WQ0030998_Modification_20231201

Initial Review
Reviewer nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
Permit Number (IR) * WQ0030998
Applicant/Permittee Triple S Farms and Cleaning, Inc.
Applicant/Permittee Address PO Box 709 Beulaville, NC 28518
Is the owner in BIMS? Yes ) No Is the facility in BIMS? Yes No
Owner Type
Facility Name
County
Fee Category Minor
Is this a complete application?*
Yes No
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if non -application)
Email Notifications
Organization
Triple S Farms and Cleaning Class B Residuals Program
Duplin
Does this need review by the hydrogeologist? * Yes No
Regional Office
CO Reviewer
Admin Reviewer
Fee Amount $348
Complete App Date
12/01 /2023
Below list any additional email address that need notification about a new project.
Email Address
Comments to be added to email notfication
Comments for Admin
Comments for RO

Comments for Reviewer
Comments for Applicant

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Robert T. Branch
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363129007
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0030998
Has Current Existing permit number
Applicant/Permittee *
Triple S Farms and Cleaning, Inc.
Applicant/Permittee Address*
PO Box 709 Beulaville, NC 28518
Facility Name*
Triple S Farms and Cleaning Class B Residuals Program
Please provide comments/notes on your current submittal below.
Check 4502 will be sent for November 30, 2023 Delivery.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Triple_S_Pluris_Mod_all.pdf 5.47MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 11/29/2023

APPLICATION FOR PERMIT MODIFICATION
PERMIT NO WQ0030998
TRIPLE S FARMS & CLEANING
BEULAVILLE, NORTH CAROLINA
Prepared For:
Triple S Farms & Cleaning, Inc.
PO Box 709
Beulaville, NC 28518
Prepared By:
Branch Residuals & Soils, LLC
1735 Heckle Blvd. Suite 103-291
Rock Hill, SC 29732
November 2023

BRANCHRESIDUALS & SOILS, LLC
1735 Heckle Blvd, Suite 103-291, Rock Hill, SC 29732
PHONE [phone] CELL [phone]
November 29, 2023
NCDENR -Division of Water Resources
Permitting Section — Land Application Unit
Mail Service Center 1617
Raleigh, North Carolina 27699-1617
Attention: Mr. Nathaniel Thornburg
Reference: MODIFICATION OF PERMIT NO. WQ0030998
Triple S Farms Land Application Program
Beulaville, North Carolina
BR&S Job No. 2007-71
Dear Mr. Thornburg:
Branch Residuals & Soils, LLC is under contract with Triple S Farms to provide assistance in the
preparation of a permit modification for the above referenced facility. For a complete listing of
enclosures with this request, please see the attached Table of Contents. The new facilities of North
Topsail and Webb Creek request that TCLP monitoring be maintained at once per permit cycle, the
same as it was in the Lewis Farms Permit.
Your attention in the review of this application would be greatly appreciated. Please contact me
immediately if you require additional information or have questions about the review of the permit
application. A minor permit modification fee is enclosed.
Sincerely,W
Robert T. Branch, L. S. S.
Project Manager
cc: Mr. Eric Smith -Triple S Fauns

TABLE OF CONTENTS
Section No. Title
RESIDUALS LAND APPLICATION PROGRAM — RLAP 06-16
Copy of Existing Permit
Operation and Maintenance Plan
II Residuals Source Facility Summary
III RSCA — Pluris North Topsail WWTP 06-16
IV RSCA — Pluris Webb Creek WWTP 06-16
Sections III & IV contain the following sections
Facility vicinity map
Process flow diagram and narrative
Justification for residuals production rate
Residuals sampling plan
Analytical Data (TCLP, Fecal and Nutrient and Metal)

RESIDUALS LAND APPLICATION PROGRAM - RLAP 06-16

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM
INSTRUCTIONS FOR FORM: RLAP 06-16 & SUPPORTING DOCUMENTATION
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit
General — This application is for treatment, storage, transport, and/or land application of Class B residuals (may include residuals that
are generated from a water treatment plant or other type facilities) on the proposed or currently approved land application site(s) under
15A NCAC 02T .1100.
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Land Application Program (FORM: RLAP 06-16) Application: (All Application Packages):
® Submit the completed and appropriately executed Residuals Land Application Program (FORM: RLAP 06-16) form. Please
do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
® The Applicant's Certification on Page 5 of this form shall be signed in accordance with 15A NCAC 02T .0I06(b). An alternate
person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A
NCAC 02T .0106(b).
❑ If this project is for a modification of an existing permit, submit one copy of the existing permit.
® Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to
operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units.
B. Application Fee (New and Major Modification Application Packages)
® Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental
Quality (NCDEQ).
Facility Classification
New Permit
Major (land are permitted for > 300 acres) ( $1,760
Minor (land are permitted for < 300 acres) j $1,160
Major Modification I
$528
$348
- A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage;
adds additional land application areas not previously approved for that particular program [including transferring of field(s) from
one program to another]; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not
previously permitted. There is no fee for minor modifications to a permit.
C. Cover Letter (All Application Packages)
® List all items included in the application package, as well as a brief description of the requested permitting action.
D. Environmental Assessments (Maybe Required— See 15A NCAC 1 C .0300)
❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include
information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals
treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for
the construction of the subject facilities.
INSTRUCTIONS FOR FORM: RLAP 06-16 Page 1 of 3

E. Operation and Maintenance Plan (New and Renewal Application Packages)
® For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan.
® Submit the O&M Plan in accordance with 15A NCAC 02T. 1110 and include at a minimum:
® Operational functions; describe the operation of the program to show what operations are necessary for the program to
function and by whom the functions are to be conducted.
® Maintenance schedules; may include equipment calibration, maintenance of signs, etc.
® Safety measures; may include safety training program, manuals, signs, etc.
® Spill response plan; including control, containment, remediation, emergency contact information, etc.
® Inspection plan including the following information;
® Names and titles of personnel responsible for conducting the inspections.
® Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the
selected location(s) and inspection frequency are representative of the residuals management program.
® Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event
that noncompliance is observed.
® Sampling and monitoring plan including the following information;
® Names and titles of personnel responsible for conducting the sampling and monitoring.
® Detailed description of monitoring procedures including parameters to be monitored.
® Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature,
flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The
sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for
residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per
year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most
likely to be negatively affected by cold temperatures.
THE FOLLOWING ADDITIONAL ITEMS (G to M) ARE REQUIRED FOR DEDICATED PROGRAM ONLY.
F. Program Determination
❑ Dedicated residuals land application programs are ones in which land application sites meet the criteria in 15A NCAC 02T
.110202). Specifically, a residuals land application program is designated as dedicated if any of the following are applicable:
❑ Any land application site certified for the residuals land application program that receives residuals at rates or frequencies
greater than agronomic rates.
❑ Any land application site certified for the residuals land application program that is used primarily for residuals disposal,
and agricultural crop production is of secondary importance.
❑ Any land application site certified for the residuals land application program that receives residuals through fixed irrigation
facilities or irrigation facilities fed through a fixed supply system.
❑ Please contact the Non -Discharge Permitting Unit if you need any assistance in determining whether your residuals program
falls under the dedicated program definitions.
G. Program Information
❑ Provide an explanation of why a dedicated system is required instead of a conventional non -dedicated system.
❑ Provide an explanation of the dedicated system and its operation.
H. Detailed Site Maps (All New or Modification Application Packages)
❑ Submit three (3) sets of standard size plans and two (2) sets of I V by 17" plans (electronic format is acceptable - Adobe PDF
only). For Modifications, submit plans specific to the modification(s) only.
❑ Plans must include the following minimum items:
❑ A general location map, a vicinity map and a topographic map with contours not exceeding 10 feet or 25% of the total site
relief and showing all facility related structures and fences within the land application area.
❑ The location of all wells (including usage and construction details if available), streams (ephemeral, intermittent, and
perennial), springs, lakes, ponds, and other surface drainage features within 500 feet of the land application site(s).
❑ Delineation of the review and compliance boundaries
❑ Setbacks as required by 15A NCAC 02T .1108
❑ Site property boundaries within 500 feet of all waste treatment, storage, and disposal site(s).
❑ A map showing the entire irrigation area with an overlay of the suitable irrigation area depicted by the soil scientist's
evaluation. The irrigation plans shall show each nozzle/emitter and wetted area (when applicable). Clearly label spray
irrigation zones as they will be operated.
❑ Plans must depict a completed design and not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR
CONSTRUCTION, etc.) that indicate that they are anything other than final plans. However, the plans may be labeled with
the phrase: FINAL DESIGN - NOT RELEASED FOR CONSTRUCTION
INSTRUCTIONS FOR FORM: RLAP 06-16 Page 2 of 3

I. Project Evaluation and Receiver Site Management Plan (All New Application Packages or Modifications that include new sites)
❑ Submit a project evaluation and a receiver site management plan (if applicable) with recommendations concerning cover crops
and their ability to accept the proposed application rates.
J. Hydrogeologic Report (All New Application Packages or Modifications involving increasing the total design capacity)
❑ Submit a detailed hydrogeologic evaluation in accordance with 15A NCAC 02T .1104(d)(4) and current Division Policy
available at: http://www.ncwater.org/Rules Policies and Regulations/. The document shall be signed, sealed and dated by a
qualified professional.
K. Engineering Design Documents (All New or Modification Application Packages with fixed irrigation facilities or irrigation
facilities fed through fixed supply system)
❑ Submit engineering design documents that have been signed, sealed, and dated by a NC licensed Professional Engineer and/or
Professional Land Surveyor in accordance with 15A NCAC 02T J 104(d)(2). For Modifications, submit an updated site map
specific to the modification(s) only.
❑ The design documents must include the following minimum items:
❑ Engineering plans for the facility and equipment except those previously permitted unless they are directly tied into the new
units or are critical to the understanding of the complete process;
❑ Specifications describing materials to be used, method of construction, and means for ensuring quality and integrity of the
finished product including leaking testing; and
❑ Engineering calculations including hydraulic and pollutant loading, sizing criteria, hydraulic profile, total dynamic head
curve analysis for each pump, and irrigation design.
❑ Soil mapping units shown on all disposal sites.
L. Water Balance (All New Application Packages or Modifications that include new sites utilizing fixed irrigation facilities or
irrigation facilities fed through fixed supply systems)
❑ Submit a completed and accurate water balance in accordance with 15A NCAC 02T .1104(d)(5) and current Division Policy
available at: http://www.ncwater.org/Rules Policies and Regulations/.
M. Property Ownership Documentation (All New or Modification Application Packages involving new and/or relocated treatment
or irrigation components)
❑ Property ownership documentation shall consist of one of the following:
❑ Legal documentation of ownership (i.e., GIS, deed or article of incorporation), or
❑ Written notarized intent to purchase agreement signed by both parties with a plat or survey map, or
❑ An easement running with the land specifically indicating the intended use of the property and meeting the requirements of
15A NCAC 02L .0107(fl, or
❑ A written notarized lease agreement signed by both parties, indicating the intended use of the property, as well as a plat or
survey map.
ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL
SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
WATER QUALITY PERMITTING SECTION
NON -DISCHARGE PERMITTING UNIT
By U.S. Postal Service:
1617 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1617
TELEPHONE NUMBER: [phone]
By Courier/Special Delivery:
512 N. SALISBURY STREET
RALEIGH, NORTH CAROLINA 27604
FAX NUMBER: [phone]
INSTRUCTIONS FOR FORM: RLAP 06-16 Page 3 of 3

DWR
State of North Carolina
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM
FORM: RLAP 06-16
I. APPLICANT INFORMATION:
1. Applicant's name: Triple S Farms & Cleaning, Inc.
Applicant type: ❑ Individual ® Corporation ❑ General Partnership ❑ Privately -Owned Public Utility
❑ Federal ❑ State ❑ Municipal ❑ County
Signature authority's name per 15A NCAC 02T .0106: Eric Smith Title: Owner
Applicant's mailing address: Post Office Box 709
City: Beulaville State: NC Zip: 28518-
Telephone number: [phone] Email Address: triplesfarms(a-)Yahoo.com
2. Consultant's name: Robert T. Branch License Number (for P.E.):
Affiliation: ❑ On Staff ® Retained (Firm: Branch Residuals & Soils, LLC.)
Consultant's mailing address: 1735 Heckle Blvd. Suite 103-291
City: Rock Hill State: SC Zip: 29732-
Telephone number: Q 6 510-0340 Email Address: bbranch(cr�branchrs.com
3. Agronomist's name: Robert T. Branch License Number:
Affiliation: ❑ N/A ❑ On Staff ® Retained (Firm: Branch Residuals & Soils, LLC)
Agronomist's mailing address: Same As Above
City: State: Zip: -
Telephone number: (__) = Email Address:
4. Soil Scientist's name: Robert T. Branch License Number: 1180
Affiliation: ❑ N/A ❑ On Staff ® Retained (Firm: Branch Residuals & Soils, LLC.)
Soil Scientist's mailing address: Same As Above
City: State: Zip: -
Telephone number: (___) = Email Address:
5. Fee submitted: $245.00 (See Instruction B)
II. PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ® modified, ❑ renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: W00030998
Date of most -recently issued permit: May 3, 2021
Date of most -recently certified Attachment A (if different than the permit): November 3, 2022
Date of most -recently certified Attachment B (if different than the permit): March 24, 2023
FORM: RLAP 06-16 Page 1 of 5

III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION:
1. Residuals Processing Facility's physical address: 3770 Highway 24 East
City: Beulaville State: NC Zip: 28518-
Coordinates: Latitude: 34' 55' 00" N Longitude: 770 44' 03" W
Datum: NAD 1983 UTM Level of accuracy: 1'
Method of measurement: May
2. County where residuals land application program is headquartered: Duplin
3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their
certification numbers, and their affiliations in the following table:
Designation
Name
Affiliation
Certification Number
Land Applier / Triple S
ORC
Eric Smith
23352
Farms
Back -Up ORC
Bob Branch
Branch Residuals & Soils
15676
Additional Back -Up ORCs
if applicable)
If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the
candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school
and certification test:
4. Complete the following tables regarding management of the residuals land application program:
a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals
source -generating facilities as currently certified and proposed for certification with this application and list the results in the
following table:
b.Maximum amount of residuals to be certified: 1,304 dry tons per year.
PAN
Pounds of PAN per Dry Ton
(Weighted Average)
Pounds of PAN per Year
Surface
Incorporation
or Injection
Surface
Incorporation
or Injection
First -Year
29.11
34.03
37,954.15
44,378.85
Five -Year Maximum Adjusted
41.30
44.64
53,849.83
58,209.84
c. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and
proposed for certification with this application:
Category
Use
Acres
Comments
Crops
Forest or Plantation
7.5
Row Crops
0
Hay
291.53
Pasture
0
Total:
299.03
Methods
Surface
7.5
Incorporation or Injection
291.53
Row Crop and bermudagtass can be injected
Total:
299.03
FORM: RLAP 06-16 Page 2 of 5

d. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently
certified and proposed for certification assuming the scenarios listed in the following table:
Assumed
Application Rate
(lbs PAN/ac yi)
Acres Required Using
First -Year PAN Concentrations
Acres Required Using
Five -Year Maximum Adjusted PAN
Concentrations
Surface
Incorporation or
Injection
Surface
Incorporation or
Injection
50
759.08
887.58
1,077.00
1,164.20
100
379.54
443.79
538.50
582.10
150
253.03
295.86
359.00
388.07
200
189.77
221.89
269.25
291.05
6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed
residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction
practices not in place, etc.):
7. Specify type of residuals program (See Instruction F): ® Non -dedicated ❑ Dedicated
If Dedicated, specify the following (check all that apply):
❑ Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic
rates, explain;
❑ Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop
production is of secondary importance, explain;
❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation
facilities fed through a fixed supply system, explain;
IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the following Residuals Source Certification and all associated documentation.
f17 1
Residuals Source
Certification
V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site)
Complete and submit the following Land Applications Site Certification and all associated documentation.
8n
Land Application Siite
Certification. doc
FORM: RLAP 06-16 Page 3 of 5

Note: Item VI. Applicable to Dedicated Program with fixed irrigation system only.
VI. DESIGN INFORMATION FOR FIXED IRRIGATION SYSTEM
1. The irrigation system is: ❑ Spray ❑ Drip
2. Disposal system is: ❑ existing ❑ proposed.
3. Minimum depth to mean seasonal high water table (SHWT) within irrigation sites(s) per Soil Scientist's Evaluation: feet
below ground surface. Rules 15A NCAC 02T .0505(y) requires at least one -foot vertical separation between SHWT and ground
surface.
4. Are there any artificial drainage or water movement structures within 200 feet of any irrigation area?
❑ Yes or ❑ No If Yes, please explain if the soil scientist report addresses artificial structures and please indicate if
structures are to be maintained or modified:
5. Loading rates recommended by the Soil Scientist Evaluation:
Soil Series
Fields within Soil Area
Recommended
Loading Rate
in/hr
Recommended
Loading Rate
in/ r
6. Design loading rates are equal or less than the loading rates recommended by Soil Scientist?
❑ Yes or ❑ No If No, explain why 15A NCAC 02T .0505(n) is not met:
7. Non -dedicated System Design (fill in the appropriate information for either a spray or drip irrigation system):
Field /Zone
Design Area
ft2)
Number of
Nozzles
Maximum Application
Rate allons/hr)
Design Annual Loading
Rate allons/ r)
Total
Spray Irrigation Design Element
Plan Sheet
Number
Specification
I, Page Number
Wetted diameter of nozzles
ft
Wetted area of nozzles
ft'-
Nozzle capacity
gpm
Nozzle manufacturer 1 model
1
Elevation of highest nozzle
ft
FORM: RLAP 06-16 Page 4 of 5

Applicant's Certification (signing authority must be in compliance with 15A NCAC 02T .0106):
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
® Yes ❑ No, Explain;
I, Eric Smith Owner
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for Triple S Farms & Cleaning, Inc. _
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.613, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature: n'� /CILDate: I' cm —a-3 _
FORM: RLAP 06-16 Page 5 of 5

Total PAN For All Sources
NDRLAP Section III 7a. Page 4 of 6
NDRLAP Section II17c. Pa e 5 of 6
Assumed Acres Required Using Acres Required Using
Application RateFirst-Year PAN Concentratio ve-Year Maximum Adjust P
(!bs PAN/ac y1) Concentrations
Incorporation Incorporation
Surface or Injection Surface or Injection
50 759.08 887.58 1,077.00 1,164.20
100 379.54 443.79 538.50 582.10
150 253.03 295.86 359.00 388.07
200 189.77 221.89 269.25 291.05
PAN
First -Year
PAN
First -Year
Pounds of PAN per Dry Ton
(Weighted Average)
Pounds of PAN per Year
Surface
Incorporation
or Injection
Surface
Incorporation
or Injection
29.11
34.03
37,954.15
44,378.85
Five Year Maximum Adjuste
41.30
44.64
53,849.83
58,209.84
Most Restricting PAN 53,849.83
Acreage Calculation Based On RYE
RYE Pounds PAN Per Field
Field Acres First Crop Second Crop First Crop Second Crop
l 36 299 50 10764 1800
2 12.6 276 50 3477.6 630
3A 14 276 50 3864 700
345 19.6 184 3606.4 0
6 17.3 299 50 5172.7 865
7 11.5 184 2116 0
8 7.5 60 450 0
9 16.1 299 50 4813.9 805
10 12.8 299 50 3827.2 640
15-1 4.39 276 50 1211.64 219.5
15-2 5.03 194 50 975.82 251.5
1S4 8.66 194 50 1680.04 433
15-3 7.27 132 50 959.64 363.5
LT-1 21.58 299 50 6452.42 1079
ST-1 14.05 276 1 50 3877.8 702.5
ST-2 20.3 299 50 6069.7 1015
MW-1 10.88 276 50 3002.88 544
MW-2A 5.93 299 50 1773.07 296.5
MW-213 14.46 276 50 3990.96 723
MW-3 6.91 276 50 1907.16 345.5
MW4 3.98 276 50 1098.48 199
MW-5 1.9 299 50 568.1 95
MW-6 6.21 270 50 1676.7 310.5
MW-7 5.36 299 50 1602.64 268
MW-8 4.72 299 50 1411.28 236
MW-9 10 270 50 2700 500
Totals Total PAN 79050.13 13021.5 92071.63
299.03
RYE Calculations indicate that sufficient land based on RYE.
Please Note:
Some sources are listed on more than one permit.
Some sources have never been land applied to these sites.
Some sources are listed on this permit as a backup.
Totals Total PAN 79050.13 13021.5 92071.63
299.03
RYE Calculations indicate that sufficient land based on RYE.
Please Note:
Some sources are listed on more than one permit.
Some sources have never been land applied to these sites.
Some sources are listed on this permit as a backup.

Copy of Existing Permit

ROY COOPER
Governor
DIONNE DELLI-GATTI
Secretary
S. DANIEL SMITH
Director
ERIC R. SMITH —PRESIDENT
TRIPLE S FARMS AND CLEANING, INC.
POST OFFICE BOX 709
BEULAVILLE, NORTH CAROLINA 28518
Dear Mr. Smith:
NORTH CAROLINA
Environmental Quality
May 3, 2021.
Subject: Permit No. WQ0030998
Triple S Farms and Cleaning RLAP
Land Application of
Class B Residuals
Duplin County
In accordance with your permit renewal with maior modification request received February 11,
2021, we are forwarding herewith Pennit No. WQ0030998 dated May 3, 2021, to Triple S Fanns and
Cleaning, Inc. for the continued operation of the subject residuals management program.
Modifications to the subject permit are as follows:
♦ Splitting of Field 3 into Fields 3A and 313, managed with different cover crops.
♦ The total permitted dry tonnage for the program has been increased to 939 dry tons per
(DTlyr) based on changes to the following facilities:
year
Increase of dry tonnage from the Warsaw WWTP (Permit No. N00021903) in Duplin
County from 38 to 75 DTlyr.
i0- Increase of di), tonnage from the Town of Clayton's Little Creek WRF (Permit No.
NC0025453) in Johnston County from 80 to 300 DTlyr.
i- Reduction of dry tonnage from the Beulaville WWTP (Permit No. N00026018) in Duplin
County from 38 to 30 DTIyr.
i Reduction of dry tonnage from the Kenansville WWTP (Permit No. NC0036668) in Duplin
County from 38 to 10 DTlyr.
Reduction of dry tonnage from the Murphy -Brown LLC's Rainbow Trailer Wash Facility
(Permit No. WQ0013921) in Duplin County from 40 to 25 DTlyr
i� Increase of dry tonnage from the Murphy -Brown LLC's Register Trailer Wash Facility
(Permit No. WQ0014247) in Duplin County from 50 to 63 DTlyr.
- Increase of dry tonnage from the Murphy-Broxvn LLC's Warsaw Sanitation Trailer Wash
Facility (Permit No. WQ0023310) in Duplin County from 50 to 63 DTlyr.
D
North Carolina Department. of Environmental Quality Division of Water Resources
EQ�> 512 North Salisbury Street 11bi7 Niail Service Center I R neigh, N[rrth Carolina 27699 tbli
ycrta , w '
^s^wuw\ 919.707-9000

Mr. Eric R. Smith
May 3, 2021
Page 2 of 3
This pennit shall be effective from the date of issuance through June 30, 2027, shall void Pennit
No. WQ0030998 issued March 9, 2016, and shall be subject to the conditions and limitations as specified
therein. The Permittee shall submit a renewal application no later than January 1, 2027.
Please pay particular attention to the monitoring requirements listed in Attachment A for they may
differ from the previous pennit issuance. Failure to establish an adequate system for collecting and
maintaining the required operational information shall result in future compliance problems.
Please note that on September 1, 2018, North Carolina Administrative Code Title 15A Subchapter
02T — Waste not Discharged to Surface Waters was readopted. Accordingly, this permit incorporates the
requirements of these rules, therefore, please take the time to review this permit thoroughly.
The Division has removed the following permit conditions since the last permit issuance dated
March 9, 2016:
i- Old Condition I.2. — This condition has been removed.
➢ Old Condition I.3. — This condition has been removed.
➢ Old Condition 11.8. — This condition has been removed because there are not treatment or
storage units permitted in this pennit.
➢ Old Condition III.10. — This condition has been removed because it is covered by the new
III.10.h.
➢ Old Condition III.1 I .h. — Soil pH requirements for land application have been removed.
Old Condition III.13. — This condition has been removed.
➢ Condition VI.2. — This condition has been removed because this pennit is not voidable.
The following permit conditions are new since the last permit issuance dated March 9, 2016:
Condition III.10.1. — Residual land application may not occur if the land application sites are
located within a WS-1 watershed pursuant to 15A NCAC 02B .0212 or within the Critical Area
of a WS-II, WS-III, or WS-IV watershed.
➢ Condition III.1l.c. — Dedicated land sites are to have public access restricted continuously
while the land is under pennit and for one year afterward. Note, there are no dedicated land
sites in the current pennit.
➢ Condition VIX — This permit shall not be renewed if the Permittee or any affiliation has not
paid the required annual fee

Mr. Eric R. Smith
May 3, 2021
Page 3 of 3
If any parts, requirements or limitations contained in this permit are unacceptable, the Permittee
has the right to request an adjudicatory hearing upon written request within 30 days following receipt of
this permit. This request shall be in the fonn of a written petition, conforming to Chapter 150B of the North
Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service
Center, Raleigh, NC 27699-6714. Otherwise, this permit shall be final and binding.
If you need additional information concerning this permit, please contact Erick Saunders at (919)
707-3659 or erickson.saunders(i)ncdenr.gov.
Sincerely,
-tS. Daniel Smith, Director
Division of Water Resources
,1
cc: Duplin County Health Department (Electronic Copy)
Jones County Health Department (Electronic Copy)
Onslow County Health Department (Electronic Copy)
Wilmington Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Bob Branch, LSS — Branch Residuals & Soils, LLC (Electronic Copy)
Beth Buffington — Protection and Enforcement Branch (Electronic Copy)
Laserfiche File (Electronic Copy)
Digital Permit Archive (Electronic Copy)

THIS PAGE BLANK

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENTAL QUALITY
RALEIGH
LAND APPLICATION OF CLASS B RESIDUALS PERMIT
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
Triple S Farms and Cleaning, Inc.
Duplin County
FOR THE
continued operation of a residuals management program for Triple S Farms and Cleaning, Inc. and
consisting of the land application of Class B residuals generated by the approved facilities listed in
Attachment A to the approved fields listed in Attachment B, with no discharge of wastes to surface waters,
pursuant to the application received February 11, 2021, and in conformity with other supporting data
subsequently filed and approved by the Department of Environmental Quality and considered a part of this
permit. The disposal of residuals is regulated under Title 40 Code of Federal Regulations Part 503. This
permit does not exempt the Pennittee from complying with Federal Regulation 40 CFR Part 503.
This permit shall be effective from the date of issuance through June 30, 2027, shall void Permit No.
WQ0030998 issued March 9, 2016, and shall be subject to the following conditions and limitations:
SCHEDULES
1. The Pennittee shall request renewal of this permit on Division -approved forms no later than January 1,
2027. [15A NCAC 02T .0105(b), 02T .0109]
II. PERFORMANCE STANDARDS
The Pennittee shall maintain and operate the subject residuals management program so there is no
discharge to surface waters, nor any contravention of groundwater or surface water standards. In the
event the residuals management program fails to perform satisfactorily, including the creation of
nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease
land applying residuals, take immediate corrective actions, and contact the Wilmington Regional Office
supervisor. [15A NCAC 02T.0108(b)(1)(A)]
2. This permit shall not relieve the Permittee of their responsibility for damages to groundwater or surface
water resulting from the operation of this residuals management program. [15A NCAC 02T
.0108(b)(1)(A)]
3. Only residuals generated by the facilities listed in Attachment A are approved for land application in
accordance with this permit. [15A NCAC 02T .1101]
WQ0030998 Version 3.0 Shell Version 200201 Page I of 12

4. Only the fields listed in Attachment B are approved for residuals land application. [G.S. 143-
215.1(a)(9)]
5. Pollutant concentrations in residuals land applied to the sites listed in Attachment B shall not exceed
the following Ceiling Concentrations or Cumulative Pollutant Loading Rates (CPLRs), on a dry
weight basis:
Parameter
Ceiling
Concentration
Cumulative Pollutant Loading Rates
(mg/kg)
(kg//7a)
(lhs/ac)
Arsenic
75
41
36
Cadmium
85
39
34
Copper
4,300
11500
1,338
Lead
840
300
267
Mercury
57
17
15
Molybdenum
75
N/A
N/A
Nickel
420
420
374
Selenium
100
100
89
Zinc
7,500
2,800
2,498
The Permittee shall determine compliance with the CPLRs using one of the following methods:
a. By calculating the existing cumulative level of pollutants using actual analytical data from all
historical land application events of residuals, or
b. For land where residuals application has not occurred or for which the required data is incomplete,
by determining background concentrations through representative soil sampling.
[15A NCAC 02T. I 105(a), 02T. I 105(b)]
6. Class B biological residuals shall meet the pathogen reduction requirements in 15A NCAC 02T .1106
(b). Exemptions to this requirement shall be specified in Attachment A. [15A NCAC 02T .1106(b),
02T .1106(d)]
7. Class B biological residuals shall meet one of the vector attraction reduction alternatives in 15A NCAC
02T .1107(a). Exemptions to this requirement shall be specified in Attachment A. [15A NCAC 02T
.1107(a), 02T 1107(c)]
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8. The facilities and sites herein were permitted per the following setbacks:
a. Setbacks for Class B land application sites are as follows (all distances in feet):
Surface
Irrigation
Injection /
Application
Surface
Incorporation
by Vehicle
Application
i. Each habitable residence or place of assembly
400
400
200
under separate ownership:
ii. Each habitable residence or places of assembly
owned by the Permittee, the owner of the land,
0
200
0
or the lessee or operator of the land:
iii. Each property line:
50
150'
50'
iv. Public right of way:
50
50
50
v. Each private or public water supply source:
100
100
100
vi. Surface waters such as intermittent and
perennial streams, perennial waterbodies, and
32.8
32.8
32.8
wetlands:
vii. Surface water diversions such as ephemeral
25
25
25
streams, waterways, and ditches:
viii.Groundwater lowering ditches where the
25
100
25
bottom of the ditch intersects the SHWT:
ix. Subsurface groundwater lowering systems:
0
100
0
x. Each well with exception of monitoring wells:
100
100
100
xi. Bedrock outcrops:
25
25
25
xii. Top of slope of embankments or cuts of two
15
15
15
feet or more in vertical height:
xiii.Each building foundation or basement:
0
•15
0
xiv. Each water line:
0
10
0
xv. Nitrification field:
0
20
0
' Setbacks to property lines are not applicable when the Permittee,
or the entity from which the
Permittee is leasing, owns both parcels separated by the property line.
[15A NCAC 02T .1108(c)]
9. Class B land application areas shall be clearly marked on each site prior to and during any residuals
application event. [ 15A NCAC 02T .0110(g)]
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10. Residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance of
agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen requirements
based on the determined Realistic Yield Expectations (RYE) using any of the following methods:
a. Division's pre -approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State
University Department of Soil Science (http://nutrients.soil.ncsu.edu/vields/index.php). A copy
shall be kept on file and reprinted every five years in accordance with Condition IV.6.
c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE
and appropriate nutrient application rates reported in any of the following documents:
Crop management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services, the Natural Resource
Conservation Service, or other agronomist.
ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance
Document: Chapter 1
(http://www.nca,izr.,izov/SWC/tech/documents/9th Guidance Doc 100109.pdf).
iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (MRCS). These plans must meet the USDA-NRCS 590 Nutrient Management
Standards(ftp://ftp-fc.sc.egov.usda.aov/NHO/practice-standards/standards/590.pdfl.
d. If the RYE and appropriate nutrient application rates cannot be determined, the Penmittee shall
contact the Division to detenmine necessary action.
[15A NCAC 02T .1109(a)(1)(K)]
11. When residuals are land applied to grazed pasture, hay crop realistic nitrogen rate shall be reduced by
25%. [15A NCAC 02T.0108(b)(1)(A)]
12. If residuals land application sites are to be over -seeded or double -cropped (e.g., bermuda grass in the
summer and rye grass in the winter with both crops to receive residuals), then the second crop can
receive an application of PAN at a rate not to exceed 50 pounds per acre per year (lbs/ac/yr). This
practice may be allowed as long as the second crop is to be harvested or grazed. If the second crop is
to be planted for erosion control only and is to be tilled into the soil, then no additional PAN shall be
applied. [15A NCAC 02T .0108(b)(1)(A)]
13. Prior to land application of residuals containing a sodium adsorption ratio (SAR) of 10 or higher, the
Penmittee shall obtain and implement recommendations from at least one of the following: the local
Cooperative Extension Office; the Department of Agriculture and Consumer Services; the Natural
Resource Conservation Service; a North Carolina Licensed Soil Scientist; or an agronomist. The
recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a
mechanism for maintaining site integrity and conditions conducive to crop growth. The Pennittee shall
maintain written records of these recommendations and details of their implementation. [15A NCAC
02T .0108(b)(1)(A)]
14. Residuals land application fields permitted on or after December 30, 1983 have a compliance boundary
that is either 250 feet from the residual land application area, or 50 feet within the property boundary,
whichever is closest to the residual land application area. Any exceedance of groundwater standards
at or beyond the compliance boundary shall require corrective action. Division -approved relocation of
the compliance boundary shall be noted in Attachment B. Multiple contiguous properties under
common ownership and permitted for use as a disposal system shall be treated as a single property with
regard to determination of a compliance boundary. [15A NCAC 02L .0106(d)(2), 02L .0107(b), 02T
.0105(h), G.S. 143-215.1(i), G.S. 143-215.1(k)]
WQ0030998 Version 3.0 Shell Version 200201 Page 4 of 12

15. The review boundary is midway between the compliance boundary and the residual land application
area. Any exceedance of groundwater standards at or beyond the review boundary shall require
preventative action. [15A NCAC 02L .0106(d)(1), 02L .0108]
III. OPERATION AND MAINTENANCE REOUIREMENTS
1. The Pennittee shall operate and maintain the residuals management program as a non -discharge system.
[15A NCAC 02T .1100]
2. The Pennittee shall notify the Wilmington Regional Office, telephone number [phone], and the
appropriate local government official (i.e., county manager, city manager, or health director) at least
two business days in advance of a site's initial residuals land application event. [15A NCAC 02T
.0108(b)(1)(A)]
3. The Pennittee shall notify the Wilmington Regional Office, telephone number [phone], at least
one business day in advance of conducting any land application activity. Notification shall include the
anticipated application date, time, and field name as listed in Attachment B. Exceptions to this
requirement shall be approved by the Wilmington Regional Office. [15A NCAC 02T .0108(b)(1)(A)]
4. The Permittee shall maintain a Division -approved Operation and Maintenance Plan that shall include:
a. Description of the program, and associated facilities and equipment, in sufficient detail to show
what operations are necessary for the program to function and by whom the functions are to be
conducted;
b. Description of anticipated maintenance of facilities and equipment associated with the program;
c. Include provisions for safety measures, including restriction of access to sites and equipment;
d. Spill control provisions:
i. Response to upsets and bypasses including control, containment, and remediation; and
ii. Contact information for plant personnel, emergency responders, and regulatory agencies;
e. Detailed inspection procedures:
i. Names or titles of personnel responsible for conducting inspections;
ii. Frequency and location of inspections, and procedures to assure that the selected locations and
inspection frequency are representative of the residuals management program; and
iii. Description of record keeping and actions to be taken by the inspector in the event that
noncompliance is observed;
f. Detailed sampling and monitoring procedures:
i. Names or titles of personnel responsible for conducting sampling and monitoring;
ii. Description of monitoring procedures including parameters to be monitored; and
iii. Sampling frequency and procedures to assure that representative samples are collected.
Fluctuation in temperature, flow, and other operating conditions can affect the quality of the
residuals gathered during a particular sampling event. The sampling plan shall account for any
foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to
meet pathogen and vector attraction reduction requirements.
[ 15A NCAC 02T . I I I0(a)]
5. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC)
classification of the residuals management program, the Permittee shall designate and employ a
certified operator in responsible charge (ORC), and one or more certified operators as back-up ORCs.
The ORC or their back-up shall visit the facilities in accordance with 15A NCAC 08G 0204 and shall
comply with all other requirement in 15A NCAC 08G 0204. [15A NCAC 02T .0117, 08G .0204]
WQ0030998 Version 3.0 Shell Version 200201 Page 5 of 12

6. The Permittee shall ensure that a copy of this permit and the Division -approved Operation and
Maintenance Plan is available when land applying residuals. [15A NCAC 02T .1110(b)]
7. The Permittee shall ensure that spill control provisions are available when transporting or land applying
residuals. [15A NCAC 02T .1110(a)(4)]
8. Class B residuals shall not be stored or staged at any land application site without prior written approval
from the Division. Class B residuals approved for storage shall be stored or staged in a manner to
prevent ninoff of leachate and other wastewaters generated. [15A NCAC 02T .1110(c), 02T .1110(e)]
9. Adequate measures shall be taken to prevent wind erosion and runoff from the land application sites
listed in Attachment B. [15A NCAC 02T .0108(b)(1)(A)]
10. Class B residuals shall not be land applied under the following conditions:
a. If the residuals are likely to adversely affect a threatened or endangered species listed tinder section
4 of the Endangered Species Act or its designated critical habitat;
b. If the application causes nuisance conditions;
c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface
water or groundwater standards;
d. If the land is flooded, frozen, or snow-covered, or is otherwise in a condition such that runoff of
the residuals would occur;
e. Within the 100-year flood elevation, unless the residuals are injected or incorporated within a 24-
hour period following a residuals land application event;
f During precipitation events, or within 24 hours following a rainfall event of 0.5 inches or greater
in a 24-hour period;
g. If the slope of the land is greater than 10% when liquid residuals are surface applied, or if the slope
of the land is greater than 18% when liquid residuals are injected or incorporated;
h. If the land does not have an established vegetative cover crop unless the land is a Division -approved
no -till site, or the residuals are injected, or incorporated within a 24-hour period following the
application of residuals;
i. If the vertical separation of the seasonal high water table and the depth of residuals application is
less than one foot;
j. If the vertical separation of the depth to bedrock and the depth of residuals application is less than
one foot;
k. if the application exceeds agronomic rates; or
1. If the land application sites are located within a WS-I watershed pursuant to 15A NCAC 02B .0212
or within the Critical Area of a WS-II pursuant to Sub -Item (4)(g) of Rule 15A NCAC 02B .0212,
or within the Critical Area of a WS-I1I or WS-IV watershed pursuant to Sub -Item (4)(h) of Rules
15A NCAC 02B .0215, and .0216.
[15A NCAC 02T .I 109(a)(1)]
11. Class B land application sites shall have the following public access restrictions:
a. Public access to public contact sites shall be restricted for one calendar year after a residuals land
application event,
b. Public access to non-public contact sites shall be restricted for 30 days after a residuals land
application event;
c. Public access to land associated with a dedicated land application site shall be restricted
continuously while the land is permitted for active use, and for one calendar year after the final
land application of residuals.
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[15A NCAC 02T .1109(a)(2)]
12. Class B land application sites shall have the following harvesting and grazing restrictions:
a. Animals shall not be allowed to graze on land for 30 calendar days after any land application of
residuals;
b. Food crops, feed crops, and fiber crops shall not be harvested for 30 calendar days after any land
application of residuals;
c. Food crops with harvested parts that touch the mixture of residuals and soil and are totally above
the land surface shall not be harvested for 14 months after any land application of residuals;
d. Food crops with harvested parts below the land surface shall not be harvested for 20 months after
any land application of residuals if the residuals remain on the land surface for four months or
longer prior to incorporation into the soil;
e. Food crops with harvested parts below the land surface shall not be harvested for 38 months after
any land application of residuals if the residuals remain on the land surface for less than four months
prior to incorporation into the soil; and
f. Turf grown on land where residuals are applied shall not be harvested for one calendar year after
any land application of residuals.
[15A NCAC 02T .1109(a)(3)]
13. The Pennittee shall acquire from each landowner or lessee/operator a statement detailing the volume
of other nutrient sources (i.e., manufactured fertilizers, manures, or other animal waste products) that
have been applied to the site, and a copy of the most recent Nutrient Management Plan (NMP) for those
operations where a NMP is required by the US Department of Agriculture — National Resources
Conservation Service (NRCS) or other State Agencies. The Pennittee shall calculate allowable nutrient
loading rates based on the provided information and use appropriate reductions.
For the purpose of this permit condition, a Crop Management Plan (CMP), Waste Utilization Plan
(WUP) or Certified Nutrient Management Plan (CNMP) shall also be considered a Nutrient
Management Plan. [15A NCAC 02T .0108(b)(1)(A), 02T .1104(c)(3)]
14. Class B residuals shall not be land applied to the fields listed in Attachment B unless the Landowner
Agreement between the Pennittee and the respective field owners or lessees/operators of the land
application site is valid. The Landowner Agreements shall expire concurrent with the permit expiration
date of June 30, 2027. [15A NCAC 02T .1104(c)(4)]
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IV. MONITORING AND REPORTING REOUIREMENTS
The Pennittee shall conduct and report any Division required monitoring necessary to evaluate this
program's impact on groundwater and surface water. [ 15A NCAC 02T .0108(c)]
The residuals from each source generating facility shall be analyzed to demonstrate they are non-
hazardous under the Resource Conservation and Recovery Act (RCRA). Residuals that test or are
classified as a hazardous or toxic waste under 40 CFR Part 261 shall not be land applied. The analyses
(i.e., corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)) shall be
performed at the frequency specified in Attachment A, and the Permittee shall maintain these results
for five years. Any exemptions from the requirements in this condition shall be specified in Attachment
A. The TCLP analysis shall include the following parameters, and the Federal regulatory level (mg/L)
is in parentheses:
Arsenic (5.0)
1,4-Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroethane (0.5)
Pentachlorophenol (100.0)
Benzene (0.5)
1,1-Dichloroethylene (0.7)
Pyridine (5.0)
Cadmium (1.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5)
Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Heptachlor (and its epoxide)
(0.008)
Tetrachloroethylene (0.7)
Chlorobenzene (100.0)
Hexachlorobenzene (0.13)
Toxaphene (0.5)
Chloroform (6.0)
Hexachlorobutadiene (0.5)
Trichloroethylene (0.5)
Chromium (5.0)
Hexachloroethane (3.0)
2,4,5-Trichlorophenol (400.0)
m-Cresol (200.0)
Lead (5.0)
2,4,6-Trichlorophenol (2.0)
o-Cresol (200.0)
Lindane (0.4)
2,4,5-TP (Silvex) (1.0)
p-Cresol (200.0)
Mercury (0.2)
Vinyl chloride (0.2)
Cresol (200.0)
Methoxychlor (10.0)
2,4-D (10.0)
Methyl ethyl ketone (200.0)
[15A NCAC 13A .0102(b), 02T .1101, 02T .1105]
The residuals from each source generating facility shall be analyzed at the frequency specified in
Attachment A, and the Permittee shall maintain the results for a minimum of five years. Each analysis
shall include the following parameters:
Aluminum
Mercury
Potassiwn
Ammonia -Nitrogen
Molybdenum
Selenium
Arsenic
Nickel
Sodium
Cadmium
Nitrate -Nitrite Nitrogen
Sodium Adsorption Ratio
(SAR)
Calcium
Percent Total Solids
TKN
Copper
pH
Zinc
Lead
Phosphorus
Magnesium
Plant Available Nitrogen
(by calculation)
[15A NCAC 02T .1101 ]
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4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction
requirements at the frequency specified in Attachment A. The monitoring results shall specify the
stabilization process utilized, and demonstrate compliance with the Class B pathogen reduction
requirements in 15A NCAC 02T .1106(b), and one vector attraction reduction requirement in 15A
NCAC 02T .1107(a) shall be met. Any exemptions from the requirements in this condition shall be
specified in Attachment A. [15A NCAC 02T .1106(b), 02T .l 107(a), 02T .1111(c)]
An annual representative soils analysis (i.e., Standard Soil Fertility Analysis) shall be conducted on
each land application site listed in Attachment B that received residuals during the calendar year. This
analysis shall be in accordance with the soil sampling guidance located in the Sampling Instructions
section of the NC Department of Agriculture & Consumer Services' website
(http://www.ncagr.gov/,igronomi/pubs.litiii . The Permittee shall maintain these results for a period of
no less than five years, and these results shall be made available to the Division upon request. Each
Standard Soil Fertility Analysis shall include the following parameters:
Acidity
Exchangeable Sodium Percentage
Phosphors
Base Saturation (by calculation)
Magnesium
Potassium
Calcium
Manganese
Sodium
Cation Exchange Capacity
Percent Humic Matter
Zinc
Copper
pH
[ 15A NCAC 02T .0108(c), 15A NCAC 02T. I l l l (d)]
Representative samples of residuals that are prepared for land application shall be collected and
analyzed. [15A NCAC 02T .l 111(a)]
The Permittee shall maintain records for all residual land application events. These records shall
include the following:
a. Residuals source (as listed in Attachment A);
b. Date of application;
c. Location of land application (field name as listed in Attachment B);
d. Approximate acreage applied;
e. Method of application;
f. Weather conditions;
g. Dominant soil series;
h. Soil conditions;
i. Proposed crop;
j. Nitrogen Application Rate based on RYEs;
k. Volume of residuals applied per acre in gallons, cubic yards, dry tons, or wet tons;
1. Volume of animal waste or other nutrient source applied per acre in gallons, cubic yards, dry tons,
or wet tons;
in. Volume of soil amendments applied per acre in gallons, cubic yards, dry tons, or wet tons; and
n. Annual and cumulative totals applied to each field for the following:
i. Class A and Class B residuals (dry tons per acre);
ii. Animal waste and other sources of nutrients (dry tons per acre);
iii. Heavy metals as specified in Condition I1.5. (pounds per acre);
iv. Plant available nitrogen (pounds per acre); and
v. Phosphors (pounds per acre).
[15A NCAC 02T .0108(c)]
WQ0030998 Version 3.0 Shell Version 200201 Page 9 of 12

8. One hard copy and one electronic copy of an annual report shall be submitted on or before March I".
The annual report shall meet the requirements described in the Instructions for Residuals Application
Annual Reporting Forms. Instructions for reporting and annual report forms are available at
h ttp://d eq.nc. gov/abo ut/di vi sions/xvater-resources/water-resources-penm its/wastewater-branch/non-
discharae-penmittinQ-unit/reporting-fonns, or can be obtained by contacting the Non -Discharge Branch
directly. The annual report shall be submitted to the following address:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[15A NCAC 02T .I 111(d)]
9. Noncompliance Notification
The Permittee shall report to the Wilmington Regional Office, telephone number [phone],
within 24 hours of first knowledge of the:
a. Any process unit failure (e.g., mechanical, electrical, etc.) rendering the facility incapable of
adequate residual treatment.
b. Any failure resulting in a discharge to surface waters.
c. Any time self -monitoring indicates the program has gone out of compliance with its permit
limitations.
d. Land application of residuals abnormal in quantity or characteristic.
e. Any discharge from a vehicle or piping system transporting residuals.
Emergencies requiring reporting outside normal business hours shall call the Division's Emergency
Response personnel at telephone number [phone], [phone], or [phone]. All
noncompliance notifications shall file a written report to the Wilmington Regional Office within five
days of first knowledge of the occurrence, and this report shall outline the actions proposed or taken to
ensure the problem does not recur. [15A NCAC 02T .0108(b)(1)(A)]
V. INSPECTIONS
1. The Pennittee shall perform inspections and maintenance to ensure proper operation of the Permittee's
storage, distribution, and application facilities. [15A NCAC 02T .1110(f)]
2. The Pennittee shall inspect the Permittee's residuals processing, storage, transport, and application
facilities to prevent malfimctions, facility deterioration, and operator errors that may result in discharges
of wastes to the environment, threats to human health, or public nuisances. The Permittee shall maintain
an inspection log that includes the date and time of inspection, observations made, and maintenance,
repairs, or corrective actions taken. The Permittee shall maintain this inspection log for a period of five
years from the date of inspection, and this log shall be made available to the Division upon request.
[ 15A NCAC 02T .0108(b)(1)(A), 02T . I I I0(f)]
Division authorized representatives may, upon presentation of credentials, enter and inspect any
property, premises, or place related to the land application sites or facilities permitted herein at any
reasonable time for determining compliance with this permit. Division authorized representatives may
inspect or copy records maintained under the terms and conditions of this permit, and may collect
groundwater, surface water, or leachate samples. [G.S. 143-215.3(a)(2)]
WQ0030998 Version 3.0 Shell Version 200201 Page 10 of 12

VI. GENERAL CONDITIONS
1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to a
Division enforcement action. [G.S. 143-215.6A, 143-215.6B, 143-215.6C]
2. This permit is effective only with respect to the nature and volume of wastes described in the permit
application, and Division -approved plans and specifications. [G.S. 143-215.1(d)]
3. Unless specifically requested and approved in this permit, there are no variances to administrative codes
or general statutes governing the construction or operation of the facilities permitted herein. [15A
NCAC 02T .0105(n)]
4. The issuance of this permit does not exempt the Penmittee from complying with all statutes, rules,
regulations, or ordinances that other jurisdictional government agencies (e.g., local, state, and federal)
may require. [15A NCAC 02T .0105(c)(6)]
5. If the permitted residuals program change ownership, or the Permittee changes their name, the
Permittee shall submit a permit modification request on Division -approved forms. The Permittee shall
comply with all terns and conditions of this permit until the permit is transferred to the successor -
owner. [G.S. 143-215.1(d3)]
6. This pen -nit is subject to revocation or modification upon 60-day notice from the Division Director, in
whole or part for:
a. violation of any terms or conditions of this permit or Administrative Code Title 15A Subchapter
02T;
b. obtaining a permit by misrepresentation or failure to disclose all relevant facts;
c. the Permittee's refusal to allow authorized Department employees upon presentation of credentials:
i. to enter the Permittee's premises where a system is located or where any records are required
to be kept;
ii. to have access to any permit required documents and records;
iii. to inspect any monitoring equipment or method as required in this permit; or
iv. to sample any pollutants;
d. the Permittee's failure to pay the annual fee for administering and compliance monitoring; or
e. a Division detennination that the conditions of this permit are in conflict with North Carolina
Administrative Code or General Statutes.
[I 5A NCAC 02T .0110]
WQ0030998 Version 3.0 Shell Version 200201 Page 11 of 12

7. Unless the Division Director grants a variance, expansion of the facilities permitted herein shall not
occur if any of the following apply:
a. The Pennittee or any parent, subsidiary, or other affiliate of the Permittee has been convicted of
environmental crimes under G.S. 143-215.6B, or under Federal law that would otherwise be
prosecuted under G.S. 143-215.6B, and all appeals of this conviction have been abandoned or
exhausted.
b. The Permittee or any parent, subsidiary, or other affiliate of the Pennittee has previously abandoned
a wastewater treatment facility without properly closing the facility.
c. The Pennittee or any parent, subsidiary, or other affiliate of the Pennittee has not paid a civil
penalty, and all appeals of this penalty have been abandoned or exhausted.
d. The Pennittee or any parent, subsidiary, or other affiliate of the Pennittee is currently not compliant
with any compliance schedule in a permit, settlement agreement, or order.
e. The Pennittee or any parent, subsidiary, or other affiliate of the Pennittee has not paid an annual
fee.
[15A NCAC 02T .0120(b), 02T .0120(d)]
8. This permit shall not be renewed if the Pennittee or any affiliation has not paid the required annual fee.
[15A NCAC 02T .0120(c)]
Pen -nit issued this the 3`d day of May 2021
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
S. Daniel Smith, Director
Division of Water Resources
By Authority of the Environmental Management Commission
Permit Number WQ0030998
WQ0030998 Version 3.0 Shell Version 200201 Page 12 of 12

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Operation and Maintenance Plan

Operation & Maintenance Plan
Pluris North Topsail WWTP
The WWTP ORC (or Backup ORC if ORC is unavailable) shall be in charge of the following
items as it relates to the current land application program:
• Collection of WWTP Samples
o TCLP Samples
o Pathogen reduction samples
o Vector attraction reduction samples
o Nutrient and Metals analyses
o Lime Stabilization (if applicable) — collecting pH measurements:
■ Initial pH
■ Raising the pH to 12
■ Monitoring the pH to see that it stays at 12 for 2 hours, and
■ Making sure it doesn't drop below 11.5 for the next 22 hours.
As Preparer for this facility under 40 CFR Part 503
o Being the individual that is familiar with the routine operation of this facility with
includes:
■ Insuring solids are ready for land application
■ Insuring solids have undergone proper treatment
■ Proper operation of treatment units
■ Proper operation of sludge holding units
■ Proper maintenance of treatment and storage units
■ Notification of state and land appliers of abnormal conditions
The Land Applier shall be in charge of:
• Buffering Land Application Fields
• Spreading Materials at Rates Given for Field, Crop & Soil.
• Calibrating Spreader
• Inspections and Inspection log
• Record keeping regarding disbursement & location of material spread.
• Spill Response
• Signage
Both the WWTP ORC and Land Appliers will complete the aforementioned responsibilities before
the commencement of each land applying event. In the event that an area of noncompliance is
observed, the NCDEQ office will be contacted as well as Bob Branch. Inspections should be
performed in the field at the beginning of every land application event, with every change in
loading rate, and post application event for run off. An additional inspection will be performed if
rain occurs after the application event and before the residuals have had time to desiccate (typically
3 - 5 days). Each field will be inspected pre and post with each application event. The frequency
of inspections will depend on the frequency of application events.
Please see form RSC for a copy of the Sampling and Monitoring Plan.

Pluris Webb Creek WWTP
The WWTP ORC (or Backup ORC if ORC is unavailable) shall be in charge of the following
items as it relates to the current land application program:
• Collection of WWTP Samples
o TCLP Samples
o Pathogen reduction samples
o Vector attraction reduction samples
o Nutrient and Metals analyses
o Lime Stabilization (if applicable) — collecting pH measurements:
■ Initial pH
■ Raising the pH to 12
■ Monitoring the pH to see that it stays at 12 for 2 hours, and
■ Making sure it doesn't drop below 11.5 for the next 22 hours.
As Preparer for this facility under 40 CFR Part 503
o Being the individual that is familiar with the routine operation of this facility with
includes:
■ Insuring solids are ready for land application
■ Insuring solids have undergone proper treatment
■ Proper operation of treatment units
■ Proper operation of sludge holding units
■ Proper maintenance of treatment and storage units
■ Notification of state and land appliers of abnormal conditions
The Land Applier shall be in charge of:
• Buffering Land Application Fields
• Spreading Materials at Rates Given for Field, Crop & Soil.
• Calibrating Spreader
• Inspections and Inspection log
• Record keeping regarding disbursement & location of material spread.
• Spill Response
• Signage
Both the WWTP ORC and Land Appliers will complete the aforementioned responsibilities before
the commencement of each land applying event. In the event that an area of noncompliance is
observed, the NCDEQ office will be contacted as well as Bob Branch. Inspections should be
performed in the field at the beginning of every land application event, with every change in
loading rate, and post application event for run off. An additional inspection will be performed if
rain occurs after the application event and before the residuals have had time to desiccate (typically
3 - 5 days). Each field will be inspected pre and post with each application event. The frequency
of inspections will depend on the frequency of application events.
Please see form RSC for a copy of the Sampling and Monitoring Plan.
2

Operation and Maintenance Plan
Duplin County
Title
Name
Office Phone
Cell Phone
WWTP ORC
As noted in RSCA
As noted in RSCA
WTPORC Back
As noted in RSCA
As noted in RSCA
Land Applier
Eric Smith
910.298-3991
910.934-7670
Backup Applierl
Bob Branch
1 336.510-0340
1 336.312-9007
Last Date Modified Name Si
29-Nov-23 Robert T. Branch '

RESIDUALS SOURCE FACILITY SUMMARY

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RSCA - PLURIS NORTH TOPSAIL WWTP 06-16

State of North Carolina
awR Department of Environment and Natural Resources
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 08-13
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and
supporting documentation
For more information or for an electronic version of this form, visit the Land Application Unit (LAU) web site at:
http: //portal. ncdenr. orQ/iveb/wq/apsllati
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 08-13, FORM: DCAR 08-13, or FORM: SDR 08-13).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 08-13):
® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 08-13) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
❑ For new or renewed permits, submit a separate certification for each source facility.
® For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
® Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Residuals Source -Generating Facility Information:
® For each source facility, attach the following:
® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for
Residuals Land Application Permits'.
® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated, treated, processed, and stored at the facility.
® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item 1. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the
permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or
disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing.
® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure
that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector
attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to
be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
® For each source facility, attach the following:
® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach
analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities.
INSTRUCTIONS FOR FORM: RSC 08-13 Page 1 of 1

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State of North Carolina
1 Department of Environment and Natural Resources r)WRDivision of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 08-13
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Pluris North Topsail WWTP
2. Facility permit holder is: ❑ Federal, ❑ State, ❑ Local Government, or ® Private.
Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health,
or ❑ Other (explain: ).
3. Facility contact person and title: Dwight Peterson, ORC
Complete mailing address: 1095 Hwy 210
City: Sneads Ferry State: NC Zip: 28460-
Telephone number: [phone] E-mail address: dpetersonRplurisusa.com
4. Facility physical address: 1095 Hwy 210
City: Sneads Ferry State: NC Zip: 28460-
Coordinates: Latitude: 34' 32' 5.33" Longitude: 77' 25' 33.85"
Datum: NAD83 Level of accuracy: Hundredths of Second
Method of measurement: MAP
5. Purpose of the facility:
❑ treatment of municipal wastewater, ® treatment of 100% domestic wastewater,
❑ treatment of potable water, ❑ treatment of 100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: . % industrial and % domestic)
❑ other (explain: ).
6. Does the facility have an approved pretreatment program: ❑ Yes ® No
7. Facility permitted/design flow: 1.542 MGD and facility average daily flow: 0.440 MGD
8. Average amount of residuals being generated at this facility 70 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 1,000,000 GPD through MBR
Type and volume of residuals storage (i.e., outside of residuals treatment units): N/A
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
® 40 CFR Part 503 or ❑ 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
® Biological ❑ Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 08-13 Page 1 of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ❑ no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: ❑ yes ❑ no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well
as those for corrosivity, ignitability, and reactivity:
Laboratory: Environmental Chemists Inc. and Date of analysis: 11/28/23
Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes ❑ no. Flashpoint: >158 IF (> 140°F)
Passed reactivity test: ® yes ❑no. HCN: 4.25 mg/kg (<250) & H2S: 62.9 mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
Arsenic
5.0
<1.0
Hexachlorobenzene
0.13
<0.05
Barium
100.0
<1.0
Hexachloro-1,3-Butadiene
0.5
<0.05
Benzene
0.5
<0.01
Hexachloroethane
3.0
<0.05
Cadmium
1.0
<1.0
Lead
5.0
<1.0
Carbon Tetrachloride
0.5
<0.01
Lindane
0.4
<0.0005
Chlordane
0.03
<0.02
Mercury
0.2
<0.0002
Chlorobenzene
100.0
<0.01
Methoxychlor
10.0
<0.0005
Chloroform
6.0
<0.01
Methyl Ethyl Ketone
200.0
<0.05
Chromium
5.0
<1.0
Nitrobenzene
2.0
<0.05
m-Cresol
200.0
<0.05
Pentachlorophenol
100.0
<0.25
o-Cresol
200.0
<0.05
Pyridine
5.0
<0.05
p-Cresol
200.0
<0.05
Selenium
1.0
<1.0
Cresol
200.0
<0.05
Silver
5.0
<1.0
2,4-D
10.0
<0.003
Tetrachloroethylene
0.7
<0.01
1,4-Dichlorobenzene
7.5
<0.05
Toxaphene
0.5
<0.05
1,2-Dichloroethane
0.5
<0.01
Trichloroethylene
0.5
<0.01
1,1-Dichloroethylene
0.7
<0.01
214,5-Trichlorophenol
400.0
<0.05
2,4-Dinitrotoluene
0.13
<0.05
2,4,6-Trichlorophenol
2.0
<0.05
Endrin
0.02
<0.0005
2,4,5-TP (Silvex)
1.0
<0.003
Heptachlor and its Hydroxide
0.008
<0.0005
Vinyl Chloride
0.2
<0.001
FORM: RSC 08-13 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate
the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Environmental Chemists, Inc. and Date of analysis: 11/28/23
Parameter
Ceiling
Monthly Average
Result
Concentration Limits
Concentration Limits
(C1assA & ClassB)
(Class A Only)
(mg/kg)
(mg/kg)
(mg/kg)
Arsenic
75
41
10.60
Cadmium
85
39
<7 77
Copper
4,300
1,500
156.00
Lead
840
300
<7 77
Mercury
57
17
<0.84
Molybdenum
75
n/a
<7 77
Nickel
420
420
<7 77
Selenium
100
100
<7 77
Zinc
7,500
2,800
3,080.00
b. For Surface Disposal Unit (landrll): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: and Date of analysis:.
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
❑ > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 08-13 Page 3 of

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 2.51 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Environmental Chemists, Inc. and Date of analysis: 11/28/23
Parameter
Result
(mg1k_g)
Aluminum
2,430.00
Ammonia -Nitrogen
17,900.00
Calcium
17,300.00
Magnesium
4,380.00
Nitrate -Nitrite Nitrogen
12,600.00
pH (Standard Unit)
7.95
Phosphorus
18,800.00
Potassium
5,420.00
Sodium
6,570.00
Total Kjeldahl Nitrogen
81,700.00
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 1.825
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and
conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 0_3 %. This rate
is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: N/A
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (15t) Year PAN
Five -Year
Maximum Adjusted PAN
(mS/kS)
(mg/k_g)
Surface
40,690
52,187
Injection/Incorporation
49,640
61,137
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 08-13 Page 4 of

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment.
❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
® Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
® Alternative 2 [ 15A NCAC 02T.1106(c)(2)] -Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion,
❑ composting, or ® lime stabilization.
c. For Surface Disposal:
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative I [15A NCAC 02T. I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
® Alternative 4 [15A NCAC 02T.1107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T.1107(a)(5)] - 14-Day Aerobic Processes.
® Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
❑ Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
® Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection.
® Alternative 10 [15A NCAC 02T.I 107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [I 5A NCAC 02T.I 107(b)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur
when these residuals are applied and left on the land surface.
FORM: RSC 08-13 Page 5 of

Facility Vicinity Map

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Pluris orth Topsail WWTP
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SCALE: 1 "= 1,500 ft Triple S Farms
Site
CHECKED BY: RTB Land Application Program Vicinity
BRANCH Pluris North Topsail WWTP Ma
DRAWN BY: RTB t
SIDUALS p
DATE: 11/14/2023 St SOILS, LLC Projnt No. 2007-71

Process Flow Diagram and Narrative

WASTEWATER TREATMENT PLANT PROCESS
The Pluris North Topsail WWTP is a domestic only 1.5 MGD wastewater plant. Attached is a copy
of the most recent copy of Permit WQ0005849 for this facility from 2020.

ROY COOPER
Governor
MICHAEL S. REGAN
Secretart
S. DANIEL SMITH
Director
RANDY HOFFMAN — REGIONAL MANAGER
PLUMS, LLC
5950 BERKSHIRE LANE — SUITE 800
DALLAS, TEXAS 75225
Dear Mr. Hoffman:
NORTH CAR01_11`4A
Environmental Quality
October 20, 2020
Subject: Permit No. WQ0005849
Pluris North Topsail WWTP
High -Rate Infiltration and
Wastewater Irrigation System
Onslow County
In accordance with your permit renewal request received February 28, 2020, and subsequent
additional information received May 19, 2020 and September 11, 2020, we are forwarding herewith Permit
No. WQ0005849 dated October 20, 2020, to Pluris, LLC for the continued operation of the existing
wastewater treatment, high -rate infiltration, and irrigation facilities, as well as the construction and
operation of the Phase II wastewater treatment facilities.
This permit shall be effective from the date of issuance through December 31, 2026, shall void
Permit No. WQ0005849 issued July 29, 2015, and shall be subject to the conditions and limitations therein.
The Permittee shall submit a renewal application no later than July 4, 2026.
Please pay attention to the monitoring requirements listed Attachments A, B, and C for they may
differ from the previous permit issuance. Failure to establish an adequate system for collecting and
maintaining the required operational information shall result in flit ure compliance problems.
The Division has removed the following permit condition since the last permit issuance dated
July 29, 2015:
Old Condition VI.2. — This condition has been removed because the permit is not voidable
The following permit conditions are new since the last permit issuance dated July 29, 2015:
Condition II. 11. —Setbacks for specific treatment/storage, infiltration, and irrigation sites have
been updated to the applicable setbacks when those facilities were originally permitted or last
modified.
Condition III.16. — Metering equipment shall be tested and calibrated annually.
Condition IV.12. — Monitoring wells MW-9 and MW-10 shall be sampled after construction,
and within 90 days of the effective date of this permit. Monitoring wells MW-9 and MW-10
shall be sampled thereafter at the frequencies and for the parameters specified in Attachment
C.
.DQ""512
Nort.h Carolina Department of Environmental Quality I Division of Water Resources
�_E North Salisbury Street ! 1b17 Mail Set vice Center R:deiyh, North Cm Mina 17699 1617
MIM-umrsaUib¢AI, 919.7074000

Mr. Randy Hoffman
October 20, 2020
Page 2 of 2
Condition IV.14. —For initial sampling of monitoring wells MW-9 and MW-10, the Permittee
shall submit a Compliance Monitoring Form (GW-59) and a Well Construction Record Form
(GW-1) listing this permit number and the appropriate monitoring well identification number.
Condition VI.10. —This permit shall not be renewed if the Pennittee or any affiliation has not
paid the required annual fee.
Attachment C —Added monitoring wells MW-4, MW-8, MW-9, and MW-10 to the list of wells
to be sampled.
If any parts, requirements, or limitations contained in this permit are unacceptable, the Permittee
has the right to request an adjudicatory hearing upon written request within 30 days following receipt of
this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North
Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service
Center, Raleigh, NC 27699-6714. Otherwise, this permit shall be final and binding.
If you need additional information concerning this permit, please contact Erick Saunders at (919)
707-3659 or crickson.saunder(cr),ncdenr.ao\ .
Sincerely,
GJ
S. Daniel Smith, Director
Division of Water Resources t`
cc: Onslow County Health Department (Electronic Copy)
Wilmington Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Laserfiche File (Electronic Copy)
Digital Permit Archive (Electronic Copy)

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENTAL QUALITY
RALEIGH
HIGH -RATE INFILTRATION SYSTEM PERMIT
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
Pluris, LLC
Onslow County
FOR THE
operation of a 1,542,635 gallon per day (GPD) wastewater treatment, high -rate infiltration, and irrigation
facility consisting of the:
construction and operation of the Phase II wastewater treatment plant modifications consisting of: ten
membrane cassettes, a 386 gallon per minute (GPM) permeate pump, and a turbidimeter serving the Phase
I MBR aeration basin; an ultraviolet (UV) disinfection system bank with 48 bulbs; a groundwater pumping
station wet well with a hydropneumatic tank, two submersible pumps, and duplex control panel; and all
associated piping, valves, controls, and appurtenances; the
continued operation of a wastewater treatment plant consisting of: a Parshall flume; an ultrasonic flow
meter; a manually cleaned bar screen; a 42.2 acre three -cell facultative lagoon with 57 million gallons of
capacity; a tablet chlorinator; a 138,875 gallon chlorine contact chamber; an irrigation pump station
containing duplex 1,800 GPM pumps; an effluent flow meter; and all associated piping, valves, controls,
and appurtenances; the
continued operation of a Phase I wastewater treatment plant consisting of: a flow splitter box with a 3-inch
spaced manual bar screen; an influent magnetic induction type flow meter totalizer; a 254,320 gallon
aerated flow equalization tank with two 1,200 GPM submersible pumps and two 10 horsepower (hp)
floating mechanical aerators; dual 2 millimeter (mm) rotary drum fine screens with auto wash using treated
effluent; a 52,229 gallon anaerobic tank with a 2 hp mechanical mixer (a spare 2 hp mechanical mixer shall
be kept on site); an alum chemical feed system with two 20 gallon per hour (GPH) chemical feed pumps; a
49,745 gallon pre -anoxic tank with a 1.5 hp mechanical mixer (a spare 1.5 hp mechanical mixer shall be
kept on site); two 121,583 gallon pre -aeration tanks with two 300 cubic foot per minute (CFM) blowers,
fine bubble diffusers and two 4.6 hp mechanical mixers (a spare 4.6 hp mechanical mixer shall be kept on
site); a pre -aeration recirculation wet well with two 2,778 GPM recirculation pumps serving the anaerobic
and pre -anoxic tanks; a 70,324 gallon post anoxic tank with a 3.6 hp mechanical mixer (a space 3.6 hp
mechanical mixer shall be kept on site) and served by a Micro C chemical feed system with two 1.8 GPH
chemical feed pumps; two 41,888 gallon membrane bio-reactor (MBR) aeration basins with ten membrane
cassettes in one basin, a 386 GPM permeate pump, fine bubble diffusers, a telescoping valve, a turbidimeter
and two 711 CFM blowers; a recycled activated sludge (RAS) and waste activated sludge (WAS) wet well
with two 2,082 GPM recycle/wasting pumps; a 330,616 gallon aerobic digester with 6-inch diameter
decanting pipes, coarse bubble diffusers and served by two 1,000 CFM blowers; an ultraviolet (UV)
WQ0005849 Version 4.0 Shell Version 200201 Page 1 of 16

disinfection unit containing one bank of 48 bulbs; a wash water lift station with two 300 GPM submersible
pumps and a gravity feed line to the high -rate infiltration basins; a 9.5 acre dewatering storage lagoon with
22.4 million gallons of storage; an auxiliary generator with an automatic transfer switch; and all associated
piping, valves, controls, and appurtenances; the
continued operation of a 542,635 GPD wastexvater irrigation system consisting of: a 129.28 acre spray
irrigation area comprised of 25 fields; and all associated piping, controls, valves and appurtenances; and
the
continued operation of a 1,000,000 GPD high -rate infiltration system consisting of two high -rate
infiltration basin effluent flow meters; a refrigerated effluent sampler; a 1.07 acre high -rate infiltration basin
(IB-1) with a loading rate of 10.77 gallons per day per square foot (GPD/ft'); a 1.52 acre high -rate
infiltration basin (IB-2) with a loading rate of 7.54 GPD/ftz; a gravity dewatering collection piping network
with a ultrasonic flow meter and drains to a water collection pond that overflows via a 400 foot rip rap and
ABC stone level spreader; and all associated piping, valves, controls, and appurtenances
to serve the Pluris North Topsail WWTP, with no discharge of wastes to surface waters, pursuant to the
application received Febniary 28, 2020, subsequent additional information received May 19, 2020 and
September 11, 2020, and in conformity with the Division -approved plans and specifications considered a
part of this permit.
This permit shall be effective from the date of issuance through December 31, 2026, shall void Permit No.
WQ0005849 issued July 29, 2015, and shall be subject to the following conditions and limitations:
I. SCHEDULES
Upon completion of constriction and prior to operation of the Phase II permitted modifications, the
Permittee shall submit an engineering certification from a North Carolina licensed Professional
Engineer certifying that the permitted facility has been constricted in accordance with G.S. 143-215.1,
Administrative Code Title 15A Subchapter 02T, this permit, and the Division -approved plans and
specifications. For phased and partially certified facilities, the Pennittee shall retain the responsibility
to track fiirther construction approved under this pennit, and shall provide a final engineering
certification upon project completion. Mail the Engineering Certification to the Division of Water
Resources, Non -Discharge Branch, 1617 Mail Service Center, Raleigh, NC 27699-1617, or Non-
DiscliarUe.Reports(a)ncdenr.izov. [15A NCAC 02T .0116(a)]
2. The Pennittee shall notify the Wilmington Regional Office, telephone number [phone], at least
two business days in advance of initial operation of the constricted facilities so that the Division can
conduct a startup inspection. [15A NCAC 02T .0108(b)(1)(B)]
3. The Pennittee shall request renewal of this pen -nit on Division -approved forms no later than July 4,
2026. [15A NCAC 02T .0105(b), 02T .0109]
WQ0005849 Version 4.0 Shell Version 200201 Paee 2 of 16

Justification for Residuals Production Rate

JUSTIFICATION FOR WWTP RESIDUALS PRODUCTION RATE
Review of dry tons produced from this facility indicates the dry tons form this facility should be 70
dry tons based on previous years application information.

Residuals Sampling Plan

WWTP SAMPLING PLAN — PLURIS NORTH TOPSAIL WWTP
Annually, multiple grab residual solid samples are collected from the sludge holding tank. These
samples are composited for nutrient and metal analyses. The composited sample is mixed to keep the
solids suspended and containers filled for this analysis. Lime stabilization occurs when the MBR
basins reaches capacity. Lime is added to reach proper stabilization requirements for vector attraction
and pathogen reduction. Field measurements of pH and temperature are collected for each
stabilization event to insure pH requirements are met. pH values are later temperature corrected.
Annually, or when the residual solids are to be land applied if application occurs less than annually,
a composite residual solid sample will be analyzed for: Arsenic, Cadmium, Copper, Lead, Mercury,
Molybdenum, Nickel, Selenium, Zinc, Aluminum, Ammonia — Nitrogen, Calcium, Nitrate -Nitrite,
Nitrogen, Magnesium, % Total Solids, pH, Phosphorus, Potassium, TKN, and Sodium. From this
information, the Plant Available Nitrogen (PAN) will be calculated. Once a permit cycle, a composite
TCLP sample will be collected to include:
Arsenic
Hexachlorobenzene
ph for Corrosivity
Barium
Hexachloro-1,3-Butadiene
Benzene
Hexachloroethane
Flash point for ignitability
Cadmium
Lead
Carbon Tetrachloride
Lindane
Sulfides and Cyanides for reactivity
Chlordane
Mercury
1,2-Dichloroethane
Chlorobenzene
Methoxychlor
1,1-Dichloroethylene
Chloroform
Methyl Ethyl Ketone
2,4-Dinitrotoluene
Chromium
Nitrobenzene
Endrin
m-Cresol
Pentachlorophenol
Heptachlor and its Hydroxide
o-Cresol
Pyridine
Trichloroethylene
p-Cresol
Selenium
2,4,5-Trichlorophenol
Cresol
Silver
2,4,6-Trichlorophenol
2,4-D
Tetrachloroethylene
2,4,5-TP (Silvex)
1,4-Dichlorobenzene
Toxaphene
Vinyl Chloride

Analytical Data From Pluris North Topsail WWTP
TCLP, Fecal and Nutrient & Metal

Waste Water Treatment Plant
North Topsail WWTP
Sneads Ferry, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2023
Date Reported: 11/28/2023 Report No: NT 2023-25009
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
81.380
PAN Inj.
99.280
P
37.600
K
10.840
Lime (estimated)
0.000
Secondary Nutrients
Calcium
34.600
Magnesium
8.760
Sodium
13.140
SAR
1.825
Chloride
0.000
Iron
0.000
Alumium
4.860
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
2.51
pH
7.950
Min Rate
0.300
Metals
Arsenic
0.021
Cadmium
0.016
Chromium
0.021
Copper
0.312
Lead
0.016
Mercury
0.002
Molybdenum
0.016
Nickel
0.016
Seleniun
0.016
Zinc
6.160

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
North Topsail WWTP
North Topsail WWTP
Sneads Ferry, North Carolina
Triple S Farms & Cleaning, Inc
Waste Water Treatment Plant
NT 2023-25009
10/26/2023 Type of Stabilization: ;]Lime
11/28/2023
Annual 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
2.510
Nitrogen (TKN)*
8.170
81,700.00
Phosphorus
1.880
18,800.00
Potassium
0.542
5,420.00
Sulfur
0.00
Calcium
1.730
17,300.00
Magnesium
0.438
4,380.00
Sodium
0.657
6,570.00
Iron
---
Aluminum
---
2,430.000
Manganese
---
Copper
---
156.000
1,500
Zinc
---
3,080.000
7,500
Ammonia Nitrogen*
1.790
17,900.000
Nitrate N / Nitrite N*
---
12,600.000
Cadmium
---
7.770
39
Chromium
---
10.700
1,200
Nickel
---
7.770
420
Lead
---
7.770
300
Arsenic
---
10.600
41
Mercury
---
0.837
17
Selenium
---
7.770
100
pH
7.950
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
6.380
Molybdenum
---
7.770
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

:en7virochhem
ANALYTICAL 8 CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
[e-mail]
Pluris LLC. Date of Report: Nov 28, 2023
P. O. Box 856 Customer PO #:
Sneads Ferry NC 28460 Customer ID: 09110001
Attention: Report #: 2023-25009
Project ID: North Topsail Sludge
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
23-60638 Site: Sludge 10/26/2023 11:26 AM Solid/Sludge Pete Peterson
Test Method Results Date Analyzed
Chlordane (TCLP)
SW-8468081 B
<0.02 mg/L
11/07/2023
Endrin (TCLP)
SW-84680818
<0.0005mg/L
11/07/2023
Heptachlor (TCLP)
SW-8488081 B
<0.0005 mg/L
11/07/2023
Heptachlor epoxide (TCLP)
SW-8468081 B
<0.0005 mg/L
11/07/2023
Lindane (TCLP)
SW-846 $081 B
<0.0005 mg/L
11/07/2023
Methoxychlor (TCLP)
SW-8488081 B
<0.0005 mg/L
11/07/2023
Toxaphene (TCLP)
SW-846 $081 B
<0.05 mg/L
11/07/2023
2,4,5-TP (TCLP)
SW-6468151 A
<0.003 mg/L
11/08/2023
2,4-13 (TCLP)
SW-8468151 A
<0.003 mg/L
11/08/2023
1,4-Dichlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
11/08/2023
2,4,5-Trichlorophenol (TCLP)
SW-8468270E
<0.050mg/L
11/08/2023
2,4,6-Trichlorophenol (TCLP)
SW-8488270E
<0.050mg/L
11/08/2023
2,4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
11/08/2023
Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
11/08/2023
Hexachloro-1,3-butadiene (TCLP)
SW-846 8270 E
<0.050 mg/L
11/08/2023
Hexachlorobenzene (TCLP)
SW-848 8270 E
<0.050 mg/L
11/08/2023
Hexachloroethane (TCLP)
SW-846 8270 E
<0.050 mg/L
11/08/2023
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
11/08/2023
Nitrobenzene (TCLP)
SW-046 6270 E
<0.050 mg/L
11/08/2023
o-Cresol (TCLP)
SW-046 8270 E
<0.050 mg/L
11/08/2023
Pentachlorophenol (TCLP)
SW-846 8270 E
<0.250 mg/L
11/08/2023
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
11/08/2023
1. 1 -Dichloroethylene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
11/9/2023
1,2-Dichloroethane (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
11/9/2023
Benzene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
I V9/2023
Carbon Tetrachloride (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
11/9/2023
Report # 2023-25009 Page 1 of 3

Eenirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Pluris LLC.
Date of Report: Nov 28, 2023
P. O. Box 856
Customer PO #:
Sneads Ferry NC
28460
Customer ID: 09110001
Attention:
Report #: 2023-25009
Project ID: North Topsail Sludge
Chlorobenzene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
11 /9/2023
Chloroform (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
11/9/2023
Methyl ethyl ketone (TCLP)
SW-e46 Method 8260D
< 0.05 mg/L
11 /9/2023
Tetrachloroethylene (TCLP)
SW -US Method 8260D
< 0.01 mg/L
11 /9/2023
Trichloroethylene (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
11 /9/2023
Vinyl Chloride (TCLP)
SW-846 Method 8260D
< 0.01 mg/L
11 /9/2023
RCI
Cyanide
SM 4500 CN 0-2016
4.25 mg/kg
11 /07/2023
Sulfide
SM 4500 S D-2011
62.9 mg/kg
11 /08/2023
Ignitability
SW 846 method 1010
>158 °F
11/10/2023
Sludge Residuals
Aluminum
EPA 200.7. Rev, 4.4. 1994
2430 mg/kg
11/01/2023
Arsenic
EPA 200.7, Rev. 4.4. 1994
10.6 mg/kg
11/01/2023
Cadmium
EPA200,7, Rev. 4.4. 1994
<7.77 mg/kg
11/01/2023
Calcium
EPA 200.7, Rev. 4.4, 1994
17300 mg/kg
11/01/2023
Chromium
EPA 200.7. Rev. 4.4. 1994
10.7 mg/kg
11/01/2023
Copper
EPA 200.7, Rev. 4.4. 1994
156 mg/kg
11/01/2023
Lead
EPA 200.7. Rev. 4.4. 1994
<7.77 mg/kg
11/01/2023
Magnesium
EPA 200.7. Rev. 4.4.1994
4380mg/kg
11/01/2023
Molybdenum
EPA 200 7, Rev. 4.4,1994
<7.77 mg/kg
11/01/2023
Nickel
EPA 200.7, Rev. 4.4. 1994
<7.77 mg/kg
11 /01/2023
Potassium
EPA 200.7, Rev. 4.4,1994
5420 mg/kg
11/01/2023
Selenium
EPA 2001, Rev. 4.4, 1994
<7.77 mg/kg
11/01/2023
Sodium
EPA 200 7, Rev 4.4,1994
6570 mg/kg
11/02/2023
Zinc
EPA 200 7, Rev 4.4, 1994
3080 mg/kg
11/01/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2
12600 mg/kg
11/07/2023
Total Solids M
SM 2540 a
2.51 %
10/30/2023
Ammonia Nitrogen
SM 4600 NH3 C-2011
17900 mg/kg
10/27/2023
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg 8-2011
81700 mg/kg
10/29/2023
Total Phosphorus
SM 4600 P (F-H)-2011
18800 mg/kg
11 /03/2023
Report #-.: 2023-26009
Page 2 of 3

Environmental Chemists, Inc.
IL envirochem A i 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
_�_ _ 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Plurls LLC. Date of Report: Nov 28, 2023
P. O. Box 856 Customer PO #:
Sneads Ferry NC 28460 Customer ID: 09110001
Attention: Report #: 2023-25009
Project ID: North Topsail Sludge
pH sw 946 Method 90451) 7.95 units 10/27/2023
Result estimated. Analyzed out of 15 minutes hold time.
Mercury
sw-a4e 7471 a
<0.837 mg/kg
11012023
TCLP Metals
Arsenic (TCLP)
EPA 200.7, Rev 4 4, 1994
<1.0 mg/L
11/09/2023
Barium (TCLP)
EPA 200 7, Rev 4 4, 1994
<1.0 mg/L
11/09/2023
Cadmium (TCLP)
EPA 200 7, Rev 4 4, 1994
<1.0 mg/L
11/09/2023
Chromium (TCLP)
EPA 200 7, Rev 4 4, 1994
<1.0 mg/L
11/09/2023
Lead (TCLP)
EPA 200 7, Rev 4 4, 1994
<1.0 mg/L
11/09/2023
Selenium (TCLP)
EPA 200 7, Rev 4 4, 1994
<1.0 mg/L
11/09/2023
Silver (TCLP)
EPA 200 7, Rev 4 4.1994
<1.0 mg/L
11/09/2023
Mercury (TCLP)
EPA 2451
<0.0002 mg/L
11082023
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: M pia, XA- D.,::: � oblo - d1i
Report * 2023-25009 Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC lab #94
Sample Receipt Checklist
6602 Windmill v
Wilmington, NC 284
910.392.0;
Client: p UY
Date:
AM& Report
Number: 2023- �hl7G
Receipt of sample:
❑ YES ❑ NO
ECHEM Pickup Client Deliver ❑ UPS ❑ FedEx O
N A Y Other ❑
/
❑ YES ❑ NO
0 N/A
1. ere custody seals present on the cooler?
2.
Original temperature upon
If custody seals were present, were they intact/unbroken?
receipt °C
Corrected temperature upon receipt
How temperature taken: ❑ Temperature Blank 0
Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869
O YES ❑ NO
IR Gun Correction Factor °C: 0.0
3. If temperature of cooler exceeded 6°C,
O YES ❑ NO
was Project Mgr. CIA notified?
4. Were proper custody procedures (relinquished/received)
Cl YES ❑ NO
followed?
S. Were sample ID's listed on the COC?
© YES ❑ NO
O YES ❑
6. Were samples ID's listed on sample containers?
NO
© YES O
7. Were collection date and time listed on the COC?
NO
I@ YES ❑
8. Were tests to be performed listed on the COC?
NO
O YES O
9. Did samples arrive in proper containers for each test?
NO
YES ❑
10. Did samples arrive in good condition for each test?
NO
11. Was adequate sample volume available?'
YES ❑ NO
12. Were sam 1
p es received within proper holding time for requested tests?
❑ YES ❑ NO 13. Were acid preserved samples received at a pH of <2?
❑ YES O NO 14. Were cyanide samples received at a pH >12?
❑ YES ❑ NO 15. Were sulfide samples received at a pH >9?
T YES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? *� ❑ ES
Y❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrect)
by adding (circle one): H SO HNO Y Preserved and were adjusted accordingly
Z a a HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time.
Volatiles Samples) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
info;nrenvi ronmcntalchemists.com
Pluris LLC. Date of Report: May 01, 2023
P. O. Box 856 Customer PO #:
Sneads Ferry NC 28460 Customer ID: 09110001
Attention: Report #: 2023-07013
Project ID: Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-17835 Site: 001 4/11/2023 11.02 AM Solid/Sludge
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 4.13 % 04/12/2023
Fecal Density SM 9221C E-2014 33899 MPN/g 04/11/2023
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-17836 Site: 002 4/11/2023 11:04 AM Solid/Sludge
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
23-17837 Site:003
SM 2540 B
SM 9221C E-2014
4.30 % 04/12/2023
125582 MPN/g 04/11/2023
Collect Date/Time Matrix Sampled by
4/11/2023 11:05 AM Solid/Sludge
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 4.12 % 04/12/2023
Fecal Density SM 9221C E-2014 31554 MPN/g 04/11/2023
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-17838 Site: 004 4/11/2023 11:07 AM Solid/Sludge
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
23-17839 Site:005
SM 2540 B
SM 9221C E-2014
3.94 % 04/12/2023
43148 MPN/g 04/11/2023
Collect Date/Time Matrix Sampled by
4/11/2023 11:10 AM Solid/Sludge
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E-2014
4.23 % 04/12/2023
30733MPN/g 04/11/2023
ReportA:. 2023-07013 Page 1 of 3

envirochem
ANALYTICAL & CONSULTING CHEMISTS
ppo'ow —. ... 7:'""l
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 , 910.347.5843 Lab/Fax
info, t: environmentalchemists.com
Pluris LLC. Date of Report: May 01, 2023
P. 0. Box 856 Customer PO #:
Sneads Ferry NC 28460 Customer ID: 09110001
Attention: Report #: 2023-07013
Project ID: Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-17840 Site: 006 4/11/2023 11:11 AM Solid/Sludge
Test Method Results Date Analyzed
Total Solids (%) SM 2540 6 4.16 % 04/12/2023
Fecal Density SM 9221 c E-2014 31250 MPN/g 04/11 /2023
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-17841 Site: 007 4/11/2023 11:13 AM Solid/Sludge
Test Method Results Date Analyzed
Total Solids (%) SM 2540 a 4.29 % 04/12/2023
Fecal Density SM 9221C E-2014 51283 MPN/g 04/11/2023
Report $ 2023.07013 Page 2 of 3

161 envirochem 14
ANALYTICAL 8 CONSULTING CHEMISTS
ro"O' -- —77
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 1, 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Pluris LLC. Date of Report: May 01, 2023
P. O. Box 856 Customer PO #:
Sneads Ferry NC 28460 Customer ID: 09110001
Attention: Report #: 2023-07013
Project ID: Sludge
Lab ID Sample ID:
23-17842 Site: Sludge
Collect Date/Time Matrix Sampled by
4/11/2023 11:15 AM Solid/Sludge
Test
Method
Results
Date Analyzed
Sludge Residuals
Aluminum
EPA 200 7 Rev 4 4 1994
4580 mg/kg
04/26/2023
Arsenic
EPA 200.7 Rev 4 4 1994
<27.0 mg/kg
04/26/2023
Cadmium
EPA 2007,Rev 44 1994
<27.Omg/kg
04/26/2023
Calcium
EPA 200 7 Rev 4 4 1994
19700 mg/kg
04/26/2023
Chromium
EPA 200 7. Rev 4 4 1994
<27.0 mg/kg
04/26/2023
Copper
EPA 200 7 Rev 4 4 1994
175 mg/kg
04/26/2023
Lead
EPA 200.7, Rev. 4 4 1994
<27.0 mg/kg
04/26/2023
Magnesium
EPA 200.7, Rev 4 4 1994
4150 mg/kg
04/26/2023
Molybdenum
EPA 200.7, Rev. 4 4 1994
<27.0 mg/kg
04/26/2023
Nickel
EPA 200.7, Rev. 4 4.1994
<27.0 mg/kg
04/26/2023
Potassium
EPA 200.7, Rev. 4 4,1994
6560 mg/kg
04/26/2023
Selenium
EPA 200.7, Rev. 44, 1994
<27.0 mg/kg
04/26/2023
Sodium
EPA 200.7, Rev. 4 4, 1994
3790 mg/kg
04/26/2023
Zinc
EPA 200.7, Rev. 4 4, 19"
3750 mg/kg
04/26/2023
Nitrate+Nitrite-Nitrogen
EPA353.2
64.4mg/kg
04/12/2023
Total Solids (%)
SM 2640 B
4.19 %
04/12/2023
Ammonia Nitrogen
SM 4500 NH3 G2011
15200 mg/kg
04/12/2023
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
70600 mg/kg
04/12/2023
Total Phosphorus
SM 4500 P (F-H)-2011
18800 mg/kg
04/20/2023
pH
SW 846 Method 9045D
7.33 units
04/24/2023
Mercury
sw 846 7471 B
<0.403 mg/kg
04/14/2023
Comment: Results, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by: -.
Repart #:: 2023-07013 _ - - Page 3 of 3

Environmental Chemist, Inc., Wilmington, NC Lab #94
Client: r Ux-"
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Date: 1/cR—R-Report Number: _ 2023- 0-N
Receipt of sample: ECHEM Pickup % Client De very O
JUPS ❑ FedEx ❑ Other ❑
❑ YES
❑ NO
® N/A
1. ere custody seals present on the cooler?
❑ YES
❑ NO
IP N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank ® Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
Llti YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
Ct YES
❑ NO
5. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
YES
❑ NO
7. Were collection date and time listed on the COO
YES
❑ NO
8. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive in proper containers for each test?
IX YES
❑ NO
10. Did samples arrive in good condition for each test?
YES
❑ NO
11. Was adequate sample volume available?'
i$ YES
13 NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
O YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCl NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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RSCA — Pluris Webb Creek WWTP 06-16

State of North Carolina
DWR
Department of Environment and Natural Resources
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 08-13
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and
supporting documentation
For more information or for an electronic version of this form, visit the Land Application Unit (LAU) web site at:
http: //portal. ncdenr. org/iveb/wyl(tpsllati
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 08-13, FORM: DCAR 08-13, or FORM: SDR 08-13).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 08-13):
® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 08-13) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
❑ For new or renewed permits, submit a separate certification for each source facility.
® For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
® Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Residuals Source -Generating Facility Information:
® For each source facility, attach the following:
® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for
Residuals Land Application Permits".
® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated, treated, processed, and stored at the facility.
® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the
permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or
disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing.
® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure
that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector
attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to
be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
® For each source facility, attach the following:
® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach
analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities.
INSTRUCTIONS FOR FORM: RSC 08-13 Page 1 of 1

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- ­- 17;,--.,, State of North Carolina
�� Department of Environment and Natural Resources
;a Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 08-13
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Pluris Webb Creek WWTP
2. Facility permit holder is: ❑ Federal, ❑ State, ❑ Local Government, or ® Private.
Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health,
or ❑ Other (explain: ).
3. Facility contact person and title: William Andrews, ORC
Complete mailing address: 1095 Hwy 210
City: Sneads Fen State: NC Zip: 28460-
Telephone number: [phone] E-mail address: wandrews0Vplurisusa.com
4. Facility physical address: 250 Zachary Lane
City: Hubert State: NC Zip: 28539-
Coordinates: Latitude: 34' 40' 10.29" Longitude: 77' 12' 5.75"
Datum: NAD83 Level of accuracy: Hundredths of Second
Method of measurement: MAP
5. Purpose of the facility:
❑ treatment of municipal wastewater, ® treatment of 100% domestic wastewater,
❑ treatment of potable water, ❑ treatment of 100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: . % industrial and % domestic)
❑ other (explain: ).
6. Does the facility have an approved pretreatment program: ❑ Yes ® No
7. Facility permitted/design flow: <0.3 MGD and facility average daily flow: 0.245 MGD
8. Average amount of residuals being generated at this facility 80 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: Aerobic
Type and volume of residuals storage (i.e., outside of residuals treatment units): N/A
II. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
® 40 CFR Part 503 or ❑ 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
® Biological ❑ Non -Biological
FORM: RSC 08-13 Page 1 of
5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ❑ no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: ❑ yes ❑ no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well
as those for corrosivity, ignitability, and reactivity:
Laboratory: Environmental Chemists, Inc. and Date of analysis: 11/21/23
Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ® yes ❑ no. Flashpoint: >158 OF (> 140°F)
Passed reactivity test: ® yes ❑no. HCN: 1.00 mg/kg (<250) & H2S: 8.08 mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
Arsenic
5.0
<1.0
Hexachlorobenzene
0.13
<0.05
Barium
100.0
<1.0
Hexachloro-1,3-Butadiene
0.5
<0.05
Benzene
0.5
<0.01
Hexachloroethane
3.0
<0.05
Cadmium
1.0
<1.0
Lead
5.0
<1.0
Carbon Tetrachloride
0.5
<0.01
Lindane
0.4
<0.0005
Chlordane
0.03
<0.02
Mercury
0.2
<0.0002
Chlorobenzene
100.0
<0.01
Methoxychlor
10.0
<0.0005
Chloroform
6.0
<0.01
Methyl Ethyl Ketone
200.0
<0.05
Chromium
5.0
<1.0
Nitrobenzene
2.0
<0.05
m-Cresol
200.0
<0.05
Pentachlorophenol
100.0
<0.25
o-Cresol
200.0
<0.05
Pyridine
5.0
<0.05
p-Cresol
200.0
<0.05
Selenium
1.0
<1.0
Cresol
200.0
<0.05
Silver
5.0
<1.0
2,4-D
10.0
<0.003
Tetrachloroethylene
0.7
<0.01
1,4-Dichlorobenzene
7.5
<0.05
Toxaphene
0.5
<0.05
1,2-Dichloroethane
0.5
<0.01
Trichloroethylene
0.5
<0.01
1,1-Dichloroethylene
0.7
<0.01
2,4,5-Trichlorophenol
400.0
<0.05
2,4-Dinitrotoluene
0.13
<0.05
2,4,6-Trichlorophenol
2.0
<0.05
Endrin
0.02
<0.0005
2,4,5-TP (Silvex)
1.0
<0.003
Heptachlor and its Hydroxide
0.008
<0.0005
Vinyl Chloride
0.2
<0.01
FORM: RSC 08-13 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate
the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Environmental Chemists, Inc. and Date of analysis: 11/21/23
Parameter
Ceiling
Monthly Average
Result
Concentration Limits
Concentration Limits
(ClassA & ClassB)
(Class A Only)
(mglkg)
(mglkg)
(mg/kg)
Arsenic
75
41
<14.70
Cadmium
85
39
<14.70
Copper
4,300
1,500
146.00
Lead
840
300
<14.70
Mercury
57
17
<1.33
Molybdenum
75
n/a
<14.70
Nickel
420
420
<14.70
Selenium
100
100
<14.70
Zinc
7,500
2,800
1,990.00
b. For Surface Disposal Unit (landFll): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: and Date of analysis:
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
❑ > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 08-13 Page 3 of

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 1.58 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Environmental Chemists, Inc. and Date of analysis: 11/21/23
Parameter
Result
(Mg/kg)
Aluminum
15,300.00
Ammonia -Nitrogen
2,270.00
Calcium
19,400.00
Magnesium
1,570.00
Nitrate -Nitrite Nitrogen
1,030.00
pH (Standard Unit)
7.44
Phosphorus
31,800.00
Potassium
3,630.00
Sodium
5,780.00
Total Kjeldahl Nitrogen
53,400.00
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 1.346
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and
conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 0_3 %. This rate
is a (check one): ® default value, or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: N/A
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (151) Year PAN
Five -Year
Maximum Adjusted PAN
(mg/kg)
(mg/k-g)
Surface
17,504
26,717
Injection/Incorporation
18,639
27,852
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 08-13 Page 4 of

7. Pathogen Reduction: Per 15A NCAC 02T.11061 specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent.
❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
❑ Alternative 1 [ 15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T. 1 106(b)(3)(B)] - Alkaline Treatment.
❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 4 [15A NCAC 02T. 1 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of Class B:
® Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration.
® Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion,
❑ composting, or ® lime stabilization.
c. For Surface Disposal:
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑ Alternative 1 [15A NCAC 02T. 1 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [15A NCAC 02T.1107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
® Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
® Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
❑ Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
® Alternative 9 [15A NCAC 02T.1107(a)(9)] - Injection.
® Alternative 10 [ 15A NCAC 02T. 1107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [ 15A NCAC 02T.1107(b)(2)].
❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur
when these residuals are applied and left on the land surface.
FORM: RSC 08-13 Page 5 of 5

Facility Vicinity Map

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CHECKED BY: RTB Land Application Program Vicinity
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RANCH Pluris Webb Creek WWTP MaP
DRAWNBY:
DATE: 11/14/2023 OILS, LLC F
Projmt No. 2007-71
1-i

Process Flow Diagram and Narrative

WASTEWATER TREATMENT PLANT PROCESS
The Pluris Webb Creek WWTP is a 0.3 MGD wastewater plant. Attached is a copy of Permit
NC0089877 for this facility from 2019 and name change from 2023.

4 '
ONWASA
onwasa corn
228 Georgetown Rd
Jacksonville, NC 28540
North Carolina Department of Environmental Quality
Division of Water Resources / NPDES Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Re: Request for Permit Ownership Change
Webb Creek WWTP, NCO089877
NPDES Staff.
September 15, 2023
RECEIVED
5 E P 2 2 2023
NCDEQ/D1NR/NPDES
Please find enclosed a completed Permit Name/Ownership Change Form and supporting
documentation for the above -referenced facility.
Based on our current schedule to obtain final approvals and secure the necessary funding,
we anticipate closing on the sale of the plant and associated collection system on November 9,
2023, and assuming operation immediately. As noted on the form, there will be no change in the
waste stream, treatment system or discharge location with this change in ownership.
Please feel free to reach out to me directly at [phone] or dmohrCaD-onwasa.com if
you have any questions or concerns over this request.
Sincerely,
David M. Mohr, PE
Chief Operations Officer
Onslow Water and Sewer Authority
Cc: Franky J. Howard, Chief Executive Officer
Seth Brown, Treatment Facilities Administrator
Encl. Executed Systems Purchase Agreement
NCPUC Order Approving Transfer

DocuSign Envelope ID: 73591442-395E4881-8F33-E81E71A023E3
STIITit '
ROY COOPER
MICHAEL S. REGAN
• � � i t- 4��
4
LINDA CULPL'•PPER
NORTH CAROLINA
E'nyironmental Quality
8/12/2019
Mr. Maurice Gallarda
Pluris Webb Creek LLC
2100 McKinney Ave, Suite 1550
Dallas, TX
Subject: Issuance of NPDES Permit
Permit Number NCO089877
Webb Creek WWTP
Grade III Biological WPCS [15A NCAC 08G .0302]
Onslow County
Dear Mr. Gallarda:
Division personnel have reviewed and approved your application for the subject permit. Accordingly, we
are forwarding the attached NPDES discharge permit. This permit is issued pursuant to the requirements of
North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North Carolina and the
U.S. Environmental Protection Agency dated October 15, 2007 (or as subsequently amended).
This final permit includes no major changes from the draft permit sent to you on May 29, 2019.
If any parts, measurement frequencies or sampling requirements contained in this permit are unacceptable
to you, you have the right to an adjudicatory hearing upon written request within thirty (30) days following
receipt of this letter. This request must be in the form of a written petition, conforming to Chapter 150B of the
North Carolina General Statutes, and filed with the Office of Administrative Hearings (6714 Mail Service Center,
Raleigh, North Carolina 27699-6714). Unless such demand is made, this decision shall be final and binding.
Please note that this permit is not transferable except after notice to the Division. The Division may
require modification or revocation and reissuance of the permit. This permit does not affect the legal
requirements to obtain any other Federal, State, or Local governmental permit that may be required. If you have
any questions concerning this permit, please contact Emily DelDuco at emily.delduco a.nedenr.gov or at the
number listed below.
Sincerely,
DocuSigned by:
8328B44CE9EB4A1...
Linda Culpepper
Director
cc: NPDES files
ec: Wilmington Regional Office
Michael Gallant ([e-mail])
North Carolina Department of Environmental Quality; Division of Water Resources
1617 Mail Service Center I Raleigh. North Carolina 27699.1617
919-707-9125

DocuSign Envelope ID: 73591442-3958-4881-8F33-E81E71A023E3
Permit NCO089877
STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Environmental Management
Commission, and the Federal Water Pollution Control Act, as amended,
Pluris Webb Creek, LLC.
is hereby authorized to discharge wastewater from a facility located at the
Webb Creek WWTP
250 Zachary Lane
Southwest of Swansboro
Onslow County
to receiving waters designated as Wallace Creek in the White Oak River Basin in accordance with
effluent limits, monitoring requirements, and other conditions set forth in Parts 1, I1, III and IV hereof.
This permit shall become effective September 1, 2019.
This permit and authorization to discharge shall expire at midnight on August 31, 2024.
Signed this day 8/12/2019
DocuSigned by:
`' ,
8328B44CE9E9q4A1...
Linda Culpepper, Director
Division of Water Resources
By Authority of the Environmental Management Commission
Pagel of 9

DocuSign Envelope ID: 73591442-395B-4881-8F33-E81E71A023E3
Permit NCO089877
SUPPLEMENT TO PERMIT COVER SHEET
Pluris Webb Creek, LLC.
is hereby authorized to:
1. Operate an existing 0.3 MGD wastewater treatment facility located at 250 Zachary Lane at the Webb Creek
WWTP (Onslow County), that includes the following components:
♦ Automatic bar screen
♦ Three sequencing batch reactors
♦ Effluent surge tank
♦ Ultraviolet disinfection
♦ Post aeration
• Sludge handling tanks
♦ Effluent pump station
♦ Standby generator
2. And, upon receiving Authorization to Construct permit from the Division, replace the existing treatment
system with an upgraded 0.35 MGD wastewater treatment facility at the same location that includes the
following components:
♦ Two (2) 1.87 MGD Rotary Drum Screen System with containment
♦ One (1) 39,300 gallon Equalization Basin (Pre -Anoxic)
♦ Two (2) 38,350 gallon Pre -Aeration Basins with air diffusers
♦ One (1) 32,800 gallon Post -Anoxic Basin with mixer
• Two (2) 20,750 gallon MBR Basins with eight (8) 0.04 micron membrane cassettes
♦ Five (5) Blowers (2 pre -aeration, mmembrane)
♦ One (1) 38,350 gallon Aerobic Digester with air diffusers
♦ One (1) Effluent Wash Water Wet Well with two (2) 128 GPM submersible Wash Water Pumps
♦ One (1) Effluent Composite Sampler
♦ One (1) Effluent Lift Station Wet Well with two (2) 1,100 GPM submersible Effluent Pumps
♦ One (1) 55 gallon Peracetic Acid Tank with containment and dual 280 GPH metering pump system
♦ One (1) 55 gallon drum Alum feed system with dual 1.8 GPH metering pumps
♦ One (1) 55 gallon Micro-C feed system with dual 20 GPH metering pumps
3. Discharge from said treatment works at the location specified on the attached map into Wallace Creek [HUC:
030203010301 ], currently classified SB-NSW waters in the White Oak River Basin.
Page 2 of 9

Justification for Residuals Production Rate

JUSTIFICATION FOR WWTP RESIDUALS PRODUCTION RATE
Review of dry tons produced from this facility indicates the dry tons from this facility should be
increased to 80 dry tons based on previous years application information.

Residuals Sampling Plan

WWTP SAMPLING PLAN — PLURIS WEBB CREEK WWTP
Annually, multiple grab residual solid samples are collected from the sludge holding tank. These
samples are composited for nutrient and metal analyses. The composited sample is mixed to keep the
solids suspended and containers filled for this analysis. Lime stabilization occurs when the sludge
holding tank reaches capacity. Lime is added to reach proper stabilization requirements for vector
attraction and pathogen reduction. Field measurements of pH and temperature are collected for each
stabilization event to insure pH requirements are met. pH values are later temperature corrected.
Annually, or when the residual solids are to be land applied if application occurs less than annually,
a composite residual solid sample will be analyzed for: Arsenic, Cadmium, Copper, Lead, Mercury,
Molybdenum, Nickel, Selenium, Zinc, Aluminum, Ammonia — Nitrogen, Calcium, Nitrate -Nitrite,
Nitrogen, Magnesium, % Total Solids, pH, Phosphorus, Potassium, TKN, and Sodium. From this
information, the Plant Available Nitrogen (PAN) will be calculated. Once a permit cycle, a composite
TCLP sample will be collected to include:
Arsenic
Hexachlorobenzene
ph for Corrosivity
Barium
Hexachloro-1,3-Butadiene
Benzene
Hexachloroethane
Flash point for ignitability
Cadmium
Lead
Carbon Tetrachloride
Lindane
Sulfides and Cyanides for reactivity
Chlordane
Mercury
1,2-Dichloroethane
Chlorobenzene
Methoxychlor
1,1-Dichloroethylene
Chloroform
Methyl Ethyl Ketone
2,4-Dinitrotoluene
Chromium
Nitrobenzene
Endrin
m-Cresol
Pentachlorophenol
Heptachlor and its Hydroxide
o-Cresol
Pyridine
Trichloroethylene
p-Cresol
Selenium
2,4,5-Trichlorophenol
Cresol
Silver
2,4,6-Trichlorophenol
2,4-D
Tetrachloroethylene
2,4,5-TP (Silvex)
1,4-Dichlorobenzene
Toxaphene
Vinyl Chloride

Analytical Data from Pluris Webb Creek WWTP
TCLP, Fecal, Nutrient & Metal

Wastewater Treatment Plant
Webb Creek WWTP
Sneads Ferry, North Carolina
Triple S Farms & Cleaning, Inc
Annual 2023
Date Reported: 11/21/2023 Report No: WC 2023-24789
Note All Units in Pounds Per Dry Ton
Macro Nutrients Physical Characteristics
PAN Surf.
35.008
PAN Inj.
37.278
P
63.600
K
7.260
Lime (estimated)
0.000
Secondary Nutrients
Calcium
38.800
Magnesium
3.140
Sodium
11.560
SAR
1.346
Chloride
0.000
Iron
0.000
Alumium
30.600
Manganese
0.000
Boron
0.000
Sulfur
0.000
% Solids
1.58
pH
7.440
Min Rate
0.300
Metals
Arsenic
0.029
Cadmium
0.029
Chromium
0.046
Copper
0.292
Lead
0.029
Mercury
0.003
Molybdenum
0.029
Nickel
0.029
Seleniun
0.029
Zinc
3.980

Facility:
Source:
Location:
Contractor:
Type of Analysis:
Report No:
Date Sampled:
Date Reported:
Reporting Period:
Webb Creek WWTP
Webb Creek WWTP
Sneads Ferry, North Carolina
Triple S Farms & Cleaning, Inc
Wastewater Treatment Plant
WC 2023-24789
10/24/2023 Type of Stabilization::Lime
11/21/2023
Annual 2023
Parameter
%
PPM
Dry Weight
EPA
Monthly Limits
Solids*
1.580
Nitrogen (TKN)*
5.340
53,400.00
Phosphorus
3.180
31,800.00
Potassium
0.363
3,630.00
Sulfur
0.00
Calcium
1.940
19,400.00
Magnesium
0.157
1,570.00
Sodium
0.578
5,780.00
Iron
---
Aluminum
---
15,300.000
Manganese
---
Copper
---
146.000
1,500
Zinc
---
1,990.000
7,500
Ammonia Nitrogen*
0.227
2,270.000
Nitrate N / Nitrite N*
---
1,030.000
Cadmium
---
14.700
39
Chromium
---
23.000
1,200
Nickel
---
14.700
420
Lead
---
14.700
300
Arsenic
---
14.700
41
Mercury
---
1.330
17
Selenium
---
14.700
100
pH
7.440
Calcium Carbonate Eq. (est)
0.000
Organic Nitrogen
5.113
Molybdenum
---
14.700
75
Chloride
---
Boron
Available P2O5
Specific Gravity
8.340

F""07 -.-Oqql
Environmental Chemists,
Inc.
envirochem
6602 Windmill Way, Wilmington, NC 28405 , 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington
Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
info®environmentalchemists.com
Pluris LLC.
Date of Report: Nov 21, 2023
P. O. Box 856
Customer PO #:
Sneads Ferry NC 28460
Customer ID: 09110001
Attention:
Report #: 2023-24789
Project ID: Webb Creek Sludge
Lab ID Sample ID:
Collect DateiTime Matrix Sampled by
23-60185 Site: Sludge
10/24/2023
8:30 AM Solid/Sludge Client
Test
Method
Results Date Analyzed
Chlordane (TCLP)
SW-848 80818
<0.02 mg/L
10/27/2023
Endrin (TCLP)
SW-846 80810
<0.0005 mg/L
10/27/2023
Heptachlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
10/27/2023
Heptachlor epoxide (TCLP)
SW-846 8081 B
<0.0005 mg/L
10/27/2023
Lindane (TCLP)
SW-846 8081 B
<0.0005 mg/L
10/27/2023
Methoxychlor (TCLP)
SW-846 8081 B
<0.0005 mg/L
10/27/2023
Toxaphene (TCLP)
SW-846 $081 B
<0.05 mg/L
10/27/2023
2,4,5-TP (TCLP)
SW-846 8151 A
<0.003 mg/L
10/30/2023
2,4-1) (TCLP)
SW-8468151 A
<0.003 mg/L
10/30/2023
1,4-Dichlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
10/30/2023
2,4,5-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
10/30/2023
2,4,6-Trichlorophenol (TCLP)
SW-846 8270 E
<0.050 mg/L
10/30/2023
2,4-Dinitrotoluene (TCLP)
SW-846 8270 E
<0.050 mg/L
10/30/2023
Cresol (TCLP)
SW-846 6270 E
<0.050 mg/L
10/30/2023
Hexachloro-1,3-butadiene (TCLP)
SW-846 6270 E
<0.050 mg/L
10/30/2023
Hexachlorobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
10/30/2023
Hexachloroethane (TCLP)
SW-846 8270 E
<0.050 mg/L
10/30/2023
m + p-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
10/30/2023
Nitrobenzene (TCLP)
SW-846 8270 E
<0.050 mg/L
10/30/2023
o-Cresol (TCLP)
SW-846 8270 E
<0.050 mg/L
10/30/2023
Pentachlorophenol (TCLP)
SW 8468270 E
<0.250 mg/L
10/30/2023
Pyridine (TCLP)
SW-846 8270 E
<0.050 mg/L
10/30/2023
1, 1 -Dichloroethylene (TCLP)
SW-846 Method82WD
< 0.01 mg/L
11/1/2023
1,2-Dichloroethane (TCLP)
SW-846 Method82600
< 0.01 mg/L
11/1/2023
Benzene (TCLP)
SW-846 Method82ND
<0.01mg/L
11/1/2023
Carbon Tetrachloride (TCLP)
SW-848Method 82600
< 0.01 mg/L
11/1/2023
Report 9: 2023.24789
Page 1 of 4

pppom'—.— -71
Environmental Chemists,
Inc.
envirochem
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
`r
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMIS
info na environmentalchemists.com
Pluris LLC.
Date of Report: Nov 21, 2023
P. O. Box 856
Customer PO #:
Sneads Ferry NC 28460
Customer ID: 09110001
Attention:
Report #: 2023-24789
Project ID: Webb Creek Sludge
Chlorobenzene (TCLP)
SW-846 Method 8260D < 0.01 mg/L
11/1/2023
Chloroform (TCLP)
SW-846 Method 8260D < 0.01 mg/L
11/1/2023
Methyl ethyl ketone (TCLP)
SW-846 Method 0260D < 0.05 mg/L
11/1/2023
Tetrachloroethylene (TCLP)
SW-846 Method 8260D < 0.01 mg/L
11/1/2023
Trichloroethylene (TCLP)
SW-846 Method 8260D < 0.01 mg/L
11 /112023
Vinyl Chloride (TCLP)
SW-846 Method 8260D < 0.01 mg/L
11 /112023
RCI
Cyanide
SM 4500 CN D-2016
1.00 mg/kg
11 /06/2023
Sulfide
SM 4500 S D-2011
8.08 mg/kg
11 /08/2023
Ignitability
SW 846 method 1010
>158 OF
11 /08/2023
Sludge Residuals
Aluminum
EPA 200 7, Rev. 4 4. 1994
15300mg/kg
11/01/2023
Arsenic
EPA 200 7, Rev. 4 4.1994
<14.7 mg/kg
11 /01/2023
Cadmium
EPA 200 7, Rev 4 4, 1994
<14.7 mg/kg
11 /01/2023
Calcium
EPA 200 ?,Rev 4 4, 1994
19400 mg/kg
11/01/2023
Chromium
EPA 200 7, Rev 4 4, 1994
23.0 mg/kg
11/01/2023
Copper
EPA 200 7, Rev. 4 4, 1994
146 mg/kg
11/01/2023
Lead
EPA 200 7, Rev 4.4, 1994
<14.7 mg/kg
11/01/2023
Magnesium
EPA 2007, Rev 4.4, 1994
1570 mg/kg
11/01/2023
Molybdenum
EPA 2007, Rev 4.4, 1994
<14.7 mg/kg
11/01/2023
Nickel
EPA 200 7, Rev 4.4, 1994
<14.7 mg/kg
11/01/2023
Potassium
EPA 200 7, Rev 4.4, 1994
3630 mg/kg
11/01/2023
Selenium
EPA200.7, Rev 4.4. 1994
<14.7 mg/kg
11/01/2023
Sodium
EPA 2007, Rev. 4.4, 1994
5780 mg/kg
11/02/2023
Zinc
EPA 200.7, Rev 4.4, 1994
1990 mg/kg
11 /01/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2
1030 mg/kg
10/25/2023
Total Solids (%)
SM 2540 B
1.58 %
10/26/2023
Ammonia Nitrogen
SM 45DO NH3 C-2011
2270 mg/kg
10/25/2023
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
53400 mg/kg
10/25/2023
Total Phosphorus
SM 4500 P (F-H)-2011
31800 mg/kg
10/31/2023
Report M. 2023-24789
Page 2 of 4

7
enviro ,hem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infon,q environmcntalchemists com
Pluris LLC. Date of Report: Nov 21, 2023
P. O. Box 856 Customer PO #:
Sneads Ferry NC 28460 Customer ID: 09110001
Attention: Report #: 2023-24789
Project ID: Webb Creek Sludge
pH SW 846 Method 9045D 7.44 units 10/27/2023
Result estimated. Analyzed out of 15 minutes hold time.
Mercury
SW-846 7471 B
<1.33 mg/kg
11012023
TCLP Metals
Arsenic (TCLP)
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
11/02/2023
Barium (TCLP)
EPA 200.7, Rev. 4.4, 1994
<1.0mg/L
11/02/2023
Cadmium (TCLP)
EPA 200.7. Rev. 4.4,1994
<1.0 mg/L
11/02/2023
Chromium (TCLP)
EPA 200.7, Rev. 4.4, 1994
<1.0 mg/L
11/02/2023
Lead (TCLP)
EPA 200.7. Rev 4.4. 1994
<1.0 mg/L
11/02/2023
Selenium (TCLP)
EPA 200 7, Rev 4.4. 1994
<1.0 mg/L
11/02/2023
Silver (TCLP)
EPA 200 7, Rev 4.4, 1994
<1.0 mg/L
11/02/2023
Mercury (TCLP)
EPA 245 1
<0.0002 mg/L
11/02/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-60186 Site: 001
10124/2023 8.31 AM
Solid/Sludge Client
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 B
1.86 %
10/26/2023
Fecal Density
SM 9221C E MPN 24 hr 503
190861 MPN/g
10/24/2023
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
23-60187 Site: 002
10/24/2023 8:32 AM
Solid/Sludge Client
Test
Method
Results
Date Analyzed
Total Solids (%)
SM 2540 B
1.92 %
10/26/2023
Fecal Density
SM 9221C E MPN 24 hr 503
833334 MPN/g
10/24/2023
Lab ID Sample ID:
Collect DatelTime
Matrix Sampled by
23-60188 Site: 003
10/24/2023 8:33 AM
Solid/Sludge Client
Test
Method
Results
Date Analyzed
Total Solids (%) SM 2540 B 1.71 % 10/26/2023
Fecal Density SM 9221C E MPN 24 hr 503 538012 MPN/g 10/24/2023
Hop011 It 2023-24789 Page 3 of 4

roo�' -- —1 �7 Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab • 910.392.4424 Fax
4, 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infol,�;environmentalchemists.com
Pluris LLC. Date of Report: Nov 21, 2023
P. O. Box 856 Customer PO #:
Sneads Ferry NC 28460 Customer ID: 09110001
Attention: Report #: 2023-24789
Project ID: Webb Creek Sludge
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-60189 Site: 004 10/24/2023 8:34 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
Lab ID Sample ID:
23-60190 Site:005
SM 2540 8
SM 9221C E MPN 24 hr 503
1.80 % 10/26/2023
888889 MPN/g 10/24/2023
Collect Date/Time Matrix Sampled by
10/24/2023 8:35 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.73 % 10/26/2023
Fecal Density SM 9221C E MPN 24 hr 503 312139 MPN/g 10/24/2023
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-60191 Site: 006 10/24/2023 8:36 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%) SM 2540 B 1.54 % 10/26/2023
Fecal Density SM 9221C E MPN 24 hr 503 155845 MPN/g 10/24/2023
Lab ID Sample ID:
23-60192 Site:007
Collect Date/Time Matrix Sampled by
10/24/2023 8:37 AM Solid/Sludge Client
Test Method Results Date Analyzed
Total Solids (%)
Fecal Density
SM 2540 B
SM 9221C E MPN 24 hr 503
0.79 % 10/26/2023
303798 MPN/g 10/24/2023
Comment: Sludge residuals, except pH, reported on a dry weight basis. pH reported on an as received basis.
Reviewed by:
- - ---- ----- Page 4 of 4

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Client: � W0 CA kc-eV Date: AJD�,29 �23 Report Number:— 2023- g-9
Receipt of sample:
ECHEM Pickup Client Delivery ❑ UPS ❑ FeclEx ❑ Other ❑
❑ YES ❑ NO
N/A 1. Were custody seals present on the cooler?
❑ YES ❑ NO
N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt `C
How temperature taken:
❑ Temperature Blank O Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
19 YES ❑ NO
3. If temperature of cooler exceeded VC, was Project Mgr./QA notified?
0 YES ❑ NO
4. Were proper custody procedures (relinquished/received) followed?
IS.
91 YES ❑ NO
Were sample ID's listed on the COC?
O YES ❑ NO
6. Were samples ID's listed on sample containers?
❑x YES ❑ NO
7. Were collection date and time listed on the COC?
0 YES ❑ NO
8. Were tests to be performed listed on the COU
❑O YES
❑ NO
9. Did samples arrive in proper containers for each test?
O YES
❑ NO
10. Did samples arrive in good condition for each test?
❑x YES
❑ NO
11. Was adequate sample volume available?'
❑x YES
❑ NO
12. Were samples received within proper holding time for requested tests?
❑ YES
❑ NO
13. Were acid preserved samples received at a pH of <27
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES ❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES ❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES ❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
11 YES 10 NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
(Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s)
were received incorrectly preserved and were adjusted accordingly
by adding (circle one):
H2SO4 HNO3 HCl NaOH
Time of preservation:
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s)
were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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