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NC0021181_Renewal (Application)_20231206
ROY COOPER Governor ELIZABETH S. BISER Secretary RICHARD E. ROGERS, JR. Director Barry Webb City of Belmont PO Box 431 Belmont, NC 28012-0431 Subject: Permit Renewal Application No. NCO021181 Belmont WWTP Gaston County Dear Applicant: NORTH CAROLINA Environmental Quality December 06, 2023 The Water Quality Permitting Section acknowledges the December 6, 2023 receipt of your permit renewal application and supporting documentation. Your application will be assigned to a permit writer within the Section's NPDES WW permitting branch. Per G.S. 150B-3 your current permit does not expire until permit decision on the application is made. Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit. The permit writer will contact you if additional information is required to complete your permit renewal. Please respond in a timely manner to requests for additional information necessary to allow a complete review of the application and renewal of the permit. Information regarding the status of your renewal application can be found online using the Department of Environmental Quality's Environmental Application Tracker at: https://deg.nc.gov/permits-regulations/permit-guidance/environmental-application-tracker If you have any additional questions about the permit, please contact the primary reviewer of the application using the links available within the Application Tracker. ec: WQPS Laserfiche File w/application Sincerely Cynthia Demery Administrative Assistant Water Quality Permitting Section D Q> North Carolina Department of Environmental Quality I Division of Water Resources Mooresville Regional Office 1 610 East Center Avenue, Suite 301 1 Mooresville, North Carolina 28115 704.663.1699 F)2 hdrinc.com November 28, 2023 Mr. Gary Perlmutter, M.Sc. Division of Water Resources Water Quality Permitting Section — NPDES 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: NPDES Renewal Application City of Belmont Belmont WWTP NCO021181 Dear Mr. Perlmutter, RECEIVED DEir 06 _023 NCDEQ1D WR/ NPpES HDR Engineering, Inc. of the Carolinas (HDR), an authorized agent of the City of Belmont, is submitting an NPDES permit renewal application to the North Carolina Department of Environmental Quality (NCDEQ). There have been no expanded facilities since the last permit submittal and the design flow rate is to remain the same. Enclosed are the following items for your review for the referenced project: • EPA Form 2A for new and existing publicly owned treatment works • Topographic Map • Flow Diagram • Chemical Addendum to NPDES Application • Mercury Minimization Plan • Sludge Management Plan • City of Belmont WWTP Effluent Pollutant Scans Whole Effluent Toxicity Reports have been previously submitted to NCDEQ on the dates listed in EPA Form 2A and therefore were not attached to the application per instruction item 3.19. An additional Whole Effluent Toxicity Report will be submitted for 2023 after the NPDES renewal application has been submitted. Sincerely, HDR Engineering, Inc. of the Carolinas Will Shull, E. Project Manager 440 S Church Street, Suite 1200, Charlotte, NC 28202-2075 704.338.6700 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000570338 NCO021181 City of Belmont WWTP OMB No. 2040-0004 U.S. Environmental Protection Agency L EPA Application for NPDES Permit to Discharge Wastewater NEW AND EXISTING PUBLICLY OWNIMXREAktol W K SECTION•N INFORMATION FOR Facility name 1.1 Belmont Wastewater Treatment Plant DEC 0 Mailing address (street or P.O. box) PO Box 431 City or town Stat o Belmont NC 28012 E Contact name (first and last) Title Phone number Email address Tanya S. Carter (704) 825-3791 tsetzer@cityofbelmont.org c ' Location address (street, route number, or other specific identifier) ❑ Same as mailing address 298 Parkdale Dr. City or town State ZIP code Belmont NC 28012 1.2 Is this application for a facility that has yet to commence discharge? ❑ Yes -* See instructions on data submission ❑✓ No requirements for new dischargers. 1.3 Is applicant different from entity listed under Item 1.1 above? ❑ Yes ❑✓ No 4 SKIP to Item 1.4. Applicant name Applicant address (street or P.O. box) 0 w <a E `o City or town State ZIP code w- c ca Contact name (first and last) Title Phone number Email address CL a a 1.4 Is the applicant the facility's owner, operator, or both? (Check only one response.) ❑ Owner ❑ Operator ❑✓ Both 1.5 To which entity should the NPDES permitting authority send correspondence? (Check only one response.) ❑✓ Facility ❑ Applicant ❑ Facility and applicant (they are one and the same) 1.6 Indicate below any existing environmental permits. (Check all that apply and print or type the corresponding permit r number for each. E a5 Existing Environmental Permits ✓❑ NPDES (discharges to surface ❑ RCRA (hazardous waste) ❑ UIC (underground injection water) control) E: NCO021181 2 ❑ PSD (air emissions) ❑ Nonattainment program (CAA) ❑ NESHAPs (CAA) c w rn N ❑ Ocean dumping (MPRSA) ❑ Dredge or fill (CWA Section ❑ Other (specify) w 404) EPA Form 3510-2A (Revised 3-19) Page 1 EPA Identification Number NPDES Permit Number acility Name Form Approved 03/05/19 110000570338 NCO021181 =BelmontWWTP OMB No. 2040-0004 1.7 Provide the collections stem information requested below for the treatment works. Municipality Population Collection System Type Served Served indicatepercentage)Ownership Status Belmont 100 % separate sanitary sewer ❑ Own ❑ Maintain Z16,489 % combined storm and sanitary sewer ❑ Own ElMaintain ❑ Unknown ElOwn ElMaintain co c % separate sanitary sewer ElOwn ElMaintain % combined storm and sanitary sewer ❑ Own ❑ Maintain cc c El Unknown ❑ Own El Maintain a % separate sanitary sewer ❑ Own ❑ Maintain a % combined storm and sanitary sewer ❑ Own ❑ Maintain c ❑ Unknown ❑ Own ❑ Maintain a % separate sanitary sewer ❑ Own ❑ Maintain combined storm and sanitary sewer ❑ Own ❑ Maintain co% c ❑ Unknown I ElOwn ❑ Maintain Z Total 16,489 Population U Served Separate Sanitary Sewer System Combined Storm and Sanitary Sewer Total percentage of each type of sewer line in miles 100 % ° 13 /° z' 1.8 Is the treatment works located in Indian Country? c _ 0 V ElYes ❑✓ No 1.9 Does the facility discharge to a receiving water that flows through Indian Country? ❑ Yes ❑✓ No 1.10 Provide design and actual flow rates in the designated spaces. Design Flow Rate 5 mgd R = Annual Average Flow Rates Actual Two Years Ago Last Year This Year c 30 1.291 mgd 1.846 mgd 1.917 mgd LZ Maximum Daily Flow Rates Actual Two Years Ago Last Year This Year 2.468 mgd 3.200 mgd 6.977 mgd N 1.11 Provide the total number of effluent discharge points to waters of the United States by type. r oTotal Number of Effluent Dischar a Points b Type a a a) Combined Sewer Constructed T Treated Effluent Untreated Effluent Overflows Bypasses Emergency Overflows 1 N/A N/A N/A N/A EPA Form 3510-2A (Revised 3-19) Page 2 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000570338 NCO021181 City of Belmont WW rP OMB No. 2040-0004 Outfalls Other Than to Waters of the United States 1.12 Does the POTW discharge wastewater to basins, ponds, or other surface impoundments that do not have outlets for discharge to waters of the United States? ❑ Yes ❑✓ No + SKIP to Item 1.14. 1.13 Provide the location of each surface impoundment and associated discharge information in the table below. Surface Im oundment Location and Dischar a Data Average Daily Volume Continuous or Intermittent Location Discharged to Surface (check one) Impoundment ❑ Continuous N/A N/A gpd ❑ Intermittent ❑ Continuous N/A N/A gpd ❑ Intermittent ❑ Continuous w -a N/A N/A gpd ❑ Intermittent w 1.14 Is wastewater applied to land? M ❑ Yes ❑✓ No SKIP to Item 1.16. 0 1.15 Provide the land application site and discharge data requested below. in Land A lication Site and Discharge Data o Average Daily Volume Continuous or 0 Location Size Applied Intermittent check one N 0 N/A N/A acres N/A gp d ❑ Continuous ❑ Intermittent c N/A N/A acres N A gp / d ❑ Continuous ❑ Intermittent 0 c N/A N/A acres N/A gpd ❑ Continuous ❑ Intermittent 1.16 Is effluent transported to another facility for treatment prior to discharge? o ElYes m No + SKIP to Item 1.21. 1.17 Describe the means by which the effluent is transported (e.g., tank truck, pipe). N/A 1.18 Is the effluent transported by a party other than the applicant? ❑ Yes ✓❑ No 4 SKIP to Item 1.20. 1.19 Provide information on the transporter below. Trans orter Data Entity name Mailing address (street or P.O. box) N/A N/A City or town State ZIP code N/A N/A N/A Contact name (first and last) Title N/A N/A Phone number Email address N/A EPA Form 3510-2A (Revised 3-19) Page 3 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000570338 NCO021181 City of Belmont WWTP OMB No, 2040-0004 1.20 In the table below, indicate the name, address, contact information, NPDES number, and average daily flow rate of the receiving facility. Receivinq IF cilitv Data Facility name Mailing address (street or P.O. box) N/A N/A City or town State ZIP code U N/A N/A N/A U) Contact name (first and last) Title 0 N/A N/A d Phone number Email address N/A QNPDES number of receiving facility (if any) ❑ None Average daily flow rate N/A mgd fq 0 1.21 Is the wastewater disposed of in a manner other than those already mentioned in Items 1.14 through 1.21 that do not C have outlets to waters of the United States (e.g., underground percolation, underground injection)? d s ❑ Yes ❑✓ No 4 SKIP to Item 1.23. A2 1.22 Provide information in the table below on these other disposal methods. Information on Other Disposal Methods o Disposal Location of Size of Annual Average Continuous or Intermittent Method Disposal Site Disposal Site Daily Discharge (check one) Description Volume r N/A N/A N/A acres N/A d gp ❑ Continuous ❑ Intermittent N/A N/A N/A acres N/A 9Pd ❑ Continuous ❑ Intermittent N/A N/A N/A acres N/A gpd El Continuous ❑ Intermittent 1.23 Do you intend to request or renew one or more of the variances authorized at 40 CFR 122.21(n)? (Check all that apply. y Consult with your NPDES permitting authority to determine what information needs to be submitted and when.) ❑ Discharges into marine waters (CWA ❑ Water quality related effluent limitation (CWA Section Er Section 301(h)) 302(b)(2)) ❑✓ Not applicable 1.24 Are any operational or maintenance aspects (related to wastewater treatment and effluent quality) of the treatment works the responsibility of a contractor? ❑ Yes ❑✓ No 4SKIP to Section 2. 1.25 Provide location and contact information for each contractor in addition to a description of the contractor's operational and maintenance responsibilities. Contractor Information Contractor 1 Contractor 2 Contractor 3 c Contractor name N/A N/A N/A ca (company name E Mailing address street or P.O. box N/A N/A N/A o City, state, and ZIP N/A N/A N/A code c Contact name (first and 0 last N/A N/A N/A Phone number Email address N/A N/A N/A Operational and maintenance N/A N/A N/A responsibilities of contractor EPA Form 3510-2A (Revised 3-19) Page 4 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000570338 NCO021181 City of Belmont WWTP OMB No. 2040-0004 SECTIOND• • •- • o Outfalls to Waters of the United States 2.1 Does the treatment works have a design flow greater than or equal to 0.1 mgd? o RV Yes ❑ No 4 SKIP to Section 3. 2.2 Provide the treatment works' current average daily volume of inflow Average Daily Volume of Inflow and Infiltration 20,000 d gp 0 R and infiltration. Indicate the steps the facility is taking to minimize inflow and infiltration. The facility inspects manholes regularly and cleans debris from the collection system to help minimize inflow and R 3 infiltration. 0 c 2.3 Have you attached a topographic map to this application that contains all the required information? (See instructions for cc specific requirements.) C 0 0 0 ❑✓ Yes ❑ No E 2.4 Have you attached a process flow diagram or schematic to this application that contains all the required information? 0 (See instructions for specific requirements.) _ a� " o ❑✓ Yes ❑ No 2.5 Are improvements to the facility scheduled? ❑ Yes ❑✓ No 4 SKIP to Section 3. Briefly list and describe the scheduled improvements. 0 1. N/A c a� E aT M 2. N/A E 0 0 M 3. N/A 2 a a� 4. N/A Cn 2.6 Provide scheduled or actual dates of completion for improvements. Scheduled or Actual Dates of Com letion for Im rovements E 0 > Scheduled Affected Outfalls Begin End Begin Attainment of Operational o Improvement (list l Construction Construction Discharge Level E (from above) number) ) (MM/DD/YYYY) (MM/DD/YYYY) (MM/DD/YYYY) MM/DDIYYYY a 1. N/A a a� s co 2. N/A 3. N/A 4. N/A 2.7 Have appropriate permits/clearances concerning other federal/state requirements been obtained? Briefly explain your response. ❑ Yes ❑ No ❑✓ None required or applicable Explanation: N/A EPA Form 3510-2A (Revised 3-19) Page 5 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000570338 NCO021181 City of Belmont WWTP OMB No. 2040-0004 SECTION•' • ON DISCHARGES 3.1 Provide the following information for each outfall. (Attach additional sheets if you have more than three outfalls.) Outfall Number 001 Outfall Number N/A Outfall Number N/A State NC N/A N/A w County Gaston N/A N/A o City or town Belmont N/A N/A 0 c w Distance from shore 345 ft. N/A ft. N/A ft. n d Depth below surface 12.23 ft. N/A ft. N/A ft. 0 Average daily flow rate 1.68 mgd N/A mgd N/A mgd Latitude 3T 13 31' N/A7 N/A' N/A" N/A N/A N/A" Longitude 81 od 52" N/A N/A' N/A" N/A- N/A' N/A" 3.2 Do any of the outfalls described under Item 3.1 have seasonal or periodic discharges? v o ❑ Yes ✓❑ No 4 SKIP to Item 3.4. d 3.3 If so, provide the following information for each applicable outfall. n Outfall Number N/A Outfall Number N/A Outfall Number N/A 0 Number of times per year discharge occurs N/A N/A N/A a Average duration of each 0 discharge (specify units N/A N/A N/A oAverage flow of each N/A mgd N/A mgd N/A mgd w discharge in Months in which discharge N/A N/A N/A occurs 3.4 Are any of the outfalls listed under Item 3.1 equipped with a diffuser? ❑ Yes ❑✓ No SKIP to Item 3.6. 3.5 Briefly describe the diffuser type at each applicable outfall. CL Outfall Number N/A Outfall Number N/A Outfall Number N/A N/A N/A N/A 0 vi 3.6 Does the treatment works discharge or plan to discharge wastewater to waters of the United States from one or more discharge points? w ❑✓ Yes ❑ No -SKIP to Section 6. EPA Form 3510-2A (Revised 3-19) Page 6 EPA Identification Number NPCES Permit Number Facility Name Form Approved 03/05/19 110000570338 NCO021181 City of Belmont WWTP OMB No.2040-0004 3.7 Provide the receiving water and related information if known for each outfall. Outfall Number 001 Outfall Number N/A Outfall Number N/A Receiving water name Catawba River N/A N/A Name of watershed, river, Lake Wylie N/A N/A 0 or stream system U.S. Soil Conservation d Service 14-digit watershed N/A N/A N/A o code m CD Name of state managemenUriver basin Catawba N/A N/A U.S. Geological Survey 8-digit hydrologic 03050101 N/A N/A cataloging unit code Critical low flow (acute) N/A cfs N/A cfs N/A cfs Critical low flow (chronic) N/A cfs N/A cfs N/A cfs Total hardness at critical N/A mg/L of N/A mg/L of N/A mg/L of low flow CaCO3 CaCO3 CaCO3 3.8 Provide the following information describing the treatment pr vided for discharges from each outfall. Outfall Number 001 Outfall Number N/A Outfall Number N/A Highest Level of 0 Primary ❑ Primary ❑ Primary Treatment (check all that ❑ Equivalent to ❑ Equivalent to ❑ Equivalent to apply per outfall) secondary secondary secondary 0 Secondary ❑ Secondary ❑ Secondary ❑ Advanced ❑ Advanced ❑ Advanced ❑ Other (specify) ❑ Other (specify) ❑ Other (specify) 0 a Design Removal Rates by N/A N/A Outfall d BOD5 or CBOD5 85 % N/A % N/A % CD d E w d TSS 85 % N/A % N/A H m Not applicable ❑ Not applicable ❑ Not applicable Phosphorus % N/A % N/A % • Not applicable ❑ Not applicable ❑ Not applicable Nitrogen % N/A % N/A % Other (specify) 0 Not applicable ❑ Not applicable ❑ Not applicable % N/A % N/A % EPA Form 3510-2A (Revised 3-19) Page 7 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000570338 NCO021181 City of Belmont WWTP OMB No. 2040-0004 3.9 Describe the type of disinfection used for the effluent from each outfall in the table below. If disinfection varies by season, describe below. Chlorine disinfection is used in all seasons for the effluent. a a� c w c 0 Outfall Number 001 Outfall Number N/A Outfall Number N/A 0 ♦/ .a Disinfection type Chlorine N/A N/A Uf N Seasons used All N/A N/A 0 E Y Dechlorination used? ❑ Not applicable ❑✓ Not applicable ❑✓ Not applicable ❑✓ Yes ❑ Yes ❑ Yes ❑ No ❑ No ❑ No 3.10 Have you completed monitoring for all Table A parameters and attached the results to the application package? ❑✓ Yes ❑ No 3.11 Have you conducted any WET tests during the 4.5 years prior to the date of the application on any of the facility's discharges or on any receiving water near the discharge points? ❑✓ Yes ❑ No 4 SKIP to Item 3.13. 3.12 Indicate the number of acute and chronic WET tests conducted since the last permit reissuance of the facility's discharges by outfall number or of the receiving water near the discharge points. Outfall Number 001 Outfall Number N/A Outfall Number N/A Acute Chronic Acute Chronic Acute Chronic Number of tests of discharge 0 20 N/A N/A N/A N/A water Number of tests of receiving N/A N/A N/A N/A N/A N/A water 3.13 Does the treatment works have a design flow greater than or equal to 0.1 mgd? ❑✓ Yes ❑ No 4 SKIP to Item 3.16. Y 0 3.14 Does the POTW use chlorine for disinfection, use chlorine elsewhere in the treatment process, or otherwise have reasonable potential to discharge chlorine in its effluent? ✓❑ Yes 4 Complete Table B, including chlorine. ❑ No 4 Complete Table B, omitting chlorine. 3.15 Have you completed monitoring for all applicable Table B pollutants and attached the results to this application package? w ❑✓ Yes ❑ No 3.16 Does one or more of the following conditions apply? • The facility has a design flow greater than or equal to 1 mgd. • The POTW has an approved pretreatment program or is required to develop such a program. • The NPDES permitting authority has informed the POTW that it must sample for the parameters in Table C, must sample other additional parameters (Table D), or submit the results of WET tests for acute or chronic toxicity for each of its discharge outfalls (Table E). Yes 4 Complete Tables C, D, and E as © ❑ No 4 SKIP to Section 4. applicable. 3.17 Have you completed monitoring for all applicable Table C pollutants and attached the results to this application package? ❑✓ Yes ❑ No 3.18 Have you completed monitoring for all applicable Table D pollutants required by your NPDES permitting authority and attached the results to this application package? ❑✓ Yes ❑ No additional sampling required by NPDES permitting authority. EPA Form 3510-2A (Revised 3-19) Page 8 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000570338 NCO021181 City of Belmont WWTP OMB No.2040-0004 3.19 Has the POTW conducted either (1) minimum of four quarterly WET tests for one year preceding this permit application or (2) at least four annual WET tests in the past 4.5 years? ✓❑ Yes ❑ No + Complete tests and Table E and SKIP to Item 3.26. 3.20 Have you previously submitted the results of the above tests to your NPDES permitting authority? ❑✓ Yes ❑ No + Provide results in Table E and SKIP to Item 3.26. 3.21 Indicate the dates the data were submitted to our NPDES permitting authority and provide a summary of the results. Date(s) Submitted Summary of Results MM/DD/YYYY One Chronic WET sample failed of the twenty samples on 8/9/2022. The failed sampled was followed up with additional sampling on 9/14/2022 and 10/11/2022, both of which passed. c c 0 3.22 Regardless of how you provided your WET testing data to the NPDES permitting authority, did any of the tests result in o toxicity? ✓❑ Yes ❑ No 4 SKIP to Item 3.26. Y 3.23 Describe the cause(s) of the toxicity: The plant effluent chlorine levels were high. a� w 3.24 Has the treatment works conducted a toxicity reduction evaluation? ❑ Yes ❑✓ No 4 SKIP to Item 3.26. 3.25 Provide details of any toxicity reduction evaluations conducted. N/A 3.26 Have you completed Table E for all applicable outfalls and attached the results to the application package? ❑ Yes ❑✓ Not applicable because previously submitted information to the NPDES p rmitting authority. SECTION-D• i Does the POTW receive discharges from SIUs or NSCIUs? 4.1 ❑✓ Yes ❑ No 4 SKIP to Item 4.7. d 4.2 Indicate the number of SIUs and NSCIUs that discharge to the POTW. Number of SIUs Number of NSCIUs 3 0 2 N/A 4.3 Does the POTW have an approved pretreatment program? cc `° x ❑✓ Yes ElNo 4.4 Have you submitted either of the following to the NPDES permitting authority that contains information substantially identical to that required in Table F: (1) a pretreatment program annual report submitted within one year of the application or (2) a pretreatment program? y ❑✓ Yes El No -* SKIP to Item 4.6. 0 -a 4.5 Identify the title and date of the annual report or pretreatment program referenced in Item 4.4. SKIP to Item 4.7. U) NCO021181_ Pretreatment _ Annual_ Report_20230213 02/13/2023 a c — 4.6 Have you completed and attached Table F to this application package? ✓❑ Yes ❑ No EPA Form 3510-2A (Revised 3-19) Page 9 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05119 110000570338 NCO021181 City of Belmont WWTP OMB No.2040-0004 4.7 Does the POTW receive, or has it been notified that it will receive, by truck, rail, or dedicated pipe, any wastes that are regulated as RCRA hazardous wastes pursuant to 40 CFR 261? ❑ Yes © No 4 SKIP to Item 4.9. 4.8 If yes, provide the follo ing information: Annual Hazardous Waste Waste Transport Method Amount of Units Number (check all that apply) Waste Received N/A ❑ Truck ❑ Rail N/A N/A ❑ Dedicated pipe ❑ Other (specify) c c 0 U a N/A ❑ Truck ❑ Rail N/A N/A c ❑ Dedicated pipe ❑ Other (specify) H O '0 ca N/A ElTruck ❑ Rail N/A N/A _ ca ❑ Dedicated pipe ❑ Other (specify) v v y N R 4.9 Does the POTW receive, or has it been notified that it will receive, wastewaters that originate from remedial activities, y including those undertaken pursuant to CERCLA and Sections 3004(7) or 3008(h) of RCRA? 0 ❑ Yes ❑✓ No 4 SKIP to Section 5. � 4.10 Does the POTW receive (or expect to receive) less than 15 kilograms per month of non -acute hazardous wastes as specified in 40 CFR 261.30(d) and 261.33(e)? ❑ Yes 4 SKIP to Section 5. ✓❑ No 4.11 Have you reported the following information in an attachment to this application: identification and description of the site(s) or facility(ies) at which the wastewater originates; the identities of the wastewater's hazardous constituents; and the extent of treatment, if any, the wastewater receives or will receive before entering the POTW? ❑ Yes ❑✓ No SECTION• OVERFLOWS (40 Does the treatment works have a combined sewer system? E 5.1 rn ❑ Yes No 4SKIP to Section 6. m 5.2 Have you attached a CSO system map to this application? (See instructions for map requirements.) `6 ❑ Yes ❑✓ No c ca 5.3 Have you attached a CSO system diagram to this application? (See instructions for diagram requirements.) 0 L) ❑ Yes ❑✓ No EPA Form 3510-2A (Revised 3-19) Page 10 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03105119 110000570338 NCO021181 W City of Belmont WTP OMB No. 2040-0004 5.4 For each CSO outfall, provide the following information. Attach additional sheets as necessary.) CSO Outfall Number N/A CSO Outfall Number N/A CSO Outfall Number N/A City or town N/A N/A N/A = 0 State and ZIP code N/A N/A N/A U CD o County N/A N/A N/A = Latitude NIX N/A' N/A" N/A' N/A' N/A" N/A N/A N/A" 0 0 U) Longitude N/A° N/A' N/A' N/A' N/A' N/A" N/A N/A' N/A" U Distance from shore N/A ft. N/A ft. N/A ft. Depth below surface N/A ft. N/A ft. N/A ft. 5.5 Did the POTW monitor any of the following items in the past year for its CSO outfalls? CSO Outfall Number N/A CSO Outfall Number N/A CSO Outfall Number N/A Rainfall ❑ Yes ❑ No ❑ Yes ❑ No ❑ Yes ❑ No rn 0 CSO flow volume ❑ Yes ❑ No ❑ Yes ❑ No ❑ Yes ❑ No CSO pollutant ❑ Yes ❑ No ❑ Yes ❑ No ❑ Yes ❑ No 0 concentrations U) 0 Receiving water quality ❑ Yes ❑ No ❑ Yes ❑ No ❑ Yes ❑ No CSO frequency ❑ Yes ❑ No ❑ Yes ❑ No ❑ Yes ❑ No Number of storm events ❑ Yes ❑ No ❑ Yes ❑ No ❑ Yes ❑ No 5.6 Provide the following information for each of your CSO outfalls. CSO Outfall Number N/A CSO Outfall Number N/A CSO Outfall Number N/A CD Number of CSO events in N/A events N/A events N/A events N the past year Average duration per N/A hours N/A hours N/A hours N event ❑ Actual or ❑ Estimated ❑ Actual or ❑ Estimated ❑ Actual or ❑ Estimated o N/A million gallons N/A million gallons N/A million gallons Average volume per event ❑ Actual or ❑ Estimated ❑ Actual or ❑ Estimated ❑ Actual or ❑ Estimated Minimum rainfall causing N/A inches of rainfall N/A inches of rainfall N/A inches of rainfall a CSO event in last year ❑ Actual or ❑ Estimated ❑ Actual or ❑ Estimated ❑ Actual or ❑ Estimated EPA Form 3510-2A (Revised 3-19) Page 11 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000570338 NC0021181 City of Belmont WWTP OMB No. 2040-0004 5.7 Provide the information in the table below for each of your CSO outfalls. CSO Outfall Number N/A CSO Outfall Number N/A CSO Outfall Number N/A Receiving water name N/A N/A N/A Name of watershed/ N streams stem N/A N/A N/A d U.S. Soil Conservation ❑ Unknown ❑ Unknown ❑ Unknown Service 14-digit c watershed code N/A N/A N/A > if known Name of state N/A N/A N/A management/river basin U.S. Geological Survey ❑ Unknown ❑ Unknown ❑ Unknown 8-Digit Hydrologic Unit Code if known)N/A N/A N/A Description of known water quality impacts on N/A N/A N/A receiving stream by CSO (see instructions for examples) SECTION• i d (d In Column 1 below, mark the sections of Form 2A that you have completed and are submitting with your application. For 6.1 each section, specify in Column 2 any attachments that you are enclosing to alert the permitting authority. Note that not all applicants are required to provide attachments. Column 1 Column 2 Section 1: Basic Application w/ variance request(s) El w/ additional attachments ElInformation for All A licants ❑ Section 2: Additional ❑✓ w/ topographic map ✓❑ w/ process flow diagram Information ❑ w/ additional attachments ❑✓ w/ Table A ❑✓ w/ Table D ❑ Section 3: Information on ❑ w/ Table B ❑ w/ Table E c Effluent Discharges E ✓❑ w/ Table C ❑ w/ additional attachments v Section 4: Industrial ❑ w/ SIU and NSCIU attachments ❑✓ w/ Table F co ❑✓ Discharges and Hazardous ❑ Wastes w/ additional attachments M ;�_ ❑ Section 5: Combined Sewer ❑ w/ CSO map El w/ additional attachments V_ Overflows ❑ w/ CSO system diagram -a m Section 6: Checklist and ❑ El w/ attachments r Certification Statement ;e 6.2 Certification Statement I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Name (print or type first and last namej, Official title isd:r IVED C tt'rµ4G6Yt Signature ; Date signed ll-2q- 23 EPA Form 3510-2A (Revised 3-19) NCDEQ /DWR /A i 9 DES Page 12 EPA Identification Number NPDES Permit Number Facility Name Outfall Number 110000570338 1 NCO021181 City of Belmont WWTP 001 Form Appruvuu uA5119 OMB No. 2040-0004 Maximum Daily Discharge Average Daily Discharge Pollutant Analytical ML or MDL Number Value Units Value Units Methods (include units) Samples Biochemical oxygen demand o BOD5 or ❑ CBOD5 66.0 mg/L 4.5 mg/L 1,146 SM 521OB-2016 DIVIL 0.18 mg/L © MDL (report one Fecal coliform 5,717 #/100 mL 263.9 #/100 mL 1,144 COLILERT-18 (2010) N/A DIVIL ❑ MDL Design flow rate MGD 5 MGD N/A pH (minimum) 6.1 S.U. ) pH (maximum) 7.7 S.U. Temperature (winter) 36.6 degC 14.5 degC 465 Temperature (summer) 31.5 degC 23.5 degC 678 Total suspended solids (TSS) 260.0 mg/L 12.3 mg/L 1,147 SM 254OD-2015 1.0 mg/L 0 ML © MDL 1 Sampling shall be conducted according to sufficiently sensitive test procedures (i.e., methods) approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I, subchapter N or 0. See instructions and 40 CFR 122.21(e)(3). EPA Form 3510-2A (Revised 3-19) Page 13 EPA Identification Number NPDES Permit Number I Facility Name Outfall Number 110000570338 NCO021181 City of Belmont WWTP Form Approved 03/05/19 OMB No. 2040-0004 Pollutant Maximum Daily Discharge Average Daily Discharge Analytical Method' ML or MDL (include units) Value Units Value Units Number of Samples Ammonia (as N) 39.0 mg/L 2.2 mg/L 1,144 350.1 El IVIL 0.03 mg/L ❑O MDL Chlorine total residual, TRC 2 174.5 ug/L 29.3 ug/L 1,145 SM 4500-CL G-2 0.015 and O MDL Dissolved oxygen 16.0 mg/L 8.9 mg/L 1,145 SM 4500-0 G-20 N/A MDL Nitrate/nitrite 29.0 mg/L 11.3 mg/L 237 353.2 0.01 mg/L ©ML MDL Kjeldahl nitrogen 32.0 mg/L 3.4 mg/L 237 351.2 IAL 0.1 mg/L © MDL Oil and grease non -detect mg/L non -detect mg/L 6 1664E IVIL 1.4 mg/L © MDL Phosphorus 7.20 mg/L 2.3 mg/L 237 365.1 0.02 mg/L © ML MDL Total dissolved solids 690 mg/L 515 mg/L 6 SM 2540C-2015 25 OML © MDL 1 Sampling shall be conducted according to sufficiently sensitive test procedures (i.e., methods) approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I, subchapter N or 0. See instructions and 40 CFR 122.21(e)(3). 2 Facilities that do not use chlorine for disinfection, do not use chlorine elsewhere in the treatment process, and have no reasonable potential to discharge chlorine in their effluent are not required to report data for chlorine. EPA Form 3510-2A (Revised 3-19) °age 15 EPA Identification Number NPDES Permit Number Facility Name Outfall Number 110000570338 NCO021181 City of Belmont WWTP •' I '• Maximum Daily Discharge Average Daily Discharge Pollutant Value Units Value Units Number of Samples Form App-- 3/05/19 OMB No. 2040-0004 Analytical ML or MDL Method' (include units) Metals, Cyanide, and Total Phenols Hardness (as CaCO3) 74.0 mg/L 51.8 mg/L 54 SM 2340C-2011 2 mg/L 0 MIL O MDL Antimony, total recoverable 72.1 ug/L 300.0 ug/L 6 200.8 2 ug/L 0 IVIL MDL Arsenic, total recoverable 5.0 ug/L 2.2 ug/L 19 200.8 1.3 ug/L O MDL Beryllium, total recoverable ND ug/L ND ug/L 6 200.8 0.4 ug/L 0IVIL MDL Cadmium, total recoverable 0.5 ug/L 0.5 ug/L 19 200.8 0.13 ug/L DIAL O MDL Chromium, total recoverable 5.0 ug/L 4.5 ug/L 19 200.8 0.13 ug/L O MDL Copper, total recoverable 18.0 ug/L 10.7 ug/L 19 200.8 0.13 ug/L OvIL O MDL Lead, total recoverable 2.0 ug/L 1.9 ug/L 19 200.8 0.25 ug/L OvIL O MDL Mercury, total recoverable 6.5 ng/L 1.3 ng/L 35 1631E 0.2 ng/L 0 MIL MDL Nickel, total recoverable 5.0 ug/L 2.5 ug/L 19 200.8 1.3 ug/L 0 MIL MDL Selenium, total recoverable 5.0 ug/L 5.0 ug/L 19 200.8 0 MIL 1.3 ug/L O MDL Silver, total recoverable 1.0 ug/L 1.0 ug/L 19 200.8 0.25 ug/L 0 IVIL MDL Thallium, total recoverable ND ug/L ND ug/L 6 200.8 0.5 ug/L ❑ MDL Zinc, total recoverable 120.0 ug/L 69.1 ug/L 19 200.8 2.5 ug/L 0MIL MDL Cyanide 20.0 ug/L 10.0 ug/L 19 SM 4500-CN E2 5 ug/L 71 ML ❑ MDL Total phenolic compounds ND mg/L ND mg/L 6 420.4 0.02 mg/L DIML O MDL Volatile Organic Compounds Acrolein ND ug/L ND ug/L 6 624.1 OML 5 ug/L 0 MDL Acrylonitrile ND ug/L ND ug/L 6 624.1 5 ug/L ML 0 MDL Benzene ND ug/L ND ug/L 6 624.1 1 ug/L 0 VIL MDL Bromoform ND ug/L ND ug/L 6 624.1 1 ug/L O MDL EPA Form 3510-2A (Revised 3-19) Page 17 EPA Identification Number NPDES Permit Number Facility Name Outfall Number 110000570338 NCOO21181 City of Belmont WWTP Ll •• Maximum Daily Discharge Average Daily Discharge Pollutant Value Units Value Units Number of Samples Form Approved 03/05119 OMB No.2040-0004 Analytical ML or MDL Method' (include units) Carbon tetrachloride ND ug/L ND ug/L 6 624.1 1 ug/L © MDL Chlorobenzene ND ug/L ND ug/L 6 624.1 IVIL 1 ug/L 0 MDL Chlorodibromomethane 3.5 ug/L 6.1 ug/L 6 624.1 1 ug/L DIVIL ❑ MDL Chloroethane ND ug/L ND ug/L 6 624.1 1 ug/L ML 0 MDL 2-chloroethylvinyl ether ND ug/L ND ug/L 6 624.1 IVIL 5 ug/L 0 MDL Chloroform 5.3 ug/L 9.5 ug/L 6 624.1 1 ug/L❑ MDL Dichlorobromomethane 1.6 ug/L 1.6 ug/L 6 624.1 IVIL 1 ug/L 0 MDL 1, 1 -dichloroethane ND ug/L ND ug/L 6 624.1 1 ug/L 0 IVIL MDL 1,2-dichloroethane ND ug/L ND ug/L 6 624.1 DIVIL 1 ug/L 0 MDL trans- 1, 2-dichloroethylene ND ug/L ND ug/L 6 624.1 ML 1 ug/L 0 MDL 1,1-dichloroethylene ND ug/L ND ug/L 6 624.1 1 ug/L 0 ML MDL 1,2-dichloropropane ND ug/L ND ug/L 6 624.1 1 ug/L 0 IVIL MDL 1,3-dichloropropylene ND ug/L ND ug/L 6 624.1 1 ug/L 0 IVIL MDL Ethylbenzene ND ug/L ND ug/L 6 624.1 1 ug/L 0 IVIL MDL Methyl bromide ND ug/L ND ug/L 6 624.1 2 ug/L 0 IVIL MDL Methyl chloride ND ug/L ND ug/L 6 624.1 2 ug/L © MDL Methylene chloride ND ug/L ND ug/L 6 624.1 1 ug/L 0 IVIL MDL 1,1,2,2-tetrachloroethane ND ug/L ND ug/L 6 624.1 IVIL 1 ug/L 0 MDL Tetrachloroethylene ND ug/L ND ug/L 6 624.1 1 ug/L 0 IVIL MDL Toluene 6 ug/L 6 ug/L 6 624.1 1 ug/L 0 IVIL MDL 1,1,1-trichloroethane ND ug/L ND ug/L 6 624.1 1 ug/L 0 ML MDL 1,1,2-trichloroethane ND ug/L ND ug/L 6 624.1 1 ug/L 0ML MDL EPA Form 3510-2A (Revised 3-19) °age 18 EPA Identification Number NPDES Permit Number Facility Name Outfall Number 110000570338 NCO021181 City of Belmont WWTP R- , -• Maximum Daily Discharge Average Daily Discharge Pollutant Number of Value Units Value Units Samples Form App,,,_ 3/05/19 OMB No. 2040-0004 Analytical ML or MDL Method' (include units) Trichloroethylene ND ug/L ND ug/L 6 624.1 1 ug/L ©ML MDL Vinyl chloride ND ug/L ND ug/L 6 624.1 1 ug/L ©ML MDL Acid -Extractable Compounds p-chloro-m-cresol ND ug/L ND ug/L 6 625.1 1.6 ug/L OML O MDL 2-chlorophenol ND ug/L ND ug/L 6 625.1 1.6 ug/L El VIL O MDL 2,4-dichlorophenol ND ug/L ND ug/L 6 625.1 1.6 ug/L OML O MDL 2,4-dimeth ylphenol ND ug/L ND ug/L 6 625.1 1.6 ug/L OML O MDL 4,6-dinitro-o-cresol ND ug/L ND ug/L 6 625.1 8 ug/L ©IVIL MDL 2,4-dinitrophenol ND ug/L ND ug/L 6 625.1 8 ug/L O MDL 2-nitrophenol ND ug/L ND ug/L 6 625.1 3.2 ug/L OML O MDL 4-nitrophenol ND ug/L ND ug/L 6 625.1 8 ug/L O MDL Pentachlorophenol ND ug/L ND ug/L 6 625.1 8 ug/L OML O MDL Phenol ND ug/L ND ug/L 6 625.1 1.6 ug/L OML O MDL 2,4,6-trichlorophenol ND ug/L ND ug/L 6 625.1 1.6 ug/L O MDL Base -Neutral Compounds Acenaphthene ND ug/L ND ug/L 6 625.1 1.6 ug/L OML O MDL Acenaphthylene ND ug/L ND ug/L 6 625.1 1.6 ug/L OML O MDL Anthracene ND ug/L ND ug/L 6 625.1 1.6 ug/L OML O MDL Benzidine ND ug/L ND ug/L 6 625.1 8 ug/L MIL El MDL Benzo(a)anthracene ND ug/L ND ug/L 6 625.1 1.6 ug/L O MDL Benzo(a)pyrene ND ug/L ND ug/L 6 625.1 1.6 ug/L O MDL 3,4-benzofluoranthene ND ug/L ND ug/L 6 625.1 1.6 ug/L O MDL EPA Form 3510-2A (Revised 3-19) Page 19 EPA Identification Number NPDES Permit Number Facility Name Outfall Number 110000570338 NC0021181 City of Belmont WWTP • •• Maximum Daily Discharge Average Daily Discharge Pollutant Number of Value Units Value Units Sam les Form Approved 03/05/19 OMB No. 2040-0004 Analytical ML or MDL Method' (include units) Benzo(ghi)perylene ND ug/L ND ug/L 6 625.1 1.6 ug/L 0 MIL 0 MDL Benzo(k)fluoranthene ND ug/L ND ug/L 6 625.1 1.6 ug/L 0 MDL Bis (2-chloroethoxy) methane ND ug/L ND ug/L 6 625.1 1.6 ug/L 0 MDL Bis (2-chloroethyl) ether ND ug/L ND ug/L 6 625.1 ML 1.6 ug/L El MDL Bis (2-chloroisopropyl) ether OML ❑ MDL Bis (2-ethylhexyl) phthalate 14.15 ug/L 26 ug/L 6 625.1 8 ug/L 1 VIL MDL 4-bromophenyl phenyl ether ND ug/L ND ug/L 6 625.1 1.6 ug/L 0 MDL Butyl benzyl phthalate ND ug/L ND ug/L 6 625.1 1.6 ug/L 0 MDL 2-chloronaphthalene ND ug/L ND ug/L 6 625.1 0 MIL 1.6 ug/L 0 MDL 4-chlorophenyl phenyl ether ND ug/L ND ug/L 6 625.1 1.6 ug/L 0 MDL Chrysene ND ug/L ND ug/L 6 625.1 1.6 ug/L © ML MDL di-n-butyl phthalate ND ug/L ND ug/L 6 625.1 1.6 ug/L © ML MDL di-n-octyl phthalate ND ug/L ND ug/L 6 625.1 1.6 ug/L © VIL MDL Dibenzo(a,h)anthracene ND ug/L ND ug/L 6 625.1 1.6 ug/L 0 MDL 1,2-dichlorobenzene ND ug/L ND ug/L 2 625.1 1.6 ug/L 0 MDL 1,3-dichlorobenzene ND ug/L ND ug/L 2 625.1 1.6 ug/L 0 MIL 0 MDL 1,4-dichlorobenzene ND ug/L ND ug/L 2 625.1 ML 1.6 ug/L © MDL 3,3-dichlorobenzidine ND ug/L ND ug/L 6 625.1 8 ug/L ©ML MDL Diethyl phthalate D ug/L ND ug/L 6 625.1 1.6 ug/L ML © MDL Dimethyl phthalate uML g/L ND ug/L 6 625.1 1.6 ug/L © MDL 2,4-dinitrotoluene D END ug/L ND ug/L 6 625.1 3.2 ug/L ML ©MDL2,6-dinitrotoluene D ug/L ND ug/L 6 625.1 3.2 ug/L © MIL MDL EPA Form 3510-2A (Revised 3-19) 'age 20 EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Appiuveu u3/05/19 110000570338 NC0021181 City of Belmont WWTP OMB No. 2040-0004 Maximu7DallyDischarge Average Daily Discharge 7Valueits Pollutant Analytical MLorMDL Number of Value Units Method' (include units) Samples 1,2-diphenylhydrazine ND ug/L ND ug/L 6 625.1 1.6 ug/L OML O MDL Fluoranthene ND ug/L ND ug/L 6 625.1 1.6 ug/L DIVIL O MDL Fluorene ND ug/L ND ug/L 6 625.1 DIVIL 1.6 ug/L O MDL Hexachlorobenzene ND ug/L ND ug/L 6 625.1 1.6 ug/L O MDL Hexachlorobutadiene ND ug/L ND ug/L 6 625.1 OML 1.6 ug/L O MDL Hexachlorocyclo-pentadiene ND ug/L ND ug/L 6 625.1 8 ug/L O MDL Hexachloroethane ND ug/L ND ug/L 6 625.1 1.6 ug/L OML O MDL Indeno(1,2,3-cd)pyrene ND ug/L ND ug/L 6 625.1 1.6 ug/L 11 MIL O MDL Isophorone ND ug/L ND ug/L 6 625.1 1.6 ug/L O MDL Naphthalene ND ug/L ND ug/L 6 625.1 1.6 ug/L OML O MDL Nitrobenzene ND ug/L ND ug/L 6 625.1 ML 1.6 ug/L © MDL N-nitrosodi-n-propylamine ND ug/L ND ug/L 6 625.1 1.6 ug/L ML © MDL N-nitrosodimethylamine ND ug/L ND ug/L 6 625.1 1.6 ug/I O MDL N-nitrosodiphenylamine ND ug/L ND ug/L 6 625.1 1.6 ug/L El IVIL O MDL Phenanthrene ND ug/L ND ug/L 6 625.1 1.6 ug/L DIVIL O MDL Pyrene ND ug/L ND ug/L 6 625.1 1.6 ug/L OML O MDL 1,2,4-trichlorobenzene ND ug/L ND ug/L 6 625.1 1.6 ug/L O MDL I Sampling shall be conducted according to sufficiently sensitive test procedures (i.e., methods) approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR Chapter I, Subchapter N or 0. See instructions and 40 CFR 122.21(e)(3). EPA Form 3510-2A (Revised 3-19) Page 21 EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19 110000570338 NCO021181 City of Belmont WWTP OMB No. 2040-0004 Maximum Dail Discharge Average Dail Discharge Pollutant Number of Analytical ML or MDL (list) Value Units Value Units Method' (include units) Samples ❑ No additional sampling is required by NPDES permitting authority. Total Monthly Flow 74.86 MG/month 51.2 MG/month 55 N/A ❑ ML N/A ❑ MDL TN 33 mg/L 14.7 mg/L 237 N/A 0 ML N/A ❑ MDL TN 17,171 lb/month 6,152 Ib/mo 55 N/A 0 ML N/A ❑ MDL TN 13,369 lb/summer 2022 N/A N/A 8 N/A ❑ ML N/A ❑ MDL TN 19,496 Ib/winter2022 N/A N/A 4 N/A N/A 0 ML ❑ MDL TP 2,244 lb/month 949 lb/month 55 365.1 0.02 mg/L 0 MDL TP 9,270 Ib/yr2022 N/A N/A 12 365.1 0.02 mg/L 0 ML ❑O MDL Total hardness - upstream 70 mg/L 19.1 mg/L 290 SM 2340C-2011 ML 2.0 mg/L © MDL D.O. - upstream 14 mg/L 8.5 mg/L 405 SM4500-0 G-20 N/A 0 ML ❑ MDL D.O. - downstream 13.9 mg/L 8.5 mg/L 404 SM4500-0 G-20 N/A 0 ML ❑ MDL Temperature - upstream 33 degC 23.2 degC 405 N/A N/A ❑ ML ❑ MDL Temperature - downstream 32.5 degC 23.3 degC 404 N/A N/A ❑ ML ❑ MDL Conductivity - upstream 179 umhos/cm 58.6 umhos/cm 356 120.1 ❑ ML 71 MDL Conductivity - downstream 653 umhos/cm 59.5 umhos/cm 356 120.1 p MDL Fecal coliform - upstream 9,500 #/100 mL 395.1 #/100 mL 404 SM 9222D-2015 0 ML N/A ❑ MDL Fecal coliform - downstream 5,500 #/100 mL 195.0 #/100 mL 404 SM 9222D-2015 N/A ❑ ML ❑ MDL Molybdenum Molybdenum ug/L 11.2 ug/L 19 200.8 2.5 ug/L O MDL 1 Sampling shall be conducted according to sufficiently sensitive test procedures (i.e., methods) approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under 40 CFR chapter I, subchapter N or 0. See instructions and 40 CFR 122.21(e)(3). EPA Form 3510-2A (Revised 3-19) °age 23 EPA Identification Number NPDES Permit Number Facility Name 110000570338 NCO021181 City of Belmont WWTP Form Appi vu 3105119 OMB No. 2040-0004 TA13LE F. INDUSTRIAL DISCHARGE IWORIVIATION Response space is provided for three SIUs. Copy the table to report information for additional SIUs. SIU 0005 SIU 001E SIU N/A Name of SIU Spartan Dyers US Cotton N/A Mailing address (street or P.O. box) 217 Sterling Street 1000 Parkdale Drive Suite 1 N/A City, state, and ZIP code Belmont, NC 28012 Belmont, NC 28012 N/A Description of all industrial processes that affect Package Yarn Dyeing Cotton Bleaching Operation N/A or contribute to the discharge. List the principal products and raw materials that affect or contribute to the SIU's discharge. Yarn, Electrolytes (NsCI, Na2SO4), Weak Unbleached Cotton, Water, Chemicals N/A Organic Acid (acetic), Alkali (NsOH, Soda Ash), Sodium Hydrosulphite, Hydrogen Peroxide, Dispersing Agents, Softeners, Detergents, Textile Dyes Indicate the average daily volume of wastewater discharged by the SIU. 223,000 gpd 50,800 gpd N/A gpd How much of the average daily volume is attributable to process flow? 206,000 gpd 40,000 gpd N/A gpd How much of the average daily volume is attributable to non -process flow? 17,000 gpd 10,800 gpd N/A gpd Is the SIU subject to local limits? ✓❑ Yes ❑ No ❑✓ Yes ❑ No ❑ Yes ❑ No Is the SIU subject to categorical standards? ❑ Yes ✓❑ No El Yes ❑✓ No ❑ Yes ❑ No EPA Form 3510-2A (Revised 3-19) Page 29 EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19 110000570338 NCO021181 City of Belmont WWTP OMB No. 2040-0004 TABLE F. INDUSTRIAL DISCHARGE INFORMATION Response space is provided for three SIUs. Copy the table to report information for additional SIUs. SIU 000S SIU 001E SIU N/A Under what categories and subcategories is the 40 CFR 410 40 CFR 410 N/A SIU subject? Has the POTW experienced problems (e.g., upsets, pass -through interferences) in the past 4.5 ❑ Yes ❑✓ No ❑ Yes ❑✓ No ❑ Yes ❑ No ears that are attributable to the SIU? If yes, describe. N/A N/A N/A EPA Form 3510-2A (Revised 3-19) °age 30 IVlou-1 Mountain ,1 Holly-' Island Quad. Lake Quad. o _ �= - Ae, � J„ N ODROW AVf K 7IIp ^ r- .BtVO' It � `' ^ R � �` CA-t.`•; .. , a.. °i' �C ) , Gr � 650 29 74 -- _ 73 ou i Cem A �,�1 . ��� Ag �" I �tEKyAR� h^ O iL_ Belmont WWTP —� 35°13'53.7"N r' 81 °00'59.7"W r m s - S IF Outfall 35*13'37.0"N p CARNEgpsC 81 °00'52.0'W 4 RD r: f c .. dim - q n LEGEND 0 OUTFALL t STREAM FLOW DIRECTION DEQ NC - SURFACE WATER CLASSIFICATION 6SO \t P O 7.5 MINUTE INDEX STATE-WIDE LAND USE SINGLE-FAMILY RESIDENTIAL �\ 1\ �o "I \\ / 4 MULTI-FMAILY RESIDENTIAL COMMERCIAL 3 SCHOOL 3 MEDICAL/DENTAL OFFICE \� a e � RELIGIOUS Z� OFFICE o ARE• ao \\ 3 PUBLIC UTILITIES aD 1 GOVERNMENT VACANT ' I $ 600 INDUSTRIAL \ --A SOURCE: -. .. - USGS TOPOGRAPHIC MAP QUAD: C BELMONT 20220823 T34 H 2,00o FT. UC:03050101, SUBBASIN: 3-08-34 FIGURE 1 — BELMONT COUNTY, NC, USA m LEGEND: SOLIDS TRAIN LIQUID TRAIN F)l bEV.qk m n IN CITY OF BELMONT - EXISTING WWTP PROCESS FLOW DIAGRAM FIGURE 2.1.1 FN Narrative Description of City of Belmont Process Flow Diagram The Belmont Wastewater Treatment Plant (WWTP) is designed for an average daily flow of 5 MGD. The plant influent enters the headworks facility, consisting of bar screens followed by grit sedimentation channels and a Parshall flume measuring structure. Following the Parshall flume, the wastewater flows by gravity to the two aeration basins. Two final clarifiers accept the flow from the aeration basins and the final clarifier effluent is chlorinated in the chlorine contact basins before dichlorination and discharge into the Catawba River. The return activated sludge from both final clarifiers is sent to the aeration basin influent and the waste activated sludge is sent to the aerobic digesters. Digested sludge is stored in the sludge holding tank before pumping the digested sludge out of the storage tank and into a truck. The solids are trucked to permitted land sites by a certified contracted company, Southern Soil Builders, under Land Application Permit #WQ003281. The Belmont WWTP has an emergency standby generator rated for 350 kW. EPA Identification Number NPDES Number Facility Name Outfall Number 110000570338 NC0021181 City of Belmont WWTP Pollutant (Required) CAS number Method Number (if Applicable) Reason Pollutant Believed Present in Discharge Estimated Concentration (If Known) Perfluorooctanoic acid (PFOA) 335-67-1 Draft Method 1633 Believed absent Samples have not been taken Perfluorooctanesulfonic acid (PFOS) 1763-23-1 Draft Method 1633 Believed absent Samples have not been taken Perfluorohexanesulfonic acid (PFHxS) 355-46-4 Draft Method 1633 Believed absent Samples have not been taken Perfluorobutanesulfonic acid (PFBS) 375-73-5 Draft Method 1633 Believed absent Samples have not been taken Perfluorononanoic acid (PFNA) 375-95-1 Draft Method 1633 Believed absent Samples have not been taken GenX Draft Method 1633 Believed absent Samples have not been taken This page is intentionally left blank. City of Belmont Wastewater Treatment Plant MODEL MUNICIPAL MERCURY MI 41�TION PLAN [l]/l/2023] SECTION I - PURPOSE The purpose of this Mercury Minimization Plan ("MMP") is to describe best management practices through which City of Belmont Wastewater Treatment Plant (WWTP) will seek to reduce the amount of mercury discharged into its system and, ultimately, to the environment. The MMP compiles mercury reduction -related efforts to -date and potential future action items. It is designed to be a working document to help guide City of Belmont in its efforts to control mercury loadings discharged into its Publicly -Owned Treatment Works (POTW) by users of the sewer system. Such a reduction in loadings to the sewer system should translate to a reduction in the amount of mercury which is discharged from the treatment plant. The management practices summarized below may also help control some of the mercury reaching our storm sewer system as well. SECTION II — FACILITY DESCRIPTION The City of Belmont operates a publicly owned treatment works (POTW), including a collection system and wastewater treatment plant (WWTP), that serves the City of Belmont, North Carolina. The City of Belmont's WWTP is permitted to treat 5.0 MGD and breaks down/removes organic waste through an Activated Sludge process. Our facility utilizes a three -step removal process inlcuding preliminary treatment, secondary treatment, and sludge handling systems. Our preliminary treatment begins when the wastewater enters our plant from various locations throughout the City including both Residential and Industrial Users. The wastewater is received from the collection system and is screened through an automatic bar -screen and grit chamber at the WWTP Influent. The purpose of our preliminary treatment is to remove debris and inorganic matter from the wastewater. Secondary treatment is composed of two parts: biological nutrient removal and secondary clarification. Biological nutrient removal begins when the wastewater travels from the preliminary treatment to the aeration basins. Wastewater enters the aeration basins and microorganisms breakdown biodegradable organic matter as the wastewater flows through the aeration basins. Aerators are used to sustain an adequate level of oxygen for the survival of microorganisms as well to mix the wastewater. This process aids in BOD, COD, Phosphorus, and Ammonia removals. Secondary clarification occurs when the water travels from the aeration basins and splits off into one of two secondary clarifiers where settling occurs. The wastewater then leaves the secondary clarifiers via v-notch weirs and travels to the chlorine contact chambers for disinfection. After disinfection, the water is de -chlorinated and then discharged into the Catawba River. The settled solids either return to the aeration basins or the solids go to the aerobic digesters/sludge holding tank for sludge removal. The aerobic digesters further break down organic material before the solids are trucked offsite to be disposed of. Most municipal treatment plants are not designed to remove mercury and it is exceedingly expensive to do so to very low levels. Incidental mercury removal occurs through typical municipal treatment with trace levels of mercury (and other metals) ending up in solids removed from the raw wastewater. Mercury is not used in the treatment processes at the WWTP. Mercury may be introduced into the sewer system through a variety of sources, such as from industrial users, laboratories, and other businesses. Residual deposits of mercury are also possible in the sewer system from historic practices. Finally, trace amounts from household products and atmospheric deposition (both wet and dry) contribute to sewer system mercury loadings. While there is typically some mercury contributed to public sewer systems statewide, it is usually in minute quantities and comprises a tiny portion of the already insignificant statewide loading for all point sources - just two percent of the annual mercury loadings to all State waters. SECTION III — PROGRAM PLAN A. EVALUATION OF POTENTIAL NON -DOMESTIC SOURCES CONTRIBUTING MERCURY TO THE POTW Within 24 months from the NPDES required 180-day period for development of an MMP, , the City of Belmont will evaluate available information to assess the potential for non -domestic users of the sewer system to contribute mercury to the system. The information to be reviewed may include: (1) POTW influent and effluent mercury data and trends; (2) industrial user permits and associated mercury monitoring data; (3) Toxics Release Inventory (TRI); (4) state hazardous site registry and the National Priority List relating to mercury contamination; and (5) historical records of industrial sites which ffmy have contributed mercury loadings to the sewer system. The City of Belmont will also survey and evaluate the following common sources of mercury in its service area: (1) dentist offices; (2) hospitals; (3) laboratories; (4) auto recyclers; and (5) other potential sources of mercury based on existing information. The City of Belmont will request that industrial users review mercury concentrations in high -volume process chemicals and demonstrate that the mercury concentrations are below industry average. The City of Belmont will request that alternative sources for chemicals be explored if the mercury levels are determined to be significantly higher than would normally be expected. The evaluation of potential non -domestic sources of mercury to the sewer system will be updated every five years, as warranted by prior sampling results and any additional new potentially significant sources to the system. B. ADDITIONAL CONTROL MEASURES This MMP identifies reasonable and cost-effective control measures to minimize mercury being discharged into the POTW. Below is a listing of initial BMPs for this POTW. Pollution Prevention Substances used at the WWTP will be evaluated to determine if they contain mercury or mercury -based compounds. Any such chemicals will be evaluated for substitution with non -mercury -containing substances. Housekeeping, Spill Control and Collection, and Education The City of Belmont will develop procedures to minimize the possibility of any spill or release at the WWTP involving mercury containing substances. The City of Belmont will add mercury identification and proper disposal to ongoing and future operator training procedures. Public Outreach The City of Belmont will make available educational information regarding sources of household mercury and appropriate use/disposal practices. This information may be posted on the City of Belmont WWTP's website and copies will be made available at the City of Belmont's WWTP. The availability of this information will be highlighted in the City of Belmont's bi-annual outreach to the City of Belmont's customers. The City of Belmont will also facilitate public awareness regarding community collection points for mercury -containing products from residents/customers for proper disposal. Periodic reminders of such collection programs will be provided as part of City of Belmont's ongoing public outreach. C. TRACKING AND MONITORING In order to assess the implementation of the control measures, the Belmont WWTP proposes to undertake the following evaluations beginning after the first full year that this MMP is implemented: Survey annually at least ten percent (10%) of any non -domestic users identified as possible significant sources of mercury to the POTW; Track the implementation of the programs outlined above; Monitor influent mercury at least annually. Require significant non -domestic sources of mercury to monitor periodically, as warranted; and Measure effluent mercury as required by the NPDES permit. These efforts will allow the Belmont WWTP to establish a baseline of influent and effluent mercury levels to assist in identifying any trends in mercury contributions from domestic and non -domestic users of the sewer system. This baseline will be tracked annually. SECTION IV — IMPLEMENTATION OF CONTROL MEASURES The City of Belmont monitors mercury levels on all industrial users. At this time, the City of Belmont does not see a need for implementation of mercury limits for our industrial users. The pretreatment department continues to monitor our influent mercury levels for potential elevated concentrations. The City will remain vigilant towards environmental concerns with regards to increased mercury levels. The Belmont WWTP will implement the control measures summarized in Section III over the permit term and will update this MMP as warranted. SECTION V - REPORTING A summary of the MNT activities will be submitted as part of the NPDES permit renewal process. FN Sludge Management Plan After the sludge holding process, before being sent to the permitted land sites by a certified contracted company, sludge sampling is conducted per our Land Application Permit #WQ003281 and/or 503 regulations. The sampling, testing, and monitoring is conducted by Southern Soil Builders. The City of Belmont has a continuous contract with them to perform the above procedures. The contract also includes hauling the sludge, soil testing, land preparation, record keeping and State reporting. This page is intentionally left blank. SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis City of Belmont PO Box 431 Belmont, NC 28012 Attention: Sandra Craft Project Name: Effluent Pollutant Scan Lot Number:TD18073 Date Completed:05/07/2018 05/08/2018 10:15 AM Approved and released by: Project Manager: Kelly M. Nance P ARM AC CA E 0 1 T E0 e / l- 00o EtAP The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 1 of 12 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative City of Belmont Lot Number: TD18073 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 2 of 12 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary City of Belmont Lot Number: TD18073 Sample Number Sample ID Matrix Date Sampled Date Received 001 Effluent Aqueous 04/18/2018 0936 04/18/2018 002 Effluent Aqueous 04/18/2018 0953 04/18/2018 (2 samples) Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 3 of 12 Client:City of Belmont Laboratory ID:TD18073-001 Description: Effluent Matrix: Aqueous de Sampled:04/18/2018 0936 e Received:04/1812018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 350.1 (Ammonia - N ) 350.1 1 04/19/2018 1552 DMA 69971 1 (Hardness (to) SM 2340C-2011 1 04/28/2018 1152 TAF 70843 1 (Nitrate-Nitr) 353.2 25 04/26/2018 1626 HKL 70623 1 (Phosphorus) 365.1 10 04/25/2018 1720 DMA 04/25/2018 1147 70431 1 (TDS) SM 2540C-2011 1 04/24/2018 1059 AMM1 70277 1 351.4 (TKN) 351.2 1 04/25/2018 1805 DMA 04/25/2018 1204 70430 CAS Analytical Parameter Number Method Result Q LOQ Units Run Ammonia - N (gas diffusion) 350.1 ND 0.10 mg/L 1 Hardness (total) SM 2340C- 38 10 mg/L 1 Nitrate -Nitrite - N 353.2 20 0.50 mg/L 1 Phosphorus 7723-14-0 365.1 3.1 0.50 mg/L 1 TDS SM 2540C- 690 25 mg/L 1 TKN 351.2 ND 0.10 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 4 of 12 Client:City of Belmont Laboratory ID:TD18073-001 Description: Effluent Matrix: Aqueous Date Sampled:04/18/2018 0936 Date Received:04/18/2018 Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 625.1 625.1 1 05/06/20181851 JCG 04/23/20181651 70206 CAS Analytical Parameter Number Method Result Q LOQ Units Run Acenaphthene 83-32-9 625.1 ND 1.6 ug/L Acenaphthylene 208-96-8 625.1 ND 1.6 ug/L Anthracene 120-12-7 625.1 ND 1.6 ug/L Benzidine 92-87-5 625.1 ND 8.0 ug/L Benzo(a)anthracene 56-55-3 625.1 ND 1.6 ug/L Benzo(a)pyrene 50-32-8 625.1 ND 1.6 ug/L Benzo(b)fluoranthene 205-99-2 625.1 ND 1.6 ug/L Benzo(g,h,i)perylene 191-24-2 625.1 ND 1.6 ug/L Benzo(k)fluoranthene 207-08-9 625.1 ND 1.6 ug/L 4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1.6 ug/L Butyl benzyl phthalate 85-68-7 625.1 ND 1.6 ug/L bis (2-Chloro-l-methylethyl) ether 108-60-1 625.1 ND 1.6 ug/L 4-Chloro-3-methyl phenol 59-50-7 625.1 ND 1.6 ug/L bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 1.6 ug/L bis(2-Chloroethyl)ether 111-44-4 625.1 ND 1.6 ug/L 2-Chloronaphthalene 91-58-7 625.1 ND 1.6 ug/L 2-Chlorophenol 95-57-8 625.1 ND 1.6 ug/L 4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1.6 ug/L Chrysene 218-01-9 625.1 ND 1.6 ug/L Dibenzo(a,h)anthracene 53-70-3 625.1 ND 1.6 ug/L 1,2-Dichlorobenzene 95-50-1 625.1 ND 1.6 ug/L Dichlorobenzene 541-73-1 625.1 ND 1.6 ug/L Dichlorobenzene 106-46-7 625.1 ND 1.6 ug/L 3,3'-Dichlorobenzidine 91-94-1 625.1 ND 8.0 ug/L 2,4-Dichlorophenol 120-83-2 625.1 ND 1.6 ug/L Diethylphthalate 84-66-2 625.1 ND 1.6 ug/L Dimethyl phthalate 131-11-3 625.1 ND 1.6 ug/L 2,4-Dimethylphenol 105-67-9 625.1 ND 1.6 ug/L Di-n-butyl phthalate 84-74-2 625.1 ND 1.6 ug/L 4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 8.0 ug/L 2,4-Dinitrophenol 51-28-5 625.1 ND 8.0 ug/L 2,4-Dinitrotoluene 121-14-2 625.1 ND 3.2 ug/L 2,6-Dinitrotoluene 606-20-2 625.1 ND 3.2 ug/L Di-n-octylphthalate 117-84-0 625.1 ND 1.6 ug/L 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625.1 ND 1.6 ug/L bis(2-Ethylhexyl)phthalate 117-81-7 625.1 2.3 1.6 ug/L Fluoranthene 206-44-0 625.1 ND 1.6 ug/L Fluorene 86-73-7 625.1 ND 1.6 ug/L Hexachlorobenzene 118-74-1 625.1 ND 1.6 ug/L Hexachlorobutadiene 87-68-3 625.1 ND 1.6 ug/L Hexachlorocyclopentadiene 77-47-4 625.1 ND 8.0 ug/L Hexachloroethane 67-72-1 625.1 ND 1.6 ug/L Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1.6 ug/L Isophorone 78-59-1 625.1 ND 1.6 ug/L LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 t of holding time W = Reported on wet weight basis _ -__ j Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 5 of 12 --.... r v. u..— v. yu...v vv...aiy vv/...v Client:City of Belmont Laboratory ID:TD18073-001 Description: Effluent Matrix: Aqueous Date Sampled:04/18/2018 0936 Date Received:04/18/2018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 2 625.1 625.1 1 05/06/20181851 JCG 04/23/20181651 70206 CAS Analytical Parameter Number Method Result Q LOQ Units Run Naphthalene 91-20-3 625.1 ND 1.6 ug/L 2 Nitrobenzene 98-95-3 625.1 ND 1.6 ug/L 2 2-Nitrophenol 88-75-5 625.1 ND 3.2 ug/L 2 4-Nitrophenol 100-02-7 625.1 ND 8.0 ug/L 2 N-Nitrosodimethylamine 62-75-9 625.1 ND 1.6 ug/L 2 N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 1.6 ug/L 2 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625.1 ND 1.6 ug/L 2 Pentachlorophenol 87-86-5 625.1 ND 8.0 ug/L 2 Phenanthrene 85-01-8 625.1 ND 1.6 ug/L 2 Phenol 108-95-2 625.1 ND 1.6 ug/L 2 Pyrene 129-00-0 625.1 ND 1.6 ug/L 2 1,2,4-Trichlorobenzene 120-82-1 625.1 ND 1.6 ug/L 2 2,4,6-Trichlorophenol 88-06-2 625.1 ND 1.6 ug/L 2 Run 2 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 66 37-129 2-Fluorophenol 37 24-127 Nitrobenzene-d5 75 38-127 Phenol-d5 46 28-128 Terphenyl-d14 93 10-148 2,4,6-Tribromophenol 71 41-144 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 6 of 12 Client:City of Belmont Laboratory ID:TD18073-001 Description: Effluent Matrix: Aqueous Date Sampled:04/18/2018 0936 )ate Received:04/18/2018 Prep Method 200.2 Analytical Method Dilution Analysis Date Analyst 200.8 1 04/21/2018 0031 BNW Prep Date Batch 04/19/2018 2140 69973 CAS Analytical Parameter Number Method Result Q LOQ Units Run Antimony 7440-36-0 200.8 300 2.0 ug/L 1 Arsenic 7440-38-2 200.8 ND 2.0 ug/L 1 Beryllium 7440-41-7 200.8 ND 0.40 ug/L 1 Cadmium 7440-43-9 200.8 ND 0.50 ug/L 1 Chromium 7440-47-3 200.8 ND 5.0 ug/L 1 Copper 7440-50-8 200.8 13 5.0 ug/L 1 Lead 7439-92-1 200.8 ND 1.0 ug/L 1 Nickel 7440-02-0 200.8 ND 5.0 ug/L 1 Selenium 7782-49-2 200.8 ND 5.0 ug/L 1 Silver 7440-22-4 200.8 ND 1.0 ug/L 1 Thallium 7440-28-0 200.8 ND 0.50 ug/L 1 Zinc 7440-66-6 200.8 56 10 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% of holding time W = Reported on wet weight basis _..__., Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 7 of 12 Client:City of Belmont Laboratory ID:TD18073-002 Description: Effluent Matrix: Aqueous ate Sampled:04/18/2018 0953 to Received:04/18/2018 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 10-204-00-1-X (Cyanide - To) SM 4500-CN E- 1 04/24/2018 0956 MSG 04/24/2018 0754 70267 1 (Phenolics) 420.4 1 04/21/2018 1424 MSG 04/20/2018 1125 70047 1 (HEM (oil and) 1664B 1 04/25/2018 0924 ARP 70391 CAS Analytical Parameter Number Method Result Q LOQ Units Run Cyanide - Total Phenolics HEM (oil and grease) 57-12-5 SM 4500-CN 0.011 420.4 ND 1664B ND LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com 0.010 mg/L 1 0.020 mg/L 1 4.8 mg/L 1 Page 8 of 12 vY Client:City of Belmont Laboratory ID:TD18073-002 Description: Effluent Matrix: Aqueous )ate Sampled:O4/18/2018 0953 ate Received:O4/18/2018 Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 624.1 624.1 1 04/21/2018 2349 ECP 70102 CAS Analytical Parameter Number Method Result Q LCQ Units Run Acrolein 107-02-8 624.1 ND 5.0 ug/L 1 Acrylonitrile 107-13-1 624.1 ND 5.0 ug/L 1 Benzene 71-43-2 624.1 ND 1.0 ug/L 1 Bromodichloromethane 75-27-4 624.1 5.1 1.0 ug/L 1 Bromoform 75-25-2 624.1 ND 1.0 ug/L 1 Bromomethane (Methyl bromide) 74-83-9 624.1 ND 2.0 ug/L 1 Carbon tetrachloride 56-23-5 624.1 ND 1.0 ug/L 1 Chlorobenzene 108-90-7 624.1 ND 1.0 ug/L 1 Chloroethane 75-00-3 624.1 ND 2.0 ug/L 1 2-Chloroethylvinylether 110-75-8 624.1 ND 5.0 ug/L 1 Chloroform 67-66-3 624.1 6.6 1.0 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 624.1 ND 2.0 ug/L 1 Dibromochloromethane 124-48-1 624.1 1.6 1.0 ug/L 1 1,1-Dichloroethane 75-34-3 624.1 ND 1.0 ug/L 1 1,2-Dichloroethane 107-06-2 624.1 ND 1.0 ug/L 1 1,1-Dichloroethene 75-35-4 624.1 ND 1.0 ug/L 1 trans-1,2-Dichloroethene 156-60-5 624.1 ND 1.0 ug/L 1 1,2-Dichloropropane 78-87-5 624.1 ND 1.0 ug/L 1 cis-1,3-Dichloropropene 10061-01-5 624.1 ND 1.0 ug/L 1 trans-1,3-Dichloropropene 10061-02-6 624.1 ND 1.0 ug/L 1 Ethvibenzene 100-41-4 624.1 ND 1.0 ug/L 1 tylene chloride 75-09-2 624.1 ND 1.0 ug/L 1 ?,2-Tetrachloroethane 79-34-5 624.1 ND 1.0 ug/L 1 Tetrachloroethene 127-18-4 624.1 ND 1.0 ug/L 1 Toluene 108-88-3 624.1 ND 1.0 ug/L 1 1,1,1-Trichloroethane 71-55-6 624.1 ND 1.0 ug/L 1 1,1,2-Trichloroethane 79-00-5 624.1 ND 1.0 ug/L 1 Trichloroethene 79-01-6 624.1 ND 1.0 ug/L 1 Vinyl chloride 75-01-4 624.1 ND 1.0 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 112 70-130 1,2-Dichloroethane-d4 113 70-130 Toluene-d8 113 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GG columns exceeds 40 t of holding time W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 9 of 12 Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 10 of 12 �U) CD os <w w � m w � CD CD< �� 8. �CD o� w < w CD m n' CD m y M Cl) 0 CD N CD ro 0 M 11[ CWA l NPDES R' Chain of Custody Record Shealy Environmental Services, Inc. 108 Vantage Pohl Drive West Colurn'tia, South Carolina 29172 Telephone No, (803) 791-97100 Fax No. (803) 7g1-A11 w6w.shealvlab.00m Number Client RPPKA to Crotnot Sampler's Rigiature !14—A I T* Sjtcy, Uwote No Relrncnt WWTD Sandra Craft O Printed Name 1472#3 Ack ess Pege Held I'9remeters (,.m. ; I trnrp, UUJ can be recorded in check boxe6 1 of 1 City Stain No I Fax Not 1 1 1 2 1 g i 9. 1 I NumbEr Cf Coatelners PA:!Imcnl INC Em=.il p K I G R E J a motile Pro*Name 1 1 3 ii 8 5 7 Preserva'iva OF Scan it Numxr r wui :x:r r�LnGD SampleIDrDescrptan Q81e Time r? ' w w (J a } "� C7 T. TU gV7 (Canranere ttu each snm frig m;ry Cie Yr. SA -Hour r, .8 c5 — Mat�tX td C � E m � 0 r�'' N c c a com ed cn one line) c3 `Y M ,i; M 0 Z Z 7 - f Mug S1FtIl ' ii+1'Y1 i EMU" � 'hb`i k; x X k tdelab-Sb, As. Be, Cd,Cr, FI h �i Cu,pb,hll,Se,Al�,Tn.Z� 9+,9r1 Eftkenf X iw t 5 FI'IRirl stry"i F�IIFI1 Stogy Tom Pwihin HaTwd ldcrGry kttNnt $a nple 01sposal Comment Non-Hazord Fiamrnatte -j $kin lrrlWj Rat.. rn •❑ c.lie:nt Disposal by Lob Poigpn WAnamin Turn Around Time Ftet7lnmo (Prier lob eppro` ill required for expaditsd TA-r W. Requitwonls lk%aso Spody; @ Simdard ❑ Fu9h gene Swm 1. i Reirqulahed by ! Samplet Gate Tme 1, Fxx eived by Dgle TMO 4r . ,lA ti � ' ' ✓ */1 >? 13 I` ii � 'i, 2. RF9wg1nd tyluiX pate Tune 2. Received by Dote Time 3. rZetinquished b5 ( mitt! 3. LaperaDp MeCelved t>)' ~i r Date Tw" f •'�� .. L• �j ' . ('�t . ', 16 1 1(0 a t ice) Te ,p. Bsrk Note: All samples are retained for six weeks from receipt unless other LAB USE CNLY ReoeiptTemp. arran emcnts c rTTado Reo-*%sd on Ice (Checki, � Y © K Ica =3tk - ° C Y N _Fieche Date MJ.)&2C•12 91 SHEALY ENVIRONMENTAL SERVICES, INC. Shealy Lnvironrumtal Svriom, Inc. Pup 1 or 1 E4=mml%um:xr: ME0015C•13 Flrwriwe M-Le: 415r2813 f , Sample Receipt Checklist (SRC} Client: - I. c W10,1'(" Cooler lnspcctod by?daac. _( ! 4 16 • I"?. Lrt tr: -r0lbb-4 5 Means ofreceipr. SESI LIClient U UPS FcdEx Uthet: .1 Y us Mil L Were custody seals present on the cools? Yesl ❑ Nol Z. NA12. If cuntudy arils were present, were they inta_t and unbroken? ;HStrip ID. /$ _i120-;' Chlorine Strip ID: I$ ;:uuler ID t Ormond tetrtperalure upon receipt f Derived (Corrected) temperature. upiln wce.ipt: 1 i_°C ? 1 °C r ! tC r41ethod-.-ZTemperature Blank ❑Against %Wlw TR Gun ID: (-,j TR Gun Correction F.tor: _°C Method ol-cnnlant_ if!rlYet Ice LJ Ice Packs ❑ Dry Ice ❑ Nolte El Yes ❑ NoF�zJONA )" If tempcyature of any cooler exceeded 6.0'C,'vas Pmjccr ManaFler Notified? Phi was Notified by. phone l email,' face-to-face (circle one). ❑ Yes ElNo JaNA form? 4. IS die commercial courier's packing slip attached to this fo? Yes No S. Were proper custody procedures (nelin uished?received) followed? Yes n No 6. Wert: 1Ds listed un the COC? Wert: ru ra, 1 [Q No 7. Were sample 1Ds listed on all sample containers? 121 Y rs ❑ Nu 8. Was collection dale & time listed on the COCA L Yas ❑ No 9. Was collection date & thnc listed on till sample containers? �3'Yas ❑ No 10. Did all rontaincr label information (ID, datm. lane) amerce with the COC? 11. Were tests to be performed listed on the COC? Yes ❑ No 12 Yes I_ I No 12. Did all swnplzi, arrive in the p,uper containers for each test and?or in {rood condition (unbroken, lids on, ctc.)? - Yes Vo 113. Watt udcyuaw sample volwne available? Yrs No 14. Were all samples ttceived within `n the hording time or 48 hours, whichever comes tirsr'1 Yrs u l 5. Were any satnplzs containers missinglexcess (circle one) samples Not listed on COC? n Yes =.1 No nA 16. For VOA Lind RSK-175 samples_ were bubbles present = "pea -size'' (i."ar 6mm in diameter) In rely of the VOA vials? ET Yes U NO UNA I?. Were. all DRUlmetaiVnutrient samples received nt a pH of <2? Yes ❑ No ONA I8. W'�rc all cyanide sianpies received at a pH,- 13 and sulfide samples received at a pli :- H? 2Yes El No ❑ NA 19. % are all npplinhle NH jYKK,'cyanideiphenn1;625 (<0.5m.!�L) samples tree o; residual chlorine? Ca Yes ❑ NU I Ir A )n' %VC:M client mnruid:.s.'requests (i.e. requestcd dilutions, MS1MS[D dcsiWuliena, correctly transcribed from the COC into the comment %=tinn in LUMS? ❑ yesi _ No 21. Was the quotc n.nnber used taken from the container label'? Sample Prc*crv2tioii (Must be completed for any sampie(sl inzorracd%, presmed or wa hesdspace.) Sairp*s) ware rwviv-.4 incormvtly ptemved and were ad used accordirglti in sample receiving with (MS04. HNO3. KC:1. NaOH) using SR R Time of preservation sarnple(s) were rcmivrd wish bubbles `-•6 min in diameter. sarnples(s) . wcrc j=ivW with TRC > 0.5 mg+L (If 419 is me) and were adjusted accordingly in sarnple receiving with sodium thiosulfate (Na2S201) witli Shealy ID: SR barcode labels applied by: Date: �� • l Il ru Comments: Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 12 of 12 SHEALY ENVIRONMENTAL SERVICES, INC. Report of Analysis City of Belmont PO Box 431 Belmont, NC 28012 Attention: Tanya Setzer Project Name: Effluent Pollutant Scan Lot Number:UE15092 Date Completed:05/28/2019 05/29/2019 11:48 AM Approved and released by: Project Manager: Kelly M. Nance A16 A C C R E D I T E D e 00�- The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 1 of 12 SHEALY ENVIRONMENTAL SERVICES, INC. SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative City of Belmont Lot Number: UE15092 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Inorganic Non -Metals The method blank associated with batch 17091 had TKN_ detected at a concentration that was above'/2 the LOQ. There were no detections for TKN in the sample associated with this method blank, negating the possibility of false positives or sample contamination. Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 2 of 12 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary City of Belmont Lot Number: UE15092 Sample Number Sample ID Matrix Date Sampled Date Received 001 Effluent Aqueous 05/15/2019 0908 05/15/2019 002 Effluent Aqueous 05/15/2019 0921 05/15/2019 (2 samples) Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 3 of 12 11 IV. <J_. ..- 1 - 1 1 I.l I".J Client: City of Belmont Laboratory ID: UE15092-001 Description: Effluent Matrix: Aqueous Date Sampled:05/15/2019 0908 Date Received:05/15/2019 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 350.1 (Ammonia - N) 350.1 1 05/17/2019 1528 DMA 17076 1 (Hardness (to) SM 2340C-2011 1 05/16/2019 1548 KFE 16973 1 (Nitrate-Nitr) 353.2 15 05/18/2019 1707 MDD 17139 1 (Phosphorus) 365.1 2 05/22/2019 1534 DMA 17494 1 (TDS) SM 2540C-2011 1 05/17/2019 1117 MGM 16997 1 351.4 (TKN) 351.2 1 05/20/2019 1218 DMA 05/17/2019 1729 17091 CAS Analytical Parameter Number Method Result Q LOQ Units Run Ammonia - N (gas diffusion) 350.1 ND 0.10 mg/L 1 Hardness (total) SM 2340C- 58 10 mg/L 1 Nitrate -Nitrite - N 353.2 16 0.30 mg/L 1 Phosphorus 7723-14-0 365.1 2.2 0.10 mg/L 1 TDS SM 2540C- 590 25 mg/L 1 TKN 351.2 ND 0.10 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 4 of 12 Client: City of Belmont Laboratory ID: UE15092-001 Description: Effluent Matrix: Aqueous Date Sampled:05/15/2019 0908 Date Received:05/15/2019 Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 625.1 625.1 1 05/22/2019 2228 JCG 05/16/2019 1658 16957 Parameter CAS Number Analytical Method Result Q LOQ Units Run Acenaphthene 83-32-9 625.1 ND 1.6 ug/L 1 Acenaphthylene 208-96-8 625.1 ND 1.6 ug/L 1 Anthracene 120-12-7 625.1 ND 1.6 ug/L 1 Benzidine 92-87-5 625.1 ND 8.0 ug/L 1 Benzo(a)anthracene 56-55-3 625.1 ND 1.6 ug/L 1 Benzo(a)pyrene 50-32-8 625.1 ND 1.6 ug/L 1 Benzo(b)fluoranthene 205-99-2 625.1 ND 1.6 ug/L 1 Benzo(g,h,i)perylene 191-24-2 625.1 ND 1.6 ug/L 1 Benzo(k)fluoranthene 207-08-9 625.1 ND 1.6 ug/L 1 4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1.6 ug/L 1 Butyl benzyl phthalate 85-68-7 625.1 ND 1.6 ug/L 1 bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND 1.6 ug/L 1 4-Chloro-3-methyl phenol 59-50-7 625.1 ND 1.6 ug/L 1 bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 1.6 ug/L 1 bis(2-Chloroethyl)ether 111-44-4 625.1 ND 1.6 ug/L 1 2-Chloronaphthalene 91-58-7 625.1 ND 1.6 ug/L 1 2-Chlorophenol 95-57-8 625.1 ND 1.6 ug/L 1 4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1.6 ug/L 1 Chrysene 218-01-9 625.1 ND 1.6 ug/L 1 Dibenzo(a,h)anthracene 53-70-3 625.1 ND 1.6 ug/L 1 1,2-Dichlorobenzene 95-50-1 625.1 ND 1.6 ug/L 1 )ichlorobenzene 541-73-1 625.1 ND 1.6 ug/L 1 )ichlorobenzene 106-46-7 625.1 ND 1.6 ug/L 1 3,3'-Dichlorobenzidine 91-94-1 625.1 ND 8.0 ug/L 1 2,4-Dichlorophenol 120-83-2 625.1 ND 1.6 ug/L 1 Diethylphtha late 84-66-2 625.1 ND 1.6 ug/L 1 Dimethyl phthalate 131-11-3 625.1 ND 1.6 ug/L 1 2,4-Dimethylphenol 105-67-9 625.1 ND 1.6 ug/L 1 Di-n-butyl phthalate 84-74-2 625.1 ND 1.6 ug/L 1 4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 8.0 ug/L 1 2,4-Dinitrophenol 51-28-5 625.1 ND 8.0 ug/L 1 2,4-Dinitrotoluene 121-14-2 625.1 ND 3.2 ug/L 1 2,6-Dinitrotoluene 606-20-2 625.1 ND 3.2 ug/L 1 Di-n-octylphthalate 117-84-0 625.1 ND 1.6 ug/L 1 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625.1 ND 1.6 ug/L 1 bis(2-Ethylhexyl) phtha late 117-81-7 625.1 26 8.0 ug/L 1 Fluoranthene 206-44-0 625.1 ND 1.6 ug/L 1 Fluorene 86-73-7 625.1 ND 1.6 ug/L 1 Hexachlorobenzene 118-74-1 625.1 ND 1.6 ug/L 1 Hexachlorobutadiene 87-68-3 625.1 ND 1.6 ug/L 1 Hexachlorocyclopentadiene 77-47-4 625.1 ND 8.0 ug/L 1 Hexachloroethane 67-72-1 625.1 ND 1.6 ug/L 1 Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1.6 ug/L 1 Isophorone 78-59-1 625.1 ND 1.6 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% t of holding time W = Reported on wet weight basis Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 5 of 12 Client: City of Belmont Laboratory ID: UE15092-001 Description: Effluent Matrix: Aqueous Date Sampled:05/15/2019 0906 Date Received:05/15/2019 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 1 05/22/2019 2228 JCG 05/16/2019 1658 16957 CAS Analytical Parameter Number Method Result Q LOQ Units Run Naphthalene 91-20-3 625.1 ND 1.6 ug/L 1 Nitrobenzene 98-95-3 625.1 ND 1.6 ug/L 1 2-Nitrophenol 88-75-5 625.1 ND 3.2 ug/L 1 4-Nitrophenol 100-02-7 625.1 ND 8.0 ug/L 1 N-Nitrosodimethylamine 62-75-9 625.1 ND 1.6 ug/L 1 N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 1.6 ug/L 1 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625.1 ND 1.6 ug/L 1 Pentachlorophenol 87-86-5 625.1 ND 8.0 ug/L 1 Phenanthrene 85-01-8 625.1 ND 1.6 ug/L 1 Phenol 108-95-2 625.1 ND 1.6 ug/L 1 Pyrene 129-00-0 625.1 ND 1.6 ug/L 1 1,2,4-Trichlorobenzene 120-82-1 625.1 ND 1.6 ug/L 1 2,4,6-Trichlorophenol 88-06-2 625.1 ND 1.6 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 61 37-129 2-Fluorophenol 61 24-127 Nitrobenzene-d5 60 38-127 Phenol-d5 74 28-128 Terphenyl-d14 101 10-148 2,4,6-Tribromophenol 80 41-144 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 6 of 12 Client: City of Belmont Laboratory ID: UE15092-001 Description: Effluent Matrix: Aqueous Date Sampled:05/15/2019 0908 Date Received:05/15/2019 Prep Method 200.2 Analytical Method Dilution Analysis Date Analyst 200.8 1 05/21/20191513 BNW Prep Date Batch 05/16/2019 1750 16950 CAS Analytical Parameter Number Method Result Q LOQ Units Run Antimony 7440-36-0 200.8 58 2.0 ug/L 1 Arsenic 7440-38-2 200.8 ND 2.0 ug/L 1 Beryllium 7440-41-7 200.8 ND 0.40 ug/L 1 Cadmium 7440-43-9 200.8 ND 0.50 ug/L 1 Chromium 7440-47-3 200.8 ND 5.0 ug/L 1 Copper 7440-50-8 200.8 10 5.0 ug/L 1 Lead 7439-92-1 200.8 ND 1.0 ug/L 1 Nickel 7440-02-0 200.8 ND 5.0 ug/L 1 Selenium 7782-49-2 200.8 ND 5.0 ug/L 1 Silver 7440-22-4 200.8 ND 1.0 ug/L 1 Thallium 7440-28-0 200.8 ND 0.50 ug/L 1 Zinc 7440-66-6 200.8 55 10 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% t of holding time W = Reported on wet weight basis --__j Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 7 of 12 Client: City of Belmont Laboratory ID: UE15092-002 Description: Effluent Matrix: Aqueous )ate Sampled:05/15/2019 0921 ate Received:05/15/2019 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 10-204-00-1-X (Cyanide - To) SM 4500-CN E- 1 05/22/2019 1723 MSG 05/22/2019 1331 17503 1 (Phenolics) 420.4 1 05/23/2019 1245 MSG 17637 1 (HEM (oil and) 1664B 1 05/23/2019 0946 ARP 17608 CAS Analytical Parameter Number Method Result Q LOQ Units Run Cyanide - Total 57-12-5 SM 4500-CN 0.016 0.010 mg/L 1 Phenolics 420.4 ND 0.0050 mg/L 1 HEM (oil and grease) 1664E ND 5.0 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 8 of 12 Client: City of Belmont Laboratory ID: UE15092-002 Description: Effluent Matrix: Aqueous Date Sampled:05/15/2019 0921 Date Received:05/15/2019 Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 624.1 624.1 1 05/17/2019 0330 KGT 16984 CAS Analytical Parameter Number Method Result Q LOQ Units Run Acrolein 107-02-8 624.1 ND 5.0 ug/L Acrylonitrile 107-13-1 624.1 ND 5.0 ug/L Benzene 71-43-2 624.1 ND 1.0 ug/L Bromodichloromethane 75-27-4 624.1 6.1 1.0 ug/L Bromoform 75-25-2 624.1 ND 1.0 ug/L Bromomethane (Methyl bromide) 74-83-9 624.1 ND 2.0 ug/L Carbon tetrachloride 56-23-5 624.1 ND 1.0 ug/L Chlorobenzene 108-90-7 624.1 ND 1.0 ug/L Chloroethane 75-00-3 624.1 ND 2.0 ug/L 2-Chloroethylvinylether 110-75-8 624.1 ND 5.0 ug/L Chloroform 67-66-3 624.1 9.5 1.0 ug/L Chloromethane (Methyl chloride) 74-87-3 624.1 ND 2.0 ug/L Dibromochloromethane 124-48-1 624.1 1.5 1.0 ug/L 1,1-Dichloroethane 75-34-3 624.1 ND 1.0 ug/L 1,2-Dichloroethane 107-06-2 624.1 ND 1.0 ug/L 1,1-Dichloroethene 75-35-4 624.1 ND 1.0 ug/L trans-1,2-Dichloroethene 156-60-5 624.1 ND 1.0 ug/L 1,2-Dichloropropane 78-87-5 624.1 ND 1.0 ug/L cis- 1,3-Dichloropropene 10061-01-5 624.1 ND 1.0 ug/L trans-1,3-Dichloropropene 10061-02-6 624.1 ND 1.0 ug/L Ethvlbenzene 100-41-4 624.1 ND 1.0 ug/L iylene chloride 75-09-2 624.1 ND 1.0 ug/L ?,2-Tetrachloroethane 79-34-5 624.1 ND 1.0 ug/L Tetrachloroethene 127-18-4 624.1 ND 1.0 ug/L Toluene 108-88-3 624.1 ND 1.0 ug/L 1,1,1-Trichloroethane 71-55-6 624.1 ND 1.0 ug/L 1,1,2-Trichloroethane 79-00-5 624.1 ND 1.0 ug/L Trichloroethene 79-01-6 624.1 ND 1.0 ug/L Vinyl chloride 75-01-4 624.1 ND 1.0 ug/L Run 1 Acceptance Surrogate Q % Recovery Limits Bromofluorobenzene 97 70-130 1,2-Dichloroethane-d4 102 70-130 Toluene-d8 96 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% t of holding time W = Reported on wet weight basis _..__.; Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 9 of 12 Chain of Custody and Miscellaneous Documents Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www,shealylab.com Page 10 of 12 o � Cn n N Shealy Environmental Services, Inc_ CWA % niFDES os viantage Pod at neive Number West Calu nt la, South Carolina AM :.f Chain at Custody Record TPlephoene No. ;803) 7�31-97D4 Fax Na. (8(l3) 791-91 ;1 w.vx.slrCalyL^>?3.ccim CI'iew Report') CxAa� sarmees sipr,aiuro w r Quote No. Eeirvx�,YvwTP _ 'Tanya Swsr a'�` — �Innbeo NA 14728 f'ega Adtlrees i'ammebers al e.. py, tuirp, Mi cm be racorded In tiler`s twMas of 1 C�. Stale Cale Telephone No. I Fax Ht. f i t 1 2 1 3 1 1 Numbe< cf Cantanels G K s I L, A E J Q Bo 8e Belgrord F{C rip Email 't(t: 4 < f 1 3 5 3 Ji 7 ?rH66�tl31Wf ProjCrcl Marne w f 1 p IILa I� Scar l Project N:a tber P.a hJurn oet 33 g _III ( a Z a ,pII�y V E 1 5092R SawP:e ICl r Geec Ilan tonUmers foreach semala may to t,.,'itC Y., l�rq@ 24-Harr U Matrix Q m zi Sry CV 5 cY,s,z ambined an owls One) p O U t— y > i ! Motets - Sq, Ae 9a. Cd,Cr_ Efluelrt Q WIN x x x Y. X Cu Pb.N-,ee,Ag.Th]_n Pir shy, I SI Ef luent 4VVtr X X x X Q ^•P 9t, rt Fln(sh Sort i Flntsh I ftri FktleJl� ljaFs ie Hazard ldenBificaWi Sample Disposal Cmment Nnn-H;rrtrrd Fbinmable ❑ Skin Irdant Met►m to C5&anl Dispcme by Le.b .• 5on Unknown TcmAround Tiny: Pcgvired (Prior web Apprr,-M requk id for axpPdited 7All QC Requkementi (PJeaw Spedy} ® wllllY(�'If ❑ ii Rlelinquis>'!ed by! Sampler 1,9tu Time 1. fteceMed Date time a- a 3 2. Prlingt tey Da Er Vnve ^ a. �eKsed by Cale Tit,* 3. RaGnquisMd, by Mile Tine 3. laboratory Recaived by r h ^ Note: All samples are retained for six week:; from receipt unless other LAB USE ONLY Ree._ Tarnp. Ttintli, rank arranq emsnta a Ire made Received on !C (C,gck) N 0IIx Pack • t ' C U) m n m z n SHEALY ENVIRONMENTAL SERVICES, INC. StxaMlGvimnmcnt#1Sc�victa,luc. [;,,,� ,. DximmtNLLmbr--W 1ISC W ;:L:_avoEXII :7;'.'I Sample Receipt Checklist (SRC) Client. Belmont Cooler Inspected h •r'date: M r 5115A9 T-ut N: UE15092 Mrs of reCeipt-, 0 SESI ❑ Client ❑ UPS FcdEx El Other: © Y cs ® No 1. W urc custody seals present on the cooler? Yes No NA 2. If cuuod • seals were resent, were they intact and unbroken'.+ H Strip ID_ 111-2225 cWorine Strip TD: 19-35 7e�kxl JSI{ — by:J _ rigulal tentperaturc upon mccipt + Derived (Corrected) temperature upon rt:ceipt %Solid, Snap -Cup ID: NA 2.8 12.8 oC NA i NA vC NA (NA or NA /AlA 'C cthnd: ( *re.mperature Blanl; ❑Agahlst Bottles IR Gun TD: 6 IR Gun Correction racwr: 0 °C Icthod of coolant: ® Wet Tee ❑ lac Packs ❑ PEX Ice ❑ None ❑ Yes ❑ No O NA 3. If tentperuturu of any cooler exceeded 6.0°C, uas Proj cot Manr get Nutifit%12 PM was Nolificd by, phone ,' email 1 face-lo-face (cur le one). ❑ Yes ❑ NO ® NA 4, U the commercial ootttier's packing; Aip atwhed to this film? ® Yes ❑ do S. Were proper custody prtwedures (rclinquishecUreceived) fnlinwod? Q� Yes flu 6. Wcrc sample IDs listed on the MC? ® Yes e1 N., 7. Wcrr sample IDs listed on all sample cnntainers? ® Yer: No 3. Wee: callcotirm date a time listed on the COC? ® Yesi ❑ No 9. Was colloedon date & time listed on all sample containers? 0 Yea ❑ No 10, Did all container IubCl information (ID, date, time') agree with the COC? ® Yes ❑ No 11. Wcre tests to be performed listed oil the COC? ® Yes El12. No Thd all satnples arrive in the Praper contatnerF for each trot and?or in good oautslition (unbroken, lids on, etc.)? Ycxl ❑ No 113. Was adequate sumpic volume available? Vj ,. cs No 14. Were all rnmplms received within ,S ttw bolding tune or 4li hamu, whichevercornes first? yCSJ W1 No 15. Were any sam Ica containtxs missirtgr'excesc eirck onc) samples Not listbd on COC? ® Y�-sl ❑ No ❑ NA 16. For VOA and KSK-175 samp1m, wcrc bubbles present>"pea-Size" (%"or 6mm in diameter) to any of the Y0A vials? ® Yrs L1 No NA 17. Were all DRO..meuals."nutricnt Famples received at a pH Of < r? Q] Yes No NA IS. Werc all cynnidr samples received at a pH > 12 and sut1-L'& ham kit rcoutved at a p1I> 9? ® Yes ❑ No ❑ NA 1 R. were all applicable ,? ,cyanidrlphanuN625 (e 0,5mg�L) samples free of rsidua chl(wine Yes ❑ No NA 20. Were client remarics4equests (i.e. ruqumled dilutions, iv VNISD desianadons, etc...) correctly transcribed from the COC into the comment section in I.IMS? LJ Yes LQN*I 121. was the cluote number listed on the containcr label'! If yes, Quote iJ NA S,,iinple PmservAtion (Must be completed for anv sample(s) incorrectly pt+r avoci or Mth headspace.) tiamplc(s) NA wero Tweiv0d incorrectly pmcrved and t,.,crc adjusted U"ordingly t'.1 sample receiving with NA ml- of circle one: TUS04, HNO3, HC I, NaOII using SR 4 NA _ lime oipreservatitm NA _ ._ If more than one preservative is needed, please note in the comments below. (s l Qd='. (3) wcxr. received with bubbles >,6 mm in diameter. s(s) NA wererocc ivcd K ith TftC > 0.5 m�7. (i F rq19 is rrn) ar_ti were d accordingly in sample receiving with sodium thiosulfate (Nu2s,O.t} xzth Shealy 1T): NA VR r>sic hhcl�ap(?lied by: ]SN Date: 5135119 Comments: Shealy Environmental Services, Inc. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Page 12 of 12 aceAnalytical (-,� Report of Analysis City of Belmont PO Box 431 Belmont, NC 28012 Attention: Tanya Setzer Project Name: Effluent Pollutant Scan Lot Number:VH12113 Date Completed:08/31/2020 4 a,, - �,e dw �7 08/31 /2020 4:21 PM Approved and released by: Project Manager I: Hannah K. Lucas o� ANSI bric al Accreditation Scud A C C R E D I T E D TESTING LABORATORY The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Page I of 10 PACE ANALYTICAL SERVICES, LLC SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative City of Belmont Lot Number: VH12113 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Pace policies. Any exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Pace Project Manager listed on the cover page. Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 2 of 10 PACE ANALYTICAL SERVICES, LLC Sample Summary City of Belmont Lot Number: VH12113 Sample Number Sample ID Matrix Date Sampled Date Received 001 EFFLUENT Aqueous 08/12/2020 0904 08/12/2020 002 EFFLUENT Aqueous 08/12/2020 0859 08/12/2020 (2 samples) Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 3 of 10 II II I yJ"I I I l I I I I I I Ili-IJ Client: City of Belmont Laboratory ID:VH12113-001 Description: EFFLUENT Matrix: Aqueous ite Sampled:08/12/2020 0904 to Received:08/12/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 350.1 (Ammonia - N ) 350.1 1 08/14/2020 1554 DMA 63567 1 (Hardness (to) SM 2340C-2011 1 08/18/2020 1524 KFE 63935 1 (Nitrate-Nitr) 353.2 15 08/19/2020 1612 AMR 64079 1 (Phosphorus) 365.1 1 08/18/2020 1516 DMA 63856 1 (TDS) SM 2540C-2011 1 08/17/2020 2232 MOM 63804 1 351.4 (TKN) 351.2 1 08/19/2020 1749 DMA 08/19/2020 1303 63990 CAS Analytical Parameter Number Method Result Q LOQ Units Run Ammonia - N (gas diffusion) 350.1 ND 0.10 mg/L 1 Hardness (total) SM 2340C-2011 52 10 mg/L 1 Nitrate -Nitrite - N 353.2 23 0.30 mg/L 1 Phosphorus 7723-14-0 365.1 1.5 0.050 mg/L 1 TDS SM 2540C-2011 410 25 mg/L 1 TKN 351.2 ND 0.10 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 4 of 10 Client: City of Belmont Laboratory ID:VH12113-001 ascription: EFFLUENT Matrix: Aqueous Sampled:08/12/2020 0904 Received: 08/12/2020 Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 200.2 200.8 1 08/20/2020 1433 BPK 08/19/2020 1609 63931 Parameter CAS Analytical Number Method Result Q LOQ Units Run Antimony 7440-36-0 200.8 9.6 2.0 ug/L 1 Arsenic 7440-38-2 200.8 ND 2.0 ug/L 1 Beryllium 7440-41-7 200.8 ND 0.40 ug/L 1 Cadmium 7440-43-9 200.8 ND 0.50 ug/L 1 Chromium 7440-47-3 200.8 ND 5.0 ug/L 1 Copper 7440-50-8 200.8 9.8 5.0 ug/L 1 Lead 7439-92-1 200.8 ND 1.0 ug/L 1 Nickel 7440-02-0 200.8 ND 5.0 ug/L 1 Selenium 7782-49-2 200.8 ND 5.0 ug/L 1 Silver 7440-22-4 200.8 ND 1.0 ug/L 1 Thallium 7440-28-0 200.8 ND 0.50 ug/L 1 Zinc 7440-66-6 200.8 52 10 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 t of holding time W = Reported on wet weight basis \nalytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 5 of 10 Client: City of Belmont Laboratory ID: VH12113-002 Description: EFFLUENT Matrix: Aqueous ate Sampled:08/12/2020 0859 to Received:08/12/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 10-204-00-1-X (Cyanide - To) SM 4500-CN E- 1 08/13/2020 1523 KFE 08/13/2020 1306 63227 1 (Phenolics) 420.4 1 08/28/2020 1326 MSG 62991 1 (HEM (oil and) 1664B 1 08/25/2020 0932 GLT 64559 CAS Analytical Parameter Number Method Result Q LOQ Units Run Cyanide - Total Phenolics HEM (oil and grease) 57-12-5 SM 4500-CN E-2 ND 420.4 ND 1664E ND LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com 0.010 mg/L 1 0.0050 mg/L 1 5.0 mg/L 1 Page 6 of 10 Client: City of Belmont Laboratory ID: VH12113-002 Description: EFFLUENT Matrix: Aqueous Date Sampled:08/12/2020 0859 Date Received:08/12/2020 Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 624.1 624.1 1 08/14/2020 0239 STM 63488 2 624.1 624.1 1 08/20/2020 0226 STM 64118 Parameter CAS Number Analytical Method Result Q LOQ Units Run Acrolein 107-02-8 624.1 ND 5.0 ug/L 1 Acrylonitrile 107-13-1 624.1 ND 5.0 ug/L 1 Benzene 71-43-2 624.1 ND 1.0 ug/L 1 Bromodichloromethane 75-27-4 624.1 1.8 1.0 ug/L 1 Bromoform 75-25-2 624.1 ND 1.0 ug/L 2 Bromomethane (Methyl bromide) 74-83-9 624.1 ND 2.0 ug/L 1 Carbon tetrachloride 56-23-5 624.1 ND 1.0 ug/L 1 Chlorobenzene 108-90-7 624.1 ND 1.0 ug/L 1 Chloroethane 75-00-3 624.1 ND 2.0 ug/L 1 2-Chloroethylvinylether 110-75-8 624.1 ND 5.0 ug/L 1 Chloroform 67-66-3 624.1 3.5 1.0 ug/L 1 Chloromethane (Methyl chloride) 74-87-3 624.1 ND 2.0 ug/L 1 Dibromochloromethane 124-48-1 624.1 ND 1.0 ug/L 1 1,1-Dichloroethane 75-34-3 624.1 ND 1.0 ug/L 1 1,2-Dichloroethane 107-06-2 624.1 ND 1.0 ug/L 1 1,1-Dichloroethene 75-35-4 624.1 ND 1.0 ug/L 1 trans- 1, 2-Dichloroethene 156-60-5 624.1 ND 1.0 ug/L 1 1,2-Dichloropropane 78-87-5 624.1 ND 1.0 ug/L 1 cis- 1,3-Dichloropropene 10061-01-5 624.1 ND 1.0 ug/L 1 trans-1,3-Dichloropropene 10061-02-6 624.1 ND 1.0 ug/L 1 (benzene 100-41-4 624.1 ND 1.0 ug/L 1 iylene chloride 75-09-2 624.1 ND 1.0 ug/L 1 1,1,2,2-Tetrachloroethane 79-34-5 624.1 ND 1.0 ug/L 1 Tetrachloroethene 127-18-4 624.1 ND 1.0 ug/L 1 Toluene 108-88-3 624.1 ND 1.0 ug/L 1 1,1,1-Trichloroethane 71-55-6 624.1 ND 1.0 ug/L 1 1,1,2-Trichloroethane 79-00-5 624.1 ND 1.0 ug/L 1 Trichloroethene 79-01-6 624.1 ND 1.0 ug/L 1 Vinyl chloride 75-01-4 624.1 ND 1.0 ug/L 1 Run 1 Acceptance Run 2 Acceptance Surrogate Q % Recovery Limits Q % Recovery Limits Bromofluorobenzene 106 70-130 102 70-130 1,2-Dichloroethane-d4 86 70-130 106 70-130 Toluene-d8 94 70-130 108 70-130 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % t of holding time W = Reported on wet weight basis ___ .analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 7 of 10 Chain of Custody and Miscellaneous Documents Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 8 of 10 o� M n ipShealy D Environmental Services, Inc. CWA / NPDES 16 Vantsgc Point Drivo 0 �Ifitl4TY `' Chain of Custody Record VVest Columbia. South Cafo;ir,a 20172 Telephone No. (8D,3)791-a7Q0 Fax Na- (&05)791-9111 � < �utuslw�lylab,tnm rD -`�� Client Hep anio Contact Sam .Shy lure erlrrnr>ewwr.f Sandra Craft X_..1 - -- A*V*ss F tzQ Bare V C o naid Fararrelem (t.P., pH, rerV, [] ) .an 6> reo=atl In cWrk'haxas 3 m Cltr Stale Curti; Tk4milwnr•- Nu ! F„x Ni I 1 1 1 2 1 3 1 < 'z 1 Jz1rJ 6e1m�,1 NC krn9il rl ! D A 2 J I n CD m PfQJ l)t Nsme 4 4 1 3 5 3 5 7 n m Project IW.mbar 1`1.0 Numt-er N - n A U 47 N .� (rJ V) 45 o CDSamplo ID? 7axrlprion rO� E 1. U Q eNj p (� Lr nente Tines �, a 'Cnntainers [If mch iarrpie may be � � Matrix � L � 0 q � Q � Ki co Yr. 24 Hour I cunrranaJ a� one Gnej m > N Z Z i 'a-t1 _ U o !1 o° Effluent C WW X X X X X Finish j 14 4 ' -- — w e• JfrSr Effluent G Yt'W X X X X Fni-.h o Shawl (b Finish Wrl CD -gin Q Smrt - --' 0 o(4ible Ii. zareJ ldaallri:allon Sa-nale Disposal Ca Nun -Hazard Flammable SS in Irritant 0 hcep.n o Client i7A DiEposel by Lab �,craon r Pvcoryxrl i m Around 71rne gequred (PVr lab apFroval :equ reJ forerpadileJ TAT) QC Regnr rernents(Plaa" Spa' iry) �9tan&d ❑Fush(aease:pan!) ellnqui �e:i by; Sumplur 17nrr. I mr+. 1. kennlviul Lw nqulsherf DraTme2. Received by W Note: All samples are retained for sic weeks from receipt unless other 11 An .L4F ONI Y arranp arrmnts are made RacoMcd on I- (Check] 14 []ImPeck Number 1 cf 1 Njmbm of Ccmtaxers ,_•._ ,. 9gltle ___ I'reserVEIve • 'I���I�!��Illlllglll VH12113 HKL r.W.Wt.- S3. AR, Fa, rd,Cr vu,ph'vri,Se hy,Tl i;Zn _.... i V' li Temp. Blank O G^ V ❑ tl PACE ANALYTICAL SERVICES, LLC Shealy r§r inmmenl:J Kmvices, Inc Jocur:rcnf Humber. M151M U-14 Sumple receipt Checklist (SRU) Client; BEL,MONT Cooler Ins ected b ;date: CMs7 1 8112120 Lot #; VIi 121 Mums urrecc:ipt: Z SES1 ❑ Client ❑ UPS ❑ FedEx Other: _ n Yes Nol 11. We -c custody scale: t rtsent on the cooler? 1-1 Yes d Nol ® NA12. If custody seals were premert, were they intact 21ld urll'OUO pl-T Strip 1D: 24-1455 Chlorine Strip ID. 20-153. Te b�tad''by, CMS? Original icmperaturc upon rmcipt f LUcr:vcd (Corrm.LCd) t::mpurulurc upor• rcc6pt $ solid snap -CUT: 1= 2.6 r2.6 aC NA ,fNA aC NA !NA DC! NA /NA aC T*-- I Oft �12F;luc Date; arV2ulS NA Mel'rnn1: ®Tearperature Blank ❑Againsl RuILICs 1R Chin iD: i IR Gn-r Comxaion Factor;11 `C Method cf caola-rt: Wet Ice ❑ Toe Packs ©Dtv lee ❑ -None , ❑ Yes ❑ No ® NA 3. If icinpLTHIUM d' arty cuuh:r cxc:'7d 6.0°C, Has Project (Manager Notified'? ' FM was Notified by: phone ! email J faoe-to faoo ,oir.lc one} Cl Yrs ❑ NU ®NA 4. Js tae cs+romenciaJ cotu'Am's pack;ng slip attar:hW to this Flinn? 91 Yes 0 No 5- W= pnnpor c4 mtody procedtlrcK (relmquishe&received) followed? I Yrc N4i 6. Were-mmple IEN l s'ed on the ® Yes ❑ No 7. Wcrc sample IN Estcd on al: sample oudainc:b? ® Yes 0 No 8- W03 collectiv:i dat. & time listc i on the COO j ® Yes ElNo _ 9 Was collection date & time liStWI On all st_rnpie container :; Ye s ❑ No 10. Did all container Iabc. information (1D, date, Iiume) agrt= with thr. COC? V1 Yes ❑ No 11. Were tests to be narrommd Iiated on t}ic COC? i 91 Yes U No 12- CH all 4amplc: arrive ir the proper containers roe etu:h (unbroken; lids on, etc.)? ® Yes [71 Nu 13_ Was adeyuutc Sam& eolumc avai:abl: ? Yes r! No ].a. Wcrc all samples received w4hir ''A the hnl::ing time o Yes ® No — 15- Were any samples eonwinurs missingicxcess (circle on 16. For VOA and RSI;-1 ,,5 samples, were bubbles present ® Yes ❑ No ©1tiA is artly of the VOA vials? 1 Yes No NA 7. Were all DRO? atetWsinument sampl_s cccivod at a p) ® Yes No El NA "S. We c all cyanide samples Tf.Mivrd at r. OH � 12 and set W'e:e ® Yrs ONO ©1tiA a rtpplrra11'. - - - _ 'pheno U625 (�- and or in good r 48 hours, whichever omes frrst3 e) Sam less Not I:Sted n COC? tpe it diameter) l T <: 2? I 1 "r)e Sam FlIcs rrccived!at a vH > W 20. 11ir'ere clued rcrnarkslruqucsls (i.e. requested dihltinne. MS NTSD designatio. Q Yes ❑ No ® NA correctly transcr,l ed front the COC into, the comment secriarm ir• LIN19? 0 Yes El Nol 121. Was the quote number liswd col tho container label? If ye*, Quote 0 147' i Imnle Preservation (Must be completed Cur any sampidk} incorrectly preserved or w'ity h; adspace.} iamplc,$) NA were rcccived irworrrmily prrseivod and were adj u,trruple rccuiving wilh h'A ml. of ci -:e one: I i?504, HNO,. HCI, NaOH asiug SR 4 NA ITr-e of preservation NA If more than ore pre:,ervative ;s ncxxled, pleasz noteirn l e comments 1 ,.'ample(s) _ 02 (3) were rect'vcd w'th bubbles >6 nurr j Sainpirs(s) NA _ - were received with TRC > 0. i mg?L (If ;f 19 is no adjusted r. ordingty in sample reccitidng %Vito sodium thiosu.Wc W;t`r gleal.� IT): NA barcode labels applied by; CM Comments: i?air.: V11120 ex. eel ticuur4ingt� OPW. t diatnGti7. I cnd ►v= Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 10 of 10 aceAnalytical Report of Analysis City of Belmont PO Box 431 Belmont, NC 28012 Attention: Tanya Setzer Project Name: Effluent Pollutant Scan Lot Number:V104079 Date Completed:09/16/2020 09/16/2020 4:40 PM Approved and released by: Project Manager I: Hannah K. Lucas iA lkiA ANSI hti-i A—dit tW Bard A C C R E D I T E D TESTING LABORATORY The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Paget of 8 PACE ANALYTICAL SERVICES, LLC SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative City of Belmont Lot Number: V104079 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the Pace Analytical Services, LLC ("Pace") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Pace policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below. If you have any questions regarding this report please contact the Pace Project Manager listed on the cover page. Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 2 of 8 PACE ANALYTICAL SERVICES, LLC Sample Summary City of Belmont Lot Number: V104079 Sample Number Sample ID Matrix Date Sampled Date Received 001 Effluent Aqueous 09/04/2020 0901 09/04/2020 (1 sample) Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 3 of 8 J1 a I II V VI"-I1 - VVI I.V VV.I I-j .J.,,.- Client: City of Belmont Laboratory ID: VI04079-001 Description: Effluent Matrix: Aqueous Date Sampled:09/04/2020 0901 Date Received:09/04/2020 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 1 09/15/2020 1838 JCG 09/08/2020 1830 65987 CAS Analytical Parameter Number Method Result Q LOQ Units Run Acenaphthene 83-32-9 625.1 ND 1.6 ug/L Acenaphthylene 208-96-8 625.1 ND 1.6 ug/L Anthracene 120-12-7 625.1 ND 1.6 ug/L Benzidine 92-87-5 625.1 ND 8.0 ug/L Benzo(a)anthracene 56-55-3 625.1 ND 1.6 ug/L Benzo(a)pyrene 50-32-8 625.1 ND 1.6 ug/L Benzo(b)fluoranthene 205-99-2 625.1 ND 1.6 ug/L Benzo(g,h,i)perylene 191-24-2 625.1 ND 1.6 ug/L Benzo(k)fluoranthene 207-08-9 625.1 ND 1.6 ug/L 4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1.6 ug/L Butyl benzyl phthalate 85-68-7 625.1 ND 1.6 ug/L bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND 1.6 ug/L 4-Chloro-3-methyl phenol 59-50-7 625.1 ND 1.6 ug/L bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 1.6 ug/L bis(2-Chloroethyl)ether 111-44-4 625.1 ND 1.6 ug/L 2-Chloronaphthalene 91-58-7 625.1 ND 1.6 ug/L 2-Chlorophenol 95-57-8 625.1 ND 1.6 ug/L 4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1.6 ug/L Chrysene 218-01-9 625.1 ND 1.6 ug/L Dibenzo(a,h)anthracene 53-70-3 625.1 ND 1.6 ug/L 3,3'-Dichlorobenzidine 91-94-1 625.1 ND 8.0 ug/L 2,4-Dichlorophenol 120-83-2 625.1 ND 1.6 ug/L Diethyl phthalate 84-66-2 625.1 ND 1.6 ug/L Dimethyl phthalate 131-11-3 625.1 ND 1.6 ug/L 2,4-Dimethylphenol 105-67-9 625.1 ND 1.6 ug/L Di-n-butyl phthalate 84-74-2 625.1 ND 1.6 ug/L 4,6- Din itro-2- methyl phenol 534-52-1 625.1 ND 8.0 ug/L 2,4-Dinitrophenol 51-28-5 625.1 ND 8.0 ug/L 2,4-Dinitrotoluene 121-14-2 625.1 ND 3.2 ug/L 2,6-Dinitrotoluene 606-20-2 625.1 ND 3.2 ug/L Di-n-octylphthalate 117-84-0 625.1 ND 1.6 ug/L 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625.1 ND 1.6 ug/L bis(2- Ethyl hexyl)phthalate 117-81-7 625.1 ND 8.0 ug/L Fluoranthene 206-44-0 625.1 ND 1.6 ug/L Fluorene 86-73-7 625.1 ND 1.6 ug/L Hexachlorobenzene 118-74-1 625.1 ND 1.6 ug/L Hexachlorobutadiene 87-68-3 625.1 ND 1.6 ug/L Hexachlorocyclopentadiene 77-47-4 625.1 ND 8.0 ug/L Hexachloroethane 67-72-1 625.1 ND 1.6 ug/L Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1.6 ug/L Isophorone 78-59-1 625.1 ND 1.6 ug/L Naphthalene 91-20-3 625.1 ND 1.6 ug/L Nitrobenzene 98-95-3 625.1 ND 1.6 ug/L 2-Nitrophenol 88-75-5 625.1 ND 3.2 ug/L LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% H = Out of holding time W = Reported on wet weight basis Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 4 of 8 Client: City of Belmont Laboratory ID:V104079-001 Description: Effluent Matrix: Aqueous Date Sampled:09/04/2020 0901 Date Received:09/04/2020 Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 625.1 625.1 1 09/15/2020 1838 JCG 09/08/2020 1830 65987 Parameter CAS Number Analytical Method Result Q LOQ Units Run 4-Nitrophenol 100-02-7 625.1 ND 8.0 ug/L 1 N-Nitrosodimethylamine 62-75-9 625.1 ND 1.6 ug/L 1 N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 1.6 ug/L 1 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625.1 ND 1.6 ug/L 1 Pentachlorophenol 87-86-5 625.1 ND 8.0 ug/L 1 Phenanthrene 85-01-8 625.1 ND 1.6 ug/L 1 Phenol 108-95-2 625.1 ND 1.6 ug/L 1 Pyrene 129-00-0 625.1 ND 1.6 ug/L 1 1,2,4-Trichlorobenzene 120-82-1 625.1 ND 1.6 ug/L 1 2,4,6-Trichlorophenol 88-06-2 625.1 ND 1.6 ug/L 1 Run 1 Acceptance Surrogate Q % Recovery Limits 2-Fluorobiphenyl 70 37-129 2-Fluorophenol 36 24-127 Nitrobenzene-d5 67 38-127 Phenol-d5 57 28-128 Terphenyl-d14 71 10-148 2,4,6-Tribromophenol 47 41-144 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% t of holding time W = Reported on wet weight basis . --- .Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 5 of 8 Chain of Custody and Miscellaneous Documents Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 6 of 8 o� cwa IlVPDFS Charm' of Custody Record Cliant Rcpnrl to Contfc f3elm0nl WN'7P Tanva ScIzR ITeaphoneNo. ; Fax No.; Shl l4ly EnvirDrimenta! Services, Inc. 106 Vantage Pc'nr Drivo "rest Col UMbIS, South Carolina Liu1 TL, TalPphone No_ (80 1791-971DO Fax Nc. (803)791-9111 arirrarn �NG 11— 1 -�rcljt+cl Name c f Scan P-olec:NumGnr PO'Number 41 •-1 1 w Santlr 1pk:ID!DLscdpn Date r Irte S J iCcrteiners for eeth sample rray � ail } fl combinod an one IInE) Yr, 24-Hoar v n Malrl% C < > 1 3:srt Y CIA-4— C WW L r , 1 Fi•,iSb Number I C26 Page son to recorded rr, owk hnmpr, 4` I NumW et Containers _ Bollic V104079 RoSsiX! I-azard Iderdlicauon In.-w D'epcanl C OMMUnt Non -He 8: Wnrnablc DSkln Ira�anl R=rn to 3Ilent ® Disposal W Lab P4son UrY.n m Turn Around -ime Nqulpp red (Prior lab atmrel ra;luinitl 'ur ;: puditcd TAT) QC RegLkernenls (FMn. t! Spearj) GA Smderd ❑ hush IFkasc a ; f Re!inqAehegby!Sampler Date TGie 1.Rereiwnl �p r 2. Rehn alwri Dale 'I-Wric _ ` - _ 2. Recei,rJ ty' 1fJ( l�-ylJ l%7' �t ( \ 9.!?el!ngUlSh&d by Dale -1me 3 L�ior..lor F?cei✓eC __ iVate: Alf Samples lire retained for six weeks from receipt unless oth&r L U USE ONLY drranaernents are made Heiviw:d a., Ice (C nk) " 1—I114 F Ike peck dte Time Itn I Stioi�TaTP• le yti. Ftlynt __ C Y ❑ N IJ Effective Dale C2•ou.2ol PACE ANALYTICAL SERVICES, LLC `yl:unlyEnvirrmwnialFwvkw,:na wAV I a't Dc euneeol h`ur-Awn Mt?1101 Er:.' 4 1=tratne Daly 902-21i:1 R Sample Receipt Checklist (SRC, Oient. Belmont Crolcrinspected +date: Mra' i 0914,2020 lAr.#: V104079 earls ofneceipt: SESi []Cli.ut ❑ UPS [] pedSx F1 Other; -- i� Yes Nal 11. Were castotly seals presrm on 'die coo:t:r`1 Yes Nol ha NA 2. if custocv seamis were . csr i• were tltev intact and turbrokan? pH Strip ID-. na Ch:orinc Strip 1D. NA Tesird by, h'A _ Onginal temperature upon receipt l Derived (Corrected) :emperatury upon receipt °i6Solid Snap -Cup ID: NA 2.8 12.8 OC. NA / NA vC NA /NA eC NA- ,NA -C -- Method_ 6dTcmperaturc Blank ❑AVainst Bottles bR Gun ID: _ 5 IR Gun CorrectionPaatnr: 0 vC,. Nfe-thod of coolant: ® Wet Ice [I!ce Packs [ID [cc f : Iwte ©Y El No Nrl i, if ten petaturti of uny cooler exceeded 6 0T. was Project 1 IAnagcr Nodried? M was Notified by, phone i entail / face -no -face (circley 1e ), © Yes ❑ No © No ®hint 4, Is the commercial courier's packing slip attached to this fonr.? 5, Wuc propercu.Yiody prumxdtaes (relirlyuishtid.+received) falt<nve t'' Qj Yee -- Ycs I No fi_ %Vrrr. sample IDs listed on fic COC? ® Yes ❑ Nv, 7. %Ycrc sample il)5 listed on all sample oonwncrs? R_ Was collection tlalr: & time listed on the COC? 19. Was collection date & Lanc listed on all sample containem') _ 110. Did tit; container label irforruation (ID, date, time) agree will the COC? Ycs (] Na ® ycsl ❑ No M Yes ❑ No ® Yes [] No I I - Wr—e tests to be pe rti mcd lisped on the COC? :2. Did ail samples arrive in the proper coatahters fur "A test and/or in grnod condi t on ® Ycs El NO (anbmkea, lids on, etc.):' W] Yes ❑ NO 13. Was adequate sample volume available? Y� ❑ No 14_'Afm rill samples reeeivcd within '/2 the holding time or 48 huurs, whichever a tires first? 15, Wm fury samples containers missac o-qs (circle one)samples Not listed on CCj(.? --� Yes 0 No ❑ Yes ❑ No 0 NA 16• For VOA and RSK-1 75 samples, wum bubbles prescm>"pca.size" ('A"ar 6mm it diameter) in tiny Df dic VOA via.s? 17. Were all DROimctalmiutrient samples received at u ptl of <2? ❑ Yesi 0 Mil 0 NA ❑ yes, ❑ No 0 NA 18. Were all c amide samples receiticd at a pl-I - 12 and sulf tde samples raceiwd a: a pl-1 >1r1 ❑ Ycs El No ® TtiA 19. Wcrc f applicable _+rKNlcyat t&-iphcnol/6?.i (<4,Smg/ samples ;t.e orreaM-W chlorine? 20. Wern client rrmarksfrequests (i.c. requested d lutions, M.S MSD designations, Q Ye! ❑ 2�0 O NA cl)rretxly transcribed from :be COC into the eo nment section itt LIMS? ❑ Yes Ww the quote nutobc- listed cui the container label? if yes, Quote # t+'A Nn, 121. Sample ['reservation (Must he completed fa- anw sumple(s) into: mly preserved or with hcadspace.) Sample(s) NA were received into rued- preserved aid wcre adjusted aucardin3ly in xample 1*ce virg with NA mL of circle one: H2SO4, HNO3, I IC'I, NaOH using 5R 9 NA _ Time of preservation NA _. If more Bran me pruscrvadve is needed, please note in the cormrenra helow, Sample(s) NA were rece;ved with bubbles =-5 mn: in diameter. Sarrples(s) NA wcre received wilt TRC > 0.5 ntg2 (if 19 is no) and ware adjusted accotd'urgty Tr sernple retxivin� with sodium th:osuWho (NaiSzOs) W[tl: 911t:aly jr)- NA R bu"xlc labels applied by: AHD Data, 09/4!1o20 Comments: Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 8 of 8 aceAnalytical Report of Analysis City of Belmont PO Box 431 Belmont, NC 28012 Attention: Tanya Setzer Project Name: Effluent Pollutant Scan Lot Number:WK09070 Date Completed:12/09/2021 12/09/2021 11:38 AM Approved and released by: Project Manager II: Edward Barnett ACAM2 ANSI NdNOnAI ACCM0010 8084 B A C C R E D I T E D TESTING LABORATORY The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC. Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 Tel:803-791-9700 Fax:803-791-9111 www.pacelabs.com Page 1 of 14 PACE ANALYTICAL SERVICES, LLC SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639 Case Narrative City of Belmont Lot Number: WK09070 This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace") Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or discussed below. Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI scope of accreditation: Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, Fecal Coliform SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 601OD, VOC SM 6200 B-2011, Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, Solid Chemical Material: TOC Walkley-Black. If you have any questions regarding this report please contact the Pace Project Manager listed on the cover page. VOCs by GCMS An LCS/LCSD was run in lieu of an MS/MSD for Analysis Batch 23265. WK09070-002 (Effluent) (Run 1) SVOCs by GCMS The Metho Blank and laboratory control sample (LCS) for analytical batch 22804 exceeded control limits for many analytes and surrogates due to heavy contamination from prep. The associated samples were re -prepared and/or re -analyzed outside holding time. Both sets of data have been reported. WK09070-001 (Effluent) (Run 1) Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 2 of 14 PACE ANALYTICAL SERVICES, LLC Sample Summary City of Belmont Lot Number: WK09070 Sample Number Sample ID Matrix Date Sampled Date Received 001 Effluent Aqueous 11/09/20210844 11/09/2021 002 Effluent Aqueous 11/09/2021 0900 11/09/2021 (2 samples) Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 3 of 14 11 I V I Lj"I I I V I I V I I j I I-1J Client: City of Belmont Laboratory ID: WK09070-001 Description: Effluent Matrix: Aqueous ate Sampled:11/09/2021 0844 Ite Received: 11 /09/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 350.1 (Ammonia - N) 350.1 1 11/20/2021 1814 DAK 23247 1 (Hardness (to) SM 2340C-2011 1 12/02/2021 0841 AAB 24308 1 (Nitrate-Nitr) 353.2 15 11/16/2021 1808 AAB 22741 1 (Phosphorus) 365.1 2 11/10/2021 1706 DMA 21986 1 (TDS) SM 2540C-2011 1 11/15/2021 1927 AMR 22557 1 351.4 (TKN) 351.2 1 11/17/2021 1639 DMA 11/17/2021 0931 22732 CAS Analytical Parameter Number Method Result Q LOO Units Run Hardness (total) SM 2340C-2011 54 10 mg/L 1 Ammonia - N (gas diffusion) 350.1 0.25 0.10 mg/L 1 Nitrate -Nitrite - N 353.2 25 0.30 mg/L 1 Phosphorus 7723-14-0 365.1 2.6 0.10 mg/L 1 TDS SM 254OC-2011 470 25 mg/L 1 TKN 351.2 ND S 0.10 mg/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCS/LCSD failure H = Out of holding time W = Reported on wet weight basis S = MSIMSD fa Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 4 of 14 Client: City of Belmont Laboratory ID: WK09070-001 Description: Effluent Matrix: Aqueous Date Sampled:11/09/2021 0844 Date Received: 11 /09/2021 Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 625.1 625.1 1 12/02/2021 1458 JCG 11/10/2021 1745 21969 2 625.1 625.1 1 12/02/2021 1522 JCG 11/23/2021 1552 23503 Parameter CAS Number Analytical Method Result Q LOQ Units Run Acenaphthene 83-32-9 625.1 ND 1.6 ug/L 1 Acenaphthylene 208-96-8 625.1 ND 1.6 ug/L 1 Anthracene 120-12-7 625.1 ND 1.6 ug/L 1 Benzidine 92-87-5 625.1 ND L 8.0 ug/L 1 Benzo(a)anthracene 56-55-3 625.1 ND 1.6 ug/L 1 Benzo(a)pyrene 50-32-8 625.1 ND 1.6 ug/L 1 Benzo(b)fluoranthene 205-99-2 625.1 ND 1.6 ug/L 1 Benzo(g,h,i)perylene 191-24-2 625.1 ND 1.6 ug/L 1 Benzo(k)fluoranthene 207-08-9 625.1 ND 1.6 ug/L 1 4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1.6 ug/L 1 Butyl benzyl phthalate 85-68-7 625.1 ND 1.6 ug/L 1 bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND L 1.6 ug/L 1 4-Chloro-3-methyl phenol 59-50-7 625.1 ND L 1.6 ug/L 1 bis(2-Chloroethoxy)methane 111-91-1 625.1 ND L 1.6 ug/L 1 bis(2-Chloroethyl)ether 111-44-4 625.1 ND L 1.6 ug/L 1 2-Chloronaphthalene 91-58-7 625.1 ND 1.6 ug/L 1 2-Chlorophenol 95-57-8 625.1 ND L 1.6 ug/L 1 4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1.6 ug/L 1 Chrysene 218-01-9 625.1 ND 1.6 ug/L 1 DihPnzo(a,h)anthracene 53-70-3 625.1 ND 1.6 ug/L 1 Dichlorobenzidine 91-94-1 625.1 ND L 8.0 ug/L 1 )ichlorophenol 120-83-2 625.1 ND L 1.6 ug/L 1 Diethylphthalate 84-66-2 625.1 ND L 1.6 ug/L 1 Dimethyl phthalate 131-11-3 625.1 ND 1.6 ug/L 1 2,4-Dimethylphenol 105-67-9 625.1 ND L 1.6 ug/L 1 Di-n-butyl phthalate 84-74-2 625.1 ND 1.6 ug/L 1 4,6-Dinitro-2- methyl phenol 534-52-1 625.1 ND 8.0 ug/L 1 2,4-Dinitrophenol 51-28-5 625.1 ND 8.0 ug/L 1 2,4-Dinitrotoluene 121-14-2 625.1 ND 3.2 ug/L 1 2,6-Dinitrotoluene 606-20-2 625.1 ND 3.2 ug/L 1 Di-n-octylphthalate 117-84-0 625.1 ND 1.6 ug/L 1 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625.1 ND 1.6 ug/L 1 bis(2-Ethylhexyl)phthalate 117-81-7 625.1 ND 8.0 ug/L 1 Fluoranthene 206-44-0 625.1 ND 1.6 ug/L 1 Fluorene 86-73-7 625.1 ND 1.6 ug/L 1 Hexachlorobenzene 118-74-1 625.1 ND L 1.6 ug/L 1 Hexachlorobutadiene 87-68-3 625.1 ND 1.6 ug/L 1 Hexachlorocyclopentadiene 77-47-4 625.1 ND 8.0 ug/L 1 Hexachloroethane 67-72-1 625.1 ND L 1.6 ug/L 1 Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1.6 ug/L 1 Isophorone 78-59-1 625.1 ND L 1.6 ug/L 1 Naphthalene 91-20-3 625.1 ND 1.6 ug/L 1 Nitrobenzene 98-95-3 625.1 ND 1.6 ug/L 1 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure Nn = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCS/LCSD failure t of holding time W = Reported on wet weight basis S = MS/MSD failure , Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 5 of 14 Client: City of Belmont Laboratory ID: WK09070-001 Description: Effluent Matrix: Aqueous Date Sampled:11/09/2021 0844 Date Received:11/09/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 1 12/02/2021 1458 JCG 11/10/2021 1745 21969 2 625.1 625.1 1 12/02/2021 1522 JCG 11/23/2021 1552 23503 CAS Analytical Parameter Number Method Result Q LOQ Units Run 2-Nitrophenol 88-75-5 625.1 ND 3.2 ug/L 1 4-Nitrophenol 100-02-7 625.1 ND L 8.0 ug/L 1 N-Nitrosodimethylamine 62-75-9 625.1 ND L 1.6 ug/L 1 N-Nitrosodi-n-propylamine 621-64-7 625.1 ND L 1.6 ug/L 1 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625.1 ND 1.6 ug/L 1 Pentachlorophenol 87-86-5 625.1 ND L 8.0 ug/L 1 Phenanthrene 85-01-8 625.1 ND 1.6 ug/L 1 Phenol 108-95-2 625.1 ND L 1.6 ug/L 1 Pyrene 129-00-0 625.1 ND 1.6 ug/L 1 1,2,4-Trichlorobenzene 120-82-1 625.1 ND L 1.6 ug/L 1 2,4,6-Trichlorophenol 88-06-2 625.1 ND 1.6 ug/L 1 Run 1 Acceptance Run 2 Acceptance Surrogate Q % Recovery Limits Q % Recovery Limits 2-Fluorobiphenyl 70 37-129 H 68 37-129 2-Fluorophenol 53 24-127 H 46 24-127 Nitrobenzene-d5 125 38-127 H 127 38-127 Phenol-d5 75 28-128 H 61 28-128 Terphenyl-d14 83 10-148 H 95 10-148 2,4,6-Tribromophenol 51 41-144 H 55 41-144 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCS/LCSD failure H = Out of holding time W = Reported on wet weight basis S = MS/MSD fa Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 6 of 14 Client: City of Belmont Laboratory ID: WK09070-001 Description: Effluent Matrix: Aqueous Date Sampled:11/09/2021 0844 Date Received: 11 /09/2021 Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 625.1 625.1 1 12/02/2021 1458 JCG 11/10/2021 1745 21969 2 625.1 625.1 1 12/02/2021 1522 JCG 11/23/2021 1552 23503 Parameter CAS Number Analytical Method Result Q LOQ Units Run Acenaphthene 83-32-9 625.1 ND H 1.6 ug/L 2 Acenaphthylene 208-96-8 625.1 ND H 1.6 ug/L 2 Anthracene 120-12-7 625.1 ND H 1.6 ug/L 2 Benzidine 92-87-5 625.1 ND H 8.0 ug/L 2 Benzo(a)anthracene 56-55-3 625.1 ND H 1.6 ug/L 2 Benzo(a)pyrene 50-32-8 625.1 ND H 1.6 ug/L 2 Benzo(b)fluoranthene 205-99-2 625.1 ND H 1.6 ug/L 2 Benzo(g,h,i)perylene 191-24-2 625.1 ND H 1.6 ug/L 2 Benzo(k)fluoranthene 207-08-9 625.1 ND H 1.6 ug/L 2 4-Bromophenyl phenyl ether 101-55-3 625.1 ND H 1.6 ug/L 2 Butyl benzyl phthalate 85-68-7 625.1 ND H 1.6 ug/L 2 bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND H 1.6 ug/L 2 4-Chloro-3-methyl phenol 59-50-7 625.1 ND H 1.6 ug/L 2 bis(2-Chloroethoxy)methane 111-91-1 625.1 ND H 1.6 ug/L 2 bis(2-Chloroethyl)ether 111-44-4 625.1 ND H 1.6 ug/L 2 2-Chloronaphthalene 91-58-7 625.1 ND HL 1.6 ug/L 2 2-Chlorophenol 95-57-8 625.1 ND H 1.6 ug/L 2 4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND H 1.6 ug/L 2 Chrysene 218-01-9 625.1 ND H 1.6 ug/L 2 DihPnzo(a,h)anthracene 53-70-3 625.1 ND H 1.6 ug/L 2 Dichlorobenzidine 91-94-1 625.1 ND H 8.0 ug/L 2 Dichlorophenol 120-83-2 625.1 ND H 1.6 ug/L 2 Diethyl phthalate 84-66-2 625.1 ND H 1.6 ug/L 2 Dimethyl phthalate 131-11-3 625.1 ND H 1.6 ug/L 2 2,4-Dimethylphenol 105-67-9 625.1 ND H 1.6 ug/L 2 Di-n-butyl phthalate 84-74-2 625.1 ND H 1.6 ug/L 2 4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND H 8.0 ug/L 2 2,4-Dinitrophenol 51-28-5 625.1 ND H 8.0 ug/L 2 2,4-Dinitrotoluene 121-14-2 625.1 ND H 3.2 ug/L 2 2,6-Dinitrotoluene 606-20-2 625.1 ND H 3.2 ug/L 2 Di-n-octylphthalate 117-84-0 625.1 ND H 1.6 ug/L 2 1,2-Diphenylhydrazine(as azobenzene) 103-33-3 625.1 ND H 1.6 ug/L 2 b is (2- Ethyl hexyl) phtha late 117-81-7 625.1 ND H 8.0 ug/L 2 Fluoranthene 206-44-0 625.1 ND H 1.6 ug/L 2 Fluorene 86-73-7 625.1 ND H 1.6 ug/L 2 Hexachlorobenzene 118-74-1 625.1 ND H 1.6 ug/L 2 Hexachlorobutadiene 87-68-3 625.1 ND H 1.6 ug/L 2 Hexachlorocyclopentadiene 77-47-4 625.1 ND H 8.0 ug/L 2 Hexachloroethane 67-72-1 625.1 ND H 1.6 ug/L 2 Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND H 1.6 ug/L 2 Isophorone 78-59-1 625.1 ND H 1.6 ug/L 2 Naphthalene 91-20-3 625.1 ND H 1.6 ug/L 2 Nitrobenzene 98-95-3 625.1 ND H 1.6 ug/L 2 LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Nn = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% t of holding time W = Reported on wet weight basis ,analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Q = Surrogate failure L = LCS/LCSD failure S = MS/MSD failure Page 7 of 14 Client: City of Belmont Laboratory ID: WK09070-001 Description: Effluent Matrix: Aqueous Date Sampled:11/09/2021 0844 Date Received: 11 /09/2021 Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 625.1 625.1 1 12/02/2021 1458 JCG 11/10/2021 1745 21969 2 625.1 625.1 1 12/02/2021 1522 JCG 11/23/2021 1552 23503 CAS Analytical Parameter Number Method Result Q LOQ Units Run 2-Nitrophenol 88-75-5 625.1 ND H 3.2 ug/L 2 4-Nitrophenol 100-02-7 625.1 ND H 8.0 ug/L 2 N-Nitrosodimethylamine 62-75-9 625.1 ND H 1.6 ug/L 2 N-Nitrosodi-n-propylamine 621-64-7 625.1 ND H 1.6 ug/L 2 N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 625.1 ND H 1.6 ug/L 2 Pentachlorophenol 87-86-5 625.1 ND H 8.0 ug/L 2 Phenanthrene 85-01-8 625.1 ND H 1.6 ug/L 2 Phenol 108-95-2 625.1 ND H 1.6 ug/L 2 Pyrene 129-00-0 625.1 ND H 1.6 ug/L 2 1,2,4-Trichlorobenzene 120-82-1 625.1 ND H 1.6 ug/L 2 2,4,6-Trichlorophenol 88-06-2 625.1 ND H 1.6 ug/L 2 Run 1 Acceptance Run 2 Acceptance Surrogate Q % Recovery Limits Q % Recovery Limits 2-Fluorobiphenyl 70 37-129 H 68 37-129 2-Fluorophenol 53 24-127 H 46 24-127 Nitrobenzene-d5 125 38-127 H 127 38-127 Phenol-d5 75 28-128 H 61 28-128 Terphenyl-d14 83 10-148 H 95 10-148 2,4,6-Tribromophenol 51 41-144 H 55 41-144 LOQ = Limit of Quantitation B = Detected in the method blank E - Quantitation of compound exceeded the calibration range Q = Surrogate failure ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40% L = LCS/LCSD fail,-- H = Out of holding time W = Reported on wet weight basis S = MS/MSD fa Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.pacelabs.com Page 8 of 14