NCG210444_2023 DMR_20231208

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report(DMR) Form for NCG080000
Transit and Transportation
Click here for instructions
Complete,sign,scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report(DMR) Upload form within
30 days of receiving sampling results. Mail the original,signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage No. NCGO8 NCG210444 Person Collecting Samples:Jay Ennis
Facility Name:Wyeth LLC. Laboratory Name: Eurofins Environmental Testing
Facility County:Lee Laboratory Cert. No.:591 (TSS)&269 (O&G)
Discharge during this period:El Yes ❑No (if no,skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances?❑Yes 0 No
If so,which Tier(I, II,or III)?N/A
A copy of this DMR has been uploaded electronically via https://edocs.deq.nc.gov/Forms/SW-DMR 0 Yes El No
Date Uploaded:08DEC2023
Analytical Monitoring Requirements for Vehicle&Equipment Maintenance Areas—Benchmarks in(Red)
Parameter Parameter Dutfall07 Outfall Outfall Outfall Outfall
Code
N/A Receiving Stream Class C
N/A Date Sample Collected MM/DD/YYYY 10/20/2023
46529 24-Hour Rainfall in inches 0.28
C0530 TSS in mg/L(100 or 50') 50
00552 Non-Polar Oil&Grease in mg/L(15) < 1.4
00400 pH in standard units(6.0—9.0 FW, N/A
6.8-8.5SW)
NCOIL Estimated New Motor/Hydraulic Oil 55
Usage in gal/month
*Outfalls to Outstanding Resource Waters(ORW),High Quality Waters(HQW),Trout Waters(Tr)and Primary Nursery Areas(PNA)
have a benchmark T55 limit of 50 mg/L.All other water classifications have a benchmark of 100 mg/L
FW(Freshwater)SW(Saltwater)
Notes(optional):
"I certify by my signature below,under penalty of law,that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my
inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information
submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there are significant penalties for submitting
false information,including the possibility of fines and imprisonment for knowing violations."
08DEC2023
Signature of Permitte Delegated Authorized Individual Date
[e-mail] 9195665210
Email Address Phone Number

tiff eurofins
Environment Testing
f ANALYTICAL REPORT
PREPARED FOR
Attn: Connor Jarvis
Pfizer Inc.
4300 Oak Park
Sanford, North Carolina 27330
Generated 10/31/2023 4:48:21 AM
JOB DESCRIPTION
Stormwater
JOB NUMBER
752-12951-1
Eurofins Raleigh
102-A Woodwinds Industrial Court
Cary NC 27511
m
Page 1 of 17 •I° Y
See page two for job notes and contact information. g G• E O L.
C,•

Eurofins Raleigh
9
Job Notes
This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the
samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this
page.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory.All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
Authorization
CifThetrack. cDairrI9m Generated
10/31/2023 4:48:21 AM
Authorized for release by
Amanda Gaines,Project Manager
[e-mail]
[phone]
Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast,LLC,a company within Eurofins Environment Testing Group of Companies
Page 2 of 17 10/31/2023

Client: Pfizer Inc. Laboratory Job ID: 752-12951-1
Project/Site:Stormwater
Table of Contents
Cover Page 1
Table of Contents 3
Definitions/Glossary 4
Case Narrative 5
Detection Summary 6
Client Sample Results 7
QC Sample Results 8
QC Association Summary 9
Lab Chronicle 10
Certification Summary 11
Method Summary 12
Sample Summary 13
Chain of Custody 14
Receipt Checklists 16
Eurofins Raleigh
Page 3 of 17 10/31/2023

Definitions/Glossary
Client:Pfizer Inc. Job ID:752-12951-1
Project/Site: Stormwater
GlossaryEl
Abbreviation These commonly used abbreviations may or may not be present in this report.
c Listed under the"D"column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio(normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit(DoD/DOE)
DL,RA,RE,IN Indicates a Dilution,Re-analysis,Re-extraction,or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration(Radiochemistry)
EDL Estimated Detection Limit(Dioxin)
LOD Limit of Detection(DoD/DOE)
LOQ Limit of Quantitation(DoD/DOE)
MCL EPA recommended"Maximum Contaminant Level"
MDA Minimum Detectable Activity(Radiochemistry)
MDC Minimum Detectable Concentration(Radiochemistry)
MDL Method Detection Limit
ML Minimum Level(Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit(or MDL or EDL if shown)
NEG Negative/Absent
POS Positive/Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio(Radiochemistry)
RL Reporting Limit or Requested Limit(Radiochemistry)
RPD Relative Percent Difference,a measure of the relative difference between two points
TEF Toxicity Equivalent Factor(Dioxin)
TEQ Toxicity Equivalent Quotient(Dioxin)
TNTC Too Numerous To Count
Eurofins Raleigh
Page 4 of 17 10/31/2023

Case Narrative
Client:Pfizer Inc. Job ID:752-12951-1
Project/Site:Stormwater
Job ID: 752-12951-1
Laboratory: Eurofins Raleigh 4
Narrative
Job Narrative
752-12951-1
Analytical test results meet all requirements of the associated regulatory program listed on the Accreditation/Certification Summary Page
unless otherwise noted under the individual analysis. Data qualifiers are applied to indicate exceptions. Noncompliant quality control
(QC)is further explained in narrative comments.
Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted.In these situations,to
demonstrate precision and accuracy at a batch level,a LCS/LCSD may be performed,unless otherwise specified in the method.
Surrogate and/or isotope dilution analyte recoveries(if applicable)which are outside of the QC window are confirmed unless attributed
to a dilution or otherwise noted in the narrative.
Regulated compliance samples(e.g.SDWA,NPDES)must comply with the associated agency requirements/permits.
Receipt
The samples were received on 10/25/2023 10:06 AM. Unless otherwise noted below,the samples arrived in good condition,and,where
required,properly preserved and on ice. The temperature of the cooler at receipt time was 5.0°C
General Chemistry
No additional analytical or quality issues were noted,other than those described above or in the Definitions/Glossary page.
Eurofins Raleigh
Page 5 of 17 10/31/2023

Detection Summary
Client:Pfizer Inc. Job ID:752-12951-1
Project/Site:Stormwater
Client Sample ID: Oil & Grease Lab Sample ID: 752-12951-1
No Detections.
Client Sample ID: Total Suspended Solids Lab Sample ID: 752-12951-2
Analyte Result Qualifier RL RL Unit Dil Fac D Method Prep Type
Total Suspended Solids 50 5.0 5.0 mg/L 1 SM 2540D Total/NA
This Detection Summary does not include radiochemical test results.
Eurofins Raleigh
Page 6 of 17 10/31/2023

Client Sample Results
Client:Pfizer Inc. Job ID:752-12951-1
Project/Site:Stormwater
Client Sample ID: Oil & Grease Lab Sample ID: 752-12951-1
Date Collected: 10/20/23 13:50 Matrix:Water
Date Received: 10/25/23 10:06
General Chemistry
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
TPH(1664B) <1.4 4.9 1.4 mg/L 10/30/23 14:10 10/30/23 18:37 1
Client Sample ID: Total Suspended Solids Lab Sample ID: 752-12951-2 6
Date Collected: 10/20/23 13:50 Matrix:Water
Date Received: 10/25/23 10:06
General Chemistry
Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac
Total Suspended Solids(SM 50 5.0 5.0 mg/L 10/27/23 08:26 1
2540D)
Eurofins Raleigh
Page 7 of 17 10/31/2023

QC Sample Results
Client: Pfizer Inc. Job ID:752-12951-1
Project/Site:Stormwater
Method: 1664E -HEM and SGT-HEM
Lab Sample ID:MB 680-805424/1-A Client Sample ID: Method Blank
Matrix:Water Prep Type:Total/NA
Analysis Batch:805442 Prep Batch:805424
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
TPH <1.4 5.0 1.4 mg/L 10/30/2314.10 10/30/23 18:37 1
Lab Sample ID: LCS 680-805424/2-A Client Sample ID: Lab Control Sample 101
Matrix:Water Prep Type:Total/NA
Analysis Batch:805442 Prep Batch:805424
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
TPH 20.0 15.80 mg/ 79 64.132
Lab Sample ID: LCSD 680-805424/3-A Client Sample ID: Lab Control Sample Dup
Matrix:Water Prep Type:Total/NA
Analysis Batch:805442 Prep Batch:805424
Spike LCSD LCSD %Rec RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
TPH 20.0 15.00 mg/L 75 64-132 5 34
Method: SM 2540D -Solids, Total Suspended (TSS)
Lab Sample ID: MB 752-4962/1 Client Sample ID: Method Blank
Matrix:Water Prep Type:Total/NA
Analysis Batch:4962
. MB MB
Analyte Result Qualifier RL RL Unit D Prepared Analyzed Dil Fac
Total Suspended Solids <2.5 2.5 2.5 mg/L 10/27/23 08:26 1
Lab Sample ID: LCS 752-4962/2 Client Sample ID: Lab Control Sample
Matrix:Water Prep Type:Total/NA
Analysis Batch:4962
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
Total Suspended Solids 100 104 mg/L 104 80.120
Eurofins Raleigh
Page 8 of 17 10/31/2023

QC Association Summary
Client:Pfizer Inc. Job ID:752-12951-1
Project/Site:Stormwater
General Chemistry
Analysis Batch:4962
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
752-12951-2 Total Suspended Solids TotaUNA Water SM 2540D
MB 752-4962/1 Method Blank Total/NA Water SM 2540D
LCS 752-4962/2 Lab Control Sample TotaUNA Water SM 2540D
Prep Batch:805424
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
752-12951-1 Oil&Grease TotaUNA Water 1664B
MB 680-805424/1-A Method Blank Total/NA Water 1664B 8
LCS 680-805424/2-A Lab Control Sample Total/NA Water 1664B
LCSD 680-805424/3-A Lab Control Sample Dup TotaUNA Water 1664E
Analysis Batch:805442
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
752-12951-1 Oil&Grease TotaUNA Water 1664B 805424
MB 680-805424/1-A Method Blank Total/NA Water 1664B 805424
LCS 680-805424/2-A Lab Control Sample TotaUNA Water 1664B 805424
LCSD 680-805424/3-A Lab Control Sample Dup TotaUNA Water 1664B 805424
Eurofins Raleigh
Page 9 of 17 10/31/2023

Lab Chronicle
Client: Pfizer Inc. Job ID:752-12951-1
Project/Site:Stormwater
Client Sample ID: Oil & Grease Lab Sample ID: 752-12951-1
Date Collected: 10/20/23 13:50 Matrix:Water
Date Received: 10/25/23 10:06
Batch Batch Dilution Batch Prepared
Prep Type Type Method Run Factor Number Analyst Lab or Analyzed
Total/NA Prep 16648 805424 TD EET SAV 10/30/23 14:10
Total/NA Analysis 16648 1 805442 TD EET SAV 10/30/23 18:37
Client Sample ID: Total Suspended Solids Lab Sample ID: 752-12951-2
Date Collected:10/20/23 13:50 Matrix:Water
Date Received: 10/25/23 10:06
Batch Batch Dilution Batch Prepared
Prep Type Type Method Run Factor Number Analyst Lab or Analyzed 9
Total/NA Analysis SM 2540D 1 4962 MDF EET ESC 10/27/23 08:26
Laboratory References:
EET ESC=Eurofins Raleigh,102-A Woodwinds Industrial Court,Cary,NC 27511,TEL[phone]
EET SAV=Eurofins Savannah,5102 LaRoche Avenue,Savannah,GA 31404,TEL[phone]
Eurofins Raleigh
Page 10 of 17 10/31/2023

Accreditation/Certification Summary
Client: Pfizer Inc. Job ID:752-12951-1
Project/Site:Stormwater
Laboratory: Eurofins Raleigh
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina(WW/SW) State 591 12-31-23
Laboratory: Eurofins Savannah
The accreditations/ertdications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina(WW/SW) State 269 12-31-23
E
Eurofins Raleigh
Page 11 of 17 10/31/2023

Method Summary
Client: Pfizer Inc. Job ID:752-12951-1
Project/Site: Stormwater
Method Method Description Protocol Laboratory
16648 HEM and SGT-HEM 1664B EET SAV
SM 2540D Solids,Total Suspended(TSS) SM EET ESC
1664E HEM and SGT-HEM (Aqueous) 1664E EET SAV
Protocol References:
1664B=EPA-821-98-002
SM="Standard Methods For The Examination Of Water And Wastewater"
Laboratory References:
EET ESC=Eurofins Raleigh,102-A Woodwinds Industrial Court,Cary,NC 27511,TEL[phone]
EET SAV=Eurofins Savannah,5102 LaRoche Avenue,Savannah,GA 31404,TEL[phone]
Eurofins Raleigh
Page 12 of 17 10/31/2023

Sample Summary
Client: Pfizer Inc. Job ID:752-12951-1
Project/Site:Stormwater
Lab Sample ID Client Sample ID Matrix Collected Received
752-12951-1 Oil&Grease Water 10/20/23 13:50 10/25/23 10:06
752-12951-2 Total Suspended Solids Water 10/20/23 13:50 10/25/23 10:06
Eurofins
Page 13 of 17 10/31/2023

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Login Sample Receipt Checklist
Client:Pfizer Inc. Job Number:752-12951-1
Login Number:12951 List Source:Eurofins Raleigh
List Number:1
Creator:Yonish,Rachel
Question Answer Comment
Radioactivity wasn't checked or is</=background as measured by a survey True
meter.
The cooler's custody seal,if present,is intact. True
Sample custody seals,if present,are intact. True
The cooler or samples do not appear to have been compromised or True
tampered with.
Samples were received on ice. True
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. True
Is the Field Sampler's name present on COC? True
There are no discrepancies between the containers received and the COC. True
Samples are received within Holding Time(excluding tests with immediate True
HTs)
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. True
There is sufficient vol.for all requested analyses,incl.any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is True
<6mm(1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. True
Eurofins Raleigh
Page 16 of 17 10/31/2023

Login Sample Receipt Checklist
Client:Pfizer Inc. Job Number:752-12951-1
Login Number:12951 List Source:Eurofins Savannah
List Number:2 List Creation:10/27/23 12:47 PM
Creator:Harley,Tynisha
Question Answer Comment
Radioactivity wasn't checked or is</=background as measured by a survey N/A
meter.
The cooler's custody seal,if present,is intact. True
Sample custody seals,if present,are intact. True
The cooler or samples do not appear to have been compromised or True
tampered with.
Samples were received on ice. True
Cooler Temperature is acceptable. True
Cooler Temperature is recorded. True
COC is present. True
COC is filled out in ink and legible. True
COC is filled out with all pertinent information. True
Is the Field Sampler's name present on COC? True
There are no discrepancies between the containers received and the COC. True
Samples are received within Holding Time(excluding tests with immediate True 14
HTs)
Sample containers have legible labels. True
Containers are not broken or leaking. True
Sample collection date/times are provided. True
Appropriate sample containers are used. True
Sample bottles are completely filled. True
Sample Preservation Verified. N/A
There is sufficient vol.for all requested analyses,incl.any requested True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is N/A
<6mm(1/4").
Multiphasic samples are not present. True
Samples do not require splitting or compositing. True
Residual Chlorine Checked. N/A
Eurofins Raleigh
Page 17 of 17 10/31/2023