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HomeMy WebLinkAboutNC0089176_Residuals Certification_20161031Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURC&GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Hoke WWTP l N C &O 8117(,) 2. Facility permit holder is: ❑ Federal, X State, ❑ Local Government, or [] Private. Facility permit issued by: X Div. of Water Resources, ❑ Div. of Environmental Health, or Q Other (explain: . 3. Facility contact person and title:Donavan Dennison Complete mailing address: 736 Ellis Rd. City: Lumber Bridge State: NC Zip: 28357 Telephone number: (910) 875-4700 E-mail address: F__� 4. Facility physical address: 736 Ellis Rd. City: Lumber Bridge State: NC Zip: 28357 Coordinates: Latitude: ❑° f 1, ❑,, Longitude: ❑° n' R,, Datum: Level of accuracy: Method of measurement: 5. Purpose of the facility: treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, [] treatment of potable water, ❑ treatment of 100% industrial wastewater, Ej treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: % industrial and �� % domestic)Fj ct Zpl other (explain: i77 ). 6. Does the facility have an approved pretreatment program: X Yes ❑ No 7. Facility permitted/design flow: 1.5 MGD and facility avera*200dry flo . 6 MGD 8. Average amount of residuals being generated at this facili tons per year. 9. Specify the following regarding treatment and storage voluable at t e acility: Type and volume of residuals treatment: 2.6 MG Aerobic digester Type and volume of residuals storage (i.e., outside of residuals treatment units):.5 MG Aerobic digester H. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: IN 40 CFR Part 503 or ❑ 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: M Biological ❑ Non -Biological FORM: RSC 06-16 Pagel of 5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD.in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: Q yes X no. If yes, list the number(s): F--Z b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes X no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Pace and Date of analysis: 3/05/2019 Passed.corrosivity test: X yes Q no. pH: s.u. (2 <�DH < 12.5) / Passed ignitability test:. X yes 0 no. Flashpoint:>Z00 OF (> 1ZOO ) Passed reactivity test: Xyes ❑no. HCN: <1 itig/kg (<250) & H- <10 g (<500J✓ TCLP Parameter Limit (Mg/7) Result (Mg/1) TCLP Parameter Limit (Mg/1) Result (Mg/1) . Arsenic 5.0 <.05 Hexachlorobenzene 0.13 <.05 Barium 100.0 <,25 Hexachloro-1,3-Butadiene 0.5 <.05 Benzene 0.5 <.I Hexachloroethane 3.0 <.05 Cadmium 1.0 <.005 Lead 5.0 <.025 Carbon Tetrachloride 0.5 <.1 Lindane 0.4 <.0005 Chlordane 0.03 <.003 Mercury 0.2 <.0002 Chlorobenzene 100.0 <.1 Methoxychlor 10.0 <1 Chloroform 6.0 <.1 Methyl Ethyl Ketone 200.0 <.2 Chromium 5.0 <.05 ✓ Nitrobenzene 2.0 <.05 m-Cresol 200.0 <.05 Pentachlorophenol 100.0 <.I o-Cresol 200.0 <.05 Pyridine 5.0 <.05 p-Cresol 200.0 <.05 Selenium 1.0 <:1 Cresol 200.0 <.05 Silver 5.0 <.025 JT 2,4-D 10.0 <,005 Tetrachloroethylene 0.7 <.1 1,4-Dichlorobenzene 7.5 <.05 Toxaphene 0.5 <.003 1,2-Dichloroethane 0.5 <,1 Trichloroethylene 0.5 <.1 1,1-Dichloroethylene 0.7 <.1 2,4,5-Trichlorophenol 400.0 <.05 2,4-Dinitrotoluene 0.13 <.05 2,4,6-Trichlorophenol 2.0 <.05 Endrin 0.02 <.0005 2,4,5-TP (Silvex) 1.0 <.01 Heptachlor and its Hydroxide 0.008 <.0005 Vinyl Chloride 0.2 <.1 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Pace and Date of analysis: 3/05/2019 Parameter Ceiling Concentration Limits (Class-4 & ClassB) (mg/kg) Monthly Average Concentration Limits (Class A Only) (mg/kg) Result (mg/kg) Arsenic 75 41 .0188 Cadmium 85 39 .0153 Copper 4,300 1,500 13.1 Lead 840 300 .12 Mercury 57 17 .0104 Molybdenum 75 n/a .0482 Nickel 420 420 .124 Selenium 100 100 .0622 Zinc 7,500 2,800 8.27 b. For Surface Disposal Unit Oandfrlb: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) [] > 0 but < 25 30 200 210 Q > 25 but < 50 34 220 240 �] > 50 but < 75 39 260 270 > 75 but < 100 46 300 320 [( > 100 but < 125 53 360 390 0 >_ 125 62 450 420 Result (mg/kg) 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 1.74 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Pace and Date of analysis: 3/05/2019 Parameter Result (mglkg) Aluminum 855 Ammonia -Nitrogen 18.6 Calcium 523 Magnesium 81.5 Nitrate -Nitrite Nitrogen .083 pH (Standard Unit) 7 Phosphorus 299 Potassium 96 -7 Sodium 46.5 Total Kjeldahl Nitrogen 511 c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): NA [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: .1 %. This rate is a (check one): X default value, or [( actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: NA e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (111 Year PAN Five -Year Maximum Adjusted PAN (mg/kg) (mg1kg) Surface Injection/Incorporation 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: None 7. Pathogen Reduction: Per 15A NCAC 02T.1106 specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): [� Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment. ❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. X Alternative 5 [15A NCAC 02T. 1 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: X composting, 0 heat drying, ❑ heat treatment, [] thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. - b. For Land Application of Class B: [I. Alternative 1 [15A NCAC 02T.1106(c)(1)] - Fecal Coliform Density Demonstration. EJ Alternative 2 [15A NCAC 02T.1106(c)(2)] -Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion, [[ composting, or ❑ lime stabilization. c. For Surface Disposal: ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item H. 7b. above. Exempt -If Daily Cover Alternative is chosen in Item H.8. below [15A NCAC 02T.1106(a)(2)]. C7 Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.1107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). [( Alternative 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). Q Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion)., X Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. ❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. EJ Alternative 7 [15A NCAC 02T.1107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals. Alternative 9 [15A NCAC 02T. 1 107(a)(9)] - Injection. Alternative 10 [15A NCAC 02T. I 107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. 10 A Q IT A. -7 cl., 7_­ IF v It: -4 i Al" lk (P -us H Facility, Longitude: 79* 6'6" 790 6! 211 W qW. - Strewn Class: B NorthFacility Location Subbasim 03-06-15 HUC: 03030004 Hoke County WWTP NCO089-176 -Receiving Stream: Rockfish Creek Hoke County Permit NCO089176 STATE OF NORTHI 'MOLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES - DIVISION OF WATER QUALITY TO DISCHARGE WASTEWATER UNDER THE NATIONAL POLLUTANT DISCHARGE1 Ei,I1ViiI�l`A 'I S TEM! In compliance with the provision of North Carolina.Pen�l Statute 143-215�1,, Athcr;lav�iul standards sad regulations promulgated stiti'a�Qopfi�i`lipti a Igo tti b&lma.19i i onztiental Management Commission, and the Federal Water Pollution Control Act, as amended, . Hoke County is hereby authorized to discharge wastewater .from the Hoke County Wastewater Treatment Plant Ellis Road near Sandy Grove Hoke County to receiving waters designated as the Rockfish Creek within the Cape Fear River Basin in accordance with effluent limitations, monitoring requirements, and other conditions set forth in Parts L II, III, and IV hereof. This permit shall become February 1, 2013. This permit and authorization to discharge shall expire at midnight on October 31, 2016. Signed this day January 9, 2013. es Wakild, P.E., Director Division of Water Quality By Authority of the Environmental Management Commission SUPPLEMENT TO PERMIT COVER SHEET Permit NCO089176 t H*-Pount3r is hereby auth6riied to: 1. Upon approval Of an Authorization to COmtrudtl-4--thd 'Division of Water Quality for a 1.5 MGD domestic, wastewater treatment facility, and aft submittal of the signed Engineering Certificate, 2. Operate a 1.S:ME#D:dorn4�tia fxgabm?rtY ': dy, 3. Discharge from said treatment works itt the location specified on the attached Map into Rockfish Creek, a class B water in the Cape Fear River Basin, ON SUPPLEMENT TO PERMIT COVER SKEET Permit NC0089176 Way, is hereby authorized to: 1. Upon approval of an Authorization to ConstrudCl* t6"Division of Water Quality for 1.5 MGD domestic wastewater treatment facility, and after submittal of the signed Engineering Certificate, 2. Operate a 1.5.M�D :dot "do ", * fhWiW ; - Iiocateti` t th6 %ire Count 9 `, . • , .. .. -. y..'EIIi�Ttoednee a"r�Saady,CrrovewnkIo�Coiu�ty,, . . Y' •1• .3.. f' 3. Discharge from said treatment works at the location specified on the attached map into Rockfish Creek, a class B water in the Cape Fear River Basin. .. . McGILL _ The compost people® Quantitative justification for residuals production rate A quantitative justification for the value provided in Item 1.8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. Hoke County WTP (NC0089176) Design flow of 1.50 MGD and an average daily flow of 0.356 MGD 241 dry tons annually to be processed by McGill Environmental Systems McGill-Delway j (0) 910-532-2539 j (F) 910-532-2542 1 www.mcgilicompost.com 1100 Herring Rd I Delway Community I Rose Hill, NC 28458 MI't �% t Stl � The compost people"'' Sampling Plan Delway Compost Facility 1100 Herring Road Rose Hill, NC 28458 WQ0006816 Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. 1) Compost is sampled monthly prior to distribution for metals, inert contamination, pathogens and nutrients. 2) Samples are sent to A & L Greatlakes Laboratories, 3505 Conestoga Drive, Ft. Wayne, IN 46808. 3) Samples are collected at the screened compost stockpile located adjacent to the screening plant. 4) Pathogen (PFRP) and Vector Attraction Reduction (VAR) are achieved prior to distribution during the composting process. PFRP and VAR records are included in the annual report submitted to NCDEQ. MCo8@-Delway I () 910-532-2539 I Q_F 910-532-2542 I vuvverv.saac!�u@Bcs�rsu@a¢r t.carba 1100 F 1prrinn Rri I nni%„ aceAna ljftaI www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Hoke - Pre Acceptance Water Pace Project No.: 92420080 Sample: HOKE Lab ID: 92420080001 Collected: 03/05/19 13:00 Received: 03/05/19 16:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 TCLP Pesticides RVE Analytical Method: EPA 8081B Preparation Method: EPA 3510C Leachate Method/Date: EPA 1311; 03/08/1915:44 gamma-BHC (Lindane) Chlordane (Technical) Endrin Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) 8161A Cl Acid Herbicides TCLP 2,4-D 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) ND ug/L 0.50 1 03/11/1917:47 03/12/1916:51 58-89-9 ND ug/L 3.01/ 1 03/11/1917:47 03/12/1916:51 57-74-9 ND ug/L 0.50 1 03/11/1917:47 03/12/1916:51 72-20-8 ND ug/L 0.50 / 1 03/11/1917:47 03/12/1916:51 76-44-8 ND ug/L 0.501 1 03/11/1917:47 03/12/1916:51 1024-57-3 ND ug/L 1000 1 03/11/1917:47 03/12/1916:51 72-43-5 ND ug/L 3.0 1 03/11/1917:47 03/12/1916:51 8001-35-2 55 % 10-138 1 03/11/1917:47 03/12/1916:51 2051-24-3 59 % 10-110 1 03/11/1917:47 03/1211916:51 877-09-8 Analytical Method: EPA 8151A Preparation Method: EPA 8151A Leachate Method/Date: EPA 1311; 03/11/1914:00 Initial pH: 7.2; Final pH: 7.08 ND mg/L 0.0050 1 03/12/19 11:00 03/13/19 00:55 94-75-7 ND mg/L 0.010 1 03/12/19 11:00 03/13/19 00:55 93-72-1 114 %. 10-155 1 03/12/19 11:00 03/13/19 00:55 19719-28-9 6010 MET ICP, TCLP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Leachate Method/Date: EPA 1311; 03/13/19 21:30 Initial pH: 7.05; Final pH: 5.5 Arsenic ND mg/L 0.050J 1 03/16/19 19:50 03/18/19 22:25 7440-38-2 Barium ND mg/L 0.25✓ 1 03/16/19 19:50 03/18/19 22:25 7440-39-3 Cadmium ND mg/L 0.0050'/ 1 03/16/19 19:50 03/18/19 22:25 7440-43-9 Chromium ND mg/L 0.050vl 1 03/16/19 19:50 03/18/19 22:25 7440-47-3 Lead ND mg/L 0.025v/ 1 03/16/19 19:50 03/18/19 22:25 7439-92-1 Selenium ND mg/L 0.10V / 1 03/16/19 19:50 03/18/19 22:25 7782-49-2 Silver ND mg/L 0.025v 1 03/16/19 19:50 03/18/19 22:25 7440-22-4 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Aluminum 855000 v ug/L 1000 10 03/14/19 07:47 03/15/19 16:09 7429-90-5 Arsenic o18.8 J ug/L 10.0 1 03/14/19 07:47 03/14/19 22:52 7440-38-2 Cadmium , 015.31 ug/L 1.0 1 03/14/19 07:47 03/14/19 22:52 7440-43-9 Calcium 523000 ✓ ug/L 1000 10 03/14/19 07:47 03/15/19 16:09 7440-70-2 Copper 13,100 /// ug/L 50.0 10 03/14/19 07:47 03/15/19 16:09 7440-50-8 Lead 12M / ug/L 5.0 1 03/14/19 07:47 03/14/19 22:52 7439-92-1 Magnesium 81�00 ✓ ug/L 100 1 03/14/19 07:47 03/14/19 22:52 7439-95-4 Molybdenum v48.2✓ ug/L 5.0 1 03/14/19 07:47 03/14/19 22:52 7439-98-7 Nickel Potassium 124 ✓/ 96000✓/ ug/L ug/L 5.0 5000 1 1 03/14/19 07:47 03/14/19 07:47 03/14/19 22:52 03/14/19 22:52 7440-02-0 7440-09-7 Selenium .062.2 J ug/L 10.0 1 03/14/19 07:47 03/14/19 22:52 7782-49-2 Sodium 46500 ug/L 5000. 1 03/14/19 07:47 03/14/19 22:52 7440-23-5 Zinc 8�270J ug/L 10.0 1 03/14/19 07:47 03/14/19 22:52 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/19/2019 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 32 acieMapical www.pacelabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Hoke - Pre -Acceptance Water Pace Project No.: 92420080 Sample: HOKE Parameters Lab ID: 92420080001 Collected: 03/05/1913:00 Received: 03/05/1916:40 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Qual 160.4 TVS and 2540B TS Analytical Method: EPA 160.4 / SM254OB-2011 Total Solids 17400 mg/L 2500 1 03/12/19 01:26 Total Volatile Solids 12600 mg/L 2500 1 03/12/19 01:26 D6 9040 pH Analytical Method: EPA 9040C pH at 25 Degrees C 7.0 Std. Units 0.10 1. 03/10/19 12:11 H3 350.1 Ammonia Analytical Meth d: EPA 350.1 Rev 2.01993 Nitrogen, Ammonia 18.6 mg/L 0.50 5 03/12/19 14:48 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.01993 Preparation Method: EPA 351.2 Rev 2.0 1993 Nitrogen, Kjeldahl, Total 611 V/ mg/L 50.0 5 03/09/19 02:55 03/12/19 01:05 7727-37-9 363.2 Nitrogen, N021NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993 Nitrogen, NO2 plus NO3 0.083 ✓ mg/L 0.040 1 03/11/19 15:39 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Phosphorus 299\/ mg/L .10.0 200 03/11/1920:19 03112/1919:32 7723-14-0 M6 5310B TOC Analytical Method: SM 531 OB-2011 Total Organic Carbon 1610 mg/L 50.0 50 03/12/19 03:07 7440-44-0 733C S Reactive Cyanide Analytical Method: EPA 9014 Preparation Method: SW-846 7.3.3.2 Cyanide, Reactive ND mg/kg 1.0 � 1 03/08/19 20:00 03/08/19 21:03 734S Reactive Sulfide Analytical Method: SM 4500S2F-00 Preparation Method: SW-846 7.3.4.2 Sulfide, Reactive ND mg/kg 1071 03/08/19 20:00 03/08/19 20:04 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/19/2019 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 32 'wxAnalj6calc wmpacelabacom Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Hoke - Pre -Acceptance Water Pace Project No.: 92420080 Sample: HOKE Parameters Lab ID: 92420080001 Collected: 03/05/19 13:00 Results Units Report Limit DF Received: 03/05/19 16:40 Matrix: Water Prepared Analyzed CAS No. Qua[ 7470 Mercury, TCLP Analytical Method: EPA 7470A Preparation Method: EPA 7470A Leachate Method/Date: EPA 1311; 03/13/19 21:30 Initial pH: 7.05; Final pH: 5.5 Mercury ND mg/L 0.00020 1 03/14/19 21:10 03/15/19 14:06 7439-97-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Mercury o 10.4 J ug/L 2.0 1 03/11/19 22:07 03/13/19 16:45 7439-97-6 D3 8270E TCLP RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C 1,4-Dichlorobenzene ND mg/L 0.050 1 03/15/19 18:58 03/18/19 11:43 106-46-7 2-Methy[phenol(o-Cresol) ND mg/L 0.050 1 03/15/19 18:58 03/18/19 11:43 95-48-7 L2 3&4-Methylphenol(m&p Cresol) ND mg/L 0.050 1 03/15/19 18:58 03/18/19 11:43 15831-10-4 Hexachloroethane ND mg/L 0.050 1 03/15/19 18:58 03/18/19 11:43 67-72-1 Nitrobenzene ND mg/L 0,050 1 03/15/19 18:58 03/18/19 11:43 98-95-3 Hexachloro-1,3-butadiene ND mg/L 0.050 1 03/15/19 18:58 03/18/19 11:43 87-68-3 2,4,6-Trichlorophenol ND mg/L 0.050 1 03/15/19 18:58 03/18/19 11:43 88-06-2 L2 2,4,5-Trichlorophenol ND mg/L- 0.050 1 03/15/19 18:58 03/18/19 11:43 95-95-4 L2 2,4-Dinitrotoluene ND mg/L 0.050 1 03/15/19 18:58 03/18/19 11:43 121-14-2 L2 Hexachlorobenzene ND mg/L 0.050 1 03/15/19 18:58 03/18/19 11:43 118-74-1 Pentachlorophenol ND mg/L 0.10 1 03/15/19 18:58 03/18/19 11:43 87-86-5 Pyridine ND mg/L 0.050 1 03/15/19 18:58 03/1811911:43 110-86-1 L2 Surrogates Nitrobenzene-d5 (S) 38 % 12-102 1 03/15/19 18:58 03/18/19 11:43 4165-60-0 H5 2-Fluorobiphenyl (S) 34 % 13-107 1 03/15/19 18:58 03/18/19 11:43 321-60-8 Terphenyl-d14 (S) 64 % 21-132 1 03/15/19 18:58 03/18/19 11:43 1718-51-0 Phenol-d6 (S) 12 % 10-110 1 03/15/19 18:58 03/18/19 11:43 13127-88-3 2-Fluorophenol (S) 5 % 10-110 1 03/15/19 18:58 03/18/19 11:43 367-124 SO 2,4,6-Tribromophenol (S) 12 % 27-108 1 03/15/19 18:58 03/18/19 11:43 118-79-6 SO 8260D MSV TCLP Analytical Method: EPA 82600 Benzene ND ug/L 100 20 03/18/19 23:14 71-43-2 2-Butanone (MEK) ND ug/L 200 20 03/18/19 23:14 78-93-3 Carbon tetrachloride ND ug/L 100 20 03/18/19 23:14 56-23-5 Chlorobenzene ND ug/L 100 20 03/18/19 23:14 108-90-7 Chloroform ND ug/L 100 20 03/18/19 23:14 67-66-3 1,4-Dichlorobenzene ND ug/L 100 20 03/18/19 23:14 106-46-7 1,2-Dichloroethane ND ug/L 100 20 03/18/19 23:14 107-06-2 1,1-Dichloroethene ND ug/L 100 20 03/18/19 23:14 75-35-4 Tetrachloroethene ND ug/L 100 20 03/18/19 23:14 127-18-4 Trichloroethene ND ug/L 100 20 03/18/19 23:14 79-01-6 Vinyl chloride NO ug/L 100 20 03/18/19 23:14 75-01-4 Surrogates 1,2-Dichloroethane-d4 (S) 91 % 70-130 20 03/18/19 23:14 17060-07-0 Toluene-d8 (S) 107 % 67-135 20 03/18/19 23:14 2037-26-5 4-Bromofluorobenzene (S) 99 % 70-130 20 03/18/19 23:14 460-00-4 1010 Flashpoint,Closed Cup Analytical Met d: EPA 1010A Flashpoint >200 deg F 70.0 1 03/11/19 14:13 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/19/2019 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 32 s aceAnalytical www.pace/abs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Hoke -.Pre-Acceptance Water Pace Project No.: 92420080 QC Batch: 462587 Analysis Method: EPA 7470A QC Batch Method: EPA7470A Analysis Description: 7470 Mercury Associated Lab Samples: 92420080001 METHOD BLANK: 2517819 Matrix: Water 1 Associated Lab Samples: 92420080001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L ND 0.20 03/1311916:40 LABORATORY CONTROL SAMPLE: 2517820 Spike' LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.2 90 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2517821 2517822 MS MSD 92420312050 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Mercury ug/L ND 2.5 2.5 2.1 2.6 84 104 75-125 22 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 03/19/2019 03:06 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 32 ZONINVA ud of Ysrht.",r -ce A� McGill Env. Sys, / Delway Plant Anthony'readwy 1100 Herring Rond Rose Hill, NC 28453 910-260-0121 Product Name: Delmly Soil Builder Sample Dam- 41311:9 9.45 Rayceh,e Date: 4/4119 10:00 AA1 A & L Lab Number. uz;w A 6, L ReporlNumber F19694-&zj:13 COMPOST TECHNICAL DATA SHE ET Ae.Ut'-L GrIpat Lakes Laboriatorles., Inc. Method IrtepOrted as (11UN11flywasure) T Tavf.Resafts ;rustResults f1hot, Nutrients: %wight, batiis %"Vvct weight basis Rro, dry weight basis Nitrogen TNIECC 04.02-D Total N 1.76 2.43 Phosphorus TNIECC-04.03=A PA 2.45 3.44 TMEICC 04.04-A K20 0.38 0.53 TNTECC, 04.05-CA On 5.66 7.96 'mqgjqsillni. TIME K05 41 M Mg 01.16 0.22 TAIFOC 03.09�- A Olo. wet %%vi lit twis 9 28.91 Yltefit -O.T-'g'3pJC:WttC1- Content 05.07-A, tea, (it), miglit basis 46.14 IME .1 T '6C 04 -1 units 7.7 S61ub.IeSkilts (elccmool rondlicljjqjp W Tit 04, 1.0-A -Tm.r-� 01m (Tnmlio.-Jcm) - - 9.25 M CC I- ;18 111.), dw basis I St Indicator (rampirome"Irl Stability RaIN9.1 Vol tion p)g.QOrC1g.Om/(h1y 0-9 TNIECC 05-.08-B ...... Very Stable till.4,•CO2wU g TS/day 0.9 0 (bionssay) .. . .. ....... 87 "Rolati%�C Seedling Vigor mm.r..cc 05.05-A. # average. % or cc mRil TME-CC07.01-B PASS-IFA19L.- per us t--.VA Class A sedmonella staridard,40 CFR k 503.32(a) PASS TIME -CC 04.06 i PASSIr-JUL: jxrpSE-lAC1a;-'K -i 4-T, Cad, Pb. 1-1c. i standard, 40 CFR § 503.13, PASS is Tables I and 3, 110, Ni, se, z?, 1 1117t.k"p1?"tq #Utlle US Cly"post4w, Cm11'1V;1'S;'S!Ca1 of Ta#11g 4'ssrlrarlce Progman have shown th.e committriefif to test Ifteir camp prr?itrects air p with Compost crud use imtractious, its a meats to tile needs qf Sea, of 'estirl:,"' McGill Ein. Sys, / Delwaay 1i.'lan t Anthony Tcachey 1100 F'Ierring Road Ruse Hill, NC 28e158 910-260-0121 lyrQducl.Nanrn,: Delway Sail .Boilder sarilnle Dale: 4r3119 9:45 Receive -Dale: 4/4/19.10:00.AM. A & L Lab Number.- 1560$ A & L Report Number: 1+1.9094-6513 ONJI.tt OST 11. ECHMC,L DATA SHEET A�,'.�'3si�_:;�A' •La�$';,ll_��CAa ti:��:a{'►relhl�inrrtrs , s�rsa. '1�RAC 7.!.a�.,...e.....,..' st... �:-.a. nn.--- on.' _ .....•...+....-....,... e'3(it()174dFR%7'AB91C%'{?l;S Il'.tL'.tOdOt� -- __—_ _ — .'."�!` .iiCIJ�PILl1�S (ltttllSl�rf7r!RSutyj - c,r v:xv yo.cv �a�m, Wl2raauF'V ��r -- `B�'tid.�L:S/IISS Ian (l;uirieuts: °lo; weight basis Not Reported ,\loisture,Contcnt- TM.ECC 03.09 ,A %,, wet weight basis 28.91 Crso rnic Matter Content THE -CC 05:07-A %,-dryNveight basis 46.14 R1:1 FM_ECC .04.1 I;A p1l units 7.7 I 564ible Saits (aiccrricrrl crnrrl rtFlrulrj� LG s J TMECC 04.10-A Win (mrnhostcrn) •9.25 6rdwa:siLc TIv1ECC 02.02-B % 9.5 mm (3/8 in.), dw basis 97:91 Sti}Uiltt�!�Cttdicator (r,'..t'pirolrretry) Stability IZatirtL': rnQ CQ -C/ OhVda f' t OtEvolutinn "11MECG 05.08-13 0.9 i -Very Stable mg COrOg TSIday } 0.9 ; ::���ittis;it��;C.iidicator (bioassay) ..., a _.....M:_....-.�..�......:..__ 1'erccnt Eittergettcc. 7'IvIECC 05.05-A. _..___.....__. .._..._......__. avcra= °fa of control €7 l�u lttGvc&edling Utpgr "RILT?C'C 05.057A { aycraf c'3o of control 0 St (ec t l'rttlrn rtis '1'iiI[50C 07.01�li PASS/FAIL. mr US -EPA Cl=A ! ' ScrhrtQltelltt :tr,ndnrd, ao Ci:lt? 503.32t1) PASS Tr cc 1vlelitls F TNIFICC 44.06 PASSTAIL: per US EPA Ckr.\-s A r PASS s �l s, Ccl, Ply, -- ' srnndprri;,tt) C[1t 303.13, i 1 Mo. !ti t.:: Se. Zr, . �y o . , r,rr rrrc s+y 4rrrntrn,,,rr :,.rtrurcrra aenrrrt..I esnnri Assurnrtce..t'rogrrmt rune Sgmr'1A lire corerertilrteetrt to rerrpresrribcil. brtsis.and rerun 1r1a�`Ilnt ri�ita; urrrtrr na11L'tnm�rnst etirl rice inrinretirisr_r; av a.nreausia:Getterseme llte neelk Of tireir com trnrl cuestnwem TMs.product meets orexceeds.tbe parameters of-Aw Acceptable Range orcotnpost charneteristic-s:contained. in [lie IJSCC's Consumer Compost UsO Program. Qoi�;pq.vvM.grec{Ierils. 1'ltis, -canpostsprdduct-has been satnpled'and tested as rcquired'by the Seal of'resting Assurance Program ol:tlte United States -Composting Council(USCC),,usingPertain, methods.frotn Hie""I'estN ethods for the Examination ofCornpostand Cornpostine' ninnual. Testrestrlls erc.-Miaflable.upan.request'by calling McGill Environmental Systerns 919-362-1 t61. 'rhe USCG makes no warranties regarding this product:;nr its:cot►tGrrts;-c)ualily,..or suitability :for and• particular use. 1't3i'IfCI(�IdlOillBJ'3f ]F li(ltlttrt-parlillAFllB = du Lu1�111os� rrs Pilo h�perifrc colll�nasl ril'ClTi7t'1L'B:s.fe'sPrtrd fur rt�idbliil Vire �selLd.Of Str'Blti 1lstildMrlPzPCe'-Al£iigraeu, or llle protrunz ljl generals log on to the Uri' Composfdirg ClJtwv;M %T/� ECC iveb-11te at Sri'tpr/fil'TYIWi►i;zear;rrr�Dlrtra/. r A ei x A q To: MCML - L 'ENV SYS/ -bE- LWAY PLANT ROSE HILL, NC 2,3458-7618 Attn: ANTHONY TEACH EY sample ID: DELW ' AY SOILBUILDEER Lab Nuffiber: 6" - 08 f S- For,:. ,,Oft 1UIL,Dt9l , S.7 . j.,A,.. :41 . . . . . 0: UZ COPY. HILARY NICHOLS Date sampled: 4/3/2019 Date Received: 4/4/20,19 Date Reported. 4/23/2019 Page: 1 of Moisture @ 70 C % TMECC 03.09-A Solids % .71JW ------ TIM ECC 03.09-A Total Nitrp&�L(N� 1.776, ---- . ..... 2.48 TMECC 04.02-D Ammonium Nitrogen (NH4-N) rtlg/kg 3436 TMECC'04.02-C ..P,�sphcTys (P) % 1.50 TMECC - 0 . 4 -03-A Phosphate (P205) . ...... % .2:45- 3A4, TMECC 04.03-A Potassium (K) % 0.44 TMECC 04.04-A Potash (K 0.53 TMECC 04.04-A .ML-Si Ir % 0.22 TMECC 04.054AG _Calcium (Ca) % 5 f5 7.96 TMECC 04.05-CA Arsenic 4-.62 US EPA 'SW846-6020 rAdmiurn -------- 0,584 US EPA S`01846-6020 -,Chromium mg/kg 5 8 26.-4 US EPA SW84,&6020 Cooper --------- - - .1 7 179 US EPA SW84-0-6010C Mercury mg/kg T_ OAA < 0.579 US EPA S11U846-6020 TMECC - fdst Mthods for the 'Ex6minaiionof Com ppsfln 9 " and Repart, Approved, By, P,, Val Dat F1 -6rt xp 904 '�513 'Ac6buq ffffuMber,s. To: N.JTCG1LL-;E DELINAY "KA-ANT C"A Attn: A N T H 0 NY TFA6 F I EY .5417!pl e 111 D LB u L26,-Nu-in.ber, 15'608 COP'* HILARY NICHOLS DateSaInDled: 4/3120-19 DaO Received:. V-4/2019 Date Reported: 4/23/2-019 p6ge, 2 of 3 Era," — ----- 4.74 US EPA SW846-6020 Nickel ^ 14.4 US EPA SW846-6' 020 Lead 1-2.4 US EPA'SW846-6020 Selenium US, EPA.SW846-6020 Zinc ----- dl, -- -- ---mg <9 483 US EPA SW846-6010C 503 Metals PASS/FAIL PASS EPA 503 eta_ Urnits PH TMECC 04. 11—A Soluble -Salts TMECC 04.1,0 A Fecal- to1lLon-nLFV1P'�!_------- <2 -2 h L-9221ETIVIECC Salmonella M'PA *Nlr <3 TM ECC 07.02 Pathogeh RedUcti..on -:1PASSLRAIL rASS 40 CFR 503 Class A Compost Ash (Ei'550 C 5186 TMECC-0i02'1-B a�niS' MItqr (.L01 .550. Pg. 32190 4.14 TMECC 05i07-A Tbtal, Oei�zihlc"Carbbn -(t) ...... 23.07 TMECC 04.01-A C. arb"PI onNit a UO 9.3:1 TMkC 05,02-A ifj -6'�if, -Ki aW t p, iviccc - Te5t'N;14e6' cmn, de­N w 2Y.36.:s w3i 7- _U sac MCGILL EN:V SYS DELWAY- PLANT For: DEDMAYSOILBUILDER -NICHOLS COPY: HILARY 11QQ: HERRING p1b ROSE HILL NC 28458 STA A.ttn: ANTHONYTEACHEY Date Sampled: 4/3/2019 •sarn.platb: DELWA-YSOILBUILDER Date Received: 4/4/2029 Lab NuMber: 15608 COMPOST NALMS DateReported: 4/23/2019 Page:. 3 os."3 % .. . .. .......... 0 100 TMECC 03.08-A Gert,nln4on - Emergence % 87 ' TMECC 05-05-A Gem% ---- -- ----- .. ...... .. ..... . ... TMECC 05.QS-A Ave Ht of -Seedlings In' Control --- centimeters - ---- --- '8.5 - ------ TMECC 05.05-A Ave Ht of Seedlings in Compost centimeters 0.00 . TMECC 0-.0--A Respiration - CO2 C/g TS mg CO2-C / TIS/Day ------ -- -- ...... 0.9 TMECC 05,08-B Respiration - CO27C19 OM -------- rng CQ2-C g OM/Dpy - ----- 0.9. ECC 05-08 -B index'' Venv Stable TMECC 05.08 R6tairied:pn,U.'S-. 2-inch Sieve ------ 0.00 TMECC 02-027B Retained on l U.S. 1-inch Sieve % 0.00 TMECC 02,02-B Retained on U;S, 5/8-inch Sieve % OM TMECC _0102-B ,TeLqined on U.S. 1/&-inch-Sleve % 2. 09 TMECC 02.02-8 .Retained an U.S. 1/4-inch Sieve % 6.81 TMECC 02.02-0 Retained on U.& 5/31- inch % ... ....... 14,95 --- ----- TM5CC 02.02-8 TMECC - T&StHMe-tho'ds.16r th6'Examination of C6-nQ'os Ing-and,CbrnPost VN16CC , The U.S. C . t, 01nPost.'A's Cou V'fi AIR ot �V r. LOH Sm wb=- ltzt�, EM! Freezer Cold Root! slomga Shelf �06qYRC:pW,)�,,q , , V. . 1* cbJuppm, 1)4, �/, i err/ -- " ac 1-1 . ..... . . . . . g iI Mn M.FIIS, //00 nIViI r-N Ci,*n I S,21noTe ID Mid GP;-c cerpo 7 1",Icota Gt3modsi Analysj� LAS USE 01ILY 'Al, opIibliType TmtyerZra(IdendtsrajobNmboraaw. "v"wWmeHonalT y 4-3 S*k o 0 Gmas% lFbIa TIA r0ofit 0 1 0 , 'Wit to 0. L —Ae cd ------ . vo 0, L -T SPXEJ-9Q' DED Rummmizaovmw ro sg7—,mUND,91?SMWY0 7HEuI0.-jFoS 1?0 -oiw 4 a 01� M VIDES use ec lei Dim, Time "Pa W, 4 4 ulawa TWO T40 4 IT# -------------- aA TY IR ra El R (it ze Z-- - AV4 LTQ QQ 91 CV :A w (A (1) -1 (D IT to. 66 > 0 cry 6", 104; McGill Environmental Temperature Report Batch Bay Initials Residuals: screened compost 19050119 13ay19 Start DatelTime: Comment 5/1/2019 9:47:25 AM Stop Date/Time. Comment 5/20/2019 8:22:16 AM Mruntime: 0 DatelTime Temperature 5/1/2019 5:00:00 PM 122 5/2/2019 5:00:00 PM 174 5/3/2019 5:00:00 PM 165 5/4/2019 5:00:00 PM 163 5/5/2019 5:00:00 PM 159 5/6/2019 5:00:00 PM 157 5/7/2019 5:00:00 PM 157 5/8/2019 5:00:00 PM 158 5/9/2019 5:00:01 PM 163 5/10/2019 5:00:00 PM 164 v 5/11/2019 5:00:00 PM 162 5/12/2019 5:00:00 PM 158 5/13/2019 5:00:00 PM 156 5/14/2019 5:00:00 PM 155 5/15/2019 5:00:00 PM 153 5/16/2019 5:00:00 PM 150 5/17/2019 5:00:00 PM 147 5/18/2019 5:00:00 PM 146 5/19/2019 5:00:00 PM 148 Unndnv "—, 9R 9n In McGill Environmental Temperature Report Batch Bay Initials Residuals: compost woodwaste biosolids . 24052219 Bay24 Start Date/Time: 5/22/2019 9:40:07 AM Stop Date/Time: 6/4/2019 7:42:51 AM Mruntime: 0 Date/Time 5/22/2019 5:00:00 PM 5/23/2019 5:00:00 PM 5/24/2019 5:00:00 PM 5/25/2019 5:00:00 PM 5/26/2019 5:00:00 PM 5/27/2019 5:00:00 PM 5/28/2019 5:00:00 PM 5/29/2019 5:00:00 PM 5/30/2019 5:00:00 PM 5/31/2019 5:00:00 PM 6/1/2019 5:00:00 PM 6/2/2019 5:00:00 PM Comment Comment Temperature 148 146 146 144 139 134 134 134 133 133 133 133 Tuesday, June 04, 2019 Pnov I of I McGill Environmental Temperature Report Batch Bay Initials Residuals: compost woodwaste bio6olids 07042619 Bay07 Start Date/Time: 4/26/2019 10:06:13 PM Stop Date-Mme: 5/8/2019 1:52:35 PM Mruntime: 0 Date/Time 4/27/2019 5:00:00 PM 4/28/2019 5:00:00 PM 4/29/2019 5:00:00 PM 4/30/2019 5:00:00 PM 5/1/2019 5:00:00 PM 5/2/2019 5:00:00 PM 5/3/2019 5:00:00 PM 5/4/2019 5:00:00 PM 5/5/2019 5:00:00 PM 5/6/2019 5:00:00 PM 5/7/2019 5:00:00 PM Comment Comment Temperature 148 147 147 147 n 139 135 134 134 134 134 134 Wedgy:esdav, Mav 08.2019 McGill Environmental Temperature Report' Batch Bay Initials Residuals: compost woodwaste biosolids 04032019 Bay04 Start Date/Time: Comment 3/20/2019 11:14:34 AM Stop Date -Mine: Comment 4/2/2019 7:39:33 AM Mruntime: 0 Date/Time Temperature 3/20/2019 5:00:00 PM 53 3/21/2019 5:00:00 PM 141 3/22/2019 5:00:00 PM 148 3/23/2019 5:00:00 PM 147 3/24/2019 5:00:00 PM 146 3/25/2019 5:00:00 PM 134 3/26/2019 5:00:00 PM n 134 3/27/2019 5:00:00 PM 134 ` 3/28/2019 5:00:00 PM 134 3/29/2019 5:00:00 PM 134 3/30/2019 5:00:00 PM 134 3/31/2019 5:00:00 PM 134 411 /2019 5:00:00 PM 126 T.. —l—, A --:I A) 1117n