NC0038377_J15060802 Report_20150902

Lab
DUI E Analytical Laboratory APagel1aof69
ENERGY
Order Number:
Project Name:
Customer Name(s):
Customer Address:
Lab Contact:
Report Authorized By:
(Signature)
Program Comments:
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
J15060802
MAYO STEAM - AB GW ASSESSMENT WATER
Tim Hunsucker, Jerry Wylie, Kathy Webb, John Toepfer
Mary Ann Ogle
Mary Ann Ogle
Phone: [phone]
Mary Ann Ogle
2015.07.03 12:35:31
-04'00' Date:
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
7/3/2015
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Collection
Sample ID Plant/Station Date and Time
Collected By
Sample Description
2015020818
MAYO STEAM
23-Jun-15 2:15 PM
Erin Black
MW-16S
2015020821
MAYO STEAM
23-Jun-15 12:30 PM
Erin Black
MW-16D
2015020822
MAYO STEAM
23-Jun-15 9:57 AM
Erin Black
MW-16BR
2015020823
MAYO STEAM
23-Jun-15 9:20 AM
Erin Black
ABMW-4BR
2015020824
MAYO STEAM
23-Jun-15 2:20 PM
Erin Black
MW-13BR
2015020837
MAYO STEAM
23-Jun-15 12:30 PM
Erin Black
MW-16D-Dup
2015020838
MAYO STEAM
23-Jun-15 9:24 AM
Erin Black
MW-3
2015020839
MAYO STEAM
23-Jun-15 4:30 PM
Erin Black
Filter Blank
2015020840
MAYO STEAM
23-Jun-15 4:30 PM
Erin Black
Equipment Blank
9 Total Samples
Analytical Lab
Page 2 of 69

Analytical Lab
Page 3 of 69
Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals 0 Yes ❑ No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes 0 No
All laboratory QA/QC requirements are acceptable. 0 Yes ❑ No
Report Sections Included:
E%-'] Job Summary Report
❑� Sample Identification
Technical Validation of Data Package
❑� Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
❑d Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
❑� Chain of Custody
❑� Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Mary Ann Ogle Date: 7/3/2015

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060802
Site: MW-16S
Collection Date: 23-Jun-15 2:15 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.144
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
13
mg/L
1
Sulfate
5.3
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
0.046
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.470
mg/L
0.01
Manganese (Mn)
0.276
mg/L
0.005
Strontium (Sr)
0.111
mg/L
0.005
Zinc (Zn)
0.065
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
9.57
mg/L
0.01
Magnesium (Mg)
4.01
mg/L
0.005
Potassium (K)
2.06
mg/L
0.1
Sodium (Na)
11.2
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.017
mg/L
0.005
Barium (Ba)
0.046
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.860
mg/L
0.01
Manganese (Mn)
0.260
mg/L
0.005
Strontium (Sr)
0.109
mg/L
0.005
Zinc (Zn)
0.039
mg/L
0.005
Sample #: 2015020818
Matrix: GW WW
Analytical Lab
Page 4 of 69
DF Method Analysis Date/Time Analyst
Vendor Method V_SHEALY
1
EPA 353.2
06/26/2015 11:28
LSTARLI
10
EPA 300.0
06/25/2015 15:57
BGN9034
1
EPA 300.0
06/25/2015 15:57
BGN9034
1
EPA 245.1
06/30/2015 10:21
ACPAYNE
1
EPA 245.1
06/30/2015 11:59
ACPAYNE
1
EPA 200.7
06/26/2015 10:03
FCJORDA
1
EPA 200.7
06/26/2015 10:03
FCJORDA
1
EPA 200.7
06/26/2015 10:03
FCJORDA
1
EPA 200.7
06/26/2015 10:03
FCJORDA
1
EPA 200.7
06/26/2015 10:03
FCJORDA
1
EPA 200.7
06/26/2015 10:03
FCJORDA
1
EPA 200.7
06/26/2015 10:03
FCJORDA
1
EPA 200.7
06/26/2015 11:54
FCJORDA
1
EPA 200.7
06/26/2015 11:54
FCJORDA
1
EPA 200.7
06/26/2015 11:54
FCJORDA
1
EPA 200.7
06/26/2015 11:54
FCJORDA
1
EPA 200.7
06/26/2015 13:53
FCJORDA
1
EPA 200.7
06/26/2015 13:53
FCJORDA
1
EPA 200.7
06/26/2015 13:53
FCJORDA
1
EPA 200.7
06/26/2015 13:53
FCJORDA
1
EPA 200.7
06/26/2015 13:53
FCJORDA
1
EPA 200.7
06/26/2015 13:53
FCJORDA
1
EPA 200.7
06/26/2015 13:53
FCJORDA

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060802
Site: MW-16S
Collection Date: 23-Jun-15 2:15 PM
Analyte
Result
Units Qualifiers
RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
4.35
ug/L
1
Copper (Cu)
4.18
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
1.23
ug/L
1
Nickel (Ni)
1.63
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
4.32
ug/L
1
Copper (Cu)
1.02
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
1.24
ug/L
1
Nickel (Ni)
1.57
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
0.303
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
100
mg/L
25
Total Carbon
TOC
0.508
mg/L
0.1
TOTAL SUSPENDED SOLIDS
TSS
< 5
mg/L
5
Sample #: 2015020818
Matrix: GW WW
Analytical Lab
Page 5 of 69
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/27/2015 16:19
SLS2560
1
EPA 200.8
06/27/2015 16:19
SLS2560
1
EPA 200.8
06/27/2015 16:19
SLS2560
1
EPA 200.8
06/27/2015 16:19
SLS2560
1
EPA 200.8
06/27/2015 16:19
SLS2560
1
EPA 200.8
06/27/2015 16:19
SLS2560
1
EPA 200.8
06/27/2015 16:19
SLS2560
1
EPA 200.8
06/27/2015 16:19
SLS2560
1
EPA 200.8
06/27/2015 16:19
SLS2560
1
EPA 200.8
06/27/2015 16:19
SLS2560
1
EPA 200.8
06/27/2015 16:19
SLS2560
1
EPA 200.8
06/27/2015 16:19
SLS2560
1
EPA 200.8
06/27/2015 16:19
SLS2560
1
EPA 200.8
06/27/2015 05:51
SLS2560
1
EPA 200.8
06/27/2015 05:51
SLS2560
1
EPA 200.8
06/27/2015 05:51
SLS2560
1
EPA 200.8
06/27/2015 05:51
SLS2560
1
EPA 200.8
06/27/2015 05:51
SLS2560
1
EPA 200.8
06/27/2015 05:51
SLS2560
1
EPA 200.8
06/27/2015 05:51
SLS2560
1
EPA 200.8
06/27/2015 05:51
SLS2560
1
EPA 200.8
06/27/2015 05:51
SLS2560
1
EPA 200.8
06/27/2015 05:51
SLS2560
1
EPA 200.8
06/27/2015 05:51
SLS2560
1
EPA 200.8
06/27/2015 05:51
SLS2560
1
EPA 200.8
06/27/2015 05:51
SLS2560
Vendor Method
V_SHEALY
Vendor Method V_ELE1
1 SM2540C 06/25/201515:24 AGIBBS5
1 SM5310C/EPA9060A 06/29/201513:32 GHUTCHI
1 SM2540D 06/25/2015 09:00 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060802
Site: MW-16D
Collection Date: 23-Jun-15 12:30 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
2.9
mg-N/L
0.05
INORGANIC IONS BY IC
Chloride
8.8
mg/L
0.1
Sulfate
7.7
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
0.012
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
0.260
mg/L
0.005
Strontium (Sr)
0.163
mg/L
0.005
Zinc (Zn)
0.009
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
25.6
mg/L
0.01
Magnesium (Mg)
5.16
mg/L
0.005
Potassium (K)
2.32
mg/L
0.1
Sodium (Na)
9.77
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.102
mg/L
0.005
Barium (Ba)
0.013
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.087
mg/L
0.01
Manganese (Mn)
0.269
mg/L
0.005
Strontium (Sr)
0.163
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015020821
Matrix: GW WW
Analytical Lab
Page 6 of 69
DF Method Analysis Date/Time Analyst
Vendor Method V_SHEALY
5 EPA 353.2
06/26/2015 11:37
LSTARLI
1 EPA 300.0
06/25/2015 16:15
BGN9034
1 EPA 300.0
06/25/2015 16:15
BGN9034
1 EPA 245.1
06/30/2015 10:23
ACPAYNE
1 EPA 245.1
06/30/2015 11:52
ACPAYNE
1 EPA 200.7
06/26/2015 10:07
FCJORDA
1 EPA 200.7
06/26/2015 10:07
FCJORDA
1 EPA 200.7
06/26/2015 10:07
FCJORDA
1 EPA 200.7
06/26/2015 10:07
FCJORDA
1 EPA 200.7
06/26/2015 10:07
FCJORDA
1 EPA 200.7
06/26/2015 10:07
FCJORDA
1 EPA 200.7
06/26/2015 10:07
FCJORDA
1 EPA 200.7
06/26/2015 11:58
FCJORDA
1 EPA 200.7
06/26/2015 11:58
FCJORDA
1 EPA 200.7
06/26/2015 11:58
FCJORDA
1 EPA 200.7
06/26/2015 11:58
FCJORDA
1 EPA 200.7
06/26/2015 13:57
FCJORDA
1 EPA 200.7
06/26/2015 13:57
FCJORDA
1 EPA 200.7
06/26/2015 13:57
FCJORDA
1 EPA 200.7
06/26/2015 13:57
FCJORDA
1 EPA 200.7
06/26/2015 13:57
FCJORDA
1 EPA 200.7
06/26/2015 13:57
FCJORDA
1 EPA 200.7
06/26/2015 13:57
FCJORDA

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060802
Site: MW-16D
Collection Date: 23-Jun-15 12:30 PM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
10.9
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
0.530
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
10.1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
0.617
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
160
mg/L
25
Total Carbon
TOC
0.208
mg/L
0.1
TOTAL SUSPENDED SOLIDS
TSS
< 5
mg/L
5
Sample #: 2015020821
Matrix: GW WW
Analytical Lab
Page 7 of 69
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/27/2015 16:40
SLS2560
1
EPA 200.8
06/27/2015 16:40
SLS2560
1
EPA 200.8
06/27/2015 16:40
SLS2560
1
EPA 200.8
06/27/2015 16:40
SLS2560
1
EPA 200.8
06/27/2015 16:40
SLS2560
1
EPA 200.8
06/27/2015 16:40
SLS2560
1
EPA 200.8
06/27/2015 16:40
SLS2560
1
EPA 200.8
06/27/2015 16:40
SLS2560
1
EPA 200.8
06/27/2015 16:40
SLS2560
1
EPA 200.8
06/27/2015 16:40
SLS2560
1
EPA 200.8
06/27/2015 16:40
SLS2560
1
EPA 200.8
06/27/2015 16:40
SLS2560
1
EPA 200.8
06/27/2015 16:40
SLS2560
1
EPA 200.8
06/27/2015 05:58
SLS2560
1
EPA 200.8
06/27/2015 05:58
SLS2560
1
EPA 200.8
06/27/2015 05:58
SLS2560
1
EPA 200.8
06/27/2015 05:58
SLS2560
1
EPA 200.8
06/27/2015 05:58
SLS2560
1
EPA 200.8
06/27/2015 05:58
SLS2560
1
EPA 200.8
06/27/2015 05:58
SLS2560
1
EPA 200.8
06/27/2015 05:58
SLS2560
1
EPA 200.8
06/27/2015 05:58
SLS2560
1
EPA 200.8
06/27/2015 05:58
SLS2560
1
EPA 200.8
06/27/2015 05:58
SLS2560
1
EPA 200.8
06/27/2015 05:58
SLS2560
1
EPA 200.8
06/27/2015 05:58
SLS2560
Vendor Method
V_SHEALY
Vendor Method V_ELE1
1 SM2540C 06/25/201515:24 AGIBBS5
1 SM5310C/EPA9060A 06/29/201513:32 GHUTCHI
1 SM2540D 06/25/2015 09:00 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060802
Site: MW-16BR
Collection Date: 23-Jun-15 9:57 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
7.0
mg/L
0.1
Sulfate
12
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.022
mg/L
0.005
Barium (Ba)
0.009
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.012
mg/L
0.01
Manganese (Mn)
0.025
mg/L
0.005
Strontium (Sr)
0.112
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
22.5
mg/L
0.01
Magnesium (Mg)
3.89
mg/L
0.005
Potassium (K)
1.70
mg/L
0.1
Sodium (Na)
23.9
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.088
mg/L
0.005
Barium (Ba)
0.011
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.080
mg/L
0.01
Manganese (Mn)
0.030
mg/L
0.005
Strontium (Sr)
0.112
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015020822
Matrix: GW WW
Analytical Lab
Page 8 of 69
DF Method Analysis Date/Time Analyst
Vendor Method V_SHEALY
1
EPA 353.2
06/26/2015 11:32
LSTARLI
1
EPA 300.0
06/25/2015 16:33
BGN9034
10
EPA 300.0
06/25/2015 16:33
BGN9034
1
EPA 245.1
06/30/2015 10:26
ACPAYNE
1
EPA 245.1
06/30/2015 12:02
ACPAYNE
1
EPA 200.7
06/26/2015 11:02
FCJORDA
1
EPA 200.7
06/26/2015 11:02
FCJORDA
1
EPA 200.7
06/26/2015 11:02
FCJORDA
1
EPA 200.7
06/26/2015 11:02
FCJORDA
1
EPA 200.7
06/26/2015 11:02
FCJORDA
1
EPA 200.7
06/26/2015 11:02
FCJORDA
1
EPA 200.7
06/26/2015 11:02
FCJORDA
1
EPA 200.7
06/26/2015 12:01
FCJORDA
1
EPA 200.7
06/26/2015 12:01
FCJORDA
1
EPA 200.7
06/26/2015 12:01
FCJORDA
1
EPA 200.7
06/26/2015 12:01
FCJORDA
1
EPA 200.7
06/29/2015 09:33
MHH7131
1
EPA 200.7
06/29/2015 09:33
MHH7131
1
EPA 200.7
06/29/2015 09:33
MHH7131
1
EPA 200.7
06/29/2015 09:33
MHH7131
1
EPA 200.7
06/29/2015 09:33
MHH7131
1
EPA 200.7
06/29/2015 09:33
MHH7131
1
EPA 200.7
06/29/2015 09:33
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060802
Site: MW-16BR
Collection Date: 23-Jun-15 9:57 AM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
2.07
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
21.8
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
2.68
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
2.05
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
23.4
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
2.79
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
170
mg/L
25
Total Carbon
TOC
3.7
mg/L
0.1
TOTAL SUSPENDED SOLIDS
TSS
6.0
mg/L
5
Sample #: 2015020822
Matrix: GW WW
Analytical Lab
Page 9 of 69
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/27/2015 16:48
SLS2560
1
EPA 200.8
06/27/2015 16:48
SLS2560
1
EPA 200.8
06/27/2015 16:48
SLS2560
1
EPA 200.8
06/27/2015 16:48
SLS2560
1
EPA 200.8
06/27/2015 16:48
SLS2560
1
EPA 200.8
06/27/2015 16:48
SLS2560
1
EPA 200.8
06/27/2015 16:48
SLS2560
1
EPA 200.8
06/27/2015 16:48
SLS2560
1
EPA 200.8
06/27/2015 16:48
SLS2560
1
EPA 200.8
06/27/2015 16:48
SLS2560
1
EPA 200.8
06/27/2015 16:48
SLS2560
1
EPA 200.8
06/27/2015 16:48
SLS2560
1
EPA 200.8
06/27/2015 16:48
SLS2560
1
EPA 200.8
06/27/2015 14:31
SLS2560
1
EPA 200.8
06/27/2015 14:31
SLS2560
1
EPA 200.8
06/27/2015 14:31
SLS2560
1
EPA 200.8
06/27/2015 14:31
SLS2560
1
EPA 200.8
06/27/2015 14:31
SLS2560
1
EPA 200.8
06/27/2015 14:31
SLS2560
1
EPA 200.8
06/27/2015 14:31
SLS2560
1
EPA 200.8
06/27/2015 14:31
SLS2560
1
EPA 200.8
06/27/2015 14:31
SLS2560
1
EPA 200.8
06/27/2015 14:31
SLS2560
1
EPA 200.8
06/27/2015 14:31
SLS2560
1
EPA 200.8
06/27/2015 14:31
SLS2560
1
EPA 200.8
06/27/2015 14:31
SLS2560
Vendor Method
V_SHEALY
Vendor Method V_ELE1
1 SM2540C 06/25/201515:24 AGIBBS5
1 SM5310C/EPA9060A 06/29/201513:32 GHUTCHI
1 SM2540D 06/25/2015 09:00 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060802
Site: ABMW-4BR
Collection Date: 23-Jun-15 9:20 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
4.8
mg/L
0.1
Sulfate
80
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.011
mg/L
0.005
Barium (Ba)
0.113
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
1.42
mg/L
0.01
Manganese (Mn)
0.410
mg/L
0.005
Strontium (Sr)
2.02
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
85.3
mg/L
0.01
Magnesium (Mg)
5.97
mg/L
0.005
Potassium (K)
6.23
mg/L
0.1
Sodium (Na)
21.2
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.020
mg/L
0.005
Barium (Ba)
0.115
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
1.59
mg/L
0.01
Manganese (Mn)
0.407
mg/L
0.005
Strontium (Sr)
2.02
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015020823
Matrix: GW WW
Analytical Lab
Page 10 of 69
DF Method Analysis Date/Time Analyst
Vendor Method V_SHEALY
1
EPA 353.2
06/26/2015 11:35
LSTARLI
1
EPA 300.0
06/25/2015 16:50
BGN9034
10
EPA 300.0
06/25/2015 16:50
BGN9034
1
EPA 245.1
06/30/2015 10:28
ACPAYNE
1
EPA 245.1
06/30/2015 12:04
ACPAYNE
1
EPA 200.7
06/26/2015 10:22
FCJORDA
1
EPA 200.7
06/26/2015 10:22
FCJORDA
1
EPA 200.7
06/26/2015 10:22
FCJORDA
1
EPA 200.7
06/26/2015 10:22
FCJORDA
1
EPA 200.7
06/26/2015 10:22
FCJORDA
1
EPA 200.7
06/26/2015 10:22
FCJORDA
1
EPA 200.7
06/26/2015 10:22
FCJORDA
1
EPA 200.7
06/26/2015 12:05
FCJORDA
1
EPA 200.7
06/26/2015 12:05
FCJORDA
1
EPA 200.7
06/26/2015 12:05
FCJORDA
1
EPA 200.7
06/26/2015 12:05
FCJORDA
1
EPA 200.7
06/29/2015 09:45
MHH7131
1
EPA 200.7
06/29/2015 09:45
MHH7131
1
EPA 200.7
06/29/2015 09:45
MHH7131
1
EPA 200.7
06/29/2015 09:45
MHH7131
1
EPA 200.7
06/29/2015 09:45
MHH7131
1
EPA 200.7
06/29/2015 09:45
MHH7131
1
EPA 200.7
06/29/2015 09:45
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060802
Site: ABMW-4BR
Collection Date: 23-Jun-15 9:20 AM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
6.10
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
1.08
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
6.12
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
0.382
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
370
mg/L
25
Total Carbon
TOC
1.8
mg/L
0.1
TOTAL SUSPENDED SOLIDS
TSS
< 5
mg/L
5
Sample #: 2015020823
Matrix: GW WW
Analytical Lab
Page 11 of 69
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/27/2015 16:55
SLS2560
1
EPA 200.8
06/27/2015 16:55
SLS2560
1
EPA 200.8
06/27/2015 16:55
SLS2560
1
EPA 200.8
06/27/2015 16:55
SLS2560
1
EPA 200.8
06/27/2015 16:55
SLS2560
1
EPA 200.8
06/27/2015 16:55
SLS2560
1
EPA 200.8
06/27/2015 16:55
SLS2560
1
EPA 200.8
06/27/2015 16:55
SLS2560
1
EPA 200.8
06/27/2015 16:55
SLS2560
1
EPA 200.8
06/27/2015 16:55
SLS2560
1
EPA 200.8
06/27/2015 16:55
SLS2560
1
EPA 200.8
06/27/2015 16:55
SLS2560
1
EPA 200.8
06/27/2015 16:55
SLS2560
1
EPA 200.8
06/27/2015 14:08
SLS2560
1
EPA 200.8
06/27/2015 14:08
SLS2560
1
EPA 200.8
06/27/2015 14:08
SLS2560
1
EPA 200.8
06/27/2015 14:08
SLS2560
1
EPA 200.8
06/27/2015 14:08
SLS2560
1
EPA 200.8
06/27/2015 14:08
SLS2560
1
EPA 200.8
06/27/2015 14:08
SLS2560
1
EPA 200.8
06/27/2015 14:08
SLS2560
1
EPA 200.8
06/27/2015 14:08
SLS2560
1
EPA 200.8
06/27/2015 14:08
SLS2560
1
EPA 200.8
06/27/2015 14:08
SLS2560
1
EPA 200.8
06/27/2015 14:08
SLS2560
1
EPA 200.8
06/27/2015 14:08
SLS2560
Vendor Method
V_SHEALY
Vendor Method V_ELE1
1 SM2540C 06/25/201515:24 AGIBBS5
1 SM5310C/EPA9060A 06/29/201513:32 GHUTCHI
1 SM2540D 06/25/2015 09:00 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060802
Site: MW-13BR
Collection Date: 23-Jun-15 2:20 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
46
mg/L
1
Sulfate
18
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.027
mg/L
0.005
Barium (Ba)
0.041
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
1.16
mg/L
0.01
Manganese (Mn)
0.486
mg/L
0.005
Strontium (Sr)
0.423
mg/L
0.005
Zinc (Zn)
0.019
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
75.2
mg/L
0.01
Magnesium (Mg)
13.1
mg/L
0.005
Potassium (K)
5.49
mg/L
0.1
Sodium (Na)
25.7
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.037
mg/L
0.005
Barium (Ba)
0.040
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
1.13
mg/L
0.01
Manganese (Mn)
0.474
mg/L
0.005
Strontium (Sr)
0.418
mg/L
0.005
Zinc (Zn)
0.036
mg/L
0.005
Sample #: 2015020824
Matrix: GW WW
Analytical Lab
Page 12 of 69
DF Method Analysis Date/Time Analyst
Vendor Method V_SHEALY
1
EPA 353.2
06/26/2015 11:36
LSTARLI
10
EPA 300.0
06/25/2015 15:21
BGN9034
10
EPA 300.0
06/25/2015 15:21
BGN9034
1
EPA 245.1
06/30/2015 10:30
ACPAYNE
1
EPA 245.1
06/30/2015 12:06
ACPAYNE
1
EPA 200.7
06/26/2015 10:26
FCJORDA
1
EPA 200.7
06/26/2015 10:26
FCJORDA
1
EPA 200.7
06/26/2015 10:26
FCJORDA
1
EPA 200.7
06/26/2015 10:26
FCJORDA
1
EPA 200.7
06/26/2015 10:26
FCJORDA
1
EPA 200.7
06/26/2015 10:26
FCJORDA
1
EPA 200.7
06/26/2015 10:26
FCJORDA
1
EPA 200.7
06/26/2015 12:09
FCJORDA
1
EPA 200.7
06/26/2015 12:09
FCJORDA
1
EPA 200.7
06/26/2015 12:09
FCJORDA
1
EPA 200.7
06/26/2015 12:09
FCJORDA
1
EPA 200.7
06/29/2015 09:48
MHH7131
1
EPA 200.7
06/29/2015 09:48
MHH7131
1
EPA 200.7
06/29/2015 09:48
MHH7131
1
EPA 200.7
06/29/2015 09:48
MHH7131
1
EPA 200.7
06/29/2015 09:48
MHH7131
1
EPA 200.7
06/29/2015 09:48
MHH7131
1
EPA 200.7
06/29/2015 09:48
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060802
Site: MW-13BR
Collection Date: 23-Jun-15 2:20 PM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
7.20
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
1.19
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
8.28
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
0.381
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
RADIOLOGICAL - (Analysis Performed by GEL)
Vendor Parameter
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS 370 mg/L 25
Total Carbon
TOC 0.900 mg/L 0.1
Sample #: 2015020824
Matrix: GW WW
Analytical Lab
Page 13 of 69
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/27/2015 17:02
SLS2560
1
EPA 200.8
06/27/2015 17:02
SLS2560
1
EPA 200.8
06/27/2015 17:02
SLS2560
1
EPA 200.8
06/27/2015 17:02
SLS2560
1
EPA 200.8
06/27/2015 17:02
SLS2560
1
EPA 200.8
06/27/2015 17:02
SLS2560
1
EPA 200.8
06/27/2015 17:02
SLS2560
1
EPA 200.8
06/27/2015 17:02
SLS2560
1
EPA 200.8
06/27/2015 17:02
SLS2560
1
EPA 200.8
06/27/2015 17:02
SLS2560
1
EPA 200.8
06/27/2015 17:02
SLS2560
1
EPA 200.8
06/27/2015 17:02
SLS2560
1
EPA 200.8
06/27/2015 17:02
SLS2560
1
EPA 200.8
06/27/2015 14:38
SLS2560
1
EPA 200.8
06/27/2015 14:38
SLS2560
1
EPA 200.8
06/27/2015 14:38
SLS2560
1
EPA 200.8
06/27/2015 14:38
SLS2560
1
EPA 200.8
06/27/2015 14:38
SLS2560
1
EPA 200.8
06/27/2015 14:38
SLS2560
1
EPA 200.8
06/27/2015 14:38
SLS2560
1
EPA 200.8
06/27/2015 14:38
SLS2560
1
EPA 200.8
06/27/2015 14:38
SLS2560
1
EPA 200.8
06/27/2015 14:38
SLS2560
1
EPA 200.8
06/27/2015 14:38
SLS2560
1
EPA 200.8
06/27/2015 14:38
SLS2560
1
EPA 200.8
06/27/2015 14:38
SLS2560
Vendor Method
V_SHEALY
Vendor Method v GEL
Vendor Method V_ELE1
1 SM2540C 06/25/201515:24 AGIBBS5
1 SM5310C/EPA9060A 06/29/201513:32 GHUTCHI

Analytical Lab
Certificate of Laboratory Analysis Page 14 of 69
This report shall not be reproduced, except in full.
Order # J15060802
Site: MW-13BR Sample #: 2015020824
Collection Date: 23-Jun-15 2:20 PM Matrix: GW WW
Analyte Result Units Qualifiers RDL DF Method Analysis Date/Time Analyst
TOTAL SUSPENDED SOLIDS
TSS 5.0 mg/L 5 1 SM2540D 06/25/2015 09:00 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060802
Site: MW-16D-Dup
Collection Date: 23-Jun-15 12:30 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
2.9
mg-N/L
0.05
INORGANIC IONS BY IC
Chloride
8.9
mg/L
0.1
Sulfate
7.8
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
0.013
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
0.250
mg/L
0.005
Strontium (Sr)
0.179
mg/L
0.005
Zinc (Zn)
0.093
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
25.4
mg/L
0.01
Magnesium (Mg)
5.10
mg/L
0.005
Potassium (K)
2.31
mg/L
0.1
Sodium (Na)
9.72
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.086
mg/L
0.005
Barium (Ba)
0.013
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.085
mg/L
0.01
Manganese (Mn)
0.261
mg/L
0.005
Strontium (Sr)
0.163
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015020837
Matrix: GW WW
Analytical Lab
Page 15 of 69
DF Method Analysis Date/Time Analyst
Vendor Method V_SHEALY
5 EPA 353.2
06/26/2015 11:43
LSTARLI
1 EPA 300.0
06/25/2015 17:26
BGN9034
1 EPA 300.0
06/25/2015 17:26
BGN9034
1 EPA 245.1
06/30/2015 10:33
ACPAYNE
1 EPA 245.1
06/30/2015 12:09
ACPAYNE
1 EPA 200.7
06/26/2015 11:06
FCJORDA
1 EPA 200.7
06/26/2015 11:06
FCJORDA
1 EPA 200.7
06/26/2015 11:06
FCJORDA
1 EPA 200.7
06/26/2015 11:06
FCJORDA
1 EPA 200.7
06/26/2015 11:06
FCJORDA
1 EPA 200.7
06/26/2015 11:06
FCJORDA
1 EPA 200.7
06/26/2015 11:06
FCJORDA
1 EPA 200.7
06/26/2015 12:13
FCJORDA
1 EPA 200.7
06/26/2015 12:13
FCJORDA
1 EPA 200.7
06/26/2015 12:13
FCJORDA
1 EPA 200.7
06/26/2015 12:13
FCJORDA
1 EPA 200.7
06/29/2015 09:52
MHH7131
1 EPA 200.7
06/29/2015 09:52
MHH7131
1 EPA 200.7
06/29/2015 09:52
MHH7131
1 EPA 200.7
06/29/2015 09:52
MHH7131
1 EPA 200.7
06/29/2015 09:52
MHH7131
1 EPA 200.7
06/29/2015 09:52
MHH7131
1 EPA 200.7
06/29/2015 09:52
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060802
Site: MW-16D-Dup
Collection Date: 23-Jun-15 12:30 PM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
10.6
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
0.537
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
11.3
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
0.729
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
150
mg/L
25
Total Carbon
TOC
0.214
mg/L
0.1
TOTAL SUSPENDED SOLIDS
TSS
< 5
mg/L
5
Sample #: 2015020837
Matrix: GW WW
Analytical Lab
Page 16 of 69
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/27/2015 17:09
SLS2560
1
EPA 200.8
06/27/2015 17:09
SLS2560
1
EPA 200.8
06/27/2015 17:09
SLS2560
1
EPA 200.8
06/27/2015 17:09
SLS2560
1
EPA 200.8
06/27/2015 17:09
SLS2560
1
EPA 200.8
06/27/2015 17:09
SLS2560
1
EPA 200.8
06/27/2015 17:09
SLS2560
1
EPA 200.8
06/27/2015 17:09
SLS2560
1
EPA 200.8
06/27/2015 17:09
SLS2560
1
EPA 200.8
06/27/2015 17:09
SLS2560
1
EPA 200.8
06/27/2015 17:09
SLS2560
1
EPA 200.8
06/27/2015 17:09
SLS2560
1
EPA 200.8
06/27/2015 17:09
SLS2560
1
EPA 200.8
06/27/2015 14:45
SLS2560
1
EPA 200.8
06/27/2015 14:45
SLS2560
1
EPA 200.8
06/27/2015 14:45
SLS2560
1
EPA 200.8
06/27/2015 14:45
SLS2560
1
EPA 200.8
06/27/2015 14:45
SLS2560
1
EPA 200.8
06/27/2015 14:45
SLS2560
1
EPA 200.8
06/27/2015 14:45
SLS2560
1
EPA 200.8
06/27/2015 14:45
SLS2560
1
EPA 200.8
06/27/2015 14:45
SLS2560
1
EPA 200.8
06/27/2015 14:45
SLS2560
1
EPA 200.8
06/27/2015 14:45
SLS2560
1
EPA 200.8
06/27/2015 14:45
SLS2560
1
EPA 200.8
06/27/2015 14:45
SLS2560
Vendor Method
V_SHEALY
Vendor Method V_ELE1
1 SM2540C 06/25/201515:24 AGIBBS5
1 SM5310C/EPA9060A 06/29/201513:32 GHUTCHI
1 SM2540D 06/25/2015 09:00 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060802
Site: MW-3
Collection Date: 23-Jun-15 9:24 AM
Analyte Result Units Qualifiers RDL DF
RADIOLOGICAL - (Analysis Performed by GEL)
Vendor Parameter Complete
Sample #: 2015020838
Matrix: GW WW
Analytical Lab
Page 17 of 69
Method Analysis Date/Time Analyst
Vendor Method
v GEL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060802
Site: Filter Blank
Collection Date: 23-Jun-15 4:30 PM
Analyte
Result
Units
Qualifiers RDL
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
6.05
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015020839
Matrix: GW WW
Analytical Lab
Page 18 of 69
DF
Method
Analysis Date/Time
Analyst
1
EPA 245.1
06/30/2015 12:11
ACPAYNE
1
EPA 200.7
06/26/2015 10:34
FCJORDA
1
EPA 200.7
06/26/2015 10:34
FCJORDA
1
EPA 200.7
06/26/2015 10:34
FCJORDA
1
EPA 200.7
06/26/2015 10:34
FCJORDA
1
EPA 200.7
06/26/2015 10:34
FCJORDA
1
EPA 200.7
06/26/2015 10:34
FCJORDA
1
EPA 200.7
06/26/2015 10:34
FCJORDA
1
EPA 200.8
06/27/2015 17:16
MHALL3
1
EPA 200.8
06/27/2015 17:16
MHALL3
1
EPA 200.8
06/27/2015 17:16
MHALL3
1
EPA 200.8
06/27/2015 17:16
MHALL3
1
EPA 200.8
06/27/2015 17:16
MHALL3
1
EPA 200.8
06/27/2015 17:16
MHALL3
1
EPA 200.8
06/27/2015 17:16
MHALL3
1
EPA 200.8
06/27/2015 17:16
MHALL3
1
EPA 200.8
06/27/2015 17:16
MHALL3
1
EPA 200.8
06/27/2015 17:16
MHALL3
1
EPA 200.8
06/27/2015 17:16
MHALL3
1
EPA 200.8
06/27/2015 17:16
MHALL3
1
EPA 200.8
06/27/2015 17:16
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060802
Site: Equipment Blank
Collection Date: 23-Jun-15 4:30 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
< 0.1
mg/L
0.1
Sulfate
< 0.1
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
UNDIGESTED METALS BY lCP
Calcium (Ca)
0.036
mg/L
0.01
Magnesium (Mg)
< 0.005
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
0.052
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.007
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015020840
Matrix: GW WW
Analytical Lab
Page 19 of 69
DF Method Analysis Date/Time Analyst
Vendor Method V_SHEALY
1 EPA 353.2
06/26/2015 11:39
LSTARLI
1 EPA 300.0
06/25/2015 13:51
BGN9034
1 EPA 300.0
06/25/2015 13:51
BGN9034
1 EPA 245.1
06/30/2015 10:35
ACPAYNE
1 EPA 200.7
06/26/2015 12:17
FCJORDA
1 EPA 200.7
06/26/2015 12:17
FCJORDA
1 EPA 200.7
06/26/2015 12:17
FCJORDA
1 EPA 200.7
06/26/2015 12:17
FCJORDA
1 EPA 200.7
06/29/2015 09:56
MHH7131
1 EPA 200.7
06/29/2015 09:56
MHH7131
1 EPA 200.7
06/29/2015 09:56
MHH7131
1 EPA 200.7
06/29/2015 09:56
MHH7131
1 EPA 200.7
06/29/2015 09:56
MHH7131
1 EPA 200.7
06/29/2015 09:56
MHH7131
1 EPA 200.7
06/29/2015 09:56
MHH7131
1 EPA 200.8
06/27/2015 14:52
SLS2560
1 EPA 200.8
06/27/2015 14:52
SLS2560
1 EPA 200.8
06/27/2015 14:52
SLS2560
1 EPA 200.8
06/27/2015 14:52
SLS2560
1 EPA 200.8
06/27/2015 14:52
SLS2560
1 EPA 200.8
06/27/2015 14:52
SLS2560
1 EPA 200.8
06/27/2015 14:52
SLS2560
1 EPA 200.8
06/27/2015 14:52
SLS2560
1 EPA 200.8
06/27/2015 14:52
SLS2560
1 EPA 200.8
06/27/2015 14:52
SLS2560
1 EPA 200.8
06/27/2015 14:52
SLS2560
1 EPA 200.8
06/27/2015 14:52
SLS2560
1 EPA 200.8
06/27/2015 14:52
SLS2560
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4) Complete Vendor Method V_SHEALY

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060802
Site: Equipment Blank
Collection Date: 23-Jun-15 4:30 PM
Analyte Result Units Qualifiers RDL DF
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete
TOTAL DISSOLVED SOLIDS
TDS < 25 mg/L 25 1
Total Carbon
Sample #: 2015020840
Matrix: GW WW
Analytical Lab
Page 20 of 69
Method Analysis Date/Time Analyst
Vendor Method
V_ELE1
SM2540C 06/25/201515:24 AGIBBS5
TOC 0.204 mg/L 0.1 1 SM5310C/EPA9060A 06/29/201513:32 GHUTCHI
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L 5 1 SM2540D 06/25/2015 09:00 AGIBBS5

Analytical Lab
Page 21 of 69
MI
REPORT OF ANALYSES
Ellernent One [Inc.
6319-D Carolina Beach Rd.
Wilmington, NC 28412
(Tone: 910 793-0128
Fax: [phone]
[e-mail]
Duke Energy
July 1, 2015
Laboratory Services
Client Project Name AB GW Assessment water (wells) Mayo
13339 Hagers
Ferry Road Bld. MG03A
Client Project Number
J15060802
Huntersville, NC 28078
PO Number
Sample Matrix
GW WW
Sample Type Grab
Date Received
06/26/2015
Date Analyzed
06/29/2015
Method
SM 4500
S2- D
Time Received
1610
Delivered by
FedEx
Received by
LLB
eOne ID
Duke Energy ID
Parameter Result
Unit
Dil
DL Date
Time
Sampled
Sampled
25194-1
MW-16S
Sulfide
< 0.1
mg/L
1
0.1 06/23/15
1415
25194-2
MW-16D
Sulfide
< 0.1
mg/L
1
0.1 06/23/15
1230
25194-3
MW-16BR
Sulfide
0.264
mg/L
1
0.1 06/23/15
0957
25194-4
ABMW-4BR
Sulfide
< 0.1
mg/L
1
0.1 06/23/15
0920
25194-5
MWA 313R
Sulfide
0.115
mg/L
1
0.1 06/23/15
1420
25194-6
MW-16D Dup
Sulfide
< 0.1
mg/L
1
0.1 06/23/15
1230
25194-7
Equipment Blank
Sulfide
< 0.1
mg/L
1
0.1 06/23/15
1630
Ken 90th, Laboratory Director ✓'
25194 Duke Report Packet Compiled by
NC Certifications: DW 37788 and DWQ DENR 604

Analytical Lab
Page 22 of 69
Q 4 (J 7 0 .-
ID
a
rM
C Y1
TT
1 I4
E a=
N T IV
n unn�c wni pai�san
�II�t II I SV aId �1U2110 fill l!'IAlll t�l"'-'
rJ
z
J .
Y
> Ch
J W
= U
I
v m
�
c
N 9
a C
d
U fJ
A '
C V1
V
U e
� O1
_
U
� 4 a
as
U U e
_ m
A a EN N E
z z v
W W
O
N
N
W W
8
q
p
Y
C
�
C
CCt
R
�ws
W

Analytical Lab
e e entOne SAMPLE SUBMISSION FORM Lab Ibge'Ai 94
TAT 5 BD Analysis Due Date 06.29.15
Hold Time Expiration 06.30.15 @ 0920 Report Due Date 07.01.15
Client: Duke Energy Date Rec: 06.26.15
LIMS No J15060802 Time Rec: 1610
Project ID Mao Rec By LLB
H >9 No Tem s 6°C Cl�e No Ref. Method:
If No, Record If No. Record SM4500 S2 D
Sample laentitication & collection Information
Lab ID
Client ID
Collection Date
Collection Time
Analysis Requested
1
MW-16S
06.23.15
1415 u fid
2
MW-16D
06.23.15
1230
3
MW-16BR
06.23.15
09._.___
57
4
ABMW-4BR
06.23.15
0920 S
23.15
1420
6
MW-16D DUP
06.23.15
1230 � t�
7
Equipment Blank
06.23.15
1630
NOTE for
Sulfide The MS/MSD spike should approximate 2 to 3
times the sample concentration. If no sulfide detected
at 100 pg/L spike the sample to render the final
spike concentration at — 500 pg/L

Analytical Lab
Page 24 of 69
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664'
Na2S•9H20 Lot #
40721
UNITS OF ANSWER
ug/mL
DETECTION LIMIT(ug)1.000
SPK LEVEL u
MAX ALIQUOT
5 "
10.00
CLIENT:
Lab ID#
Duke
25194 / 195 / 196
Date:
06/29/15
STANDARD conc(ppm)
- X
Time Analysis Begun
8:00
Cal Std Lot: SD-14-1
10
Time Analysis Ended
10:00
QC Std Lot: SD-14-2
10
Analyst:
KAM
STD ABSORPTION
Y
X
Y
- -
ug STD
SOLUTION
ABS
°'°°0.
----
--
Ck
_ -
-o�
--
0.00
1.00
2.50
5.00 '
7.50
10;00
0.000
0.095
0.223
0.435
0.608
0.785
y
Q'
0300
-
- °
°.+�
---.-low
0.00o m son e.m 6.60 8.60 +o.00 12m
x
SAMPLE x
I.D.
Std. B. 0.00
Std. B. 1.00
Std. B. 2.50
Std. B. 5.00
Std. B. 7.50
Std. B. 10.00
k
SAMP
ABS
0.000
0.098
0.229
0.446
0.634
0.798
Sloe
0.078305495r
Correlation 0.998579076
ug PER
ALIQUOT
0.0000
0.8257
2.5953
5.5266
8.0661
10.2814
ALI in mL
ANALYZED
10
10
10
10
10
10
PREP
VOL in mL
10
10
10
10
10
10
ALI in mL
TAKEN
10
10
10
10
10
10
RESULTS
ug/mL
<
<
0.260
0.553
0.807
1.028
LESS THAN
% SPK REC
82.57%
103.81 %
110.53%
107.55%
102.81 %
SPIKE
LEVEL
0.0
1.0
2.5
5.0
7.5
10.0
LRB
0.000
0.0000
10
10
10
<
0.0
LRB SPK
0.433
5.3509
10
10
10
0.535
107%
5.0
QC
0.447
5.5401
10
10
10
0.554
111 %
5.0
25194-1
0.003
-0.4575
10
10
10
'`` < 0
25194-1 s k
0.405
4.9727
10
10
10
0.497
99%
5.0
25194-2
0.002
-0.4711
10
10
10 1
25194-2 dup
0.001
-0.4846
10
10
10
< 0.1
25194-2 spk
0.400
4.9052
10
10
10
0.491
98%
5.0
25194-3
0.232
2.6358
10
10
10
�64°
25194-3 s k
0.623
7.9175
10
10
10
0.792
106%
5.0
25194-4
0.079
0.5691
10
10
10
25194-4 s k
0.464
5.7697
10
10
10
0.577
115%
5.0
25194-5
0.122
1.1499
10
10
10
25194-5 s k
0.495
6.1884
10
10
10
0.619
101 %
5.0
25194-6
0.001
-0.4846
10
10
10
25194-6 s k
0.394
4.8241
10
10
10
0.482
96%
5.0
25194-7
0.002
-0.4711
10
10
10
5.0
25194-7 s k
0.432
5.3374
10
10
10
0.534
107%
25195-1
0.004
-0.4440
10
10
10
<
25195-1 s k
0.334
4.0136
10
10
10
0.401
80%
5.0
25195-2
0.008
-0.3900
10
10
10
25195-2 spk
0.386
4.7161
10
10
10
0.472
94%
5.0
Blank
-0.001
0.0000
10
10
10
<
QC 0.447 5.5401 10
Submitted for QA/QC- Date: 06/29/15
10
By: (Print)
10 0.554
KAM
111 % 5.
(sign):
Page 1 of 2

Analytical Lab
Page 25 of 69
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
u /mL-
DETECTION LIMIT u
1.000
CLIENT:
Duke
SPK LEVEL u
5
Lab ID#
25194 / 195 / 196
Na2S•9H2O Lot #
40721
MAX ALIQUOT
10.00
Date:
06/29/15
STANDARD conc(ppm)
X
Time Analysis Begun
8:00
Cal Std Lot: SD-14-1
10
Time Analysis Ended
10:00
QC Std Lot: SD-14-2
10
Analyst:
M.
STD ABSORPTION
Y
Xy
-----
0.000
ug STD
SOLUTION
STD
ABS
Um
0.700
0.sa0o�
0.00
1.00
2.50
5.00
7.50
10:00
0.000
0.095
0.223
0.435
0.608
0,785
0.em
U400
gas
--s:
0.=
_
O.zOo
�_ so
0.ID0
o.oro
0.00 200 4.00 6.60 8.00 10.00 12,00
x
I
SAMPLE
I.D.
Std. B. 0.00
Std. B. 1.00
Std. B. 2.50
Std. B. 5.00
Std. B. 7.50
Std. B. 10.00
�
SAMP
ABS
0.000
0.098
0.229
0.446
0.634
0.798
ug PER
ALIQUOT
1 0.0000
0.8257
2.5953
5.5266
8.0661
10.2814
ALI in mL PREP
ANALYZED VOL in mL
10 10
10 10
10 10
10 10
10 10
10 10
Sloe 0,078305495
ALI in mL RESULTS
TAKEN u /mL
10 <
10 <
10 0.260
10 0.553
10 0.807
10 1.028
Correlation 0.998679076'
LESS THAN SPIKE
% SPK REC LEVEL
0.0
82.57-% 1.0
103.81 % 2.5
110.53% 5.0
107.55% 7.5
102.81 % 10.0
LRB
0.000
0.0000
10
10
10
<
0.0
LRB SPK
0.433
5.3509
10
10
10
0.535
107%
5.0
QC
0.447
5.5401
10
10
10
0.554
111%
5.0
25195-3
0.009
-0.3765
10
10
10
"01
25195-3 s k
0.427
5.2699
10
10
10
0.527
105%
5.0
25196-1
0.013
-0.3225
10
10
10
< p�
25196-1 dup
0.011
-0.3495
10
10
10
< 0.1
25196-1 s k
0.410
5.0403
10
10
10
0.504
101%
5.0
25196-2
0.002
-0.4711
10
10
10
25196-2 s k
0.433
5.3509
10
10
10
0.535
107%
5.0
25195-1
0.003
-0.4575
10
10
5
<
25195-1 s k
0.345
4.1622
10
10
5
0.832
83%
5.0
25195-1
0.004
-0.4440
10
10
2
`� c
25195-1 s k
0.387
4.7296
10
10
2
2.365
95%
5.0
Blank
-0.001
0.0000
10
10
10
<
QC 0.447 5.5401 10
Submitted for QA/QC- Date: 06/29/15
10
By: (Print)
10 0.554
KAM
111 % 5.0
(sign):
Page 2 of 2

® Laboratories LLc
..,,Analytical Lab
,_ age 26 of 69
a member of The GEL Group IN'.
July 02, 2015
Mary Ann Ogle
Duke Energy Analytical Laboratory
13339 Hagers Ferry Road
Mail Code: MGO3A2
Huntersville, North Carolina 28078
Re: AB GW Assessment Water
Work Order: 375757
SDG: J15060802
Dear Mary:
P4 Box 30712 Charleston. SC 29417
2040 Sange Road Chad eston.SC29407
P 843556.8171
F 843.76Gi.1178
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the
sample(s) we received on June 25, 2015. This original data report has been prepared and reviewed in accordance
with GEL's standard operating procedures.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs
on time every time. We trust that you will find everything in order and to your satisfaction. If you have any
questions, please do not hesitate to call me at [phone], ext. 4443.
Sincerely,
Lindsay Fabra
Project Manager
Purchase Order: 1142110
Enclosures
gel.com

Analytical Lab
Page 27 of 69
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis Report
for
DUP0002 Duke Energy
Client SDG: J15060802 GEL Work Order: 375757
The Qualifiers in this report are defined as follows:
* A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a Tracer compound
** Analyte is a surrogate compound
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the Certificate of Analysis.
The designation ND, if present, appears in the result column when the analyte concentration is not detected above
the limit as defined in the 'U' qualifier above.
This data report has been prepared and reviewed in accordance with GEL Laboratories LLC
standard operating procedures. Please direct any questions to your Project Manager, Lindsay Fabra.
JU,&Y ,
Reviewed by

Analytical Lab
GEL LABORATORIES LLC Page 28 of 69
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis
Company:
Duke Energy Analytical Laboratory
Address :
13339 Hagers Ferry Road
Mail Code: MG03A2
Huntersville, North Carolina 28078
Contact:
Mary Ann Ogle
Project:
AB GW Assessment Water
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
2015020824
375757001
Water
23-JUN-15 14:20
25-JUN-15
Client
Report Date: July 2, 2015
Project: DUKE00225
Client ID: DUP0002
Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method
Metals Analysis-ICP-MS
SW846 3010A/6020A Liquid "As Received"
Uranium-238 U 0.000047
0.000067
0.0002
ug/mL
1
SKJ 07/01/15
1547 1488554 1
Uranium-233 U 0.00
0.00001
0.00005
ug/mL
1
SKJ 07/01/15
1911 1488554 2
Uranium-234 U 0.00
0.00001
0.00005
ug/mL
1
Uranium-236 U 0.00
0.00001
0.00005
ug/mL
1
Rad Gas Flow Proportional Counting
GFPC, Ra228, Liquid "As Received"
Radium-228 U -0.618
1.41
3.00
pCi/L
AXM6 07/01/15
1137 1488665 3
Rad Radium-226
Lucas Cell, Ra226, liquid "As Received"
Radium-226 1.22
0.400
1.00
pCi/L
CXP3 07/01/15
0920 1488667 4
The following Prep Methods were performed:
Method Description
Analyst
Date
Time Prep Batch
SW846 3010A SW 846 3010 Acid Digestion
JXM5
06/26/15
0800
1488553
The following Analytical Methods were performed:
Method Description Analyst Comments
1 SW846 3010A/6020A
2 SW846 3010A/6020A
3 EPA 904,0/SW846 9320 Modified
4 EPA 903.1 Modified
Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits
Barium-133 Tracer GFPC, Ra228, Liquid "As Received" 83.6 (15%-125%)
Notes:

Analytical Lab
GEL LABORATORIES LLC Page 29 of 69
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis
Company:
Duke Energy Analytical Laboratory
Address :
13339 Hagers Ferry Road
Mail Code: MG03A2
Huntersville, North Carolina 28078
Contact:
Mary Ann Ogle
Project:
AB GW Assessment Water
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
2015020838
375757002
Water
23-JUN-15 09:24
25-JUN-15
Client
Report Date: July 2, 2015
Project: DUKE00225
Client ID: DUP0002
Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method
Metals Analysis-ICP-MS
SW846 3010A/6020A Liquid "As Received"
Uranium-238 0.00173
0.000067
0.0002
ug/mL
1
SKJ 07/01/15
1549 1488554 1
Uranium-233 U 0.00
0.00001
0.00005
ug/mL
1
SKJ 07/01/15
1913 1488554 2
Uranium-234 U 0.00
0.00001
0.00005
ug/mL
1
Uranium-236 U 0.00
0.00001
0.00005
ug/mL
1
Rad Gas Flow Proportional Counting
GFPC, Ra228, Liquid "As Received"
Radium-228 U 0.238
1.37
3.00
pCi/L
AXM6 07/01/15
1137 1488665 3
Rad Radium-226
Lucas Cell, Ra226, liquid "As Received"
Radium-226 3.13
0.261
1.00
pCi/L
CXP3 07/01/15
0920 1488667 4
The following Prep Methods were performed:
Method Description
Analyst
Date
Time Prep Batch
SW846 3010A SW 846 3010 Acid Digestion
JXM5
06/26/15
0800
1488553
The following Analytical Methods were performed:
Method Description Analyst Comments
1 SW846 3010A/6020A
2 SW846 3010A/6020A
3 EPA 904,0/SW846 9320 Modified
4 EPA 903.1 Modified
Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits
Barium-133 Tracer GFPC, Ra228, Liquid "As Received" 75.7 (15%-125%)
Notes:

Analytical Lab
Page 30 of 69
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
QC Summary
Report Date: July 2, 2015
Duke Energy Analytical Laboratory Page 1 of 3
13339 Hagers Ferry Road
Mail Code: MG03A2
Huntersville, North Carolina
Contact: Mary Ann Ogle
Workorder: 375757
Parmname
NOM
Sample
Qual
QC
Units
RPD%o
REC%
Range Anlst
Date Time
Metals Analysis - ICPMS
Batch 1488554
QC1203344242
375756001 DUP
Uranium-233
U
ND
U
ND
ug/mL
N/A
SKJ
07/01/1519:03
Uranium-234
U
ND
U
ND
ug/mL
N/A
Uranium-236
U
ND
U
ND
ug/mL
N/A
Uranium-238
0.000232
0.000209
ug/mL
10.4 ^
(+/-0.0002)
07/01/1517:08
QC1203344241
LCS
Uranium-238
0.0496
0.0552
ug/mL
111
(80%-120%)
07/01/1517:01
QC1203344250
LCS
Uranium-233
0.0005
0.00054
ug/mL
108
(80%-120%)
07/01/1519:01
Uranium-234
0.00055
0.000575
ug/mL
105
(80%-120%)
Uranium-236
0.005
0.00601
ug/mL
120
(80%-120%)
QC1203344240
MB
Uranium-233
U
ND
ug/mL
07/01/1518:59
Uranium-234
U
ND
ug/mL
Uranium-236
U
ND
ug/mL
Uranium-238
U
ND
ug/mL
07/01/1517:00
QC1203344243
375756001 MS
Uranium-238
0.0496
0.000232
0.0553
ug/mL
111
(75%-125%)
07/01/1517:09
QC1203344251
375756001 MS
Uranium-233
0.0005
U
ND
0.00054
ug/mL
108
(75%-125%)
07/01/1519:05
Uranium-234
0.00055
U
ND
0.000577
ug/mL
105
(75%-125%)
Uranium-236
0.005
U
ND
0.00601
ug/mL
120
(75%-125%)
QC1203344244
375756001 SDILT
Uranium-233
U
ND
U
ND
ug/L
N/A
07/01/1519:06

Analytical Lab
Page 31 of 69
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
QC Summary
Workorder: 375757
Page 2 of 3
Parmname
NOM
Sample
Qual
QC
Units
RPD%
REC%
Range Anlst
Date Time
Metals Analysis - ICPMS
Batch 1488554
Uranium-234
U
ND
U
ND
ug/L
N/A
Uranium-236
U
ND
U
ND
ug/L
N/A
(0%-10%) SKJ
07/01/1519:06
Uranium-238
0.232
U
ND
ug/L
N/A
(0%-10%)
07/01/1517:10
Rad Gas Flow
Batch 1488665
QC1203344535 375757001 DUP
Radium-228
U
-0.618
U
1.32
pCi/L
N/A
N/AAXM6
07/01/1511:38
QC1203344536 LCS
Radium-228
30.7
29.1
pCi/L
95
(75%-125%)
07/01/1511:38
QC1203344534 MB
Radium-228
U
1.05
pCi/L
07/01/1511:35
Rad Ra-226
Batch 1488667
QC1203344538 375757001 DUP
Radium-226
1.22
1.99
pCi/L
47.6
(0% - 100%) CXP3
07/01/15 09:55
QC1203344540 LCS
Radium-226
24.7
25.2
pCi/L
102
(75%-125%)
07/01/15 09:55
QC1203344537 MB
Radium-226
U
0.431
pCi/L
07/01/15 09:20
QC1203344539 375757001 MS
Radium-226
124
1.22
113
DCi/L
90.8
(75%-125%)
07/01/15 09:55
Notes:
The Qualifiers in this report are defined as follows:
** Analyte is a Tracer compound
< Result is less than value reported
> Result is greater than value reported
BD Results are either below the MDC or tracer recovery is low
E %difference of sample and SD is >10%. Sample concentration must meet flagging criteria
FA Failed analysis.
FB Mercury was found present at quantifiable concentrations in field blanks received with these samples. Data associated with the blank are deemed
invalid for reporting to regulatory agencies
H Analytical holding time was exceeded

Analytical Lab
Page 32 of 69
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
QC Summary
Workorder: 375757
Parmname NOM Sample Qual QC Units RPD%o REC'%
Page 3 of 3
Range Anlst Date Time
J Value is estimated
K Analyte present. Reported value may be biased high. Actual value is expected to be lower.
L Analyte present. Reported value may be biased low. Actual value is expected to be higher.
M M if above MDC and less than LLD
M REMP Result > MDC/CL and < RDL
N Metals --The Matrix spike sample recovery is not within specified control limits
N/A RPD or %Recovery limits do not apply.
N1 See case narrative
ND Analyte concentration is not detected above the detection limit
NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
R Sample results are rejected
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma Spectroscopy --Uncertain identification
UJ Gamma Spectroscopy --Uncertain identification
UL Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.
X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Y Other specific qualifiers were required to properly define the results. Consult case narrative.
^ RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
h Preparation or preservation holding time was exceeded
N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable.
^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than
five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the
RL is used to evaluate the DUP result.
* Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the QC Summary.

Analytical Lab
Page 33 of 69
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Analytical Lab
Page 34 of 69
SAMPLE RECEIPT & REVIEW FORM
Client:
SDG/AR/COCAVork Order: M
Received I3 Y
1
Date Received:
Suspected Hazard Information
o *If Net Counts > 100cpm on samples not marked "radioactive", contact the Radiation Saf ty Group for further
>'
z investigation.
COC/Samples marked as radioactive?
Maximum Net Counts Observed* (Observed Counts - Area Background Counts):
Classified Radioactive 1I or III by RSO?
If yes, Were swipes taken of sample containers < action levels?
COC/Samples marked containing PCBs?
Package, COC, and/or Samples marked as
beryllium or asbestos containing?
If yes, samples are to be segregated as Safety Controlled Samples, and opened by the GEL Safety Group.
Shipped as a DOT Hazardous?
Hazard Class Shipped: UN#:
Samples identified as Foreign Soil?
Sample Receipt Criteria
y
T 2
Comments/Qualifiers (Required for Non -Conforming Items)
1
Shipping containers received intact
Circle Applicable:
?
and sealed.
Sexy m broken Daaged container Leaking container Other (describe)
2
Samples requiring cold preservation
Preservation Method: lee bags Blue ice Dry ice None ther (describe)
within (0 <6 deg. C)?*
*all temperatures are recorded in Celsius
2a
Daily check performed and passed on
Temperature Device Serial #: Y
Secondary Temperature
IR temperature gun?
Device Serial # (If Applicable): Lw` t r ,,,{
[�/ tJl
3
Chain of custody documents included
r
with shipment?
4
Sample containers intact and sealed?
Circle Applicable:
Seals broken Damaged container Leaking container Other (describe)
5
Samples requiring chemical
xx
Sample ID's, containers affected and observed pH:
preservation at proper pH?
f Preservation added, tW
Do Low Level Perchlorate samples
Sample ID's and containers affected:
6
(EPA 6850) have headspace as
re uired?
VOA vials free of headspace (defined
Sample ID's and containers affected:
7
as < 6mm bubble)?
(If yes, immediately deliver to VoLuiles laboratory)
8
Are Encore containers present?
9
Samples received within holding
to's and tests affected:
time?
10
Sample M's on COC match ID's on
Sample ID's and containers affected:
bottles?
11
Date & time on COC match date &
\a
Sample ID's affected:
time on bottles?
/y\
12
Number of containers received match
Sample ID's affected:
number indicated on COC?
13
Are sample containers identifiable as
GEL provided?
14
COC form is properly signed in
relinquished/received sections?
Circle Applicable:
FedEx Air Fed Ex Ground UPS Field Services Courier Other
15
Carrier and tracking number.
Comments (Use Continuation Form if needed):
PM (or PMA) review: Initials --� Date -4/2w c Page % of __j GL-CHL-SR-001 Rev 1

Analytical Lab
Page 35 of 69
List of current GEL Certifications as of 02 July 2015
State
Certification
Alaska
UST-110
Arkansas
88-0651
CLIA
42D0904046
California
2940 Interim
Colorado
SC00012
Connecticut
PH-0169
Delaware
SC000122013-10
DoD ELAP/ ISO17025 A2LA
2567.01
Florida NELAP
E87156
Foreign Soils Permit
P330-12-00283, P330-12-00284
Georgia
SC00012
Georgia SDWA
967
Hawaii
SC000122013-10
Idaho Chemistry
SC00012
Idaho Radiochemistry
SC00012
Illinois NELAP
200029
Indiana
C—SC-01
Kansas NELAP
E-10332
Kentucky SDWA
90129
Kentucky Wastewater
90129
Louisiana NELAP
03046 (AI33904)
Louisiana SDWA
LA150001
Maryland
270
Massachusetts
M—SC012
Michigan
9976
Mississippi
SC000122013-10
Nebraska
NE—OS-26-13
Nevada
SC000122014-1
New Hampshire NELAP
2054
New Jersey NELAP
SC002
New Mexico
SC00012
New York NELAP
11501
North Carolina
233
North Carolina SDWA
45709
Oklahoma
9904
Pennsylvania NELAP
68-00485
Plant Material Permit
PDEP-12-00260
S.Carolina Radchem
10120002
South Carolina Chemistry
10120001
Tennessee
TN 02934
Texas NELAP
T104704235-15-10
Utah NELAP
SC000122015-17
Vermont
VT87156
Virginia NELAP
460202
Washington
C780
West Virginia
997404

Analytical Lab
There are no "Data Exception Reports" associated with this analytical rePAgt.36 of 69

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
Project Name: AB GW Assessment Water - Mayo
Project Number:J15060802
Lot Number:QF26039
Date Completed:07/01/2015
Grant Wilton
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Duke Energy
Lot Number: QF26039
Project Name: AB GW Assessment Water - Mayo
Project Number: J15060802
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QF26039
Project Name: AB GW Assessment Water - Mayo
Project Number: J15060802
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
20150201818
Aqueous
06/23/20151415
06/26/2015
002
20150201821
Aqueous
06/23/20151230
06/26/2015
003
20150201822
Aqueous
06/23/2015 0957
06/26/2015
004
20150201823
Aqueous
06/23/2015 0920
06/26/2015
005
20150201824
Aqueous
06/23/20151420
06/26/2015
006
20150201837
Aqueous
06/23/20151230
06/26/2015
007
20150201840
Aqueous
06/23/20151630
06/26/2015
(7 samples)
Shealy Environmental Services, Inc. Page: 3 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QF26039
Project Name: AB GW Assessment Water - Mayo
Project Number: J15060802
Sample Sample ID
Matrix
Parameter Method
Result Q
Units
Page
001
20150201818
Aqueous
Alkalinity SM 2320B-
43
mg/L
5
001
20150201818
Aqueous
Bicarbonate Alkalinity SM 2320B-
43
mg/L
5
002
20150201821
Aqueous
Alkalinity SM 2320B-
76
mg/L
7
002
20150201821
Aqueous
Bicarbonate Alkalinity SM 2320B-
75
mg/L
7
003
20150201822
Aqueous
Alkalinity SM 2320B-
97
mg/L
9
003
20150201822
Aqueous
Bicarbonate Alkalinity SM 2320B-
96
mg/L
9
004
20150201823
Aqueous
Alkalinity SM 2320B-
190
mg/L
11
004
20150201823
Aqueous
Bicarbonate Alkalinity SM 2320B-
190
mg/L
11
005
20150201824
Aqueous
Alkalinity SM 2320B-
210
mg/L
13
005
20150201824
Aqueous
Bicarbonate Alkalinity SM 2320B-
210
mg/L
13
006
20150201837
Aqueous
Alkalinity SM 2320B-
76
mg/L
15
006
20150201837
Aqueous
Bicarbonate Alkalinity SM 2320B-
76
mg/L
15
(12 detections)
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QF26039-001
Description: 20150201818 Matrix: Aqueous
Date Sampled:06/23/2015 1415 Project Name: AB GW Assessment Water -
Date Received:06/26/2015 Project Number: J15060802
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 06/30/2015 2036 HMA 78532
1 (Bicarbonate ) SM 2320B-2011 1 06/30/2015 2036 HMA
1 (Carbonate Al) SM 2320B-2011 1 06/30/2015 2036 HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
43
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
43
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane
Client: Duke Energy Laboratory ID: QF26039-001
Description: 20150201818 Matrix: Aqueous
Date Sampled:06/23/2015 1415 Project Name: AB GW Assessment Water -
Date Received:06/26/2015 Project Number: J15060802
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/29/2015 2154 JJG 78405
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF26039-002
Description: 20150201821 Matrix: Aqueous
Date Sampled:06/23/2015 1230 Project Name: AB GW Assessment Water -
Date Received:06/26/2015 Project Number: J15060802
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 06/30/2015 2042 HMA 78532
1 (Bicarbonate ) SM 2320B-2011 1 06/30/2015 2042 HMA
1 (Carbonate Al) SM 2320B-2011 1 06/30/2015 2042 HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
76
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
75
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane
Client: Duke Energy Laboratory ID: QF26039-002
Description: 20150201821 Matrix: Aqueous
Date Sampled:06/23/2015 1230 Project Name: AB GW Assessment Water -
Date Received:06/26/2015 Project Number: J15060802
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/29/2015 1434 DCS 78365
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF26039-003
Description: 20150201822 Matrix: Aqueous
Date Sampled:06/23/2015 0957 Project Name: AB GW Assessment Water -
Date Received:06/26/2015 Project Number: J15060802
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 06/30/2015 2048 HMA 78532
1 (Bicarbonate ) SM 2320B-2011 1 06/30/2015 2048 HMA
1 (Carbonate Al) SM 2320B-2011 1 06/30/2015 2048 HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
97
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
96
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane
Client: Duke Energy Laboratory ID: QF26039-003
Description: 20150201822 Matrix: Aqueous
Date Sampled:06/23/2015 0957 Project Name: AB GW Assessment Water -
Date Received:06/26/2015 Project Number: J15060802
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/29/2015 2207 JJG 78405
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 10 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF26039-004
Description: 20150201823 Matrix: Aqueous
Date Sampled:06/23/2015 0920 Project Name: AB GW Assessment Water -
Date Received:06/26/2015 Project Number: J15060802
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 06/30/2015 2055 HMA 78532
1 (Bicarbonate ) SM 2320B-2011 1 06/30/2015 2055 HMA
1 (Carbonate Al) SM 2320B-2011 1 06/30/2015 2055 HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
190
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
190
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 11 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane
Client: Duke Energy Laboratory ID: QF26039-004
Description: 20150201823 Matrix: Aqueous
Date Sampled:06/23/2015 0920 Project Name: AB GW Assessment Water -
Date Received:06/26/2015 Project Number: J15060802
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/29/2015 2231 JJG 78405
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 12 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF26039-005
Description: 20150201824 Matrix: Aqueous
Date Sampled:06/23/2015 1420 Project Name: AB GW Assessment Water -
Date Received:06/26/2015 Project Number: J15060802
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 06/30/2015 2102 HMA 78532
1 (Bicarbonate ) SM 2320B-2011 1 06/30/2015 2102 HMA
1 (Carbonate Al) SM 2320B-2011 1 06/30/2015 2102 HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
210
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
210
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 13 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane
Client: Duke Energy Laboratory ID: QF26039-005
Description: 20150201824 Matrix: Aqueous
Date Sampled:06/23/2015 1420 Project Name: AB GW Assessment Water -
Date Received:06/26/2015 Project Number: J15060802
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/30/2015 1348 DCS 78512
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF26039-006
Description: 20150201837 Matrix: Aqueous
Date Sampled:06/23/2015 1230 Project Name: AB GW Assessment Water -
Date Received:06/26/2015 Project Number: J15060802
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 06/30/2015 2108 HMA 78532
1 (Bicarbonate ) SM 2320B-2011 1 06/30/2015 2108 HMA
1 (Carbonate Al) SM 2320B-2011 1 06/30/2015 2108 HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
76
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
76
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 15 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane
Client: Duke Energy Laboratory ID: QF26039-006
Description: 20150201837 Matrix: Aqueous
Date Sampled:06/23/2015 1230 Project Name: AB GW Assessment Water -
Date Received:06/26/2015 Project Number: J15060802
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/30/2015 1358 DCS 78512
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF26039-007
Description: 20150201840 Matrix: Aqueous
Date Sampled:06/23/2015 1630 Project Name: AB GW Assessment Water -
Date Received:06/26/2015 Project Number: J15060802
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 06/30/2015 2113 HMA 78532
1 (Bicarbonate ) SM 2320B-2011 1 06/30/2015 2113 HMA
1 (Carbonate Al) SM 2320B-2011 1 06/30/2015 2113 HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 17 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane
Client: Duke Energy Laboratory ID: QF26039-007
Description: 20150201840 Matrix: Aqueous
Date Sampled:06/23/2015 1630 Project Name: AB GW Assessment Water -
Date Received:06/26/2015 Project Number: J15060802
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/30/2015 1410 DCS 78512
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: QF26039
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Inorganic non-metals - MB
Sample ID: QQ78532-001 Matrix: Aqueous
Batch:78532
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 06/30/20151829
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF26039
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Inorganic non-metals - LCS
Sample ID: QQ78532-002 Matrix: Aqueous
Batch:78532
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 97 1 97 90-110 06/30/20151834
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF26039
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane - MB
Sample ID: QQ78365-001 Matrix: Aqueous
Batch:78365
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 06/29/20151015
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF26039
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane - LCS
Sample ID: QQ78365-002 Matrix: Aqueous
Batch:78365
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 130 1 83 70-130 06/29/2015 0949
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF26039
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane - LCSD
Sample ID: QQ78365-003 Matrix: Aqueous
Batch:78365
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 110 1 75 10 70-130 30 06/29/20151002
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF26039
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane - MB
Sample ID: QQ78405-001 Matrix: Aqueous
Batch:78405
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 06/29/20151615
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF26039
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane - LCS
Sample ID: QQ78405-002 Matrix: Aqueous
Batch:78405
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 120 1 80 70-130 06/29/20151544
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF26039
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane - LCSD
Sample ID: QQ78405-003 Matrix: Aqueous
Batch:78405
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 110 1 73 8.9 70-130 30 06/29/20151554
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF26039
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane - MB
Sample ID: QQ78512-001 Matrix: Aqueous
Batch:78512
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 06/30/20151255
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF26039
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane - LCS
Sample ID: QQ78512-002 Matrix: Aqueous
Batch:78512
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 120 1 82 70-130 06/30/20151233
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF26039
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane - LCSD
Sample ID: QQ78512-003 Matrix: Aqueous
Batch:78512
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 120 1 80 2.7 70-130 30 06/30/20151244
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF26039
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC
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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
Slimly Fnv-sunro_ental Servi:cc, Inc, gage I ur' !
Ixsumcm rFWrobsr F-AQ41!6 RepliLcea Dacz,. I UO3. i4
ft-Onion htimheb' 11 Effw6kz Draw- WWI 5
atuple Rectipl Checklist SRQ
Client:Cooler Inspected hyldat€='-f I.ot
Merino of receipt, ❑ SESI ❑ Client ❑ UPS ❑ FedEx ❑ Airborne Exp 2"Otlter
Yes LJ
No Z
I
1 1. Were custody seals pre&enl on the 000let?
Yes ❑ No A 2. If custody seals wim: presunl, w= they intact and unbroken?
Cooler IDiOriginaI tcrnperaturr upon rmvipb erived (Correr.;Led) temperature upon receipt:
? '" 1 W �A °C 1 4 °C i + cc I 1 MC
Iw :And- ❑ Temperature lank Against Boale� iR Ciuu 11Jh,- _ IR Gun Correction Factor: C�-cz- aC
Method of coulant: L2rWetice ❑ filue Ice El I) ' lee lgoue
Yes ❑
Na ❑
NA
3_ If temperature aE any coulcr vxecvdrd 6.00C, was Project Manager notified?
notified by SRC, phone, note (eircle oneot ), her: _
(tor
(>;or coolers received aria commercial courier, P s are to he notified
immediately,)
Yes ❑
o ❑
l a
4. Is the oommmial. courier's packing slip att iched to this farm'?
5- Were proper custody procedures 7 ' uishedlrecesved) followed?
Yes
Nis ❑
Yes ❑
No ❑
LEA
5a Wcm samples reli,lc�uish+ad by client t,� caommercia] oi>urier?
Yes
No
6, 'Were sample IDs lasted OR the COC?
Yes
140 ❑
7. Wcr'e sam lq JDs listed on all sam lc containers?
Yes
No ❑
8- Was collection elate & time listed on the . C?
-YU
No ❑
9- Was oollootion date & time listed on all sF,tn le conwiners?
Yes
NO ❑
10. Did all contatnk-r label irkformati n (11D, date, time) a with the C-00
yc;
No ❑
1 I - Were tests to bc formed hstcd pan the COC?
y s
[do ❑
12- Dud all sawplcs surive in the proper containers for each test`?
Yes
Na
13, Dirt all containers arrive in goad cononditiunbrakSEL lids en atc. ?
-
Yes
No
14- Was adequate sample. vol arne availahle?
Ycs ❑
No
15. We:re aU samples received within ii the holding time or 48 hours, whichever
comcs first?
16- Were any samples containers missing?
Yes ❑
Yes ❑
NuZv�
No
170 - Wcrc thcrc.any gvoess symples not listed on COC?
Yes
Tv
Ids ❑
18, Were bubbles prescot �" a -size" (W'or 6uun in diameter in any VOA vials
NA
19. Were all metals1G&G[HENVwutrient sam leg received at a H of <2`�
�Yesff���D
NA
20- Wcre nil cyanide andfor sulfide sam lbs rtteivtd at a pH ] 12?
Vcs []
No❑
NA
21. Were all applicable NUBr1Y-N.+cyunidclphcnvl (<0-2rag ) sarsiptes free of
residual chlorine? _
Yes
No ❑
-NA
22- Were collection temperatures docurneated on the COC for NC samples?
Yes ❑
No ❑
MA 0,,23-
Were client remarkOrNuests (i.c. requested dilutions, MSIMSD desigliations,
etc --- cormcdy transcribed from the 00C into the comment seotion in I.114 S?
24-- Was the quotc nutnher used taken from the coaminer labc0
Yes ❑
IVa
ample Preservatlon (Must he completed for allay samples) incorrectly presened or with beacispacc.)
sarnplu(s)� were received incorrectly preserved and were adjusted;
accordingly in sample rcceivin with '14,SO4jEl 0.3,HC1,Na0H using SR 9
Som la(s) r we received v4iih bubbles >6 mm in diary =.
Sam lc s) wepe received with TRC >02h rn 11 if #21 is Colo)
SC Ilrinki>lig Water Project 5amplc(3) pH verified to be - 2 by Lute
sump le(s) vw'crc nui Teceiv'ed at a pH of f2 and were Austed accordln i' L;Siag q1. .
tam lc labels applied by: Verified by: D me'
mmcnts:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

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Analytical Lab
t,mAIN OF GU-S-1 ODY RtCOKU ANO ANALYSIS REQUEST FORM Page 69 of 69
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IE Energy Analytical Laboratory Aftlytical Laboratory Use Only
'Order al, 7 NC
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Sample Log M47 ITS'SZ46 ;L0%Vw By Emu & Tk" SAMPLE PROGRAM
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ELEMENTS by ICP MS (TRM): As. Be. CA. Co. Cr. Cu, Mo. Ni. Pb. Sb, Se, TI (ILL). V (LU
ELEMENTS by ICP rkTRU): At, Ba, 13, Fc, Un, Sr, Zn JCP Undigestad Ca, Mg, K,Nj I-Ig by 245A
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Add. Cost Will Apply
Dissolved metals: all metals ICP, IMS,Hg
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