERMITTED OPERATION BEING MONITOSED1
Lagoon Remediallon: Infillratlog;,0alle y ,
Spray Field R-�a
emedlallon: °
Rotary Distributor Land Application of Slud�ga
a r-i
_X Other:
NOTE: Values should reflect dissolved and
colloidal concentrations.
bate sample collected: 3 C Date sample a aly5d:
Laboratory Name: Fbroc iam QrWNp+i(0I i3O_boY0.- QY-i65 `
Certification No.
;ered A YES _No
and field acidified
Nitrite (NO2) as N
mg/I
Nitrate (NO3) as N
mg/I
Phosphorus: Total as P
mg/I
Orthophosphate
mg/1
Al - Aluminum
mg/1
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mgll
Chromium: Total
mgll
Cu - Copper
mg/1
Fe - Iron •
mg/I
Hg -.Mercury
mg/I
K - Potassium
mg/I
Mg'- Magnesium
mg/I
Mn - Manganese
mg/I
✓ YES _ NO)
Ni - Nickel mg/1
Pb - Lead mg/1
Zn -Zinc mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
ei 5-1, a. - D'c.hlaroethenxn, - Tf u�
Tr,nhlnrnether�f 57uO,1-
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method It. Attach lab report.)
Report Attached? Yes X (1) No—(0)
VOC Ge : method#= UO I
method # _
method#=
..............
GW-59 Rev. 4/98

SUBMIT FORM ON YELLOW PAPER ONLY
Facility Name:_
Permit Name (if
Well Location/ Site Name:=+
Please
Type
County p Irl ' "
Telephone #:(5s3) '+,+5
No. of Wells to be Sampled:
Well IdentificationNumber(fromPermity_ \lt-''I For GroundwaterTrealmentSyslems
Well Depth: 23 •D ft. Well Diameter: in. Check One:
Screened Interval: ft. to .11. 0 ft' ❑ Influent (98)
Depth to Water Level: I1 7 0 ft. below measuring point. ❑ Effluent (99)
Measuring Point is ft. above land surface.
Gallons of water pumped/bailed before s mplingctance uMhos
Field analysis: pH' P Appearance
Temp. V,_ 3 "C, Odor pP
PERMIT #: EXPIRATION DATE: 113 D -oa-
Non-Discharge Wo 00D-i-191^. UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remedialion: Infiltration Gallery,
Spray Field Remedlatlon: o
Rotary Distributor Land Application of SI49e c:
-o
X_ Other:
NOTE: values should reflect dissolved and
colloidal concentrations.
:
Date sample collected: -�a-�--
Date samplQnal�zed
Laboratory Name: Porn �t� n�c ty+' cna L�hc€tr ��rrt s
Certification No. H R I z
PARAMETERS (Samples for metals were collected unfiltered�_YES _NO
and field adgi�led
COD
mg/I
/100ml
Nitrite (NO2) as N
Nitrate (NO3) as N
mg/I
Coliiorm: MF Fecal
Coliform: MF Total
A 00ml
Phosphorus: Total as P
mg11
(Note: Use MPN method for highly turbid samples)'
mg/I
A11
Aluminum
Al -Aluminum
t
- mg/I
Dissolved Solids: Total �—
pH (when analyzed) .5•U-7
.
units
ea - Barium
mg/I
mg/I
TOC
mg/I
mg/I
Ca - Calcium
Cd - Cadmium
Chloride
Arsenic
mg/I
Chromium: Total
mg/I
mg/I
Grease and Oils
mg/I
mg/I
Cu - Copper
Fe - Iron •
mgll
Phenol
Sulfate
mgll
UMhos
Hg --Mercury
K - Potassium
mg/I
mg/I
Specific Conductance
mg/I
Mg'- Magnesium
mg/I
Total Ammonia
TKN as N
mg/I
Mn - Manganese
mg/1
\/YES _NO)
Ni - Nickel mg/I
Pb - Learl mg/I
Zn - Zinc mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and ConcentrationUnits)
4uaILC15 1- DrchiocQc-i-nen - 43D
Cl IDn Ci-hene - 1100 ua I L
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes, X (1) No—.(0)
VOC GC.ms method# - $2L+D fl
method #
method#=
Permitlee (or Authorized Agenq Namo and Tltlo - Please print or typo _ i , ,,. I nip
nru_r a Rav AJAR

SUBMIT FORM ON yELLQA PAPER ONLY
or
Facility Name:_
Permit Name (if
Facility Address: ,rw, YlC 263� County
L(CRY) lour a Lcl Telephone #: � � � ��4 i5-'g in
Contact Person: Larr r
�} _ ay= MW No. of Wells to be Sampled. r1m erm,
Well Location/ Site Name: �o o ;r
� — For Groundwater Treatment Systems
Well Identification Number (from Per el : P _5 Cheek 0ne:
"& p ft. WeII Diameter: I" ❑Influent (98)
Well Depth: �� ftto
it.
Screened Interval: ft: below measuring point. ❑ Effluent (99)
Depth to Water Level: J1 R—n above land surface.
Measuring Point Is y
Gallons of water pumped/bailed before sampling: uMhos
Field analysts: pH 5r Specific Conductance
> 1 ^C Odor Appearance
EXP
PERMIT #: IRATION DATE: 11' o - o a
Non -Discharge
NPDES
TYPE OF PERM03 D OPERATION m dEI GlnlilOtraITOREDtion Gall . ery
Lagoon
Spray Field Remedladon:
Rotary Distributor Land Applicallon of $IudAg ri —
Other:
NOTE: Values should reflect dissolved and I
fV r i
colloidal concentrations.
5 Date sample aoalytecly
Date sample collected: pr
Laboratory Name:
CertiticationNo. � • ---
Temp. . . NO YES and field acidified
LJ�E
PARAMETERS (Samples for metals were bollected unfiltered mg/I
mg/I Nitrite (NO2) as N mg/I
COD /100m1 Nitrate (NO3) as N mg/I
Coliform: MF Fecal /100m1 Phosphorus: Total as mgll
Coliform: MF Total Orthophosphate mg/I
(Note: Use MPN method for highly turbid samples)' mg/I Al - Aluminum mg/I .
Dissolved Solids: Total K q l�units Ba - Barium mg/I
pH (when analyzed) mg/I Ca - Calcium mg/1
TOC mgll Cd - Cadmium mg/I
Chloride - mg/l Chromium: Total mg/I
Arsenic mg/I Cu - Copper mg/I
Grease and Oils mg/I Fe - Iron mg/l
Phenol mg/l Hg - Mercury -- mg/1
Sulfate uMhos K - Potassium mgll
Specific Conductance�� mg/I. Mg'_ Magnesium mg 11
Total Ammonia mg/I Mn - Manganese
TKN as N
_G.YES — NO) mg/I
Ni - Nickel mgll
Pb - Lea mg/l
Zn - Zinc mg/I
Ammonia Nitrogen
Other (Specify Compounds and Concentration Units)
by -a- ±heme 101 unlL
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach I Nrep=rt•)(0)
Report Attached? Yeses_( )D
VOC CSC : method #
method #
_: method # _�

SUBMIT FORM ON YELLOW PAPER ONLY
print Clearly or Type
Facility Name: S L- ,— P c Fcicil
Permit Name (if different):
263�_ ')l'.0-MW La
La t rin bwrnr s,a,al 1�1 County
ICAYI rr�l iPtrR Telephone#: 51 5 5
Contact Person:
tar - *1 4, 5s. �' No. o1 Wells to be Sampled:
Well Location/Site Name: 9„
Well Identification Number (from Permit): 1W-n I For Groundwater Treatment Systems
Well Depth: ' AT15 ft. Well Diameter: 2.0 in. I Check One:
Screened Interval: 1 7- ft. t9 -'s • V h• ❑Influent
Depth to, Water Level:115_ft. below measuring point. ❑Effluent
Measuring Point Is • li' ft. above land surface.
Gallons of water pumped/balled before sampling: y
Field analysis: pH 4.52 , Specific Conductance uMhos
Temp. 13 --4 - °C, Odor Appearance
PERMIT #: EXPIRATION DATE: I i- 30 -0 a
Non -Discharge W& 000.1-79g UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediallon:lnliNaliorLQallel!�
Spray Field Remediallon: — L'
Rotary Distributor Land Application of Sludge
__J\_ Other:
N -
(98) NOTE: Values should reflect dissolved and
colloidal concentrations. = =�
(99) o
Date sample collected: S O Date sample ahalyed�
Laboratory Name- PnrndIClm lJ_l11±CG9�ct YGltori-e5
Certification No. `'(•l I
PARAMETERS (Samples for metals were collected unflllered t✓ A YES _NO
and field acidified
COD
mg/I
Nitrite (NO2) as N
mg/I
mg/I
Coliform: MF Fecal
Coliform: MF Total
/100ml
/100ml
Nitrate (NO3) as N
Phosphorus: Total as P.
mg/I
(Note: Use MPH method for highly turbid samples(
Dissolved Solids: Total
mg/I
Orthophosphate
Al - Aluminum
mg/I
mg/I
pH (when analyzed) 5. 0 4
units
Ba - Barium
mg/I
mg/I
TOC
mg/ I
mg/l
Ca - Calcium
Cd - Cadmium
mg/I
Chloride
Arsenic
mg/I
Chromium: Total
mg/I
mg/I
Grease and Oils
mg/I
mg/I
Cu - Copper
Fe - Iron
mg/I
Phenol
Sulfate
mg/I
Hg --Mercury
mg/I
Specific Conductance
uMhos
mg/I
K - Potassium
Mg'- Magnesium
mg/I
Total Ammonia
TKN as N
mg/I
Mn - Manganese
mg/I
YES _ NO)
Ni - Nickel mg/I
Pb - Lead mg/I
Zn - Zinc mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
DichloPue, he.ne - 1-iu DaIL
Trir'hlomethene - �ISaILYI-
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
ReportAttached7 Yes_.&_(1) No_(0)
VOC GC' method # = le 0 l
method #
method #
r cu I—— I.. ..........
......, _......_..._ __. ..
GW-59 Rev. 4198

SUBMIT FORM ON YELLOW PAPER ONLY
SING � .,
Please Print Clearly or Type
___1,,,11_ r_.,.,l;t., PERMITM
Facility Name: Iau3T7nLL.
Permit Name (if different):
LcaCr, r) V)11 Y IL County
t l' LQvVU 1CLrht$1B1e1 tvvl Telephone #:(51D 4y5 V(a(Ola
Contact Person:. 3H° v�" 13
Well Location/Site Name: No. of Wells to be Sampled: rum arm I)
Lorin-'19-1-t' 4'7 .1"
Well IdentificationNumber(froinPermlt): 1AW-1 For Groundwater Treatment Systems
Well Depth: * 3 6 0 ft. Well Diameter:. -0 In. Check One:
Screened Interval: 15 11 ft. to 3 `i • O ft. ❑ Influent
Depth to Water Level: ft. below measuring point. ❑ Effluent
Measuring Point is -t • ,qu ft. above land surface.
Gallons of water pumped/bailed before sampling: 4
Field analysis: pH1$y , Specific Conductance uMhos
Temo. -1 0. 5 °C, Odor Appearance
DATE: II - -10- or}
NPDES
TyPF OF PERMITTED OPERATION BEING MONITBRED-
Lagoon Remedialion:Inliltra1I%GalleFy,
Spray Field Remedlatlon:
Rotary Distributor Land Application of Sltydge .,
�_ Other: tv
(98) NOTE: Values should reflect dissolved and
(99) colloidal concentrations. o
����''�����,.,,,'' c
Dale sample collected: ��-- Date sampid a'naI — d- i
Laboratory Name: on^'l e ++� it p m n m i -j pt N n I L0.Y
Certification No. 4 R t
PARAMETE$$ (Samples for metals were collected unfilteredl✓/a- YES _NO
and field acidified
COD
mg/I
Nitrite (NO2) as N
mg/I
mg/I
Coliform: MF Fecal
Coliform: MF Total
/100ml
/100ml
Nitrate (NO3) as N
Phosphorus: Total as P.
mgll
(Note: Use MPH method for highly turbid samples)
mg/I
Orthophosphate
AI - Aluminum
mg/1
mg/I
Dissolved Solids: Total
pH (when analyzed) 15• 3 P)
units
Ba - Barium
mg/I
mg/I
TOC
mg/l
mg/I
Ca - Calcium
Cd - Cadmium
mg/I
Chloride
Arsenic
mg/I
Chromium: Total
mg/I
mg/I
Grease and Oils
mg/I
mg/I
Cu - Copper
Fe - Iron '
mgll
Phenol
Sulfate
mg/l.
Hg --Mercury
mg/I
m9/I
Specific Conductance
uMhos
mg/I
K - Potassium
Mg'- Magnesium
Total Ammonia
TKN as N
mg/l
Mn - Manganese
mg/I
✓ YES _ NO)
Ni - Nickel mg/I
Pb - Lead mg/I
Zn - Zinc mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
Tel rar hloroe- ene - AgC0_ u c, I L
T✓4 .. I,.t...,. e1J..a v,o - I'sDOo U I L
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
ReportAttachedl Yes-9-0) No_(0)
VOC U` L : method # = La 01
method # _
methodit
Perminee (or Authorized Agent) Name and Title - Please print or type I t
GW-59 Rev. 4/98

SUBMIT FORM ON YELLOW PAPER ONLY
Please Print Clearly or
Facility Name:_
Permit Name (if
Ic"rl ' LLLYy�I LIfLYIZ'"' , "' Telephone.M
Contact Person:
LL' No. of Wells to be
Well Location/ Site Name: -, _ 7, _, . , ..
Well Identification Number(from'Permlt): AAVN/' 4 I For Groundwater Treatment Systems
Well Depth: 61 ft. Well Diameter:�;20 In. Check One:
Screened Interval: Q • 5 ft. to `25il)_ ft. ❑ Influent
Depth to Water Level: 1 • t ft. below measuring point. ❑ Effluent
Measuring Point is - ft. above land surface.
Gallons of water pumped/balled before sampling: 4
Field analysis: pH 151A . Specific Conductance uMhos
Temp. a I • U °C, Odor Appearance
PERMIT #: EXPIRATION DATE: 1 1 • a0 - Oa
Non -Discharge WQ W-0-1-ISS _UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITOREDn
Lagoon Remediallon:Infillratlortgallerl?
r,
Spray Field Remedlallon:
Rotary Distributor Land Application of SlAe s'
Other: r
(98) NOTE: Values should reflect dissolved and
(99) colloidal concentrations.
Date sample collected: Wa 4loo Date sampleanal zed:
Laboratory Name. lVb yn4` i 4ry n m 1, i {i c WL rtt i OYI Q 5
Certification No. 420
for metals were collected unfilteredy --YES _NO
and field acidified
PARAMETERS (Samples
mg/I
Nitrite (NO2) as N
COD
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P.
mglI
ll
(Note: Use MPN method for highly turbid samples)'
Dissolved Solids: Total
mg/I
Orthophosphate
Al - Aluminum
pH (when analyzed) y• q -1
units
Ba - Barium
mg/I
mg/I
TOC
mg/I
mg/l
Ca - Calcium
Cd - Cadmium
mg/I
Chloride
Arsenic
mg/I
Chromium: Total
mg/I
mg/I
Grease and Oils
mg/I
mg/I
Cu - Copper -
Fe - Iron
mg/I
Phenol
Sulfate
mg/I
Hg -.Mercury
mgll
mg/I
Specific Conductance
uMhos
mg/I
K - Potassium
Mg'- Magnesium
mg/I
Total Ammonia
TKN as N
mg/I
Mn - Manganese
mg/I
_YES _NO)
Ni - Nickel mg/I
Pb - Lead mg/I
Zn - Zinc mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
015- t� �1,- 71th(ofoe-H n�_
'TvichloYbe�l�leYle--11cuo�1.
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
ReportAttached? Yes_�Q1) NO_(0)
VOC GC method#= UOI
method # =
method # =
Perminee (or Authorized Agent) Name and 7IIle - Please print ar type — r
GW-59 Rev. 4198

PARAME19RS (samples for metals were collected un fete
mg/I Nitrite (NO2) as N
mg/1
COD
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/l
(Note: Use MPN method for highly turbid eamplesl
mg/1
Orthophosphate
At - Aluminum
mg/1
Dissolved Solids: Total
pH (when analyzed) ` 26
units
Ba - Barium
mg/I
mg/I
TOC
mg/ I
mg/ I
Ca - Calcium
Cd - Cadmium
mg/1
Chloride
Arsenic
mg/I
Chromium: Total
mg/I
mg/I
Grease and Oils
mg/1
mg/I
Cu - Copp&
Fe - Iron •
mg/I
Phenol
Sulfate
mg/l
Hg -,Mercury
mg/I
Specific Conductance
uMhos
mg/I
K - Potassium
Mg'- Magnesium
mg/I
Total Ammonia
TKN as N
mg/I
Mn - Manganese
mg/I
Facility Name:_
Permit Name (if
Well Location/ Site Name: -
SUBMIT FORM ON YELLOW PAPER ONLY
z g1a �ti, tale>u e r(OIVIS�OOF,}NATEgUU!(LT,j��1��saT o-T
(NG £y * GR6Qfl,D(r1ATEfj�5E T10t) PERMITS DCOI NCEUFttt
g ,W A g� �T d"F '4s
y{��a?�,•.�k RbLEIGN,Nb276269578iP.fione 919s733322)
Please Print Clearly or Type
PERMIT #: EXPIRATION DATE: I I - 3 0 - 0 3-
rtme pndui±5 Foci litU Non -Discharge V16 bm*l I q A UIC
County `I n nut
Telephone#:t5-
No. of Wells to be Sampled:
Well Identification Number (from Permit): I For Groundwater Treatment Systems
Well Depth: ft. Well Dlameter: . D in. Check One:
Screened Interval: . �. ft. to A 5 ft. ❑Influent (98)
Depth to Water Level: i I • ft. below measuring point. ❑ Effluent (99)
Measuring Point is > ,15 ft. above land surface.
Gallons of water pum ed/bailed before sampling: 'AField analysis: pH�— , Specific Conductance uMhos
Temp. 2 1 • i� °C, Odor Appearance
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remedialiom lnfiltrallon Gallery
Spray Field Remedlallon:
Rotary Distributor Land Application of SIT d1e c-
ci
NOTE: Values should reflect dissolved and
colloidal concentrations.
Date sample collected: rl=r+ Date
Laboratory Name: �I Y—m la a•+
Certification No. J'' B I
tit dsL�& YES NO and field acidified YES
N1- Nickel mg/I
Pb - Lead mg/I
Zn - Zinc mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
Cis-43 D(chlrrcP+hFn_ e =IO�IL
NO)
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method#. Attach lab report.)
ReportAttached? Yes-_X_(1) No _. (0)
VOC Cy method #= t.o01
method #=
method # _
Permillee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 4198

SUBMIT FORM ON YELLOW PAPER ONLY
Facility Name: --
Permit Name (if
Well Location/ Site Name:
m
County
Telephone MC21
No. of Wells to be
or Type
WeIlldentilicationNumber(iromPermit): W1W—rt For Groundwater Treatment Systems
Well Depth: �� °�• A ft. Well Diameter: 4.0 in. Check One:
Screened Interval: t, • tZ ' it. to 9/i - 0 ft. ❑ influent (98)
13.4 ft. below measuring point. ❑ _ (99)
Depth to Water Level: 9 P Effluent
Measuring Point is •�. 15 ft. above land surface.
Gallons of water pumped/bailed before sampling: 9 uMhos
Field analysis: pH— , Specific Conductance
Temp. I cf • -�1 °C, Odor Appearance
PERMIT M EXPIRATION DATE: i t• ;0 o a
Non -Discharge W& 000-119 S UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field Remediation:
Rotary Distributor Land Application of Sluc8e
Other:
..,� _-e,--� .rl.. ..I.,nd end �-O ''•r-•
colloidal concentrations. K) ='
Date sample collected:gJa4loo Date sample i palyzed'-
r rl I A rrl Q jt(l t lr I C[l 1 i 111�rt�
Laboratory Name:0.
Certification No. 49,1
c�
. , Pe kin end frald arldlflPri YES
PARAMETERS_ (Samples for metals were couecceu uruura,a.._u f u • --
mg/I Nitrite (NO2) as N
mg/I
COD
Coliform: MF Fecal
/100ml
/100ml
Nitrate (NO3) as N
Phosphorus: Total as P.
mg/I
mg/1
Coliform: MF Total
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Dissolved Solids: Total
mg/I
Al -Aluminum
mg/I
pH (when analyzed) • a y
units
mg/I
Ba - Barium
Ca -Calcium
mg/1
TOC
Chloride
mg/I
mg/I
Cd - Cadmium
Chromium: Total
mg/1
mg/I
Arsenic
Grease and Oils
mg/I
Cu -'Copper
mg/I
mg/I
Phenol
mg/I
mg/I
Fe - Iron •
Hg -Mercury
mg/I
Sulfate
Specific Conductance
whos
mg/I,
K -Potassium
Mg'- Magnesium
mg/I
Total Ammonia
TKN as N
mg/I
Mn - Manganese
mg/I
NO)
Ni- Nickel mg/I
Pb - Lead— mg/I
Zn - Zinc mg/I
Ammonia Nitrogen mg/I
Other (Specify Compounds and Concentration Units)
Tnrhlrrun+hPne - .240 tup JL
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes1(_(1) No—(0)
VOC GC M5 : method#= 8LUO 97
: method #
: method #
Permilleo (or Aulhodzed Agem) Name and Title -Please print or type ^ 1 n
GW-59 Rev. 4/98

SUBMIT FORM ON YELLOW PAPER ONLY
Please Print Clearly or Type
Facility Name:_
Permit Name (if
County rc r - ruLLA—
tcztd l§ierel (zip)3 d
Contact Person: Layvv CT V Telephone #:
Well Location/ Site Name: No. of Wells to be Sampled:
Well Identification Number (from Permit): Mom— For Groundwater Treatment Systems
Well Depth: Well Diameter: Q o In. Check One:
Screened Interval: 15, IV ft. to a ft- ❑ Influeni
Depth to Water Level: • 0 • 6 ft• below measuring point. ❑ Effluen'
Measuring Paint Is__.?. 5 ft. above land surface.
Gallons of water pumpedlbailed before sampling: uMhos
Field analysis: pH y.2a , Specific Conductance
Temp. 49,1 °C, Odor Appearance
PERMIT #: EXPIRATION DATE: I I - ao- o a
Non-Discharge`4G Lyy)-1199 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITOREil,
Lagoon, Rerhediallon: lnliltratlo%Galke k
Spray Field Remedlalion: n -
Rotary Distributor Land Application of SIAO
X Other: i
(98) NOTE: values should reflect dissolved and
(99) colloidal concentrations.
Date sample collected: 5 1,;LLA 100. Date samplee-4nalgaed: Laboratory Name: RrnrltaYY\ LL10.1)rftr 9 OraioYlfS
Certification No. °tk I
PARAMETERS (Samples for metals were collected unfiltered_Y/i-YES _NO
and field acidified
mg/i
COD
Coliform: MF Fecal
mg/I
J100ml
Nitrite (NO2) as N
Nitrate (1\103) as N
mg/I
mgll
Coliform: MF Total
/100ml
Phosphorus: Total as P
Orthophosphate
mg/I
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
Al - Aluminum
mg/I
pH (when analyzed) 5• N-
units
mg/I
Ba - Barium
Ca - Calcium
mg/I
TOC
Chloride
mg/I
mg/I
Cd - Cadmium
Chromium: Total
mg/I
mg/I
Arsenic
Grease and Oils
mg/I
Cu -Copper
mg/l
Phenol
mgll
mg/1
Fe -Iron
Hg --Mercury
mg/I
g
Sulfate
Specific Conductance
Umhos
mg/1
K - Potassium
Mg'- Magnesium
mg/I
mg/I
Total Ammonia
TKN as N
mg/I
Mn - Manganese
mg/I
YES _ NO)
Ni - Nickel
mg/I
Pb - Lead
mg/I
Zn - Zinc
mg/I
Ammonia Nitrogen
mg/I
Other (Specify Compounds and Concentration Units)
�Y(C1�10r�E W1eY1P
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? YeSl_(1) No _ (0)
VOID 4 �. _: method # _ )r D I
method # _
method #
Permiltee (or Authorized Agent) Name and TI'M - Please print or type —. t - r ^
GW-59 Rev.4/98

SUBMIT FORM ON FY -LLOW PAPER ONLY
please print Clearly or Type
Facility Name:
Permit Name (if different):
Facility Address:
LQurin12Wf hG a835a County
t��Y� 7 `late) (ZIP)
Contact Person: �n Clo rIL Telephone #: A-L
Lat•3voys,ow•3" No. of Wells to be
Well Location/ Site Name: ,„ , , q. .
Well Identification Number (from Permit): 11 1 3 For Groundwater Treatment Systems
Well Depth: ' s0.® ft. Well Diameter: ,_o In. Check One:
Screened Interval: a . o' It. to `D 0 ft. ❑ Influent (98)
Depth to Water Level: a A ti ft. below measuring point. ❑ Effluent (99)
Measuring Point is eft. above land surface.
Gallons of water pumped/bailed before sampling: y
Field analysis: pH y•52-' , Specific Conductance uMhos
Temp. 253__°C,OdorAppearance
PERMIT #: EXPIRATION DATE:.) 1- _40-C2-
Non-Discharge Wa rIOD-1-196UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONI%RE[S
Lagoon Remedialion:lnfiltratiffinl3allery
Spray Field Remedlallon: ro
Rotary Distributor Land Application of Siydge
7X Other: N -
NOTE: Values should reflect dissolved and Z5 - r
colloidal concentrations.
ni
Date sample collected: 5 124U Date sampl&dnalped:
Laboratory Name: rnd t ' M R n (i+t��i i LQ t7L7�rCl tout e
Certification No.
PARAMETER$ (Samples for metals were collected unfiltered_"YES _NO
and field acidified
COD
mg/I
/100ml
Nitrite (NO2) as N
Nitrate (NO3) as N
mg/1
Coliform: MF Fecal
Coliform:'MF Total
/100m1
Phosphorus: Total as P.
mg/1
mg/1
(Note: Use MPN method for highly turbid samples)'
mg/I
Orthophosphate
Al - Aluminum
mg/I
Dissolved Solids: Total
pH (when analyzed) 5. 35
units
Ba - Barium
mg/l
mg/l
TOC
mg/ I
mg/I
Ca - Calcium
Cd - Cadmium
mgll
Chloride
Arsenic
mg/l
Chromium: Total
mg/1
mg/I
Grease and Oils
mg/I
mg/l
Cu - Copper
Fe - Iron
_
g/1
Phenol
Sulfate
mgll
Hg -Mercury
mg
mg/Total
Specific Conductance
uMhos
mg/I
K - Potassium -
Mg,- Magnesium
Total Ammonia
TKN as N
mg/I
Mn - Manganese
mg/I
.YES
_ NO)
Ni - Nickel
mg/1
Pb - Lead
mg/I
mg/I
Zn - Zinc
Ammonia Nitrogen mg/l
Other (Specify
Compounds and Concentration Units)
�T,; nhIcIr„a-Hnune
RP)ILq IL
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes_-,Q1) No _ (0)
VOC Go- method # -fit o 1
method #
method # _
Permitlee (or Authorized Agent) Name and Titlo - Please print or type ^ t ^
GW-59 Rev. 4198

SUBMIT FORM ON YELLOW PAPER ONLY
Clearly or Type
Facility Name: -
Permit Name (if
I_QCL,r1 e County
Judy) #:hone Telephone Jsrai0) lap) -7 445 -
Contact Person: P (s �
La -ova 4V No. of Wells to be Sampled:
Well Location/ Site Name: o, , , „o ,_ - P
Well ldentificalionNumber (from Permit):_MVJ-14 I For Groundwater Treatment Systems
Well Depth: 10.0 ft. Well Diameter: y •b In. Check One:
Screened Interval: 6.0 ft. to 3o, 0 ft. ❑ Influent (98)
Depth to Water Level:l_it. below measuring point. ❑ Effluent (99)
Measuring Point is 3. ;to ft. above land surface.
Gallons of water pumped/bailed before sampling: 4
Fieldanalysis: pH-•5•o2 , Specific Conductance uMhos
Temp. =L 3. :jL aC, Odor Appearance
PERMIT#: EXPIRATION DATE: 11-.90-oa.
Non -Discharge W Q 000-1191 P, UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery,
Spray Field Remediallon: _o ' `=
Rotary Distributor Land Application of Sludge
Other: -a
NOTE: Values should reflect dissolved and N '
colloidal concentrations. _v ;
Date sample collected: ` aup Date sampleZAalyiWi
LaboratoryName: Pn rQGttQn rAYrLI�+i tca l-4.ct.V�7im-Ircne
Certification No. t{ E3)
x
PARAMETERS (Samples for metals were collected unfiltered-9�LYES _NO and field acidified
COD mg/I Nitrite (NO2) as N mg/I
Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I
Coliform: MF Total /100ml Phosphorus: Total as P mg/I
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed) 5. 113
units
TOC
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/l
TKN as N
mg/I
Aln Aluminum te
m/I
)mg
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron •
mg/I
Hg -.Mercury
mg/I
K - Potassium
mg/I
Mg'- Magnesium
mg/I
Mn - Manganese
mg/I
-/YES _NO)
NI - Nickel mg/I
Pb - Lead mg/I
Zn - Zinc mg/I
Ammonia Nitrogen mg/I
Other (SpecilyCompounds and Concentration Units)
c Is- DJChic
rue-+hene - 3ua
Trtchloruei-hPne — laua I _
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes__�L(1) No_(0)
VOC Cr, : method # = too t
: method # =
: method # =
rermelee tur humunceu muuin) rvaiim auu , nia -„ u ., r"'• w• ur-
GW-59 Rev. 4/98

APPENDIX V
LABORATORY ANALYTICAL RESULTS

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
-
by GC 601
Client Sample ID: MW-1
Analyzed By:
EKR
Client Project ID: Laurinburg Groundwater Monitoring Wells
Date Collected:
05/24/00
Lab Sample ID: 88451
Date Received:
05/26/00
Lab Project ID: G420-2
Matrix:
Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
- Bromodichloromethane
6/7/00
1
1
BQL
Bromoform
6/7/00
1
2
BQL
,- Bromomethane
6/7/00
1
2
BQL
_ Carbon tetrachloride
6/7/00
1
1
BQL
Chlorobenzene
6/7/00
1
1
BQL
Chloroethane
6/7/00
1
1
BQL
Chloroform
6/7/00
1
1
BQL
Chloromethane
6/7/00
1
1
BQL
Dibromochloromethane
617/00
1
1
BQL
1,2-Dibromoethane (EDB)
6/7/00
1
1
BQL
1,2-Dichlorobenzene
6/7/00
1
1
BQL
1,3-Dichlorobenzene
6/7/00
1
1
BQL
1,4-Dichlorobenzene
617100
1
1
BQL
1,1-Dichloroethane
6/7100
1
1
BQL
,z 1,2-Dichloroethane
6/7/00
1
1
BQL
1,1-Dichloroethene
6/7/00
1
1
BQL
cis-1,2-Dichloroethene
6/7/00
1
1
BQL
trans-1,2-Dichloroethene
6/7/00
1
1
BQL
1,2-Dichloropropane
6/7/00
1
1
BQL
cis-1,3-Dichloropropene
6/7100
1
1
BQL
trans-1,3-Dichloropropene
6/7/00
1
1
BQL
Methylene Chloride
6/7/00 '
1
5
BQL
1,1,2,2-Tertrachloroethane
6/7/00
1
1
BQL
Tetrachloroethene
6/7/00
1
1
BQL
1,1,1-Trichloroethane
617/00
1
1
BQL
1,1,2-Trichloroethane
6/7/00
1
1
BQL
Trichloroethene
6/7/00
1
1
Trichlorofluoromethane
617/00
1
1
j
BQL
Vinyl Chloride
6/7/00
1
1
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
41
102
Comments:
All values corrected for dilution.
Flags:
BQL = Below quantitation limit.
Reviewed By:
Pa 1 of 1
North Carolina Vastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Client Sample ID: MW-2
Analyzed By:
EKR
Client Project ID: Laurinburg Groundwater Monitoring Wells
Date Collected:
05/24/00
Lab Sample ID: 88450
Date Received:
05/26/00
Lab Project ID: G420-2
Matrix:
Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
6/7/00
50
50
BQL
Bromoform
617/00
50
100
BQL
,—
Bromomethane
6/7/00
50
100
BQL
_
Carbon tetrachloride
617/00
50
50
BQL
Chlorobenzene
6/7/00
50
50
BQL
Chloroethane
6/7/00
50
50
BQL
Chloroform
6/7/00
50
50
BQL
Chloromethane
6/7/00
50
50
BQL
Dibromochloromethane
6/7/00
50
50
BQL
_
1,2-Dibromoethane (EDB)
6/7/00
50
50
BQL
1,2-Dichlorobenzene
6/7/00
50
50
BQL
1,3-Dichlorobenzene
6/7/00
50
50
BQL
1,4-Dichlorobenzene
6/7/00
50
50
BQL
1,1-Dichloroethane
6/7/00
50
50
BQL
1,2-Dichloroethane
6/7/00
50
50
BQL
1,1-Dichloroethene
6/7/00
50
50
BQL
cis-1,2-Dichloroethene
6/7/00
50
50
BQL
trans-1,2-Dichloroethene
6/7/00
50
50
BQL
1,2-Dichloropropane
6/7/00
50
50
BQL
cis-1,3-Dichloropropene
6/7/00
50
50
BQL
trans-1,3-Dichloropropene
6/7/00
50
50
BQL
Methylene Chloride
6/7/00 '
50
250
BQL
1,1,2,2-Tertrachloroethane
6/7/00
50
50
BQL
Tetrachloroethene
6/7/00
50
50
BQL
1,1,1-Trichloroethane
6/7/00
50
50
BQL
1,1,2-Trichloroethane
6/7/o0
50
50
BQL
Trichloroethene
6/7/00
50
50
850
Trichlorotluoromethane
6/7/00
50
50
BQL
Vinyl Chloride
6/7/00
50
50
gQL
N
Surrogate Spike Recoveries
SpikeAl
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
45
111
Comments:
Flags
All values corrected for dilution.
BQL = Below quantitation limit.
Reviewed By: 1yvr�
L North Carolina wastoewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
to
1,
Comments:
Flags:
Client Sample ID: MW-3 Analyzed By: EKR
Client Project ID: Laurinburg Groundwater Monitoring Wells Date Collected: 05/24/00
Lab Sample ID: 88449 Date Received: 05/26/00
Lab Project ID: G420-2 Matrix: Water
Compound Date Quantitation Result
Analyzed Dilution Limit (ug/L) (ug/L)
Bromodichloromethane
6/7/00
4
4
Bromoform
6/7/00
4
8
Bromomethane
6/7/00
4
8
Carbon tetrachloride
617/00
4
4
Chlorobenzene
6/7/00
4
4
Chloroethane
6/7/00
4
4
Chloroform
617/00
4
4
Chloromethane
6/7/00
4
4
Dibromochloromelhane
6/7/00
4
4
1,2-Dibromoethane (EDB).
6/7/00
4
4
1,2-Dichlorobenzene
6/7/00
4
4
1,3-Dichlorobenzene
6/7100
4
4
1,4-Dichlorobenzene
6/7100
4
4
1,1-Dichloroethane
6/7/00
4
4
1,2-Dichloroethane
6/7/00
4
4
1,1-Dichloroethene
6/7/00
4
4
cis-1,2-Dichloroethene
6/7/00
4
4
trans-1,2-Dichloroethene
6/7100
4
4
1,2-Dichloropropane
6/7100
4
4
cis-1,3-Dichloropropene
6/7/00
4
4
trans-1,3-Dichloropropene
617/00
4
4
Methylene Chloride
6/7/00
4
20
1,1,2,2-Tertrachloroethane
6/7/00
4
4
Tetrachloroethene
6/7/00
4
4
1,1,1-Trichloroethane
6/7/00
4
4
1,1,2-Trichloroethane
6/7/00
4
4
Trichloroethene
6/7/00
4
4
Trichlorofluoromethane
6/7/00
4
4
Vinyl Chloride
6/7/00
4
4
Surrogate Spike Recoveries
Spike
Spike
Added
Result
1,4-Dichlorobutane
40
43
All values corrected for dilution.
BQL = Below quantitation limit.
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
rl
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
57
BQL
BQL
Percent
Recovered
108
Reviewed By:
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Method 601 Volatiles
by GCMS 8260E
Client Sample ID: MW-4 Date Analyzed: 6/7/00
Client Project ID: Laurinburg Groundwater Monitoring W Analyzed By: EKR
Lab Sample ID: 88448 Date Collected: 5124/00
Lab Project ID: G420-2 Date Received: 5/26/00
Matrix: Water Dilution: 80
Compound
Quantitation
Limit (ug/L)
Bromodichloromethane
80
Bromoform
80
Bromomethane
80
Carbon tetrachloride
80
_ Chlorobenzene
S0
Chloroethane
80
Chloroform
80
Chloromethane
80
Dibromochloromethane
80
1,2-Dibromoethane (EDB)
80
1,2-Dichlorobenzene
80
1,3-Dichlorobenzene
80
_ 1,4-Dichlorobenzene
80
1,1-Dichloroethane
80
1,1-Dichloroethene
80
• 1,2-Dichloroethane
80
cis-1,2-Dichloroethene
80
trans-1,2-dichloroethene
80
_ 1,2-Dichloropropane
80
cis-1,3-Dichloropropene
80
trans-1,3-Dichloropropene
80
Methylene chloride
400
1,1,2,2-Tetrachloroethane
80
Tetrachloroethene
80
Trichloroethene
80
1,1,1-Trichloroethane
80
1,1,2-Trichloroethane
80
Trichlorofluoromethane
80
Vinyl chloride
80
Surrogate Spike Recoveries
Spike
Added
Compound
(ug/L)
Bromofluorobenzene
10
1,2-Dichloroethane-d4
10
Toluene-d8
10
Comments:
All results are corrected for dilution.
9
Flags: BQL = Below Quantitation Limit
Surrogate
Result
(ug/L)
10.0
10.0
9.9
Result
(ug/L)
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
430
BQL
BQL
BQL
BQL
BQL
BQL
BQL
1100
BQL
BQL
BQL
BQL
%Rec
100
100
99
Reviewed by: MT\
North Carolina Wastewater Certification #481
Page 1 of 1

PARADIGM A ORATORIES, INC.
for Vo LABORATORIES,
Results
es
by GC 601
Client Sample ID: MW-5
Analyzed By:
EKR
Client Project ID: Laudnburg Groundwater Monitoring Wells
111
Date Collected:
05/24/00
Lab Sample ID: 88447
Date Received:
05126/00
Lab Project ID: G420-2
Matrix:
Water
Compound
Date
Quantitation
Result
Analyzed Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
6/7/00
50
50
BQL
l Bromoform
6/7/00
50
100
BQL
- Bromomethane
6/7/00
50
100
BQL
Carbon tetrachloride
6/7/00
50
50
BQL
l Chlorobenzene
6/7/00
50
50
BQL
Chloroethane
6/7/00
50
50
BQL
Chloroform
6/7/00
50
50
BQL
Chloromethane
6/7/00
50
50
BQL
Dibromochloromethane
6/7/00
50
50
BQL
1,2-Dibromoethane (ED13).
6/7/00
50
50
BQL
1,2-Dichlorobenzene
6/7/00
50
50
BQL
1,3-Dichlorobenzene
6/7/00
50
50
BQL
1,4-Dichlorobenzene
6/7/00
50
50
BQL
1,1-Dichloroethane
6/7/00
50
50
BQL
1,2-Dichloroethane
6/7100
50
50
BQL
1,1-Dichloroethene
6/7/00
50
50
BQL
cis-1,2-Dichloroethene
6/7/00
50
50
BQL
trans-1,2-Dichloroethene
6/7/00
50
50
BQL
1,2-Dichloropropane
6/7/00
50
50
BQL
cis-1,3-Dichloropropene
6/7/00
50
50
BQL
trans-1,3-Dichloropropene
617/00
50
50
BQL
Methylene Chloride
6/7/00 '
50
250
BQL
1.1,2,2-Tertrachloroethane
6/7/00
50
50
Tetrachloroethene
0/00
50
50
gQL
1, 1. 1 -Trichloroethane
6/7/00
50
50
BQL
• 1,1,2-Trichloroethane
6/7/00
50
50
BQL
Trichloroethene
6/7/00
50
50
BQL
Trichlorofluoromethane
6/7/00
50
50
610
Vinyl Chloride
6/7/00
50
50
BQL
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
44
110
Comments:
All values corrected for dilution.
Flags:
BQL = Below quantitation limit.
�
Page 1 of 1 Reviewed By:
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Client Sample ID: MW-6
Analyzed By:
EKR
Client Project ID: Laurinburg Groundwater Monitoring wells
Date Collected:
05/24/00
Lab Sample ID: 88446
Date Received:
05/26/00
Lab Project ID: G420-2
Matrix:
Water
Compound
I
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
6/7/00
100
100
BQL
Bromoform
6/7/00
100
200
BQL
Bromomethane
6/7100
100
200
BQL
Carbon tetrachloride
6/7/00
100
100
BQL
Chlorobenzene
6/7/00
100
100
BQL
Chloroethane
6/7/00
100
100
BQL
Chloroform
6/7/00
100
100
BQL
Chloromethane
6/7/00
100
100'
BQL
Dibromochloromethane
6/7/00
100
100
BQL
1,2-Dibromoethane (EDB)
6/7/00
100
100
BQL
1,2-Dichlorobenzene
6/7/00
100
100
BQL
1,3-Dichlorobenzene
6/7/00
100
100
BQL
1,4-Dichlorobenzene
6/7/00
100
100
BQL
1,1-Dichloroethane
6/7/00
100
1p0
BQL
1,2-Dichloroethane
617/00
100
100
BQL
1,1-Dichloroethene
6/7/00
100
100
BQL
cis-1,2-Dichloroethene
6/7/00
100
100
170
trans-1,2-Dichloroethene
6/7/00
100
100
BQL
1,2-Dichloropropane
6/7/00
100
100
BQL
cis-1,3-Dichloropropene
6/7/00
100
100
BQL
trans-1,3-Dichloropropene
6/7/00
100
100
BQL
Methylene Chloride
617/00 '
100
500
BQL
1,1,2,2-Tertrachloroethane
6/7/00
100
100
BQL
Tetrachloroethene
6/7100
100
100
BQL
1,1,1-Trichloroethane
617/00
100
100
BQL
1,1,2-Trichloroethane
6/7/00
100
100
BQL
Trichloroethene
6/7/00
100
100
Trichlorofluoromethane
6/7/00
100
100
950
Vinyl Chloride
6/7/00
.100
100
BQL
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
45
112
Comments
Flags:
All values corrected for dilution.
BQL = Below quantitation limit.
Reviewed By:_Lir,L
!, North Carolinaastewater Certification #481

PARADIGM A-Resul a for Vole $ORATORIES, INC.
es
by GC 601
Client Sample ID: MW-7 Analyzed By: EKR
Client Project ID: Laurinburg Groundwater Monitoring Wells Date Collected: 05/24/00
Lab Sample ID: 88445 Date Received: 05/26/00
Lab Project ID: G420-2 Matrix: Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
6/7/00
1000
1000
BQL
Bromoform
617/00
1000
2000
BQL
Bromomethane
617/00
1000
2000
BQL
Carbon tetrachloride
6/7/00
1000
1000
BQL
Chlorobenzene
617/00
1000
1000
BQL
- Chloroethane
6/7/00
1000
1000
BQL
Chloroform
6/7/00
1000
1000
BQL
Chloromethane
6/7/00
1000
1000
BQL
Dibromochloromethane
6/7/00
1000
1000
BQL
1,2-Dibromoethane (EDB)
6/7/00
1000
1000
BQL
1,2-Dichlorobenzene
6/7/00
1000
1000
BQL
_ 1,3-Dichlorobenzene
6/7/00
1000
1000
BQL
1,4-Dichlorobenzene
6/7/00
1000
1000
BQL
1,1-Dichloroethane
6/7/00
1000
1000
BQL
1,2-Dichloroethane
6/7/00
1000
1000
BQL
1,1-Dichloroethene
6/7100
1000
1000
BQL
cis-1,2-Dichloroethene
6/7/00
1000
1000
BQL
trans-1,2-Dichloroethene
6/7/00
1000
1000
BQL
1,2-Dichloropropane
6/7/00
1000
1000
BQL
cis-1,3-Dichloropropene
6/7/00
1000
1000
BQL
trans-1,3-Dichloropropene
6/7100
1000
1000
BQL
Methylene Chloride
6/7/00
1000
5000
BQL
1,1,2,2-Tertrachloroethane
6/7/00
1000
1000
BQL
Tetrachloroethene
6/7/00
1000
1000
2900
1,1,1-Trichloroethane
6/7/00
1000
1000
BQL
1,1,2-Trichloroethane
6/7/00
1000
1000
BQL
Trichloroethene
6/7100
1000
1000
15000
Trichlorofluoromethane
6/7/00
1000
1000
BQL
Vinyl Chloride
6/7/00
.1000
1000
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
Comments:
Flags:
1,4-Dichlorobutane 40 45 113
All values corrected for dilution.
BQL = Below quantitation limit.
Reviewed By: h r,
1 Page 1 of 1
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Comments:
Flags:
Client Sample ID: GT-9
Analyzed By: EKR
Client Project ID: Laurinburg Groundwater Monitoring Wells
Date Collected:
05/24/00
Lab Sample ID: 88444
Date Received:
05/26/00
Lab Project ID: G420-2
Matrix:
Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
6/6/00
5
5
BQL
Bromoform
6/6/00
5
10
BQL
Bromomethane
6/6/00
5
10
BQL
Carbon tetrachloride
6/6/00
5
5
BQL
Chlorobenzene
6/6/00
5
5
BQL
Chloroethane
6/6/00
5
5
BQL
Chloroform
6/6/00
5
5
BQL
Chloromethane
6/6/00
5
5
BQL
Dibromochloromethane
616/00
5
5
BQL
1,2-Dibromoethane (EDB)
6/6/00
5
5
BQL
1,2-Dichlorobenzene
6/6/00
5
5
BQL
1,3-Dichlorobenzene
6/6/00
5
5
BQL
1,4-Dichlorobenzene
6/6/00
5
5
BQL
1,1-Dichloroethane
6/6100
5
5
BQL
1,2-Dichloroethane
6/6/00
5
5
BQL
1,1-Dichloroethene
616/00
5
5
BQL
cis-1,2-Dichloroethene
6/6100
5
5
7
trans-1,2-Dichloroethene
6/6/00
5
5
BQL
1,2-Dichloropropane
6/6/00
5
5
BQL
cis-1,3-Dichloropropene
6/6/00
5
5
BQL
trans-1,3-Dichloropropene
6/6/00
5
5
BQL
Methylene Chloride
6/6/00
5
25
BQL
1,1,2,2-Tertrachloroethane
6/6100
5
5
BQL
Tetrachloroethene
6/6/00
5
5
BQL
1,1,1-Trichloroethane
6/6/00
5
5
BQL
1,1,2-Trichloroethane
6/6/00
5
5
BQL
Trichloroethene
6/6/00
5
5
76
Trichlorofluoromethane
6/6/00
5
5
BQL
Vinyl Chloride
6/6100
5
5
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
45
112
All values corrected for dilution.
BQL = Below quantitation limit.
Reviewed By: yr p
North Carolina-WaMewater Certification #481

PARADIGM AV subs for V LABlatileO�RATORIES, INC.
by GC sot
Comments:
Flags:
Client Sample ID: GT-10
Analyzed By:
EKR
Client Project ID: Laurinburg Groundwater Monitoring Wells
Date Collected:
05/24/00
Lab Sample ID: 88443
Date Received:
05/26/00
Lab Project ID: G420-2
Matrix:
Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
6/7/00
2
2
BQL
Bromoform
6/7100
2
4
BQL
Bromomethane
6/7/00
2
4
BQL
Carbon tetrachloride
6/7/00
2
2
BQL
Chlorobenzene
6/7/00
2
2
BQL
Chloroethane
6/7/00
2
2
BQL
Chloroform
6/7/00
2
2
BQL
Chloromethane
6/7/00
2
2
BQL
Dibromochloromethane
6/7/00
2
2
BQL
1,2-Dibromoethane (EDB).
6/7/00
2
2
BQL
1,2-Dichlorobenzene
6/7100
2
2
BQL
1,3-Dichlorobenzene
6/7/00
2
2
BQL
1,4-Dichlorobenzene
6/7100
2
2
BQL
1,1-Dichloroethane
6/7/00
2
2
BQL
1,2-Dichloroethane
6/7/00
2
2
BQL
1,1-Dichloroethene
6/7/00
2
2
cis-1,2-Dichloroethene
6/7/00
2
2
BQL
trans-1,2-Dichloroethene
6/7/00
2
2
6
1,2-Dichl6ropropane
6/7/00
2
BQL
cis-1,3-Dichloropropene
617/00
2
2
2
BQL
trans-1,3-Dichloropropene
6/7/00
2
2
BQL
Methylene Chloride
6/7/00
2
10
BQL
1,1,2,2-Tertrachloroethane
6/7100
2
2
BQL
Tetrachloroethene
617100
2
2
BQL
1,1,1-Trichloroethane
6/7/00
2
2
BQL
1,1,2-Trichloroethane
6/7/00
2
2
BQL
Trichloroethene
6/7/00
2
2
BQL
Trichlorofluoromelhane
6/7/00
2
2
27
Vinyl Chloride
6/7/00
2
2
BQL
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
45
114
All values corrected for dilution.
BQL = Below quantitation limit.
PReviewed By: �
Pa e1of1
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES,
INC.
Results for Method 601 Volatiles
by GCMS 6260B
Client Sample ID: GT-11
Date Analyzed:
617/00
Client Project ID: Laurinburg Groundwater Monitoring W Analyzed By:
EKR
Lab Sample ID: 88442
Date Collected:
5/2410D
Lab Project ID: G420-2
Date Received:
5/26/00
Matrix: Water
Dilution:
20
Compound
Quantitation
Result
Limit (ug/L)
(ug/L)
Bromodichloromelhane
20
BQL
Bromoform
20
BQL
Bromomethane
20
BQL
Carbon tetrachloride
20
BQL
Chlorobenzene
20
BQL
Chloroethane
20
BQL
Chloroform
20
BQL
Chloromethane
20
BQL'
Dibromochloromethane
20
BQL
1,2-Dibromoethane (EDB)
20
BQL
1,2-Dichlorobenzene
20
BQL
1,3-Dichlorobenzene
20
BQL
1,4-Dichlorobenzene
20
BQL
1,1-Dichloroethane
20
BQL
1,1-Dichloroethene
20
BQL
1,2-Dichloroethane
20
BQL
cis-1,2-Dichloroethene
20
BQL
trans-1,2-dichloroethene
20
BQL
1,2-Dichloropropane
20
BQL
cis-1,3-Dichloropropene
20
BQL
trans-1,3-Dichloropropene
20
BQL
Methylene chloride
100
BQL
1,1,2,2-Tetrachloroethane
20
BQL
Tetrachloroethene
20
Trichloroethene
20
BQL
1. 1, 1 -Trichloroethane
20
240
1,1,2-Trichloroethane
20
BQL
Trichlorofluoromethane
20
BQL
Vinyl chloride
20
BQL
BQL
Surrogate Spike Recoveries
Spike
Surrogate
Compound
Added
Result
%Rao
(ug/L)
(ug/L)
Bromofluorobenzene
10
10.7
107
1,2-Dichloroethane-d4
10
10.1
101
Toluene-d8
10
9.9
99
Comments:
All results are corrected for dilution.
Reviewed by:yvyr,
J
Flags: BQL = Below Quantitation Limit
North Carolina Wastewater Certification #481
Page 7 of 7

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Comments:
Flags:
Client Sample ID: GT-12
Analyzed By: EKR
Client Project ID: Laudnburg Groundwater Monitoring wells
Date Collected:
05/24/00
Lab Sample ID: 88441
Date Received:
05/26/00
Lab Project ID: G420-2
Matrix:
Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
6/7100
10
10
BQL
Bromoform
6/7/00
10
20
BQL
Bromomethane
617/00
10
20
BQL
Carbon tetrachloride
6/7/00
10
10
BQL
Chlorobenzene
6/7/00
10
10
BQL
Chloroethane
6/7100
10
10
BQL
Chloroform
6/7/00
10
10
BQL
Chloromethane
6/7/00
10
10
BQL
Dibromochloromethane
6/7/00
10
10
BQL
1,2-Dibromoethane (EDB).
617/00
10
10
BQL
1,2-Dichlorobenzene
6/7100
10
10
BQL
1,3-Dichlorobenzene
6/7/00
10
10
BQL
1,4-Dichlorobenzene
6/7/00
10
10
BQL
1,1-Dichloroethane
6/7/00
10
10
BQL
1,2-Dichloroethane
617/00
10
10
BQL
1,1-Dichloroethene
6/7100
10
10
BQL
cis-1,2-Dichloroethene
6/7/00
10
10
BQL
trans-1,2-Dichloroethene
6/7/00
10
10
BQL
1,2-Dichloropropane
617/00
10
10
BQL
cis-1,3-Dichloropropene
6/7/00
10
10
BQL
trans-1,3-Dichloropropene
6/7/00
10
10
BQL
Methylene Chloride
6/7/00
10
50
BQL
1,1,2,2-Tertrachloroethane
6/7/00
10
10
BQL
Tetrachloroethene
617100
10
10
BQL
1,1,1-Trichloroethane
6/7100
10
10
BQL
1,1,2-Trichloroethane
6/7/00
10
10
BQL
Trichloroethene
617/00
10
10
130
Trichlorofluoromethane
6/7/00
10
10
BQL
Vinyl Chloride
6/7/00
10
10
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
45
114
All values corrected for dilution.
BQL = Below quantitation limit.
Reviewed By: Mom=_
North Carolina Masiewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Comments:
Flags:
Client Sample ID: GT-13
Analyzed By:
EKR
Client Project ID: Laurinburg Groundwater Monitoring
Wells
Date Collected:
05/24/00
Lab Sample ID: 88440
Date Received:
05/26/00
Lab Project ID: G420-2
Matrix:
Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
6/7/00
8
8
BQL
Bromoform
6/7/00
8
16
BQL
Bromomethane
6/7/00
8
16
BQL
Carbon tetrachloride
6/7/00
8
8
BQL
Chlorobenzene
6/7/00
8
8
BQL
Chloroethane
6/7/00
8
8
BQL
Chloroform
6/7/00
8
8
BQL
Chloromethdne
6/7/00
8
8
BQL
Dibromochloromethane
6/7/00
8
8
BQL
1,2-Dibromoethane (EDI3).
6/7/00
8
8
BQL
1,2-Dichlorobenzene
6/7/00
8
8
BQL
1,3-Dichlorobenzene
6/7/00
8
8
BQL
1,4-Dichlorobenzene
6/7/00
8
8
BQL
1,1-Dichloroethane
6/7/00
8
8
BQL
1,2-Dichloroethane
6/7/00
8
8
BQL
1,1-Dichloroethene
6/7/00
8
8
BQL
cis-1,2-Dichloroethene
6/7/00
8
8
BQL
trans-1,2-Dichloroethene
6/7/00
8
8
BQL
1,2-Dichloropropane
6/7/00
8
8
BQL
cis-1,3-Dichloropropene
6/7/00
8
8
BQL
trans-1,3-Dichloropropene
6/7/00
8
8
BQL
Methylene Chloride
6/7/00 '
8
40
BQL
1,1,2,2-Tertrachloroethane
6/7/00
8
8
BQL
Tetrachloroethene
6/7100
8
8
BQL
1,1,1-Trichloroethane
6/7/00
8
8
BQL
1,1,2-Trichloroethane
6/7100
8
8
BQL
Trichloroethene
6/7/00
8
8
Trichlorofluoromethane
6/7/00
8
8
88
BQL
Vinyl Chloride
6/7/00
8
8
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
45
112
All values corrected for dilution.
BQL = Below quantitation limit.
Reviewed By: ri r,
North CarolinaaWastewater Certification #481

PARADIGM AJeSull IfoAr VolatieORATORIE5, INC.
by GC 601
Comments:
Client Sample ID: GT-14
Analyzed By:
EKR
Client Project ID: Laurinburg Groundwater Monitoring Wells
Date Collected:
05/24/00
Lab Sample ID: 88439
Date Received:
05/26/00
Lab Project ID: G420-2
Matrix:
Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug1L)
(ug/L)
Bromodichloromethane
6/6100
1
1
BQL
Bramoform
6/6/00
1
2
BQL
Bromomethane
6!6l00
1
2
BQL
Carbon tetrachloride
6/6/00
1
1
BQL
Chlorobenzene
6/6/00
1
1
BQL
Chloroethane
6/6/00
1
1
BQL
Chloroform
6/6/00
1
1
BQL
Chloromethane
6/6/00
1
1
BQL
Dibromochloromethane -
6/6100
1
1
BQL
1,2-Dibromoethane (EDB)
6/6/00
1
1
BQL
1,2-Dichlorobenzene
616/00
1
1
BQL
1,3-Dichlorobenzene
6/6/00
1
1
BQL
1,4-Dichlorobenzene
616100
1
1
BQL
1,1-Dichloroethane
6/6/00
1
1
BQL
1,2-Dichloroethane
6/6/00
1
1
BQL
1,1-Dichloroethene
6/6/00
1
1
BQL
cis-1,2-Dichloroethene
6/6/00
1
1
3
trans-1,2-Dichloroethene
6/6100
1
1
BQL
1,2-Dichloropropane
6/6/00
1
1
BQL
cis-1,3-Dichloropropene
6/6/00
1
1
BQL
trans-1,3-Dichloropropene
6/6/00
1
1
BQL
Methylene Chloride
6/6/00 '
1
5
BQL
1,1,2,2-Tertrachloroethane
6/6/00
1
1
BQL
Tetrachloroethene
616100
1
1
BQL
1,1,1-Trichloroethane
6/6/00
1
1
BQL
1,1,2-Trichloroethane
6/6/00
1
1
BQL
Trichloroethene
6/6/00
1
1
12
Trichlorofluoromethane
6/6/00
1
1
BQL
Vinyl Chloride
6/6/00
1
1
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
45
112
All values corrected for dilution.
Flags:
BQL = Below quantitation limit.
Reviewed By: �y
Page 1of1
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Client Sample ID: Influent
Analyzed By:
EKR
Client Project ID: Laurinburg Groundwater Monitoring Wells
Date Collected:
05/24/00
Lab Sample ID: 88453
Date Received:
05/26/00
Lab Project ID: G420-2
Matrix:
Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
6/7/00
50
50
BQL
Bromoform
6/7100
50
100
BQL
_ Bromomethane
617/00
50
100
BQL
_ Carbon tetrachloride
6/7/00
50
50
BQL
Chlorobenzene
6/7/00
50
50
BQL
Chloroethane
6/7/00
50
50
BQL
Chloroform
6/7/00
50
50
BQL
Chloromethane
617/00
50
50
BQL
Dibromochloromethane
617/00
50
50
BQC
1,2-Dibromoethane (EDB)
6/7/00
50
50
BQL
1,2-Dichlorobenzene
6/7/00
50
50
BQL
1,3-Dichlorobenzene
617/00
50
50
BQL
1,4-Dichlorobenzene
6/7100
50
50
BQL
1,1-Dichloroethane
6/7/00
50
50
BQL
1,2-Dichloroethane
6/7/00
50
50
BQL
1,1-Dichloroethene
6/7/00
50
50
BQL
cis-1,2-Dichloroethene
6/7/00
50
50
BQL
trans-1,2-Dichloroethene
6/7100
50
50
BQL
1,2-Dichloropropane
6/7/00
50
50
BQL
cis-1,3-Dichloropropene
6/7/00
50
50
BQL
trans-1,3-Dichloropropene
6/7/00
50
50
BQL
Methylene Chloride
6/7/00 '
50
250
BQL
1,1,2,2-Tertrachloroethane
6/7/00
50
50
BQL
Tetrachloroethene
617/00
50
50
BQL
1,1,1-Trichloroethane
6/7/00
50
50
BQL
1,1,2-Trichloroethane
6/7/00
50
50
BQL
Trichloroethene
6/7/00
50
50
750
Trichlorofluoromethane
6/7/00
50
50
BQL
Vinyl Chloride
6/7/00
50
50
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
44
109
Comments:
Flags:
All values corrected for dilution.
BQL = Below quantitation limit.
Reviewed By:
Pa e1of1
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Client Sample ID: Effluent Analyzed By: EKR
Client Project ID: Laurinburg Groundwater Monitoring Wells Date Collected: 05/24/00
Lab Sample ID: 88452 Date Received: 05/26/00
Lab Project ID: G420-2 Matrix: Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
6/7/00
1
1
BQL
Bromoform
6/7/00
1
2
BQL
Bromomethane
6/7/00
1
2
BQL
Carbon tetrachloride
6/7/00
1
1
BQL
Chlorobenzene
6/7/00
1
1
BQL
- Chloroethane
6/7/00
1
1
BQL
_ Chloroform
6/7/00
1
1
BQL
Chloromethane
617/00
1
1
BQL
Dibromochloromethane
6/7/00
1
1
1,2-Dibromoethane (EDB)
6/7/00
1
1
BQL
1,2-Dichlorobenzene
6/7/00
1
1
BQL
_ 1,3-Dichlorobenzene
6/7/00
1
1
BQL
1,4-Dichlorobenzene
6/7100
1
1
BQL
1,1-Dichloroethane
6/7/00
1
1
BQL
1,2-Dichloroethane
6/7/00
1
1
BQL
1,1-Dichloroethene
6/7/00
1
1
BQL
cis-1,2-Dichloroethene
6/7100
1
1
BQL
trans-1,2-Dichloroethene
6/7/00
1
1
BQL
1,2-Dichloropropane
6/7/00
1
1
BQL
cis-1,3-Dichloropropene
6/7/00
1
1
BQL
trans-1,3-Dichloropropene
6/7/00
1
1
BQL
Methylene Chloride
6/7/00
1
5
BQL
1,1,2,2-Tertrachloroethane
6/7/00
1
1
BQL
Tetrachloroethene
617/00
1
1
BQL
1,1,1-Trichloroethane
617/00
1
1
BQL
- 1,1,2-Trichloroethane
6/7/00
1
1
BQL
Trichloroethene
6/7/00
1
1
BQL
Trichlorofluoromethane
6/7/00
1
BQL
Vinyl Chloride
6/7/00
1
1
BQL
1
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
45
111
Comments:
Flags:
All values corrected for dilution.
BQL = Below quantitation limit.
Pa e1of1 Reviewed By:
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID: MW-1 Date Collected: 5/24100
Client Project ID: Laurinburg Groundwater Monitoring Wells Date Received: 5/26/00
Lab Sample ID: 88451 Analyzed By: EES
Lab Project ID: G420-2
Matrix: Water
Parameter Result Date
Analyzed
PH 6.18 613/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was Performed outside of the 15 minute holding time.
Reviewed By: fyb�
North Carolina Wastewater Certification #481

PARADIGM AJJM)aWAb LrgAaBORATORIES, INC.
Client Sample ID:
MW-2 Date Collected:
5/24/00
Client Project ID:
Laurinburg Groundwater Monitoring Wells Date Received:
5/26/00
Lab Sample ID:
88450 Analyzed By:
EES
Lab Project ID:
G420-2
Matrix:
Water
Parameter
Result
yi
Date
Analyzed
i PH 5.80 6/3/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By: pnj-j�—
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for inorganics
Client Sample ID: MW3 Date Collected: 5/24/00
Client Project ID: Laurinburg Groundwater Monitoring Wells Date Received: 5/26/00
Lab Sample ID: 88449 Analyzed By: EES
Lab Project ID: G420-2
Matrix: Water
Parameter Result Date
Analyzed
pH 6.07 ' 6/3/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By: pA7._
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID: MW-4 Date Collected: 5/24/00
Client Project ID: Laurinburg Groundwater Monitoring Wells Date Received: 5126/00
Lab Sample ID: 88448 Analyzed By: EES
Lab Project ID: G420-2
Matrix: Water
Parameter Result Date
Analyzed
pH 5.67 ' 6/3/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By: hV1—
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID: MW-5 Date Collected: 5/24/00
Client Project ID: Laurinburg Groundwater Monitoring Wells Date Received: 5/26/00
Lab Sample ID: 88447 Analyzed By: EES
Lab Project ID: G420-2
Matrix: Water
Parameter Result Date
Analyzed
pH 5.96 ' 6/3/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By:
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-6 Date Collected:
5/24/00
Client Project ID:
Laurinburg Groundwater Monitoring Wells Date Received:
5/26/00
Lab Sample ID:
88446 Analyzed By:
EES
Lab Project ID:
G420-2
Matrix:
Water
Parameter
Result
Date
Analyzed
pH
5,04 '
6/3/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By:
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID: MW-7 Date Collected: 5/24/00
Client Project ID: Laurinburg Groundwater Monitoring Wells Date Received: 5/26/00
Lab Sample ID: 88445 Analyzed By: EES
Lab Project ID: G420-2
Matrix: Water
Parameter Result Date
Analyzed
J pH 5.38 ' 6/3/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By: jMti
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
W-9
Date Collected: 5/24/00
Client Project ID:
Laurinburg Groundwater Monitoring Wells
Date Received: 5126100
Lab Sample ID:
88444
Analyzed By: EES
Lab Project ID:
G420-2
Matrix:
Water
Parameter Result Date
Analyzed
pH 4.97 5/27/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By: tenon_
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
GT-10 Date Collected: 5/24/00
Client Project ID:
Laurinburg Groundwater Monitoring Wells Date Received: 5/26/00
Lab Sample ID:
88443 Analyzed By: EES
Lab Project ID:
G420-2
Matrix:
Water
Parameter Result Date
Analyzed
PH 4.84 ' 6/3/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By: ►�
North Carolina Wastewater Certification #481

PARADIGM ANResul s fore'Inorg BORATORIES, INC.
Client Sample ID: GT-11 Date Collected: 5/24/00
Client Project ID: Laurinburg Groundwater Monitoring Wells Date Received: 5/26/00
Lab Sample ID: 88442 Analyzed By: EES
Lab Project ID: G420-2
Matrix: Water
Parameter Result Date
Analyzed
pH 5.24 6/3/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By: DL�__
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
GT-12 Date Collected: 5/24/00
Client Project ID:
Laurinburg Groundwater Monitoring Wells Date Received: 5/26/00
Lab Sample ID:
88441 Analyzed By: EES
Lab Project ID:
G420-2
Matrix:
Water
Parameter Result
Date
Analyzed
pH 5•22 - 6/3/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By: yyyL
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client. Sample ID:
GT-13 Date Collected:
5/24/00
Client Project ID:
Laurinburg Groundwater Monitoring Wells Date Received:
5/26/00
Lab Sample ID:
88440 Analyzed By:
EES
_ Lab Project ID:
G420-2
Matrix:
Water
Parameter
Result
Date
Analyzed
pH 5.35 6/3/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By: WV.,, —
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
- Client Sample ID:
GT-14 Date Collected: 5/24/00
Client Project ID:
Laurinburg Groundwater Monitoring Wells Date Received: 5/26/00
Lab Sample ID:
88439 Analyzed By: EES
Lab Project ID:
G420-2
Matrix:
Water
Parameter Result Date
Analyzed
pH 5.18 ' 6/3/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By: nNk,
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
_ Client Sample ID: Influent Date Collected: 5/24/00
Client Project ID: Laurinburg Groundwater Monitoring Wells Date Received: 5126/00
Lab Sample ID: 88453 Analyzed By: EES
Lab Project ID: G420-2
Matrix: Water
Parameter Result Date
Analyzed
pH 5.32 ' 6/3/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
_. collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By:
North Carolina Wastewater Certification #481

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID: Effluent Date Collected:
5/24/00
Client Project ID: Laurinburg Groundwater Monitoring Wells Date Received:
5/26/00
Lab Sample ID: 88452 Analyzed By:
EES
Lab Project ID: G420-2
Matrix: Water
Parameter Result
Date
Analyzed
pH 7.00
6/3l00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
_ collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By: h4X.,
North Carolina Wastewater Certification #481

m ,
SUBMI1 1-OHM ON.YVL UVV VAVI:R ONLY �6 �d-�. — .. Q 0 (Do =--kAL%
EACILITY I FORMATION Please Print Clearly or Type
FacilityNanie:—Toaskmesic2 ZU(_, (-TA1g)TAhA." TAAG
Permit Name (if different):
Well Location/ Site
County -x-Q
Telephone #:!
No. of Wells to
Well ldentificalionNumber (from Permit): MW-1 For Groundwater Treatment Systems
Well Depth: ZS, O ft. Well Diameter: 10 In. Check One:
Screened Interval: i s o ft, to Z5� C) ft. 13 Influent (98)
Depth to Water Level:Ifs— ft. below measuring point. ❑ Effluent 99
Measuring Point Is 7-.t 8. above land surface. ( )
Gallons of water pumped/balled before sampling: R
Field analysis: pH S,81 , Specific Conductance uMhos
Temp. a °C, Odor Appearance
PERMIT #: EXPIRATION DATE: 11- 30 -0
Non-Dlschargewn Oon'4m-49E UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remedialion: Infillralion Gallery
Spray Retd Remedialion:
Rotary Distributor Land Application of Sludge
_ X Other:
NOTE: Values should reflect dissolved and
colloidal concentrations.
Date sample collect d: I -Liz 62 Date sample an a zed: I--ZS-tx
Laboratory Name: lanZte�m �Na4\X1_cnl oLag-p�csz;ec
Certification No.. 4R1 0 "'
-- n
EARAME[09 (Samples for metals were collected untillered YES _NO
and field acidified
_YES _ NO) E�6 `
COD
mg/l
Nitrite (NO2) as N
mg/I
NI -Nickel r `'- mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
mg/I
Pb - Lead _, ;-'°=' mgll
Coliform: MF Total
1100ml
Phosphorus: Total as P
mgll
Zn -ZincF I mg/1
(Hole: Ilse MPH method for highlyturbrd samples)
Orthophosphate
mg/l
L :Y_
Ammonia Nitrogen �-' m-a mg/l
Dissolved Solids: Total
mg/I
At - Aluminum
mg/I
Other (Specify Compounds and'Concehtration Units)
pH (when analyzed) C, 26
units
Ba - Barium
mg/I
T
TOO
mg/l
Ca -Calcium
mg/I
Chloride
mg/l
Cd - Cadmium
mg/I
Arsenic
mgll
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/1
Phenol
mg/I
Fe -Iron
mg/I
ORGANICS: (GC,GC/MS,HPLC)
Sulfate
Specific Conductance
mg/l
uMhos
Fig - Mercury
K - Potassium
mgll
mg/I
(Specify lest and method #. Attach lab report.)
Report Attached? Yes No _ (0)
Total Ammonia
mg/I
Mg - Magnesium
mg/I
VOC CC- : method # = GO\
TKN as N
mg/I
Mn - Manganese
mg/l
: method # _-
method # o

$UUMI I FORM ON
PAFLKONLY
FACILITY INFORMATION Please Print Clearly or Type
Fatiilfly�Name: IJhSj"MAs��Lal jTa�e��arn T''n�� p�2� is GRc I'1`y
Permit Name (if different):
Facility Address: PIAAI - ZnI+Z
Well Location/ Site
county Scot14Nd
Telephone #:
No. of Wells to be Sampled:
Well identification Number (from Permit): (y\MI -Z For Gmundwaler Treatment Systems
Well Depth: '?b, ft. Well Dlemeter:l,.S._ In. Check One:
Screened Interval: ft. to ft. ❑ Influent (98)
Depth to Water Level: -.. Olt _ft. below measuring point. ❑, Effluent 99
Measuring Point Is 1, 30 ft. above land surface. ( )
Gallons of water pum edlpalled before sampling: It S
Field analysis: pH 6 Z 3 , Specific Conductance uMhos.
Temp. 6a-S °C, Odor Appearance
PERMIT M
EXPIRATION DATE: 11- 30 -o Z
Non -Discharge wfa 000'+'41R6
UIC
NPDES
TYPE OF PERMITTED
OPERATION BEING MONITORED
Lagoon
Remedlation: Infiltration Gallery
Spray Field
Remedlation:
Rotary Distributor
Land Application of Sludge
NOTE: Values should reflect dissolved and
colloidal concentrations.
Date sample collec�ed: I -1-1--00 Date sample analyzed:i Zg cn
Laboratory Name: A� ANw\y4tcal LAbozalai'es
Certification No. �-NR\ o -
0
P9BAtd€WER (Samples for metals were collected unfiltered YES _NO and field acidified
COD mg/l Nitrite (NO2) as N mg/I
Collform: MFFecal /100ml Nitrate (NO3) as N__-.- -mgll
Coliform MF Total /100ml Phosohorus: Total as P mn/l
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
mg/I
pH (when analyzed) .-ate
units
TOG
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sullate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
GW-59 Rev. 4/9e
Orthophosphate
mg/1
AI- Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/1
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
ma/I
_YES _NO)
Ni - Nickel mg/l
Pb - Lead "' =_ ' mg/I
Zn - Zinc = mg/I
Ammonia Nitrogen
Other (Specily Compounds and egnceRfalion Units)
�1L:C1n\nnl-,ei\{eNe7-1
5IL
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach tab report.)
Report Attached? Yes X (1) No _ (0)
VOC d L : method # - Ct \
method # e
,method #

'SUdMI I FUHM ON Y17LLUW NAYttt UNLY
FACILITY Y INFORMATION Please Print Clearly or Type
Facility)Jame:-T-onAMa-sine-rN(, Pz,sQe4l1AM --:n\v-lPA 3 Fs F'r�c 1.4r
Permit Name (if dilferenl)i
Well Location/ Site Name:
County-S�Qt1
Telephone #: 5
No. of Wells to be
Well Identification Number (from Permit): MW-3- For Groundwater Treatment Systems
Well Depth: 30:y ft. Well Diameter: 1.2S- In. 'Check One:
Screened Interval: ft. to fl.
Depth to Water Level o S ft. below measuring, point. 13 i7 Influent (98)
Measuring Point is !Cl ft. above land surface. Effluent (99)
Gallons of water pumped/balled before sampling: 2,S
field analysis: pH C%cA l , Specific Conductance uMhos
Temp. (la, I DC, Odor Appearance
PERMIT
EXPIRATION DATE: I I -- TO - o z
TYPE40F PERMli fED OPERATION BEING MONITORED
Lagoon Remedlation: Infiltration Gallery
Spray Field Remeolalon:
Rotary Distributor Land Application of Sludge
otherd-
NOTE: Values should reflect dissolved and
colloidal concentrations.
Dale sample collected: ' t%-OO Date sample analyzed: l- Zsam -c
LaboratoryName: Ian.r 3*4 A� rA31 ',r a\ (� boeA teQ;< s
QerlilicationNo. _ L1a1 a
EARAM€T€HS (Samples for metals were collected unfiltered - -YES _NO
and field acidified
_YES _ NO)
COD
mgA
Nitrite (NO2) as N
mgA
NI - Nickel
m /I
Coliform: MF Fecal
/100mi
Nitrate (NO3) as N
mg/I
Pb - Leap .�
mg/I
Colibrm: MF Total
/100ml
Phosphorus: Total as P _
mg/I
Zn - Zinc
mg/I
(Hole; Ilse MPH method for hlahtyw.cta samples)
Orthophosphate
mg/l
r_
Ammonia Nitrogen -° -- �
mg/I
Dissolved Solids: Total
(when analyzed) S,�I
mgA
At - Aluminum
Be
mg/I
Other (speclly Comppounds and:GoncpnIIr�
lion Units)
pH
units
- Barium
mg/l
T'2:c.N,.\oa�eitleNt-
TOG
mg/I
Ca - Calcium
mg/I
ro
Chloride
mg/I
Cd - Cadmium
mg/I
Arsenic
mg/l
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
Phenol
mg/I
Fe - Iron
mg/I
ORGANICS: (GC,GC/MS,HPLC)
Sulfate
mg/I
Hg - Mercury
mg/I
(Specify test and method #. Attach lab report.)
Specific Conductance
uMhos
K - Potassium
mg/I
Report Attached? Yes—,Q1) No
Total Ammonia
mg/I
Mg - Magnesium
mg/l
_(0)
VOC gc- method # = 6 Ol
TKN as N
mg/I
Mn - Manganese
mg/I
; method # _
method #

b'U11MI I FOKM ON YtLLUW VAVt-H ONLY
FACILITY INFORMATION Please Print Clearly or Type -
FacilitylName:- 10l`sS1 fr§ 'Cam IT.��ealvw•n Trine $¢,�Zacis Fk 4c_;L PERMIT#: EXPIRATION DATE:
Permit, Name (if different): I Non -Discharge WO too n9lb UIC
ContablPerson: f-AeeY CAAev- "' Telephone#:L,7-f 4t-
Well Location/ Site Name: No, of Wells to be Sampled:
Well Identification Number (from Permlt): M\,J-L4 For Gmundwaler Treatment Systems
Well Depth: ' 2\. d ft. Well Diameter: -WZ5' In. Check One:
Screened Interval: - - ft. to ft.
Depth to Water Level: q _- ft. below measuring point. 13 0 E f luent (98)
Measuring Point Is ft. above land surface. Effluent (99)
Gallons of water pumpadlballed before sampling: I• S
Field analysis. pH ) i �, 3 , Specific Conductance uMhos
Temp- "C, Odor Appearance
1F PERMITTED OPERATION BEING MONITORED
Lagoon Relhedlailon: Inftltrallon Gallery
Spray Field Remedialion:
Rotary Distributor Land Application of Sludge
Other.
NOTE: Values should reflect dissolved and
colloidal concentrations.
Date sample collected:-1-11-02 Dale
LaboratoryName: Amw.\Y�,
Certification No. 4A\
EARA64919ES (Samples for metals were collected unfiltered YES _NO
and field acidified'
COD
mgll
Nitrite (NO2) as N
mg/l
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
mg/l
Coliform: MF Total
A 00ml
Phosphorus: Total as P _
mgll
(Note: Use MPH method for highly turbid samples)
Orthophosphate
mg/l
Dissolved Solids: Total
mg/I
At - Aluminum
mg/I
pH (when analyzed) S sy
units
Be - Barium
mg/I
TOG
mg/I
Ca - Calcium
mg/I
Chloride
mg/I
Cd - Cadmium
mgll
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
Phenol
mg/I
Fe - Iron
mg/l
Sulfate
mg/I
Hg - Mercury
mg/I
Specific Conductance
uMhos
K - Potassium
mg/I
Total Ammonia
mg/I
Mg - Magnesium
mg/I
TKN as N
mg/I
Mn - Manganese
mg/I
_YES _NO)
Iv
NI - Nickel
- mg/l
Pb - Lead
MIC x,• `� mg/l
Zn - Zinc
`' mg/I
Ammonia Nitrogen
s mg/1
Other
(Specily Compounds
an Coraxniration Units)
T�te�
\nnne��.eNc—
13D� u�Jz
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes X (1) No_(0)
VOC C (L : method # = 6O\ . -
: method # o
: method #

SUUMI.1 f UKM ON YtLLUW YANtK ONLY
Facility Name:_
Permit Name (if
Well location/ Site
or
County Sc0tlanZ
Telephone #: LAt
No. of Wells to be Sampled:
Well Identilication Number (from Permit): wl W - S For Groundwater Treatment Systems
Well Depth; 'Zy.y ft. Well Diameter: L2.5 In. Check One:
Screened lnleival: ft. to ft. ❑ Influent (98)
Depth to Water Level:_lil ft. below measuring point. ❑ Effluent (99)
Measuring Point is 17-0 ft. above land surface.
Gallons of water pump edlballed before sampling: 2,9
Field analysis: pH L37 , Specific Conductance . _ uMhos
Temp. III °C, Odor Appearance
PERMIT M EXPIRATION DATE: 11 30 —02
Non -Discharge WO rwa 99 UIC
)PERATION'BEING MONITORED
Rehledlallon: Inftllration Gallery
Spray Field Remedlation:
Rotary Distributor Land Application of Sludge
Other.•
NOTE: Values should reflect dissolved and
colloidal concentrations.
Dale sample collected: 1- EL OO Date sample analyzed: EZS =OP
LaboratoryName: �g Atir+_1vk;ctit tLMnOltJjrht'cs
Certification No. yak—?
MAMisT€95— (Samples for metals were collected unfiltered YES _NO and field acidified
COD mg/I Nitrite (NO2) as N mg/I
Coliform: MF Fecal A00ml Nitrate (NO3) as N mg/I
Coliform: MF Total /100ml Phosphorus: Total as P mg/I
(Note; Use MPH method for highly turbld samples)
Dissolved Solids; Total
mg/I
pH (when analyzed) s. c S
units
TOG
mg/I
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/l
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/I
TKN as N
mg/I
urinopnospnate
mg/I
At - Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/l
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg -'Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
_YES _ NO) N
NI - Nickel
Pb - Learn °
Zn - Zinc
Ammonia Nitrogen
Other (Specify Compounds an"
�s
mg/I
mg/I
Units)
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach tab report.)
Report Attached? Yes K (1) No _ (0)
VOC C_ : method# CO1
: method # e
: method #

>r
SUUMI I FUIHM ON YELLUW YAMH ONLY
Facility Name:_
Permit Name (if
Well Location/ Site
County Y0-11
Telephone #:-K.E-
No.. of Wells to be
or
Well Identification Number Permit): Mw-6 For Groundwater Treatment Systems
Well Depth: 3S'.0
ft. Well Diameter: ?,0 In. Check One:
Screened Interval: 1-t..a ft. to1i_ ft. ❑ Influent (98)
Depth to Water Level: 117 b ft. below measuring point. ❑ Effluent (99)
Measuring Point Is LA ZO ft. above land surface.
Gallons of water pumpedfbailed before sampling: t l
Field analysis: pH CA 1 , Specific Conductance uMhos
Temp. (tea °C,Odor Appearance
P-AHAMI T.€9S (Samples for metals were collected unfiltered YES _NO
Non-Discharge-wQ Goa-4- "% UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediallon: Infiltration Gallery
Spray Field Remedlatlon:
Rotary Distributor Land Application of Sludge
_ Omer:
NOTE: Values should reflect dissolved and
colloidal concentrations.
Date sample colle
Laboratory Name:
Certification No. _
and field acidified
COD
mg/I
Nitrite (NO2) as N
mgll
Coliform: MF Fecal
/100m1
Nitrate (NOO as N
mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN methoddor highly turhld samples)
Orthophosphate
mg/l
Dissolved Solids: Total
mgA
At - Aluminum
mg/I
pH (when analyzed) 5—,Do
units
Ba - Barium
mg/I
TOO
mg/I
Ca - Calcium
mg/I
Chloride
mg/l
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
Phenol
mg/I
Fe - Iron
mg/1
Sulfate
mg/I
Hg - Mercury
mg/I
Specific Conductance
uMhos
K - Potassium
mg/I
Total Ammonia
mg/I
Mg - Magnesium
mg/I
TKN as N
mg/I
Mn - Manganese
mg/I
_YES _ NO)
NI - Nickel
Pb - Learl
Zn - Zinc
Ammonia Nitrogen —
As an'aTyzed:1
fa�IeAV' icS
rr e`=a'r
mg/I
2
mg/I
44�`r—
mg/I
r
mg/l
iftonddntratlon Units)
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
Repots Attached? Yes__t_<(1) No — (0)
VOC _ CC_ : method # = 6C)k
: method #
method # e

SUHMI I FORM ON
YAIJI=R ONLY
Facility Name:_
Permit Name (if
Well Location/ Site
Please
County ->c-6h
Telephone #:(E2
No. of Wells to be
Well ldenlificallon Number (from Permltl AAW -�-
For Groundwater Treatment Systems
Well Depth: 3151 co ft. Well Diameter: -L D In.
Check One:
Screened Interval: IS':.o 1t. to 35:: o it.
❑ Influent (98)
Depth to Water Level:ILEA ft. below measuring point.
13 Effluent (99)
Measuring Point is L-1 20 ft. above land surface.
Gallons of water pumpedlballed before sampling: 11
Fleld analysis: pH LZE , Specific Conductance
uMhos
Temp. Ig.'a °C, Odor Appearance
PERMIT - EXPIRATION DATE: 11- 30 -oz
Non -Discharge WO uo;T�LgO UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Rerhediallon:Infiltration Gallery
Spray Field Remedlation:
Rotary Distributor Land Application of Sludge
-� Other:
NOTE: Values should reflect dissolved and
colloidal concentrations.
Date sample collected:..'
Laboratory Name: PA
CerlilicellonNo. LARN
Zy-' o
MAM€T€99 (Samples for metals were collected unfiltered YES _NO
and field acidified
_YES _ NO) 9
COD
mg/I
Nitrite (NO2) as N
mg/I
NI - Nickel =- Q
mg/l
Colliorm: MF Fecal
/100ml
Nitrate (NO3) as N
mgA
Pb - Lead w « a
mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
Zn - Zinn `y
mg/l
(Hole: Ilse MPH method for highly turhld samples)
Orthophosphate
- mg/I
Ammonia Nitrogen_ `" o -:mgA
Dissolved Solids: Total
- mgA
At - Aluminum
mg/I
Qjher Specify Com�
pounds and Concentration Units),
pH (when analyzed) 'S', 3�
units
Be - Barium
mg/I
1 P_Z(VNo¢Z etti,e
�t - 160� ��IL_
TOO
mgA
Ca - Calcium
mg/I
1 L
Chloride
mg/I
Cd - Cadmium
mg/I
�f
P
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/i
Cu - Copper
mg/I
Phenol
mgll
Fe - Iron
mg/I
ORGANICS: (GC,GCiMS,HPLC)
Sulfate
mg/I
Hg - Mercury
mg/I
(Specify test and method #. Attach lab report.)
Specific Conductance
uMhos
K - Potassium
mg/I
Report Attached? Yes n (1) No
_ (0)
Total Ammonia
mg/i
Mg - Magnesium
mg/I
VOC ( C_ : method # = 601
TKN as N
mg/I
Mn - Manganese
mg/I
: method #
: method # m

bUdMl l I -OHM ON,yI=LLUW VAVLK ONLY
Facility Name: IaN5i ry
Permit Name (if different):
Well Location/ Site Name:
or Type
County
Telephone,#: CS11-'S �tyS-
No. of Wells to be Sampled:
Well Identification Number (from Permit) AA w-9 For Groundwater Treatment Systems
Well Depth: 2.e_ ft. Well Diameter:2.0 In. Check One:
Screened Interval: ft. to ft. ❑ Influent (98)
Depth to Water Level: _ft. below measuring point. ❑Effluent (99)
Measuring Point is -ft. above land surface.
Gallons of water pumped/balled before sampling: 6
Field analysis: pH S. 1(- , Specific Conductance uMhos
Temp. 19. 3 "C, Odor Appearance
PERMIT'M EXPIRATION'DATE: /1-30-02
Non -Discharge 1.08 o0o-+198 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remedlallon: Infiltration Gallery
Spray Field Remedlation:
Rotary Distributor Land Appllcation of Sludge
'_ Other:
NOTE: Values should reflect dissolved and
colloidal concentrations.
Date sample colle
Laboratory Name:
Qertllicatlon No. _
EAHAIVIRT€.8A (Samples for metals were collected untfltered Y,ES _NO
and field acidified
COD
mg/I
Nitrite (NO2) as N
mg/I
Coliform: MF Fecal
A60ml
Nitrate (NOO as N
mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
_ mg/I
lNote. Use MPH method for highly turbid samples)
Orthophosphate
- mg/I
Dissolved Solids: Total
mg/I
At - Aluminum
mg/I
pH (when analyzed) LA 30
units
Be - Barium
mg/I
TOO
mg/I
Ca - Calcium
mg/I
Chloride
mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I'
Grease and Oils
mg/I
Cu - Copper
mg/1
Phenol
mg/l
Fe - Iron
mg/I
Sulfate
mg/I
Hg - Mercury,
mg/I
Specific Conductance
uMhos
K - Potassium
mg/I
Total. Ammonia
mg/I
Mg - Magnesium
mg/l
TKN as N -
mg/I
Mn - Manganese
mg/I
GW-59 Rev. 4/99
_YES _NO)
Ni - Nickel
Pb - Lead
Zn - Zinc
Ammonia Nitrogen_
mpRan*zed:
l i>~�DozA-�eeies
'° f^
mg/I
mg/l
t;_
mg/I
LI
mg/l
and Concentrallon Units)'
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method P. Attach lab report.)
Report Attached? Yes zC (1) No _(0)
VOC 6L : method#= 60\
method #
method # e

SUdMI1 FUHM UN.YtLLUW VAVI=K UNLY
or Type
Facility Name: I CASH
D-.mil �hme fit .IlU...e..n.
Well Location/ Site Name: No. of Wells to be Sampled:„ I.,
Well Identillo8llon Number (from Permit): - 4 w =10 For Groundwater Treatment Systems
Well Depth: 2Jr0 It. WellDlameler:4 0 In. Check One:
Screened Interval: ft. to ft. ❑ Influent (98)
Depth to Water Level: 1.6S ft. below measuring point.
Measuring Point Is 1 Z 5' R. above land surface. ❑ Effluent (99 )
Gallons of water pumped/balled before sampling: 35-
Field analysis: pH 4yL , Specific Conductance uMhos
Temp. J 04 OC, Odor Appearance
PERMIT#:
EXPIRATION DATE:
NPDES
TYPE OF PERM17T -n OPERATION BEING MONITORED
Lagoon Rerhedlatlon: Infiltration Gallery
Spray Field Remediatlon:
Rotary Distributor _ Land Application of Sludge
NOTE: Values should reflect dissolved and
colloidal concentrations.
Date sample collected: 4 Date sample one yzed: I-2S o
Laboratory Name: k RQR '%@NA:y�V_at
Certification No.
o 0
EABAMPIT€BA (Samples for metals were collected unfiltered YES _NO
and field acidified
COD
mg/1
Nitrite (NO2) as N
mg/l
Conform: MF Fecal
- /100ml
Nitrate (NO3) as N
mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note; Use MR4 melhod for highly turbid samples)
Orthophosphate
mg/I
Dissolved Solids: Total
mg/l
At - Aluminum
_
mg/I
pH (when analyzed) W, 9
units
Ba - Barium
mg/I
TOG
mg/I
Ca - Calcium
mg/I
Chloride
mgll
Cd - Cadmium
- mg/l
Arsenic
mg/l
Chromium: Total
mg/I
Grease and Oils _
mg/l
Cu - Copper
mg/I
Phenol
mg/I
Fe - Iron
mg/I
Sulfate
mg/l
Hg - Mercury
mg/I
Specific Conductance
uMhos
K - Potassium
mg/I
Total Ammonia
mg/l
Mg - Magnesium
mg/l
TKN as N
mg/1
Mn - Manganese
mg/I
_YES
NI - Nicke
Pb - Lead
Zn - Zinc.
Ammonia.
— NO)
=_ mg/I
mg/1
mg/I
mg/I
fillon Units)
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. Attach lab report.)
Report Attached? Yes x (1) No _ (0)
VOC 6-L : method # = b01
: method #
: method #
GW-59 Rev. 4198

SUUMI I FUHM UN YtLLUW NAl-tK UNLY
Facility Name:_
Permit Name, (if
Well Location/ Site Name:I
Please Print Clearly or
County t.�+\
Telephone #: CS
No. of Wells to be
Well Identification Number (from Permit): M w- i t For Groundwater Treatment Systems
Well Depth: ' 2S , � ft. Well Diameter: u ! In. Check One:
Screened Interval: (.,O ft. to ZS, o it. p. Influent
Depth to Water Level: 3 9L D ft. below measuring point. ❑Effluent
Measuring Point is tS ft. above land surface.
Gallons of water pumped/balled before sampNng: 3a
Field analysts: pH 5.0 2 , Specific Conductance uMhos
Temp. 1H,�L4_"C, Odor Appearance
(98)
PERMIT #: EXPIRATION DATE: 11-30- 02
Non -Discharge �Q c�oy � it3 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remediatlon: Infiltration Gallery
Spray Field Remediatlon:
Rotary Distributor Lend Application of Sludge
NOTE: Values should reflect dissolved and
colloidal concentrations.
Date sample colle
Laboratory Name:
Qedificalion No. _
EAHAM919BS (Samples for metals were collected unfiltered YES _NO
and field acidified
COD
mg/I
Nitrite (NO2) as N
mgA
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
mg/l
Colilorm: MF Total
/100mf
Phosphorus: Total as. P
mgA
(Note: Use MPN method for hlghly turbid samples)
Orthophosphate
mg/I
Dissolved Solids: Total
pH (when analyzed)
mgA
y 3 units
At - Aluminum
Ba - Barium
mg/I
mg/I
TOG
mg/I
Ca -Calcium
mg/I
Chloride
mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
Phenol
mg/I
Fe - Iron
mgA
Sulfate
mg/l
Hg - Mercury
mg/I
Specific Conductance
uMhos
K - Potassium
mg/I
Total Ammonia
mg/I
Mg - Magnesium
mg/I
TKN as N
mg/I
Mn - Manganese
mg/1
YES
NI - Nick
Pb - Lea
Zn - Zin(
_ NO)
-25--o�
mg/I
mg/I
mg/l
ORGANICS: (GC,GC/MS,HPLC)
(Specify lest and method #. Attach lab report.)
Report Attached? Yes 7C (1) No _ (0)
VOC Cc— : method #. i,01
: method # .
: method # .
GW-59 Rev. 4/90

SUBMI I I -OHM ON Yt-LLOW PAPEN ONLY
FACILITY INFORMATION Please Print Clearly or Type
Facilily'Name:I��ealnpM Tim + YL,. FAc;l;l-
Permit Name (it different. _
Contaot Person•LUA- P laF\/'-" "w' Telephone #: (SM) 44t - rri
Well Location/ Site Name: No. of Wells to be Sampled:,,_„„
Well WellI entiicationNu bbeer(fromfPeWetl: Me . r-t2 _ For Groundwater Treatment Systems
p - In. Check One:
Screened Interval: I:` m ft. to 75.0 ft. ❑ Influent (98)
Depth to Water Level:_ L36 ft. below measuring, point. ❑ Effluent (99)
Measuring Point Is 2. S' ft. above land surface.
Gallons of water pumped/balled before sampling: IR
Field analysis: pH L 1 _ , Specific Conductance uMhos
Temp. ,R•$ 'C,Odor Appearance
PERMIT #: IEXPIRATION DATE: I l - 3D- O2
Non -Discharge wQ 0o0'T-V`113 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remedlatlon:Infiltration Gallery
Spray Field Remedlatlon
Rotary Distributor Land Application of Sludge
Y,_ Other:
NOTE: Values should reflect dissolved and
colloidal concentrations. o
O o
Date sample collected: _( -�� Date saa ans
Laboratory Name: VFOXLgM w\y\:cal �rL1,e
Certification No. Lk R\
P9HAM€iC€BS (Samples for metals were collected unfiltered YES _NO
and field acidified ,_YES
_ NO) -v f
COD
mg/I
Nitrite (NO2) as N
mg/I
NI - Nickel z " mg/l
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
mg/I
Pb - Lead mgll
Coliform: MF Total
/100m1.
Phosphorus: Total as P
mg/I
Zn - Zinc _-' mg/I
INole: u90 MPN method for highly turbid eamples).
Orthophosphate
mg/I
Ammonia Nitrogen == mg/)..
Dissolved Solids: Total
mgll
At - Aluminum
mg/I
Other ((Specify Compounds and Concentratlon Units)
pH (when analyzed) , 00t
units
Ba -Barium
mg/l
Ta; c�h 9_0 e+A .N e - Qa Y
TOO
mg/I
Ca - Calcium
mg/1
Chloride
mg/l
Cd -Cadmium
mg/I
Arsenic
mg/1
Chromium: Total
mg/I
Grease and Oils,
mg/l
Cu - Copper
mg/1
Phenol
mgll
Fe - Iron
mg/l
ORGANICS: (GC,GC/MS,HPLC)
Sulfate
mg/I
Fig - Mercury
mg/l
(Specify lest and method#. Attach lab report.)
Specific Conductance
uMhos
K - Potassium
mg/l
Report Attached? Yes-2Q1) No _ (0)
Total Ammonia
mg/I
Mg - Magnesium
mg/I
VOC [ _ : method # Q 6�l
TKN as N
mg/l
Mn - Manganese
mg/I
: method # _
method # o
GW-59 Rev. 4/98

SUtlMIT FOHM UN YhLLTW FAYtK UNLY
fw , Kip' ex ! eE { Fro 83 �( `qi' Sr-jE, �'' 3'xfi � E �E i E :�^ i r ,y 1 Y s� Y�1. FS° � a S • �
GF�O1Nb�A1�TERQUAL'TYMOIiTORING�Mx,��`���
NIWNCE 4PO sz r dF c S t {&�wk M•xan ai'4
XOMPLRE_ �I FOFIM�r' ` .; sx�I
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Tnr.� INc. (lw]pQQ�AM �:Mt d x i s FAc;l;�y PERMITW
Permit Name (if different) _ II Non-Dischl
Well Location/
county SW"7k4,z6
Telephone #: L5231 44E
No. of Wells to be Sampled:
Well ldentificatfonNumber (from Permit): PAw-t-3 For Groundwater Treatment Systems
Well Depth: ; D.O It. Well Diameter: in. Check One:
Screened Interval: 4EQ ft. to CO o It. ❑ Influent (98)
Depth to Water Level: 20 33 ft. below measuring point. ❑ Effluent (99)
Measuring Paint is 3. Z ft. above land surface.
Gallons of water pumped/balledbefore sampling: 2y R. 6
Field analysis: pH S .20 , Specific Conductance uMhos
Temp. A) lA °C, Odor Appearance
TYPE OF PERMITTED
Lagoon
Spray Field
v Rolary Distributor
X Other:
EXPIRATION DATE:
BEING MONITORED
Remedialion; Infiltration Gallery
Remedialion:
Land Applicallon of Sludge
NOTE: Values should reflect dissolved and
colloidal concentrations.
O Q
Date sample collected:-I-w-OO Date sampl�ea
LaboraloryName: QAa�+rc4r"A AaA NI V:em � V+a
Certification No. SR k
MAMEiE6M (Samples for metals were collected unfiltered YES _NO and field acidified
COD mg/l Nitrite (NO2) as N mgA
Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/I
Coliform: MF Total /100ml Phosphorus: Total as P mg/1
(Holed Use MPH method for highly turbld,eamplep)
Dissolved Solids: Total
mgA
pH (when analyzed) C, 4 6
units
TOG
mg/l
Chloride
mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
uMhos
Total Ammonia
mg/1
TKN as N
mg/I
urtnopnospnate
mg/I
Al - Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/l
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/l
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/l
Mn - Manganese
mg/I
_YES _ NO) -0 {n
Ni -Nickel b3 " a mg/1
Pb - Lead mg/I
Zn - Zinc mg/I
Ammonia Nitrogen mg/I
Other (Specily Compo�unds and Concentration Units)•
T¢tC. k?Q-e;1-IneN2 — is k,g) L
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method If. Attach lab report.)
ReportAttached? Yes-_Q1) No _ (0)
VOC method#.
method # 9
method #

SUBMIT FORM ON
ONLY
rAU1.1 r r l"ry"iVIA.1 AAV t-tease rrmr cteany or type
Facility Name: Tnw5'�MfNS)r2 � r-3c l T'-jr; r lnAN. T;
Permit Name fit different):
Well Location/ Site Name:
Telephone #: LS' It 5 1 'tv s -
,T,— No. of Wells to be Sampled:,,
Well Identification umber (from Permit): M W -14 for Groundwater Treatment Systems.
Well Depth: O #. Well Diameter;4, o In. Check One:
Screened Inteival: L o ft.to 30.0 it. ❑ Influent (98)
Depth to Water Level: 9,12 ft. below measuring point. ❑ Effluent (99)
Measuring Point is Z ZO ft. above land surface.
Gallons of water pumpedfballed before sampling: q Z
Field analysis: pH L .13 , Specific Conductance uMhos
Temp. L%2_°C, Odor Appearance
PERMIT #: EXPIRATION DATE: t L 312-0Z
Non -Discharge WO caoo-f-f9t3 UIC
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon Remedlallon: Infiltration Gallery
Spray Field nemedlation:
Rotary Distributor Land Application of Sludge
-Other.
NOTE: Values should reflect dissolved and
colloidal concentrations.,
Dale sample collected: -I-1 -F-oo [
Laboratory Name: Yft2A clean ANA-(
Cedlficalion No. 4 91
-ZS-0o
MAMETUB111(Samples for metals were collected unfiltered -YES _NO
and field acidified
_YES —NO) a'
COD
mg/I
Nitrite (NO2) as N
mg/I
NI - Nickel �� `-_
mgn
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
mg/I
Pb - Lead ,3 =
mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
Zn - Zinc v
mg/1
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Ammonia Nitrogen CIOg
m /I
Dissolved Solids: Total
mg/I
At - Aluminum
mg/I
Other (Spscily Compounds andConQ61ratlon Units)
pH (when analyzed) 5.5-G
units
Be - Barium
mg/I
T¢:c.h1o2� ctHe ,e
mg/I
Ca - Calcium
mg/I
Chloride
mg/I
Cd - Cadmium
mg/I
Arsenic
mg/1
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/l
Phenol.
mg/I
Fe - Iron
mg/l
ORGANICS: (GC,GC/MS,HPLC)
Sulfate
mg/I
Hg - Mercury _
mg/I
(Specify test and method #. Attach lab report.)
Specific Conductance
uMhos
K - Potassium
mg/I
Report Attached? Yes_.K_(1) No
_(0)
Total Ammonia
mg/I
Mg - Magnesium
mg/I
VOID 6c : method #- G,n1
TKN as N
mg/I
Mn - Manganese
mg/I
: method #
: method # .

APPENDIX V
LABORATORY ANALYTICAL RESULTS
a

PARADIGM ANALYTICAL LABORATORIES,
INC.
_-
Results for Volatiles
_I
by GC 601
Client Sample ID: MW-1
Analyzed By:
RNP
Client Project ID: Toastmaster
Date Collected:
01/17/00
— Lab Sample ID: 79798
Date Received:
01/18/00
Lab Project ID: G122-995
Matrix: Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
1/28/00
1
1
BQL
Bromoform
1/28/00
1
2
BQL
Bromomethane
1/28/00
1
2
BQL
- Carbon tetrachloride
1/28/00
1
1
BQL
Chlorobenzene
1/28/00
1
1
BQL
Chloroethane
1/28/00
1
1
BQL
- Chloroform
1/28/00
1
1
BQL
Chloromethane
1/28/00
1
1
BQL
Dibromochloromethane
1/28/00
1
1
BQL
1,2-Dibromoethane (EDB)
Wli
1/28/00
1
1
BQL
1,2-Dichlorobenzene
1/28/00
1
1
BQL
1,3-Dichlorobenzene
1/28/00
1
1
BQL
1,4-Dichlorobenzene
1128/00
1
1
BQL
1,1-Dichloroethane
1128/00
1
1
BQL
1,2-Dichloroethane
1/28/00
1
1
BQL
1,1-Dichloroethene
1/28/00
1
1
BQL
cis-1,2-Dichloroethene
1/28/00
1
1
BQL
trans-1,2-Dichloroethene
1/28/00
1
1
BQL
1,2-Dichloropropane
1128/00
1
1
BQL
cis-1,3-Dichloropropene
1/28/00
1
1
BQL
trans-1,3-Dichloropropene
1/28/00
1
1
BQL
Methylene Chloride
1/28/00
1
5
BQL
1,1,2,2-Tertrachloroethane
1/28/00
1
1
BQL
Tetrachloroethene
1/28/00
1
1
BQL
1,1,1-Trichloroethane
1/28/00
1
1
BQL
1,1,2-Trichloroethane
1/28/00
1
1
BQL
Trichloroethene
1/28/00
1
1
BQL
Trichlorofluoromethane
1/28/00
1
1
BQL
Vinyl Chloride
1/28/00
1
1
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
44
109
I
Comments:
Flags:
All values corrected for dilution.
BQL = Below quantitation limit.
Page 1 of 1
Reviewed By: 41 -,

PARADIGM ANALYTICAL LABORATORIES, INC.
-- Results for Volatiles
by GC 601
JClient Sample ID: MW-2 Analyzed By: RNP
Client Project ID: Toastmaster Date'Collected: 01/17/00
Lab Sample ID: 79799 Date Received: 01/18/00
Lab Project ID: G122-995 Matrix: Water
— Comments:
— Flags:
Compound
Date Quantitation Result
Analyzed Dilution Limit (ug/L) (ug/L)
Bromodichloromethane
1/28/00
100
100
Bromoform
1/28/00
100
200
Bromomethane
1/28/00
100
200
Carbon tetrachloride
1128/00
100
100
Chlorobenzene
1128/00
100
100
Chloroethane
1/28/00
100
100
Chloroform
1128100
100
100
Chloromethane
1/28/00
100
100
Dibromochloromethane
1/28/00
100
100
1,2-Dibromoethane (EDB)
1128/00
100
100
1,2-Dichlorobenzene
1/28/00
100
100
1,3-Dichlorobenzene
1/28/00
100
100
1,4-Dichlorobenzene
1/28/00
100
100
1,1-Dichloroethane
1/28/00
100
100
1,2-Dichloroethane
1/28/00
100
100
1,1-Dichloroethene
1/28/00
100
100
cis-1,2-Dichloroethene
1128/00
100
100
trans-1,2-Dichloroethene
1/28100
100
100
1,2-Dichloropropane
1/28/00
100
100
cis-1,3-Dichloropropene
1/28/00
100
100
trans-1,3-Dichloropropene
1/28/00
100
100
Methylene Chloride
1/28/00
100
500
1,1,2,2-Tertrachloroethane
1/28/00
100
100
Tetrachloroethene
1/28/00
100
100
1,1,1-Trichloroethane
1/28/00
100
100
1,1,2-Trichloroethane
1/28/00
100'
100
Trichloroethene
1/28/00
100
100
TrichloroFluoromethane
1/28/00
100
100
Vinyl Chloride
1/28/00
100
100
Surrogate Spike Recoveries
1,4-D ichlorobutane
All values corrected for dilution.
BQL = Below quantitation limit.
Spike Spike
Added Result
40 43
Page 1 of 1
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
810
BQL
BQL
Percent
Recovered
107
Reviewed By:

`i PARADIGM ANALYTICAL LABORATORIES, INC.
Results
for Volatiles
by GC 601
J' Client Sample ID: MW-3
Analyzed By:
RNP
Client Project ID: Toastmaster
Date Collected:
01/17/00
Lab Sample ID: 79800
Date Received:
01/18/00
Lab Project ID: G122-995
Matrix:
Water
l� Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
1/25/00
4
4
BQL
J Bromoform
1/25/00
4
8
BQL
Bromomethane
1/25/00
4
8
BQL
—1 Carbon tetrachloride
1/25100
4
4
BQL
Chlorobenzene
1/25/00
4
4
BQL
Chloroethane
1/25/00
4
4
BQL
5 Chloroform
1/25/00
4
4
BQL
Chloromethane
1/25/00
4
4
BQL
Dibromochloromethane
1/25/00
4
4
BQL
1,2-Dibromoethane (EDB)
1/25/00
4
4
BQL
1,2-Dichlorobenzene
1/25/00
4
4
BQL
_ 1,3-Dichlorobenzene
1/25/00
4
4
BQL
1,4-Dichlorobenzene
1/25/00
4
4
BQL
1,1-Dichloroethane
1/25/00
4
4
BQL
_ 1,2-Dichloroethane
1/25/00
4
4
BQL
1,1-Dichloroethene
1/25/00
4
4
BQL
cis-1,2-Dichloroethene
1/25/00
4
4
BQL
trans-1,2-Dichloroethene
—
1/25/00
4
4
BQL
1,2-Dichloropropane
1/25/00
4
4
BQL
cis-1,3-Dichloropropene
1/25/00
4
4
BQL
trans-1,3-Dichloropropene
1/25/00
4
4
BQL
Methylene Chloride
1125/00
4
20
BQL
_ 1,1,2,2-Tertrachloroethane
1/25/00
4
4
BQL
fTetrachloroethene
1/25/00
4
4
BQL
1,1,1-Trichloroethane
1/25/00
4
4
BQL
1,1,2-Trichloroethane
1/25100
4
4
BQL
Trichloroethene
1/25/00
4
4
54
J TrichloroFluoromethane
1/25/00
4
4
BQL
Vinyl Chloride
1/25/00
4
4
BQL .
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result Recovered
j 1,4-Dichlorobutane
40
40
gg
Comments:
Flags:
All values corrected for dilution.
BQL = Below quantitation limit.
• Page 1 of 1 \_0_Reviewed By:

I
Comments:
Flags:
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Client Sample ID: MW-4 Analyzed By: RNP
Client Project ID: Toastmaster Date Collected: 01/17/00
Lab Sample ID: 79801 Date Received: 01/18/00
Lab Project ID: G122-995 Matrix: Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
1/25/00
40
40
BQL
Bromoform
1/25/00
40
80
BQL
Bromomethane
1/25/00
40
80
BQL
Carbon tetrachloride
1/25/00
40
40
BQL
Chlorobenzene
1/25/00
40
40
BQL
Chloroethane
1/25/00
40
40
BQL
Chloroform
1/25100
40
40
BQL
Chloromethane
1/25/00
40
40
BQL
Dibromochloromethane
1/25/00
40
40
BQL
1,2-Dibromoethane (EDB)
1/25/00
40
40
BQL
1,2-Dichlorobenzene
1/25/00
40
40
BQL
1,3-Dichlorobenzene
1/25/00
40
40
BQL
1,4-Dichlorobenzene
1/25/00
40
40
BQL
1,1-Dichloroethane
1/25/00
40
40
BQL
1,2-Dichloroethane
1/25/00
40
40
BQL
1,1-Dichloroethene
1/25/00
40
40
BQL
cis-1,2-Dichloroethene
1/25/00
40
40
350
trans-1,2-Dichloroethene
1/25100
40
40
BQL
1,2-Dichloropropane
1/25/00
40
40
BQL
cis- 1,3-Dichloropropene
1/25/00
40
40
BQL
trans-1,3-Dichloropropene
1/25/00
40
40
BQL
Methylene Chloride
1/25/00
40
200
BQL
1,1,2,2-Tertrachloroethane
1/25/00
40
40
BQL
Tetrachloroethene
1/25100
40
40
BQL
1,1,1-Trichloroethane
1/25100
40
40
BQL
1.1,2-Trichloroethane
1125/00
40
40
BQL
Trichloroethene
1/25/00
40
40
1300
Trichlorofluoromethane
1/25/00
40
40
BQL
Vinyl Chloride
1/25/00
40
40
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
39
97
All values corrected for dilution.
BQL = Below quantitation limit.
Reviewed By:'I�.,.L Page.1 of 1 �—

PARADIGM ANALYTICAL LABORATORIES, INC.
I
Results for Volatiles
by GC 601
Client Sample ID: MW-5
� P Analyzed By: RNP
Client Project ID: Toastmaster Date Collected: 01/17/00
Lab Sample ID: 79802 Date Received: 01/18/00
j Lab Project ID: G122-995 Matrix: Water
i Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
J Bromodichloromethane
1/25/00
10
10
BQL
Bromoform
1/25/00
10
20
BQL
Bromomethane
1/25/00
10
20
BQL
Carbon tetrachloride
1/26/00
10
10
BQL
j Chlorobeniene
1/25/00
10
10
BQL
Chloroethane
1/25/00
10
10
BQL
Chloroform
1/25/00
10
10
BQL
Chloromethane
1/25/00
10
10
BQL
Dibromochloromethane
1/25/00
10
10
BQL
1,2-Dibromoethane (EDB)
1/25100
10
10
BQL
1,2-Dichlorobenzene
1/25/00
10
10
BQL
-- 1,3-Dichlorobenzene
1/25/00
10
10
BQL
1,4-Dichlorobenzene
1/25/00
10
10
BQL
1,1-Dichloroethane
1/25/00
10
10
BQL
_ 1,2-Dichloroethane
1/25/00
10
10
BQL
1,1-Dichloroethene
1/25/00
10
10
BQL
cis-1,2-Dichloroethene
1/25/00
10
10
BQL
trans-1,2-Dichloroethene
1/25/00
10
10
BQL
1,2-Dichloropropane
1/25100
10
10
BQL
cis-1,3-Dichloropropene
1125/00
10
10
BQL
trans-1,3-Dichloropropene
1/25/00
10
10
BQL
Methylene Chloride
1/25/00
10
50
BQL
- I 1,1,2,2-Tertrachloroethane
1/25/00
10
10
BQL
Tetrachloroethene
1/25/00
10
10
BQL
1,1,1-Trichloroethane
1/25100
10
10
BQL
1,1,2-Trichloroethane
1/25/00
10
10
BQL
Trichloroethene
1/25(00
10
10
390
_. Trichlorofluoromethane
1/25/00
10
10
BQL
Vinyl Chloride
1/25100
10
10
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
41
103
I
J Comments:
Flags:
All values corrected for dilution.
BQL = Below quantitation limit.
Page 1 of 1
Reviewed By:
�—

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
_
by GC 601
J Client Sample ID: MW-6
Analyzed By:
RNP
Client Project ID: Toastmaster
Date Collected:
01/17/00
Lab Sample ID: 79803
Date Received:
01/18/00
Lab Project ID: G122-995
Matrix:
Water
i Compound
Date
Quantitation
Result
--I
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
1/25/00
20
20
BQL
Bromoform
1/25/00
20
40
BQL
Bromomethane
1/25/00
20
40
BQL
Carbon tetrachloride
1/25/00
20
20
BQL
J Chlorobenzene
1/25/00
20
20
BQL
Chloroethane
1/25/00
20
20
BQL
- Chloroform
1/25/00
20
20
BQL
Chloromethane
1/25/00
20
20
BQL
- Dibromochloromethane -
1/25100
20
20
BQL
_ 1,2-Dibromoethane (EDB)
1/25/00
20
20
BQL
1,2-Dichlorobenzene
1/25100
20
20
BQL
1,3-Dichlorobenzene
1/25/00
20
20
BQL
1,4-Dichlorobenzene
1/25/00
20
20
BQL
1,1-Dichloroethane
1/25/00
20
20
BQL
y 1,2-Dichloroethane
1/25/00
20
20
BQL
1,1-Dichloroethene
1/25/00
20
20
BQL
cis- 1,2-Dichloroethene
1/25/00
20
20
76
trans-1,2-Dichloroethene
1/25/00
20
20
BQL
1,2-Dichloropropane
1/25/00
20
20
BQL
cis-1,3-Dichloropropene
1/25/00
20
20
BQL
trans-1,3-Dichloropropene
1/25/00
20
20
BQL
Methylene Chloride
1/25/00
20
100
BQL
1,1,2,2-Tertrachloroethane
1/25/00
20
20
BQL
Tetrachloroethene
1/25/00
20
20
BQL
1,1,1-Trichloroethane
1/25/00
20
20
BQL
1,1,2-Trichloroethane
1/25/00
20
20
BQL
Trichloroethene
1/25100
20
20
610
TrichloroFluoromethane
1/25/00
20
20
BQL
Vinyl Chloride
1/25/00
20
20
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result Recovered
JI 1,4-Dichlorobutane
40
38
96
- Comments:
l Flags:
All values corrected for dilution.
BQL = Below quantitation limit.
Reviewed By:
V
Page 1 of 1

J
Comments:
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Client Sample ID: MW-7 Analyzed By: RNP
Client Project ID: Toastmaster Date Collected: 01/17/00
Lab Sample ID: 79804 Date Received: 01/18/00
Lab Project ID: G122-995 Matrix: Water
Compound
Date Quantitation Result
Analyzed Dilution Limit(ug/L) (ug/L)
Bromodichloromethane
1/25/00
40
40
Bromoform
1/25/00
40
80
Bromomethane
1125/00
40
80
Carbon tetrachloride
1/25/00
40
40
Chlorobenzene
1/25/00
40
40
Chloroethane
1/25/00
40
40
Chloroform
1125/00.
40
40
Chloromethane
1/25/00
40
40
Dibromochloromethane
1/25/00
40
40
1,2-Dibromoethane (EDB)
1/25/00
40
40
1,2-Dichlorobenzene
1/25/00
40
40
1,3-Dichlorobenzene
1125/00
40
40
1,4-Dichlorobenzene
1/25100
40
40
1,1-Dichloroethane
1/25/00
40
40
1,2-Dichloroethane
1/25/00
40
40
1,1-Dichloroethene
1/25/00
40
40
cis-1,2-Dichloroethene
1/25/00
40
40
trans-1,2-Dichloroethene
1/25/00
40
40
1,2-Dichloropropane
1/25/00
40
40
cis-1,3-Dichloropropene
1/25/00
40
40
trans-1,3-Dichloropropene
1/25/00
40
40
Methylene Chloride
1/25/00
40
200
1,1,2,2-Tertrachloroethane
1/25/00
40
40
Tetrachloroethene
1/25/00
40
40
1,1,1-Trichloroethane
1/25/00
40
40
1,1,2-Trichloroethane
1/25/00
40
40
Trichloroethene
1/25/00
40
40
Trichlorofluoromethane
1/25/00
40
40
Vinyl Chloride
1125/00
40
40
Surrogate Spike Recoveries
Spike
Spike
Added
Result
1,4-Dichlorobutane
40
41
All values corrected for dilution.
Flags:
BQL = Below quantitation limit.
Page 1 of 1
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
BQL
58
BQL
BQL
BQL
BQL
BQL
BQL
560
BQL
BQL
1600
BQL
BQL
Percent
Recovered
104
Reviewed By:�

PARADIGM ANALYTICAL LABORATORIES, INC.
Results
for Volatiles
_
by GC 601
Client Sample ID: MW-9
Analyzed By:
RNP
Client Project ID: Toastmaster
Date Collected:
01/17/00
Lab Sample ID: 79805
Date Received:
01/18/00
Lab Project ID: G122-995
Matrix:
Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
1125/00
1
1
BQL
Bromoform
1125/00
1
2
BQL
Bromomethane
`
1/25100
1
2
BQL
Carbon tetrachloride
1/26100
1
1
BQL
Chlorobenzene
1125100
1
1
BQL
Chloroethane
1/25/00
1
1
BQL
Chloroform
1/25/00
1
1
BQL
Chloromethane
1/25/00
1
1
BQL
Dibromochloromethane
1/25/00
1
1
BQL
1,2-Dibromoethane (EDB)
1/25/00
1
1
BQL
1,2-Dichlorobenzene
1/25/00
1
1
BQL
1,3-Dichlorobenzene
1/25/00
1
1
BQL
1,4-Dichlorobenzene
1/25/00
1
1
BQL
1,1-Dichloroethane
1/25/00
1
1
SQL
1,2-Dichloroethane
1/25/00
1
1
BQL
1,1-Dichloroethene
1/25/00
1
1
BQL
cis-1,2-Dichloroethene
1125/00
1
1
BQL
J trans-1,2-Dichloroethene
1/25/00
1
1
BQL
1,2-Dichloropropane
1/25/00
1
1
BQL
cis-1,3-Dichloropropene
1/25/00
1
1
BQL
trans-1,3-Dichloropropene
1/25/00
1
1
BQL
Methylene Chloride
1/25/00
1
5
BQL
-) 1,1,2,2-Tertrachloroethane
1/25/00
1
1
BQL
Tetrachloroethene
1/25/00
1
1
BQL
1,1,1-Trichloroethane
1/25/00
1
1
BQL
1.1,2-Trichloroethane
1/25100
1
1
BQL
Trichloroethene
1/25/00
1
1
21
Trichlorofluoromethane
1/25/00
1
1
BQL
Vinyl Chloride
1/25/00
1
1
SQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result Recovered
1,4-Dichlorobutane
40
44
109
— Comments:
Flags:
All values corrected for dilution.
BQL = Below quantitation limit. 1
Page 1 of 1
Reviewed By: I',v
��-

PARADIGM ANALYTICAL LABORATORIES, INC.
—I Results for Volatiles
by GC 601
J Client Sample ID: MW-10 . Analyzed By: RNP
Client Project ID: Toastmaster Date'Collected: 01/17/00
-� Lab Sample ID: 79806 Date Received: 01/18/00
Lab Project ID: G122-995 Matrix: Water .
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
_f Bromodichloromethane
1/25/00
1
1
BQL
J Bromoform
1/25/00
2
BQL
Bromomethane
1/25/00
1
2
BQL
Carbon tetrachloride
1/25100
1
1
BQL
Chlorobenzene
1/25100
1
1
BQL
Chloroethane
1125/00
1
1
BQL
- Chloroform
1/25/00
1
1
BQL
Chloromethane
1/25100
1
1
BQL
1 Dibromochloromethane
1/25/00
1
1
BQL
1,2-Dibromoethane (EDB)
1/25/00
1
1
BQL
1,2-Dichlorobenzene
1/25/00
1
1
BQL
1,3-Dichlorobenzene
1/25/00
1
1
BQL
1,4-Dichlorobenzene
1/25/00
1
1
BQL
1,1-Dichloroethane
1/25/00
1
1
BQL
1,2-Dichloroethane
1/25/00
1
1
BQL
1,1-Dichloroethene
1/25/00
1
1
BQL
-� cis-1,2-Dichloroethene
1/25/00
1
1
1
trans-1,2-Dichloroethene
1/25/00
1
1
BQL
1 1,2-Dichloropropane
1/25/00
1
1
BQL
cis-1,3-Dichloropropene
1/25/00
1
1
BQL
trans-1,3-Dichloropropene
1/25/00
1
1
BQL
Methylene Chloride
1/25/00
1
5
BQL
1,1,2,2-Tertrachloroethane
1/25/00
1
1
BQL
Tetrachloroethene
1/25/00
1
1
BQL
1,1,1-Trichloroethane
1/25/00
1
1
BQL
1,1,2-Trichloroethane
1/25/00
1
1
Trichloroethene
1/25/00
1
1
BQL
` Trichlorofluoromethane
1/25/00
1
1
21
Vinyl Chloride
1/25/00
1
1
BQL
BQL
JSurrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
i
1,4-Dichlorobutane
40
43
108
Comments:
Flags:
All values corrected for dilution.
BQL =Below quantitation limit.
Page 1 of 1 Reviewed By:

PARADIGM ANALYTICAL LABORATORIES, INC.
I
Results
for Volatiles
by GC 601
Client Sample ID: MW-11
p
Analyzed By:
RNP
Client Project ID: Toastmaster
Date Collected:
01/17/00
— Lab Sample ID: 79807
Date Received:
01/18/00
Lab Project ID: G122-995
Matrix:
Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
1125/00
8
8
BQL
Bromoform
1/25/00
8
16
BQL
Bromomethane
1/25100
8
16
BQL
Carbon tetrachloride
1/25/00
8
8
BQL
Chlorobenzene
1/25/00
8
8
BQL
Chloroethane
1/25/00
8
8
BQL
- Chloroform
1/25/00
8
8
BQL
Chloromethane
1/25/00
8
g
BQL
Dibromochloromethane
1/25/00
8
8
BQL
1,2-Dibromoethane (EDB)
1/25/00
8
8
BQL
1,2-Dichlorobenzene
1/25/00
8
8
BQL
1,3-Dichlorobenzene
1/25/00
8
8
BQL
1,4-Dichlorobenzene
1/25/00
8
8
BQL
1,1-Dichloroethane
1/25/00
8
8
BQL
1,2-Dichloroethane
1/25/00
8
8
BQL
1,1-Dichloroethene
1/25/00
8
8
BQL
cis-1,2-Dichloroethene
1/25/00
8
8
BQL
trans-1,2-Dichloroethene
1/25/00
8
8
BQL
1,2-Dichloropropane
1125100
8
8
BQL
cis-1,3-Dichloropropene
1125/00
8
8
BQL
trans-1,3-Dichloropropene
1/25/00
8
8
BQL
Methylene Chloride
1/25/00
8
40
BQL
1,1,2,2-Tertrachloroethane
1/25/00
8
8
Tetrachloroethene
1/25100
8
g
BQL
1,1,1-Trichloroethane
1/25/00
8
8
BQL
1,1,2-Trichloroethane
1/25/00
8
8
BQL
Trichloroethene
1125100
8
8
BQL
Trichlorofluoromethane
1/25100
8
8
180
Vinyl Chloride
1/25/00
8
8
BQL
BQL .
Surrogate Spike Recoveries
Spike
Spike
Percent
i
Added
Result Recovered
1,4-Dichlorobutane
40
39
97
_I Comments:
All values corrected for dilution.
Flags:
BQL = Below quantitation limit.
Reviewed By: 4
Page 1 of 1 \J"

Comments:
Flags:
PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Volatiles
by GC 601
Client Sample ID: MW-12 Analyzed By: RNP
Client Project ID: Toastmaster Date Collected: 01/17/00
Lab Sample ID: 79808 Date Received: 01/18/00
Lab Project ID: G122-995 Matrix: Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
1/25/00
1
1
BQL
Bromoform
1/25/00
1
2
BQL
Bromomethane
1/25/00
1
2
BQL
Carbon tetrachloride
1126100
1
1
BQL
Chlorobenzene
1125/00
1
1
BQL
Chloroethane
1/25/00
1
1
BQL
Chloroform
1/25/00
1
1
BQL
Chloromethane
1/25/00
1
1
BQL
Dibromochloromethane
1/25/00
1
1
BQL
1,2-Dibromoethane (EDB)
1/25/00
1
1
BQL
1,2-Dichlorobenzene
1/25/00
1
1
BQL
1,3-Dichlorobenzene
1/25/00
1
1
BQL
1,4-Dichlorobe6zene
1/25/00
1
1
BQL
1,1-Dichloroethane
1/25/00
1
1
BQL
1,2-Dichloroethane
1/25/00
1
1
BQL
1,1-Dichloroethene
1/25/00
1
1
BQL
cis-1,2-Dichloroethene
1/25/00
1
1
BQL
trans-1,2-Dichloroethene
1/25/00
1
1
BQL
1,2-Dichloropropane
1/25/00
1
1
BQL
cis-1,3-Dichloropropene
1/25/00
1
1
BQL
trans-1,3-Dichloropropene
1/25/00
1
1
BQL
Methylene Chloride
1/25/00
1
5
BQL
1.1,2,2-Tertrachloroethane
1/25100
1
1
BQL
Tetrachloroethene
1/25/00
1
1
BQL
1,1,1-Trichloroethane
1/25/00
1
1
BQL
1,1,2-Trichloroethane
1/25/00
1
1
BQL
Trichloroethene
1/25/00
1
1
Trichlorofluoromethane
1/25/00
1
1
7
BQL
Vinyl Chloride
1/25/00
1
1
BQL
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
39
99
All values corrected for dilution.
BQL = Below quantitation limit.
Page 1 of 1 Reviewed By: 11,E

PARADIGM ANALYTICAL LABORATORIES,
INC.
Results for Volatiles
by GC 601
J Client Sample ID: Well #13
Analyzed By:
RNP
Client Project ID: Laurinburg
Groundwater
Date Collected: 01/20/00
-i Lab Sample ID: 80007
Date Received: 01/21/00
Lab Project ID: G122-1001
Matrix: Water
I Compound
Date
Quantitation
Result
2
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane.
2/2/00
1
1
BQL
Bromoform
2/2/00
1
2
BQL
Bromomethane
2/2100
1
2
BQL
Carbon tetrachloride
2/2/b0
1
1
BQL
Chlorobenzene
2/2/00
1
1
BQL
Chloroethane
2/2/00
1
1
BQL
Chloroform
2/2/00
1
1
BQL
Chloromethane
2/2/00
1
1
BQL
- Dibromochloromethane
2/2/00
1
1
BQL
1,2-Dibromoethane (EDS)
2/2/00
1
1
BQL
1,2-Dichlorobenzene
2/2/00
1
1
BQL
1,3-Dichlorobenzene
2/2/00
1
1
BQL
1,4-Dichlorobenzene
2/2/00
1
1
BQL
1,1-Dichloroethane
2/2100
1
1
BQL
1,2-Dichloroethane
2/2/00
1
1
BQL
1,1-Dichloroethene
2/2/00
1
1
BQL
cis-1,2-Dichloroethene
212/00
1
1
BQL
trans-1,2-Dichloroethene
2/2/00
1
1
BQL
1,2-Dichloropropane
2/2/00
1
1
BQL
i cis- 1,3-Dichloropropene
212/00
1
1
BQL
trans-1,3-Dichloropropene
2/2/00
1
1
BQL
Methylene Chloride
2/2/00
1
5
BQL
1,1,2,2-Tertrachloroethane
2/2/00
1
1
BQL
Tetrachloroethene
212100
1
1
BQL
1,1,1-Trichloroethane
2/2/00
1
1
BQL
1,1,2-Trichloroethane
2/2/00
1
1
BQL
Trichloroethene
2/2/00
1
1
15
U Trichlorofluoromethane
212/00
1
1
BQL
Vinyl Chloride
2/2100
1
1
BQL
J Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
39
98
I
- Comments:
Flags:
All values corrected for dilution.
BQL = Below quantitation limit.
Reviewed By:�
Page 1 of 1

PARADIGM ANALYTICAL LABORATORIES, INC.
—
Results for Volatiles
by GC 601
Client Sample ID: MW-14
Analyzed By:
RNP
Client Project ID: Toastmaster
Date Collected:
01/17/00
- Lab Sample ID: 79809
Date Received:
01/18/00
Lab Project ID: G122-995
Matrix:
Water
Compound
Date
Quantitation
Result
--
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
1/25/00
1
1
BQL
Bromoform
1/25/00
1
2
BQL
Bromomethane
1/25100
1
2
BQL
Carbon tetrachloride
1/25/00
1 .
1
BQL
Chlorobenzene
1/25/00
1
1
BQL
Chloroethane
1125/00
1
1
BQL
Chloroform
1125/00
1
1
BQL
Chloromethane
1/25/00
1
1
BQL
Dibromochloromethane
1/25/00
1
1
BQL
1,2-Dibromoethane (EDS)
1125/00
1
1
BQL
1,2-Dichlorobenzene
1/25/00
1
1
BQL
-. 1,3-Dichlorobenzene
1/25/00
1
1
BQL
1,4-Dichlorobenzene
1/25/00
1
1
BQL
1,1-Dichloroethane
1/25/00
1
1
gQL
1,2-Dichloroethane
1/25/00
1
1
BQL
1,1-Dichloroethene
1/25/00
1
1
BQL
cis-1,2-Dichloroethene
1/25/00
1
1
BQL
trans-1,2-Dichloroethene
1/25/00
1
1
BQL
1,2-Dichloropropane
1/25/00
1
1
BQL
cis-1,3-Dichloropropene
1/25/00
1
1
BQL
trans-1,3-Dichloropropene
1/25/00
1
1
BQL
Methylene Chloride
1/25100
1
5
BQL
_ 1,1,2,2-Tertrachloroethane
1/25/00
1
1
BQL
Tetrachloroethene
1/25/00
1
1
BQL
1,1,1-Trichloroethane
1/25100
1
1
BQL
1,1,2-Trichloroethane
1/25/00
1
1
BQL
l Trichloroethene
1/25100
1
1
_ Trichlorofluoromethane
1/25/00
1
1
8
Vinyl Chloride
1/25/00
1
1
BQL
i
SQL
—I Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result Recovered
1,4-Dichlorobutane 40 39 98
Comments:
All values corrected for dilution.
Flags:
BQL =Below quantitation limit.
~ Reviewed By:
Page 1 of 1

PARADIGM ANALYTICAL LABORATORIES, INC.
Results
for Volatiles
by GC 601
Client Sample ID: Influent
Analyzed By:
RNP
Client Project ID: Laurinburg
Groundwater
Date Collected:
01/20/00
Lab Sample ID: 60006
Date Received:
01/21/00
Lab Project ID: G122-1001
Matrix:
Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
2/3/00
20
20
BQL
Bromoform
2/3/00
20
40
BQL
Bromomethane
2/3/00
20
40
BQL
Carbon tetrachloride
213/00
20
20
BQL
Chlorobenzene
2/3/00
20
20
BQL
Chloroethane
2/3/00
20
20
BQL
Chloroform
213/00
20
20
BQL
Chloromethane
2/3/00
20
20
BQL
Dibromochloromethane
213/00
20
20
BQL
1,2-Dibromoethane (EDB)
2/3/00
20
20
BQL
1,2-Dichlorobenzene
2/3100
20
20
BQL
1,3-Dichlorobenzene
2/3/00
20
20
BQL
1,4-Dichlorobenzene
2/3/00
20
20
BQL
1,1-Dichloroethane
213/00
20
20
BQL
1,2-Dichloroethane
2/3/00
20
20
BQL
1,1-Dichloroethene
2/3/00
20
20
BQL
cis-1,2-Dichloroethene
213/00
20
20
BQL
trans-1,2-Dichloroethene
2/3/00
20
20
BQL
1,2-Dichloropropane
2/3/00
20
20
BQL
-1 cis-1,3-Dichloropropene
2/3/00
20
20
BQL
I trans-1,3-Dichloropropene
213/00
20
20
BQL
- Methylene Chloride
2/3/00
20
100
BQL
1,1,2,2-Tertrachloroethane
2/3/00
20
20
BQL
Tetrachloroethene
2/3/00
20
20
BQL
- 1,1,1-Trichloroethane
2/3100
20
20
BQL
._ 1,1,2-Trichloroethane
2/3/00
20
20
BQL
Trichloroethene
2/3100
20
20
310
Trichlorofluoromethane
2/3/00
20
20
BQL
Vinyl Chloride
2/3/00
20
20
BQL '
Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result Recovered
Ji 1,4-Dichlorobutane
40
41
103
I
- Comments:
All values corrected for dilution.
Flags:
BQL =Below quantitation limit.
Reviewed By:
Page 1 of 1

PARADIGM ANALYTICAL LABORATORIES,
INC.
'
Results for Volatiles
_
by GC 601
Client Sample ID: Effluent
Analyzed By: RNP
Client Project ID: Laurinburg
Groundwater
Date Collected: 01/20/00
Lab Sample ID: 80004
Date Received: 01/21/00
Lab Project ID: G122-1001
Matrix: Water
JCompound
Date
Quantitation
Result
Analyzed Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
2/2100
1
1
BQL
Bromoform
2/2/00
1
2
BQL
Bromomethane
2/2/00
1
2
BQL
Carbon tetrachloride
2/2/b0
1
1
BQL
Chlorobenzene
2/2100
1
1
BQL
Chloroethane
2/2/00
1
1
BQL
Chloroform
2/2/00
1
1
BQL
Chloromethane
2/2/00
1
1
BQL
Dibromochloromethane
2/2/00
1
1
BQL
_ 1,2-Dibromoethane (EDB)
2/2/00
1
1
BQL
I 1,2-Dichlorobenzene
2/2100
1
1
BQL
1,3-Dichlorobenzene
2/2/00
1
1
BQL
1,4-Dichlorobenzene
2/2100
1
1
BQL
1,1-Dichloroethane
2/2100
1
1
BQL
1,2-Dichloroethane
2/2/00
1
1
BQL
1,1-Dichloroethene
2/2/00
1
1
BQL
-� cis-1,2-Dichloroethene
2/2100
1
1
BQL
trans-1,2-Dichloroethene
J
212/00
1
1
BQL
1,2-Dichloropropane
2/2/00
1
1
BQL
cis-1,3-Dichloropropene
2/2/00
1
1
BQL
trans-1,3-Dichloropropene
2/2/00
1
1
BQL
' Methylene Chloride
2/2/00
1
5
BQL
1,1,2,2-Tertrachloroethane
2/2/00
1
1
BQL
Tetrachloroethene
2/2/00
1
1
BQL
- 1,1,1-Trichloroethane
2/2/00
1
1
BQL
1,1,2-Trichloroethane
212/00
1
1
BQL
Trichloroethene
2/2/00
1
1
2
Trichlorofluoromethane
2/2/00
1
1
BQL
Vinyl Chloride
212/00
1
1
BQL
{{
_I Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
39
97
I
J
Comments:
All values corrected for dilution.
Flags:
BQL = Below quantitation limit. \
Reviewed By:. J
Page 1 of 1 TT"—

PARADIGM ANALYTICAL LABORATORIES, INC.
Results
for Volatiles
by GC 601
Client Sample ID: Cooling Tower
Analyzed By:
RNP
Client Project ID: Laurinburg
Groundwater
DateCollected:
01/20/00
Lab Sample ID: 80005
Date Received:
01/21/00
Lab Project ID: G122-1001
Matrix:
Water
Compound
Date
Quantitation
Result
Analyzed
Dilution
Limit (ug/L)
(ug/L)
Bromodichloromethane
2/2/00
1
1
BQL
Bromoform
2/2/00
1'
2
BQL
Bromomethane
2/2/00
1
2
BQL
Carbon tetrachloride
2/2/00
1
1
BQL
Chlorobenzene
2/2/00
1
1
BQL
Chloroethane
2/2/00
1
1
BQL
Chloroform
2/2/00
1
1
BQL
Chloromethane
2/2/00
1
1
BQL
Dibromochloromethane
2/2/00
1
1
BQL
1,2-Dibromoethane (EDB)
2/2/00
1
1
BQL
1,2-Dichlorobenzene
212/00
1
1
BQL
1,3-Dichlorobenzene
2/2/00
1
1
BQL
1,4-Dichlorobenzene
2/2/00
1
1
BQL
1,1-Dichloroethane
2/2/00
1
1
BQL
1,2-Dichloroethane
2/2100
1
1
BQL
1,1-Dichloroethene
2/2/00
1
1
BQL
cis-1,2-Dichloroethene
2/2/00
1
1
BQL
trans-1,2-Dichloroethene
2/2/00
1
1
BQL
1,2-Dichloropropane
2/2/00
1
1
BQL
cis-1,3-Dichloropropene
2/2/00
1
1
BQL
trans-1,3-Dichloropropene
212/00
1
1
BQL
Methylene Chloride
2/2/00
1
5
BQL
1,1,2,2-Tertrachloroethane
2/2100
1
1
BQL
Tetrachloroethene
212/00
1
1
BQL
1,1,1-Trichloroethane
2/2/00
1
1
BQL
1,1,2-Trichloroethane
2/2/00
1
1
BQL
Trichloroethene
2/2/00
1
1
BQL
Trichlorofluoromethane
2/2/00
1
1
BQL
Vinyl Chloride
_I
2/2100
1
1
BQL
J Surrogate Spike Recoveries
Spike
Spike
Percent
Added
Result
Recovered
1,4-Dichlorobutane
40
37
92
Comments:
Flags:
All values corrected for dilution.
BQL = Below quantitation limit..
Reviewed By:
Page 1 of 1

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID: MW-1
Client Project ID: Toastmaster
Lab Sample ID: 79798
Lab Project ID: G122-995.
Matrix: Water
Parameter Result
pH
6.26
Date Collected:
1/17100
Date Received:
1/18/00
Analyzed By:
EES
Date
Analyzed
1 /21 /00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By:

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
I
J
Client Sample ID: M W-2
Client Project ID: Toastmaster
Lab Sample ID: 79799
Lab Project ID: G122-995
Matrix: Water
Parameter Result
pH
5.88
Date Collected:
1/17/00
Date Received:
1/18/00
Analyzed By:
EES
Date
Analyzed
1 /21 /00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By: \„/

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID: MW-3
Client Project ID: Toastmaster
Lab Sample ID: 79800
Lab Project ID: G122-995
Matrix: Water
Parameter Result
ME
5.97
Date Collected:
1/17/00
Date Received:
1/18/00
Analyzed By:
EES
Date
Analyzed
1/21/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By:

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID: MW-4
Client Project ID: Toastmaster
Lab Sample ID: 79801
Lab Project ID: G122-995
Matrix: Water
Parameter Result
pH
5.54
Date Collected:
1/17/00
Date Received:
1/18/00
Analyzed By:
EES
Date
Analyzed
1 /21 /00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
J
Reviewed By:\

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID: MW-5 Date Collected: 1/17/00
Client Project ID: Toastmaster Date Received: 1/18/00
Lab Sample ID: 79802 Analyzed By: EES
Lab Project ID: G122-995
Matrix: Water
Parameter Result Date
Analyzed
pH 5.55 1/21/00
0
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By: V"

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID: MW-6
Client Project ID: Toastmaster
Lab Sample ID: 79803
Lab Project ID: G122-995
Matrix: Water
Parameter Result
pH
5.00
Date Collected:
1/17/00
Date Received:
1/18/00
Analyzed By: •
EES
Date
Analyzed
1/21/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By:\,;,

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID: MW-7 Date Collected: 1/17100
Client Project ID: Toastmaster Date Received: 1/18/00
Lab Sample ID: 79804 Analyzed By: EES
Lab Project ID: G122-995
Matrix: Water
Parameter Result Date
Analyzed
pH 5.37 1/21/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By:

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID: MW-9
Client Project ID: Toastmaster
Lab Sample ID: 79805
Lab Project ID: G122-995
Matrix: Water
Parameter Result
pH
4.90
Date Collected:
1/17100
Date Received:
1/18/00
Analyzed By:
EES
Date
Analyzed
1 /21 /00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By:

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
41
J
J
Client Sample ID: MW-10
Client Project ID: Toastmaster
Lab Sample ID: 79806
Lab Project ID: G122-995
Matrix: Water
Parameter
pH
Date Collected:
1/17/00
Date Received:
1/18/00
Analyzed By:
EES
Result Date
Analyzed
4.79 1 /21 /00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By:\0--

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID:
MW-11
Date Collected: 1/17/00
Client Project ID:
Toastmaster
Date Received: 1/18/00
Lab Sample ID:
79807
Analyzed By: EES
Lab Project ID:
G122-995
Matrix:
Water
Parameter
Result
Date
Analyzed
pH
5.03
1/21/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By: \, 1

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID: MW-12
Client Project ID: Toastmaster
Lab Sample ID: 79808
Lab Project ID: G122-995
Matrix: Water
Parameter Result
pH 5.09
Date Collected:
1/11/00
Date Received:
1/18/00
Analyzed By:
EES
Date
Analyzed
1/21/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By: j� `

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID: Well #13 Date Collected: 1/20/00
Client Project ID: Laurinburg Groundwater Date Received: 1/21/00
Lab Sample ID: 60007 Analyzed By: EES
Lab Project ID: G122-1001
Matrix: Water
Parameter Result Date
Analyzed
pH 5.46 1124/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of'the 15 minute holding time.
Reviewed By:

PARADIGM ANALYTICAL LABORATORIES,
INC.
Results for Inorganics;
Client Sample ID: MW-14 Date Collected:
1/17/00
--) Client Project ID: Toastmaster Date Received:
1/18/00
Lab Sample ID: 79809 Analyzed By:
EES
Lab Project ID: G122-995
Matrix: Water
-- Parameter Result
Date
Analyzed
- pH 5.59
1/21/00
l
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By:\

PARADIGM ANALYTICAL LABORATORIES, INC.
i
— Results for Inorganics
Client Sample ID: Influent Date Collected: 1/20/00
Client Project ID: Laurinburg Groundwater Date Received: 1/21/00
Lab Sample ID: 80006 Analyzed By: EES
Lab Project ID: G122-1001.
Matrix: Water
Parameter Result Date
Analyzed
pH 5.08 1/24/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By:�

PARADIGM ANALYTICAL LABORATORIES, INC.
Results for Inorganics
Client Sample ID: Effluent
Client Project ID: Laurinburg Groundwater
Lab Sample ID: 80004
Lab Project ID: G122-1001.
Matrix: Water
Parameter Result
pH
6.44
Date Collected: 1/20/00
Date Received: 1/21/00
Analyzed By: EES
Date
Analyzed
1/24/00
Comments:
Per NCDENR, pH measurements taken more than 15 minutes after sample
collection are non -reportable for NPDES compliance monitoring.
This analysis was performed outside of the 15 minute holding time.
Reviewed By:�

MRADIGM ANALYTICAL LAB6KxiOk1hN,ISU.-
527 Northchase Parkway SE, Wilmington, NC 28405
,ione: (910)-350-1903 FAX: [phone]
Chain -of Custody Record & Analytical Request
Bent: Ai3-&nNP,jLc- Az Z4-4 Project ID: Date: 11(si(OL)
Jdress:21z9 '(-,N (?i VN\ *02- P.O. Number: Turnaround:
ddress:k--)U24nV6A1 .,5-- Contact: Job Number:
note #: Phone: AkU -ick3-I451
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kRADIGM ANALYTICAL LABORATORIES, INC.
27 Northchase Parkway SE, Wilmington, NC 28405
ione: (910)-350-1903 FAX: [phone]
Chain -of Custody Record & Analytical Request
'� i9 ient: / Project ID: J4&Fry%0kShe2 Date: — ALW—C-0 Report To:
[dress:_ZM% V`z P.O. Number: Turnaround: 5Y9.
(dress: k,,5,Arv% -"+!3 V.,q rsc Contact: 5r,MA--0-Job Number: qd(M) W�
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627 Nortfichase Parkway SE, Wilmington, NC 28405 Chain -of Custody Record & Analytical Request coc# 1498 7
hone: (910)-350-1903 FAX: [phone] Page — of
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