NC0001899_Permit Issuance_20021230 (2)

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FACILITY:
COLTINTYiFZENUSE NUMEER -------
crrY' PERN= NUMBER
COUNTY:
Permit Information that Needs to be Incorpora.ed into Future Permit Revisions:
DATE
6.4.
n
CONaIENTS

State of North Carolina 0
Department of Environment
and Natural Resources
Division of Water Quality
Michael F. Easley, Governor
William G. Ross, Jr., Secretary
Alan W. Klimek, P.E., Director
Ms. Elin E. Gabriel, Plant Manager
Honeywell International, Incorporated
383 Pea Ridge Road
Moncure, North Carolina 27559
Dear Ms. Gabriel:
WA
NCOD ENR
NORTH CAROLINA DEPARTMENT OF
ENVIRONMENT AND NATURAL F'ESOURCES
December 30, 2002
JAN 2 2 0003
SzC �e�r,eif � na", a C/
( - 3 —0)� I e Tf_ —,
Subject: NPDES Permit Issuance
Honeywell International WWTP
NPDES Permit No. NCOOOIS99
Chatham County
Attached to this letter is the final NPDES permit for Honeywell International, Incorporated,
NPDES Permit No. NC0001899. This permit is issued pursuant to the requirements of North
Carolina General Statute 143-215.1 and the Memorandum of Agreement between North Carolina
and the U.S. Environmental Protection Agency dated May 9, 1994.
Based on your letter dated December 4, 2002, the following changes (and clarifications) have been
made to the permit from the draft permit:
• Thank you for bringing up the minor errors (sampling types) in the draft permit. They have
now been corrected.
• The monitoring and sampling points have been clarified in the permit (refer to Condition
A.(6.)I.
• Fle)dbflity has been provided in the permit for the OCPSF analytical detection levels (refer to
Condition A.(7.)1.
• After careful review of the previous permit, we cannot determine why hexachlorobenzene and
benzo(k)fluoranthene were limited as 0.300 and 0.440 lbs/day daily maximums, respectively.
Both the OCPSF value and the human health values were compared and reviewed again. The
limit listed in the draft permit and this final permit reflect the appropriate mass -based limit
using the OCPSF concentration and process flow. We regret the error in the previous permit.
• The daily maximum monitoring for polynuclear aromatic hydrocarbons (PAH's) was inserted
based on the North Carolina human health standard. Please note that because individual
parameters are limited via the OCPSF parameters, this limit has been changed to a monitoring
requirement. The values will be evaluated at the next permit renewal to determine if a limit
may be necessary.
1617 Mal Service Center, Raleigh, North Carolina 27699-1617 919 733-5083, extension 510 (tax) 919 733-0719
An Equal Opportunity Affirmative Action Employer Susan.A.Wilson0ranail.net

0
If any parts, measurement frequencies, or sampling requirements contained in this permit
are unacceptable to you, you have the right to an adjudicatory hearing upon written request
within thirty (30) days following receipt of this letter. This request must be in the form of a
written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed
with the office of Administrative Hearings, Mail Service Center 6714, Raleigh, North Carolina
27699-6714. Unless such a demand is made, this permit shall be final and binding.
Please take notice that this permit is not transferable except after notice to the Division of
Water Quality. The Division of Water Quality may require modification or revocation and
reissuance of the permit.
This permit does not affect the legal requirements to obtain other permits which may be required
by the Division of Water Quality, the Division of Land Resources. the Coastal Area Management Act, or
any other federal or local governmental permit.
If you have any questions regarding the NPDES permit, please contact Susan Wilson at
(919) 733 - 5083, extension 510.
Sincerely,
Original Signed BY
David K Goodrich
Alan W. Klimek, P.E.
cc: Raleigh Regional Office/Water Quality Section
Central Files
NPDES Unit
Aquatic Toxicology Unit
EPA Region IV, Roosevelt Childress (Permit, Fact Sheet amendment)
W.L. Boyer, REM
Honeywell International, Inc.
c38 Pea Ridge Road
Moncure, NC 27559

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STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful
standards and regulations promulgated and adopted by the North Carolina Water Quality
Commission, and the Federal Water Pollution Control Act, as amended,
Honeywell International, Incorporated
is hereby authorized to discharge wastewater from a facility located at the
Honeywell International WWTP
East of Moncure off Pea Ridge Road
Chatham County
to receiving waters designated as the Haw River in the Cape Fear River Basin in accordance
with the discharge limitations, monitoring requirements, and other conditions set forth in
Parts I, II, III and IV hereof.
This permit shall become effective February 1, 2003.
This permit and the authorization to discharge shall expire at midnight on July 31, 2006.
Signed this day December 30, 2002.
Original Signed By
David A. Goodrich
Alan W. Klimek, P.E., Director
Division of Water Quality
By the Authority of the Environmental Management Commission
Permit NC0001899

SUPPLEMENT TO PERMIT COVER SHEET
Honeywell International, Incorporated is hereby authorized to:
1. Continue to discharge process and domestic effluent at a permitted flow not
to exceed 0.244 MGD (outfall 001). from a wastewater treatment facility
consisting of an aeration basin with floating aerators, clarifier, sludge
drying bed, 2 alum settling ponds and polishing pond (for water treatment -
decant to chlorination basin), chlorination/chlorine contact basin, and
effluent flow measurement, and
2. Continue to discharge stormwater, condensate, and firepond overflow
(outfall 002) from facilities located at the Honeywell International
Wastewater Treatment Facility, off Pea Ridge Road east of Moncure in
Chatham County, and,
3. Discharge wastewater from said treatment works via outfall 001 at the
location specified on the attached map into the Haw River and via outfall
002 into an unnamed tributary to Shaddox Creek, both of which are
classified WS-fV waters in the Cape Fear River Basin.
NPDFS No. NCOD01899

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HONEYWELL INTERNATIONAL INC
NPDES NC0001399
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NPDES OUTFALL 002
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A. (1) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS (001)
During the period beginning on the effective date of the permit and lasting until expiration, the
Permittee is authorized to discharge 0.244 MGD of industrial and domestic wastewater from outfall
001. Such discharges shall be limited and monitored by the Permittee as specified below:
Effluent
Characteristics
Limits
Monitorina Requirements
Monthly Average
Weekly
Average
Daily Maximum
Measurement
Frequency
Sample
Type
Sample Locationi
Flow
0.244 MGD
Continuous
Recording
Influent or Effluent
BOD, 5 day (2VC)
10.4 pounds/day
16.7 poundstday
Weekly
Composite
Effluent
Total Suspended Solids
5.0 pounds/day
10.6 pounds/day
Weekly
Composite
Effluent
Oil and Grease
20 pounds/day
30 pounds/day
Weekly
Grab
Effluent
Fecal Coliform
Monthly
Grab
Effluent
Temperature ("C)
Monthly
Grab
Effluent
Upstream & Downstream
Conductivity
Monthly
Grab
Effluent
Upstream & Downstream
Dissolved Oxygen
Monthly
Grab
Effluent
Upstream & Downstream
ChronicToxiety2
Quarterly
Composite
Effluent
Total Nitrogen
(NO2 + NO3 +TKN)
Monthly
Composite
Effluent
Total Phosphorus
Monthly
Composite
Effluent
OCPSF3
Annually
Grab
Effluent
p114
6-9
Continuous
Recording
Effluent
Total Residual Chlorine5
Monthly
Grab
Effluent
Footnotes:
1. Upstream: valve at Permittee's river water pump house. Downstream: nearest accessible point at
least 100 yards below the outfall and above the confluence of the Deep and Haw Rivers. Instream
monitoring is provisionally waived due to the permittee's participation in the Lower Cape
Fear River Basin Association. Instream monitoring shall be conducted as stated in this
permit should the permittee end its participation in the Association.
2. Chronic Toxicity (Ceriodaphnia) Chronic P/F at 0.94%: January, April, July, and October (see
Condition A. (3)).
3. Refer to Conditions A. (7) and A. (8) regarding OCPSF monitoring. Where any compound is
detected, quarterly monitoring is required for that compound until not detected in twelve
consecutive samples. Honeywell may use EPA test method 524.2 to monitor OCPSF parameters
(provided the method allows a detection level at or below the permitted limit).
4. The pH shall be monitored continuously at the effluent. In accordance with 40 CFR 401.17, the
total time during which the pH values are allowed to be less than 6.0 standard units or greater
than 9.0 standard units shall not exceed 7 hours and 26 minutes in any calendar month, and no
individual excursion outside the 6 to 9 range shall exceed 60 minutes.
5. Chlorine monitoring is required if chlorine is used as a disinfectant or elsewhere in the treatment
process.
There shall be no discharge gffloating solids or visible foam in other than trace amounts.
NPDES No. NC0001899

% 4b
A. (2.) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS (002)
During the period beginning on the effective date of the permit and lasting until expiration, the
Permittee is authorized to discharge stormwater, steam condensate, and firepond overflow
wastewater from Outfall 002. Such discharges shall be limited and monitored by the Permittee as
specified below:
Effluent Characteristics
Limits
Monitoring Requirements
Monthly
Average
Weekly
Average
Daily
Maximum
Measurement
Frequency
Sample Type
Sample
Location
Flow
Weekly
Instantaneous
Effluent
Temperature 'C i
Weekly
Grab
Effluent
Total Residual Chlorine2
Weekly
Grab
Effluent
Total Fluoride
Annually
Composite
Effluent
Total Zinc
Annually
Composite
Effluent
Acute Toxicity,
Annually
Grab
Effluent
H4
6-9
Weekly
Grab
Effluent
Footnotes:
1. The temperature of the effluent shall be such as not to cause an increase in the temperature of the
receiving stream of more than 2.8°C and in no case cause the ambient water temperature to exceed
32°C.
2. Chlorine monitoring is required only if chlorine is added in the wastewater contributors stated
above.
3. Acute Toxicity (Fathead Minnow Annual Monitoring [see Condition A. (4)1.
4. The pH shall not be less than 6.0 standard units nor greater than 9.0 standard units.
There shall be no discharge of floating solids or visible foam in other than trace amounts.
A. (3) CHRONIC TOXICITY PERMIT LIMIT (Quarterly)
The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant
mortality to Ceriodaphnia dubia at an effluent concentration of 0.94 %.
The permit holder shall perform at a minimum, quarterlu monitoring using test procedures outlined in
the "North Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised February 1998, or
subsequent versions or "North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure"
(Revised -February 1998) or subsequent versions. The tests will be performed during the months of
January, April, July, and October. Effluent sampling for this testing shall be performed at the
NPDES permitted final effluent discharge below all treatment processes.
If the test procedure performed as the first test of any single quarter results in a failure or ChV
below the permit limit, then multiple -concentration testing shall be performed at a minimum, in
each of the two following months as described in "North Carolina Phase II Chronic Whole
Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent versions.
The chronic value for multiple concentration tests will be determined using the geometric mean of the
highest concentration having no detectable impairment of reproduction or survival and the lowest
concentration that does have a detectable impairment of reproduction or survival. The definition of
"detectable impairment," collection methods, exposure regimes, and further statistical methods are
specified in the "North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -
February 1998) or subsequent versions.
NPDES No. NC0001899

A. (3) CHRONIC TOXICITY PERMIT LIMIT (Quarterly)
(continued)
All toxicity testing results required as part of this permit condition will be entered on the Effluent
Discharge Monitoring Form (MR-1) for the months in which tests were performed, using the parameter
code TGP3B for the pass/fail results and THP3B for the Chronic Value. Additionally, DWQ Form AT-3
(original) is to be sent to the following address:
Attention: NC DENR / DWQ / Environmental Sciences Branch
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
Completed Aquatic Toxicity Test Forms shall be flied with the Environmental Sciences Branch no later
than 30 days after the end of the reporting period for which the report is made.
Test data shall be complete, accurate, include all supporting chemical/physical measurements and all
concentration/response data, and be certified by laboratory supervisor and ORC or approved designate
signature. Total residual chlorine of the effluent toxicity sample must be measured and reported if
chlorine is employed for disinfection of the waste stream.
Should there be no discharge of flow from the facility during a month in which toxicity monitoring is
required, the permittee will complete the information located at the top of the aquatic toxicity (AT) test
form indicating the facility name, permit number, pipe number, county, and the month/year of the
report with the notation of "No Flow" in the comment area of the form. The report shall be submitted to
the Environmental Sciences Branch at the address cited above.
Should the permittee fail to monitor during a month in which toxicity monitoring is required,
monitoring will be required during the following month.
Should any test data from this monitoring requirement or tests performed by the North Carolina
Division of Water Quality indicate potential impacts to the receiving stream, this permit may be re-
opened and modified to include alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control
organism survival, minimum control organism reproduction, and appropriate environmental controls,
shall constitute an invalid test and will require immediate follow-up testing to be completed no later
than the last day of the month following the month of the initial monitoring.
A. (4) ACUTE TOXICITY MONITORING (ANNUAL)
The permittee shall conduct annual toxicity tests using protocols defined as definitive in E.P.A.
Document EPA/600/4-90/027 entitled "Methods for Measuring the Acute Toxicity of Effluents to
Freshwater and Marine Organisms." The monitoring shall be performed as a Fathead Minnow
(Pimephales promelas) 24-hour static test. Effluent samples for self -monitoring purposes must be
obtained below all waste treatment. The permittee will conduct one test annually, with the annual
period beginning in January of the calendar year of the effective date of the permit. The annual test
requirement must be performed and reported by June 30. If no discharge occurs by June 30,
notification will be made to the Division by this date. Toxicity testing will be performed on the next
discharge event for the annual test requirement.
The parameter code for this test is TAE6C. All toxicity testing results required as part of this permit
condition will be entered on the Effluent Discharge Form (MR-1) for the month in which it was
performed, using the appropriate parameter code. Additionally, DWQ Form AT-1 (original) is to be sent
to the following address:
Attention: NC DENR / DWQ / Environmental Sciences Branch
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
NPDES No. NC0001899

% 04
A. (4) ACUTE TOXICITY MONITORING (ANNUAL)
(continued)
Test data shall be complete and accurate and include all supporting chemical/physical measurements
performed in association with the toxicity tests, as well as all dose/response data. Total residual
chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for
disinfection of the waste stream.
Should any test data from either these monitoring requirements or tests performed by the North
Carolina Division of Water Quality indicate potential impacts to the receiving stream, this permit may
be re -opened and modified to include alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control
organism survival and appropriate environmental controls, shall constitute an invalid test and will
require immediate follow-up testing to be completed no later than the last day of the month following
the month of the initial monitoring.
A. (5) WASTEWATER TREATMENT PONDS
The wastewater treatment ponds at the facility shall maintain a freeboard height of 2 feet.
A. (6) SAMPLING POINTS
The permittee may perform sampling after the chlorine contact chamber, for all parameters except
those listed below:
➢ Toxicity sampling may be conducted near the end -of -pipe prior to discharge into the Haw River.
➢ In order to avoid interference with chlorine addition, sampling for chloroform may be collected
after the clarifier.
A. (7) ANALYTICAL DETECTION LEVELS
When an approved analytical protocol with the appropriate minimum detection level is followed and a
result of "non -detectable" or "below quantitation limit" is obtained, the permittee will be considered to
be in compliance with the numerical permit limit for that pollutant.
)This condition is inserted to acknowledge that the low equivalent concentration limits imposed by the
OCPSF guidelines, combined with the additional non-OCPSF process flows, will result in situations
where the detection limit of the EPA approved analytical protocols will not be sufficiently low enough to
verify that a particular pollutant is in compliance with the permit limits.)
NPDES No. NC0001899

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PART I
(Continued)
Section B. Schedule of Com fiance
1. The perrrnttee shall comply with Final Effluent Limitations specified for discharges in accordance with
the following schedule:
Pemtittee shall comply with Final Effluent limitations by the effective date of the permit
unless specified below.
2. Permittee shall at all times provide the operation and maintenance necessary to operate the existing
facilities at optimum efficiency.
3. No later than 14 calendar days following a date identified in the above schedule of compliance, the
pernuttee shall submit either a report of progress or, in the case of specific actions being required by
identified dates, a written notice of compliance or noncompliance. In the latter case, the notice shall
include the cause of noncompliance, any remedial actions taken, and the probability of meeting the neat
schedule requirements.

PART II
STANDARD CONDITIONS FOR NPDES PERMITS
SECTION A. DEFINITIONS
1. Permit Issuing Authority: The Director of the Division of Water Quality.
2. DEM or "die Dinsion" Means the Division of Water Quality, Department of Environment and Natural
Resources.
3. LU, Used herein means the North Carolina Environmental Management Commission.
4. Act or, "the Act" The Federal Water Pollution Control Act, also known as the Clean Water Act, as amended,
33 USC 1251, et. seq.
5. Mass/Day Measurements
a. The "monthly average discharge" is defined as the total mass of all daily discharges sampled and/or
measured during a calendar month on which daily discharges are sampled and measured, divided by the
number of daily discharges sampled and/or measured during such month. It is therefore, an arithmetic
mean found by adding the weights of the pollutant found each day of the month and then dividing this sum
by the number of days the tests were reported. The limitation is identified as "Monthly Average" in Part I of
the pemhit.
b. The "weekly average discharge" is defined as the total mass of all daily discharges sampled and/or measured
during the calendar week (Sunday - Saturday) on which daily discharges are sampled and measured, divided
by the number of daily discharges sampled and/or measured during such week. It is, therefore, an
arithmetic mean found by adding the weights of pollutants found each day of the week and then dividing
this sum by the number of days the tests were reported. This limitation is identified as "Weekly Average" in
Pan I of the permit.
c. The "maximum daily discharge" is the total mass (weight) of a pollutant discharged during a calendar day. If
only one sample is taken during any calendar day the weight of pollutant calculated from it is the "maximum
daily discharge." This limitation is identified as "Daily Maximum;' in Part I of the permit.
d. The "average annual discharge" is defined as the total mass of all daily discharges sampled and/or measured
during the calendar year on which daily discharges are sampled and measured, divided by the number of
daily discharges sampled and/or measured during such vear. It is, therefore, an arithmetic mean found by
adding the weights of pollutants found each day of the year and then dividing this sum by the number of
days the tests were reported. This limitation,
is defined as "Annual Average" in Part I of the pemdt.
G. Concentration Measurement
a. The "average monthly concentration," other than for fecal coliform bacteria, is the sum of the concentrations
of all daily discharges sampled and/or measured during a calendar month on which daily discharges are
sampled and measured, divided by the number of daily discharges sampled and/or measured during such
month (arithmetic mean of the daily concentration values). The daily concentration value is equal to the
concentration of a composite sample or in the case of grab samples is the arithmetic mean (weighted by flow
value) of all the samples collected during that calendar day. The average monthly count for fecal coliform
bacteria is the geometric mean of the counts for samples collected during a calendar month. This limitation
is identified as "Monthly Average" under "Other Limits" in Part I of the permit.

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6. b. The "average weekly concentration," other than for fecal colifotm bacteria, is the sum of the concentrations
of all daily discharges sampled and/or measured during a calendar week (Sunday/Saturday) on which daily
discharges are sampled and measured divided by the number of daily discharges sampled and/or measured
during such week (arithmetic mean of the daily concentration values). The daily concentration value is equal
to the concentration of a composite sample or in the case of grab samples is the arithmetic mean (weighted
by flow value) of all the samples collected during that calendar day. The average weekly count for fecal
coliform bacteria is the geometric mean of the counts for samples collected during a calendar week. This
limitation is identified as "Weekly Average" under "Other Limits" in Part I of the permit.
c. The "maximum daily concentration" is the concentration of a pollutant discharge during a calendar day. if
only one sample is taken during any calendar day the concentration of pollutant calculated from it is the
"Maximum Daily Concentration". It is identified as "Daily Maximum" under "Other Limits" in Part I of the
permit.
d. The "average annual concentration," other than for fecal coliform bacteria, is the sum of the concentrations
of all daily discharges sampled and/or measured during a calendar year on which daily discharges are
sampled and measured divided by the number of daily discharges sampled and/or measured during such
year (arithmetic mean of the daily concentration values). The daily concentration value is equal to the
concentration of a composite sample or in the case of grab samples is the arithmetic mean (weighted by flow
value) of all the samples collected during that calendar day. The average yearly count for fecal coliform
bacteria is the geometric mean of the counts for samples collected during a calendar year. This limitation is
identified as "Annual Average" under "Other Limits" in Part I of the permit.
e. The "daily average concentration" (for dissolved oxygen) is the minimum allowable amount of dissolved
oxygen required to be available in the effluent prior to discharge averaged over a calendar day. If only one
dissolved oxygen sample is taken over a calendar day, the sample is considered to be the "daily average
concentration" for the discharge. It is identified as "daily average" in the text of Part I.
f. The "quarterly average concentration" is the average of all samples taken over a calendar quarter. It is
identified as "Quarterly Average Limitation" in the text of Part I of the permit.
g. A calendar quarter is defined as one of the following distinct periods: January through March, April through
June, July through September, and October [!rough December.
7. Other Measurements
a. Flow, (NIGD): The flow limit expressed in this permit is the 24 hours average flow, averaged monthly. It is
determined as the arithmetic mean of the total daily flows recorded during the calendar month.
b. An "instantaneous flow measurement" is a measure of flow taken at the time of sampling, when both the
sample and flow will be representative of the total discharge.
c. A "continuous flow measurement" is a measure of discharge flow from the facility, which occurs continually
without interruption throughout the operating hours of the facility. Flow shall be monitored continually
except for the infrequent times when there may be no flow or for infrequent maintenance activities on the
flow device.
a. Composite Sample: A composite sample shall consist of:
(1) a series of grab samples collected at equal time intervals over a 24 hour period of discharge and
combined proportional to the rate of flow measured at the time of individual sample collection, or

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8. a. (2) a series of grab samples of equal volume collected over a 24-hour period with the time intervals between
samples determined by a preset number of gallons passing the sampling point. Flow measurement
between sample intervals shall be determined by use of a flow recorder and totalizer, and the present
gallon interval between sample collection fixed at no greater than 1 /24 of the expected total daily flow at
the treatment system, or
(3) a single, continuous sample collected over a 24-hour period proportional to the rate of flow.
In accordance with (1) above, the time interval between influent grab samples shall be no greater than
once per hour, and the time interval between effluent grab samples shall be no greater than once per hour
except at wastewater treatment systems having a detention time of greater than 24 hours. In such cases,
effluent grab samples may be collected at time intervals evenly spaced over the 24-hour period which are
equal in number of hours to the detention time of the system in number of days. However, in no case
may the time interval between effluent grab samples be greater than six (6) hours nor the number of
samples less than four (4) during a 24-hour sampling period.
b. Grab Sample: Grab samples are individual samples collected over a period of time not exceeding 15
minutes; the grab sample can be taken manually. Grab samples must be representative of the discharge or
the receiving waters.
9. Calculation of Means
Arithmetic Mean: The arithmetic mean of any set of values is the summation of the individual values divided
by the number of individual values.
b. Geometric Mean: The geometric mean of any set of values is the Nth root of the product of the individual
values where N is equal to the number of individual values. The geometric mean is equivalent to the antilog
of the arithmetic mean of the logarithms of the individual values. For purposes of calculating the geometric
mean, values of zero (0) shall be considered to be one 0).
c. Weighted by Flow Value: Weighted by flow value means the summation of each concentration times its
respective flow divided by the summation of the respective flows.
10. Calendar Dav A calendar day is defined as the period from midnight of one day until midnight of the next
day. However, for purposes of this permit, any consecutive 24-hour period that reasonably represents the
calendar day may be used for sampling.
11. Hazardous Substance: A hazardous substance means any substance designated under 40 CFR Part 116
pursuant to Section 311 of the Clean Water Act.
12. Toxic Pollutant: A toxic pollutant is any pollutant listed as toxic under Section 307(a)(1) of the Clean Water
Act.
SECTION B. GENERAL CONDITIONS
L Duty to Compll
The pemrittee must comply with all conditions of this permit. Any permit noncompliance constitutes a violation
of the Clean Water Act and is grounds for enforcement action; for permit termination, revocation and reissuance,
or modification; or denial of a permit renewal application.
a. The permittee shall comply with effluent standards or prohibitions established under section 307(a) of the
Clean Water Act for toxic pollutants and with standards for sewage sludge use or disposal established under
section 405(d) of the Clean Water Act within the time provided in the regulations that establish these
standards or prohibitions or standards for sewage sludge use or disposal, even if the permit has not yet been
modified to incorporate the requirement.

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1. b. The Clean Water Act provides that any person who violates a permit condition is subject to a civil penalty
not to exceed $25,000 per day for each violation. Any person who negligently violates any permit condition
is subject to criminal penalties of $2,500 to $25,000 per day of violation, or imprisonment for not more than
1 year, or both. Any person who knowingly violates pemtit conditions is subject to criminal penalties of
$5,000 to $50,000 per day of violation, or imprisonment for not more than 3 years, or both. Also, any
person who violates a permit condition may be assessed an administrative penalty not to exceed $10,000 per
violation with the maximum amount not to exceed $125,000. [Ref. Section 309 of the Federal Act 33 U.S.C.
1319 and 40 CFR 122.41 (a)]
c. Under state law, a civil penalty of not more than ten thousand dollars ($10,000) per violation may be assessed
against any person who violates or fails to act in accordance with the terms, conditions, or requirements of a
permit. [Ref: North Carolina General Statute's § 143-215.6A]
d. Any person may be assessed an administrative penalty by the Administrator for violating section 301, 3021
306, 307, 308, 318, or 405 of the Act, or any permit condition or limitation implementing any of such
sections in a permit issued under section 402 of the Act Administrative penalties for Class I violations are
not to exceed $10,000 per violation, with the maximum amount of any Class I penalty assessed not to
exceed $25,000. Penalties for Class II violations are not to exceed $10,000 per day for each day during
which the violation continues, with the maximum. amount of any Class II penalty not to exceed $125,000.
2. Dui to Miljp e
The permince shall take all reasonable steps to minimize or prevent any discharge or sludge use or disposal in
violation of this permits which has a reasonable likelihood of adversely affecting human health or the
environment
3. Civil and Criminal Liahilin+
Except as provided in peanut conditions on "Bypassing" (Part II, C-4) and "Power Failures" (Part II, C-7),
nothing in this permit shall be construed to relieve the permittee from any responsibilities, liabilities, or penalties
for noncompliance pursuant to NCGS 143-215.3, 143-215.6 or Section 309 of the Federal Act, 33 USC 1319.
Furthermore, the permittee is responsible for consequential damages, such as fish kills, even though the
responsibility for effective compliance may be temporarily suspended.
4. Oil and Hazardous Sub nce Liablity
Nothing in this permit shall be construed to preclude the institution of any legal action or relieve the permittee
from any responsibilities, liabilities, or penalties to which the permittee is or may be subject to under NCGS 143-
215.75 et seq. or Section 311 of the Federal Act, 33 USG 1321. Furthermore, the permittee is responsible for
consequential damages, such as fish kills, even though the responsibility for effective compliance may be
temporarily suspended.
5. Properly- Rights
The issuance of this permit does not convey any property rights in either real or personal property, or any
exclusive privileges, nor does it authorize any injury to private property or any invasion of personal rights, nor any
infringement of Federal, State or local laws or regulations.
6. Onshore or Offshore Construction
This permit does not authorize or approve the construction of any onshore or offshore physical structures or
facilities or the undertaking of any work in any navigable waters.
The provisions of this permit are severable, and if any provision of this permit, or the application of any
provision of this permit to any circumstances, is held invalid, the application of such provision to other
circumstances, and the remainder of this permit, shall not be affected thereby.

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8. Dut to Provide Information
The perittee shall furnish to the Permit Issuing Authority, within a reasonable time, any information which the
Permit Issuing Authority may request to determine whether cause exists for modifying, revoking and reissuing, or
terminating this permit or to determine compliance with this permit. The permittee shall also famish to the
Permit Issuing Authority upon request, copies of records required to be kept by this permit.
9. Dury to Reapp
If the pemnittee wishes to continue an activity regulated by this perrit after the expiration date of this permit, the
permitter must apply for and obtain a new permit.
10. Expiration of Permit
The permittee is not authorized to discharge after the expiration date. In order to receive automatic authorization
to discharge beyond the expiration date, the permittee shall submit such information, forms, and fees as are
required by the agency authorized to issue permits no later than 180 days prior to the expiration date. Any
permittee that has not requested renewal at least 180 days prior to expiration, or any permittee that does not have
a permit after the expiration and has not requested renewal at least 180 days prior to expiration, will subject the
permittee to enforcement procedures as provided in NCGS 143-215.6 and 33 USC 1251 et. seq.
11. 2MIM ReQuirements
All applications, reports, or information submitted to the Pert Issuing Authority shall be signed and certified.
a. All permit applications shall be signed as follows:
m For a corporation: by a responsible corporate officer. For the purpose of this Section, a responsible
corporate officer means: (a) a president, secretary, treasurer or vice president of the corporation in
charge of a principal business function, or any other person who performs similar policy or decision
making functions for the corporation, or (b) the manager of one or more manufacturing production or
operating facilities employing more than 250 persons or having gross annual sales or expenditures
exceeding 25 million (in second quarter 1980 dollars), if authority to sign documents has been assigned or
delegated to the manager in accordance with corporate procedures.
(2) For a partnership or sole proprietorship: by a general partner or the proprietor, respectively, or
(3) For a municipality, State, Federal, or other public agency: by either a principal executive officer or ranking
elected official.
b. All reports required by the permit and other information requested by the Permit Issuing Authority shall be
signed by a person described above or by a duly authorized representative of that person. A person is a duly
authorized representative only if.
T A person described above makes the authorization in writing;
(2) The authorization specified either an individual or a position having responsibility for the overall operation
of the regulated facility or activity, such as the position of plant manager, operator of a well or well field,
superintendent, a position of equivalent responsibility, or an individual or position having overall
responsibility for environmental matters for the company. (A duly authorized representative may thus be
either a named individual or any individual occupying a named position.); and
(3) The written authorization is submitted to the Permit Issuing Authority.
c. Certification. Any person signing a document under paragraphs a. or b. of this section shall make the
following certification:
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and
evaluate the information submitted. Based on my inquiry of the person or persons who manage the system,
or those persons directly responsible for gathering the information, the information submitted is, to the best
of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."

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12. Permit Actions
This permit may be modified, revoked and reissued, or terminated for cause. The filing of a request by the
permittee for a permit modification, revocation and reissuance, or termination, or a notification of planned
changes or anticipated noncompliance does not stay any permit condition.
13. Permit Modification. Revocation and Reissuance. or Temu nation
The issuance of this permit does not prohibit the permit issuing authority from reopening and modifying the
permit, revoking and reissuing the permit, or terminating the permit as allowed by the laws, roles, and regulations
contained in Title 40, Code of Federal Regulations, Parts 122 and 123; Title 15A of the North Carolina
Administrative Code, Subchapter 2H .0100; and North Carolina General Statute 143-2151 et. al.
14. Previous Permits
All previous National Pollutant Discharge Elimination System Permits issued to this facility, whether for
operation or discharge, are hereby revoked by issuance of this permit. [The exclusive authority to operate this
facility anises under this permit. The authority to operate the facility under previously issued permits bearing this
number is no longer effective. ] The conditions, requirements, terms, and provisions of this permit authorizing
discharge under the National Pollutant Discharge Elimination System govem discharges from this facility.
SECTION C. OPERATION AND MAINTENANCE OF POLLUTION CONTROL
Certified Operator
Pursuant to Chapter 90A-44 of North Carolina General Statutes, and upon classification of the facility by the
Certification Commission, the permittee shall employ a certified wastewater treatment plant operator in
responsible charge (ORC) of the wastewater treatment facilities. Such operator must hold a certification of the
grade equivalent to or greater than the classification assigned to the wastewater treatment facilities by the
Certification Commission. The permittee must also employ a certified back-up operator of the appropriate type
and any grade to comply with the conditions of Title 15A NCAC Chapter 8G.0202. The ORC of the facility
must visit each Class I facility at least weekly and each Class II, III, and W facility at least daily, excluding
weekends and holidays, and must properly manage and document daily operation and maintenance of the facility
and must comply with all other conditions of Title 15A, NCAC Chapter 8G.0202. Once the facility is classified,
the permittee shall submit a letter to the Certification Commission, which designates the operator in responsible
charge within thirty days after the wastewater treatment facilities are 50% complete.
2. Proper Operation and Maintenance
The permittee shall at all times properly operate and maintain all facilities and systems of treatment and control
(and related appurtenances) which are installed or used by the permittee to achieve compliance with the
conditions of this permit. Proper operation and maintenance also includes adequate laboratory controls and
appropriate quality assurance procedures. This provision requires the operation of back-up or auxiliary facilities
or similar systems installed by a permittee only when the operation is necessary to achieve compliance with the
conditions of the permit.
3. Need to Halt or Reduce not a Defense
It shall not be a defense for a permittee in an enforcement action that it would have been necessary to halt or
reduce the permitted activity in order to maintain compliance with the condition of this permit.
4. Daass no of Treatment Facilities
a. Definitions
(I) "Bypass" means the known diversion of waste streams from any portion of a treatment facility including
the collection system, which is not a designed or established or operating mode for the facility.
(2) "Severe property damage" means substantial physical damage to property, damage to the treatment
facilities which causes them to become inoperable, or substantial and permanent loss of natural resources
which can reasonably be expected to occur in the absence of a bypass. Severe property damage does
not mean economic loss caused by delays in production.

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4. b. Bypass not exceeding limitations.
The Permittee may allow any bypass to occur which does not cause effluent limitations to be exceeded, but
only if it also is for essential maintenance to assure efficient operation. These bypasses are not subject to the
provisions of Paragraphs c. and d. of this section.
c. Notice
(1) Anticipated bypass. If the permittee knows in advance of the need for a bypass, it shall submit prior
notice, if possible at least ten days before the date of the bypass; including an evaluation of the
anticipated quality and affect of the bypass.
(2) Unanticipated bypass. The permittee shall submit notice of an unanticipated bypass as required in Part II,
E. 6. of this permit. (24-hour notice).
d. Prohibition of Bypass
(!) Bypass is prohibited and the Permit Issuing Authority may take enforcement action against a permittee
for bypass, unless:
(A) Bypass was unavoidable to prevent loss of life, personal injury or severe property damage;
(B) There were no feasible alternatives to the bypass, such as the use of auxiliary treatment facilities,
retention of untreated wastes or maintenance during normal periods of equipment downtime. This
condition is not satisfied if adequate backup equipment should have been installed in the exercise of
reasonable engineering judgment to prevent a bypass which occurred during normal periods of
equipment downtime or preventive maintenance; and
(C) The permittee submitted notices as required under Paragraph c. of this section.
(2) Bypass from the collection system is prohibited. The Permit Issuing Authority may take enforcement
action against a Pemuttee for a bypass as provided in any current or future system -wide collection
system permit associated with the treatment facility.
(3). The Permit Issuing Authority may approve an anticipated bypass, after considering its adverse affects, if
the Pemmit Issuing Authority determines that it will meet the three conditions listed above in Paragraph d.
m of this section.
5. Upsets
a. Definition: "Upset" means an exceptional incident in which there is unintentional and temporary
noncompliance with technology based permit effluent limitations because of factors beyond the reasonable
control of the permittee. An upset does not include noncompliance to the extent caused by operational
error, improperly designed treatment facilities, inadequate treatment facilities, lack of preventive maintenance,
or careless or improper operation.
b. Effect of an upset: An upset constitutes an affirmative defense to an action brought for noncompliance
with such technology based permit effluent limitations if the requirements of paragraph c. of this condition
are met. No determination made during administrative review of claims that noncompliance was caused by
upset, and before an action for noncompliance, is final administrative action subject to judicial review.
c. Conditions necessary for a demonstration of upset: A permittee who wishes to establish the
affirmative defense of upset shall demonstrate, through properly signed, contemporaneous operating logs, or
other relevant evidence that
(1) An upset occurred and that the permittee can identify the cause(s) of the upset;
(2) The permittee facility was at the time being properly operated; and
(3) The permittee submitted notice of the upset as required in Par II, E. G. (b) (2) of this permit.
(4) The permittee complied with any remedial treasures required under Part II, B. 2. of this permit.
d. Burden of proof: In any enforcement proceeding the permittee seeking to establish the occurrence of an
upset has the burden of proof.

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6. Removed Substances
Solids, sludges, filter backwash, or other pollutants removed in the course of treatment or control of wastewaters
shall be utilized/disposed of in accordance with NCGS 143-215.1 and in a manner such as to prevent any pollutant
from such materials from entering waters of the State or navigable waters of the United States. The permittee
shall comply with all existing federal regulations governing the disposal of sewage sludge. Upon promulgation of
40 CFR Part 503, any permit issued by the Permit Issuing Authority for the utilization/disposal of sludge may be
reopened and modified, or revoked and reissued, to incorporate applicable requirements at 40 CFR Part 503.
The pemrittee shall comply with applicable 40 CFR Part 503 Standards for the Use and Disposal of Sewage
Sludge (when promulgated) within the time provided in the regulation, even if the permit is not modified to
incorporate the requirement. The pemtittee shall notify the Permit Issuing Authority of any significant change in
its sludge use or disposal practices.
7. Power Failures
The permitter: is responsible for maintaining adequate safeguards as required by DEM Regulation, Title 15A,
North Carolina Adnutustrative Code, Subchapter 2H, .0124 Reliability, to prevent the discharge of untreated or
inadequately treated wastes during electrical power failures either by means of alternate power sources, standby
generators or retention of inadequately treated effluent.
SECTION D. MONITORING AND RECORDS
Representative Smplinn
Samples collected and measurements taken, as required herein, shall be characteristic of the volume and nature of
the permitted discharge. Samples collected at a frequency less than daily shall be taken on a day and time that is
characteristic of the discharge over the entire period which the sample represents. All samples shall be taken at
the monitoring points specified in this permit and, unless otherwise specified, before the effluent joins or is
diluted by any other wastestream, body of water, or substance. Monitoring points shall not be changed without
notification to and the approval of the Permit Issuing Authority.
2. Reporting
Monitoring results obtained during the previous months) shall be summarized for each month and reported on
a monthly Discharge Monitoring Report (DMR) Form (DEM No. MR 1, 1.1, 2, 3) or alternative forts approved
by the Director, DEM, postmarked no later than the 30th day following the completed reporting period.
The first DMR is due on the last day of the month following the issuance of the permit or in the case of a new
facility, on the last day of the month following the commencement of discharge. Duplicate signed copies of
these, and all other reports required herein, shall be submitted to the following address:
NC DENR / Division of Water Quality / Water Quality Section
ATTENTION: Central Files
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
3. Flow Measurement
Appropriate flow measurement devices and methods consistent with accepted scientific practices shall be selected
and used to ensure the accuracy and reliability of measurements of the volume of monitored discharges. The
devices shall be installed, calibrated and maintained to ensure that the accuracy of the measurements are consistent
with the accepted capability of that type of device. Devices selected shall be capable of measuring flows with a
maximum deviation of less than 10% from the true discharge rates throughout the range of expected discharge
volumes. Once -through condenser cooling water flow which is monitored by pump logs, or pump hour meters
as specified in Part I of this permit and based on the manufacturer's pump curves shall not be subject to this
requirement.

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4. Test Procedures
Test procedures for the analysis of pollutants shall conform to the Eb1C regulations published pursuant to
NCGS 143-215.63 et. seq, the Water and Air Quality Reporting Acts, and to regulations published pursuant to
Section 304(p), 33 USC 1314, of the Federal Water Pollution Control tact, as Amended, and Regulation 40 CFR
136; or in the case of sludge use or disposal, approved under 40 CFR 136, unless otherwise specified in 40 CFR
503, unless other test procedures have been specified in this permit.
To meet the intent of the monitoring required by this permit, all test procedures must produce minimum
detection and reporting levels that are below the permit discharge requirements and all data generated must be
reported down to the minimum detection or lower reporting level of the procedure. If no approved methods
are determined capable of achieving minimum detection and reporting levels below permit discharge
requirements, then the most sensitive (method with the lowest possible detection and reporting level) approved
method must be used.
5. Penalties for Ta=dug
The Clean Water Act provides that any person who falsifies, tampers with, or knowingly renders inaccurate, any
monitoring device or method required to be maintained under this permit shall, upon conviction, be punished by
a fine of not more than $10,000 per violation, or by imprisonment for not more than two years per violation, or
by both. If a conviction of a person is for a violation comnritted after a fast conviction of such person under
this paragraph, punishment is a fine of not more than $20,000 per day of violation, or by imprisonment of not
more than 4 years, or both.
6. Records Retention
Except for records of monitoring information required by this permit related to the permittee's sewage sludge
use and disposal activities, which shall be retained for a period of at least five years (or longer as required by 40
CFR 503), the pemvttee shall retain records of all monitoring information, including all calibration and
maintenance records and all original strip chart recordings for continuous monitoring instnunentation, copies of
all reports required by this permit, for a period of at least 3 years from the date of the sample, measurement,
report or application. This petiod may be extended by request of the Director at any time.
7. Recording Results
For each measurement or sample taken pursuant to the requirements of this permit, the pemrittee shall record the
following information:
a. The date, exact place, and time of sampling or measurements;
b. The individual(s) who performed the sampling or measurements;
c. The date(s) analyses were performed;
d. The individual(s) who performed the analyses;
e. The analytical techniques or methods used; and
f The results of such analyses.
8. Inspection and EnteF
The pemnttee shall allow the Director, or an authorized representative (including an authorized contractor acting
as a representative of the Director), upon the presentation of credentials and other documents as may be required
by law, to;
a. Enter upon the permittee's premises where a regulated facility or activity is located or conducted, or where
records must be kept under the conditions of this permit;
b. Have access to and copy, at reasonable times, any records that must be kept under the conditions of this
permit;
c. Inspect at reasonable times any facilities, equipment (including monitoring and control equipment), practices,
or operations regulated or required under this permit; and
d. Sample or monitor at reasonable times, for the purposes of assuring permit compliance or as otherwise
authorized by the Clean Water Act, any substances or parameters at any location.

40
60 Part II
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SECTION E REPORTING REQUIREMENTS
I. Change in Discharrgg
All discharges authorized herein shall be consistent with the temps and conditions of this pennit. The dischatge of
any pollutant identified in this permit more frequently than or at a level in excess of that authorized shall constitute
a violation of the permit.
2. Planned a=
The pennittee shall give notice to the Director as soon as possible of any planned physical alterations or additions
to the permitted facility. Notice is required only when:
a. The alteration or addition to a permitted facility may meet one of the criteria for determining whether a
facility is a new source in 40 CFR Part 122.29 (b); or
b. The alteration or addition could significantly change the nature or increase the quantity of pollutants
discharged. This notification applies to pollutants which are subject neither to effluent limitations in the
permit, nor to notification requirements under 40 CFR Part 122.42 (a) (1).
c. The alteration or addition results in a significant change in the petmittee's sludge use or disposal practices, and
such alteration, addition or change may justify the application of permit conditions that are different from or
absent in the existing permit, including notification of additional use or disposal sites not reported during the
permit application process or not reported pursuant to an approved land application plan.
3. Anticlnated Noncoml2hance
The pemmittee shall give advance notice to the Director of any planned changes in the permitted facility or activity
which may result in noncompliance with permit requirements.
4. Transfers
This permit is not transferable to any person except after notice to the Director. The Director may require
modification or revocation and reissuance of the permittee and incorporate such other requirements as may be
necessary under the Clean Water Act.
5. Monitoring Reportc
Monitoring results shall be reported at the intervals specified elsewhere in this permit.
a. Monitoring results must be reported on a Discharge Monitoring Report (DMR) (See Part II. D. 2 of this
permit) or forms provided by the Director for reporting results of monitoring of sludge use or disposal
practices.
b. If the permittee monitors any pollutant more frequently than required by the permit, using test procedures
specified in Part II, D. 4. of this permit or in the case of sludge use or disposal, approved under 40 CFR
503, or as specified in this permit, the results of this monitoring shall be included in the calculation and
reporting of the data submitted in the DMR.
c. Calculations for all limitations which require averaging of measurements shall utilize an arithmetic mean unless
otherwise specified by the Director in the permit.
G. Twenty-four Hour Reporting
a. The permittee shall report to the central office or the appropriate regional office any noncompliance which
may endanger health or the environment. Any information shall be provided orally within 24 hours from the
time the pemmittee became aware of the circumstances. A written submission shall also be provided within 5
days of the time the perrmittee becomes aware of the circumstances. The written submission shall contain a
description of the noncompliance, and its cause; the period of noncompliance, including exact dates and
times, and if the noncompliance has not been corrected, the anticipated time it is expected to continue; and
steps taken or planned to reduce, eliminate, and prevent reoccurrence of the noncompliance.

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6. b. The following shall be included as information which must be reported within 24 hours under this
paragraph:
(1) Any unanticipated bypass which exceeds any effluent limitation in the pemnit.
(2) Any upset which exceeds any effluent limitation in the permit.
(3) Violation of a maximum daily discharge limitation for any of the pollutants listed by the Director in the
permit to be reported within 24 hours.
c. The Director may waive the written report on a case -by -case basis for reports under paragraph b. above of
this condition if the oral report has been received within 24 hours.
Other Noncompliance
The pemmittee shall report all instances of noncompliance not reported under Part II. E. 5 and 6. of this permit at
the time monitoring reports are submitted. The reports shall contain the information listed in Part H. E. 6. of this
permit.
8. Other Information
Where the pernittee becomes aware that it failed to submit any relevant facts in a permit application, or
submitted incorrect information in a permit application or in any report to the Director, it shall promptly submit
such facts or information.
9. Noncomnl_ance Notification
The permittee shall report by telephone to either the central office or the appropriate regional office of the
Division as soon as possible, but in no case more than 24 hours or on the next working day following the
occurrence or first knowledge of the occurrence of any of the following.
a. Any occurrence at the water pollution control facility which results in the discharge of significant amounts of
wastes which are abnormal in quantity or characteristic, such as the dumping of the contents of a sludge
digester; the known passage of a slug of hazardous substance through the facility; or any other unusual
circumstances.
b. Any process unit failure, due to known or unknown reasons, that render the facility incapable of adequate
wastewater treatment such as mechanical or electrical failures of pumps, aerators, compressors, etc.
c. Any failure of a pumping station, sewer line, or treatment facility resulting in a by-pass directly to receiving
waters without treatment of all or any portion of the influent to such station or facility.
Persons reporting such occurrences by telephone shall also file a written report in letter form within 5 days
following first knowledge of the occurrence.
10. Availab ty of Reps;
Except for data determined to be confidential under NCGS 143-215.3 (a)(2) or Section 308 of the Federal Act, 33
USC 1318, all reports prepared in accordance with the terms shall be available for public inspection at the offices
of the Division of Water Quality. As required by the Act, effluent data shall not be considered confidential
Knowingly making any false statement on any such report may result in the imposition of criminal penalties as
provided for in NCGS 143-215.1(b)(2) or in Section 309 of the Federal Act.
11. Penalties for Falsification of Reports
The Clean Water Act provides that any person who knowingly makes any false statement, representation, or
certification in any record or other document submitted or required to be maintained under this permit, including
monitoring reports or reports of compliance or noncompliance shall, upon conviction, be punished by a fine of
not more than $10,000 per violation, or by imprisonment for not more than two years per violation, or by both.

0 0
PART III
OTHER REQUIREMENTS
A. Construction
No construction of wastewater treatment facilities or additions to add to the plant's treatment capacity or to
change the type of process utilized at the treatment plant shall be begun until Final Plans and Specifications have
been submitted to the Division of Water Quality and written approval and Authorization to Construct has been
issued.
B. Groundwater monitoring
The permittee shall, upon written notice from the Director of the Division of Water Quality, conduct
groundwater monitoring as may be required to determine the compliance of this NPDES permitted facility with
the current groundwater standards.
C. Changes in Discharges of Toxic Substanccc
The permittee shall notify the Pennit Issuing Authority as soon as it knows or has reason to believe:
a. That any activity has occurred or will occur which would result in the discharge, on a routine or frequent
basis, of any toxic pollutant which is not limited in the permit, if that discharge will exceed the highest of the
following "notification levels';
(I) One hundred micrograms per liter 000 µg/L);
(2) Two hundred micrograms per liter (200 p$/L) for acrolein and acrylonitrile; five hundred micrograms
per liter (500 µg/L) for 2.4-dinitmphenol and for 2-methyl-4.6-dinitrophenol; and one milligram per
liter P mg/L) for antimony;
(3) Five (5) times the maximum concentration value reported for that pollutant in the permit application.
b. That any activity has occurred or will occur which would result in any discharge, on a non -routine or
infrequent basis, of a toxic pollutant which is not limited in the permit, if that discharge will exceed the
highest of the following "notification levels";
(f) Five hundred micrograms per liter (500 µg/L);
(2) One milligram per liter 0 mg/L) for antimony;
(3) Ten (10) times the maximum concentration value reported for that pollutant in the permit application.
D. Requirement to Continually Evaluate Alternatives to Wastewater Discharges
The permittee shall continually evaluate all wastewater disposal alternatives and pursue the most environmentally
sound alternative of the reasonably cost effective alternatives. If the facility is in substantial noncompliance with
the terms and conditions of the NPDES permit or governing rules, regulations or laws, the permittee shall
submit a report in such form and detail as required by the Division evaluating these alternatives and a plan of
action within sixty (60) days of notification by the Division.
PART IV
ANNUAL ADMINISTERING AND COMPLIANCE MONITORING FEE
REQUIREMENTS
A. The permittee must pay the annual administering and compliance monitoring fee within 30 (thirty)
days after being billed by the Division. Failure to pay the fee in a timely manner in accordance with
15A NCAC 2H .0105(b)(4) may cause this Division to initiate action to revoke the permit.

4 DENR/DWQ fff
FACT SHEET FOR NPDES PERNUT DEVELOPMENT
NPDES No. NC0001899, Honeywell International, Inc.
AMENDMENT
Facility Information
Applicant/ FaciliName:
Honeywell International, Inc./ Honeywell WWTP
Applicant Address:
338 Pea Ridge Road. Moncure, NC 27559
Facility Address:
(same as above)
Permitted Flow
Outfall 001 - .244 MGD; 002 - Variable
Type of Waste:
96 % Industrial: 4% domestic (001); 100% non -process
industrial (002)
Facility/Permit Status:
Renewal
County:
Chatham
Miscellaneous
Receiving Stream:
Haw River (001)
UT Shaddox
Creek (002)
Regional Office:
RRO
Stream Classification:
WS-IV (001)
SI: 16-(42)
Quad
E22SE
_
303(d) Listed?:
No
Permit Writer:
S. Wilson
Subbasin:
030607 (CPF)
Date:
1)eC:
Drainage Area (mi2):
980
• J
j✓
j
Summer 7Q10 (cfs)
Minimum
release (40 cfs)
30Q2 (cfs):
Average Flow (cfs):
1848
IWC (%):
0.94% (001)
Primary SIC Code:
12821
TP for outfall 001 was changed to composite (in error - it had been listed as grab)
Acute toxicity sampling for outfall 002 was changed from composite to grab (same as the
previous permit)
Monitoring points were clarified. Chloroform can be monitored prior to any chlorine
interference (this meets the spirit of the OCPSF limit - as this limit must be met from the
OCPSF flow).
PAH was inadvertently inserted as a limit. Monitoring is appropriate, as the specific
compounds are limited via OCPSF parameters. PAH will be evaluated upon the next renewal.
Sampling levels were explained. See Part A.7. This is appropriate, as the dilution from other
non-OCPSF sources is so great that achieving a detection level below the mass based limit
would be difficult to impossible.
L7, 2ccZ
4% /..
Honeywell WWTP
NPDES Renewal
Page 1

Performance re 0
May 22, 2014
MAY 21 2M
WPCSOCC
1618 Mail Service Center
Raleigh, NC 27699-1618
FAX: [phone]
Subject: Additional Backup ORC (BUORC) Designation
NPDES # NC0001899
Mailing Address: Performance Fibers Inc.
338 Pea Ridge Road
New Hill, NC 27562
We have attached the WPCSOCC (Water Pollution Control System Operator)
Designation Form to document our change in BUORC (Back-up Operator in Responsible
Charge) at our waste treatment plant. If you have questions or need additional
information please contact me 704-642-2197.
Sincerely,
Ic
Marty Stewart
Regional Environmental Leader
Performance Fibers, Inc.
CC: I) Raleigh Regional Office
3800 Barrett Drive
Raleigh, NC 27609
Performance Fibers Inc. 338 Pea Ridge Road, New Hill, North Carolina 27562

W Pollution Control System Ope r Designation Form
WPCSOCC
NCAC 15A 8G .0201
Permittee Owner/Officer Name: Performance Fibers, Inc./Donald Peterson, Plant Manager
Mailing Address:
City: New Hill
Email address: Donald.
Signature:
Pea
State: NC Zip: 27562 -
Phone #: ( 919) 542-2200
Date: 51- al )*
Facility Name: Performance Fibers. Inc. Permit#: NCOOO1899
SUBMIT A SEPARATE FORM FOR EACH TYPE SYSTEM!
Facility TvDe/Grade:
Biological WWTP % Surface Irrigation
Physical/Chemical Land Application
Collection System
zn
....................................................................................................................................
Operator in Responsible Charge (ORC)
Print Full Name:
Certificate Type Grade / Number: IiH-Grade _ 2 #25810 Work Phone #: (919 P45-3247 I ��
Signature: Date:__ Q �1 / g f%/
/
I certify that I agree to y designation as the Operator in Respon Charge for the facility noted. I understand and will abide by the rules
and regulations pertaining to the responsibilities of the ORC as set forth in 15A NCAC 08G .0204 and failing to do so can result in Disciplinary
Actions by the Water Pollution Control System Operators Certification Commission."
.................................................................................................................................................
Back -Up Operator in Responsible Charge (BU ORC)
Print Full Name:
Certificate Ty e / Grade / Number: lift —Grade 2 1989336 Work Phone #: ( 919) 545-3247
Signature: e Date: 5'14' lti
"I certify that I agree to my esignation as a Back-up Operator in Responsible Charge for the facility noted. I understand and will abide by the
rules and regulations pertaining to the responsibilities of the BU ORC as set forth in I SA NCAC 08G .0205 and failing to do so can result in
Disciplinary Actions by the Water Pollution Control System Operators Certification Commission."
...................................................................................................................................................
Mail, jar or email the WPCSOCC, 1618 Mail Service Center, Raleigh, NC 27699-1618 Fax: [phone]
original to: Email: certadminoncdenneov
Mail orfax a copy to the Asheville
appropriate Regional Office. 2090 US Hwy 70
Swanmmoa 28778
Fax: [phone]
Phone: [phone]
Washington
943 Washington Sri Mall
Washington 27889
Fax: [phone]
Phone: [phone]
Fayetteville
225 Green St
Suite 714
Fayetteville 28301-5043
Fax: [phone]
Phone: [phone]
Wilmington
127 Cardinal Dr
Wilmington 28405-2845
Fax: [phone]
Phone: [phone]
Mooresville
610 E Center Ave
Suite 301
Mooresville 28115
Fax: [phone]
Phone: [phone]
Winston-Salem
585 Waughtown St
Winston-Salem 27107
Fax: [phone]
Phone: [phone]
Raleigh
3900 Barrett Dr
Raleigh 27609
Fax: [phone]
Phone:[phone]
Revised 03-2014

Facility Name:
Performance Fibers, Inc.
..................................................................................
Back -Up Operator in Responsible Charge (BU ORC)
Print Full Name: Steve 11 Abrams
Certificate Type / Grade / Number: WW-1 / It 986568
Permit#: NC0001899
Work Phone #: P19 ) 545-3247
Signature:4;99�2&k, Gz4rawi�_ Date: .J - /L - /L/
I certify that I agree to my designation as a Back-up Operator in Responsible Charge for the facility noted. I understand and will abide by the
mles and regulations pertaining to the responsibilities of the BU ORC as set forth in 15A NCAC 08G .0205 and failing to do so can result in
Disciplinary Actions by the Water Pollution Control System Operators Certification Commission."
..................................................................................................................................................
Back -Up Operator in Responsible Charge (BU ORC)
Print Full Name: Ronnie Autry
Certificate Type / Grade / Number: WW-1 / #996828
Work Phone #:
( 919)
545-3247
Signature: �aY 44Ae
Date:
S I (fl
I
`9 certify that I agree to my designation as a Back-up Operator in Responsible Charge for the facility noted. 1 understand and will abide by the
rules and regulations pertaining to the responsibilities of the BU ORC as set forth in 15A NCAC 08G .0205 and failing to do so can result in
Disciplinary Actions by the Water Pollution Control System Operators Certification Commission."
Back -Up Operator in Responsible Charge (BU ORC)
Print Full Name: Andy Everette
Certificate Type
e//�JGrade / Number: WW-1 / # 996280 Work Phone #: (919 ) 545-32tc47
Signature: ( jai Date:
"I certify that I agree to my designation as a Back-up Operator in Responsible Charge for the facility noted. I understand and will abide by the
rules and regulations pertaining to the responsibilities of the BU ORC as set forth in I5A NCAC NO .0205 and failing to do so can result in
Disciplinary Actions by the Water Pollution Control System Operators Certification Commission."
Back -Up Operator in Responsible Charge (BU ORC)
Print Full Name: Robert Glosson
Certificate Type / Grade / Number: WW 1 / # 25504
Work Phone #: ( 919 ) 545-3247
Signature: Date:
"I certify that I agree to my designation as a Back-up Operator in Responsible Charge for the facility noted. I understand and will abide by the
rules and regulations pertaining to the responsibilities of the BU ORC as set forth in 15A NCAC 08G .0205 and failing to do so can result in
Disciplinary Actions by the Water Pollution Control System Operators Certification Commission."
Revised 03-2014

Facility Name: Performance Fibers, Inc. Permit#: NC0001899
Back -Up Operator in Responsible Charge (BU ORC)
Print Full Name: Donald Brook Harrington
Certificate Type / Grade / Number: WW-1 / # 27713 Work Phone #: ( 919) 545-3247
Signature: ,)m4kl 4 4 L% �� w Date: S- t 6-1 4-
I certify that I agree to my designation as a Back-up Operator in Responsible Charge for the facility noted. I understand and will abide by the
rules and regulations pertaining to the responsibilities of the BU ORC as set forth in 15A NCAC 080 .0205 and failing to do so can result in
Disciplinary Actions by the Water Pollution Control System Operators Certification Commission."
..................................................................................................................................................
Back -Up Operator in Responsible Charge (BU ORC)
Print Full Name: Gary Lent
Certificate Type / Grade / Number: WW-1 / 113331 Work Phone #: ( 919 ) 545-3247
Signature: Q S6ej&..4 Date: 5S-17-1Y
"I certify that 1 agree to my designation as a Back-up Operator in Responsible Charge for the facility noted. I understand and will abide by the
rules and regulations pertaining to the responsibilities of the BU ORC as set forth in 15A NCAC 08G .0205 and failing to do so can result in
Disciplinary Actions by the Water Pollution Control System Operators Certification Commission."
................................................................................................................................................
Back -Up Operator in Responsible Charge (BU ORC)
Print Full Name:
Certificate Type / Grade / Number: WW-1 / 126417 Work Phone #: ( 919 )545-3247
Signature: ZQ Date:
'[ certify that I agree to my designation as a Back-up Operator in Responsible Charge for the facility noted. I understand and will abide by the
rules and regulations pertaining to the responsibilities of the BU ORC as set forth in 15A NCAC 08G .0205 and failing to do so can result in
Disciplinary Actions by the Water Pollution Control System Operators Certification Commission."
.................................................................................................................................................
Back -Up Operator in Responsible Charge (BU ORC)
Print Full Name:
Certificate Type / Grade / Number:
Signature:
Work Phone #:
" 1 certify that I agree to my designation as a Back-up Operator in Responsible Charge for the facility noted. 1 understand and will abide by the
rules and regulations pertaining to the responsibilities of the BU ORC as set forth in 15A NCAC 08G .0205 and failing to do so can result in
Disciplinary Actions by the Water Pollution Control System Operators Certification Commission."
Revised 03-2014

5024
Mr. Larry Murray
Performance Fibers, Inc. (PFI)
338 Pea Ridge Road
New Hill, NC 27562-8951
Michael F. Easley, Governor
tQi
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E. Director
Division of Water Quality
November 30, 2006
AfC OO O l'59 `j
SUBJECT: Wastewater/Groundwater Laboratory Certification Renewal
FIELD PARAMETERS ONLY
Dear Mr. Murray:
The Department of Environment and Natural Resources, in accordance with the provisions of NC GS
143-215-.3 (a) (10), 15 NCAC 2H .0800, is pleased to renew certification for your laboratory to perform
specified environmental analyses required by EMC monitoring and reporting regulations 15 NCAC 2B
.0500, 2H .0900 and 2L .0100, .0200, .0300, and 2N .0100 through .0800.
Enclosed for your use is a certificate describing the requirements and limits of your certification. Please
review this certificate to insure that your laboratory is certified for all parameters required to property meet
your certification needs.
Please contact your assigned inspector Jeffrey R. Adams at 919-733-3908, if you have questions or
need additional information.
Sincerely,
Pat Donnelly
Branch Manager
Enclosure
cc: Jeffrey R. Adams
Raleigh Regional Office
u�
t
DE` M� R AEEiGH REG��r
Laboratory Section 1623 Mail Service Center Raleigh, NC 27699.1623 Phone [phone] Customer Service
Internet: www dwmlab ore Location: 4405 Reedy Creek Rd.Raleigh, NC 27607 Fax [phone]
An Equal Opportunity/Afinnative Action Employer— 50% Recycled/10% Post Consumer Paper

STATE OF NORTH CAROLINA DEPARTMENT OF THE
ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
LABORATORY CERTIFICATION PROGRAM
In accordance with the provisions of N.C. G.S. 143-215.3 (a) (1), 143-215.3 (a)(10) and NCAC 2H.0800:
Q
W
16
Field Parameter Only
tssev
�_ QtrAM
PERFORMANCE FIBERS, INC. (PFI)
Is hereby certified to perform environmental analysis as listed on Attachment I and report monitoring data to DWQ for
compliance with NPDES effluent, surface water, groundwater, and pretreatment regulations.
By reference 15A NCAC 2H .0800 is made a part of this certificate.
This certificate does not guarantee validity of data generated, but indicates the methodology, equipment, quality control procedures,
records, and proficiency of the laboratory have been examined and found to be acceptable.
This certificate shall be valid until December 31, 2007
Certificate No. 5024
Pat Donnelly

Attachment
North Ca Wastewater/Groundwater Laboratory Certifies
Certified Parameters Listing
FIELD PARAMETERS ONLY
.ab Name: Performance Fibers, Inc. (PFI) Certificate Number: 5024
kddress: 338 Pea Ridge Road Effective Date: 01/012007
New Hill, NC 27562-8951 Expiration Date: 12/312007
Date of Last Amendment:
he above named laboratory, having duty met the requirements of I SA NCAC 2H.0800, is hereby certlfied for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
NORGANICS
ZESIDUAL CHLORINE
Std Method 4500 CI G
EPA Method 330.5
;ONDUCTIVITY
Sid Method 2510B
ASSOLVED OXYGEN
Std Method 4500 O G
EPA Method 360.1
H
Std Method 4500 H B
EPA Method 150.1
'EMPERATURE
Std Method 2550B
EPA Method 170.1
-his certification requires maintance of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are
subjectto civil penalties and/or decertification for infractions as set forth in 15A NCAC 2H.0907.

November 21, 2006
Mr. Don Peterson, Plant Manager
Performance Fibers, Inc.
338 Pea Ridge Road
New Hill, North Carolina 27559
Subject:
Dear Mr. Peterson
Michael F. Easley, Governor
State of North Carolina
William G. Ross, Jr., Secretary
Department of Environment and Natural Resources
Alan W. Klimek, P.E., Director
Division of Water Quality
Draft NPDES Permit
Permit NC0001899
Performance Fibers WWTP
Chatham County
Enclosed with this letter is a copy of the draft permit for your facility. Please review the draft very
carefully to ensure thorough understanding of the conditions and requirements it contains.
This draft has the following significant changes from your current permit:
➢ Fecal coliform monitoring has been removed from outfall 001. Division policy recommends fecal
coliform limits for discharges into class B waters, or domestic dischargers with an instream
dilution of less than 331:1. Your facility's discharge does not meet these requirements, therefore
fecal coliform monitoring is not required.
➢ Total residual chlorine monitoring has been removed from outfall 001. Chuck Powell with
Performance Fibers has indicated that the facility only chlorinates in order to meet past NPDES
permit's fecal coliform requirements. Mr. Powell has indicated that the facility will cease
chlorination once the fecal coliform requirements are removed.
➢ Fluoride and zinc monitoring have been removed due to the lack of reasonable potential for levels of
these parameters to cause an exceedance of water quality standards.
➢ Total nitrogen and total phosphorus monitoring has been reduced to quarterly as recommended
by the Middle Cape Fear permitting strategy. Special condition A(7) has also been added in
accordance with this strategy.
Please submit any comments to me no later than thirty days following your receipt of the draft.
Comments should be sent to the address listed at the bottom of this page. If no adverse comments are
received from the public or from you, this permit will likely be issued in two months.
If you have any questions or comments concerning this draft permit, please contact me at [phone] x
551 or via email at [e-mail].
Sincerely,
E ode
I e oya Fields D II Ili
Western NPDES Program
■M 2 T 2006 j
cc: Raleigh Regional Office, Surface Water Protection
NPDES Unit IDENR RALEIGH REGIONAL OFFICE;
Marshall Hyatt, EPA Region IV --
Aquatic Toxicology Unit
Chuck Powell, Environmental Engineer, 338 Pea Ridge Road, New Hill, NC 27562
Michael Douglas, DEH, Raleigh Regional Office
1617 Mail Service Center, Raleigh, North Carolina 27699-1617 Telephone [phone] FAX [phone] t o ` Carolina
512 N. Salisbury Street, Raleigh, North Carolina 27604 On the Internet at http://w .ncwaterquality.org tgturally
An Equal Opportunity/Affirmative Action Employer

STATE OF NORTH CAROLINA
DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
PERMIT
TO DISCHARGE WASTEWATER UNDER THE
NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards
and regulations promulgated and adopted by the North Carolina Water Quality Commission, and the
Federal Water Pollution Control Act, as amended,
Performance Fibers, Inc.
is hereby authorized to discharge wastewater from a facility located at the
Performance Fibers, Inc. WWTP
East of Moncure off Pea Ridge Road
Chatham County
to receiving waters designated as the Haw River in the Cape Fear River Basin in accordance with the
discharge limitations, monitoring requirements, and other conditions set forth in Parts I, II, III and IV
hereof.
This permit shall become effective.
This permit and the authorization to discharge shall expire at midnight on July 31, 2011.
Signed this day.
,0 DRAFT
Alan W. Klimek, P.E., Director
Division of Water Quality
By the Authority of the Environmental Management Commission
Permit NC0001899

SUPPLEMENT TO PERMIT COVER SHEET
All previous NPDES Permits issued to this facility, whether for operation or discharge are hereby revoked. As of this permit
issuance, any previously issued permit bearing this number is no longer effective. Therefore, the exclusive authority to
operate and discharge from this facility arises under the permit conditions, requirements, terms, and provisions included
herein.
Performance Fibers, Inc. is hereby authorized to:
1. Continue to discharge process and domestic effluent at a permitted flow not to exceed
0.244 MGD (outfall 001), from a wastewater treatment facility consisting of the following:
➢ Sanitary flow bar screen and grinder
➢ Process wastewater bar screen
➢ Neutralization chamber
➢ Aeration basin
➢ Clarifier
➢ Sludge drying bed
➢ Optional polishing pond
➢ Chlorine gas disinfection (not in service)
➢ Chlorine gas contact chamber
2. Continue to discharge stormwater, condensate, and firepond overflow (outfall 002) from
facilities located at the Performance Fibers, Inc. Facility, off Pea Ridge Road east of
Moncure in Chatham County, and,
3. Discharge wastewater from said treatment works via outfall 001 at the location specified
on the attached map into the Haw River and via outfall 002 into an unnamed tributary to
Shaddox Creek, both of which are classified WS-IV waters in the Cape Fear River Basin.
NPDES No. NC0001899

4 Sf J
tCV 11 1
.i r rr
Outfall 001
` . ! Outfall 002
s v
1�
gig
go
13
1 t a F� Wnt r
NCO00343'
1 Cer yriaht t�f Znn� Mart€ah, i =
Performance Fibers, Inc — NC0001899 0
Facility
Location
USGS Quad Name: Moncure 001 - Lat.: 35°37'01"
Receiving Streams: Long.: 79003'25"
001 —Haw River, 002 — Shaddox Creek
Stream
m Class: WS-IV 002-Lat.:35°37'00" N Not to SCALE
Subbasin: Cape Fear— 03 06 07 Long.: 79002,36"

A. (1) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS (001)
During the period beginning on the effective date of the permit and lasting until expiration, the Permitee is
authorized to discharge 0.244 MGD of industrial and domestic wastewater from outfall 001. Such discharges
shall be limited and monitored by the Permitee as specified below:
Effluent
Characteristics
Limits
Monitoring Requirements
Monthly
Average
Weekly
Average
Daily
Maximum
Measurement
Frequency
Sample
Type
Sample
Location
Flow
0.244 MGD
Continuous
RecordingInfluent
or
Effluent
pH2
Between 6.0 and 9.0 s.u.
Continuous
Recording
Effluent
BOD, 5 day (20'C)
10.4 Ibs/day
16.71bs/day
Weekly
Composite
Effluent
Total Suspended Solids
5.01bs/day
10.6 Ibs/day
Weekly
Composite
Effluent
Oil and Grease
20.0lbs/day
30.0 lbs/day
Weekly
Grab
Effluent
Temperature (°C)
Monthly
Grab
Effluent
Upstream &
Downstream
Conductivity
Monthly
Grab
Effluent
Upstream &
Downstream
Dissolved Oxygen
Monthly
Grab
Effluent
Upstream &
Downstream
Total Nitrogen (mg/L)s
Quarterly
Composite
Effluent
Total Phosphorus (mg/L)
Quarterly
Composite
Effluent
Chronic Toxicity*
Quarterly
Composite
Effluent
OCPSFs
Annually
Grab
Effluent
Footnotes:
1. Upstream: valve at Pemuttee's river water pump house. Downstream: nearest accessible point at least 100
yards below the outfall and above the confluence of the Deep and Haw Rivers. Instream monitoring is
provisionally waived due to the permittee's participation in the Lower Cape Fear River Basin Association.
Instream monitoring shall be conducted as stated in this permit should the permittee end its participation
in the Association.
2. The pH shall be monitored continuously at the effluent. In accordance with 40 CFR 401.17, the total time
during which the pH values are allowed to be less than 6.0 standard units or greater than 9.0 standard units
shall not exceed 7 hours and 26 minutes in any calendar month, and no individual excursion outside the 6 to 9
range shall exceed 60 minutes.
3. TN = TKN + NO,-N + NOrN, where TN is Total Nitrogen, TKN is Total Kjeldahl Nitrogen, and NO,-N and
NO.-N are Nitrate and Nitrite Nitrogen, respectively.
4. Chronic Toxicity (Ceriodaphnia) Chronic P/F at 0.94%: January, April, July, and October [see Condition A. (3)].
5. Refer to Conditions A. (8) and A. (9) regarding OCPSF monitoring. Where any compound is detected,
quarterly monitoring is required for that compound until not detected in twelve consecutive samples.
Honeywell may use EPA test method 524.2 to monitor OCPSF parameters (provided the method allows a
detection level at or below the permitted limit).
There shall be no discharge of floating solids or visible foam in other than trace amounts.
NPDES No. NC0001899

A. (2.) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS (002)
During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is
authorized to discharge stormwater, steam condensate, and firepond overflow wastewater from Outfall 002.
Such discharges shall be limited and monitored by the Permittee as specified below:
Effluent
Characteristics
Limits
Monitoring Requirements
Monthly
Average
Weekly
Average
Daily
Maximum
Measurement
Fre uenc
Sample Type
Sample
Location
lq,
Weekly
Instantaneous
Effluent
Temperature (°C)1
Weekly
Grab
Effluent
Total Residual Chlorine2
Weekly
Grab
Effluent
pH
Between 6.0 and 9.0 s.u.
Weekly
Grab
Effluent
Acute Toxicity3
Annually
Grab
Effluent
Footnotes:
1. The temperature of the effluent shall be such as not to cause an increase in the temperature of the receiving
stream of more than 2.8°C and in no case cause the ambient water temperature to exceed 32°C.
2. Chlorine monitoring is required only if chlorine is added in the wastewater contributors stated above.
3. Acute Toxicity (Fathead Minnow) Annual Monitoring [see Condition A. (4)).
There shall be no discharge of floating solids or visible foam in other than trace amounts.
NPDES No. NCOOO 1899

A. (3) CHRONIC TOXI( ( PERMIT LIMIT (Quarterly)
The effluent discharge shall at no time exhibit observable inhibition of reproduction or significant mortality to
Ceriodaphnia dubia at an effluent concentration of 0.94%.
The permit holder shall perform at a minimum, uag rterly monitoring using test procedures outlined in the "North
Carolina Ceriodaphnia Chronic Effluent Bioassay Procedure," Revised February 1998, or subsequent versions or
"North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or
subsequent versions. The tests will be performed during the months of January, April, July, and October.
Effluent sampling for this testing shall be performed at the NPDES permitted final effluent discharge below all
treatment processes.
If the test procedure performed as the first test of any single quarter results in a failure or ChV below the
permit limit, then multiple -concentration testing shall be performed at a minimum, in each of the two
following months as described in "North Carolina Phase II Chronic Whole Effluent Toxicity Test Procedure"
(Revised -February 1998) or subsequent versions.
The chronic value for multiple concentration tests will be determined using the geometric mean of the highest
concentration having no detectable impairment of reproduction or survival and the lowest concentration that does
have a detectable impairment of reproduction or survival. The definition of "detectable impairment," collection
methods, exposure regimes, and further statistical methods are specified in the "North Carolina Phase II Chronic
Whole Effluent Toxicity Test Procedure" (Revised -February 1998) or subsequent versions.
All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge
Monitoring Form (MR-1) for the months in which tests were performed, using the parameter code TGP3B for the
pass/fail results and THP3B for the Chronic Value. Additionally, DWQ Form AT-3 (original) is to be sent to the
following address:
Attention North Carolina Division of Water Quality
Environmental Sciences Section
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
Completed Aquatic Toxicity Test Forms shall be filed with the Environmental Sciences Section no later than 30
days after the end of the reporting period for which the report is made.
Test data shall be complete, accurate, include all supporting chemical/physical measurements and all
concentration/response data, and be certified by laboratory supervisor and ORC or approved designate
signature. Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is
employed for disinfection of the waste stream.
Should there be no discharge of flow from the facility during a month in which toxicity monitoring is required, the
perndttee will complete the information located at the top of the aquatic toxicity (AT) test form indicating the
facility name, permit number, pipe number, county, and the month/year of the report with the notation of "No
Flow" in the comment area of the form. The report shall be submitted to the Environmental Sciences Section at
the address cited above.
Should the permittee fail to monitor during a month in which toxicity monitoring is required, monitoring will be
required during the following month.
Should any test data from this monitoring requirement or tests performed by the North Carolina Division of
Water Quality indicate potential impacts to the receiving stream, this permit may be re -opened and modified to
include alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism
survival, minimum control organism reproduction, and appropriate environmental controls, shall constitute an
invalid test and will require immediate follow-up testing to be completed no later than the last day of the month
following the month of the initial monitoring.
NPDES No. NC0001899

A. (4) ACUTE TOXICITY MONITORING (ANNUAL)
The permittee shall conduct annual toxicity tests using protocols defined as definitive in E.P.A. Document
EPA/600/4-90/027 entitled "Methods for Measuring the Acute Toxicity of Effluents to Freshwater and Marine
Organisms." The monitoring shall be performed as a Fathead Minnow (Pimephales pramelas) 24 hour static test.
Effluent samples for self -monitoring purposes must be obtained below all waste treatment. The permittee will
conduct one test annually, with the annual period beginning in January of the calendar year of the effective date
of the permit.
The annual toxicity test must be performed by Tune 30. Should there be no discharge of flow from the facility
during the six month period January 1-June 30, the permittee will complete the information located at the top of
the aquatic toxicity (AT) test form indicating the facility name, permit number, pipe number, county and in the
comments section indicate "No Flow for January 1-June 30, (calendar year)." The report must be signed and
submitted to the Environmental Sciences Section at the address noted below.
If no discharge event occurs from Tanuary 1-Tune 30, yet a discharge event occurs from July 1-December 31, then
the facility must perform toxicity monitoringand nd report the data as noted below.
The parameter code for this test is TAE6C. All toxicity testing results required as part of this permit condition will
be entered on the Effluent Discharge Fors (MR-1) for the month in which it was performed, using the appropriate
parameter code. Additionally, DWQ Form AT-1 (original) is to be sent to the following address:
Attention: North Carolina Division of Water Quality
Environmental Sciences Section
1621 Mail Service Center
Raleigh, N.C. 27699-1621
Completed Aquatic Toxicity Test Forms shall be filed with the Environmental Sciences Section no later than 30
days after the end of the reporting period for which the report is made.
Test data shall be complete and accurate and include all supporting chemical/physical measurements performed
in association with the toxicity tests, as well as all dose/response data. Total residual chlorine of the effluent
toxicity sample must be measured and reported if chlorine is employed for disinfection of the waste stream.
Should any test data from either these monitoring requirements or tests performed by the North Carolina Division
of Water Quality indicate potential impacts to the receiving stream, this permit may be re -opened and modified to
include alternate monitoring requirements or limits.
NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism
survival and appropriate environmental controls, shall constitute an invalid test and will require immediate
follow-up testing to be completed no later than the last day of the month following the month of the initial
monitoring.
A. (5) WASTEWATER TREATMENT PONDS
The wastewater treatment ponds at the facility shall maintain a freeboard height of 2 feet.
A. (6) SAMPLING POINTS
The permittee may perform sampling after the chlorine contact chamber, for all parameters except those listed
below:
➢ Toxicity sampling may be conducted near the end -of -pipe prior to discharge into the Haw River.
In order to avoid interference with chlorine addition, sampling for chloroform may be collected after the
clarifier.
NPDES No. NC0001899

A. (7) PERMIT REOPENER: SUPPLEMENTARY NUTRIENT MONITORING
Pursuant to N.C. General Statutes Section 143-215.1 and the implementing rules found in Title 15A of the North
Carolina Administrative Code, Subchapter 02H, specifically,15A NCAC 02H.0112(b)(1) and 02H.0114(a), and
Part II, Sections B.12. and B.13. of this Permit, the Director of DWQ may reopen this permit to require
supplemental nutrient monitoring of the discharge. The additional monitoring will be to support water quality
modeling efforts within the Cape Fear River Basin, and shall be consistent with a monitoring plan developed
jointly by the Division and affected stakeholders.
A. (8) ANALYTICAL DETECTION LEVELS
When an approved analytical protocol with the appropriate minimum detection level is followed and a result of
"non -detectable" or "below quantitation limit" is obtained, the pernuttee will be considered to be in compliance
with the numerical permit limit for that pollutant.
[This condition is inserted to acknowledge that the low equivalent concentration limits imposed by the OCPSF
guidelines, combined with the additional non-OCPSF process flows, will result in situations where the detection
limit of the EPA approved analytical protocols will not be sufficiently low enough to verify that a particular
pollutant is in compliance with the permit limits.]
NPDES No. NC0001899

A(9) EFFLUENT LIMITATIC AND MONITORING REQUIREMED (001/OCPSF)
During the period beginning on the e.-__we date of the permit and Lasting until expirz__-, the Permittee is authorized to
discharge OCPSF related process wastewater from outfall serial number 001. Such discharges shall be limited and monitored
by the Permittee as specified below:
Effluent Characteristic
Daily Maximum
pounds/day
Monthly Average
pounds/day
Measurement
Frequency
Sample
Type
Sample
Location'
cena hthene
0.004
0.001
Annually
Grab
Effluent
cena hthlene
0.004
0.001
Annually
Grab
Effluent
Acrylonitrile
0.015
0.006
Annually
Grab
Effluent
thracene
0.004
0.001
Annually
Grab
Effluent
Benzene
0.008
0.002
Annually
Grab
Effluent
Benzo a anthracene'
0.004
0.001
Annually
Grab
Effluent
3 4-Benzofluoranthene
0.004
0.001
Annually
Grab
Effluent
Benzo k fluoranthene'
0.004
0.001
Annually
Grab
Effluent
Benzo a rene'
0.004
0.001
Annually
Grab
Effluent
Bis 2-eththe Iphthalate
0.017
0.006
Annually
Grab
Effluent
Carbon Tetrachloride
0.002
0.001
Annually
Grab
Effluent
lorobenzene
0.002
0.001
Annually
Grab
Effluent
loroethane
0.016
0.006
Annually
Grab
Effluent
Chloroform
0.003
0.001
Annually
Grab
Effluent
2-Chlorohenol
0.006
0.002
Annually
Grab
Effluent
Chrysenel
0.004
0.001
Annually
Grab
Effluent
Di-n-butylhthalate
0.003
0.002
Annually
Grab
Effluent
12-Dichlorobenzene
0.010
0.005
Annually
Grab
Effluent
13-Dichlorobenzene
0.003
0.002
Annually
Grab
Effluent
1 4-Dichlorobenzene
0.002
0.001
Annually
Grab
Effluent
I1-Dichloroethane
0.004
0.001
Annually
Grab
Effluent
1 2-Dichloroethane
0.013
0.004
Annually
Grab
Effluent
11-Dichloroethlene
0.002
0.001
Annually
Grab
Effluent
1 2-trans-Dichloroethlene
0.003
0.001
Annually
Grab
Effluent
24-Dichlorohenol
0.007
0.002
Annually
Grab
Effluent
1,2-Dichloropropane
0.014
0.009
Annually
Grab
Effluent
1,3-Dichloropropylene
0.003
0.002
Annually
Grab
Effluent
Diethyl phthalate
0.012
0.005
Annually
Grab
Effluent
2,+Dimethylphenol
0.002
0.001
Annually
Grab
Effluent
Dimethyi phthalate
0.003
0.001
Annually
Grab
Effluent
6-Dinitro-o-cresol
0.017
0.005
Annually
Grab
Effluent
2 4-Dinitrohenol
0.007
0.004
Annually
Grab
Effluent
2 4-Dinitrotoluene
0.017
0.007
Annually
Grab
Effluent
2 6-Dinitrotoluene
0.039
0.016
Annually
Grab
Effluent
Eth (benzene
0.007
0.002
Annually
Grab
Effluent
Fluoranthene
0.004
0.002
Annually
Grab
Effluent
Fluorene
0.004
0.001
Annually
Grab
Effluent
Hexachlorobenzene
0.002
0.001
Annually
Grab
Effluent
Hexachlorobutadiene
0.003
0.001
Annually
Grab
Effluent
Hexachloroethane
0.003
0.001
Annually
Grab
Effluent
Methyl Chloride
0.012
0.005
Annually
Grab
Effluent
Methylene Chloride
0.005
0.002
Annually
Grab
Effluent
Naphthalene
0.004
0.001
Annually
Grab
Effluent
Nitrobenzene
0.004
0.002
Annually
Grab
Effluent
2-Nitrophenol
0.004
0.002
Annually
Grab
Effluent
-Nitro henol
0.008
0.004
Annually
Grab
Effluent
Phenanthrene
0.004
0.001
Annually
Grab
Effluent
Phenol
0.002
0.001
Annually
Grab
Effluent
rene
0.004
0.002
Annually
Grab
Effluent
etrachloroethlene
0.003
0.001
Annually
Grab
Effluent
Toluene
0.005
0.002
Annually
Grab
Effluent
1 2 4-Trichlorobenzene
0.009
0.004
Annually
Grab
Effluent
111-Tdchloroethane
0.003
0.001
Annually
Grab
Effluent
112-Trichloroethane
0.003
0.001
Annually
Grab
Effluent
richloroeth lene
0.003
0.001
AnnuallyGrab
Effluent
n Chloride
0.016
0.006
Annually
Grab
Effluent
otal PAW
Annually
Grab
Effluent
PAH' = Polynuclear aromatic hydrocarbons; benzo(a)anthracene, benzo(a)pyrene, 3,4-benzofluoranthene, benzo(k)fluoranthene,
chrysene, dibenz(a,h)anthracene, indeno(1,2,3 - cd)pyrene
Permit NC0001899

NCDENR/DWQ
FACT SHEET FOR NPDES PERMIT DEVELOPMENT
Performance Fibers, Inc
NC0001899
Facility Information
(IJ Facility Name:
Performance Fibers Inc k% W I P
(2.) Permitted Flow MGD): j
0.244
(6.) County:
Chatham
(3.) Facility Class:
(N/A
(7.) Regional Office
Raleigh
(4.) Pretreatment Program:
(9.) USGS l'opo Quad:
E22SE
(5.) Permit Status: '..
Existing
(9.) USGS Quad Name:
Stream Characteristics
0.) Receiving Stream:
Haw River (001)
(7.) Drainage Area (mi2):
9E0 (001)
UT to Shaddox Creck (002)
(2.) Sub -basin:
03-06-07
(8.) Summer 7Q10 (cfs):
40 (min release)
(3.) Stream Assessment Unit: '
16-(42)
(9.) Winter 7Q10 (cfs).
(4J Stream Classification:
WS-W (001)
(10) 30Q2 (cfs)-.
(5.) 303(d) Status:
(11.) Avera&e Flow (cfs):
181,4
(6.)305(b) Status:
(12.) IWC %:
_ -.
0.91 (001)
I. Proposed Changes Incorporated into Permit Renewal
• Remove fecal coliform and TRC monitoring from outfall 001.
• Remove zinc and fluoride monitoring from outfall 002.
• Reduce nutrient monitoring to quarterly and add nutrient reopener as recommended in the Middle Cape
Fear permitting strategy.
II. Summary
Performance Fibers (formerly Honeywell) manufactures polyester/synthetic fibers to be used in automobile
seatbelts.
Outfall 001 consists of process wastewater and sanitary wastewater. Process wastewater is generated from non -
process cooling tower blowdown, steam condensate, regenerated water from water softeners, demineralizer
blowdown, water rinse from polyester parts cleaning operations, stormwater from raw material handling areas,
finish oil pretreatment (ultrafiltration permeate), beam cleaning and floor drains. Sanitary wastewater is estimated
as 10,000 gpd. Performance Fibers recycles process wastewater and reclaims oil from the process.
Outfall 002 consists of stormwater, steam condensate, air dryer condensate, and fire pond overflow water.
The facility falls under the OCPSF guidelines for Other Fibers (40 CFR 414 Subpart C) and direct discharge, end of
pipe biological treatment. Performance Fibers has no guideline -defined metal bearing waste streams.
This portion of the Haw River is below the dam at Lake Jordan and prior to the confluence of the Cape Fear River.
Although this particular portion is not classified NSW, the Middle Cape Fear permitting strategy applies. The
modeling unit expects to conduct streams studies and modeling in the next permit cycle to determine limits for
nutrients and oxygen demanding wastes in these waters. The strategy recommends quarterly TP and TN
monitoring and the addition of a reopener clause for additional nutrient monitoring in the future.

NPDFS Permit Fact Sheet - 11, _ _/06
Page 2
Performance Fibers
NC0001899
Limit Development
Process and non -process wasteflows have been historically difficult to characterize at this facility. In 1995 a
monitoring study was conducted to characterize wastewater sources and their contribution to the total BOD
loading. Based on that study it was determined that non -process flows contribute a significant BOD load (unlike
typical OCPSF facilities) and that an additional allowance should be granted. The existing BOD and TSS limits are
therefore based on effluent guidelines for OCPSF process wastewater (40 CFR 414.30), non -process wastewater and
sanitary wastes. No change to these calculated limits is recommended for his renewal.
III. Compliance Summary
DMR Data Review
Monthly average flows are at 33% capacity with maximum monthly average flows at 45% capacity. This is a slight
decrease from the previous renewal. All limited parameters are well within permit requirements. The facility does
currently chlorinate and past permits did include a fecal coliform limit. That limit was removed in the previous
permit on the basis that the dilution ratio for the 0.01 MGD sanitary flow is approximately 2500:1 based on a 40 cfs
7Q10 flow in the Haw River. Current policy requires a fecal coliform limit for facilities with a dilution ratio of less
than 331:1 (unless the discharge is to a class B or a coliform impaired waterbody). Performance Fibers chlorinates
the entire wasteflow (process, non -process, and sanitary) in order to comply with the fecal coliform limit, and has
indicated that they would have no reason to add chlorine to the wastestream if there were no fecal coliform
requirement. Therefore both fecal coliform and chlorine monitoring will be removed from the draft permit.
Table 1. Summary of 2004-2006 Monthly Average DMR Data
Flow
(MGD)
Temp.
(de C)
TRC
(m )
BOD
(#/da)
TSS
(#/da)
D.O.
(m )
TN
(#/da)
TP
(#/da)
Specific
Conductance
pH
O&G
(#Ida )
Avg
0.08
18.77
0.14
1.29
2.94
9.05
4.48
1.00
949.07
7.37
3.21
Max
0.11
26.29
0.2
2.00
4.46
12.60
10.25
2.00
1440.00
7.70
5.50
Min
0.05
9.69
0.08
0.22
1.48
6.00
1.25
0.35
0.00
7.13
0.60
Limit
0.244
10.4
5.0
6-9
20
Instream Data Review
The permit requires temperature, conductivity, and DO monitoring instream, however these requirements are
waived while the facility is a member of the Lower Cape Fear River Basin Association. Currently there is a
downstream coalition monitoring station, but no upstream station to provide comparative data. Therefore instream
data was not reviewed for this renewal. However the 2005 Cape Fear Basin Plan lists this segment of Haw River as
supporting for its aquatic life and recreational uses.
RPA Analysis
The facility does not currently have monitoring for toxicants (other than OCPSF requirements) at outfall 001.
Although several metals were present in the pollutant scan submitted as part of the permit application, none existed
in concentrations that could be expected to cause an exceedance of water quality standards. Also, no parameters
were detected as part of the yearly OCPSF scans.
The facility currently has annual monitoring for zinc and fluoride at outfall 002. Based on the low levels of these
pollutants present in the discharge and the high dilution instream, an RPA was not conducted for these parameters.
Table 2 summarizes fluoride and zinc data. Since there are so few data points, values from the previous renewal
were reviewed as well, but are not included in the table. Based on the data, fluoride and zinc monitoring will be
removed from the permit.

NPDES Permit Fact Sheet — 11 /06 Performance Fibers
Page 3 NC0001899
Table 2: 2004-2006 Zinc and Fluoride Values
Date
Parameter
Unit
Value
Allowable
1/13/2004
00951- Fluoride, Total (as F)
m /l
0.12
192,175.5 mg/L
1 /12/2005
00951- Fluoride, Total (as F)
mg/1
0.14
1/25/2006
00951- Fluoride, Total (as F)
mg/l
0.19
1/12/2005
01092- Zinc, Total (as Zn)
u /l
15
5338.2ug/L
1/25/2006
01092 - Zinc, Total (as Zn)
ug/L
39
WET Test Results
The facility has a quarterly, chronic whole effluent toxicity testing requirement at 0.94% effluent concentration at
outfall 001. They have passed 19 of 19 tests administered since January 2002.
The facility also has an annual acute toxicity testing requirement at outfall002. They have passed 5/5 test conducted
since April 2002.
Correspondence File Review/Compliance History
The facility appears to be well operated. No concerns were noted in compliance inspections performed during
the 2002-2006 review period. There have been no violations of the permitted limits.
IV. Proposed Schedule for Permit Issuance
Draft Permit to Public Notice: November 22, 2006
Permit Scheduled to Issue: February 1, 2006
V. State Contact Information
If you have any questions on any of the above information or on the attached permit, please contact Toya
Fields at [phone], extension 551.
Copies of the following are attached to provide further information on the permit development:
• Draft permit
NPDES Recommendation by:
Signature Date
Regional Office Comments:
Regional Recommendation by:
Signature Date
Regional Supervisor:
Signature Date

MIDDLE CAPE FEAR STRATEGY
(Subbasins 30607, 30613-30616r 30618-30620)
Backeround
The Middle Cape Fear includes the Haw River (from Jordan Dam to Deep River) and the Upper Cape Fear
and Little Rivers. The Haw River is classified as NSW, and nutrient -related impacts are apparent downstream
of the Jordan Dam. The Division added a 6.7-mile stretch of the Cape Fear River (from the confluence of the
Haw and Deep Rivers to Sanford) to the 2006 303(d) list due to chlorophyll a exceedances; and 6.2 miles of
streams due to low D.O. The Modeling Unit expects to initiate stream studies in 2010 and modeling in 2012
to determine limits for nutrient and oxygen -demanding wastes in these waters.
Permit Requirements
Table 3 summarizes the requirements for dischargers in the Middle Cape Fear sub -watershed. Dischargers
here should monitor nutrients at the frequencies set in 2B .0508 and report the results as concentrations. It is
possible that we (DWQ) will expect these dischargers to conduct supplementary TN and TP monitoring to
support stream studies and modeling, beginning around January 2009. The permits will include a special
condition, similar to one used in the Jordan Lake permits, noting that the Division may require this
monitoring later in the permit cycle.
Table 3. Permitting Strategy - Middle Cape Fear - REVISED
Subbasins: 30607 30613 30615 30619
30614 30616 30618 30620
DISCHARGER TYPE
PERMITTED
FLOW (MGD)
TN, TP
LIMITS
NUTRIENT MONITORING
SPECIAL CONDITIONS
Frequency
(TN, TP) tit
Units
(TN, TP)
Report N
Species
Mass
Calcs
Re -Opener
All Dischargers
21.0
See
"General
Req`ts"
1/Month
Conc.
Y
>0.05 to <I.0
1/Quarter
Conc.
Y
<0.05
N/A
N/A
Y
(1) Per 2B .0508, Footnote (*)(2)(B)
Supplement to NPDES Permitting Strategies — Cape Fear, 2006 - REVISED !!

MIC E CAPE FEAR STRATEGY
Permit Language
The following are nutrient -related conditions for the Middle Cape Fear sub -watershed permits. They include
effluent sheets and special conditions. Refer to Table 3 of the permitting strategy to determine which of these
requirements apply to a given permit. The effluent sheet below includes standard as well as nutrient -related
language in order to provide some context.
Tmit Writers
ach effluent sheet:
harry over existing permit limits for nutrients!
Include nutrient parameters and set monitoring
requirements per Table 3 )
Legend
EFFLUENT Standard permit text
Flow (MGD)
EFFLUENT New text for permits in this basin
Flow (MGD)
Input from Permit Writer (facility or sub -
watershed -specific)
(test text] Comments to Permit Writers (delete prior
to Public Notice)
A.(1.) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS
a. During the period beginning on the effective date of this permit and lasting until expiration. the
Perntittee shall be authorized to discharge treated effluent from Outfall 001 subject to the following
effluent limitations and monitoring requirements:
EFFLtt E"T
CHARACTERISTICS
EFFLUENT LIMITATIONS
MONITORING REQUIREMENTS
Monthly
Average
Weekly
Average
Daily
Maximum
Measurement
Frequency
sample
Type
Sample
Location t't
Flow (MGD)
Continuous
Recording
t or E
Total Nitrogen (mg/L) t:f
[existing]
[See Table 31
Comp. Grab
E
Total Phosphorus (mg/L) 9
fexisbngi
[See Table 31
Comp.Grab
E
Footnotes:
0) Sa triple Loca tlon: I - Influent, E - Effluent.
(2) TN=TKN+NO3-N+NOrN, where TNisTotal Nitrogen,TKNisTotaIKeldahINitrogen,andNO;--Nand
NOrN are Nitrate and Nitrite Nitrogen, respectively. I6iclude this footnote onht i f parameters iuctnde TN. I
(3) The quarterly average for total phosphorus shall be the aN erage of composite.grab samples collected weekly
during each calendar quarter Qanuary-March, April -June, July -September, October -December). Unclude this
footnote only for fagih, lies with a iluatterly average TP limit.]
b. There shall be no discharge of floating solids or visible foam in other than trace amounts.
A.(2.) PERMIT RE -OPENER: SUPPLEMENTARY NUTRIENT MONITORING
Pursuant to N.C. General Statutes Section 143-215.1 and the implementing rules found in Title 15A of the
North Carolina Administrative Code, Subchapter 02H, specifically, 15A NCAC 02H.0112(b)(1) and
02H.0114(a), and Part II, Sections B.12. and B.13. of this Permit, the Director of DWQ may reopen this
permit to require supplemental nutrient monitoring of the discharge. The additional monitoring will be to
support water quality modeling efforts within the Cape Fear River Basin, and shall be consistent with a
monitoring plan developed jointly by the Division and affected stakeholders.
-- end of middle cape fear sub -watershed strategy --
Supplement to NPDES Permitting Strategies - Cape Fear, 2006 - REVISED 12

-Per o�Fbers NPDES V as-tawater Permit
Subject: Performance Fibers NPDES Wastewater Permit Renewal
From: "Powell, Chuck" <[e-mail]>
Date: Tue, 14 Nov 2006 16:10:54 -0500
To: "Toys Fields" <[e-mail]>
Ms. Fields:
Per our meeting at your office in Raleigh a few weeks ago, Performance Fibers understands that there is a
possibility that the Fecal Coliform Monthly monitoring requirement may be taken out of our new NPDES
permit that is currently undergoing renewal with DWQ. If the Fecal Coliform monitoring requirement is
taken out of the renewed permit, then Performance Fibers will cease chlorination treatment activity at our
wastewater treatment plant. Ceasing chlorination activity will enhance safety and reduce treatment costs.
We currently chlorinate at the tail end of our treatment process at our chlorine contact chamber. We
would disconnect chlorine cylinder operations and simply send effluent and polishing pond, blend through
the contact chamber without chlorination.
We also understand that there is a possibility that DWQ could also take out monitoring requirements for
Zinc and Fluoride.
We appreciate your meeting with us in person at your office to discuss specifics related to the renewal of
our NPDES permit. Please contact me if you have any further questions.
Sincerely,
Chuck
Perforrrtanoe Y' Fibers
Charles E. Powell, Jr., REM
EnvironmentalAndustrial Hygiene Leader
Performance Fibers, Inc.
338 Pea Ridge Road
New Hill, NC 27562
[phone]-Off ice
[phone]-Fax
[e-mail]
Disclaimer:
This e-mail communication and any attachments may contain confidential
and privileged information and is for use by the designated
addressee(s) named above only. If you are not the intended addressee,
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Thank you.
1 of 1 11/14/20064:17 PM

MONITORING REPORT(MR) VIOLATIONS for: Repon Date: 11/15/06 Page: 1 of 6
Permit: nc0001899 MRs Between: 1-2004 and 10-2006 Region:% Violation Category: 95 Program Category:
Facility Name: % Param Name: % County:% Subbasin: / Violation Action:
Major Minor:
PERMIT: NC0001899 FACILITY: Performance Fibers Inc - Performance Fibers / Moncure COUNTY: Chatham REGION: Raleigh
Limit Violation
MONITORING OUTFALL VIOLATION UNIT OF CALCULATED
REPORT / PPI LOCATION PARAMETER DATE FREQUENCY MEASURE LIMIT VALUE VIOLATION TYPE VIOLATION ACTION
01 - 2004 001 Effluent Chlorobenzene 01/31/04 Annually Ibs/day 0.001 0.002 Monthly Average Exceeded E roArction, Data Entry
Monitoring Violation
MONITORING
OUTFALL
VIOLATION
UNIT OF CALCULATED
REPORT
/PPI
LOCATION
PARAMETER
DATE
FREQUENCY
MEASURE LIMIT VALUE
VIOLATION TYPE
VIOLATIONACTION
12-2005
001
Effluent
1,1,1-tdchloro- ethane
12/31/05
Annually
Ibs/day
Frequency Violation
None
12-2005
001
Effluent
1,1,2-trichloro-ethane
12/31/05
Annually
Ibs/day
Frequency Violation
None
12-2005
001
Effluent
1,1-dichlorcethane
12/31/05
Annually
Ibs/day
Frequency Violation
None
12-2005
001
Effluent
1,1-dichloroethylene
12/31/05
Annually
Ibs/day
Frequency Violation
None
12 - 2005
001
Effluent
1,2,4-trichloro- benzene
12/31/05
Annually
Ibs/day
Frequency Violation
None
12.2005
001
Effluent
1,2-dichlorobenzene
12/31/05
Annually
Ibs/day
Frequency Violation
None
(ortho-dichlorobenzene;
1,2-DCB)
12-2004
001
Effluent
1,2-dichlorothane
12/31/04
Annually
Ibs/day
Frequency Violation
None
12-2005
001
Effluent
12-dichlorcethane
12/31/05
Annually
Ibs/day
Frequency Violation
None
12-2005
001
Effluent
1,2-dichloropropane
12/31/05
Annually
Ibs/day
Frequency Violation
None
12.2005
001
Effluent
1,2-trans-dichloro-ethylene
12/31/05
Annually
Has/day
Frequency Violation
None
12-2004
001
Effluent
1,3 dichloropropene
12/31/04
Annually
Ibs/day
Frequency Violation
None
12-2005
001
Effluent
1,3 dichloropropene
12/31/05
Annually
Ibs/day
Frequency Violation
None
12-2005
001
Effluent
1,3-dichlorobenzene
12/31/05
Annually
IIts/day
Frequency Violation
None
(meta-dichlorobenzene;
•
1,3-DCB)

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MONITORING REPORT(MR) VIOLATIONS for: Report Date: 11/15/06 Page: 3 of 6
Permit: nc0001899 MRs Between: 1-2004 and 10-2006 Region: % Violation Category: go Program Category: %
Facility Name: % Param Name: % County: % Subbasin: % Violation Action: %
Major Minor, %
PERMIT: NC0001899 FACILITY: Performance Fibers Inc - Performance Fibers / Moncure COUNTY: Chatham REGION: Raleigh
Monitoring Violation
MONITORING
OUTFALL
VIOLATION
UNITOF CALCULATED
REPORT
/ PPI
LOCATION
PARAMETER
DATE
FREQUENCY
MEASURE LIMIT VALUE
VIOLATION TYPE
VIOLATION ACTION
12.2005
001
Effluent
Benzene
12/31/05
Annually
Ibs/day
Frequency Violation
None
12-2005
001
Effluent
Senzo(A)anthracene
12/31/05
Annually
Ibs/day
Frequency Violation
None
12 - 2005
001
Effluent
Benzo(A)pyrene
12/31/05
Annually
Ibs/day
Frequency Violation
None
12 - 2005
001
Effluent
Benzo(K)fluoramhene
12/31/05
Annually
Ibs/day
Frequency Violation
None
12 - 2004
001
Effluent
Bis (2-Ethylhexyl) Phthalate
12131/04
Annually
Its/day
Frequency Violation
None
(dl(2-ethylhexyl )phthalate)
12 - 2005
001
Effluent
Bis (2-Ethylhexyl) Phthalate
12/31/05
Annually
Ibslday
Frequency Violation
None
(di(2-ethy1hexyl )phthalate)
12 - 2004
001
Effluent
Carbon Tetrachloride
12/31/04
Annually
Ibs/day
Frequency Violation
None
12 - 2005
001
Effluent
Carbon Tetrachloride
12131/05
Annually
Ibs/day
Frequency Violation
None
12.2005
001
Effluent
Chlorobenzene
12/31/05
Annually
Ibslday
Frequency Violation
None
12 - 2005
001
Effluent
Chloroethane
12/31/05
Annually
Ibs/day
Frequency Violation
None
12-2004
001
Effluent
Chloroform
12/31/04
Annually
Ibs/day
Frequency Violation
None
12-2005
001
Effluent
Chloroform
12/31/05
Annually
Ibslday
Frequency Violation
None
12.2005
001
Effluent
Chrysene
12/31/05
Annually
Ibs/day
Frequency Violation
None
06.2004
001
Effluent
DO, Oxygen, Dissolved
06/30/04
Monthly
mg/1
Frequency Violation
None
12 - 2005
001
Effluent
Di-n-Butyl Phthalate
12/31/05
Annually
Ibs/day
Frequency Violation
None
12 - 2005
001
Effluent
Diethyl Phthalate
12/31/05
Annually
Ibs/day
Frequency Violation
None
12 - 2005
001
Effluent
Dlmethyl Phthalate
12/31/05
Annually
Ibs/day
Frequency Violation
None

MONITORING REPORT(MR) VIOLATIONS for: -
Repod Date: 11/15/06
Page: 4 of 6
Permit:
nc0001899
MRS Between: 1-2004
and 10-2006
Region: %
Violation Category: .%
Program Category:
Facility Name:
%
Param Name: %
County: %
Subbasin: %
Violation Action: %
Major Minor,
%
PERMIT: NC0001899
FACILITY: Performance Fibers Inc - Performance Fibers / Moncure
COUNTY: Chatham
REGION:
Raleigh
Monitoring Violation
I
MONITORING OUTFALL
VIOLATION
UNIT OF
CALCULATED
REPORT
/ PPI
LOCATION
PARAMETER
DATE
FREQUENCY
MEASURE
LIMIT VALUE
VIOLATION TYPE
VIOLATION ACTION
12.2005
001
Effluent
Ethylbenzene
12/31/05
Annually
Ibs/day
Frequency Violation
None
03.2004
001
Effluent
Flow, in conduit or thru treatment
03/21/04
Continuous
mgd
Frequency Violation
None
plant
12 - 2004
001
Effluent
Flow, in conduit or thru treatment
12/18/04
Continuous
mgd
Frequency Violation
None
plant
12 - 2004
001
Effluent
Flow, in conduit or thru treatment
12/19/04
Continuous
mgd
Frequency Violation
None
plant
I I
12 - 2004
001
Effluent
Flow, in conduit or thru treatment
12/20/04
Continuous
mgd
Frequency Violation
None
plant
03-2006
001
Effluent
Flow, in conduit or thru treatment
03/31/06
Continuous
mgd
Frequency Violation
None
plant
06 - 2006
001
Effluent
Flow, in conduit or thru treatment
06/30/06
Continuous
mgd
Frequency Violation
None
plant
12-2005
001
Effluent
Fluoranthene
12/31/05
Annually
Ibs/day
Frequency Violation
None
12-2005
001
Effluent
Fluorene
12/31/05
Annually
Ibs/day
Frequency Violation
None
12-2005
001
Effluent
Hexachlorobenzene
12/31/05
Annually
Ibs/day
Frequency Violation
None
12 - 2005
001
Effluent
Hexachlorobutadiene
12/31/05
Annually
Ibs/day
Frequency Violation
None
12 - 2005
001
Effluent
Hexachloroethane
12/31/05
Annually
Ibs/day
Frequency Violation
None
12 - 2005
001
Effluent
Methyl Chloride (chloromethane)
12/31/05
Annually
Ibs/day
Frequency Violation
None
12-2005
001
Effluent
Methylene Chloride
(dlchloromethane, methylene
12/31/05
Annually
Ibs/day
Frequency Violation
None
dichloride)
12-2005
001
Effluent
Naphthalene
12/31/05
Annually
Ibs/day
Frequency Violation
None

MONITORING REPORT(MR) VIOLATIONS for:
Repod Date: 11/15/o6
Page: 5 of 6
Permit:
nc0001899
MRS Between: 1-2004
and 10-2006
Region: %
Violation Category: %
Program Category:
%
Facility Name:
%
Param Name: %
County: %
Subbasin: %
Violation Action:
Major Minor:
%
PERMIT: NC0001899
FACILITY: Performance Fibers Inc - Performance Fibers / Moncure
COUNTY: Chatham
REGION:
Raleigh
Monitoring Violation
MONITORING OUTFALL
VIOLATION
UNITOF
CALCULATED
REPORT
/ PPI
LOCATION
PARAMETER
DATE
FREOUENCY
MEASURE
LIMIT VALUE
VIOLATION TYPE
VIOLATION ACTION
12.2005
001
Effluent
Nitrobenzene
12/31/05
Annually
Ibs/day
Frequency Violation
None
04 - 2006
001
Effluent
Oil 8 Grease
Q4l29/06
Weekly
Ibs/day
Frequency Violation
None
12.2005
001
Effluent
Phenanthrene
12/31/05
Annually
Ibs/day
Frequency Violation
None
12 - 2005
001
Effluent
Phenol, Single Compound
12/31/05
Annually
Ibs/day
Frequency Violation
None
12 - 2005
001
Effluent
Pyrene
12/31/05
Annually
Ibs/day
Frequency Violation
None
04 - 2006
001
Effluent
Solids, Total Suspended
04/29/06
Weekly
Ibs/day
Frequency Violation
None
12-2005
001
Effluent
Tetrachloroethylene
12/31/05
Annually
Ibs/day
Frequency Violation
None
12 -2005
001
Effluent
Toluene
12/31/05
Annually
Ibs/day
Frequency Violation
None
12 - 2005
001
Effluent
Trichloroethylene
12/31/06
Annually
Ibs/day
Frequency Violation
None
12-2005
001
Effluent
Vinyl Chloride
12/31/05
Annually
Ibs/day
Frequency Violation
None
03-2004
001
Effluent
pH
03/21/04
Continuous
su
Frequency Violation
None
12-2004
001
Effluent
pH
12/18/04
Continuous
su
Frequency Violation
None
12-2004
001
Effluent
pH
12/19/04
Continuous
su
Frequency Violation
None
12 - 2004
001
Effluent
pH
12/20/04
Continuous
su
Frequency Violation
None
05-2006
001
Effluent
pH
05/11/06
Continuous
su
Frequency Violation
None
04 - 2004
002
Effluent
Flow, in conduit or thru treatment
04/03/04
Weekly
mgd
Frequency Violation
None
plant
09 - 2005
002
Effluent
Flow, in conduit or thru treatment
09/03/05
Weekly
mgd
Frequency Violation
None
plant

MONITORING REPORT(MR) VIOLATIONS for: ReportDate: 11/15106 Page: 6 of 6
Permit: nc0001899 MRs Between: 1-2004 and 10-2006 Region: % Violation Category: % Program Category: %
Facility Name: % Param Name: % County: % Subbasin: V. Violation Action: "o
Major Minor: %
PERMIT: NC0001899 FACILITY: Performance Fibers Inc - Performance Fibers / Moncure COUNTY: Chatham REGION: Raleigh
Monitoring Violation
MONITORING OUTFALL
VIOLATION
UNIT OF CALCULATED
REPORT /PPI
LOCATION
PARAMETER
DATE
FREQUENCY
MEASURE LIMIT VALUE
VIOLATION TYPE
VIOLATION ACTION
04 - 2006 002
Effluent
Flow, in conduit or lhm treatment
04/29/06
Weekly
mgd
Frequency Violation
None
plant
04 - 2004 002
Effluent
Temperature, Water Deg.
04/03/04
Weekly
deg c
Frequency Violation
None
Centigrade
09-2005 002
Effluent
Temperature, Water Deg.
09/03/05
Weekly
deg c
Frequency Violation
None
Centigrade
04.2006 002
Effluent
Temperature, Water Deg.
04/29/06
Weekly
deg c
Frequency Violation
None
Centigrade
12 -2004 002
Effluent
Zinc, Total (as Zn)
12/31/04
Annually
mgA
Frequency Violation
None
04-2004 002
Effluent
pH
04103/04
Weekly
su
Frequency Violation
None
09-2005 002
Effluent
pH
09/03/05
Weekly
su
Frequency Violation
None
04 - 2006 002
Effluent
pH
04/49/06
Weekly
su
Frequency Violation
None
Reporting Violation
MONITORING OUTFALL
VIOLATION
UNIT OF
CALCULATED
REPORT / PPf
LOCATION
PARAMETER
DATE
FREQUENCY
MEASURE
LIMIT VALUE VIOLATION TYPE
VIOLATION ACTION
10-2004
10/31/04
Signature Missing
None
07-2004 001
Effluent
Benzo(A)pyrene
07/31/04
Annually
Ibs/day
Parameter Missing
None
07-2004 001
Effluent
Benzo(K)fluoranthene
07/31/04
Annually
Ibs/day
Parameter Missing
None
07-2004 001
Effluent
Chlorobenzene
07/31/04
Annually
Ibs/day
Parameter Missing
None
07-2004 001
Effluent
Chloroethane
07/31/04
Annually
Ibs/day
Parameter Missing
None
01 - 2006 002
Effluent
Zinc, Total (as Zn)
01/31/06
Annually
mgA
Parameter reported with invalid
None
Unit of Measure

Whole Effluent Toxicity Testing Self -Monitoring Summary November 14, 2006
FACILITY REQUIREMENT
YEAR )AN
FED
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
NOV
DEC
P(:S Phosphate Company lec:004 48hr LC50 ac monthly it Md or mysW FOtd4BAc
Zoe$ N
N
N
N
N
N
N
N
N
N
N
N
NC0003255AX4 Begin 3/IR005 Frequmry:M
NonComp:
2003 N
N
N
—
N
N
N
N
N
N
N
N
Comfy. Besurn. Region: WARD Subbssin:TAR02
2004 R
—
N
N
N
H,N
H
H
H
H
H
H
PF: a oast
2005 H
H
N
H
H
H
H
H
H
H
H
H
1Q10: NA IWC(%)NA
2006 H
H
H
N
N
H
H
H
H
KS Phosphate Company lne.405 48hr LC50 monthly s mount Md or myaid Fthd48Ac
2
NCW03255IU05 Begin 6/29R006 Frequemy.M
NonComp:
2013
Cowry B... run Region: WARD Subbnnin:TAROT
2W4
PF: NA 5mml
200a
2010: NA IWC(%)0 Onw:
20tla
�.
PCS Phosphate Company loc.-N7 48hr LC50 monthly ac mmil Md or small FIM48AC
20M >IN
>1
>1N
- a1N
pop
alm
>1m
-IN
IN
-IN
-IN
-IN
NC003255/W7 Begin 3/IRW5 FrequencyM
NmComP
7= >1N
stop
1100
aIN
-IN
'>1N
atop
a100
IN
stop
-IN
>1w
Cowsy. Bmufon Re pn: WARO Subbuln: TARu]
20d >1m
slop r
>100
-IN
>1W
IN
>1W
-IN
>100
-IN
-IN
-100
PF: VAR Small
2005 >too
slop
-IN
IN
atop
>1N
-IN
atop
stop
-IN
>1N
>1N
7Ql0: TIDAL MC(Y.)NA a4v.
2" >100
MN
-IN
>100
IN
Mw
-IN
IN
stop
amo
'
PCs Phosphate Company lnc.lW 48hr LC50 ruca lY see mmit Md or mvsid FrIaMS&c
202 >10
>tN
>IN
>100
site
-IN
atop
-IN
-IN
>I00
aI00
'IN
NCM32551100 Begin 3/IRW5 Frequwcy.M
NonComp:
2003 -IN
IN
able
-IN
still
aIN
aIN
-IN
>100
atop
.atop
-IN
County: Bemfan Region: WARD SubbawTARW
M>1N
'IN
IN
>100
-IN
-IN
>tm
>IN
>1N
atop
,stop
>100
SgeN
2WF stun
-100
>IN
IN
atop
>1e0
-IN
IN
IN
-100
IN
IN
IWC(%) OrJv:
20110 stop
-IN
stop
-IN
>IN
IN
>1W
IN
IN
IN
remmalux WWTP clulim: I.TA
Cm74PF
2N2 Penn
—
—
Paso
—
—
Penn
—
—
Pass
—
—
NCW2T103/WI Begin'9/120W Formal J. Apr Jul Oct
F NonCom,'. Single
2N3 Paen
—
—
Pau
—
—
Penn
—
—
Pus
—
—
Coutny Robeson Region: FRO Subbusin: LlIM51
2004 Pau,>fi.hlp)
—
—
>6d8('tpmtt
—
—
Penn
—
—
prim
—
—
PF: 1.33 Spe ial
2W5 Pau
—
—
Pa.
—
—
Penn
—
—
Pass
—
—
TQ10:120 WC(%)1.8 oma:
2006 Paac
-_
_
pass
—
—
Fos
—
—
Pas
Partial Helium Church onshore 31%
Cerill
20(2 —
Pass
—
—
Pass
—
—
Pew
—
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Pace
—
NCW468W/WI Begin.NIQWI Fres tency.Q Feb May Aug Nov
+ NMCM Sm le
2003 —
Pus
—
—
Pena
—
—
Penn
—
—
Pus
—
Country, Guilfom Region: WSRO Subbuin:CPRI
2. —
Poo.
—
—
pus
—
—
Pass
—
—
Fan
sat
PF: 002 spxul
2W5 12
Pus
-
—
Penn
—
—
Fee
43.8
>62
Pua
—
7010:0.07 IWC(%)MA th sr.
2006 _
Pare
For
247
l0N
Penn
—
Ford.,In. LawHloe chr liar: 0.41%
CenTdPF
g 2002 Pus
—
-
Pass
—
—
Paw
—
—
Penn
—
—
NCO28835/001 BeginaLV2W] Frequemy.Q J. Amlul Oct
+ NonComp'. Single
M03 Pm
—
—
pass
—
—
Pass
—
—
Penn
—
—
Counly Beme Region: WARD Subbwin: ROA08
Nor Pena
—
—
Peas
—
—
over
—
—
Penn
—
—
PF:3A Spalnl
no Paw
—
-
Pass
—
—
Paw
—
—
Penn
—
—
7Q1(x1102 MCC%)0.42 ordc:
Man Puts
Pass
—
—
Pena
—
—
Fears
Perforeneam Flben, lee elulim0.94%
CenTdPF
2N2 IN
—
—
-100
—
—
s100
—
—
>100
—
—
NC0MR99/WI BeVn VlI 003 Placental Q Iw Am lul Oct
+ NonConp:Single
IDN IN
—
—
I.M.
Pys
—
Pau
—
—
Paw
—
—
County: Chatham Region: FRO Subbwin: CPR]
2004 wu
—
—
Pau
—
—
Pau
—
—
Pau
—
—
PF: 0.244 last
20N Paw
—
—
Pew
—
—
Paen
.-
—
Paen
—
—
7Q10:40 IWC(Y.)0.94 won:
20w Pan&
—
—
Pass
—
—
Pau
—
—
Parrormenm Fibma, Ito 24m W50 w mpoil emu Md
Fthd24Ac
2002 — - — >100 — — — — — — — —
*189o/W2 Begun VMWl Frequmry.A
NonComp:
2N0 — — — — >1N- — — — — — — —
ty Chalhmn Region: PRO Sumal CPFO)
2Ne — '- — >i00—
_ _ 4A smut
200 _ _ — — _ _ _ _ — — Paen —
TQI(bLLO DVC(Y.)NA oars:
MIN — _ _ ago
Perquimens County - Barbel WTP chrmonit 91P16
CenTdPF
=2— — — — — — — — — — — —
NCN69961/001 Begin:l/I12W5 Fp Fpesacy0 Feb May Aug Nov
+ NonComp:
=3 — — — — — — — — — — — —
County Pcmuimms Region: WARO Subteen: PAS52
200s — — — — — — — — — — — —
PF: (til Sµvul
2W5 — FY — — Fee — — Far — — Fall —
7010:Tidel MC(-A)NA Odin:
2008 — Fen — — Far — — Far —
Per9ulmeva Count, - whireiII WTP Chr Mmut: N14 CedOdPF 2N2 — — — — — — — — — — —
NL'W5I303/001 Begin l/IR005 Fremmay,.Q Feb May Aug Nov + NmComp: 2opn — -- — — — — — — — — —
County:Pemuimary Region: WARD Subbasin: PAS52 2op4— — — — — — — — — —
PF: NA 5 xi 2305 — Fal — — Far — — Fee — — Fell
7QI0:0 IWC('6)IW Ondm 20N — Fee — — Feu — — Fae —
4 Pre 2002 Data Asmiahk
LEGEND:
PERM- Permit Requimnmm LEf-Adminisunrive Collar -Target Frequency- Monitoring frequency: Q. Quarterly: M. Monthly; SM. Bimonthly; SA. Sentine lly; A. Annually; OWD- Onh when discharging; D. Discontinued monitoring retiiremem
Begin-Firstmonlhlegqvircd 2QIl-Rweiving suearn low Row cntmon (crs) +-quarterlyy monitoring increases to monthly upon failurem NR Months that\estingmut occur -ex. Ito, Apr, lu, On NNCM,- Current Compliance Requirement
PF-Perm mbinme(MGo) IWCb-Iuuormwasuconcmtntion PT P=iltmt AC - Acute CHR- Chronic
. Data Nowi et: f- FeNeW Mmu w; e -Ci nedapMia P.; my - Mysid shrimp; ChV -Chronic value P - Moruliry of noted pxrocolgx at highest concentration; at, Prrfomaed by DWQ Atlantic Tax Unit; In- Bad test
Reporting Notation:- Dom not required; NR-Not reported Facility ActivitySWm; I - laumlve.N -Newly lasued(To....eQ; H-Active but rot discharging;l.Mom&u available fmmomh in question;-ORC.ignnlummucld
33

Performance f*Fibers
5rP •8�' � �
September 6, 2006
Mr. Jerry Rimmer, Supervisor
Technical Assistance and Certification Unit
NC Dept. of Environment & Natural Resources
NC Water Pollution Control System Operators Certification Commission
1618 Mail Service Center
Raleigh, North Carolina 27699-1815
Dear Mr. Rimmer.
This letter is to noitify the WPCSOCC of an addition to the Back Up Operator In Responsible Charge (ORC) of the
wastewater treatment system at Performance Fibers, Inc., New Hill, Chatham County, North Carolina facility (NPDES
Pemtit No. NC0001899). Please add Mr. Charles E. Powell, Jr., (Certificate # 22306) as a second Back Up ORC in
addition to the current Back Up ORC, Mr. Linwood Mann (Certificate # 987028). Additionally, please remove from
your records Mr. Michael M. Borchers from your records as ORC as he is no longer employed at Performance Fibers,
Inc.
Attached is a new ORC Designation Form, complete with signatures and information on Lawrence Murray, ORC,
Linwood Mann, Back Up ORC, and Charles Powell, Back Up ORC. Please note this change in your records for this
facility.
Please call me if you have any questions at [phone].
Sincerely,
a---rrrrleess rrr"E.. Powell, Jr., REM
Environmental Engineer
Enclosure:
cc: Mr. Jeffrey Adams
Lab Certification Auditor
NCDENR
Div. of Water Quality
1623 Mail Service Center
Raleigh, NC 27699-1623
D. Peterson
B. Ferree
G.Gardner
D.Stidham
J. Sieber
Ms. Judy Garrett
Environmental Chemist II
NCDENR
Division of Water Quality
1628 Mail Service Center
Raleigh, NC 27699-1628
„.. R11!1r R(IAi) I CFV Hil I. NL
I TF I. 1111 >a, "uu

Water Pollution Control System ORC Designation Form
WPCSOCC
NCAC 15A:08G .0201
General Information:
Permittee Owner/Officer Name: Performance Fibers, Inc / Donald Peterson, Plant Manager
Mailing Address: 338 Pea Ridge Road
City:
New Hill
State: NC Zip:
Telephone Number: 542-2200
Signature. DI -It
27562 8951
9-7-06
..................................................,............... ,...... I
Facility Information:
Facility: performance Fibers Inc.
Permit Number: NC0001899 County: Chatham
! SUBMIT A SEPARATE FORM FOR EACH TYPE OF SYSTEM!
Mark (X) Type of Facile Class (1— 4)
Wastewater Plant _X 2
Physical/Chemical _
Collection System
Class
Spray Irrigation N/A
Land Application N/A
Subsurface N/A
.................................................................. a......
Operator in Responsible Charge:
Print Name: Lawranre n_ rr.,rray Social Security # : 240-98-9193
Certificate Type and Grade: WW—Grade 2 A Certificate #: 25810
Work Telephone: [phone] Signature:
........................................."I ... V.......... P. •.... 4.....I
Back -Up Operator in Responsible Charge: SEE ADDITIONAL BACK —OP ORC ON PAGE 2
Print Name: Charles E. Powell. Jr. Social Security # : 237-33-0325
Certificate Type and Grade: wastewater —Grade 2 Certificate #:
Work Telephone: (919 ) 545-3154 Signature:
Mail or Fax to: WPCSOCC
1618 Mail Service Center
Raleigh, N.C. 27699-1618
Fax:[phone]
Revised 10/2000

PAGE 2 - 2nd BACK- IRC DESIGNATION
Water Pollution Control System ORC Designation Form
WPCSOCC
NCAC 15A:08G .0201
General Information:
Permittee Owner/Officer Name:
Mailing Address:
City: State: Zip:
Telephone Number: (
— -:7/
Signature: _ Daic:
..................................................................
Facility Information: ... .
Facility:
Permit Number:
! SUBMIT A SEPARATE
7 County:
FOR EACH TYPE OF SYSTEM!
Mark 00 T_)W of Facility /Class (1 — 4) Class
Wastewater Plant Spray Irrigation N/A
Physical/Chemical Land Application N/A
Collection Syste _ Subsurface N/A
.......................................................................�
Operatoyln Responsible Charge
Name:
Social Security # :
Certificate Type and Grade: Certificate #:
Work Telephone: (__) Signature:
.........................................................................
Back -Up Operator in Responsible Charge:
Print Name: Linvood S. Mann Social Security # : 243-82-3852
Certificate Type and Grade: Lraxrnvater—rra lr Certificate #: gR7n7a
Work Telephone: [phone] Signature )�L
Mail or Fax to: WPCSOCC
1618 Mail Service Center
Raleigh, N.C. 27699-1618
Fax:[phone]
Revised 1012000

W ATE9 • Michael F. Easley, Governor
O(� William G. Ross, Jr., Secretary
rNorth Carolina Deparmcent of Environment and Natural Resources
gal"<
—i Alan W. Klimek, P.E., Director
owmftft� Division of Water Quality
April 24, 2006
Mr. Charles Powell, Jr.
Environmental Engineer
Performance Fibers
338 Pea Ridge Road
New Hill, NC 27562
Subject: Compliance Evaluation Inspection
Performance Fibers
NPDES Permit Number NC00bl899,
Stormwater Permit Number NCS000100
Chatham County
Dear Mr. Powell:
On April 24, 2006 Mr. Christopher Wu of the Raleigh Regional Office conducted a compliance
evaluation inspection of the Performance Fibers facility with the assistance of Mr. Lawrence
Murray, ORC of the facility, and yourself, Environmental Engineer. All help was appreciated as
it facilitated the inspection process.
The following observations were made:
1. The Performance Fibers WWTP is currently permitted to discharge at a rate of 0.244
MGD and consists of: a bar screen and grinder, aeration basin, neutralization
chamber, secondary clarifier, sludge drying bed, polishing pond, chlorine gas
disinfection, and a chlorine contact chamber. The facility does not currently have a
limit for TRC and will have difficulty meeting a new limit (that will be issued with
the new permit) without the aid of additional dechlorination.
2. Performance Fibers has a contract with Brunswick Waste Management Facility, LLC
located in Lawrenceville, VA. Sludge is collected and hauled to Virginia where it is
later placed in a landfill.
3. While Performance Fibers has its own certified laboratory it still contracts Pace
Analytical and TriTest Laboratories to conduct analyses.
4. In December 2005, it was discovered that the calibration curve for TRC was too high.
As a result, all DMRs prior to December were amended and re -submitted.
5. An inspection of stormwater permit NCS000100 was also conducted during the site
Jvalufina
mAY
North Carolina Division of Water Quality Raleigh Regional Office Surface Water Protection Phone [phone] Customer Service
Internet h2o.enr.state.nc.us 3800 Barrett Drive Raleigh, NC 27699-1628 FAX [phone]
An Equal OpportunitylAfhnnalive Action Employer— 50% Recyded110% Post Consumer Paper

Performance Fibers •
NC0001899
visit. Mr. Powell is keeping the stormwater files in excellent condition. All required
facets of the plan were easily accessible for review. A comprehensive SPPP plan was
present, as were a SPCC, site maps with clearly labeled outfalls, semi-annual
qualitative monitoring, semi-annual quantitative monitoring, a list of potential
pollutants of concern, and annual stormwater employee training.
6. Mr. Powell is keeping all of the files and data in a well organized fashion. Such order
eased the file review process.
The overall conditions of the Performance Fibers WWTP are compliant with Division standards.
If you have any questions regarding the attached report or any of our findings, please contact
Christopher Wu at: [phone] (or email: [e-mail]).
Sincerely,
Christopher Wu
Environmental Specialist
Cc: Mr. Lawrence Murray, Performance Fibers
Toya Fields, DWQ — NPDES
Christopher Wu, RRO
Central Files

Permit: NC0001899
Inspection Date: 04/24/2006
n
Owner - Facility: Performance Fibers / Moncure
Inspection Type: Compliance Evaluation
Operations & Maintenance Yes No NA NE
Is the plant generally clean with acceptable housekeeping? ■
❑
❑
❑
Does the facility analyze process control parameters, for ex: MLSS, MCRT, Settleable Solids, pH, DO, Sludge ■
❑
❑
❑
Judge, and other that are applicable?
Comment:
Permit Yes
No
NA
NE
(If the present permit expires in 6 months or less). Has the permittee submitted a new application? ■
❑
❑
❑
Is the facility as described in the permit?
■
❑
❑
❑
# Are there any special conditions for the permit?
❑
■
❑
❑
Is access to the plant site restricted to the general public?
■
❑
❑
❑
Is the inspector granted access to all areas for inspection?
■
❑
❑
❑
Comment: There are no special conditions for the permit.
Effluent Pipe
Yes
No
NA
NE
Is right of way to the ouffall properly maintained?
■
❑
❑
❑
Are the receiving water free of foam other than trace amounts and other debris?
■
❑
❑
❑
If effluent (diffuser pipes are required) are they operating properly?
❑
❑
■
❑
Comment:
Record Keepinn
Yes
No
NA
NE
Are records kept and maintained as required by the permit?
■
❑
❑
❑
Is all required information readily available, complete and current?
■
Cl
❑
❑
Are all records maintained for 3 years (lab. reg. required 5 years)?
■
❑
❑
❑
Are analytical results consistent with data reported on DMRs?
■
❑
❑
❑
Is the chain -of -custody complete?
■
❑
❑
❑
Dates, times and location of sampling
■
Name of individual performing the sampling
■
Results of analysis and calibration
■
Dates of analysis
■
Name of person performing analyses
■
Transported COCs
■
Are DMRs complete: do they include all permit parameters?
■
❑
❑
Cl
Has the facility submitted its annual compliance report to users and DWQ?
❑
❑
■
❑
Page # 3

Permit: NC0001899 Owner - Facility: Performance Fibers / Moncure
Inspection Date: 04/24/2006 Inspection Type: Compliance Evaluation
Record Keepng Yes No NA NE
(If the facility is = or > 5 MGD permitted flow) Do they operate 24/7 with a certified operator on each shift? ■ ❑ ❑ ❑
Is the ORC visitation log available and current? ■ ❑ ❑ ❑
Is the ORC certified at grade equal to or higher than the facility classification?
■
Cl
❑
❑
Is the backup operator certified at one grade less or greater than the facility classification?
■
Cl
Cl
❑
Is a copy of the current NPDES permit available on site?
■
❑
❑
❑
Facility has copy of previous year's Annual Report on file for review?
❑
❑
■
❑
Comment:
Flow Measurement - Effluent
Yes
No
NA
NE
# Is flow meter used for reporting?
■
❑
❑
❑
Is flow meter calibrated annually?
■
❑
❑
❑
Is the flow meter operational?
■
❑
❑
❑
(If units are separated) Does the chart recorder match the flow meter?
❑
❑
■
❑
Comment: The meter is calibrated on a quarterly basis.
Drying Beds
Yes
No
NA
NE
Is there adequate drying bed space?
■
❑
❑
❑
Is the sludge distribution on drying beds appropriate?
■
❑
❑
❑
Are the drying beds free of vegetation?
■
❑
❑
❑
# Is the site free of dry sludge remaining in beds?
■
❑
❑
❑
Is the site free of stockpiled sludge?
■
❑
❑
❑
Is the filtrate from sludge drying beds returned to the front of the plant?
■
❑
❑
❑
# Is the sludge disposed of through county landfill?
■
❑
❑
❑
# Is the sludge land applied?
❑
■
❑
❑
(Vacuum filters) Is polymer mixing adequate?
❑
❑
❑
■
Comment: The sludge is hauled and landfilled in Lawrenceville, VA.
Chemical Feed
Yes
No
NA
NE
Is containment adequate?
■
❑
❑
❑
Is storage adequate?
■
❑
❑
❑
Are backup pumps available?
❑
❑
❑
■
Is the site free of excessive leaking?
■
❑
❑
❑
Comment:
Page # 4

11
Permit: NC0001899 Owner - Facility:
Inspection Date: 04/242006 Inspection Type:
Performance Fibers I Moncure
Compliance Evaluation
Second ryClarifier
Yes
No
NA
NE
Is the clarifier free of black and odorous wastewater?
■
❑
❑
❑
Is the site free of excessive buildup of solids in center well of circular clarifier?
■
❑
❑
❑
Are weirs level?
■
❑
❑
❑
Is the site free of weir blockage?
■
❑
❑
❑
Is the site free of evidence of short-circuiting?
■
❑
❑
❑
Is scum removal adequate?
■
❑
❑
❑
Is the site free of excessive floating sludge?
■
❑
❑
❑
Is the drive unit operational?
■
❑
❑
❑
Is the return rate acceptable (low turbulence)?
■
❑
❑
❑
Is the overflow clear of excessive solids/pin floc?
■
❑
❑
❑
Is the sludge blanket level acceptable? (Approximately 1A of the sidewall depth)
■
❑
❑
❑
Comment: The sludge blanket was 2 feet (8 foot deep clarifier).
Disinfection -Gas
Yes
No
NA
NE
Are cylinders secured adequately?
■
❑
❑
❑
Are cylinders protected from direct sunlight?
■
❑
❑
❑
Is there adequate reserve supply of disinfectant?
■
❑
❑
❑
Is the level of chlorine residual acceptable?
■
❑
❑
❑
Is the contact chamber free of growth, or sludge buildup?
■
❑
❑
❑
Is there chlorine residual prior to de -chlorination?
■
❑
❑
❑
Comment:
Lagoon s
Yes
No
NA
NE
Type of lagoons?
# Number of lagoons in operation at time of visit?
1
Are lagoons operated in?
# Is a re -circulation line present?
■
❑
❑
❑
Is lagoon free of excessive floating materials?
■
❑
❑
❑
# Are baffles between ponds or effluent baffles adjustable?
❑
❑
■
❑
Are dike slopes clear of woody vegetation?
■
❑
❑
❑
Are weeds controlled around the edge of the lagoon?
■
❑
❑
❑
Page # 5

Permit: NC0001899 Owner - Facility: Performance Fibers / Moncure
Inspection Date: 04/24/2006 Inspection Type: Compliance Evaluation
Lagoons
Yes
No
NA
NE
Are dikes free of seepage?
■
0
C1
O
Are dikes free of erosion?
■
Q
El
0
Are dikes free of burrowing animals?
■
0
❑
O
# Has the sludge blanket in the lagoon (s) been measured periodically in multiple locations?
0
■
# If excessive algae is present, has barley straw been used to help control the growth?
Cl
Q
■
0
Is the lagoon surface free of weeds?
■
❑
❑
Is the lagoon free of short circuiting?
■
❑
0
❑
Comment: The sludge blanket is not measured in the lagoon.
Laboratory
Yes
No
NA_
NE
Are field parameters performed by certified personnel or laboratory?
■
0
Are all other parameters(excluding field parameters) performed by a certified lab?
■
❑
❑
❑
# Is the facility using a contract lab?
■
O
❑
❑
Is proper temperature set for sample storage (kept at 1.0 to 4.4 degrees Celsius)?
■
0
Q
❑
Incubator (Fecal Coliform) set to 44.5 degrees Celsius+/- 0.2 degrees?
0
O
■
O
Incubator (BOD) set to 20.0 degrees Celsius +/- 1.0 degrees?
0
O
■
0
Comment: The facility uses both Pace Analytical and TriTest Laboratories.
Aeration Basins
Yes
No
NA
NE
Mode of operation
Type of aeration system
Is the basin free of dead spots?
■
0
0
0
Are surface aerators and mixers operational?
■
0
O
Are the diffusers operational?
■
Q
0
0
Is the foam the proper color for the treatment process?
■
0
❑
Does the foam cover less than 25% of the basin's surface?
■
0
Is the DO level acceptable?
0
O
0
■
Is the DO level acceptable?(1.0 to 3.0 mg/I)
0
0
0
■
Comment:
Page # 6

NPDES REGIONAL WATER QUALITY
STAFF REPORT AND RECOMMENDATIONS
(This form is best filled out on computer, rather than hard copy)
Date: April 24, 2006 County: Chatham
To: NPDES Discharge Permittine Unit Permitee: Performance Fibers, Inc.
Attn. NPDES Reviewer: Tova Fields Application/ Permit No.: NC0001899
Staff Report Prepared By: Christopher Wu
Project Name: Performance Fibers, Inc.
SOC Priority Project? (Y/N) NL If Yes, SOC No.
A. GENERAL INFORMATION
1. This application is (check all that apply): ❑ New ® Renewal
❑ Modification
2. Was a site visit conducted in order to prepare this report? ® Yes or ❑ No.
a. Date of site visit: April 24, 2006
b. Person contacted and telephone number: Charles Powell; 545-3154
c. Site visit conducted by: Christopher Wu
d. Inspection Report Attached: ® Yes or ❑ No.
3. Keeping BIMS Accurate: Is the following BIMS information (a. through e. below) correct?
® Yes or ❑ No. If No, please either indicate that it is correct on the current application or the
existing permit or provide the details. If none can be supplied, please explain:
(If there is more than one discharge pipe, put the others on the last page of this form.)
a. Location OK on Application ❑,
OK on Existing Permit ❑, or provide Location:
b. Driving Directions OK on Application ❑,
OK on Existing Permit ❑, or provide Driving Directions (please be accurate):
c. USGS Quadrangle Map name and number OK on Application ❑,
OK on Existing Permit ❑, or provide USGS Quadrangle Map name and number:
d. Latitude/Longitude OK on Application ❑, (check at htto://www.topozone.com These are often
inaccurate) OK on Existing Permit ❑, or provide Latitude: Longitude:
e. Receiving Stream OK on Application ❑,
OK on Existing Permit ❑, or provide Receiving Stream or affected waters:
a. Stream Classification:
b. River Basin and Sub basin No.:
c. Describe receiving stream features and downstream uses:
For NEW FACILITIES Proceed to Section C. Evaluation and Recommendations
(For renewals or modiiicadons continue to section B)

NPDES REGIONAL WATER IUALITY
STAFF REPORT AND RECOMMENDATIONS
B. DESCRIPTION OF FACILITIES AND WASTE(S) (renewals and rnodificadons only)
1. Describe the existing treatment facility: The facility is permitted for 0.244 MGD and consists of: a bar
screen and grinder, aeration basin, neutralization chamber, clarifier, sludge drying bed, polishing pond,
chlorine gas disinfection, and a chlorine contact chamber.
2. Are there appropriately certified ORCs for the facilities? ❑ Yes or ❑ No.
Operator in Charge: Lawrence Murray Certificate # 25810 (Available in BIMS or Certification
Website)
Back- Operator in Charge: Linwood Mann Certificate # 987028
3. Does the facility have operational or compliance problems? Please comment: None
Summarize your BIMS review of monitoring data (Notice(s) of violation within the last permit cycle;
Current enforcement action(s)):
Are they currently under SOC, ❑ Currently under JOC, ❑ Currently under moratorium ❑? Have
all compliance dates/conditions in the existing permit, SOC, JOC, etc. been complied with? ❑ Yes
or ❑ No. If no, please explain:
4. Residuals Treatment: PSRP N (Process to Significantly Reduce Pathogens, Class B) or
PFRP ❑ (Process to Further Reduce Pathogens, Class A)?
Are they liquid or dewatered to a cake?
Land Applied? Yes ❑ No ❑ If so, list Non -Discharge Permit No.
Contractor Used:
Landfilled? Yes N No❑ If yes, where? Lawrenceville, VA; Brunswick Waste Management
Other?
Adequate Digester Capacity? Yes ❑ No ❑ Sludge Storage Capacity? Yes ❑ No ❑
Please comment on current operational practices:
5. Are there any issues related to compliance/enforcement that should be resolved before issuing this
permit? ❑ Yes or N No. If yes, please explain:
C. EVALUATIONAND RECOMMENDATIONS
1. Alternative Analysis Evaluation: has the facility evaluated the non -discharge options available? Give
regional perspective for each option evaluated:
Spray Irrigation: N/A
Connect to Regional Sewer System: N/A
Subsurface: N/A
Other Disposal Options: N/A
FORM: NPDES-RRO 06/03, 9/03 2

NPDES REGIONAL WATER QUALITY
STAFF REPORT AND RECOMMENDATIONS
2. Provide any additional narrative regarding your review of the application: The facility is not equipped
for a low-level TRC limit.
3. List any items that you would like NPDES Unit to obtain through an additional information
request. Make sure that you provide a reason for each item:
4. List specific Permit requirements that you recommend to be removed from the permit when
issued. Make sure that you provide a reason for each condition:
5. List specific special requirements or compliance schedules that you recommend to be included in
the permit when issued. Make sure that you provide a reason for each special condition:
6. Recommendation: ❑ Hold, pending receipt and review of additional information by regional office;
❑ Hold, pending review and approval of required additional information by NPDES permitting
office; ® Issue; ❑ Deny. If deny, please state reasons:
Reminder: attach inspection report if Yes was checked for 1 d.
7. Signature of reportpreparer:
Signature of WQS regional supervisor:
Date:
FORM: NPDES-RRO 06/03, 9/03

Performance f * Fibers
April 4, 2006
Ms. Judy Garrett
Environmental Chemist II
Division of Water Quality
NC Department of Environment & Natural Resources
1628 Mail Service Center
Raleigh, North Carolina 27699-1628
Subject: Notification of recording device malfunction
Performance Fibers, Inc., New Hill, NC
NPDES Permit No. NC0001899
Dear Ms. Garrett:
This letter is a follow up to confirm our telephone conversation on April 4, 2006 regarding a loss of
function of recording devices in our wastewater treatment plant operation. On April 3, 2006 a severe
thunderstorm resulted in lightning that disabled our influent flow recording device as well as our influent
and effluent pH chart recording devices. Repair has been initiated for these devices with an expected
completion within 2 weeks.
Influent and Effluent pH continuous monitoring was not affected by the chart recording device being
down, as the actual pH measurement device showing the continuous pH units continues to function, which
thereby allows Performance Fibers to monitor and make any changes necessary to keep pH within
permitted limits. As discussed, this exception will also be reported with the next monthly Discharge
Monitoring Report.
If you have any questions regarding this notification, please contact me at [phone].
Sincerely,
n 4
Charles E. Powell, Jr,REM�1
Environmental Engineer
cc: B. Ferree
D. Peterson
G. Gardner
S. Mann/L. Murray ORC
138 PEA RIDGE ROAD I NEW HILL, NC 2-i62 I TEL [phone]D
u, , ,r pe,/o ,,, an,, f, be, s. c om

FaceAnalytical
www. pacelabs. corn
March 08. 2006
Mr. Chuck Powell
Performance Fibers
338 Pea Ridge Road
New Hill, NC 27562
RE: Lab Project Number: 92112133
Client Project ID: Outfall 001
Dear Mr. Powell:
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
704.875.9092
Copy Phone:fax: [phone]
Resu/Inm�ltted Data
-¢rof yAv e-t- b )
Enclosed are the analytical results for sample(s) received by the laboratory on January 25. 2006. Results
reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the
body of the report.
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic testing
was performed at our Pace Charlotte laboratory unless otherwise footnoted.
If you have any questions concerning this report please feel free to contact me.
Sincerely,
Kate Knauff
[e-mail]
Project Manager
Enclosures
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
�n eb
RECEIVED
H S E Dept
PFI
harlott Certification IDs
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

t
�PaceAnalytical"
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite too
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Lab Sample No: 926579269
Project Sample
Number: 92112133.001
Date Collected: 01/24/06 14:25
Client Sample ID: OUTFALL 001 COMP
Matrix: Water
Date Received: 01/25/06 17:00
Parameters Results
Units Report Limit
OF Analyzed
By CAS No. Qual ReaLmt
Client Services
Total Organic Nitrogen Method:
Total Organic Nitrogen 0.57
mg/l 0.10
1.0 01/30/06
WWB
Metals
Trace ICP Metals
Prep/Method:
/ EPA 200.7
Aluminum
0.18
mg/l
0.10
1.0
01/27/06
17:38
SAJ
7429-90-5
Antimony
0.019
mg/l
0.0050
1.0
01/27/06
17:38
SAJ
7440-36-0
Arsenic
NO
mg/l
0.0050
1.0
01/27/06
17:38
SAJ
7440-38-2
Barium
0.017
mg/l
0.0050
1.0
01/27/06
17:38
SAJ
7440.39-3
Beryllium
NO
mg/l
0.0010
1.0
01/27/06
17:38
SAJ
7440-41-7
Boron
0.14
mg/l
0.010
1.0
01/27/06
17:38
SAJ
7440-42-8
Cadmium
NO
m9/1
0.0010
1.0
01/27/06
17:38
SAJ
7440-43-9
Chromium
NO
mg/l
0.0020
1.0
01/27/06
17:38
SAJ
7440.47-3
Copper
0.022
mg/1
0.0020
1.0
01/27/06
17:38
SAJ
7440-50-8
Iron
0.11
mg/1
0.050
1.0
01/27/06
17:38
SAJ
7439-89-6
Lead
NO
mg/l
0.0050
1.0
01/27/06
17:38
SAJ
7439-92-1
Magnesium
7.5
mg/l
0.10
1.0
01/27/06
17:38
SAJ
7439-95-4
Manganese
0.12
mg/l
0.0050
1.0
01/27/06
17:38
SAJ
7439-96-5
Molybdenum
0.014
mg/1
0.0050
1.0
01/27/06
17:38
SAJ
7439.98-7
Nickel
0.078
mg/1
0.0050
1.0
01/27/06
17:38
SAJ
7440-02-0
Selenium
NO
mg/l
0.0050
1.0
01/27/06
17:38
SAJ
7782-49-2
Silver
NO
mg/1
0.0020
1.0
01/27/06
17:38
SAJ
7440-22-4
Thallium
NO
mg/l
0.010
1.0
01/27/06
17:38
SAJ
7440.28-0
Zinc
0.63
mg/1
0.010
1.0
01/27/06
17:38
SAJ
7440-66.6
Date Digested
01/26/06 15:30
01/26/06
15:30
Mercury, CVAAS. in Water
Method:
EPA
7470
Mercury
ND
mg/1
0.00020
1.0
01/26/06
10:48
ALV
7439-97-6
Wet Chemistry
Cyanide, Total. Water
Method:
EPA
335.2
Cyanide
ND
mg/l
0.0050
1.0
02/01/06
13:30
BMF
57-12-5
Fluoride
Method:
EPA
340.2
Fluoride
0.32
mg/l
0.10
1.0
01/26/06
09:35
TMR
16984-48.8
Ammonia
Method:
EPA
350.1
Nitrogen. Ammonia
NO
mg/l
0.10
1.0
01/28/06
14:23
ARM
7727-37-9
Date: 03/08/06
RECENED 32
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
-ol IGk
HSECDept
'ham]RrCIrtification IDs
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

.FaceAnalytical
www.pacelabs.com
Lab Sample No: 926579269
Client Sample I0: OUTFALL 001 COMP
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax., 704.875.9091
Lab Project Number: 92112133
Client Project ID: Outfall 001
Project Sample Number: 92112133-001 Date Collected: 01/24/06 14:25
Matrix: Water Date Received: 01/25/06 17:00
Parameters
Results
Units
Report Limit
OF
_ Analyzed
By CAS No. Qual RegLmt
Total Kjeldahl Nitrogen
Method:
EPA
351.2
Nitrogen, Kjeldahl, Total
0.65
mg/l
0.50
1.0
01/26/06
22:40
ARM
28 day NOX
Method:
EPA
353.2
Nitrate -Nitrite (as N)
2.0
mg/l
0.10
1.0
01/26/06
21:00
CD1 7727-37-9
Sulfate.Turbidimetric
Method:
EPA
375.4
Sulfate
110
mg/l
25.
5.0
01/26/06
18:34
ARM
Chemical Oxygen Demand
Method:
EPA
410.4
Chemical Oxygen Demand
93.
mg/l
25.
1.0
01/27/06
07:45
TMR
Phenolics. Total Recoverable
Method:
EPA
420.2
Phenolics. Total Recoverable
0.011
mg/l
0.010
1.0
02/01/06
16:40
EWS
Total Organic Carbon
Method:
SM 53108
Total Organic Carbon
14.
mg/l
1.0
1.0
01/30/06
07:30
BMF 7440-44-0
GUMS Semivolatiles
Extractables in Water by 625
Benzidine
Benzo(g.h.i)perylene
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
4-Chlorophenylphenyl ether
Chrysene
3,3'-Dichlorobenzidine
Di-n-octylphthalate
1.2-Diphenylhydrazine
Hexachlorocyclopentadiene
Isophorone
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Date: 03/08/O6
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
Prep/Method:
EPA 625 SF / EPA 625
NO
ug/l
200
ND
ug/l
20.
NO
ug/l
20.
NO
ug/l
20.
ND
ug/l
20.
ND
ug/i
20.
NO
ug/l
20.
NO
ug/1
20.
NO
ug/l
20.
NO
ug/l
20.
NO
ug/l
20.
NO
ug/l
40.
NO
ug/l
20.
NO
ug/l
20.
NO
ug/l
40.
NO
ug/l
20.
NO
ug/l
20.
NO
ug/l
20.
NO
ug/l
20.
4.0 02/03/06 00:12 BET
4.0 02/03/06 00:12 BET
4.0 02/03/06 00:12 BET
4.0 02/03/06 00:12 BET
4.0 02/03/06 00:12 BET
4.0 02/03/06 00:12 BET
4.0 02/03/06 00:12 BET
4.0 02/03/06 00:12 BET
4.0 02/03/06 00:12 BET
4.0 02/03/06 00:12 BET
4.0 02/03/06 00:12 BET
4.0 02/03/06 00:12 BET
4.0 02/03/06 00:12 BET
4.0 02/03/06 00:12 BET
4.0 02/03/06 00:12 BET
4.0 02/03/06 00:12 BET
4.0 02/03/06 00:12 BET
4.0 02/03/06 00:12 BET
4.0 02/03/06 00:12 BET
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
nmV Cpq�■,^^ x
92-87-5
191-24-2
101.55-3
85-68-7
59-50-7
111-91-1
111-44-4
39638-32-9
91.58-7
7005-72-3
218-01-9
91.94-1
117-84-0
122-66-7
77-47.4
78-59-1
62-75-9
621-64-7
86-30-6
RFQEI of F
H S E Dept
PFI
aralottte Certification ID
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

t c�
---.PaceAnalytical"
www. pacelabs. corn
Lab Sample No: 926579269
Client Sample ID: OUTFALL 001 COMP
Pace Analytical Services, Inc.
9800 Kincey Avenue, Sute 100
Huntersville, NO 28078
Phone., 704,675.9092
Fax: [phone]
Lab Project Number: 92112133
Client Project I0: Outfall 001
Project Sample Number: 92112133-001 Date Collected: 01/24/06 14:25
Matrix: Water Date Received: 01/25/06 17:00
Parameters
Results
Units
Report Limit
OF
Analyzed
By
CAS No. Qual ReaLmt
Pentachlorophenol
NO
ug/l
100
4.0
02/03/06
00:12
BET
87.86-5
Phenanthrene
NO
ug/l
20.
4.0
02/03/06
00:12
BET
85-01-8
Pyrene
NO
ug/l
20.
4.0
02/03/06
00:12
BET
129-00.0
1.2.4-Trichlorobenzene
ND
ug/l
20.
4.0
02/03/06
00:12
BET
120-82-1
2.4,6-Trichlorophenol
NO
ug/l
20.
4.0
02/03/06
00:12
BET
88-06-2
Nitrobenzene-d5 (S)
52
X
1.0
02/03/06
00:12
BET
4165-60-0
2-Fluorobiphenyl (S)
72
%
1.0
02/03/06
00:12
BET
321-60-8
Terphenyl-d14 (S)
80
%
1.0
02/03/06
00:12
BET
1718-51-0
Phenol-d5 (S)
29
%
1.0
02/03/06
00:12
BET
4165-62-2
2-Fluorophenol (S)
39
%
1.0
02/03/06
00:12
BET
367-12-4
2,4,6-Tribromophenol (S)
97
%
1.0
02/03/06
00:12
BET
118-79-6
Date Extracted
01/31/06
01/31/06
GC Semivolatiles
Organochlorine Pesticides
Prep/Method:
EPA 3535 /
EPA 8081
Aldrin
NO
ug/l
0.050
1.0
01/30/06
21:56
JEM
309-00-2
alpha-BHC
NO
ug/l
0.050
1.0
01/30/06
21:56
JEM
319-84-6
beta-BHC
NO
ug/l
0.050
1.0
01/30/06
21:56
JEM
319-85-7
delta-BHC
NO
ug/l
0.10
1.0
01/30/06
21:56
JEM
319-86-8
gamma-BHC (Lindane)
NO
ug/l
0.050
1.0
01/30/06
21:56
JEM
58-89-9
Chlordane
NO
ug/l
0.50
1.0
01/30/06
21:56
JEM
57.74-9
4,4'-DDD
NO
ug/l
0.10
1.0
01/30/06
21:56
JEM
72-54-8
4.4'-DDE
NO
ug/l
0.10
1.0
01/30/06
21:56
JEM
72-55.9
4.4'-DDT
NO
ug/l
0.10
1.0
01/30/06
21:56
JEM
50-29-3
Oieldrin
ND
ug/l
0.10
1.0
01/30/06
21:56
JEM
60-57-1
Endosulfan I
NO
ug/l
0.10
1.0
01/30/06
21:56
JEM
959-98-8
Endosulfan II
NO
ug/l
0.10
1.0
01/30/06
21:56
JEM
33213-65-9
Endosulfan sulfate
NO
ug/l
0.10
1.0
01/30/06
21:56
JEM
1031-07-8
Endrin
No
ug/l
0.060
1.0
01/30/06
21:56
JEM
72-20.8
Endrin aldehyde
NO
ug/l
0.10
1.0
01/30/06
21:56
JEM
7421-93-4
Heptachlor
NO
ug/l
0.050
1.0
01/30/06
21:56
JEM
76-44-8
Heptachlor epoxide
NO
ug/1
0.80
1.0
01/30/06
21:56
JEM
1024-57-3
Toxaphene
NO
ug/l
1.0
1.0
01/30/06
21:56
JEM
8001-35-2
Tetrachloro-m-xylene (S)
50
X
1.0
01/30/06
21:56
JEM
877-09-8
Decachlorobiphenyl (S)
38
X
1.0
01/30/06
21:56
JEM
2051-24-3
Date Extracted
01/26/06
01/26/06
Organochlorine PCBs
Prep/Method:
EPA 3535 /
EPA 8082
PCB-1016 (Aroclor 1016)
NO
ug/l
1.0
1.0
01/30/06
21:56
JEM
12674-11.2
Date: 03/08/06
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
C I -Mc pqe\/'z
RE vff`
Ch rld § ' ws
NC Wastew 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

a
t
FaceAnalytical"
www.pacelabs.com
Lab Sample No: 926579269
Client Sample ID: OUTFALL 001 COMP
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 26078
Phone: [phone]
Fax., 704.875.9091
Lab Project Number: 92112133
Client Project ID: Outfall 001
Project Sample Number: 92112133.001 Date Collected: 01/24/06 14:25
Matrix: Water Date Received: 01/25/06 17:00
Parameters
Results
Units
Report Limit
OF
Analyzed
By
CAS No. Qual ReaLmt
PCB-1221 (Aroclor 1221)
NO
ug/l
1.0
1.0
01/30/06
21:56
JEM
11104.28-2
PCB-1232 (Aroclor 1232)
ND
ug/l
1.0
1.0
01/30/06
21:56
JEM
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/l
1.0
1.0
01/30/06
21:56
JEM
53469-21-9
PCB-1248 (Aroclor 1248)
NO
ug/l
1.0
1.0
01/30/06
21:56
JEM
12672-29-6
PCB-1254 (Aroclor 1254)
NO
ug/l
1.0
1.0
01/30/06
21:56
JEM
11097-69-1
PCB-1260 (Aroclor 1260)
NO
ug/l
1.0
1.0
01/30/06
21:56
JEM
11096-82-5
Decachlorobiphenyl (S)
38
X
1.0
01/30/06
21:56
JEM
2051-24.3
Date Extracted
01/26/06
01/26/06
GUMS Volatiles
Volatile GUMS by 624
Method: EPA
624
Acrolein
ND
ug/l
25.
1.0
02/01/06
11:29
DLK
107-02-8
Bromodichloromethane
ND
ug/l
5.0
1.0
02/01/06
11:29
DLK
75.27-4
Bromoform
NO
ug/l
5.0
1.0
02/01/06
11:29
DLK
75-25-2
Bromomethane
NO
ug/l
5.0
1.0
02/01/06
11:29
DLK
74-83-9
2-Chloroethylvinyl ether
NO
ug/l
10.
1.0
02/01/06
11:29
DLK
110-75-8
Dibromochloromethane
NO
ug/l
5.0
1.0
02/01/06
11:29
DLK
124-48.1
Dichlorodifluoromethane
ND
ug/l
5.0
1.0
02/01/06
11:29
DLK
75-71-8
1,1,1,2-Tetrachloroethane
ND
ug/l
5.0
1.0
02/01/06
11:29
DLK
630.20.6
1,1,2.2-Tetrachloroethane
ND
ug/l
5.0
1.0
02/01/06
11:29
DLK
79.34-5
Trichlorofluoromethane
ND
ug/l
5.0
1.0
02/01/06
11:29
DLK
75.69-4
Toluene-d8 (S)
94
X
1.0
02/01/06
11:29
DLK
2037-26.5
4-Bromofluorobenzene (S)
105
%
1.0
02/01/06
11:29
DLK
460-00.4
Dibromofluoromethane (S)
99
X
1.0
02/01/06
11:29
DLK
1868-53-7
RECEIVED
Date: 03/08/06
Page:
1 of 32
HSEUepi
PEI
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDS
This report shall not be reproduced, except in full,
Charlotte Certification
IDs
NC Wastewater 40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water 37712
NC Drinking Water
37706
SC Environmental 99030
SC
99006
FL NELAP E87648
n&&
FL NELAP
E87627

r c
�PaceAnalytical"
www.pacelabs.com
Lab Sample No: 926579277
Client Sample ID: OUTFALL 001 GRAB
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone:[phone]
Fax: 704.875,9091
Lab Project Number: 92112133
Client Project ID: Outfall 001
Project Sample Number: 92112133-002 Date Collected: 01/24/06 14:25
Matrix: Water Date Received: 01/25/06 17:00
Parameters
Results
Units Report Limit DF Analyzed
By CAS No. Qual ReaLmt
Field Services
Field Grab Data
Method:
Collected By
AGN
01/27/06
KAK
Collected Date
1/24/06
Dl/27/06
KAK
Collected Time
14:25
01/27/06
KAK
Field pH
6.83
01/27/06
KAK
Field Temperature
13.9
01/27/06
KAK
Date: 03/08/06
RECEIVEn
H S E Dept
PPI
REPORT OF LABORATORY ANALYSIS
Asheville Certification IN This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712 «o,o
SC Environmental 99030 1
Page: 5 of 32
Chv�e Certification ID
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627
FL NELAP E87648

,G
(�PaceAnalyfical'T
www.pacelabs.com
PARAMETER FOOTNOTES
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax., 704.875.9091
Lab Project Number: 92112133
Client Project ID: Outfall 001
Dilution factor shown represents the factor applied to the reported result and reporting limit due to changes
in sample preparation, dilution of the extract, or moisture content
Method 90718 modified to use ASE.
All pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate
hold time.
Depending on the moisture content the PRLs can be elevated for all soil samples reported on a dry weight basis.
2-Chloroethyl vinyl ether has been shown to degrade in the presence of acid.
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MOL Adjusted Method Detection Limit
(S) Surrogate
RECEIVED
Date: 03/08/06 HSEClap Page: 6 of 32
PH
REPORT OF LABORATORY ANALYSIS
Asheville Certification
IDs
This report shall not be reproduced, except in full,
Charlotte Certification
IN
NC Wastewater
40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water
37712
«,o,
NC Drinking Water
37706
SC Environmental
99030
Sc
99006
FL NELAP
E87648
5r1mc.
FL NELAP
E87627

I
FaceAnalytical
www.pac6labs.com
QC Batch: 148314
QC Batch Method: EPA 3535
Associated Lab Samples: 926579269
METHOD BLANK: 926586496
Associated Lab Samples: 926579269
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 8081
Analysis Description: Organochlorine Pesticides
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Aldrin
ug/l
NO
0.050
alpha-BHC
ug/l
ND
0.050
beta-BHC
ug/l
NO
0.050
delta-BHC
ug/l
NO
0.10
gamma-BHC (Lindane)
ug/l
NO
0.050
Chlordane
ug/l
NO
0.50
4.4'-DDD
ug/l
NO
0.10
4,4'-DDE
ug/l
NO
0.10
4.4'-DDT
ug/l
NO
0.10
Dieldrin
ug/l
NO
0.10
Endosulfan I
ug/l
N0
0.10
Endosulfan II
ug/l
NO
0.10
Endosulfan sulfate
ug/l
NO
0.10
Endrin
ug/1
ND
0.060
Endrin aldehyde
ug/l
ND
0.10
Heptachlor
ug/l
NO
0.050
Heptachlor epoxide
ug/l
ND
0.80
Toxaphene
ug/l
NO
1.0
Tetrachloro-m-xylene (S)
%
78
Decachlorobiphenyl (S)
X
82
LABORATORY CONTROL SAMPLE: 926586504
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec Footnotes
alpha-BHC
ug/l
0.1600
0.1099
69
gamma-BHC (Lindane)
ug/l
0.1600
0.1093
68
beta-BHC
ug/l
0.1600
0.1345
84
Heptachlor
ug/l
0.1600
0.1036
65
delta-BHC
ug/l
0.1600
0.1555
97
Date: 03/08/06
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
RECEIVED
HSEDept
FFI
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
`nelac
Page: 7 of 32
harlotte Certification
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Analytical Kl
www.pacelabs.com QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE: 926586504
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec
Aldrin
ug/l
0.1600
0.0838
52
Heptachlor epoxide
ug/l
0.1600
0.1195
75
Endosulfan I
ug/l
0.1600
0.1350
84
4,4'-DDE
ug/l
0.1600
0.1447
90
Dieldrin
ug/l
0.1600
0.1190
74
Endrin
ug/l
0.1600
0.1344
84
4.4'-DDD
ug/l
0.1600
0.1462
91
Endosulfan II
ug/l
0.1600
0.1209
76
4.4'-DDT
ug/l
0.1600
0.1486
93
Endrin aldehyde
ug/l
0.1600
0.1713
107
Endosulfan sulfate
ug/l
0.1600
0.1127
70
Decachlorobiphenyl (S)
66
Tetrachloro-m-xylene (S)
68
LABORATORY CONTROL SAMPLE: 926597139
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec
alpha-BHC
ug/l
0.1600
0.1099
69
gamma-BHC (Lindane)
ug/l
0.1600
0.1093
68
beta-BHC
ug/l
0.1600
0.1345
84
Heptachlor
ug/l
0.1600
0.1036
65
delta-BHC
ug/l
0.1600
0.1555
97
Aldrin
ug/l
0.1600
0.0838
52
Heptachlor epoxide
ug/l
0.1600
0.1195
75
Endosulfan I
ug/l
0.1600
0.1350
84
4,4'-DDE
ug/l
0.1600
0.1447
90
Dieldrin
ug/l
0.1600
0.1190
74
Endrin
ug/l
0.1600
0.1344
84
4.4'-DDD
ug/l
0.1600
0.1462
91
Endosulfan II
ug/l
0.1600
0.1209
76
4,4'-ODT
ug/l
0.1600
0.1486
93
Endrin aldehyde
ug/l
0.1600
0.1713
107
Endosulfan sulfate
ug/l
0.1600
0.1127
70
Decachlorobiphenyl (S)
66
Tetrachloro-m-xylene (S)
68
Date: 03/08/06
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Footnotes
Footnotes
RECEIVED
H S E Dept
PFI
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
10 „CC1.,.
-' ek.
Page: 8 of 32
Charlotte Certification ID
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

I"
(---.PaceAna1yfica1"?J
www. pacelabs. coin
LABORATORY CONTROL SAMPLE: 926617820
QUALITY CONTROL DATA
Spike
-CS
LCS
Parameter
Units
Conc.
Result
X Rec
alpha-BHC
ug/l
0.1600
0.0865
54
gamma-BHC (Lindane)
ug/l
0.1600
0.0876
55
beta-BHC
ug/l
0.1600
0.1087
68
Heptachlor
ug/l
0.1600
0.0991
62
delta-BHC
ug/l
0.1600
0.0854
53
Aldrin
ug/l
0.1600
0.0848
53
Heptachlor epoxide
ug/l
0.1600
0.0949
59
Endosulfan I
ug/l
0.1600
0.1165
73
4.4'-DDE
ug/l
0.1600
0.1061
66
Dieldrin
ug/l
0.1600
0.0936
58
Endrin
ug/l
0.1600
0.0958
60
4.4'-DDD
ug/l
0.1600
0.0949
59
Endosulfan II
ug/l
0.1600
0.1022
64
4.4'-DDT
ug/1
0.1600
0.1001
63
Endrin aldehyde
ug/l
0.1600
0.0960
60
Endosulfan sulfate
ug/l
0.1600
0.0983
61
Decachlorobiphenyl (S)
42
Tetrachloro-m-xylene (S)
39
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 926586512 926586520
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Footnotes
926578980
Spike
MS
MSD
MS
MSD
Parameter
Units
Result
Conc.
Result
Result %
Rec %
Rec
RPD Footnotes
gamma-BHC (Lindane)
ug/1
0
0.1600
0.1224
0.1097
76
69
11
Heptachlor
ug/l
0
0.1600
0.1283
0.1256
80
78
2
Aldrin
ug/l
0
0.1600
0.0966
0.0975
60
61
1
Dieldrin
ug/1
0
0.1600
0.1160
0.1110
72
69
4
Endrin
ug/1
0
0.1600
0.1658
0.1651
104
103
0
4.4'-DDT
ug/l
0
0.1600
0.1458
0.1646
91
103
12
Decachlorobiphenyl (S)
75
81
Tetrachloro-m-xylene (S)
74
81
RECEIVED
Date: 03/08/06 Page: 9 of 32
HSEDepi
PH
REPORT OF LABORATORY ANALYSIS
Asheville Certification
IDs
This report shall not be reproduced, except in full,
Charlotte Certification
IDs
NC Wastewater
40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water
37712
^
NC Drinking Water
37706
SC Environmental
99030
M
Sc
99006
FL NELAP
E87648
: I ebel
FL NELAP
E87627

I
FaceAnalyical
www.pace/abs.com
QC Batch: 148315
QC Batch Method: EPA 3535
Associated Lab Samples: 926579269
METHOD BLANK: 926586538
Associated Lab Samples: 926579269
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 8082
Analysis Description: Organochlorine PCBs
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
PCB-1016 (Aroclor
1016)
ug/l
NO
1.0
PCB-1221 (Aroclor
1221)
ug/l
NO
1.0
PCB-1232 (Aroclor
1232)
ug/l
NO
1.0
PCB -1242 (Aroclor
1242)
ug/l
NO
1.0
PCB-1248 (Aroclor
1248)
ug/l
NO
1.0
PCB-1254 (Aroclor
1254)
ug/1
NO
1.0
PCB-1260 (Aroclor
1260)
ug/l
NO
1.0
Decachlorobiphenyl
(S)
X
82
LABORATORY CONTROL SAMPLE: 926586546
Parameter
PCB-1016 (Aroclor 1016)
PCB-1260 (Aroclor 1260)
Decachlorobiphenyl (S)
Date: 03/08/06
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
Spike LCS
Units Conc. Result
ug/l 10.00 10.50
ug/l 10.00 8.344
LCS
X Rec Footnotes
105
83
64
RECEIVED
H S E Dept
PFI
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
.. �11,
el'i
Page: 30 of 32
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Face Analytical
www.pacelabs.com
QC Batch: 147755
QC Batch Method: EPA 625 SF
Associated Lab Samples: 926579269
METHOD BLANK: 926596339
Associated Lab Samples: 926579269
QUALITY CONTROL DATA
Pace Analytical Services, Inc,
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 625
Analysis Description: Extractables in Water by 625
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Benzidine
ug/l
NO
50.
Benzo(g.h.i)perylene
ug/l
NO
5.0
4-Bromophenylphenyl ether
ug/l
NO
5.0
Butylbenzylphthalate
ug/1
NO
5.0
4-Chloro-3-methylphenol
ug/l
NO
5.0
bis(2-Chloroethoxy)methane
ug/l
NO
5.0
bis(2-Chloroethyl) ether
ug/l
NO
5.0
bis(2-Chloroisopropyl) ether
ug/l
NO
5.0
2-Chloronaphthalene
ug/l
NO
5.0
4-Chlorophenylphenyl ether
ug/l
NO
5.0
Chrysene
ug/l
NO
5.0
3.3'-Dichlorobenzidine
ug/l
NO
10.
Di-n-octylphthalate
ug/l
NO
5.0
1,2-Diphenylhydrazine
ug/l
NO
5.0
Hexachlorocyclopentadiene
ug/l
NO
10.
Isophorone
ug/l
NO
5.0
N-Nitrosodimethylamine
ug/l
NO
5.0
N-Nitroso-di-n-propylamine
ug/l
NO
5.0
N-Nitrosodiphenylamine
ug/l
NO
5.0
Pentachlorophenol
ug/l
NO
25.
Phenanthrene
ug/l
NO
5.0
Pyrene
ug/l
NO
5.0
1.2,4-Trichlorobenzene
ug/l
NO
5.0
2.4.6-Trichlorophenol
ug/l
NO
5.0
Nitrobenzene-d5 (S)
%
54
2-Fluorobiphenyl (S)
%
69
Terphenyl-d14 (S)
%
82
Phenol-d5 (5)
%
27
2-Fluorophenol (S)
%
13
2.4.6-Tribromophenol (S)
%
14
1
Date: 03/08/06
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
RECEIVE®
HSEDept
FFB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
�nelac
Page: 11 of 32
Charlotte Certification ID
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Analytical
www.pacelabs.com QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE: 926561416
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec
Benzidine
ug/l
100.00
26.49
26
Benzo(g,h,i)perylene
ug/l
50.00
36.94
74
4-Bromophenylphenyl ether
ug/l
50.00
35.40
71
Butylbenzylphthalate
ug/1
50.00
38.10
76
4-Chloro-3-methylphenol
ug/l
50.00
36.01
72
bis(2-Chloroethoxy)methane
ug/l
50.00
36.20
72
bis(2-Chloroethyl) ether
ug/l
50.00
37.37
75
bis(2-Chloroisopropyl) ether
ug/l
50.00
34.44
69
2-Chloronaphthalene
ug/l
50.00
39.07
78
4-Chlorophenylphenyl ether
ug/l
50.00
35.76
72
Chrysene
ug/l
50.00
36.65
73
3.3'-Dichlorobenzidine
ug/l
100.00
41.97
42
Di-n-octylphthalate
ug/l
50.00
37.50
75
Hexachlorocyclopentadiene
ug/l
50.00
20.43
41
Isophorone
ug/l
50.00
37.71
75
N-Nitrosodimethylamine
ug/l
50.00
23.74
48
N-Nitroso-di-n-propylamine
ug/l
50.00
36.60
73
N-Nitrosodiphenylamine
ug/l
100.00
104.5
104
Pentachlorophenol
ug/l
50.00
31.24
62
Phenanthrene
ug/1
50.00
36.78
74
Pyrene
ug/1
50.00
37.13
74
1,2.4-Trichlorobenzene
ug/l
50.00
31.19
62
2.4.6-Trichlorophenol
ug/1
50.00
37.05
74
Nitrobenzene-d5 (S)
74
2-Fluorobiphenyl (S)
74
Terphenyl-d14 (S)
79
Phenol-d5 (S)
33
2-Fluorophenol (S)
51
2.4.6-Tribromophenol (S)
85
LABORATORY CONTROL SAMPLE: 926571258
Parameter
Benzidine
Benzo(g,h,i)perylene
Date: 03/08/06
Asheville Certification IDs
NO Wastewater 40
NO Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Spike LCS LCS
Units Conc. Result X Rec
ug/l 100.00 0 0
ug/l 50.00 35.19 70
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone., 704.875.9092
Fax. [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Footnotes
Footnotes
2
RECEIVED
HSEDepp
IP9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent ofPaceAnalytical Services, Inc.
en
1 elk
Page: 12 of 32
Charlotte Certification IDs
NO Wastewater
12
NO Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical
www.pacelabs.com
LABORATORY CONTROL SAMPLE: 926571258
QUALITY CONTROL DATA
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec
4-Bromophenylphenyl ether
ug/l
50.00
31.56
63
Butylbenzylphthalate
ug/l
50.00
33.91
68
4-Chloro-3-methylphenol
ug/l
50.00
32.66
65
bis(2-Chloroethoxy)methane
ug/l
50.00
29.63
59
bis(2-Chloroethyl) ether
ug/l
50.00
26.11
52
bis(2-Chloroisopropyl) ether
ug/l
50.00
25.16
50
2-Chloronaphthalene
ug/l
50.00
26.83
54
4-Chlorophenylphenyl ether
ug/l
50.00
30.77
62
Chrysene
ug/l
50.00
31.62
63
3.3'-Dichlorobenzidine
ug/l
100.00
31.61
32
Di-n-octylphthalate
ug/l
50.00
33.04
66
Hexachlorocyclopentadiene
ug/l
50.00
19.18
38
Isophorone
ug/l
50.00
30.26
60
N-Nitrosodimethylamine
ug/l
50.00
18.16
36
N-Nitroso-di-n-propylamine
ug/l
50.00
28.99
58
N-Nitrosodiphenylamine
ug/l
50.00
40.45
81
Pentachlorophenol
ug/l
50.00
33.94
68
Phenanthrene
ug/l
50.00
31.19
62
Pyrene
ug/l
50.00
31.23
62
1.2.4-Trichlorobenzene
ug/l
50.00
23.52
47
2,4.6-Trichlorophenol
ug/l
50.00
30.74
62
Nitrobenzene-d5 (S)
53
2-Fluorobiphenyl (S)
55
Terphenyl-d14 (S)
64
Phenol-d5 (S)
23
2-Fluorophenol (S)
35
2.4,6-Tribromophenol (S)
74
LABORATORY CONTROL SAMPLE: 926574732
Parameter
Benzidine
Benzo(g.h,i)perylene
4-Bromophenylphenyl ether
Butylbenzylphthalate
Date: 03/08/06
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
Spike LCS
Units Conc. Result
ug/l 100.00 3.988
ug/l 50.00 49.37
ug/l 50.00 36.38
ug/1 50.00 36.97
Pace Analytical Services, Inc.
98001(incey/lvenue, Suite 100
Huntersville, PIC 28078
Phone., 704.875.9092
Fax., 704.875.9091
Lab Project Number: 92112133
Client Project ID: Outfall 001
Footnotes
2
LCS
% Rec Footnotes
4 2
99
73
74 RECEIVED
HSEDepi
PFI
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
o4.
Page: 13 of 32
harlotte Certification ID
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

-Face Analytical
www. pacelabs. corn
LABORATORY CONTROL SAMPLE: 926574732
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax., 704.875.9091
Lab Project Number: 92112133
Client Project ID: Outfall 001
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec Footnotes
4-Chloro-3-methylphenol
ug/l
50.00
39.28
79
bis(2-Chloroethoxy)methane
ug/l
50.00
37.96
76
bis(2-Chloroethyl) ether
ug/l
50.00
34.95
70
bis(2-Chloroisopropyl) ether
ug/l
50.00
36.19
72 '
2-Chloronaphthalene
ug/l
50.00
33.98
68
4-Chlorophenylphenyl ether
ug/l
50.00
38.27
76
Chrysene
ug/l
50.00
36.35
73
3,3'-Dichlorobenzidine
ug/l
100.00
35.40
35
Di-n-octylphthalate
ug/l
50.00
37.57
75
Hexachlorocyclopentadiene
ug/l
50.00
25.87
52
Isophorone
ug/l
50.00
37.93
76
N-Nitrosodimethylamine
ug/l
50.00
23.54
47
N-Nitroso-di-n-propylamine
ug/1
50.00
38.40
77
N-Nitrosodiphenylamine
ug/l
50.00
45.31
91
Pentachlorophenol
ug/l
50.00
38.65
77
Phenanthrene
ug/l
50.00
36.60
73
Pyrene
ug/l
50.00
34.45
69
1.2.4-Trichlorobenzene
ug/l
50.00
32.33
65
2,4,6-Trichlorophenol
ug/l
50.00
37.13
74
Nitrobenzene-d5 (S)
74
2-Fluorobiphenyl (S)
72
Terphenyl-d14 (S)
74
Phenol-d5 (S)
31
2-Fluorophenol (S)
47
2.4.6-Tribromophenol (S)
84
LABORATORY CONTROL SAMPLE: 926596347
Spike
LCS LCS
Parameter
Units Conc.
Result X Rec Footnotes
Benzidine
ug/l
100.00
65.36 65
eenzo(g,h.i)perylene
ug/l
50.00
36.91 74
4-Bromophenylphenyl ether
ug/l
50.00
43.90 88
Butylbenzylphthalate
ug/l
50.00
37.11 74
4-Chloro-3-methylphenol
ug/l
50.00
36.62 73
bis(2-Chloroethoxy)methane
ug/l
50.00
36.66 73
RECEIVED
Date: 03/08/06
Page: 14
of 32
HSEDePt
99
REPORT OF
LABORATORY ANALYSIS
Asheville Certification Ills
This report shall not be reproduced, except in full,
Charlotte Certification
IDs
NC Wastewater 40
without the written
consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water 37712
_,,
NC Drinking Water
37706
SC Environmental 99030
SC
99006
FL NELAP E87648
t
FL NELAP
E87627

I
Face Analytical("
www.pacelabs.com
LABORATORY CONTROL SAMPLE: 926596347
QUALITY CONTROL DATA
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec
bis(2-Chloroethyl) ether
ug/l
50.00
13.09
26
bis(2-Chloroisopropyl) ether
ug/l
50.00
33.69
67
2-Chloronaphthalene
ug/1
50.00
43.79
88
4-Chlorophenylphenyl ether
ug/1
50.00
41.59
83
Chrysene
ug/l
50.00
41.84
84
3.3'-Dichlorobenzidine
ug/l
100.00
50.93
51
Di-n-octylphthalate
ug/l
50.00
35.66
71
Hexachlorocyclopentadiene
ug/l
50.00
21.87
44
Isophorone
ug/l
50.00
37.95
76
N-Nitrosodimethylamine
ug/l
50.00
23.05
46
N-Nitroso-di-n-propylamine
ug/l
50.00
33.22
66
N-Nitrosodiphenylamine
ug/l
100.00
98.19
98
Pentachlorophenol
ug/l
50.00
20.15
40
Phenanthrene
ug/l
50.00
42.38
85
Pyrene
ug/l
50.00
42.18
84
1.2,4-Trichlorobenzene
ug/l
50.00
33.06
66
2.4.6-Trichlorophenol
ug/l
50.00
12.08
24
Nitrobenzene-d5 (S)
68
2-Fluorobiphenyl (S)
80
Terphenyl-d14 (S)
84
Phenol-d5 (S)
33
2-Fluorophenol (S)
43
2.4,6-Tribromophenol (S)
38
LABORATORY CONTROL SAMPLE: 926607029
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite too
Huntersville, NC 28078
Phone: [phone]
Fax [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Footnotes
2
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec Footnotes
Benzidine
ug/l
100.00
0
0 2
Benzo(g,h.i)perylene
ug/l
50.00
36.60
73
4-Bromophenylphenyl ether
ug/l
50.00
26.80
54
Butylbenzylphthalate
ug/l
50.00
26.94
54
4-Chloro-3-methylphenol
ug/l
50.00
25.60
51
bis(2-Chloroethoxy)methane
ug/l
50.00
23.23
46
bis(2-Chloroethyl) ether
ug/l
50.00
21.81
44
bis(2-Chloroisopropyl) ether
ug/l
50.00
21.60
43
RECEIVED
Date: 03/08/06
HSEDepi
0F4
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712
SC Environmental 99030 M+
FL NELAP E87648
Page: 15 of 32
had0_ttefiertification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

------ .pace Analytical `)
www. pacelabs. com
LABORATORY CONTROL SAMPLE: 926607029
QUALITY CONTROL DATA
Spike
LCS
1-CS
Parameter
Units
Conc.
Result
X Rec
2-Chloronaphthalene
ug/l
50.00
22.93
46
4-Chlorophenylphenyl ether
ug/l
50.00
25,86
52
Chrysene
ug/l
50.00
25.62
51
3.3'-Dichlorobenzidine
ug/l
100.00
7.419
7
Di-n-octylphthalate
ug/l
50.00
27.61
55
Hexachlorocyclopentadiene
ug/l
50.00
18.25
36
Isophorone
ug/l
50.00
23.89
48
N-Nitrosodimethylamine
ug/l
50.00
13.91
28
N-Nitroso-di-n-propylamine
ug/l
50.00
23.85
48
N-Nitrosodiphenylamine
ug/l
50.00
8.464
17
Pentachlorophenol
ug/l
50.00
24.55
49
Phenanthrene
ug/l
50.00
27.94
56
Pyrene
ug/l
50.00
27.36
55
1.2.4-Trichlorobenzene
ug/l
50.00
20.70
41
2.4.6-Trichlorophenol
ug/l
50.00
24.65
49
Nitrobenzene-d5 (S)
48
2-Fluorobiphenyl (S)
50
Terphenyl-d14 (S)
56
Phenol-d5 (S)
20
2-Fluorophenol (S)
31
2.4.6-Tribromophenol (S)
62
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 926571266 926571274
Parameter
Benzidine
Benzo(g,h,i)perylene
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
4-Chlorophenylphenyl ether
Date: 03/08/06
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone., 704.875.9092
Far 704.875,9091
Lab Project Number: 92112133
Client Project I0: Outfall 001
Footnotes
2
2
2
926569799
Spike
MS
MSD
MS MSD
Units
Result
Conc.
Result
Result
X Rec % Rec
RPD Footnotes
ug/l
0
200.00
0
0
0 0
0 2,2
ug/l
0
100.00
62.15
67.96
62 68
9
ug/l
0
100.00
57.31
63.03
57 63
10
ug/l
0
100.00
59.01
63.68
59 64
8
ug/l
0
100.00
60.92
70.13
61 70
14
ug/l
0
100.00
53.74
61.80
54 62
14
ug/l
0
100.00
41.64
48.25
42 48
15
ug/l
0
100.00
38.99
45.68
39 46
16
ug/l
0
100.00
50.44
53.69
50 54
6 2.2
ug/l
0
100.00
56.63
61.34
57 61
8
RECEIVED
Page: 16 of 32
HSEDept
Pip
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full, Charlotte Certification IDs
without the written consent of Pace Analytical Services, Inc. NC Wastewater 12
°, NC Drinking Water 37706
��. SC 99006
-�Ineh = FL NELAP E87627

�PaceAnalytical`
www.pacelabs.com
QUALITY CONTROL DATA
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 926571266 926571274
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
926569799
Spike
MS
MSD
MS
MSD
Parameter
Units
Result
Conc.
Result
Result
k Rec X
Rec
RPD Footnotes
Chrysene
ug/l
0
100.00
57.07
60.58
57
61
6
3.3'-Dichlorobenzidine
ug/l
0
100.00
21.07
15.35
21
15
31 3
Di-n-octylphthalate
ug/1
0
100.00
56.84
59.37
57
59
4
Hexachlorocyclopentadiene
ug/1
0
100.00
36.45
38.49
36
38
5
Isophorone
ug/l
0
100.00
53.63
61.30
54
61
13
N-Nitrosodimethylamine
ug/1
0
100.00
34.89
40.49
35
40
15
N-Nitroso-di-n-propylamine
ug/1
0
100.00
48.08
56.91
48
57
17
N-Nitrosodiphenylamine
ug/1
0
100.00
72.06
78.02
72
78
8
Pentachlorophenol
ug/1
0
100.00
63.49
75.80
64
76
18
Phenanthrene
ug/1
0
100.00
56.59
60.86
57
61
7
Pyrene
ug/1
0
100.00
55.66
61.51
56
62
10
1,2,4-Trichlorobenzene
ug/1
0
100.00
40.44
42.92
40
43
6 2.2
2,4.6-Trichlorophenol
ug/1
0
100.00
61.91
68.59
62
69
10
Nitrobenzene-d5 (S)
46
52
2-Fluorobiphenyl (S)
52
56
Terpheny1-d14 (S)
57
63
Phenol-d5 (S)
23
26
2-Fluorophenol (S)
31
36
2.4.6-Tribromophenol (S)
67
74
RECEIVED
Date: 03/08/06
Page: 17 of 32
HSEDept
PFI
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs
This report shall not be reproduced, except in full,
Charlotte Certification IDs
NC Wastewater
40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater 12
NC Drinking Water
37712
v
NC Drinking Water 37706
SC Environmental
99030
`.
SC 99006
FL NELAP
E87648
: 11C s
FL NELAP E87627

Pace Analytical"
www.pacelabs.com
QC Batch: 148560
QC Batch Method: EPA 624
Associated Lab Samples: 926579269
METHOD BLANK: 926596313
Associated Lab Samples: 926579269
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
980OKinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax., 704.875.9091
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 624
Analysis Description: Volatile GC/MS by 624
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Acrolein
ug/l
NO
25.
Bromodichloromethane
ug/l
ND
5.0
Bromoform
ug/l
ND
5.0
Bromomethane
ug/l
NO
5.0
2-Chloroethylvinyl ether
ug/l
NO
10.
Dibromochloromethane
ug/l
NO
5.0
Dichlorodifluoromethane
ug/l
NO
5.0
1.1,1,2-Tetrachloroethane
ug/l
NO
5.0
1,1,2.2-Tetrachloroethane
ug/l
NO
5.0
Trichlorofluoromethane
ug/l
NO
5.0
Toluene-d8 (S)
X
99
4-Bromofluorobenzene (S)
X
102
Dibromofluoromethane (S)
X
96
LABORATORY CONTROL SAMPLE: 926596321
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec Footnotes
Bromodichloromethane
ug/l
20.00
18.81
94
Bromoform
ug/l
20.00
18.74
94
Bromomethane
ug/l
20.00
30.84
154
2-Chloroethylvinyl ether
ug/l
20.00
25.79
129
Dibromochloromethane
ug/l
20.00
18.85
94
1,1,2,2-Tetrachloroethane
ug/l
20.00
19.53
98
Trichlorofluoromethane
ug/l
20.00
22.13
111
Toluene-d8 (S)
99
4-Bromofluorobenzene (S)
102
Dibromofluoromethane (S)
96
RECEIVE®
Date: 03/OB/06
Page: le of 32
HSEI'Dep�
PF9
REPORT OF LABORATORY ANALYSIS
Asheville Certification IN
This report shall not be reproduced, except in full,
Charlotte Certification IN
NC Wastewater
40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater 12
NC Drinking Water
37712
0,
NC Drinking Water 37706
SC Environmental
99030
�'
SC 99006
FL NELAP
E87648
"�n
FL NELAP E87627

, Face Analytical
www.pacelabs.com
0C Batch: 148154
QC Batch Method: EPA 7470
Associated Lab Samples: 926579269
METHOD BLANK: 926580051
Associated Lab Samples: 926579269
Parameter Units
Mercury mg/l
LABORATORY CONTROL SAMPLE: 926580069
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone., 704.875.9092
Fax. [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 7470
Analysis Description: Mercury, CVAAS, in Water
Blank Reporting
Result Limit Footnotes
NO 0.0002
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Mercury mg/l 0.0025 0.0027 106
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 926580077 926580085
926578980 Spike MS MSD MS MSD
Parameter Units Result Conc. Result Result % Rec % Rec RPD Footnotes
Mercury mg/l 0.00006 0.0025 0.0025 0.0025 99 99 0
Date: 03/08/06
H S E Jepii.
PFA
REPORT OF LABORATORY ANALYSIS
Asheville Certification IN This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648 "nebet
o
Page: 19 of 32
rlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

I
----.FaceAnalytical`
www.pacelabs.com
QC Batch: 148224
QC Batch Method:
Associated Lab Samples: 926579269
METHOD BLANK: 926582396
Associated Lab Samples: 926579269
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax., 704,875.9091
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 200.7
Analysis Description: Trace ICP Metals
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Aluminum
mg/l
NO
0.10
Antimony
mg/l
NO
0.0050
Arsenic
mg/l
NO
0.0050
Barium
mg/l
NO
0.0050
Beryllium
mg/l
ND
0.0010
Boron
mg/l
ND
0.010
Cadmium
mg/l
ND
0.0010
Chromium
mg/l
ND
0.0020
Copper
mg/l
ND
0.0020
Iron
mg/l
ND
0.050
Lead
mg/l
NO
0.0050
Magnesium
mg/l
NO
0.10
Manganese
mg/l
NO
0.0050
Molybdenum
mg/l
ND
0.0050
Nickel
mg/l
ND
0.0050
Selenium
mg/l
ND
0,0050
Silver
mg/l
NO
0.0020
Thallium
mg/l
NO
0.010
Zinc
mg/l
NO
0.010
LABORATORY CONTROL SAMPLE: 926582404
Spike LCS LCS
Parameter
Units Conc. Result X Rec Footnotes
Aluminum
mg/l
5.000 5.080 102
Antimony
mg/l
0.5000 0.5040 101
Arsenic
mg/l
0.5000 0.4930 99
Barium
mg/l
0.5000 0.4980 100
Beryllium
mg/l
0.5000 0.4990 100
Boron
mg/l
0.5000 0.4920 98
RECEIVED
Date: 03/08/06
Page: 20
of 32
H S E Dept
001
REPORT OF LABORATORY ANALY09-
Asheville Certification IDs
This report shall not be reproduced, except in full,
Charlotte Certification
IDs
NC Wastewater 40
without the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water 37712
a,,
NC Drinking Water
37706
SC Environmental 99030
OnE
SC
99006
FL NELAP E87648
9
FL NELAP
E87627

Pace Analytical"
www. pacelabs. corn
LABORATORY CONTROL SAMPLE: 926582404
QUALITY CONTROL DATA
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec
Cadmium
mg/l
0.5000
0.5000
100
Chromium
mg/l
0.5000
0.5160
103
Copper
mg/1
0.5000
0,5050
101
Iron
mg/l
5.000
5.080
102
Lead
mg/l
0.5000
0.5000
100
Magnesium
mg/l
5.000
5.020
100
Manganese
mg/1
0.5000
0.5070
101
Molybdenum
mg/l
0.5000
0.5120
102
Nickel
mg/l
0.5000
0.4950
99
Selenium
mg/l
0.5000
0.4930
99
Silver
mg/l
0.2500
0.2480
99
Thallium
mg/1
0.5000
0.4770
95
Zinc
mg/1
0.5000
0.5520
110
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 926582412 926582420
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Nuntersville, NC 28078
Phone: 704.875,9092
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Footnotes
926576752
Spike
MS
MSD
MS
MSD
Parameter
Units
Result
Conc.
Result
Result X
Rec X
Rec
RPD Footnotes
Aluminum
mg/l
0.03150
5.000
5.230
4.570
104
91
13
Antimony
mg/l
0.00071
0.5000
0.5050
0.4430
101
88
13
Arsenic
mg/l
0
0.5000
0.4960
0.4350
99
87
13
Barium
mg/l
0.00411
0.5000
0.4980
0.4380
99
87
13
Beryllium
mg/l
0.00006
0.5000
0.4930
0.4420
99
88
11
Boron
mg/l
0.1190
0.5000
0.6200
0.5630
100
89
10
Cadmium
mg/l
0.00007
0.5000
0.4960
0,4370
99
87
13
Chromium
mg/l
0
0.5000
0.5100
0.4500
102
90
12
Copper
mg/l
0.00665
0.5000
0.5150
0.4540
102
90
13
Iron
mg/l
0.05610
5.000
5.080
4,490
100
89
12
Lead
mg/1
0.00367
0.5000
0.5010
0.4440
100
88
12
Magnesium
mg/l
2.030
5.000
7.110
6.500
102
89
9
Manganese
mg/l
0.00257
0.5000
0.5040
0.4450
100
88
12
Molybdenum
mg/l
0.00883
0.5000
0.5200
0.4620
102
91
12
Nickel
mg/l
0.00991
0.5000
0.5010
0.4430
98
87
12
Selenium
mg/l
0.00102
0.5000
0.4910
0.4330
98
86
13
Silver
mg/l
0
0.2500
0.2500
0.2210
100
88
12
Thallium
mg/l
0.00240
0.5000
0.4950
0.4330
98
86
13
RECEIVED
Date: 03/08/06
Page: 21
of 32
H S
E I)epi
PFI
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs
This report shall
not be reproduced,
except
in full,
Charlotte Certification
IDs
NC Wastewater
40
without the written consent of Pace
Analytical Services, Inc.
NC Wastewater
12
NC Drinking Water
37712
Drinking Water
37706
SC Environmental
99030
11�NC
s
Sc
99006
FL NELAP
E87648
FL NELAP
E87627

PaceAna lytical
www, pacelabs. cony
QUALITY CONTROL DATA
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 926582412 926582420
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax., 704.875.9091
Lab Project Number: 92112133
Client Project ID: Outfall 001
926576752 Spike MS MSD MS MSD
Parameter Units Result Conc. Result Result % Rec % Rec RPD Footnotes
Zinc mg/l 0.04880 0.5000 0.5730 0.5130 105 93 11
SAMPLE DUPLICATE: 926582438
926576760
DUP
Parameter
Units
Result
Result
RPD Footnotes
Aluminum
mg/l
1.800
1.800
2
Antimony
mg/l
ND
ND
NC
Arsenic
mg/1
ND
ND
NC
Barium
mg/1
0.06600
0.06500
2
Beryllium
mg/l
ND
ND
NC
Boron
mg/l
0.1200
0.1200
0
Cadmium
mg/l
ND
ND
NC
Chromium
mg/l
0.00340
0.00320
7
Copper
mg/1
0.05300
0.05100
3
Iron
mg/1
2.100
2.000
6
Lead
mg/l
0.00820
0.00700
17
Magnesium
mg/l
2.300
2.300
1
Manganese
mg/l
0.1400
0.1400
1
Molybdenum
mg/l
0.01200
0.01200
2
Nickel
mg/l
0.02800
0.02700
6
Selenium
mg/l
ND
ND
NC
Silver
mg/l
0.00410
0.00410
0
Thallium
mg/l
ND
ND
NC
Zinc
mg/1
0.1400
0.1300
4
Date: 03/08/06
RECEIVED
HSEDept
REPORT OF LABORATORY ANALYSIS'
Asheville Certification IDs This report shall not be reproduced, except in full,
INC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712 «o,,
SC Environmental 99030 a
FL NELAP E87648 IIGICR.
Page: 22 of 32
Charlotte Certification ID
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

Pace Analytical Services, Inc.
PQ t1 9800 Kincey Avenue, Suite 100
ace Analytical"' Huntersville, NC 28078
www,pacelabs.com QUALITY CONTROL DATA Phone: 704.875.909
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
QC Batch: 148145
0C Batch Method: EPA 340.2
Associated Lab Samples: 926579269
METHOD BLANK: 926579749
Associated Lab Samples: 926579269
Parameter Units
Fluoride mg/l
LABORATORY CONTROL SAMPLE: 926579756
Parameter Units
Fluoride mg/l
MATRIX SPIKE: 926579764
Analysis Method: EPA 340.2
Analysis Description: Fluoride
Blank Reporting
Result Limit Footnotes
NO 0.10
Spike LCS LCS
Conc. Result X Rec Footnotes
2.500 2.610 104
926576216 Spike MS MS
Parameter Units Result Conc. Result % Rec Footnotes
Fluoride mg/l 1.430 2.500 3.960 101
SAMPLE DUPLICATE: 926579772
Parameter Units
Fluoride mg/l
Date: 03/08/06
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
926576240 DUP
Result Result RPD Footnotes
1.200 1.100 9
9El DV E;D
HSEDept
F19
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
" ,«,,,
nelac
Page: 23 of 32
Charlotte Certification ID
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

�FaceAnalytical
www.pacelabs.com
QC Batch: 148233
OC Batch Method: EPA 353.2
Associated Lab Samples: 926579269
METHOD BLANK: 926583279
Associated Lab Samples: 926579269
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NO 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 353.2
Analysis Description: 28 day NOX
Blank Reporting
Parameter Units Result Limit Footnotes
Nitrate -Nitrite (as N) mg/1 NO 0.10
LABORATORY CONTROL SAMPLE: 926583287
Spike
LCS
Parameter
Units
Conc.
Result
Nitrate -Nitrite (as N)
mg/l
5.000
5.230
MATRIX SPIKE: 926583295
926552878
Spike
Parameter
Units
Result
Conc.
Nitrate -Nitrite (as N)
mg/l
0
5.000
SAMPLE DUPLICATE: 926583303
Parameter Units
Nitrate -Nitrite (as N) mg/1
Date: 03/08/06
Asheville Certification IDs
NO Wastewater
40
NO Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
LCS
% Rec Footnotes
105
MS MS
Result x Rec Footnotes
5.160 103
926557570 DUP
Result Result RPD Footnotes
8.700 8.700 0
RECEIVED
HSEDept
Pip
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent offPPace
, Analytical Services, Inc.
en
Page: 24 of 32
Charlotte Certification ID
NO Wastewater
12
NO Drinking Water
37706
SC
99006
FL NELAP
E87627

FaceAnalyticalo
www. pacelabs. cam
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
QC Batch: 148256 Analysis Method: EPA 375.4
QC Batch Method: EPA 375.4 Analysis Description: Sulfate,Turbidimetric
Associated Lab Samples: 926579269
METHOD BLANK: 926585019
Associated Lab Samples: 926579269
Blank Reporting
Parameter Units Result Limit Footnotes
Sulfate mg/l NO 5.0
LABORATORY CONTROL SAMPLE: 926585027
Spike
LCS
Parameter
Units
Conc.
Result
Sulfate
mg/l
20.00
20.68
MATRIX SPIKE: 926585043
926578980
Spike
Parameter
Units
Result
Conc.
Sulfate
mg/1
919.5
20.00
SAMPLE DUPLICATE: 926585035
Parameter Units
Sulfate mg/l
Date: 03/0e/D6
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
LCS
X Rec Footnotes
103
MS MS
Result % Rec Footnotes
917.5 0 4
926578980 DUP
Result Result RPD Footnotes
920.0 920.0 0
RECEIVED
"-i S E Dept
0CJ
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 25 of 32
Charlotte Certification ID
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical")
www. pacelabs. cam
QC Batch: 148280
QC Batch Method: EPA 351.2
Associated Lab Samples: 926579269
METHOD BLANK: 926585399
Associated Lab Samples: 926579269
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone:[phone]
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 351.2
Analysis Description: Total Kjeldahl Nitrogen
Blank Reporting
Parameter Units Result Limit Footnotes
Nitrogen, Kjeldahl, Total mg/l NO 0.50
LABORATORY CONTROL SAMPLE: 926585407
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Nitrogen, Kjeldahl, Total mg/l 10.00 8.410 84
MATRIX SPIKE: 926585415
926578360 Spike MS MS
Parameter Units Result Conc. Result X Rec Footnotes
Nitrogen, Kjeldahl, Total mg/l 1.120 10.00 9.020 79
SAMPLE DUPLICATE: 926585423
Parameter Units
Nitrogen, Kjeldahl, Total mg/l
Date: 03/08/06
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
9903D
FL NELAP
E87648
926575853 DUP
Result Result RPD Footnotes
2.700 2.700 2
RECEIVED
HSEDept
PFI
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 26 of 32
harlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical
www, pacelabs. com
QC Batch: 148287
0C Batch Method: EPA 410.4
Associated Lab Samples: 926579269
METHOD BLANK: 926585639
Associated Lab Samples: 926579269
Parameter Units
Chemical Oxygen Demand mg/l
LABORATORY CONTROL SAMPLE: 926585647
Parameter Units
Chemical Oxygen Demand mg/l
MATRIX SPIKE: 926585993
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: 704,875.9091
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 410.4
Analysis Description: Chemical Oxygen Demand
Blank Reporting
Result Limit Footnotes
ND 25.
Spike LCS LCS
Conc. Result X Rec Footnotes
750.00 786.0 105
926579269 Spike MS MS
Parameter Units Result Conc. Result % Rec Footnotes
Chemical Oxygen Demand mg/1 93.00 750.00 933.0 112
SAMPLE DUPLICATE: 926586009
926579285 DUP
Parameter Units Result Result RPD Footnotes
Chemical Oxygen Demand mg/l 77.00 66.00 15
Date: 03/08/06
RECEIVED
HSEDept
PFI
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
INC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
Page: 27 of 32
Charlotte Certification ID
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

•f4O
Pace Analytical Services, Inc.
Pace AlIalytical `
9800 KinceyAvenue, Suite 100
Huntersville, NC 26078
www.pacelabs.conr
QUALITY CONTROL DATA
Phone:704,875.9092
Fax: [phone]
Lab Project Number:
92112133
Client Project ID:
Outfall 001
OC Batch: 148396
Analysis Method: EPA 350.1
QC Batch Method: EPA 350.1
Analysis Description: Ammonia
Associated Lab Samples: 926579269
METHOD BLANK: 926591017
Associated Lab Samples: 926579269
Blank Reporting
Parameter Units
Result Limit Footnotes
Nitrogen, Ammonia mg/l
NO 0.10
LABORATORY CONTROL SAMPLE: 926591025
Spike LCS LCS
Parameter Units
Conc. Result % Rec Footnotes
Nitrogen, Ammonia mg/l
1.000 1.065 107
MATRIX SPIKE: 926591033
926578360 Spike MS MS
Parameter Units Result Conc. Result x Rec Footnotes
Nitrogen. Ammonia mg/l 0.1730 1.000 0.9730 80
SAMPLE DUPLICATE: 926591041
Parameter Units
Nitrogen. Ammonia mg/l
Date: 03/08/06
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
926578550 DUP
Result Result RPD Footnotes
0.1900 0.1900 1
RECEIVE®
HSEDept
PFs
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
,M EC<pyp'
ue`I� i
Page: 28 of 32
Charlotte Certification I
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

G
Face Analytical
www.pacelabs.com
QC Batch: 148416
QC Batch Method: SM 5310B
Associated Lab Samples: 926579269
METHOD BLANK: 926592049
Associated Lab Samples: 926579269
Parameter Units
Total Organic Carbon mg/l
LABORATORY CONTROL SAMPLE: 926592056
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax., 704.875.9091
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: SM 5310B
Analysis Description: Total Organic Carbon
Blank Reporting
Result Limit Footnotes
NO 1.0
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Total Organic Carbon mg/l 10.00 9.440 94
MATRIX SPIKE: 926592064
926557349 Spike MS MS
Parameter Units Result Conc. Result X Rec Footnotes
Total Organic Carbon mg/l 23.03 40.00 52.20 73
SAMPLE DUPLICATE: 926592072
Parameter Units
Total Organic Carbon mg/l
Date: 03/08/06
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
926557364 OUP
Result Result RPD Footnotes
20.00 25.00 19
RECEIVED
HSEDept
REPORT OF LABORATORY ANALYSIS FA
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
. rmC i
Page: 29 of 32
Charlotte Certification I
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

1 ,
ace Analytical °
www.pacelabs.com
QC Batch: 148641
QC Batch Method: EPA 335.2
Associated Lab Samples: 926579269
METHOD BLANK: 926597394
Associated Lab Samples: 926579269
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: 704.875,9092
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 335.2
Analysis Description: Cyanide, Total, Water
Blank Reporting
Parameter Units Result Limit Footnotes
Cyanide mg/l NO 0.0050
LABORATORY CONTROL SAMPLE: 926597402
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Cyanide mg/l 0.1000 0,0930 93
MATRIX SPIKE: 926597444
926588393 Spike MS MS
Parameter Units Result Conc. Result % Rec Footnotes
Cyanide mg/l 0 0.1000 0.0950 95
SAMPLE DUPLICATE: 926597451
Parameter Units
Cyanide mg/1
Date: 03/08/06
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
926588401 DUP
Result Result RPD Footnotes
ND NO NC
RECEIVE®
H V E DePS
,PF9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent ofPaceAnalytical Services, Inc.
„
\I elac
Page: 30 of 32
Charlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

----.'FaceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Far: 704.875.9091
Lab Project Number: 92112133
Client Project ID: Outfall 001
Consistent with EPA guidelines. unrounded concentrations are displayed and have been used to calculate % Rec and RPD values.
LCS(D) Laboratory Control Sample (Duplicate)
MS(D) Matrix Spike (Duplicate)
DUP Sample Duplicate
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
RPD Relative Percent Difference
(S) Surrogate
11) Acid surrogate recovery outside of control limits. The data was accepted based on valid recovery of the two
remaining acid surrogates.
[21 The surrogate and/or spike recovery was outside acceptance limits.
[31 RPD value was outside control limits, however both percent recoveries were acceptable. Sample results for the
QC batch were accepted based on percent recoveries and completeness of QC data.
[41 The spike recovery was outside acceptance limits for the MS and /or MSD due to matrix interference. The LCS
and/or LCSD were within acceptance limits showing that the laboratory is in control and the data is
acceptable.
Date: 03/08/06
RECEIVED
HSEDWI
PFI
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs
This report shall not be reproduced, except in full,
NC Wastewater 40
without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712
o,e
SC Environmental 99030
t °
Page: 32 of 32
haillotte Certification I
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627
FL NELAP E87648

PaceAnalytical'
www.pacelabs.com
DUI
March 06, 2006
Mr. Chuck Powell
Performance Fibers
338 Pea Ridge Road
New Hill, NC 27562
RE: Lab Project Number: 92114023
Client Project ID: Outfall 001 Resample
Dear Mr. Powell:
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax [phone]
Enclosed are the analytical results for sample(s) received by the laboratory on February 23, 2006. Results
reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the
body of the report.
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic testing
was performed at our Pace Charlotte laboratory unless otherwise footnoted.
If you have any questions concerning this report please feel free to contact me.
Sincerely,
k04 /�' L-4111-
Kate Knauff
[e-mail]
Project Manager
Enclosures
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
s 1 IGk
RECEIVED
H S E Dept
PFI
harlotte Certificati
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

Subcontracted Results
Pace Project #
,-1 2 ll �-r Ur i )-
This report includes
page 1 to �,A

TestAmerica
ANAIYTIC'AL TESTING CORPORATION
March 06, 2006
Client: Pace Analytical (7228)
9800 Kincy Avenue, Suite 100
Huntersville, NC 28078
Attn: Kate Knauff
SAMPLE IDENTIFICATION
926681610/outfall 001 comp
2960 FosW Creighton Road Na6hvRe, TN 37204. 60&765-MO - Fax 615-72&3404
Work Order:
NPB2962
Project Name:
Pace Analytical
Project Nbr:
92114023
Date Received:
02/24/06
LAB NUMBER COLLECTION DATE AND TIME
NPB2962-01 02/22/06 14:33
An executed copy of the chain of custody, the project quality control data, and the sample receipt form are also included as an addendum
to this report. If you have any questions relating to this analytical report, please contact your Laboratory Project Manager at
1-800-765-0980. Any opinions, if expressed, are outside the scope of the Laboratory's accredidation.
This material is intended only for the use of the individual(s) or entity to whom it is' addressed, and may contain information that is
privileged and confidential. If you are not the intended recipient, or the employee or agent responsible for delivering this material to the
intended recipient, you are hereby notified that any dissemination, distribution, or copying of this material is strictly prohibited. If you
have received this material in error, please notify us immediately at 615-726-0177.
North Carolina Certification Number: 387
RECEIVE®
H S E Dep(
PFI
The Chain(s) of Custody, 4 pages, are included and are an integral pan of this report.
These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory.
Report Approved By:
Jessica Vickers
Senior Project Manager
Page 1 of 6

TestAmerica
ANALYTICAL TESTING CORPORATION
2960 Foner Creighton Rod NaMwRe, TN 372U * 800-765-0960 - Fax [phone],104
Client Pace Analytiral(7228)
Work Order:
NPB2962
9800 Kincy Avenue, Suite 100
Project Name:
Pace Analytical
Huntersville, NC 28078
Project Number:
92114023
Arm Kate Knauf!
Received:
02/2410608,05
ANALYTICAL REPORT
Dilution Analysis
Analyte Result Flag Units. MRL
Factor Date/Time
Method
Batch
Sample ID: NPB2962-01 (926681610/outfall 001 comp - Water) Sampled: 0222/06 14:33
Selected Volatile Organic Compounds by EPA Method 8260B
Bis(chloromethyl)ether ND ug/L 2.00
1 03/03/0617:32
SW8468260B
6030035
Surr.1,2-Dichloroethane-d4(70-130%) 101%
0310210609.,32
SW8468260B
6030035
Surr: Dibro q luoromethane (79-112%) 100 %
03/02/06 09:32
SW846 8260E
6030035
Surr: Tohrene-d8 (78-121 %) 100 %
03/02U 09: 31
SW846 8260E
6030035
Surr 4-BromoJfuorobewene (78-126%) 104 %
03102106 09:32
SW8468260B
6030035
RECEIVED
MAI, j fl-:;;;r;
H S E Dept
PFI
Page 2 of 6

TestAmerica
ANMYTICAL TFSTI C CORPORATION 2950 Foster Creighton Road Nashville. TN 37204. W0 765-0980• Fez6167263404
Client Pace Analytical (7228)
Work Order:
NPB2962
9800 Kinry Avenue, Suite 100
Project Name:
Pace Analytical
Huntersville, NC 28078
Project Number:
92114023
Ann Kate KnautT
Received:
022410608:05
PROJECT QUALITY CONTROL DATA
Blank
Analyte
Blank Value Q Unns
Selected Volatile Organic Compounds by EPA Method 8260E
6030035-BLKI
Bis(chlarornethyl).ther
<0.250 ug/L
Numagule: 1,2-Dluhloroelhone-d4
98%
Su ragula: Dibromofiuornnrelhnne
92%
,Svrmgala: Toluene-dN
101%
.5'urrogole: 4-BromgJluorobenzene
104%
Q C Batch Lab Numbcr Analyzed DateRime
6030035
6030033-BLKI
03/03/06 17:32
6030035
6030035-BLKI
03/02/06 06:25
6030035
6030035-BLKI
03/02/06 06:25
6030035
6030035-BLKI
03/02/06 06:25
6030035
6030035-BLKI
03/02/06 06:25
9
RECEIVED
:A
H S E reps
PFI
Page 3 of 6

'TestAmerica
ANAI.YTICAI, TESTING, CORPO"TION
2%0 Foster Creighton Road Nashville, TN372U'NO-765-0980• Faae15�726-3404
Client Pace Analytical(7228)
Work Order:
NPB2962
9800 Kincy Avenue, Suite 100
Project Name:
Pace Analytical
Hunteraville, NC 28078
Project Number:
92114023
An Kale KnaufT
Received:
022410608:05
PROJECT QUALITY CONTROL DATA
LCS
Target
Anaiyud
Analyse Known Val.
Analyzed Val Q
Units %Rm
Range
Batch
Date/Rime
Selected Volatile Organic Compounds by EPA Method 8260E
6030035-BS2
Bis(6Ior=ethyI)edia 50.0
28.1 L2, MNRI
ug/L 56%
60-137
6030035
03102/0616:38
Surrngole: 1.2-Uich7ororrhae,-d4 50.0
42.7
85%
70-130
6030033
03/02/06 16;38
Sermgam: Dib. Jleo whaae $0.0
47.7
95%
79- 122
6030035
03/02/06 16:39
.iurrogate: Toluene-dN 50.0
92.2 Z2
194%
78-121
6030D35
03/02/06 16:38
Ma,gon: 4-Broar.&lu brnrene 50.0
44.9
90%
78-126
W30035
03/02/06 16:39
RECEIVED
HSEDept
PE1
Page 4 of 6

TestAmerica
ANALYTICAL TESTING CORPORATION
2960 Fostar Creighton Road Nas lle. TN 37MI - 800.765-0980 - Fax [phone]
Client Pace Analytical (7228)
Work Order:
NPB2962
9800 Kincy Avenue, Suite 100
Project Name:
Pace Analytical
Huntersville, NC 28078
Project Number:
92114023
Ann Kate Knauff
Received:
0224/0608:05
SUMMARY
TestAmeriea Analytical - Nmhville
Method Matrix AIHA Nelae North Carolina
SW8468260B Water N/A X X
RECEIVED
.H S E Depa
FIR
Page ? of 6

TestAmerica
ANALYTICAL TESTING CORPORATION
Client Pace Analytical (7228)
9900 Kincy Avenue, Suite 100
Huntersville, NC 28078
Ann Kate Knauff
2960 Foster Creighton Road Nashville, TN 37MI • 900,765-0990 - Fax a11726-ado/
Work Order:
NPB2962
Project Name:
Pace Analytical
Project Number:
92114023
Received:
02/24/06 08:05
DATA QUALIFIERS AND DEFINITIONS
L2 Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was below acceptance limits.
MNRI There was no MS/MSD analyzed with this batch due to insufficient sample volume. See Blank Spike,
Z2 Surrogate recovery was above the acceptance limits. Data not impacted.
METHOD MODIFICATION NOTES
RECEIVED
HSEUep;:
'F1
PaZe 6 of 6

eAnalytical
Section A
Required Cliem Information:
Address
Email To:
Phone Fax
Requested Due Date?AT:
Section D Required Client Information
SAMPLE ID
One Character per box.
W (A-Z, 0-9 f . )
F, Samples IDS MUST BE UNIQUE
Additional Comments:
SEE REVERSE SIDE FOR INSTRUCTIONS
CHAIN -OF -CUSTODY / Analytical Request Document
The Cham-of-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Page: of
Section B
Required Project Information:
Section C
Invoice Information:
REGULATORY
Report To:
Attention:
❑ NPDES �. GROUND WATER DRINKING WATER
❑ US7 ❑ RCRA Li Other
Copy To:
Company Name:
Address:
•• a OOA OIL ❑IN ❑MI ❑MN ONC
DOM ❑SC O WI ❑OTHER
Purchase Order No.:
Pace Quote Reference:
Project Name:
Pace Project Manager:
V . K-..' -.(f
Filtered (YIN) _
Project Number:
Pace Profile #:
Requested
atax Coda
Anelyais:
( CODE
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SAMPLER NAME AND SIGNATURE
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,91GNATURE of SAMPLER: e •e
SAMPLE CONDITION
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A
aceAnalytical
www.pacelabs.com
February 10, 2006
Mr. Chuck Powell
Performance Fibers
338 Pea Ridge Road
New Hill, NC 27562
RE: Lab Project Number: 92112133
Client Project ID: Outfall 001
Dear Mr. Powell:
Pace Analytical Sery Inc.
9800 Kincey Avenue, 100
Huntersville, Nu zrr078
Phone: [phone]
Fax: 704.875,9091
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Enclosed are the analytical results for sample(s) received by the laboratory on January 25. 2006. Results
reported herein conform to the most current NELAC standards, where applicable. unless otherwise narrated in the
body of the report.
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic testing
was performed at our Pace Charlotte laboratory unless otherwise footnoted.
If you have any questions concerning this report please feel free to contact me.
Sincerely,
Kate Knauff
[e-mail]
Project Manager
Enclosures
[RECEIVE®
H .S E Depi
PR
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
SC 99039030
NC Drinking Water 2 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648
sel I�q�.
rlotte Certification ID
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

A4
'aceAnalytical
www.pacelabs.com
Lab Sample No: 926579269
Client Sample ID: OUTFALL 001 COMP
Pace Analytical Sery Inc.
9800 Kincey Avenue, ; 100
Huntersville, NO 28078
Phone: [phone]
Fax:[phone]
Pace Analytical Services, ins.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 92112133
Client Project ID: Outfall 001
Project Sample Number: 92112133-001 Date Collected: 01/24/06 14:25
Matrix: Water Date Received: 01/25/06 17:00
Parameters
Results
Units
Report Limit
OF
Analyzed
By
CAS No. Qual
Re9Lmt
Client Services
Total Organic Nitrogen
Method:
Total Organic Nitrogen
0.57
mg/l
0.10
1.0
01/30/06
WWB
Metals
Trace ICP Metals
Prep/Method:
/ EPA 200.7
Aluminum
0.18
mg/l
0.10
1.0
01/27/06
17:38
SAJ
7429.90-5
Antimony
0.019
mg/l
0.0050
1.0
01/27/06
17:38
SAJ
7440-36-0
Arsenic
NO
mg/l
0.0050
1.0
01/27/06
17:38
SAJ
7440-38-2
Barium
0.017
mg/l
0.0050
1.0
01/27/06
17:38
SAJ
7440-39-3
Beryllium
NO
mg/l
0.0010
1.0
01/27/06
17:38
SAJ
7440-41-7
Boron
0.14
mg/l
0.010
1.0
01/27/06
17:38
SAJ
7440-42-8
Cadmium
NO
mg/l
0.0010
1.0
01/27/06
17:38
SAJ
7440-43.9
Chromium
NO
mg/l
0.0020
1.0
01/27/06
17:38
SAJ
7440-47-3
Copper
0.022
mg/l
0.0020
1.0
01/27/06
17:38
SAJ
7440-50-8
Iron
0.11
mg/l
0.050
1.0
01/27/06
17:38
SAJ
7439-89-6
Lead
NO
mg/l
0.0050
1.0
01/27/06
17:38
SAJ
7439-92-1
Magnesium
7.5
mg/l
0.10
1.0
01/27/06
17:38
SAJ
7439.95-4
Manganese
0.12
mg/l
0.0050
1.0
01/27/06
17:38
SAJ
7439-96-5
Molybdenum
0.014
mg/l
0.0050
1.0
01/27/06
17:38
SAJ
7439-98-7
Nickel
0.078
mg/l
0.0050
1.0
01/27/06
17:38
SAJ
7440-02-0
Selenium
NO
mg/l
0.0050
1.0
01/27/06
17:38
SAJ
7782-49-2
Silver
NO
mg/l
0.0020
1.0
01/27/06
17:38
SAJ
7440-22-4
Thallium
NO
mg/l
0.010
1.0
01/27/06
17:38
SAJ
7440-28-0
Zinc
0.63
mg/l
0.010
1.0
01/27/06
17:38
SAJ
7440-66-6
Date Digested
01/26/06 15:30
01/26/06
15:30
Mercury, CVAAS, in Water
Method:
EPA
7470
Mercury
NO
mg/l
0.00020
1.0
01/26/06
10:48
ALV
7439-97-6
Wet Chemistry
Cyanide, Total, Water
Method:
EPA
335.2
Cyanide
NO
mg/l
0.0050
1.0
02/01/06
13:30
BMF
57-12-5
Fluoride
Method:
EPA
340.2
Fluoride
0.32
mg/l
0.10
1.0
01/26/06
09:35
TMR
16984-48-8
Ammonia
Method:
EPA
350.1
Nitrogen, Ammonia
NO
mg/l
0.10
1.0
01/228/
V'1
7727-37-9
Date: 02/10/06
-
Page: 1
of 32
Asheville Certification IDs
REPORT OF LABORATORY
ANALYSIS
Charlotte Certification IDs
NC Wastewater 40
NC Wastewater
12
NC Drinking Water 37712
This report shall not be reproduced,
except in full,
NC Drinking Water
37706
SC 99030
without
the written consent of Pace Analytical Services, Inc.
SC
99006
FL NELAP E87648
"�°
M
1 Ieb
FL NELAP
E87627

JAI
I
ce Analytical
www.pacelabs.com
Pace Analytical Serv, nc.
9800 Kincey Avenue, t 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Lab Sample No: 926579269
Project Sample
Number: 92112133.001 Date Collected:
01/24/06 14:25
Client Sample ID: OUTFALL 001 COMP
Matrix: Water Date Received:
01/25/06 17:00
Parameters Results
Units Report Limit
OF Analyzed By CAS No.Qua]
RegLmt
Total Kjeldahl Nitrogen Method: EPA
351.2
Nitrogen, Kjeldahl, Total 0.65
mg/l 0.50
1.0 01/26/06 22:40 ARM
28 day NOX Method: EPA 353.2
Nitrate -Nitrite (as N) 2.0 mg/l 0.10
Sulfate,Turbidimetric Method: EPA 375.4
Sulfate 110 mg/l 25.
Chemical Oxygen Demand Method: EPA 410.4
Chemical Oxygen Demand 93. mg/l 25.
Phenolics, Total Recoverable Method: EPA 420.2
Phenolics, Total Recoverable 0.011 mg/l 0.010
Total Organic Carbon
Total Organic Carbon
GUMS Semivolatiles
Extractables in Water by 625
Benzidine
Benzo(g.h.i)perylene
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
4-Chlorophenylphenyl ether
Chrysene
3.3'-Dichlorobenzidine
Di-n-octylphthalate
1,2-Diphenylhydrazine
Hexachlorocyclopentadiene
Isophorone
N-Nitrosodimethylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Date: 02/10/06
Asheville Certification
IN
NC Wastewater
40
NC Drinking Water
37712
SC
99030
FL NELAP
E87648
Method: SM 5310B
14. mg/l 1.0
1.0 01/26/06 21:00 CD1 7727-37-9
5.0 01/26/06 18:34 ARH
1.0 01/27/06 07:45 TMR
1.0 02/01/06 16:40 EWS
1.0 01/30/06 07:30 BMF 7440.44-0
Prep/Method: EPA 625
SF / EPA 625
NO
ug/l
200
4.0
02/03/06
00:12
BET
92-87-5
NO
ug/l
20.
4.0
02/03/06
00:12
BET
191-24-2
NO
ug/l
20.
4.0
02/03/06
00:12
BET
101.55-3
NO
ug/l
20.
4.0
02/03/06
00:12
BET
85-68.7
NO
ug/l
20.
4.0
02/03/06
00:12
BET
59.50-7
NO
ug/l
20.
4.0
02/03/06
00:12
BET
111-91-1
NO
ug/1
20.
4.0
02/03/06
00:12
BET
111-44-4
NO
ug/l
20.
4.0
02/03/06
00:12
BET
39638-32-9
NO
ug/l
20.
4.0
02/03/06
00:12
BET
91-58-7
NO
ug/l
20.
4.0
02/03/06
00:12
BET
7005.72-3
NO
ug/l
20.
4.0
02/03/06
00:12
BET
218-01-9
NO
ug/l
40.
4.0
02/03/06
00:12
BET
91-94-1
NO
ug/l
20.
4.0
02/03/06
00:12
BET
117.84-0
NO
ug/l
20.
4.0
02/03/06
00:12
BET
122-66-7
NO
ug/l
40.
4.0
02/03/06
00:12
BET
77-47.4
ND
ug/l
20.
4.0
02/03/06
00:12
BET
78-59-1
NO
ug/l
20.
4.0
02/03/06
00:12
BET
62-75-9
NO
ug/l
20.
4.0
02/03/06
00:12
BET
86-30;6
NO
ug/l
100
4.0
02/03/06
00:12
BET
87-86.5
RECEIVE®
. r Page: 2
of 32
�B
7
E
08
JP�
REPORT OF
LABORATORY ANALYSIS
Charlotte certification
IN
This report shall
not be reproduced,
except
in full,
NC Wastewater
12
NC Drinking Water
37706
without
the written
consent of Pace Analytical
Services, Inc.
Sc
99006
�.
:� 1 MIX
MIX
FL NELAP
E87627

C' a
aceAnalytical"
www. pacelabs. com
Lab Sample No: 926579269
Client Sample TD: OHiFALL 001 COMP
Pace Analytical Servi ac.
9800 Kincey Avenue, 6 00
Huntersville, NU26078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone. [phone]
Fax., 828.252,4618
Lab Project Number: 92112133
Client Project ID: Outfall 001
Project Sample Number: 92112133.001 Date Collected: 01/24/06 14:25
Matrix: Water Date Received: 01/25/06 17:00
Parameters
Results
Units
Report Limit
OF
Analyzed
By
CAS No. Qual
RegLmt
Phenanthrene
NO
ug/l
20.
4.0
02/03/06
00:12
BET
85-01-8
Pyrene
NO
ug/l
20.
4.0
02/03/06
00:12
BET
129-00-0
1.2.4-Trichlorobenzene
NO
ug/l
20.
4.0
02/03/06
00:12
BET
120-82-1
2,4.6-Trichlorophenol
NO
ug/l
20.
4.0
02/03/06
00:12
BET
88-06-2
Nitrobenzene-d5 (S)
52
X
1.0
02/03/06
00:12
BET
4165.60-0
2-Fluorobiphenyl (S)
72
%
1.0
02/03/06
00:12
BET
321.60-8
Terphenyl-d14 (S)
80
X
1.0
02/03/06
00:12
BET
1718-51-0
Phenol-d5 (S)
29
%
1.0
02/03/06
00:12
BET
4165.62-2
2-Fluorophenol (S)
39
%
1.0
02/03/06
00:12
BET
367.12-4
2.4,6-Tribromophenol (S)
97
%
1.0
02/03/06
00:12
BET
118-79-6
Date Extracted
01/31/06
01/31/06
GC Semivolatiles
Organochlorine Pesticides
Prep/Method:
EPA 3535 /
EPA 8081
Aldrin
ND
ug/l
0.050
1.0
01/30/06
21:56
JEM
309-00-2
alpha-BHC
ND
ug/l
0.050
1.0
01/30/06
21:56
JEM
319.84.6
beta-BHC
NO
ug/l
0.050
1.0
01/30/06
21:56
JEM
319-85.7
delta-BHC
NO
ug/l
0.10
1.0
01/30/06
21:56
JEM
319-86-8
gamma-BHC (Lindane)
NO
ug/l
0.050
1.0
01/30/06
21:56
JEM
58-89-9
Chlordane
NO
ug/1
0.50
1.0
01/30/06
21:56
JEM
57-74-9
4.4'-DDO
NO
ug/l
0.10
1.0
01/30/06
21:56
JEM
72.54-8
4.4'-DDE
NO
ug/1
0.10
1.0
01/30/06
21:56
JEM
72-55.9
4,4'-DDT
NO
ug/1
0.10
1.0
01/30/06
21:56
JEM
50.29-3
Dieldrin
NO
ug/l
0.10
1.0
01/30/06
21:56
JEM
60-57-1
Endosulfan I
NO
ug/l
0.10
1.0
01/30/06
21:56
JEM
959-98.8
Endosulfan II
NO
ug/1
0.10
1.0
01/30/06
21:56
JEM
33213.65-9
Endosulfan sulfate
NO
ug/l
0.10
1.0
01/30/06
21:56
JEM
1031-07-8
Endrin
NO
ug/l
0.060
1.0
01/30/06
21:56
JEM
72-20.8
Endrin aldehyde
NO
ug/l
0.10
1.0
01/30/06
21:56
JEM
7421-93-4
Heptachlor
NO
ug/l
0.050
1.0
01/30/06
21:56
JEM
76-44-8
Heptachlor epoxide
NO
ug/l
0.80
1.0
01/30/06
21:56
JEM
1024-57-3
Toxaphene
NO
ug/l
1.0
1.0
01/30/06
21:56
JEM
8001-35-2
Tetrachloro-m-xylene (S)
50
X
1.0
01/30/06
21:56
JEM
877-09-8
Decachlorobiphenyl (S)
38
X
1.0
01/30/06
21:56
JEM
2051-24-3
Date Extracted
01/26/06
01/26/06
Organochlorine PCBs
Prep/Method:
EPA 3535 /
EPA 8082
PCB-1016 (Aroclor 1016)
NO
ug/l
1.0
1.0
01/30/06
21:56
JEM
12674-11-2
PCB-1221 (Aroclor 1221)
NO
ug/l
1.0
1.0
01/30/06
21:56
JEM
11104-28-2
RECOVF-0
Date: 02/10/06
Page: 3
of 32
�i
S E Dopi
PR
Asheville Certification ID s
REPORT OF LABORATORY
ANALYSIS
Charlotte Certification
IDs
NC Wastewater 40
NC Wastewater
12
NC Drinking Water
This report shall not
be reproduced,
except in full,
NC Drinking Water
06
99030
Sc 99030
without the written consent of Pace Analytical Services, Inc.
Sc
990
99006
FL NELAP E87648
:1
n
me
FL NELAP
E87627

•
;5'neAnalyficalll�
www.pacelahs.com
Lab Sample No: 926579269
Client Sample ID: OUTFALL 001 COMP
Pace Analytical Servh 7c.
9800 Kincey Avenue, S 00
Huntersville, No z6u78
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Project Sample Number: 92112133-001 Date Collected: 01/24/06 14:25
Matrix: Water Date Received: 01/25/06 17:00
Parameters
Results
Units
Report Limit
DF
Analyzed
By
CAS No. Dual Re9Lmt
PCB-1232 (Aroclor 1232)
ND
ug/l
1.0
1.0
01/30/06
21:56
JEM
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/l
1.0
1.0
01/30/06
21:56
JEM
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/l
1.0
1.0
01/30/06
21:56
JEM
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/l
1.0
1.0
01/30/06
21:56
JEM
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/l
1.0
1.0
01/30/06
21:56
JEM
11096-82-5
Decachlorobiphenyl (S)
38
%
1.0
01/30/06
21:56
JEM
2051-24-3
Date Extracted
01/26/06
01/26/06
GUMS Volatiles
Volatile GUMS by 624
Method: EPA
624
Acrolein
ND
ug/l
25.
1.0
02/01/06
11:29
DLK
107-02-8
Bromodichloromethane
ND
ug/l
5.0
1.0
02/01/06
11:29
DLK
75-27-4
Bromoform
ND
ug/1
5.0
1.0
02/01/06
11:29
DLK
75-25-2
Bromomethane
ND
ug/l
5.0
1.0
02/01/06
11:29
DLK
74.83-9
2-Chloroethylvinyl ether
ND
ug/l
10.
1.0
02/01/06
11:29
DLK
110-75-8
Dichlorodifluoromethane
ND
ug/l
5.0
1.0
02/01/06
11:29
DLK
75-71-8
1.1.1.2-Tetrachloroethane
ND
ug/l
5.0
1.0
02/01/06
11:29
DLK
630-20-6
Trichlorofluoromethane
ND
ug/l
5.0
1.0
02/01/06
11:29
DLK
75.69-4
Toluene-d8 (S)
94
%
1.0
02/01/06
11:29
DLK
2037-26-5
4-Bromofluorobenzene (S)
105
%
1.0
02/01/06
11:29
DLK
460-00-4
Dibromofluoromethane (S)
99
%
1.0
02/01/06
11:29
DLK
1868-53-7
Date: 02/10/06
RECEIVED
H S E Dep1
PR
Asheville Certification
IDs
REPORT OF LABORATORY ANALYSIS
NC Wastewater
40
NC Drinking Water
This report shall not be reproduced, except in full,
SC
99030
9030
without the written consent of Pace Analytical Services, Inc.
FL NELAP
E87648
"O-MC
Page: 4 of 32
Charlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

A
;a?ceAnalyfical
www. pacelabs. cam
Lab Sample No: 926579277
Client Sample ID: OUTFALL 001 GRAB
Pace Analytical ServL V.
9800 Kincey Avenue, 5 00
Huntersville, Ns 2nu78
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Project Sample Number: 92112133.002 Date Collected: 01/24/06 14:25
Matrix: Water Date Received: 01/25/06 17:00
Parameters
Results
Units Report Limit DF Analyzed
By CAS No. Qual Re9Lmt
Field Services
Field Grab Data
Method:
Collected By
AGN
O1/27/06
KAK
Collected Date
1/24/06
01/27/06
KAK
Collected Time
14:25
01/27/06
KAK
Field pH
6.83
01/27/06
KAK
Field Temperature
13.9
01/27/06
KAK
RECEIVED
Date: 02/10/06
H S E 6epl
Page: 5
of 32
PR
Asheville Certification
IDs
REPORT OF LABORATORY ANALYSIS
Charlotte Certification
IDs
NC Wastewater
40
NC Wastewater
12
NC Drinking Water
37712
This
s report shall not be reproduced, except in full,
NC Drinking Water
37706
SC
99030
t theA written
wren consent of Pace Analytical Services, Inc.
SC
99006
FL NELAP
E87648
°`°
FL NELAP
E87627

aceAnalytical
www. pacelabs. corn
PARAMETER FOOTNOTES
Pace Analytical Servic - ic.
9800 Kincey Avenue, & 70
Huntersville, NG cou78
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax.- 828.252.4618
Lab Project Number: 92112133
Client Project ID: Outfall 001
Dilution factor shown represents the factor applied to the reported result and reporting limit due to changes
in sample preparation, dilution of the extract. or moisture content
Method 90718 modified to use ASE.
All pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate
hold time.
Depending on the moisture content the PRLs can be elevated for all soil samples reported on a dry weight basis.
2-Chloroethyl vinyl ether has been shown to degrade in the presence of acid.
NO Not detected at or above adjusted reporting limit
NC Not Calculable
.l Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
(S) Surrogate
Date: 02/10/06
RECENED
H a E vew Pages 6 of 32
PF&
Asheville Certification ID s REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 99030 This report shall not be reproduced, except in full,
SC 9030
NC Drinking Water without the written consent of Pace Analytical Services, Inc.
.«aAe
FL NELAP E87648 10
Charlotte Certification
IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Sery Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, 100 2225 Riverside Drive
Nuntersville, NC28078 Asheville, NC28804
Analvtiral Phone:[phone] Phone.,828.254.7176
Fax:[phone] Fax: [phone]
www.pacelahs.cort? QUALITY CONTROL DATA
Lab Project Number: 92112133
Client Project ID: Outfall 001
QC Batch: 148314 Analysis Method: EPA 8081
QC Batch Method: EPA 3535 Analysis Description: Organochlorine Pesticides
Associated Lab Samples: 926579269
METHOD BLANK: 926586496
Associated Lab Samples: 926579269
Blank
Reporting
Parameter
Units
Result
Limit
Footnotes
Aldrin
ug/l
ND
0.050
alpha-BHC
ug/l
NO
0.050
beta-BHC
ug/l
NO
0.050
delta-BHC
ug/l
NO
0.10
gamma-BHC (Lindane)
ug/l
NO
0.050
Chlordane
ug/l
NO
0.50
4,4'-DOD
ug/l
NO
0.10
4,4'-DDE
ug/l
NO
0.10
4.4'-DDT
ug/l
ND
0.10
Dieldrin
ug/1
ND
0.10
Endosulfan I
ug/l
ND
0.10
Endosulfan II
ug/l
NO
0.10
Endosulfan sulfate
ug/l
NO
0.10
Endrin
ug/l
NO
0.060
Endrin aldehyde
ug/l
NO
0.10
Heptachlor
ug/l
NO
0.050
Heptachlor epoxide
ug/l
NO
0.80
Toxaphene
ug/l
NO
1.0
Tetrachloro-m-xylene (S)
X
78
Decachlorobiphenyl (S)
X
82
LABORATORY CONTROL SAMPLE: 926586504
Parameter
Units
alpha-BHC
ug/l
gamma-BHC (Lindane)
ug/1
beta-BHC
ug/l
Heptachlor
ug/l
delta-BHC
ug/l
Date: 02/10/06
Spike LCS
Conc. Result
0.1600 0.1099
0.1600 0.1093
0.1600 0.1345
0.1600 0.1036
0.1600 0.1555
LCS
% Rec Footnotes
69
68
84
65
97
iH S � j 0epp Page: 7 of 32
PF„
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 99030 This report shall not be reproduced, except in full,
Sc 9030
NC Drinking Water without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 I , y
Ill
harlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

aceAnalytical
www. pacelahs. conl
LABORATORY CONTROL SAMPLE: 926586504
Pace Analytical Sery Inc.
9800 Kincey Avenue,, 100
Huntersville, NC 28078
Phone: [phone]
Fax.' 704.875.9091
QUALITY CONTROL DATA
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec
Aldrin
ug/l
0.1600
0.0838
52
Heptachlor epoxide
ug/l
0.1600
0.1195
75
Endosulfan I
ug/l
0.1600
0.1350
84
4.4'-DOE
ug/l
0.1600
0.1447
90
Dieldrin
ug/l
0.1600
0.1190
74
Endrin
ug/l
0.1600
0.1344
84
4.4'-DDD
ug/l
0.1600
0.1462
91
Endosulfan II
ug/l
0.1600
0.1209
76
4,4'-DDT
ug/1
0.1600
0.1486
93
Endrin aldehyde
ug/l
0.1600
0.1713
107
Endosulfan sulfate
ug/l
0.1600
0.1127
70
Decachlorobiphenyl (S)
66
Tetrachloro-m-xylene (S)
68
LABORATORY CONTROL SAMPLE: 926597139
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec
alpha-BHC
ug/l
0.1600
0.1099
69
gamma-BHC (Lindane)
ug/l
0.1600
0.1093
68
beta-BHC
ug/l
0.1600
0.1345
B4
Heptachlor
ug/l
0.1600
0.1036
65
delta-BHC
ug/l
0.1600
0.1555
97
Aldrin
ug/l
0.1600
0.0838
52
Heptachlor epoxide
ug/l
0.1600
0.1195
75
Endosulfan I
ug/l
0.1600
0.1350
84
4.4'-DOE
ug/1
0.1600
0.1447
90
Dieldrin
ug/l
0.1600
0.1190
74
Endrin
ug/l
0.1600
0.1344
84
4,4'-DDD
ug/l
0.1600
0.1462
91
Endosulfan II
ug/l
0.1600
0.1209
76
4.4'-DDT
ug/l
0.1600
0.1486
93
Endrin aldehyde
ug/l
0.1600
0.1713
107
Endosulfan sulfate
ug/l
0.1600
0.1127
70
Decachlorobiphenyl (S)
66
Tetrachloro-m-xylene (S)
68
Date: 02/10/06
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Footnotes
Footnotes
Asheville Certification REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 99030 This report shall not be reproduced, except in full,
SC 9030
NC Drinking Water without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 M,
:a1 IGm
H S E bap)
PFf Page: 8 of 32
e Certification ID
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Servi Inc.
9800 Kincey Avenue, ; 100
Hunters ville, NC28078
Phone: [phone]
Anal ll iral Fax, 704.875.9091
www.pacelabs.com QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE: 926617820
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec
alpha-BHC
ug/l
0.1600
0.0865
54
gamma-BHC (Lindane)
ug/l
0.1600
0.0876
55
beta-BHC
ug/l
0.1600
0.1087
68
Heptachlor
ug/l
0.1600
0.0991
62
delta-BHC
ug/1
0.1600
0.0854
53
Aldrin
ug/l
0.1600
0.0848
53
Heptachlor epoxide
ug/1
0.1600
0.0949
59
Endosulfan I
ug/l
0.1600
0.1165
73
4.4'-DDE
ug/l
0.1600
0.1061
66
Dieldrin
ug/l
0.1600
0.0936
58
Endrin
ug/l
0.1600
0.0958
60
4,4'-DDD
ug/l
0.1600
0.0949
59
Endosulfan II
ug/l
0.1600
0.1022
64
4.4'-DDT
ug/l
0.1600
0.1001
63
Endrin aldehyde
ug/l
0.1600
0.0960
60
Endosulfan sulfate
ug/1
0.1600
0.0983
61
Decachlorobiphenyl (S)
42
Tetrachloro-m-xylene (S)
39
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 926586512 926586520
Parameter
gamma-BHC (Lindane)
Heptachlor
Aldrin
Dieldrin
Endrin
4.4'-DDT
Decachlorobiphenyl (S)
Tetrachloro-m-xylene (S)
Date: 02/10/06
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 92112133
Client Project ID: Outfall 001
Footnotes
926578980
Spike
MS
MSD
MS
MSD
Units
Result
Conc.
Result
Result %
Rec %
Rec
RPD
ug/l
0
0.1600
0.1224
0.1097
76
69
11
ug/1
0
0.1600
0.1283
0.1256
80
78
2
ug/l
0
0.1600
0.0966
0.0975
60
61
1
ug/l
0
0.1600
0.1160
0.1110
72
69
4
ug/l
0
0.1600
0.1658
0.1651
104
103
0
ug/l
0
0.1600
0.1458
0,1646
91
103
12
75
81
74
81
Footnotes
H S E ` 9 j Page: 9 of 32
P
Asheville Certification
REPORT OF LABORATORY ANALYSIS
NC Wastewater
40
NC Drinking Water
This report shall not be reproduced, except in full,
Sc
9030
99030
without the written consent of Pace Analytical Services, Inc.
FL NELAP
E87648
- nelac
arlotte Certification ID
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Sere Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, 100 2225 Riverside Drive
}7%'�� Huntersville, NC 26078 Asheville, NC 28804
Phone: Phone:[phone]
Fax: [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92112133
Client Project ID: Outfall 001
QC Batch: 148315 Analysis Method: EPA 8082
OC Batch Method: EPA 3535 Analysis Description: Organochlorine PCBs
Associated Lab Samples: 926579269
METHOD BLANK: 926586538
Associated Lab Samples: 926579269
Blank
Reporting
Parameter
Units
Result
Limit
Footnotes
PCB-1016
(Aroclor
1016)
ug/l
NO
1.0
PCB-1221
(Aroclor
1221)
ug/l
NO
1.0
PCB-1232
(Aroclor
1232)
ug/l
NO
1.0
PCB-1242
(Aroclor
1242)
ug/l
NO
1.0
PCB-1248
(Aroclor
1248)
ug/l
NO
1.0
PCB-1254
(Aroclor
1254)
ug/l
NO
1.0
PCB-1260
(Aroclor
1260)
ug/l
NO
1.0
Decachlorobiphenyl
(S)
%
82
LABORATORY CONTROL SAMPLE: 926586546
Parameter
PCB-1016 (Aroclor 1016)
PCB-1260 (Aroclor 1260)
Decachlorobiphenyl (S)
Date: 02/10/06
Spike LCS
Units Conc. Result
ug/l 10.00 10.50
ug/l 10.00 8.344
LCS
% Rec Footnotes
105
83
64
Asheville Certification
IDs
REPORT OF LABORATORY ANALYSIS
NC Wastewater
40
NC Drinking Water
2
This report shall not be reproduced, except in full,
Sc
903
99030
without the written consent of Pace Analytical Services, Inc.
FL NELAP
E87648
RECEIVED
S E 0ep,q Page: 10 of 32
PF1
harlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Servl Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, : '00 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
Ana 1 irtii^. a f Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
www.pacelahs.coin QUALITY CONTROL DATA
QC Batch: 147755
QC Batch Method: EPA 625 SF
Associated Lab Samples: 926579269
METHOD BLANK: 926596339
Associated Lab Samples: 926579269
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 625
Analysis Description: Extractables in Water by 625
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Benzidine
ug/l
NO
50.
Benzo(g.h,i)perylene
ug/l
NO
5.0
4-Bromophenylphenyl ether
ug/l
NO
5.0
Butylbenzylphthalate
ug/l
NO
5.0
4-Chloro-3-methylphenol
ug/l
NO
5.0
bis(2-Chloroethoxy)methane
ug/l
NO
5.0
bis(2-Chloroethyl) ether
ug/l
NO
5.0
bis(2-Chloroisopropyl) ether
ug/l
NO
5.0
2-Chloronaphthalene
ug/l
NO
5.0
4-Chlorophenylphenyl ether
ug/1
NO
5.0
Chrysene
ug/l
ND
5.0
3.3'-Dichlorobenzidine
ug/l
NO
10.
Oi-n-octylphthalate
ug/1
NO
5.0
1.2-Diphenylhydrazine
ug/l
NO
5.0
Hexachlorocyclopentadiene
ug/l
NO
10.
Isophorone
ug/1
ND
5.0
N-Nitrosodimethylamine
ug/l
ND
5.0
N-Nitrosodiphenylamine
ug/l
NO
5.0
Pentachlorophenol
ug/l
NO
25.
Phenanthrene
ug/l
NO
5.0
Pyrene
ug/l
ND
5.0
1.2.4-Trichlorobenzene
ug/l
ND
5.0
2.4,6-Trichlorophenol
ug/l
ND
5.0
Nitrobenzene-d5 (S)
It
54
2-Fluorobiphenyl (S)
%
69
Terphenyl-d14 (S)
%
82
Phenol-d5 (S)
%
27
2-Fluorophenol (S)
%
13
2.4,6-Tribromophenol (S)
%
14
1
Date: 02/10/06
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
NC Wastewater
40
NC Drinking Water
This report shall not be reproduced, except in full,
SC
9030
99030
without the written consent of Pace Analytical Services, Inc.
FL NELAP
E87648
°
Iela
Page: 11 of 32
PFR
Charlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Servi uc. Pace Analytical Services, Inc.
9800 Kincey Avenue, f 00 2225 Riverside Drive
Hunters ville, NuzaU78 Asheville, NC28804
Phone:[phone] Phone:[phone]
Anal iltiral ' Fax. [phone] Fax: [phone]
www.pacelabs.coin QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE: 926561416
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec
Benzidine
ug/1
100.00
26.49
26
Benzo(g.h.i)perylene
ug/l
50.00
36.94
74
4-Bronophenylphenyl ether
ug/l
50.00
35.40
71
Butylbenzylphthalate
ug/l
50.00
38.10
76
4-Chloro-3-methylphenol
ug/l
50.00
36.01
72
bis(2-Chloroethoxy)methane
ug/1
50.00
36.20
72
bis(2-Chloroethyl) ether
ug/l
50.00
37.37
75
bis(2-Chloroisopropyl) ether
ug/l
50.00
34.44
69
2-Chloronaphthalene
ug/l
50.00
39.07
78
4-Chlorophenylphenyl ether
ug/l
50.00
35.76
72
Chrysene
ug/l
50.00
36.65
73
3,3'-Dichlorobenzidine
ug/l
100.00
41.97
42
Di-n-octylphthalate
ug/l
50.00
37.50
75
Hexachlorocyclopentadiene
ug/l
50.00
20.43
41
Isophorone
ug/l
50.00
37.71
75
N-Nitrosodimethylamine
ug/l
50.00
23.74
48
N-Nitrosodiphenylamine
ug/l
100.00
104.5
104
Pentachlorophenol
ug/l
50.00
31.24
62
Phenanthrene
ug/l
50.00
36.78
74
Pyrene
ug/l
50.00
37.13
74
1.2,4-Trichlorobenzene
ug/l
50.00
31.19
62
2,4,6-Trichlorophenol
ug/1
50.00
37.05
74
Nitrobenzene-d5 (S)
74
2-Fluorobiphenyl (S)
74
Terphenyl-d14 (S)
79
Phenol-d5 (S)
33
2-Fluorophenol (S)
51
2,4.6-Tribromophenol (S)
85
LABORATORY CONTROL SAMPLE: 926571258
Parameter
Benzidine
Benzo(g.h,i)perylene
4-Bromophenylphenyl ether
Date: 02/10/06
Lab Project Number: 92112133
Client Project ID: Outfall 001
Footnotes
Spike
LCS
LCS
Units
Conc.
Result
X Rec Footnotes
ug/l
100.00
0
0 2
ug/l
50.00
35.19
70
ug/1
50.00
31.56
63
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 99030 This report shall not be reproduced, except in full,
Sc 903
NC Drinking Water 2 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648n0
:ol ICIQ,C
P7ECEIVF-i i
PR
Page: 12 of 32
arlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

Pace Analytical Servi 'nc.
9800 Kincey Avenue, ' '00
Huntersville, Ncztt078
Phone: [phone]
Ana /�/ I+ ir.q' Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE: 926571258
Parameter
Units
Butylbenzylphthalate
ug/l
4-Chloro-3-methylphenol
ug/l
bis(2-Chloroethoxy)methane
ug/l
bis(2-Chloroethyl) ether
ug/l
bis(2-Chloroisopropyl) ether
ug/l
2-Chloronaphthalene
ug/l
4-Chlorophenylphenyl ether
ug/l
Chrysene
ug/1
3.3'-Dichlorobenzidine
ug/l
Di-n-octylphthalate
ug/1
Hexachlorocyclopentadiene
ug/1
Isophorone
ug/l
N-Nitrosodimethylamine
ug/l
N-Nitrosodiphenylamine
ug/l
Pentachlorophenol
ug/l
Phenanthrene
ug/1
Pyrene
ug/l
1,2.4-Trichlorobenzene
ug/l
2,4,6-Trichlorophenol
ug/l
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d5 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
LABORATORY CONTROL SAMPLE: 926574732
Parameter
Benzidine
Benzo(g,h.i)perylene
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
bis(2-Chloroethoxy)methane
Date: 02/10/06
Units
ug/l
ug/l
ug/1
ug/l
ug/1
ug/l
Spike LCS
Conc. Result
50.00 33.91
50.00 32.66
50.00 29.63
50.00 26.11
50.00 25.16
50.00 26.83
50.00 30.77
50.00 31.62
100.00 31.61
50.00 33.04
50.00 19.18
50.00 30.26
50.00 18.16
50.00 40.45
50.00 33.94
50.00 31.19
50.00 31.23
50.00 23.52
50.00 30.74
Spike LCS
Conc. Result
100.00 3.988
50.00 49.37
50.00 36.38
50.00 36.97
50.00 39.28
50.00 37.96
LCS
% Rec
68
65
59
52
50
54
62
63
32
66
38
60
36
81
68
62
62
47
62
53
55
64
23
35
74
LCS
X Rec
4
99
73
74
79
76
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, N028804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 92112133
Client Project ID: Outfall 001
Footnotes
2
Footnotes
2
RECEIVED.
Asheville Certification 10s REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 99030 This report shall not be reproduced, except in full,
Sc 9030
NC Drinking Water without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648
.
nmc-
PF$
Page: 13 of 32
Charlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Servi 'nc. Pace Analytical Services, Inc.
9800 Kincey Avenue, : 00 2225 Riverside Drive
Huntersville, k cod78 Asheville, NC 28804
} Phone:[phone] Phone.[phone]
A na I V! I �, a I Fax. [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
LABORATORY CONTROL SAMPLE: 926574732
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec
bis(2-Chloroethyl) ether
ug/l
50.00
34.95
70
bis(2-Chloroisopropyl) ether
ug/l
50.00
36.19
72
2-Chloronaphthalene
ug/l
50.00
33.98
68
4-Chlorophenylphenyl ether
ug/l
50.00
38.27
76
Chrysene
ug/l
50.00
36.35
73
3.3'-Dichlorobenzidine
ug/l
100.00
35.40
35
Di-n-octylphthalate
ug/l
50.00
37.57
75
Hexachlorocyclopentadiene
ug/l
50.00
25.87
52
Isophorone
ug/l
50.00
37.93
76
N-Nitrosodimethylamine
ug/l
50.00
23.54
47
N-Nitrosodiphenylamine
ug/l
50.00
45.31
91
Pentachlorophenol
ug/l
50.00
38.65
77
Phenanthrene
ug/l
50.00
36.60
73
Pyrene
ug/l
50.00
34.45
69
1,2,4-Trichlorobenzene
ug/l
50.00
32.33
65
2.4,6-Trichlorophenol
ug/l
50.00
37.13
74
Nitrobenzene-d5 (S)
74
2-Fluorobiphenyl (S)
72
Terphenyl-d14 (S)
74
Phenol-d5 (S)
31
2-Fluorophenol (S)
47
2.4.6-Tribromophenol (S)
84
LABORATORY CONTROL SAMPLE: 926596347
Lab Project Number: 92112133
Client Project ID: Outfall 001
Footnotes
Spike
LCS LCS
Parameter
Units
Conc.
Result X Rec Footnotes
Benzidine
ug/l
100.00
65.36 65
Benzo(g.h.i)perylene
ug/1
50.00
36.91 74
4-Bromophenylphenyl ether
ug/l
50.00
43.90 88
Butylbenzylphthalate
ug/l
50.00
37.11 74
4-Chloro-3-methylphenol
ug/l
50.00
36.62 73
bis(2-Chloroethoxy)methane
ug/l
50.00
36.66 73
bis(2-Chloroethyl) ether
ug/l
50.00
13.09 26
RECEIVED
bis(2-Chloroisopropyl) ether
ug/l
50.00
33.69 67
2-Chloronaphthalene
ug/l
50.00
43.79 88
r
4SE0up�
Date: 02/10/06
PRPage: 31
of 32
Asheville Certification IN
REPORT OF
LABORATORY ANALYSIS
Charlotte Certification
IDs
NC Wastewater 40
NC Wastewater
12
NC Drinking Water 37712
This report shall not be reproduced, except in full,
NC Drinking Water
37706
SC 99030
without the written
consent of Pace Analytical Services, Inc.
Sc
99006
FL NELAP E87648
,<o,o
�y ..
1 Imc t
FL NELAP
E87627

Pace Analytical Servi, 1c. Pace Analytical Services, Inc.
9800 Kincey Avenue, S 00 2225 Riverside Drive
Huntersville, No cau78 Asheville, NC 28804
,} Phone.[phone] Phone.,828.254.7176
A na I V 1 I �. a' Fax. [phone] Fax., 828.252.4618
www.pacelabs.corn QUALITY CONTROL DATA
Lab Project Number: 92112133
Client Project ID: Outfall 001
LABORATORY CONTROL SAMPLE: 926596347
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec Footnotes
4-Chlorophenylphenyl ether
ug/l
50.00
41.59
83
Chrysene
ug/l
50.00
41.84
84
3,3'-Oichlorobenzidine
ug/l
100.00
50.93
51
Di-n-octylphthalate
ug/l
50.00
35.66
71
Hexachlorocyclopentadiene
ug/l
50.00
21.87
44
Isophorone
ug/l
50.00
37.95
76
N-Nitrosodimethylamine
ug/l
50.00
23.05
46
N-Nitrosodiphenylamine
ug/l
100.00
98.19
98
Pentachlorophenol
ug/l
50.00
20.15
40
Phenanthrene
ug/l
50.00
42.38
85
Pyrene
ug/l
50.00
42.18
84
1.2.4-Trichlorobenzene
ug/l
50.00
33.06
66
2.4,6-Trichlorophenol
ug/l
50.00
12.08
24 2
Nitrobenzene-d5 (S)
68
2-Fluorobiphenyl (S)
80
Terphenyl-d14 (S)
84
Phenol-d5 (S)
33
2-Fluorophenol (S)
43
2,4,6-Tribromophenol (S)
38
LABORATORY CONTROL SAMPLE: 926607029
Spike
LCS LCS
Parameter
Units
Conc.
Result X Rec Footnotes
Benzidine
ug/l
100.00
0 0 2
Benzo(g.h,i)perylene
ug/l
50.00
36.60 73
4-Bromophenylphenyl ether
ug/l
50.00
26.80 54
Butylbenzylphthalate
ug/l
50.00
26.94 54
4-Chloro-3-methylphenol
ug/l
50.00
25.60 51
bis(2-Chloroethoxy)methane
ug/l
50.00
23.23 46
bis(2-Chloroethyl) ether
ug/l
50.00
21.81 44
bis(2-Chloroisopropyl) ether
ug/l
50.00
21.60 43
2-Chloronaphthalene
ug/l
50.00
22.93 46 2 RECEIVED
ether
ug/l
50.00
25.86 52
Chrysene
ug/l
50.00
25.62 51
3.3'-Dichlorobenzidine
ug/l
100.00
7.419 7
H S ECI)r
Date: 02/10/06
gQp
PF11 Page: 15
of 32
Asheville Certification IN
REPORT OF
LABORATORY ANALYSIS Charlotte Certification
IN
INC Wastewater 40
NC Wastewater
12
NC Drinking Water 2NC
This report shall breproduced,i anot except n full,
Drinking Water
37706
9903
without the written
consent of Pace Analytical Services, Inc.
Sc
99006
FL E8764
FL NELAP 87648
„ o,,,
FL NELAP
E87627
„ ^

Pace Analytical Servi Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, ; t00 2225 Riverside Drive
Huntersville, Nu zvJ78 Asheville, NC 28804
Phone.,704.875.9092 Phone.[phone]
Analytical Fax., 704.875.9091 Fax., 828.252.4618
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92112133
Client Project ID: Outfall 001
LABORATORY CONTROL SAMPLE: 926607029
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec Footnotes
Di-n-octylphthalate
ug/l
50.00
27.61
55
Hexachlorocyclopentadiene
ug/l
50.00
18.25
36
Isophorone
ug/l
50.00
23.89
48
N-Nitrosodimethylamine
ug/l
50.00
13.91
28
N-Nitrosodiphenylamine
ug/l
50.00
8.464
17 2
Pentachlorophenol
ug/l
50.00
24.55
49
Phenanthrene
ug/l
50.00
27.94
56
Pyrene
ug/l
50.00
27.36
55
1.2,4-Trichlorobenzene
ug/l
50.00
20.70
41 2
2.4.6-Trichlorophenol
ug/l
50.00
24.65
49
Nitrobenzene-d5 (S)
48
2-Fluorobiphenyl (S)
50
Terphenyl-d14 (S)
56
Phenol-d5 (S)
20
2-Fluorophenol (S)
31
2.4.6-Tribromophenol (S)
62
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 926571266 926571274
926569799
Spike
MS
MSD MS
MSD
Parameter
Units
Result
Conc.
Result
Result X Rec %
Rec
RPD Footnotes
Benzidine
ug/l
0
200.00
0
0 0
0
0 2.2
Benzo(g.h,i)perylene
ug/l
0
100.00
62.15
67.96 62
68
9
4-Bromophenylphenyl ether
ug/l
0
100.00
57.31
63.03 57
63
10
Butylbenzylphthalate
ug/l
0
100.00
59.01
63.68 59
64
8
4-Chloro-3-methylphenol
ug/l
0
100.00
60.92
70.13 61
70
14
bis(2-Chloroethoxy)methane
ug/l
0
100.00
53.74
61.80 54
62
14
bis(2-Chloroethyl) ether
ug/1
0
100.00
41.64
48.25 42
48
15
bis(2-Chloroisopropyl) ether
ug/1
0
100.00
38.99
45.68 39
46
16
2-Chloronaphthalene
ug/l
0
100.00
50.44
53.69 50
54
6 2.2
4-Chlorophenylphenyl ether
ug/l
0
100.00
56.63
61.34 57
61
8
Chrysene
ug/l
0
100.00
57.07
60.58 57
61
6
3.3'-Dichlorobenzidine
ug/l
0
100.00
21.07
15.35 21
15
31 3
Di-n-octylphthalate
ug/l
0
100.00
56.84
59.37 57
59
4
Hexachlorocyclopentadiene
ug/T
0
100.00
36.45
38.49 36
38
5
Isophorone
ug/l
0
100.00
53.63
61.jgECMVE(g,
6'�
11
13
Date: 02/10/06
Page: 16 of 72
7 1 L oup
Qi�pil
Asheville Certification IDs
REPORT OF
LABORATORY ANALYSIS
Charlotte Certification
IN
NC Wastewater 40
NC Wastewater
12
NC Drinking Water
This report shall not be reproduced, except in full,
NC Drinking Water
06
Sc 9030
99030
without the written
consent of Pace
Analytical
Services, Inc.
SC
99006
990
FL NELAP E87648
y°�. °"°�
FL NELAP
E87627

Pace Analytical Servi 'nc. Pace Analytical Services, Inc.
9800 Kincey Avenue, f 00 2225 Riverside Drive
Huntersville, 16�cod78 Asheville, NC28804
Ana 1 vtir, 1 Phone: [phone] Phone: [phone]
Far.- 704.875.9091 Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92112133
Client Project ID: Outfall 001
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 926571266 926571274
926569799
Spike
MS
MSD
MS
MSD
Parameter
Units
Result
Conc.
Result
Result
X Rec %
Rec
RPD Footnotes
N-Nitrosodimethylamine
ug/l
0
100.00
34.89
40.49
35
40
15
N-Nitrosodiphenylamine
ug/l
0
100.00
72.06
78.02
72
78
8
Pentachlorophenol
ug/l
0
100.00
63.49
75.80
64
76
18
Phenanthrene
ug/l
0
100.00
56.59
60.86
57
61
7
Pyrene
ug/l
0
100.00
55.66
61.51
56
62
10
1,2.4-Trichlorobenzene
ug/l
0
100.00
40.44
42.92
40
43
6 2.2
2.4,6-Trichlorophenol
ug/1
0
100.00
61.91
68.59
62
69
10
Nitrobenzene-d5 (S)
46
52
2-Fluorobiphenyl (S)
52
56
Terphenyl-d14 (S)
57
63
Phenol-d5 (S)
23
26
2-Fluorophenol (S)
31
36
2,4,6-Tribromophenol (S)
67
74
Date: 02/10/06
Page: 17 of 32
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
Charlotte Certification
IN
NC Wastewater 40
NC Wastewater
12
NC Drinking Water 37712
This report shall not be reproduced, except in full,
NC Drinking Water
37706
Sc 99030
tic Pace Anal t t the
written consent of Payal Services, Inc.
Sc
99006
FL NELAP E87648
. y.
"o m
FL NELAP
E87627

Pace Analytical Servic ic. Pace Analytical Services, Inc.
9800 Kincey Avenue, Si 10 2225 Riverside Drive
Hunfersville, NG eou78 Asheville, NC 28804
Anall/1iral° Phone:[phone] Phone:[phone]
Fax: [phone] Fax., 828.252.4618
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92112133
Client Project ID: Outfall 001
QC Batch: 148560 Analysis Method: EPA 624
QC Batch Method: EPA 624 Analysis Description: Volatile GC/MS by 624
Associated Lab Samples: 926579269
METHOD BLANK: 926596313
Associated Lab Samples: 926579269
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Acrolein
ug/l
NO
25.
Bromodichloromethane
ug/l
NO
5.0
Bromoform
ug/l
NO
5.0
Bromomethane
ug/l
NO
5.0
2-Chloroethylvinyl ether
ug/l
NO
10.
Oichlorodifluoromethane
ug/l
NO
5.0
1,1,1,2-Tetrachloroethane
ug/l
NO
5.0
Trichlorofluoromethane
ug/l
NO
5.0
Toluene-d8 (S)
X
99
4-Bromofluorobenzene (S)
%
102
Dibromofluoromethane (S)
%
96
LABORATORY CONTROL SAMPLE: 926596321
Spike
LCS LCS
Parameter
Units
Conc.
Result X Rec Footnotes
Bromodichloromethane
ug/l
20.00
18.81 94
Bromoform
ug/1
20.00
18.74 94
Bromomethane
ug/1
20.00
30.84 154
2-Chloroethylvinyl ether
ug/l
20.00
25.79 129
Trichlorofluoromethane
ug/l
20.00
22.13 ill
Toluene-d8 (S)
99
4-Bromofluorobenzene (S)
102
Dibromofluoromethane (S)
96
Date: 02/10/06
Asheville Certification IDs
REPORT OF
LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water
This report shall not be reproduced, except in full,
99030
SC 9030
without the written
consent of Pace Analytical Services, Inc.
FL NELAP E87648
1 IQQ,C
RECEA/F
l"Y S E I c-IL,
'PF1 Page: 18 of 32
harlotte Certification ID
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

Pace Analytical Servic-- '-c. Pace Analytical Services, Inc.
9800 Kincey Avenue, Si 10 2225 Riverside Drive
Huntersville, NL ....8 Asheville, NC 28804
Anall/tical ° Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
OC Batch: 148154
OC Batch Method: EPA 7470
Associated Lab Samples: 926579269
METHOD BLANK: 926580051
Associated Lab Samples: 926579269
Parameter Units
Mercury mg/l
LABORATORY CONTROL SAMPLE: 926580069
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 7470
Analysis Description: Mercury, CVAAS, in Water
Blank Reporting
Result Limit Footnotes
ND 0.0002
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Mercury mg/l 0.0025 0.0027 106
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 926580077 926580085
926578980 Spike MS MSD MS MSO
Parameter Units Result Conc. Result Result X Rec X Rec RPO Footnotes
Mercury mg/l 0.00006 0.0025 0.0025 0.0025 99 99 0
Date: 02/10/06
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 NC Drinking Water 37712 This report shall not be reproduced, except in full,
Sc 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 .,�14,
5 1 Imc
RECEIVED
Page: 19 of 32
S f 0,''w
PF1
Charlotte Certification IN
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

Pace Analytical Servii ic.
9800 Kincey Avenue, S 90
Huntersville, Nl, eou78
�Phone: [phone]
4 n. W i/ II ir,71 Fax. [phone]
www. pacelabs. coin QUALITY CONTROL DATA
QC Batch: 148224
QC Batch Method:
Associated Lab Samples: 926579269
METHOD BLANK: 926582396
Associated Lab Samples: 926579269
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC26804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 200.7
Analysis Description: Trace ICP Metals
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Aluminum
mg/1
NO
0.10
Antimony
mg/l
NO
0,0050
Arsenic
mg/l
NO
0.0050
Barium
mg/1
NO
-0.0050
Beryllium
mg/1
NO
0.0010
Boron
mg/l
NO
0.010
Cadmium
mg/l
NO
0.0010
Chromium
mg/1
NO
0.0020
Copper
mg/1
NO
0.0020
Iron
mg/l
NO
0.050
Lead
mg/l
NO
0.0050
Magnesium
mg/l
NO
0.10
Manganese
mg/l
NO
0.0050
Molybdenum
mg/l
NO
0.0050
Nickel
mg/l
NO
0.0050
Selenium
mg/l
NO
0.0050
Silver
mg/l
NO
0.0020
Thallium
mg/l
NO
0.010
Zinc
mg/l
NO
0.010
LABORATORY CONTROL SAMPLE: 926582404
Spike
1-CS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
Aluminum
mg/l
5.000
5.080
102
Antimony
mg/l
0.5000
0.5040
101
Arsenic
mg/l
0.5000
0.4930
99
Barium
mg/1
0.5000
0.4980
100
Beryllium
mg/1
0.5000
0.4990
100
Boron
mg/l
0.5000
0.4920
98
Date: 02/10/06
RECEIVED
rH eS. E 09 p
P9
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 99030 This report shall not be reproduced, except in full,
SC 903
NC Drinking Water 2 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648
SAC
Page: 20 of 32
Charlotte Certification IN
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

,
aceAnalytical`"
www.pacelabs.com
LABORATORY CONTROL SAMPLE: 926582404
Pace Analytical Servii- '7c.
9800 Kincey Avenue, S 00
Huntersville, No 4ou78
Phone: [phone]
Fax., 704.875.9091
QUALITY CONTROL DATA
Spike
LCS
LCS
Parameter
Units
Conc.
Result
X Rec
Cadmium
mg/l
0.5000
0.5000
100
Chromium
mg/l
0.5000
0.5160
103
Copper
mg/l
0.5000
0.5050
101
Iron
mg/1
5.000
5.080
102
Lead
mg/1
0.5000
0.5000
100
Magnesium
mg/l
5.000
5.020
100
Manganese
mg/l
0.5000
0.5070
101
Molybdenum
mg/l
0.5000
0.5120
102
Nickel
mg/l
0.5000
0.4950
99
Selenium
mg/l
0.5000
0.4930
99
Silver
mg/1
0.2500
0.2480
99
Thallium
mg/1
0.5000
0.4770
95
Zinc
mg/l
0.5000
0.5520
110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 926582412 926582420
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Footnotes
RECEIVED
PF�
926576752
Spike
MS
MSO
MS
MSD
Parameter
Units
Result
Conc.
Result
Result X
Rec X
Rec
RPD Footnotes
Aluminum
mg/1
0.03150
5.000
5.230
4.570
104
91
13
Antimony
mg/l
0.00071
0.5000
0.5050
0.4430
101
88
13
Arsenic
mg/1
0
0.5000
0.4960
0.4350
99
87
13
Barium
mg/1
0.00411
0.5000
0.4980
0.4380
99
87
13
Beryllium
mg/1
0.00006
0.5000
0.4930
0.4420
99
88
11
Boron
mg/l
0.1190
0.5000
0.6200
0.5630
100
89
10
Cadmium
mg/l
0.00007
0.5000
0.4960
0.4370
99
87
13
Chromium
mg/l
0
0.5000
0.5100
0.4500
102
90
12
Copper
mg/l
0.00665
0.5000
0.5150
0.4540
102
90
13
Iron
mg/l
0.05610
5.000
5.080
4.490
100
89
12
Lead
mg/l
0.00367
0.5000
0.5010
0.4440
100
88
12
Magnesium
mg/l
2.030
5.000
7.110
6.500
102
89
9
Manganese
mg/l
0.00257
0.5000
0.5040
0.4450
100
88
12
Molybdenum
mg/l
0.00883
0.5000
0.5200
0.4620
102
91
12
Nickel
mg/l
0.00991
0.5000
0.5010
0.4430
98
87
12
Selenium
mg/l
0.00102
0.5000
0.4910
0.4330
98
86
13
Silver
mg/l
0
0.2500
0.2500
0.2210
100
88
12
Thallium
mg/1
0.00240
0.5000
0.4950
0.4330
98
86
13
Date: 02/10/06
Page: 21 of 32
Asheville Certification
ID s
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IDs
NC Wastewater
40
NC Wastewater
12
NC Drinking Water
This report shall not be reproduced, except in full,
NC Drinking Water
06
Sc
99030
99030
without the written consent of Pace Analytical Services, Inc.
SC
990
99006
FL NELAP
E87648
FL NELAP
E87627

Pace Analytical Servic-- '-c. Pace Analytical Services, Inc.
9800 Kincey Avenue, Si 10 2225 Riverside Drive
Huntersville, Nit, —, 8 Asheville, NC 28804
Phone:[phone] Phone:[phone]
Anal vtir, al �' Fax: [phone] Fax., 828.252.4618
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92112133
Client Project ID: Outfall 001
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 926582412 926582420
926576752 Spike MS MSO MS MSD
Parameter Units Result Conc. Result Result % Rec % Rec RPD Footnotes
Zinc mg/l 0.04880 0.5000 0.5730 0.5130 105 93 11
SAMPLE DUPLICATE: 926582438
926576760
DUP
Parameter
Units
Result
Result
RPD Footnotes
Aluminum
mg/l
1.800
1.800
2
Antimony
mg/l
ND
NO
NC
Arsenic
mg/l
NO
NO
NC
Barium
mg/1
0.06600
0.06500
2
Beryllium
mg/l
NO
ND
NC
Boron
mg/l
0.1200
0.1200
0
Cadmium
mg/1
NO
ND
NC
Chromium
mg/l
0.00340
0.00320
7
Copper
mg/l
0.05300
0.05100
3
Iron
mg/l
2.100
2.000
6
Lead
mg/l
0.00820
0.00700
17
Magnesium
mg/l
2.300
2.300
1
Manganese
mg/1
0.1400
0.1400
1
Molybdenum
mg/l
0.01200
0.01200
2
Nickel
mg/1
0.02800
0.02700
6
Selenium
mg/l
NO
ND
NC
Silver
mg/l
0.00410
0.00410
0
Thallium
mg/l
ND
ND
NC
Zinc
mg/l
0.1400
0.1300
4
Date: 02/10/O6
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 99030 This report shall not be reproduced, except in full,
SC 9030
NC Drinking Water without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 yy A
}� F- uep3 t
9R
Page: 22 of 32
Charlotte Certification ID
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

=aceAnalytical
www.pacelabs.com
QC Batch: 148145
QC Batch Method: EPA 340.2
Associated Lab Samples: 926579269
METHOD BLANK: 926579749
Associated Lab Samples: 926579269
Parameter Units
Fluoride mg/l
LABORATORY CONTROL SAMPLE: 926579756
Pace Analytical Service 1-^.
Pace Analytical Services, Inc.
9800 Kincey Avenue, Su. 9
2225 Riverside Drive
Huntersville, NC _--, 3
Asheville, NC 28804
Phone: [phone]
Phone., 828.254,7176
Fax: 704,875.9091
Fax., 828.252.4618
QUALITY CONTROL DATA
Lab Project Number: 92112133
Client Project IO: Outfall 001
Analysis Method: EPA 340.2
Analysis Description: Fluoride
Blank Reporting
Result Limit Footnotes
NO 0.10
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Fluoride mg/l 2.500 2.610 104
MATRIX SPIKE: 926579764
926576216 Spike MS MS
Parameter Units Result Conc. Result X Rec Footnotes
Fluoride mg/l 1.430 2.500 3.960 101
SAMPLE DUPLICATE: 926579772
Parameter Units
Fluoride mg/l
Date: 02/10/06
926576240 DUP
Result Result RPD Footnotes
1.200 1.100 9
Asheville Certification
IN
REPORT OF LABORATORY ANALYSIS
NC Wastewater
40
NC Drinking Water
This report shall not be reproduced, except in full,
SC
99030
9030
without the written consent of Pace Analytical Services, Inc.
FL NELAP
E87648
-nelaC
RECE IEL
9Ff
Page: 23 of 32
harlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

aceAnalytical
www.pacelabs.com
QC Batch: 148233
QC Batch Method: EPA 353.2
Associated Lab Samples: 926579269
METHOD BLANK: 926583279
Associated Lab Samples: 926579269
Parameter Units
Nitrate -Nitrite (as N) mg/l
LABORATORY CONTROL SAMPLE: 926583287
Parameter Units
Nitrate -Nitrite (as N) mg/l
MATRIX SPIKE: 926583295
Pace Analytical Service- '^^ Pace Analytical Services, Inc.
9800 Kincey Avenue, Su, ) 2225 Riverside Drive
Huntersville, NC.,3 Asheville, NC28804
Phone:[phone] Phone:[phone]
Fax., 704.875.9091 Fax: [phone]
QUALITY CONTROL DATA
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 353.2
Analysis Description: 28 day NOX
81ank Reporting
Result Limit Footnotes
ND 0.10
Spike LCS LCS
Conc. Result X Rec Footnotes
5.000 5.230 105
926552878 Spike MS MS
Parameter Units Result Conc. Result % Rec Footnotes
Nitrate -Nitrite (as N) mg/l 0 5.000 5.160 103
SAMPLE DUPLICATE: 926583303
Parameter Units
Nitrate -Nitrite (as N) mg/l
Date: 02/10/06
926557570 DUP
Result Result RPD Footnotes
8.700 8.700 0
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 NC Drinking Water This report shall not be reproduced, except in full, Sc 990309030 without the written consent of Pace Analytical Services, Inc.
FLNELAP E87648
1 Ia�IC
RECE EE,,
14 G E0C3p'
PFI1
Page: 24 of 32
rlotte Certification ID
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

PaceAnalytical"
www.pacefabs.com
QC Batch: 148256
QC Batch Method: EPA 375.4
Associated Lab Samples: 926579269
METHOD BLANK: 926585019
Associated Lab Samples: 926579269
Parameter Units
Sulfate mg/l
LABORATORY CONTROL SAMPLE: 926585027
Pace Analytical Service- •_
Pace Analytical Services, Inc.
9800 Kincey Avenue, Sui 7
2225 Riverside Drive
Huntersville, NCcourd
Asheville, NC26804
Phone:[phone]
Phone.,828.254.7176
Fax., 704.875.9091
Fax: [phone]
QUALITY CONTROL DATA
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 375.4
Analysis Description: Sulfate,Turbidimetric
Blank Reporting
Result Limit Footnotes
NO 5.0
Spike LCS 1-CS
Parameter Units Conc. Result % Rec Footnotes
Sulfate mg/l 20.00 20.68 103
MATRIX SPIKE: 926585043
926578980 Spike MS MS
Parameter Units Result Conc. Result k Rec Footnotes
Sulfate mg/1 919.5 20.00 917.5 0 4
SAMPLE DUPLICATE: 926585035
Parameter Units
Sulfate mg/l
Date: 02/10/06
926578980 DUP
Result Result RPD Footnotes
920.0 920.0 0
Asheville Certification REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 99030 This report shall not be reproduced, except in full,
SC 9030
NC Drinking Water without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 MM" "
:�`I IC.7QC
RECOVED!
Page: 25 of 32
Charlotte Certificatio
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Servicr Pace Analytical Services, Inc.
9800 Kincey Avenue, Su 0 2225 Riverside Drive
Huntersville, NC zbru18 Asheville, NC 28804
Anali�tiral p Phone:[phone] Phone:[phone]
Fax., 704.875.9091 Fax [phone]
www.pacelahs.com QUALITY CONTROL DATA
QC Batch: 148280
QC Batch Method: EPA 351.2
Associated Lab Samples: 926579269
METH00 BLANK: 926585399
Associated Lab Samples: 926579269
Parameter Units
Nitrogen, Kjeldahl. Total mg/l
LABORATORY CONTROL SAMPLE: 926585407
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 351.2
Analysis Description: Total Kjeldahl Nitrogen
Blank Reporting
Result Limit Footnotes
NO 0.50
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Nitrogen, Kjeldahl, Total mg/1 10.00 8.410 84
MATRIX SPIKE: 926585415
926578360 Spike MS MS
Parameter Units Result Conc. Result it Rec Footnotes
Nitrogen. Kjeldahl, Total mg/l 1.120 10.00 9.020 79
SAMPLE DUPLICATE: 926585423
Parameter Units
Nitrogen, Kjeldahl, Total mg/l
Date: 02/10/06
926575853 DUP
Result Result RPD Footnotes
2.700 2.700 2
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
NC Wastewater
40
NC Drinking Water
This report shall not be reproduced, except in full,
SC
9030
99030
without the written consent of Pace Analytical Services, Inc.
FL NELAP
E87648
°"°•
RECBVF�'
H 8 E Depj
IPFQ
Page: 26 of 32
rlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Servia 1. Pace Analytical Services, Inc.
9800 Kincey Avenue, Su 0 2225 Riverside Drive
Huntersville, NC28078 Asheville, NC28804
Ana 1 i�tir, a 1 Phone: [phone] Phone: [phone]
Fax: [phone] Fax., 828.252.4618
www.pacelabs.com QUALITY CONTROL DATA
QC Batch: 148287
QC Batch Method: EPA 410.4
Associated Lab Samples: 926579269
METHOD BLANK: 926585639
Associated Lab Samples: 926579269
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 410.4
Analysis Description: Chemical Oxygen Demand
Blank Reporting
Parameter Units Result Limit Footnotes
Chemical Oxygen Demand mg/l ND 25.
LABORATORY CONTROL SAMPLE: 926585647
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Chemical Oxygen Demand mg/l 750.00 786.0 105
MATRIX SPIKE: 926585993
926579269 Spike MS MS
Parameter Units Result Conc. Result % Rec Footnotes
Chemical Oxygen Demand mg/l 93.00 750.00 933.0 112
SAMPLE DUPLICATE: 926586009
Parameter Units
Chemical Oxygen Demand mg/l
Date: 02/10/06
926579285 DUP
Result Result RPD Footnotes
77.00 66.00 15
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
NC Wastewater
40
NC Drinking Water
2
This report shall not be reproduced, except in full,
SC
99030
903
without the written consent of Pace Analytical Services, Inc.
FL NELAP
E87648
ACC°"
mehel
RECEIVED
UPI 8 E DE>pf
Pr
Page: 27 of 32
tte Certification ID
NC Wastewater
12
NC Drinking Water
37706
sc
99006
FL NELAP
E87627

-�-PdceAna1ytica1
www.pacelabs.com
QC Batch: 148396
OC Batch Method: EPA 350.1
Associated Lab Samples: 926579269
METHOD BLANK: 926591017
Associated Lab Samples: 926579269
Parameter Units
Nitrogen. Ammonia mg/l
LABORATORY CONTROL SAMPLE: 926591025
Parameter Units
Nitrogen, Ammonia mg/l
MATRIX SPIKE: 926591033
Pace Analytical Servlcr 4 Pace Analytical Services, Inc.
9800 Kincey Avenue, Su 0 2225 Riverside Drive
Huntersville, NC28078 Asheville, NC28804
Phone.,704.875.9092 Phone:828,254.7176
Fax: [phone] Fax: [phone]
QUALITY CONTROL DATA
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 350.1
Analysis Description: Ammonia
Blank Reporting
Result Limit Footnotes
NO 0.10
Spike LCS LCS
Conc. Result X Rec Footnotes
1.000 1.065 107
926578360
Spike
MS
MS
Parameter
Units
Result
Conc.
Result
% Rec Footnotes
Nitrogen. Ammonia
mg/l
0.1730
1.000
0.9730
80
SAMPLE DUPLICATE: 926591041
926578550
DUP
Parameter
Units
Result
Result
RPD
Footnotes
Nitrogen. Ammonia
mg/l
0.1900
0.1900
1
Date: 02/10/06
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712 Sc 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 „�
:Ile._
RECEI Et,
Page: 29 of 32
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

aceAnalytical
www. pacelahs. corn
QC Batch: 148416
QC Batch Method: SM 5310B
Associated Lab Samples: 926579269
METHOD BLANK: 926592049
Associated Lab Samples: 926579269
Parameter Units
Total Organic Carbon mg/l
LABORATORY CONTROL SAMPLE: 926592056
Pace Analytical Servic C.
Pace Analytical Services, Inc.
9800 Kincey Avenue, Si 10
2225 Riverside Drive
Hunters ville, NC 28078
Asheville, NC 28804
Phone:[phone]
Phone.[phone]
Fax: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: SM 5310B
Analysis Description: Total Organic Carbon
Blank Reporting
Result Limit Footnotes
NO 1.0
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Total Organic Carbon mg/1 10.00 9.440 94
MATRIX SPIKE: 926592064
926557349 Spike MS MS
Parameter Units Result Conc. Result x Rec Footnotes
Total Organic Carbon mg/1 23.03 40.00 52.20 73
SAMPLE DUPLICATE: 926592072
Parameter Units
Total Organic Carbon mg/l
Date: 02/10/06
926557364 DUP
Result Result RPD Footnotes
20.00 25.00 19
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 99030 This report shall not be reproduced, except in full,
SC 903
NC Drinking Water 2 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648
a. ._RYA 4
H3EDepu:
PAP
Page: 29 of 32
Charlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Servic ic. Pace Analytical Services, Inc.
9800 Kincey Avenue, Si 70 2225 Riverside Drive
Huntersville, NC 28078 Asheville, NC 28804
Analytical Phone: [phone] Phone: [phone]
Fax., 704.875.9091 Fax: [phone]
www.pacelabs.corn QUALITY CONTROL DATA
Lab Project Number: 92112133
Client Project ID: Outfall 001
QC Batch: 148641 Analysis Method: EPA 335.2
QC Batch Method: EPA 335.2 Analysis Description: Cyanide, Total, Water
Associated Lab Samples: 926579269
METHOD BLANK: 926597394
Associated Lab Samples: 926579269
Blank Reporting
Parameter Units Result Limit Footnotes
Cyanide mg/l NO 0.0050
LABORATORY CONTROL SAMPLE: 926597402
Spike LCS LCS
Parameter Units Conc. Result % Rec Footnotes
Cyanide mg/l 0.1000 0.0930 93
MATRIX SPIKE: 926597444
926588393
Spike
MS
MS
Parameter
Units
Result
Conc.
Result
% Rec Footnotes
Cyanide
mg/l
0
0.1000
0.0950
95
SAMPLE DUPLICATE: 926597451
926588401
DUP
Parameter
Units
Result
Result
RPD
Footnotes
Cyanide
mg/l
NO
NO
NC
Date: 02/10/06
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 99030 This report shall not be reproduced, except in full,
Sc 903
NC Drinking Water 2 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 All,"
:„
of Imc
RECEIVEP
HSEDGps
ap;
Page: 30 of 32
harlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Servic ic. Pace Analytical Services, Inc.
9800 Kincey Avenue, SL.._ .70 2225 Riverside Drive
Huntersville, NC28078 Asheville, NC28804
Phone:[phone] Phone:[phone]
Analvtiral " Fax:[phone] Fax.,828,252.4618
www.pacelabs.coin QUALITY CONTROL DATA
QC Batch: 148688
QC Batch Method: EPA 420.2
Associated Lab Samples: 926579269
METHOD BLANK: 926598798
Associated Lab Samples: 926579269
Parameter Units
Phenolics. Total Recoverable mg/l
LABORATORY CONTROL SAMPLE: 926598806
Lab Project Number: 92112133
Client Project ID: Outfall 001
Analysis Method: EPA 420.2
Analysis Description: Phenolics, Total Recoverable
Blank Reporting
Result Limit Footnotes
NO 0.010
Spike
LCS
Parameter
Units
Conc.
Result
Phenolics, Total Recoverable
mg/l
0.1000
0.0960
MATRIX SPIKE: 926598814
926564253
Spike
Parameter
Units
Result
Conc.
Phenolics. Total Recoverable
mg/l
0.01910
0.1000
SAMPLE DUPLICATE: 926598822
Parameter Units
Phenolics, Total Recoverable mg/l
Date: 02/10/06
LCS
X Rec Footnotes
96
MS MS
Result % Rec Footnotes
0.1038 85
926565078 DUP
Result Result RPD Footnotes
1.400 1.400 0
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 99030 This report shall not be reproduced, except in full,
SC 9030
NC Drinking Water without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 ►ry, °°°° °
sol IG.�.
PR
Page: 31 of 32
harlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

aceAnalytical(")
www. pacelahs. corn
QUALITY CONTROL DATA PARAMETER FOOTNOTES
Pace Analytical Servir 1c.
9800 Kincey Avenue, S_.__ .30
Huntersville, NC28078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NO 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112133
Client Project ID: Outfall 001
Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate X Rec and RPD values.
LCS(D) Laboratory Control Sample (Duplicate)
MS(D) Matrix Spike (Duplicate)
DUP Sample Duplicate
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
RPD Relative Percent Difference
(S) Surrogate
Ell Acid surrogate recovery outside of control limits. The data was accepted based on valid recovery of the two
remaining acid surrogates.
[21 The surrogate and/or spike recovery was outside acceptance limits.
[31 RPD value was outside control limits, however both percent recoveries were acceptable. Sample results for the
QC batch were accepted based on percent recoveries and completeness of QC data.
[41 The spike recovery was outside acceptance limits for the MS and /or MSD due to matrix interference. The LCS
and/or LCSD were within acceptance limits showing that the laboratory is in control and the data is
acceptable.
REGEW---
PCB
Date. 02/10/06 Page: 32 of 32
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
Charlotte Certification IDs
NC Wastewater
40
NC Wastewater
12
NC DrinkingWater
37712
This report shall not be reproduced, except in full,
NC Drinking Water
06
SC
99030
without the written consent of Pace Analytical Services, Inc.
Sc
9006
990
FL NELAP
E87648
°4.
FL NELAP
E87627
K
I eac

aceAnalytical°
Waltz Mill Laboratory
February 10, 2006
Ms. Kate Knauff
Pace Analytical Services, Inc
9600 Kincey Ave
Suite 100
Huntersville, NC 28047
Wastewater Characterization
92112133, Performance Fibers; Charlotte Laboratory
Pace Project No. 06-0597
Dear Ms. Knauff:
Pace Analytical Services, Inc.
Exit 54,1-70
Madison, PA 15663
Phone: [phone]
Fax: [phone]
www.pacelabs.com
Enclosed are analytical results for the sample submitted by Pace Analytical
Services, Inc. The sample was received on January 27, 2006 and logged in for
analysis on February 2, 2006.
Methods used are indicated on the attached data table. Appropriate quality
assurance/quality control analyses were performed in accordance with Pace, Waltz
Mill Site Quality Assurance Plan. The results reported in this project meet the
requirements as specified in Chapter 5 of the NELAC Standards. Any deviations
or discrepancies from the NELAC standards are documented in the case
narrative(s) of this report. If you have any questions, please call me at
724-722-.5219.
Sinc y,
i�
Richard M. Kinne
Radiochemistry Laboratory Supervisor
RMK: jac
Enclosures
RECEIVED
j' REPORT OF LABORATORY ANALYSIS
Page 1 of This report shall not be reproduced, except in full,
g without the written consent of Pace Analytical Services, Inc.l'

I
PACE ANALYTICAL SERVICES, INC.
CASE NARRATIVE
I. PROJECT LOGIN INFORMATION:
A: PROJECT NUMBERS:
PACE: 06-0597
CLIENT: 92112133, Performance Fibers
B: SAMPLE IDENTIFICATIONS:
PACE: 0601-1666
CLIENT: Outfall 001
C: SHIPPING/RECEIVING COMMENTS:
Final Report 02/10/06.
II. PREPARATION/ANALYSIS COMMENTS:
A: RADIOLOGICAL:
NONE
III. GENERAL COMMENTS:
Trailing zeroes and decimal places appearing on the data should not
be interpreted as precision of the analytical procedure but rather
as a result of reporting format.
Sample(s) analyzed and reported on an as -received basis.
RECEIVED-
4 S E Dopif
0600002 Pao

0
0
c�
Table 1
General Data Table
WPace Analytical Services, Inc.
Pace Project No. 06-0597
Wastewater Characterization; 92112133, Performance Fibers
Parameter Identification
Gross Beta
EPA 900.0
Pace Client Date pCi/L
Sample ID Sample ID Collected Analyzed Act + Unc (MDC)
0601-1666 Outfall 001 (1/24/06) 02/07/06 8.62 ± 2,02 (1.65)
0601-1667 Method Blank (1/27/06) 02/08/06 0.046 ± 0.753 (1.78)
Act=Activity, Unc=2 sigma Uncertainty and (MDC)=the associated Minimum
Detectable Concentration.
RECOVER)
H S E 'bap'
pew

E
rochem
EnvironmentaI. Chemists, Inc.
6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE 994. DIS CERTIFICATE #37729
Customer:
PACE ANALYTICAL SERVICES, INC.
2225 Riverside Drive
Asheville, NC 28804
Ann: Kate Knauff
REPORT OF ANALYSIS
Date Sampled: 01/24/06
Sampled By: Client
111 14 10Idl► h1:7:N-C".
Date of Report: February 2, 2006
Purchase Order #: 92112133
Report Number: 6-0711
Report To: Kate Knauff
Project No. 216579269
Sample ID
Lab ID
Quantitation
Limit mg[L
Bromide, mg/L
926579269
# 1489
0.010
0.276
Method Code
EPA Method 300.1
Date Analyzed
02-01-06
Comments:
BQL = Below Quantitation Limit
Reviewer
gFC;ENED
V� S E Dept

TesltAmerica
ANALYTICAL TESTING" CORPORATION
February 07, 2006
Client: Pace Analytical (7228)
9800 Kincy Avenue, Suite 100
Huntersville, NC 28078
Attu: Kate Knauff
SAMPLE IDENTIFICATION
926579269/outfall 001 comp
2960 Foster Creighton Road Nashville, TN 37204 - 800-785-0980 - Fax 615-726-W4
Work Order:
NPA2967
Project Name:
Pace Analytical
Project Nbr:
92112133
Date Received:
01/28/06
LAB NUMBER COLLECTION DATE AND TIME
NPA2967-01 01/24/06 14:25
An executed copy of the chain of custody, the project quality control data, and the sample receipt form are also included as an addendum
to this report. If you have any questions relating to this analytical report, please contact your Laboratory Project Manager at
1-800-765-0980. Any opinions, if expressed, are outside the scope of the Laboratory's accredidation.
This material is intended only for the use of the individual(s) or entity to whom it is addressed, and may contain information that is
privileged and confidential. If you are not the intended recipient, or the employee or agent responsible for delivering this material to the
intended recipient, you are hereby notified that any dissemination, distribution, or copying of this material is strictly prohibited. If you
have received this material in error, please notify us immediately at 615-726-0177.
North Carolina Certification Number: 387
The Chain(s) of Custody, 5 pages, are included and are an integral part of this report.
These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory.
Report Approved By:
i�dmt/,, Cyr
Roxanne Connor
Senior Project Manager
RECEIVED;
1HaEp up,
PR Page I of 6

TestA m rica
ANALYTICAL TESTING CORPORATION
Client Pace Analytical (7228)
9800 Kincy Avenue, Suite 100
Nuntersville, NC 28078
Ann Kate Knauff
2960 Foster Creighton Road Nashville, TN 37204 • BM765-0 80 -Fax [phone]
Work Order:
NPA2967
Project Name:
Pace Analytical
Project Number:
92112133
Received:
0128/06 08:00
ANALYTICAL REPORT
Dilution Analysis
Analyte Result Flag Units MRL Factor Date/rime Method Batch
Sample ID: NPA2967-01 (926579269/outfall 001 comp - Water) Sampled: 01/24/06 14:25
Selected Volatile Organic Compounds by EPA Method 8260E
Bis(chloromethyl)ether NO ug/L 4400
Surr: 1,2-Dichloroethune-d4 (70-130%) 89 %
Surr: DibromoJluoromethane (79-122%) 123 % Z10
Surr: Toluene-& (78-12111) 128 % ZIO
Suff. 4-BromoJluorobenzene (78-126%) 107 %
2198 02101/0621:58
SW846 8260B
6020104
02101106 21:58
SW846 8260B
6020104
OZ/01/06 21:58
SW846 8260B
6020104
02101106 21:58
SW846 8260B
6020104
02101106 21:58
SW846 8260B
6020104
RECEIVED
OFP;
Page 2 of 6

TestAmerica
ANALYTICAL TESTING CORPORATION
Client Pace Analytical (7228)
9800 Kincy Avenue, Suite 100
Huntersville, NC 28078
Arm Kate Knauff
2960 Foster Creighton Read Nashville, TN 07204 • NO-765-MBO • Feu 615-726-3 04
Work Order:
Project Name:
Project Number:
Received:
PROJECT QUALITY CONTROL DATA
Blank
NPA2967
Pace Analytical
92112133
01/28/06 08:00
Analyte Blank V.I. Q Units Q.C. BatcM1 Leb Number
Selected Volatile Organic Compounds by EPA Method 8260B
6020104-BLKI
Bts(chloromethyl)ether <550
ug/L 6020104
6020104-BLK
Surrogate: I,2-1)khloroethone-d4 89-A
6020104
6020104-BLK:
Sarrogme: Dibromofluorometham 122%
6020104
6020104-BLK'
Surrogate: Talaene-A 126% ZIO
6020104
6020104-BLKI
Surrogate: 4-8ronmJluamhenaene 107%
6020104
6020104-BLKI
Analyzed Oatdl'ime
02/OM6 21:29
02/01/06 21:29
02/01/06 2129
02/01/06 21:29
02/01/06 21:29
RECEIVED
HSEDept
FIR
Page 3 of 6

TestAmerica
ANAL7TICAL TESTING CORPORATION
2960 Foster Creighton Road Nashville,
TN 372U - 800-765-0980 - Fax 615-72&3404
Client Pace Analytical (7228)
Work Order;
NPA2967
9800 Kincy Avenue, Suite 100
Project Name:
Pace Analytical
Huntersville, NC 28078
Project Number:
92112133
Atm Kate Knauff
Received:
0128/0608:00
PROJECT
QUALITY CONTROL DATA
LCS
Analyte
Known Val,
Analyzed Val
Selected Volatile Organic Compounds by EPA Method 8260B
6020104-BSI
Bis(chl0rome1hyl)ether
50.0
52.5
S'urrogem: 1,2-Dn,h1orne1honed4
50.0
45.4
SLrrogme: Dibromy/hmromerhane
50.0
62.3
SLrrogaw 761uene-rd4
50.0
63.7
Sarrogule: 4-Bromq(tuarohenzene
50.0
54.2
Terget
Analyzed
Q
Units %Rec.
Range
Batch
Datw7ene
u&?L 105%
80 - 120
6020104
02/01/06 20.31
91%
70- 130
6020104
02/01/06 20:31
Z10
125%
79 -122
6020104
02/01/06 20:31
Zlo
127%
78- 121
6020104
02/01/06 20:31
108%
78-126
6020104
02/01/06 20:31
RECEIVED
HSEOep4
FIR
Page 4 of 6

TestAmerica
ANALYTICAL. TESTING CORPORATION
Client Pace Analytical (7228)
9800 Kincy Avenue, Suite 100
Huntersville, NC 28078
Ann Kate Knauff
TestAmerica Analytical - Nashville
2960 Foster Creighton Road Nashville, TN 372U - Wo765-0960 - Fax 615-728d 4
Work Order:
NPA2967
Project Name:
Pace Analytical
Project Number:
92112133
Received:
0128106 08:00
CERTIFICATION SUMMARY
Method Matrix ATHA Nelac North Carolina
SW8468260H Water N/A X X
i. rj p!
OR
Page 5 of 6

TestAmerica
ANALYTICAL TESTING CORPORATION
Client Pace Analytical (7228)
9800 Kincy Avenue, Suite 100
Huntersville, NC 28078
Arm Kate Knauff
Z10
2960 Foster Creighton Road Nashville, TN 372N - 800-765-0980 'Fax 615726-J
Work Order:
NPA2967
Project Name:
Pace Analytical
Project Number:
92112133
Received:
01)28Po6 08:00
DATA QUALIFIERS AND DEFINITIONS
Surrogate outside laboratory historical limits but within method guidelines. No effect on data.
METHOD MODIFICATION NOTES
RECEIVED
H S E Dept
PFI
Page 6 of 6

2960 Foster Creighton Drive ' Nashville, TN 372D4
000-765-0980 '615-726-3404 Fax
01/31/06
North Carolina Department of Environment
Attn: Gary Francies
59 Woodfin Place
Asheville, NC 28801
United States
VIA EMAIL NOTIFICATION TO Garv.FranciesCmncmail.net
RE: Laboratory Non -Conformance Notification
REF. 15A NCAC 2H.0805 (a) (7) (N).
This letter is regarding the laboratory's requirement of notification for sample non -Conformance to the State of North Carolina. The
following dlent/contact has been notified of this non-conformance as well as the proper corrective action for this issue. Upon this
notification, the client has requested we proceed with analysis:
Pace Analytical Services, Inc. (7228)
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
United States
The following Work Order (W.O. # NPA2967) had the following non-conformance recorded on their analytical report. This is fully
documented in Non -Conformance (NC) # 34940 .
TestAmerica's Cooler receipt form indicates that we received a 1 liter amber glass Non -preserved
container, but the requested analysis is a VOC 8260 compound [bis(chloromethyl)ether], so we
poured up the sample into 2 40 ml VOA vials with HCL. I checked with Kate Knauff and she said
to go ahead and run the sample from the vials and said it is reporting to the state of NC. She
wasn't sure if the compound was a Volatile or Semi -Volatile. Their project # is 92112133, sample
ID: 926579269/outfall 001 comp.
This again is for the above noted requirement for our Laboratory Certification Requirement. If you have any questions, please
contact us by phone of email.
Sincerely,
TestAmerica Analytical Testing Corp.
Nashville Division
Jennifer Huckaba
Project Management Team
Phone: [phone] ext. 1118
Direct: 615-301-5042
Fax: [phone]
Email: ihuckaba()testamericainc.com
This material is intended only for the use of the indlOdual(s) or entity to whom it is addressed, and may contain information that is
privileged and confidential. If you are not the intended recipient or the employee or agent responsible for delivering this material to the
intended recipien4 you are hereby notified that any dissemination, distribution or Copying of this e-mail is strictly prohibited If you have
received this communication in error, please notify us immediately by a -mail or by phone [phone]) and delete this material from any
computer.
RECEIVED
www.testamericainc.com
TestAmerica Analytical Testing Corporation I TestAmerica Drilling Corporation I TestAmenca Air Emission Corporation
HS EDep�
F�FP

Analytical Results
Pace Analytical -Asheville For: 92112133
2225 Riverside Drive
Asheville NC 28804
Entered 1/25/2006
Reported: 1 /27/2006
Sample Remark
Sample ID
Parameter
Cust ID
Result
Units
Method
Date Analyzed
Analyst
060125-3.1
Color
001
<25
ADMI units
SM2120E
1/26/06
MD
060125-3.1
Color Adj.
001
<25
ADMI units
SM2120E
1/26/06
MD
060125-3.1
MBAs
001
0.25
mg/L
SM5540C
1/25/06
MD
Respectfully submitted,
Dena Myers j
NC Cert #440,
NCDW Cert #37755,
EPA NC00909
REGOVED
PFf '
P.O. Box 228 • Statesville, North Carolina 28687. 704/872/4697

2/.2aceAnalvtical
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Page: of
coon A
Section B
Section C
Required Client Information:
Required Project
Report To:
Information:
Invoice Information
Attanticn:
REGULATORY
/
Company
Copy To:
Company Nal
❑ NPOES
❑ GROUNDWATER DRINKING WATER
Address
Address:
❑ UST
❑ RCRA
❑ Other
Purchase Order No.:
Project Name:
Pace Quote Reference:
Pap Project �Maanger:
•
//
• ❑OA OIL ❑IN El MI ❑MN ©NC
❑OH ❑SC ❑ WI ❑OTHER_
Email To:
Phone
Fax
Project Number:
K M
Pace Profile R:
Fifterod (YIN)
Requested Due DatelTAT
Matrb Cmdea
CODE
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Pnservaavea
Requested
Anetysis:
valid
Section D Required Client Information MATRIX
GRINp
NG WATER DW
w
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SAMPLE I D
WATER
WASTE
WT
WATER WW
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One Character per box.
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COMPOSITE START COMPOSITE END(GRAS
0
a
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AIR
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Number
Samples IDs MUST BE UNIQUE
OTHER
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TISSUE
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DATE TIME DATE TIME
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SAMPLER NAME e SIGNATURE
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SEE REVERSE SIDE FOR INSTRUCTIONS
SIGNATUREof SAMPLER:
DATE Signed (MM / DO / YY)
`0
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aceAnalytical
Section A
Required Client Information:
Coppany
Email To:
Phone Fax
Requested Due DatelrAT
Section D Required Client Information
SAMPLE ID
One Character per box.
W (A-Z, 0-9
F Samples IOs MUST BE UNIQUE
o I -, I �, I C, a. I { I i i
CHAIN -OF -CUSTODY If Analytical
Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields
must be completed accurately.
Page: of
Sections
section C
Required Project Information:
Invoice Information:
0 9 6 2 8 9
Report To:
Attention:
REGULATORY
Copy To:
Company Name: ❑ NPDES
GROUND WATER ❑ DRINKING WATER
❑ UST
LJ RCRA ❑Other
Address:
OGA OIL ❑IN ❑MI ❑MN ❑NC
Purchase Order No.:
Pace Quote Reference:
OOH ❑SC ❑ WI ❑OTHER
Number:
Pace Profile #:
u
CODE
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VJT
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SL
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COMPOSITE START
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DATE
TIME
I DATE
TIME
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Additional Comments:
r 9 '
Luc y-t,
SEE REVERSE SIDE FOR INSTRUCTIONS
n
1R�gJ 6AMPLEq
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e' SAMPLE CONDITION
DATE S'�netl (Mp1/DO/V1)
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E

aceAnalytical®
www.pacolabs.com
February 03. 2006
Mr. Chuck Powell
Performance Fibers
338 Pea Ridge Road
New Hill. NC 27562
RE: Lab Project Number: 92112135
Client Project ID: Outfall 002
Dear Mr. Powell:
Pace Analytical Servi Inc.
9800 Kincey Avenue, 1 100
Huntersville, NG 28078
Phone., 704,875.9092
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC28804
Phone: [phone]
Fax: [phone]
Enclosed are the analytical results for sample(s) received by the laboratory on January 25. 2006. Results
reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the
body of the report.
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic testing
was performed at our Pace Charlotte laboratory unless otherwise footnoted.
If you have any questions concerning this report please feel free to contact me.
Sincerely.
Kate Knauff
[e-mail]
Project Manager
Enclosures
Asheville Certification IDs
REPORT OF LABORATORY ANALYSIS
NC Wastewater 40
NC Drinking Water 37712 This report shall not be reproduced, except in full,
Sc 99030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648
harlotte Certificat
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

aceAnalytical `'
www. pacelabs. cum
Lab Sample No: 926579285
Client Sample ID: OUTFALL 002 COMP
Pace Analytical Servi Inc.
9800 Kincey Avenue, ! 100
Huntersville, Nu coO78
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone., 828.254.7176
Fax: [phone]
Lab Project Number: 92112135
Client Project ID: Outfall 002
Project Sample Number: 92112135-001 Date Collected: 01/24/06 15:07
Matrix: Water Date Received: 01/25/06 17:05
Parameters
Results
Units
Report Limit
OF
Analyzed
By
CAS No. Qual ReaLmt
Metals
Trace ICP Metals
Prep/Method:
/ EPA 200.7
Barium
0.025
mg/l
0.0050
1.0
01/27/06
17:42
SAJ
7440-39-3
Boron
0.054
mg/l
0.010
1.0
01/27/06
17:42
SAJ
7440-42-8
Iron
0.97
mg/l
0.050
1.0
01/27/06
17:42
SAJ
7439-89.6
Magnesium
3.3
mg/l
0.10
1.0
01/27/06
17:42
SAJ
7439-95-4
Manganese
0.092
mg/l
0.0050
1.0
01/27/06
17:42
SAJ
7439-96-5
Date Digested
01/26/06 15:30
01/26/06
15:30
Wet Chemistry
Total Suspended Solids
Method:
EPA
160.2
Total Suspended Solids
18.
mg/l
Ammonia
Method:
EPA
350.1
Nitrogen. Ammonia
ND
mg/l
28 day NOX
Method:
EPA
353.2
Nitrate -Nitrite (as N)
0.42
mg/l
Phosphorus. Total
Method:
EPA
365.2
Phosphorus
ND
mg/1
Sulfate.Turbidimetric
Method:
EPA
375.4
Sulfate
18.
mg/l
Biochemical Oxygen Demand, 5 d Method: EPA 405.1
BOD, 5 day 2.0 mg/l
Chemical Oxygen Demand
Chemical Oxygen Demand
Total Organic Carbon
Total Organic Carbon
Date: 02/03/06
Method: EPA 410.4
77. mg/l
Method: SM 5310B
7.2 mg/l
3.3
0.10
0.10
0.100
5.0
2.0
25.
1.0
3.3 01/26/06 21:07 JMW
1.0 01/28/06 14:23 ARH 7727-37-9
1.0 01/26/06 21:00 CD1 7727-37-9
1.0 01/27/06 21:02 TMR 7723-14-0
1.0 01/26/06 18:25 ARH
1.0 01/26/06 14:00 JMW
1.0 01/27/06 07:45 TMR
1.0 01/30/06 07:30 BMF 7440-44-0
Asheville Certification
Cs
REPORT OF LABORATORY ANALYSIS
NC Wastewater
40
NC Drinking Water
This report shall not be reproduced, except in full,
Sc
99030
9030
without the written consent of Pace Analytical Services, Inc.
FL NELAP
E87648
*4
'. I
`nek
1
Page: 1 of 15
Charlotte Certification ID
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

ace Analytical °
www. pacelabs. cam
Lab Sample No: 926579293
Client Sample ID: OUTFALL 002 GRAB
Pace Analytical SeryInc.
9800 Kincey Avenue, , 100
Huntersville, 1vo co078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112135
Client Project ID: Outfall 002
Project Sample Number: 92112135.002 Date Collected: 01/24/06 15:07
Matrix: Water Date Received: 01/25/06 17:05
Parameters
Results
Units Report Limit DF Analyzed
By CAS No. Qual ReaLmt
Field Services
Field Grab Data
Method:
Collected By
AGN
01/27/06
KAK
Collected Date
1/24/06
01/27/06
KAK
Collected Time
15:07
01/27/06
KAK
Field pH
7.19
01/27/06
KAK
Field Temperature
13.8
01/27/06
KAK
GC Semivolatiles
Hexane Extractable Material
Oil and Grease
Date: 02/03/06
Method: EPA 1664A
5.2 mg/l 5.0 1.0 01/26/06 10:34 LMM
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water
37712
SC 990309030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648
l me
Page: 2 of 15
Charlotte Certification ID
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

aceAnalytical`'
www.pacelahs.com
Pace Analytical Serm Inc.
9800 Kincey Avenue, ; 100
Huntersville, Nu z6078
Phone: [phone]
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112135
Client Project ID: Outfall 002
Dilution factor shown represents the factor applied to the reported result and reporting limit due to changes
in sample preparation, dilution of the extract, or moisture content
Method 9071E modified to use ASE.
All pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate
hold time.
Depending on the moisture content the PRLs can be elevated for all soil samples reported on a dry weight basis.
2-Chloroethyl vinyl ether has been shown to degrade in the presence of acid.
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
Ill The glucose/glutamic acid standard exceeded the range of 198 plus or minus 30.5 mg/L.
Date: 02/03/06
Asheville Certification ID
NC Wastewater
40
NC Drinking Water
37712
Sc
99030
FL NELAP
E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
0.
�a1
Page: 3 of 15
harlotte Certificatio
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

Pace Analytical Servi Inc.
9800 Kincey Avenue, ! 100
Huntersville, No m078
Anah/tiral o Phone:Fax.,704.875.9091
www.pacelabs.com QUALITY CONTROL DATA
QC Batch: 148166
QC Batch Method: EPA 1664A
Associated Lab Samples: 926579293
METHOD BLANK: 926580473
Associated Lab Samples: 926579293
Parameter Units
Oil and Grease mg/l
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NO28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112135
Client Project ID: Outfall 002
Analysis Method: EPA 1664A
Analysis Description: Hexane Extractable Material
Blank Reporting
Result Limit Footnotes
ND 5.0
LABORATORY CONTROL SAMPLE 8 LCSD: 926581695 926581703
Spike LCS LCSD LCS LCSD
Parameter Units Conc. Result Result X Rec % Rec RPD Footnotes
Oil and Grease mg/l 40.00 34.50 33.60 86 84 3
Date: 02/03/06
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 99030 This report shall not be reproduced, except in full,
SC 9030
NC Drinking Water without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 y
`e1 IGILLC
Page: 4 of 15
harlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

Pace Analytical Servi 'nc. Pace Analytical Services, Inc.
9800 Kincey Avenue, 1 100 2225 Riverside Drive
Huntersville, Nu zod78 Asheville, NC 28804
Phone.,704.875.9092 Phone.[phone]
°Analytical Fax [phone] Fax.,828.252.4618
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92112135
Client Project ID: Outfall 002
QC Batch: 148224 Analysis Method: EPA 200.7
OC Batch Method: Analysis Description: Trace ICP Metals
Associated Lab Samples: 926579285
METHOD BLANK: 926582396
Associated Lab Samples:
926579285
Blank
Reporting
Parameter
Units
Result
Limit Footnotes
Barium
mg/l
ND
0.0050
Boron
mg/l
ND
0.010
Iron
mg/1
NO
0.050
Magnesium
mg/l
ND
0.10
Manganese
mg/l
ND
0.0050
LABORATORY CONTROL SAMPLE: 926582404
Spike
LCS
LCS
Parameter
Units
Conc.
Result
% Rec Footnotes
Barium
mg/1
0.5000
0.4980
100
Boron
mg/1
0.5000
0.4920
98
Iron
mg/1
5.000
5.080
102
Magnesium
mg/1
5.000
5.020
100
Manganese
mg/l
0.5000
0.5070
101
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 926582412 926582420
926576752
Spike
MS
MSD
MS
MSD
Parameter
Units
Result
Conc.
Result
Result %
Rec %
Rec
RPD Footnotes
Barium
mg/1
0.00411
0.5000
0.4980
0.4380
99
87
13
Boron
mg/l
0.1190
0.5000
0.6200
0.5630
100
89
10
Iron
mg/1
0.05610
5.000
5.080
4.490
100
89
12
Magnesium
mg/l
2.030
5.000
7.110
6.500
102
89
9
Manganese
mg/l
0.00257
0.5000
0.5040
0.4450
100
88
12
Date: 02/03106
Page: 5 of 15
Asheville Certification
ID s
REPORT OF LABORATORY ANALYSIS
Charlotte Certification
Ws
NC Wastewater
40
NC Wastewater
12
NC Drinking Water
This report shall not be reproduced, except in full,
NC Drinking Water
37706
Sc
9030
99030
without the written consent of Pace Analytical Services, Inc.
Sc
99006
FL NELAP
E87648
,. ,«°'°
FL NELAP
E87627

Pace Analytical Servl nc. Pace Analytical Services, Inc.
9800 Kincey Avenue, 1 100 2225 Riverside Drive
Huntersville, NU Z6078 Asheville, NC 28804
Anall/lir°al ® Phone: [phone] Phone: [phone]
Fax., 704.875.9091 Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Lab Project Number: 92112135
Client Project ID: Outfall 002
SAMPLE DUPLICATE: 926582438
926576760
DUP
Parameter
Units
Result
Result
RPD
Barium
mg/l
0.06600
0.06500
2
Boron
mg/l
0.1200
0.1200
0
Iron
mg/l
2.100
2.000
6
Magnesium
mg/l
2.300
2.300
1
Manganese
mg/l
0.1400
0.1400
1
Date: 02/03/06
Footnotes
Asheville Certification
IDs
REPORT OF LABORATORY ANALYSIS
NC Wastewater
40
NC Drinking Water
37712
This report shall not be reproduced, except in full,
SC
99030
without the written consent of Pace Analytical Services, Inc.
FL NELAP
E87648
10
Page: 6 of 15
harlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Servi 'nc.
9800 Kincey Avenue, t 100
Huntersville, Ncza078
1 Phone:704.875.909
Ana1i�t' . Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: 828.254,7176
Fax: [phone]
Lab Project Number: 92112135
Client Project ID: Out -fall 002
QC Batch: 148213 Analysis Method: EPA 405.1
QC Batch Method: EPA 405.1 Analysis Description: Biochemical Oxygen Demand, 5 d
Associated Lab Samples: 926579285
METHOD BLANK: 926581893
Associated Lab Samples: 926579285
Blank Reporting
Parameter Units Result Limit Footnotes
BOD, 5 day mg/l NO 2.0 1
LABORATORY CONTROL SAMPLE: 926581901
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
B00. 5 day mg/l 198.00 149.0 75 1
SAMPLE DUPLICATE: 926581919
Parameter Units
BOO. 5 day mg/l
Date: 02/03/06
926577974 OUP
Result Result RPD Footnotes
45.00 45.00 0 1
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water
37712
SC 990309030 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 �y'""
sWo1 IIE=
Page: 7 of 15
harlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Servi nc. Pace Analytical Services, Inc.
9800 Kincey Avenue, t 00 2225 Riverside Drive
Huntersville, NC28078 Asheville, NC28804
Anahrtiral Phone:[phone] Phone:828,254.7176
Fax. [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
QC Batch: 148273
QC Batch Method: EPA 160.2
Associated Lab Samples: 926579285
METHOD BLANK: 926585118
Associated Lab Samples: 926579285
Parameter Units
Total Suspended Solids mg/l
LABORATORY CONTROL SAMPLE: 926585126
Lab Project Number: 92112135
Client Project ID: Outfall 002
Analysis Method: EPA 160.2
Analysis Description: Total Suspended Solids
Blank Reporting
Result Limit Footnotes
NO 1.0
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Total Suspended Solids mg/l 250.00 258.0 103
SAMPLE DUPLICATE: 926585142
Parameter Units
Total Suspended Solids mg/l
Date: 02/03/06
926576463 DUP
Result Result RPD Footnotes
3500 3500 1
Asheville Certification
IN
REPORT OF LABORATORY ANALYSIS
NC Wastewater
40
This report shall not be reproduced, except in full,
NC Drinking Water
37712
without the written consent of Pace Analytical Services, Inc.
SC
990309030
FL NELAP
E87648
o " ,
.wI c
Page: 8 of 15
rlotte Certificatio
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
FL NELAP
E87627

Pace Analytical Sery Inc.
9800 Kincey Avenue, ; 100
Huntersville, NC 28078
Ana l V I bra l Phone: [phone]
Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
QC Batch: 148233
OC Batch Method: EPA 353.2
Associated Lab Samples: 926579285
METHOD BLANK: 926583279
Associated Lab Samples: 926579285
Parameter Units
Nitrate -Nitrite (as N) mg/l
LABORATORY CONTROL SAMPLE: 926583287
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112135
Client Project ID: Outfall 002
Analysis Method: EPA 353.2
Analysis Description: 28 day NOX
Blank Reporting
Result Limit Footnotes
NO 0.10
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Nitrate -Nitrite (as N) mg/l 5.000 5.230 105
MATRIX SPIKE: 926583295
926552878 Spike MS MS
Parameter Units Result Conc. Result X Rec Footnotes
Nitrate -Nitrite (as N) mg/1 0 5.000 5.160 103
SAMPLE DUPLICATE: 926583303
Parameter Units
Nitrate -Nitrite (as N) mg/1
Date: 02/03/06
926557570 DUP
Result Result RPD Footnotes
8.700 8.700 0
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 99030 This report shall not be reproduced, except in full,
Sc 9030
NC Drinking Water without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648it
n°"°�•.
Page: 9 of 15
rlotte Certification ID
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Pace Analytical Servi Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, f 100 2225 Riverside Drive
Huntersville, NC28078 Asheville, NC28804
Phone: Anaone:704.875.9092 Phone:[phone]
Fax: [phone] Fax: [phone]
www.pacelabs.com QUALITY CONTROL DATA
QC Batch: 148256
QC Batch Method: EPA 375.4
Associated Lab Samples: 926579285
METHOD BLANK: 926585019
Associated Lab Samples: 926579285
Parameter Units
Sulfate mg/l
LABORATORY CONTROL SAMPLE: 926585027
Lab Project Number: 92112135
Client Project ID: Outfall 002
Analysis Method: EPA 375.4
Analysis Description: Sulfate,Turbidimetric
Blank Reporting
Result Limit Footnotes
NO 5.0
Spike LCS LCS
Parameter Units Conc. Result % Rec Footnotes
Sulfate mg/l 20.00 20.68 103
MATRIX SPIKE: 926585043
926578980 Spike MS MS
Parameter Units Result Conc. Result % Rec Footnotes
Sulfate mg/1 919.5 20.00 917.5 0 2
SAMPLE DUPLICATE: 926585035
926578980 DUP
Parameter Units Result Result RPD Footnotes
Sulfate mg/l 920.0 920.0 0
Date: 02/03/06
Asheville Certification ID s REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 99030 This report shall not be reproduced, except in full,
Sc 9030
NC Drinking Water without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 K,.. 1.'
Page: 10 of 15
harlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

ace Analytical
www.pacelabs.com
QC Batch: 148285
QC Batch Method: EPA 365.2
Associated Lab Samples: 926579285
METHOD BLANK: 926585555
Associated Lab Samples: 926579285
Parameter Units
Phosphorus mg/l
LABORATORY CONTROL SAMPLE: 926585563
Pace Analytical Sera Inc.
Pace Analytical Services, Inc.
9800 Kincey Avenue, ; 100
2225 Riverside Drive
Huntersville, Nc z8078
Asheville, NC 28804
Phone:[phone]
Phone:[phone]
Fax: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Lab Project Number: 92112135
Client Project ID: Outfall 002
Analysis Method: EPA 365.2
Analysis Description: Phosphorus, Total
Blank Reporting
Result Limit Footnotes
NO 0.100
Spike LCS LCS
Parameter Units Conc. Result X Rec Footnotes
Phosphorus mg/l 1.000 1.033 103
MATRIX SPIKE: 926585571
926578360 Spike MS MS
Parameter Units Result Conc. Result % Rec Footnotes
Phosphorus mg/l 2.364 1.000 3.252 89
SAMPLE DUPLICATE: 926585589
Parameter Units
Phosphorus mg/l
Date: 02/03/06
926575218 DUP
Result Result RPO Footnotes
0.1290 0.1200 8 3
Asheville Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 99030 This report shall not be reproduced, except in full,
Sc 903
NC Drinking Water 2 without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648 M
Page: 11 of 15
harlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

Pace Analytical ServL Dc. Pace Analytical Services, Inc.
9800 Kincey Avenue, S 00 2225 Riverside Drive
Y7 7 Huntersville, NC 28078 Asheville, NC28804
aI ICGI Phone:[phone] Phone.[phone]
�Al1
Fax. [phone] Fax: [phone]
www.PaC61abs.com QUALITY CONTROL DATA
OC Batch: 148287
QC Batch Method: EPA 410.4
Associated Lab Samples: 926579285
METHOD BLANK: 926585639
Associated Lab Samples: 926579285
Parameter Units
Chemical Oxygen Demand mg/l
LABORATORY CONTROL SAMPLE: 926585647
Parameter Units
Chemical Oxygen Demand mg/1
MATRIX SPIKE: 926585993
Lab Project Number: 92112135
Client Project ID: Outfall 002
Analysis Method: EPA 410.4
Analysis Description: Chemical Oxygen Demand
Blank Reporting
Result Limit Footnotes
ND 25.
Spike LCS LCS
Conc. Result % Rec Footnotes
750.00 786.0 105
926579269
Spike
MS
MS
Parameter
Units
Result
Conc.
Result
% Rec Footnotes
Chemical Oxygen Demand
mg/1
93.00
750.00
933.0
112
SAMPLE DUPLICATE: 926586009
926579285
DUP
Parameter
Units
Result
Result
RPD
Footnotes
Chemical Oxygen Demand
mg/l
77.00
66.00
15
Date: 02/03/06
1i
NC Wastewater
40
NC Drinking Water
37712
Sc
99030
FL NELAP
E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
.01 1aQ�.
Page: 12 of 15
rlotte Certification ID
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

Pace Analytical Sery Inc. Pace Analytical Services, Inc.
9800 Kincey Avenue, 100 2225 Riverside Drive
Huntersville, NC28078 Asheville, NC28804
Y1 �}
Phone.[phone] Phone:[phone]
Anal vocal Fax [phone] Fax: 828.252,4618
www.Pact,labs.com QUALITY CONTROL DATA
QC Batch: 148396
0C Batch Method: EPA 350.1
Associated Lab Samples: 926579285
METHOD BLANK: 926591017
Associated Lab Samples: 926579285
Parameter Units
Nitrogen, Ammonia mg/1
LABORATORY CONTROL SAMPLE: 926591025
Lab Project Number: 92112135
Client Project ID: Outfall 002
Analysis Method: EPA 350.1
Analysis Description: Ammonia
Blank Reporting
Result Limit Footnotes
NO 0.10
Spike
LCS
Parameter
Units
Conc.
Result
Nitrogen, Ammonia
mg/l
1.000
1.065
MATRIX SPIKE: 926591033
926578360
Spike
Parameter
Units
Result
Conc.
Nitrogen. Ammonia
mg/l
0.1730
1.000
SAMPLE DUPLICATE: 926591041
Parameter Units
Nitrogen. Ammonia mg/l
Date: 02/03/06
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NELAP E87648
LCS
X Rec Footnotes
107
MS MS
Result X Rec Footnotes
0.9730 80
926578550 DUP
Result Result RPD Footnotes
0.1900 0,1900 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
,M ,I[Cpya.
Page: 13 of 15
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Serv, Inc.
9800 Kincey Avenue, ; 100
Huntersville, NC 28078
Phone: [phone]
Analytical F Fax•704.875.9091
www.pacelabs.com QUALITY CONTROL DATA
QC Batch: 148416
QC Batch Method: SM 53108
Associated Lab Samples: 926579285
METHOD BLANK: 926592049
Associated Lab Samples: 926579285
Parameter Units
Total Organic Carbon mg/l
LABORATORY CONTROL SAMPLE: 926592056
Parameter Units
Total Organic Carbon mg/l
MATRIX SPIKE: 926592064
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC26804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92112135
Client Project ID: Outfall 002
Analysis Method: SM 5310B
Analysis Description: Total Organic Carbon
Blank Reporting
Result Limit Footnotes
NO 1.0
Spike LCS LCS
Conc. Result x Rec Footnotes
10.00 9.440 94
926557349 Spike MS MS
Parameter Units Result Conc. Result % Rec Footnotes
Total Organic Carbon mg/l 23.03 40.00 52.20 73
SAMPLE DUPLICATE: 926592072
926557364 DUP
Parameter Units Result Result RPD Footnotes
Total Organic Carbon mg/l 20.00 25.00 19
Date: 02/03/06
Asheville Certification IN
REPORT OF LABORATORY ANALYSIS
NC Wastewater
40
NC Drinking Water
2
This report shall not be reproduced, except in full,
Sc
99030
903
without the written consent of Pace Analytical Services, Inc.
FL NELAP
E87648
ry
c
Page: 14 of 15
lotte Certification ID
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA PARAMETER
Pace Analytical Servi nc.
98DO Kincey Avenue, ; 100
Huntersville, NC28078
Phone., 704.875.9092
Fax: [phone]
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 92112135
Client Project ID: Outfall 002
Consistent with EPA guidelines, unrounded concentrations are displayed and have been used to calculate X Rec and RPD values.
LCS(D) Laboratory Control Sample (Duplicate)
MS(D) Matrix Spike (Duplicate)
DUP Sample Duplicate
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
RPD Relative Percent Difference
[1] The glucose/glutamic acid standard exceeded the range of 198 plus or minus 30.5 mg/L.
[21 The spike recovery was outside acceptance limits for the MS and /or MSD due to matrix interference. The LCS
and/or LCSD were within acceptance limits showing that the laboratory is in control and the data is
acceptable.
[31 Sample preservation does not meet EPA recommendations for analyte.
Date: 02/03/06
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 99030 This report shall not be reproduced, except in full,
SC 9030
NC Drinking Water without the written consent of Pace Analytical Services, Inc.
FL NELAP E87648
Page: 15 of 15
lotte Certificat
NC Wastewater
12
NC Drinking Water
37706
SC
99006
FL NELAP
E87627

Analytical Results
Pace Analytical -Asheville For: 92112135
2225 Riverside Drive
Asheville NC 28804
Entered 1/25/2006
Reported: 1 /27/2006
Sample Remark
Sample ID
Parameter
Cust ID
Result
Units
Method
Date Analyzed
Analyst
060125-3.2
Color
002
<25
ADMI units
SM2120E
1/26/06
MD
060125-3.2
Color Adj.
002
<25
ADMI units
SM2120E
1/26/06
MD
060125-3.2
MBAs
002
<0.10
mg/L
SM5540C
1/25/06
MD
Respectfully/ submitted,
-.i
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA NC00909
P.O. Box 228 • Statesville, North Carolina 28687. 704/872/4697

/! 25ce/InalvtIcal
CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Page: of
Section A
Section B
Section C
Required Client Information:
Required Project
Information:
Invoice Information:
-
Company
Report To:
Attention:
REGULATORY
Address
Copy To:
Company Name:
air `M
NPDES _ GROUNDWATER _. DRINKING WATER
❑ UST
G RCRA
❑ Other
-..
Address:
❑OA OIL
❑IN ❑MI ❑MN CAC
Email To:
Purchase Order No.:
Pace Quote Reference:
DON ❑SC
❑ WI ❑OTHER_
Phone Fax
Project Name:
Pace Project Njanager:
r^ "� �-
FiRered (YIN)
Requested Due Date/TAT
Project Number:
Pace Profile #:M%0�-s
Requested
Section Required Client Information
Valid Matra Codes
MATRIX CODE
o.
Analysis:
DRINKING WATER DW
SAMPLE I D
WT
WASTE WATER WATER yM
PRODUCT
SL
m
COLLECTED
#
D
x
One Character per box.
o-g /
Da OL
WIPEI
COMPOSITE START COMPOSITE END/GRAB
-:
W(A-Z. _)
AMR
pp•c• Projett
Number
Samples IDs MUST BE UNIDUE
nSUE
O
TS
DATE nw DATE TIME
?•
L•b LD
i
I ')
Additional Comments:
•
■ • • TIMEACCEPTE■
`
• DATE
TISAMPLE
CONDITION
z
z
—. _.
SAMPLER NAME ■ SIGNATURES
PRINT Name of SAMPLER:
SEE REVERSE SIDE FOR INSTRUCTIONS
SIGNATURE of SAMPLER:
DATE SlI 7 / OD I IY
t=
C aU'
�i
0
9
:I_,

1i
3r�a3 o�lY
„L .__witch). For Approved. OMB No. 2040-0086. Approval expires 5-31-92
FORM
U.S. ENVIRONMENTAL PROTECTION AGENCY
I. EPA
I.D. NUMBER
\/EP_/�
GENERAL INFORMATION
NCD053488409 T1A o
F
Gf �'l
Consolidated Permits Program
GENERAL (Read the "General Instructions" before starting.)
1
2 ,3 -14 1s
LABEL ITEMS
_
GENERAL INSTRUCTIONS
If a preprinted label has been provided,
I. EPA I.D. NUMBER
{ �' ;f
L1information
`_,incorrect
L
affix itin the designated space. Review the
carefully; if any of It is
cross through it and enter the
correct Bala in the appropriate fill-in area
III. FACILITY NAME
below. Also, if any of the preprinted data is
absent the area to the leR or the label
/stl the information that
V. FACILITY
PLEASE
PLACE LABEL IN THIS SPACE
space should
appear) please provide it in the proper fill -
in below. If the label is
MAILING LIST
area complete
and need Items
correct you not complete
i, III, V, and VI (except VI-B which must be
completed regardless). Camplete all items
VI. FACILITY
if no label has been proved. Refer to the
LOCATION
instructions for detailed item descriptions
and for the legal authorization under which
this data is collected.
_
11. POLLUTANT CHARACTERISTICS
INSTRUCTIONS: complete A through J to determine whether you need to submit any permit application fortes
to the EPA. If you answer "yes" to any
questions, you must submit this form and the supplemental from listed in the parenthesis following the question.
Mark "X" in the box in the third column If .
the supplemental forth is attached. If you answer
"no' to each question, you need not submit any of these forms.
You may answer 'no" if your activity is
excluded from permit requirements; see Section C of the instructions. See also. Section D of the instructions
for definitions of bold-faced terms.
MARI
MARK "X"
SPECIFIC QUESTIONS
SPECIFIC QUESTIONS
FOFM
FORM
YES NO
ATiACHEO
YES
NO
ATTACHED
A Is this facility a publicly owned treatment works
B. Does or will this facility (either existing or
which results In a discharge to waters of the
❑ ®
❑
proposed) Include a concentrated animal
❑
®
ElU.S.?
IFORM 2A)
feeding operation or aquatic animal
production facility which results in a discharge
to waters of the I IFORM 2E)
IS T-7
18
19
20"'11
"2tgn-:._
Is this icility which currently results In
D. Isthis proposal facility(other man Grose described
El
Z
El
to waters of the U.S. other than
in A or a above) which wilt result in a discharge
22 23
24
25
26
27
hose described in A or B above? FORM 2C
to waters of the U.S.? FORM 20
F. Does or will this facility treat, stare, or dispose of
F. Do you or will you inject at this facility industrial or
hazardous wastes? (FORM 3)
® ❑
❑
municipal effluent below Ire loweri stratum
❑
®
❑
containing, within one quarter mile of the well
bore, underground sources of drinking water?
2a 25
30
(FORM 4j
31
32
33
G, Do you or will you inject at this facility any
H. Do you or will you inject at INS facility fluids for
produced water other fluids which are brought to
the surface in connection with conventional ail or
El®
ElFrasch
special processes such as mining of suffer by the
process, solution mining of minerals. In
❑
®
❑
natural gas production, inject fluids used for
situ combustion of fossil fuef, or recovery of
enhanced recovery of oil or natural gas,. or inject
geothermal energy? (FORM 4)
fluids for storage of liquid hydrocarbons?
I
34 35
36
37
FORM 4
1
L Is this facility a proposed stationary source
1. Is this aclllly e' proposed stationary soul
which is one of the 28 industrial categories fleted
which is NOT one of the 28 industrial categories
El El El ❑ ® ❑
In the instructions and which will potentially emit
listed in the instructions and which wit potentially
100 tons per year of any air pollutant regulated
emit 250 tons par year of any air pollutant
under the Clean Air Act and may affect or be
regulated under the Clean Air AG and may affect
located in an altetnme nt area? FORM 5
40 41 42 or be located In an attainment are? FORM 5 43 44 45
III. NAME OF FACILITY
SKIP Performance Fibers, Inc.
15 16-2a 30
69
IV. FACILITY CONTACT
A. NAME & TITLE last, first, & title B. PHONE area code & no. - - - '
2 Powell, Charles, Environmental Engineer 919
15 16
"5453154
45 46 '43 62 55
V. FACILITY MAILING ADDRESS
A. STREET OR P.O. BOX
Pea Ridge Road
qc338
15 16
45
B. CITY OR TOWN
C. STATE D. ZIP CODE
c New Hill
NC 27562
A
15 16
40 41 42 4] 51
VI. FACILITY LOCATION
A. STREET ROUTE NO. OROTHER SPECIFIC IDENTIFIER
$ 338 Pea Ridge Road
15 1 16
45
- B. COUNTY NAME
Chatham
46
70
C. CITY OR TOWN
I
D. STATE
E. ZIP CODE
F. COUNTY CODE -
c
New Hill
NC
27562
019
s
15
16
40
41 d2
4] 51
52 54
EPA FORM 3510-1 (8-90)
CONTINUED ON REVERSE

�1
FROM THE
A FIRST
c 2824
specify)
2821
(specify)
5 ,6
Manmade Organic Fibers, except
5
Plastics, Materials, Synthetic Resins, and
6 e
celluosic
Nonvulcanizable Elastomers
C. THIRD D. FOURTH:.':
c 7
(specify) (specify)
T
7
15 16 - 17 15 18 19
Vill. OPERATOR INFORMATION
A. NAME B.ls the name listed In Item
Performance Fibers, Inc. VIII-A also the owner- -.
INc ® E]NO
19 ss: YES
C. STATUS OF OPERATOR fEnter then0 to note letter into
the answer box; if "other "s eci.t ,
D. PHONE area code & no
F=FEDERAL x , M-PUBLIC (other than federalorstate)
`,i'
P
(specify)
C
919
542
2200
AI,
S = STATE - O = OTHER (specify)
P=PRIVATE-
1s 21
z2 2s
,e.
E. STREET OR PO BOX
338 Pea Ridge Road
26 55
' F. CITY OR TOWN, :
_
G. STATE H. ZIP CODJESX;heNDIAN
LANDo
New Hill
NC 27562 facility located on Indian lands?
YESNO
42 42 47 "8
1s 16 40
X. EXISTING ENVIRONMENTAL PERMITS
A: NPDES Dischar es to Surface Water
D. PSD Air Emissions /corn Pro posed Sources
9 P 6 02657T27
NC0001899
9
N
15 1 fle 1 17 is 30
15
1 16
1 17
t6'< 30 1
B.1-11C(Undergroundirilection(of Fluids
E. OTHER (spoci6,(specify)
WTP Alum Residuals
c
T
'
°
a
Wg0023197
s
D
15
Application
15
18
,7..
118 30
15
16:
17
18 30 Land
Program
Permit
C. RCRA Hazardous Wastes E. OTHER (specify) (Specify)
9 R ' NCO053488409-R1 a T" a NC5000100 NPDES Stormwater
1s 1s 1r is 3o s 1e n 1a 36 Per
XI. MAP
Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must
show the outline of the facility, the location of each of its existing and proposed' intake and discharge structures, each of its,
hazardouswaste treatment, storage, or disposal facilities,. and each well where it. injects fluids underground. Include all springs, l
rivers and other surface water bodies in the map area. See instructions for precise requirements.
XII. NATURE OF BUSINESS(provide a brief descri tion
A chemical plant engaged in the manufacture of industrial synthetic polyester fiber and organic polyester resin.
XIII. CERTIFICATION see instructions
certify under penalty of law that I have personally examined and am familiar with the information submitted. in this application and ".
iI I;`
all attachments and that, based onmy inquiry of those persons immediately responsible for obtaining the information contained in •. ''
the application, -I believe that the: information is true, accurate and complete. i aim aware that there are significant penalties for:' ,
submitting 'false information, including `the possibiihof fine: andimnsonmerl -
A. NAME & OFFICIAL TITLE (type orprint) B. SIGNA
C. DATE SIGNED
Don Peterson, Plant Manager
lip/
COMMENTS FOR OFFICIAL USE ONLY
c
C
55
EPA FORM 3510-1 (8-90)

s
EPA FORM 1
Item XI.
Topographic Map
Performance Fibers, Inc.

.ayM61 th$}Rd.WQRmiY ally be
L
i
I � l �J
i
r
10 A\
1 } SITE
{!j
\ d
'all 001
71
a sef rOutfall
002,
l
'
v
-...—
R.N�`ly3,�
�� i-•4.�{`
f �`~J fi
an
IL
f
0 0,3 0.6 0.9 1.2 1.5 kr:
0 012 0.4 0.6 0.8 1 mi
Map center is 350 37' 12"N, 790 02' 41"W (WG584/NAD83)
Moncure quadrangle
Projection is UTM Zone 17 NAD83 Daturn
Performance Fibers, Inc
.N7oneure, Chatham County, NC
EPA Form 1, item XI
M*
I
H--8.527
G=1.139

Form Approved.
PA I.D. NUMBED copy Inom Item IofF.rm 1) OMB No. 2040-0088.
Please print or type In the unshaded anal only. NCDO53488409 Approval expires 8-31-98,
:FjORCM1— U.S. ENVIRONMENTAL PROTECTION AGENCY
%EPA APPLICATION FOR PERMIT TO DISCHARGE WASTEWATER
EXISTING MANUFACTURING, COMMERCIAL, MINING AND SILVICULTURAL OPERATIONS
Consolidated Permlrs Program
1. OUTPALL LOCATION
For each outfall, lilt the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A.OUTFALLNUMBER
0. LATITUDE
C. LONGITUDE
D. RECEIVING WATXR (name)
001
35
37
01
79
03
25
Haw River
002
35
37
00
79
02
36
Shaddox Creek
11. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES
A. Attach a line crewing showing the vrer flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent,
NW treatment units labeled to Correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by slowing evan"
flats between Intakes, openrtle w,. it Rit unite, and outfalls. If a water balance annot be determined (Lg, for certain mining sctNider), provide e
pictorial deecription of the nature and ernountOf any source of water and any collection or treatment measures.
B. Fee each ouffall, provide a clawri on trf: 1 All moons contributing wasurNater to the affluent, including prone wastewater, senitry, wastewater,
cooling water, and storm voter runoff; 121 TM EYEragE-flow contributed by each operation; and (3) The treatment received by the we rtaweter. Continue
On additional sheets If necessary. -
I.OUT-
a. OFORATION(S) CONTRIBUTING FLOW
S. TREATMENT
PALLN
ANO
e. OPERATION (lLt)
. AV [RAGL ILOW
(include units)
S. DESCRIPTION
. LIST COD 9 FROM
TABLE aC-1
001
See additional information for complete 001 c
ascription
002
Firepond Overflow
33,000 GPD
Discharge to Surface Water
4-A
Stormwater Runoff
78,500 GPD
Oil Baffles and Weirs. Discharge to Surfaca Water
1.H
4-A
Steam and HVAC Condensate
1,000 GPD
Discharge to Surface Water
4-A
Air Dryer
500 GPD
Discharge to Surface Water
4-A
9FIFICIAL. USE ONLY (affluent N w )
-44 _; -... I .. . ,.,.
EPA Form 5510.2C (8-90) PAGE I OF 4 CONTINUE ON REVERSE

CONTINIIFn ranss rup CnrvMT
C. Except for It runoff, leaks, or spills, an any of the discharges described in Items I I -A or B intermittent or seasonal?
I0Tell (tam➢Ifte the following table) ®NO (go to section III)
3. FREQUENCY
4. FLOW
1. OUTFALL
2. OPERATION(!)
e. DAYS
b. MONTHS
e. FLow RAT[
b, TOTAL VOLUME
NUMBER
CONTRIBUTING FLOW
'reR w[ER
F[R YEAR
(In med)
(epfeflY wffh unfu)
c OUR.
1. LOXO TawY
3. Yw1t1YYY
v
t. LOMO T
V w
1. Mw11Y VM
wLLv
(list)
()(it)
(specify
avenge)
(... 1fY
average)
ATIDN
(in days)
III. PRODUCTION
A. Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility?
®YES (complete item III-B) Refer to Supplementary Information ❑ No (to to section IV)
B. An the limitations in the applicable effluent guideline expressed In terms of production for other measure of operation)?
�Y[s. (eomDpn fMm fff•C) NO (go to Section IV)
C. If you answered "yes"to Item Ill-B, list the quantity which represents an actual measurement of your level of production, expressed in the terms and units
used In the applicable effluent guideline, and indicate the affected outfalls.
1. A RAGE DAILY PRODUCTION
a. AFF[CT[D
�, ouwwDTr ru aw.
b. YXIv er Yuenwe
C. oruwnox, rwoeucr, YwTcwlwL, cTc.
OVTFALLS
(JDeUIY)
(list out/all numbers)
NIA
IV.IMPROVEMENTS
A. An you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operation of waste-
water treatment equipment or practices or any other environmental programs which may affect the discharges described in this application? This includes,
but is not limited to, permit conditions, administrative or enforcement
orders, enforcement compliance schedule letters, stipulations, court orders, and grant
or loan conditions. -
❑T[[ (template the following table) NO (go to Item IV-B)
I- IDENTIFICATION OF CONDITION,
2, AFFECTED ONTFALLE
AO R[[M[NT,.[TC.
S. BRIEF DEeCRJ"ION OF FROJ[CT
E
a. YO.
dtW11aE N MKYanla
wVlwio
lInC� O
B, OPTIONAL yew, may attach additional sheets descriWtq any additional water pollution control programs (or other environmental projects which may affect
.youiPlanrle�argg) You now have underway or whkl .�y"�t4O'y. plan. ind'eat. whether each program is now underway or planned, and indicate your actual or
eehwulef COnetructl0n.
7, ❑MART(, 14X �rD aCR1e740114 0I ADDITIONAL CONTROL PROGRAMS IB ATTACHED
EPA 3 .
•.-�.. 1 .. e.-oVr rwun z Ur 4 CONTINUE ON PAGE 3

A, 8, h Cr See instructions before proceeding — Complete one set of tables for each outfall — Annotate the outfall number In the space provided.
NOTE: Tables V-A, V-B, and V-C are included on separate sheets numbered V-1 through V-9.
D. Use the space below to list any of the pollutants listed in Table 2c-3 of the Instructions, which you know or have reason to believe Is discharged or may be
discharged from any outfall. For awry pollutant you list, briefly describe the reasons you believe it to be present and report env analytical data in your
Possession.
r. POLLUTANT 2. SOURCE t.POLLUTANT 2. SOURCE
Acetaldehyde Cresol Possible process by-product
Used in QC lab
Crotonaldehyde Possible process by-product
Cyclohexane Used in QC Lab
Xylene Used in QC Lab
-C a substance or a component or a substance which you
® YES (ifaf all such Porto ton is below)
Antimony
Phthalate Esters (Possible process by-product)
(Refer to Supplementary Information)
use or manufacture as an intermediate or anal product or
❑ No (so to Item VI-B)
EPA Form 3510.2C (8.90) PAGE 3 OF 4 CONTINUE ON REVERSI

CONTINUED FROM THE FRONT
VII. BIOLOGICAL TOXICITY TESTING DATA
Do you have any knowledge or reason to believe that easy biological tort fee .am" cr chronic, toxicity fgq been made kany Of your ditohari n or on a
receiving water in relation to your discharge within the fast 3 years? '.
©Y as (Identify the test(s) and describe theirpurposes below) ON (so to Section RI71)
Chronic Toxicity at Discharge 001 and
Acute Toxicity at Discharge 002
per monitoring requirements of NPDES permit.
IIICONTRACT ANALYSIS INFORMATION
Were any of the_enalyses reported in item V performed by a contract laboratory or consulting firm?
® YES (list the name, address, and telephone number of and pollutants NO (so to Section fX)
analysed by, each such laboratory or firm below)
A. NAME
B. ADDRESS
TELEPHONEC.
area code a no.
T ANALYZED
list
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
[phone]
Huntersville, NC 28078
ext. 236
Tritest, Inc.
6701 Conference Drive
Roger Thomas
Raleigh, NC 27607
[phone]
NC WW Cart #067
NCIDW Carl #37731
IX. CERTIFICATION
/certify underpenshy oflawthat this document and
eBattechments were prepared under medirection
or supervision in accordance
with a system designad to
assure that quelifiedpononnelproperlygether andeveluate
the informotionsubmitted Based on my
inquiry ofthe person orpersons
who menage the system or
thosepersons direcdyresponsible forgathering theinformetion,
the inlamationsubmittedis, to thebestofm
yknowledge andbelief,
true, accurate, and complete.
l am aware that there are significam penalties for
submitting false information, including the possibility
of fine and imprisonment
for knowing violations.
A. NAME hrO�F�JGYALTITLE (fype orprint)
-
B. PNONE NO. (else CUde G n0.)
/ {1~/Z
Ww— —
Don Peterson Plant Manager
919-545-3114
C. SIGNATURE
D. DATE SIGNED
4 111cJ(0
PAGE 4OF4
EPA Form 3510.2C (8.90)

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report
EPA I.D. NUMBER (COPY tram Item I Of arm 1)
some or all of
this information on separate sheets fuse the same format) instead of completing these
SEE INSTRUCTIONS. pages.
NCDM 188409
a
V. INTAKE AND EFFLUENT CHARACTERISTICS !continued from page 3 0/Form 2-CI
our FA LL No.
001
PART A - You must provide the results of at least one analysis for every pollutant in this table.
Complete one table for each outfall. See instructions for additional details.
t. POLLUTANT
2. EFFLUENT
3, UNITS
(specify It blank)
4. INTAKE (oprfon.il
a" MAXIMUM DAILY VALUE
. MAXI M I
p�Y VALUE
C. /t
V LU
(0
1 available
1 .Vella
a
d. NO. OF
S. LONG
TERM
b. NO. OF
li) cocoas
hI
cancawswwnow
lal ..cos•
„'r
IaI nwss
ANALYSES
a.CONCEN-
TRATION
b. MASS
ANALYSES
I-1
(:) Nwn
a. Biochemical
s
Oxygen Demand
8.34
5.6
(BOD)
3.3
2.2
2.4
1.6
52
mg/L
Ibs/day
b. Chemical
Oxygen Demand
93
124
(COD)
.9
1
mg/L
Ibs/da y
c. Total Organic
Carbon (TOC)
14
18.8
1
mg/L
Ibslday
d. Total Suspended
Solids (TSS)
7.5
5.8
5.8
4.5
.12
3.0
52
mg/L
Ibslday
e. Ammonia (as N)
< 0.10
< 0.13
1
mg/L
Ibslday
f, Flow
VALUE
VALUE
VALUE
VALUE
0.161
0.105
0.080
365
MGD
9. Temperature
VALUE
VALUE
VALUE
(winter)
205
17.2
13.1
365
°C
VALUE
It. Temperature
VALUE -
VALUE
VALUE
VALUE
(summer)
30.3
26.3
24.2
365
aC
MINIMUM MAXIMUM
INIMUM MAXIMUM
I. pH
6.8 8.3
6.8 8.3
365
STANDARD UNITS
PART 8 - Mark "X" in column 2-a for each pollutant you know or have reason to believe is
"X"
present. Mark in column 2-b for each pollutant you believe to be absent. If you mark column 2a for any pollutant
which is limitedeither directly, or indirectly but expressly, inan effluent limilationsguideline,
you
column 2a, you must provide quantitative data" an explanation of their
must provide the results of at least one analysis far that pollutant. For other pollutantsfor which you mark
pregame in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements.
t. POLLUT-
z. MAR% 'X•
3. EFFLUENT
ANT AND
CAS NO.
a'evi- bivi
Veins
• MA%IMUM DAILY VALUE b, MAXI y%a Y VALUE c.
l%aO.&Ia)
/t�[ VA E
a.eallaDl QNO.O
4. UNITS
5. INTAKE /opfiona!)
a.L NG TERM
(if available)
a. CONCEN- b. MA55
TRATION
AVERAGE VALUE No.i
ANA
wwnon
la) rwss
(°) Nwss
Ial Nwss
ANAL-
.ncen.wwnon
concxntw
VIES
la) Nqs YBEs
A. Bromide
(24959-67-9)
X
0.276
0.37
1
mg/L
Ibslday
b. Chlorine,
Total Residual
X
< 1.0
< 1.0
< 1.0
< 1.0
< 1.0
< 1.0
365
mg/L
Ibslday
c. Color
X
<25
N/A
1
ADMI
N/A
d. Fein
Conform
X
1200
NIA
1200
370
12
#I100 ml
N/A
e- Fluoride
115984.46.8)
X
0.32
0.93
1
mglL
Ibs/day
-.
f. Nit
Nitrne (ae N) X
s-n e
2.0
2.69
1
mglL
Ibs/day
«.. r....R .aa.a-N to-i of ' """' - CONTINUE ON REVERSE

ITEM V-13 CONTINUED
FROM
FROPIT
'Y .PRECUT-.
i. MARK •X•
3. EFFLUENT
4. UNITS
5. INTAKE (opriminll
T AND
'j .-
'
..[[-
L MAXIMUM GAILY VALU[
- MAXI M
I
Y VA UE
��
C.L
wotWO
AyVALUEd.
NO.O
L CONCaN•
a �p
AJERA��AME
. NO. OF
'!iCAB NO.
(jftlmWbl[)
wa-
uwx
[
ANAL-
VSES
TR ATION
b. MASS
ANAL-
VISES
xc[xrwwnc
(al twee
lair
CONCwwT,a
lal rwu
xc [xv nnox
lal r
9r:NINo9an,
Tdgtzl`or9amc
X
0.57
0.765
1
mg/L
Ibs/day
r[ i
11.,Oil and
Give..
X
13.4
9.4
7.1
5.5
6
4
52
mg/L
Ibs/day
L Phosphorus
(a.PJ,23 Tata
X
2.1
1.6
1.6
1.3
1.3
25
mg/L
Ibs/day
(7723.ota
.9
1. padloactivity
(1) Alpha,
Tout
X
(2) Bab,
Teal_
X
8.62
N/A
1
pCi/L
N/A
(3) Radium,
Total
X
(4) Radium
226, Total
X
Sulfate
X
110
147.7
1
mg/L
Ibs/day
79-81
FS.rf�snu
X
))45.3)
X
otanta
X
0.25
0.34
1
mglL
Ibs/day
o. Aluminum,
Total 90.51
(742
X
0.18
0.242
1
m /L
9
Ibs/da y
p. Bar um,
Total
(7440.39-3)
X
0.017
0.023
1
mg/L
Ibs/day
Q. Boron,
Total
(7440-42-8)
X
0.14
0.188
1
mg/L
Ibs/day
r. Coba ,
Total
X
(7440-48-4)
L Iron, Total
(7439-89.6)
X
0.11
0.148
1
mg/L
Ibs/day
L Magnesium,
Total
X
7.5
10.07
1
mglL
Ibslday
(7439.95-4)
. Molybdenum,
To79-9e.7)
X
0.014
0.019
1
mg/L
Ibslday
Total
(7439-96.5)
X
0.12
0.161
1
1
1
mg/L
Ibslday
w. Tln, Total
X
x. Titanium,
Total
X
(7M0.32-61
-
EPA Form 3510-20 (5.90) PAGE V-2 CONTINUE ON PAGE V -3

[PA LD. N(copy from Item I i;7 1/
DUTFALL NUMBER
NCD053488409
001UMBER
CONTINUED FROM PAGE 3 OF FORM 2-C
PARTC- If you area primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark ­X" in column
2-a for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a /secondary industries, nonprocess
wastewater oudalls, and nonrequired GC/MS fractions). mark ••X" in column 2-b for each pollutant you know or have reason to believe is present. Mark'•X•• in column 2-c for each pollutant you
believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results
of at least one analysis for that pollutant It you know or have reason to believe it v-ill be discharged in concentrations of 10 ppb or greater. If you mark column 2b for scrolem, acrylonitrile, 2,4
dinitrophanol, or 2-methyl-4, 6 dinitrophanol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in
concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you mus! either submit at least one analysis or briefly describe the reasons the pollutant is expected to
be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table fair 7 pages) for each outfall. See instructions for additional details and requirements.
1. POLLUTANT
Z. MARK 'x•
3. EFFLUENT -
4. UNITS
3. INTAKE (optional)
AND CAS
NUMBER
ror
b a[-
C [o
a. MAXIMUM DAILY VALUE
b. MAXI M lo
aaa(la°le
ppAY VALUE
C.LONG Tg M
!i °val�aaiee
y .VALUE
a NO OF
[. co Mc[N-
a. LONG
RA
TERM
[
b. NO.OF
(1/aualbble )
a
•,ova
ANAL-
YSES
TRATION
b. MAsa
ANAL-
YSES 4
1�)
(a) cow[[
(�)
cowcawown
lal r
(�1
a.rw wrow
la1
(,) cowc an-
lal rnaa
METALS, CYANIDE, AND TOTAL PHENOLSwrw
Touts 17440--as-0)
X
0.019
0.026
1
mglL
Ibs/day
+t3Arsenic.)Tout
X
< 0.005
< 0.007
1
mg/L
Ibslday
Totall,er0, 74441.7)
X
< 0.001
< 0.001
-
1
mglL
Ibslday
Cadmium,
Total
X
< 0.001
< 0.001
1
mg/L
Ibslday
Chromium,
Tobl (7440-4731
To
X
< 0.002
< 0.003
1
mg/L
Ibs/day
f4C4ppM; total
X
0.022
0.03
1
mg/L
Ibs/day
71%. 1"Tow
(7439-92-11
X
< 0.005
< 0.007
1
m 9 /L
Ibs/da Y
aM. Mercury, Total
(7439-976)
X
< 0.002
< 0.003
1
mg/L
Ibs/day
9M. Nicest, Total
(70"2:0)
X
0.078
0.105
1
mg/L
Ibs/day
Tootal(778249-2)
X
< 0.005
< 0.007
1
mg/L
Ibslday
var, Total
1 44.0-27-4)
X
< 0.002
< 0.003
1
mg/L
Ibs/day
Thallium,
12MTout
Total hailluz ,
X
< 0.01
< 0.013
1
m /L
9
Ibs/da Y
13M.Zinc, Total
(7440-66-6)
X
0.63
0.846
1
m /L
9
Ibs/da Y
cy.-1lea'
Total
Tob
X
< 0.005
< 0.007
1
mg/L
Ibs/day
15M. Pnols,
Tout
X
0.011
0.015
1
mg/L
Ibs/day
DIOXIN
2,3,7A-.TaTFa-
DESCRIBE RESULTS
chledaeibanxo-P-
X
Dlmtln (176"I-B)
EPA Fora 7610-2C (9-90) PAGE V-3 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
1.POLLUTANT z.,MARK'A'
AND CAS
].EFFLUENT
NUMBER •ee• 4 ��- ��'
"�.a
A MA1�'MUMY VALUE MAXI M tpy p//��Y VALUE LLONG T M ll��11((pp VA
.VeWDle
4. UNITS
5- INTAKE (optional)
(it �llabtr) •�«'
evaYeD4 d No.OF
PI ..Aee co«<. i.'i. 11,1 rA.e vises
e. CONCEN-
TRATION4 Mwss
e. LONG TERM p, NO-0r
pl ce««- w1awOC/MS
FRACTION - VOLATILE COMIPOUN
bl .e...ys[s
iV. Acroleln
(107-028)
x<
0.034ug/1
1(107-13-1)
Ibs/day
2V• Acrylonitrlle
X
<
0.0131
ug/1
Ibs/day
3V. Benzene
(71r3-2)
X
<
0.0013
4V. Blr Xhlor
1
ugn
Ibs/day
(542.8MethY8-Ether
X
<2.0
G0.0026
-
1
ug/1
Ibs/day
6V. Bromoform
(76-25-2)
X
G 5.0
< 0.0067
1
6V. Cerbon
ugll
Ibs/day
Tetrachloride
(56-23-61
X
< 1.0
< 0.0013
1
Ug/1
IbS/day
7V. Chlorobenzene
(108-90-7)
X
G 1.0
< 0.0013
1
ugll
Bv-cnloroal.
Ibs/day
b,omar ;t)hene
X
< 5.0
< 0.0067
1
ugll
Ibs/day
9V. ChloroetherM
(75-00-3)
X
< 2.0
< 0.0026
1
ug/1
Ibs/day
IOV. 2-Chloro-
athylOn
(110.75b)Ether
X
< 10.0
< 0.013
1
ug/1
Ibs/day
I IV. Chloroform
(67.66.3)
X
< 5.0
< 0.0067
12V. Dlchloro-
1
u9/I
Ibs/day
bromomethene
(75.274)
X
< 5.0
< 0.0067
13V. Dlchloro-
1
ug/I
Ibs/day
diflu rmethene
1$
X
G 5.0
G 0.0067
1
ug/1
Ibs/day
14V. 1,1-Dichioro-
eth,ne (75-34-3)
X
G 1.0
< 0.0013
1
ug/I
Ibs/day
15V. 1,2-Diehloro-
etnene (107-06-2)
X
< 1.0
< 0.0013
Ug/I
1
Ibs/day
16v, t,1-Dkmoro-
eMylerR (76 35.41
X
< 1.0
< 0.0013
1
ug/I
Ibslday
17V. 1,2-01chloro-
,rover» (7887-5)
X
< 1.0
< 0.0013
1
ug/1
Ibslda y
18V. 1.3-)ichl o
°°^'"' 768j
X
G 1.0
< 0.0013
1
ug/1
Ibs/day
19V. Ethylbenzene
1100-41-4)
X
< 1.0
< 0.0013
1
ug/1
Ibs/day
20V. Methyl
Bromide (7"3-9)
X
< 5.0
< 0.0067
1
ug/1
Ibs/day
21V-Methyl
chlorlde (7"7.3) X I I < 2.0 < 0.0026
1
ug/1
Ibs/day
EPA For[ 3510.2C (6•90)
CONTINUE ON PAGE V-1

r-z1I.TINUED FROM
PAGE V-4 t
1. POLLUTANT
AND CAS
a. MARN •x•
3, EFFLUENT
4. UNITS
S, INTAKE (oprional/
'NUMBER W. MAXIMUM DAILY VALUE
'nor A �`- :V.
. MAXI M
am
Y VALUE
SSG
c.LONG T Me
WQILOY
yp . VALUE
Q NO.OF
N.
w. LONG
T[RM
b. NO.OF
<orcewiwwnow
(a) rwu
conc[nrwwn
(a) rww
)• emu- rirr a).
(I/au./bb4 conce"Twwnon (al r
ANAL-
•- CONC[N-
TRATION
b. MAf3
AV
(al ..!R6-
(al rwq
YfAe
GC/MS FRACTION - VOLATILE COMPOUNDS (eontlnu•d)
CV- M.MyI'"•-2)
ChbrlG'(7=
X
< 1.0
< 0.0013
1
ug/I
Ibslday
23V 11,1,2,2-TM.
aa•
X
< 5.0
< 0.007
1
ug/I
Ibs/day
24V. Tear hloro
•thyl•R. (127.18-4
X
< 1.0
< 0.0013
1
ugll
Ibslday
�V�To31.w
X
< 1.0
< 0.0013
1
ug/I
Ibs/day
28V. 1,2.Tranr
oleh�cethyIMv
X
< 1.0
< 0.0013
1
ugll
Ibslday
27V. 1,1,1-Trl-
chbro.ttl.n.
(71.56-e)
< 1.0
< 0.0013
1
ug/I
Ibslday
28V. 1,1,2-Trl-
ehlorwthaw
P (79-38)
X
< 1.0
< 0.0013
1
ug/I
Ibs/day
.rhyl:: (7"1-e)
X
< 1.0
< 0.0013
1
ug/l
Ibslday
flow T`omftn•n.
X
(76.88-4)
< 5.0
0.0067
1
ug/I
Ibs/day
31V,Vm l
Chlorld. r75-01-4)
X
<2.0
<0.0026
1
ug/I
Ibs/day
GC/MS FRACTION - ACID COMPOUNDS
(97-8)c Pn."°
X
< 10
< 0.013
1
ug/I
Ibs/day
2/1. 2al (120- 3-2
Phw+°� (12P832)
X
< 10
< 0.013
1
ug/l
lbs/day
oh.2. 1 1meth 1.
Phmol(106-6 -9)
X
< 10
< 0.013
1
ugll
Ibs/day
ii: of (534 321)
X
< 50
< 0.067
1
ugll
Ibslday
4-Dlnl phw%*l (61-28-5)
pheno-5
X
< 5Q
< Q,Q67
1
ug/l
Ibs/day
oab."ol
ta
iai
X
< 10
< 0.013
1
ugll
tbs/day
(104Ct �phs"°I
X
- < 10
< 0.013
1
uy/I
Ibs/day
8A, P.Chloro-M-
Cr l (59-So-7)
X
< 20
< 0.027
1
ug/I
Ibslday
eAGPentmhloro-
p W (87.81i-s)
w.?ar..i....
X
< 100
< 0.134
1
ug/I
Ibs/day
•10#�Yh.rwl
f,ser2f...
X
< 10
< 0.013
1
u9/1
Ibs/day
T74
< 20
< 0.027
1
ug/I
Ibs/day
EPA Form 3510-2C (s-90) PAGE Vs CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
I.POLLUTANT 2.MwRK 'x• 3. EFFLUENT
AND CAS
4. UNITS
S. INTAKE (oprinnelJ
/�
NUMBER •tear 4 w`- C we- e. MAXIMUM DAILY VALUE 0. MAXIM M 10 81 Y VALUE c.LON E�M AYRG. VALUE
I eUp111p0 a I YYOIIODIrI LL NO.OF
l LONG TERM
(if available) At., .ANAL
��wwnar ,corc vwrx�rvew Id rya• (a) rue YS[5
cowccn-
bMass
TRATION
corcaw- bNO.OF
I+I rwo YSES(.
GCA W FRACTION - BASE/NEUTRAL COMPOUNDS
18. Acenaphthene
(B3-32-9)
X
< 10
< 0.013
1
ug/1
Ibs/day
28. Arensphtylene
(208-96-8)
X
< 10
< 0.013
1
ug/1
Ibs/day
38. Anthrecene
(12012.7)
X
< 10
< 0.013
1
ugll
Ibslday
48. Benzldlne
(92-87-5)
X
< 200
< 0.269
-"""--
1
ugll
Ibs/day
60. Santa (a)
Anthrepan.
66 66-3)
< 10
< 0.013
1
ugll
Ibs/day
Santo (e
6B. )
Pyrana to (a) )
X
< 10
< 0.013
1
1 ugll
Ibs/day
78. 3,4.Benzo.
Ruoranthene
<10
< 0.013
1
-
(206-09-2)
ug/1
Ibs/day
813. Benzo Ohl)
pervlans
X
< 20
< 0.027
1
(191-24-2)
ug/1
Ibs/day
Flubramhane
X
(207.08-9t
< 10
< 0.013
1
ug/I
Ibs/day
1 OB. BM (2-Chlaro
ethosy) Mathens
—
(111.91-1)
< 20
< 0.027
1
ugll
Ibs/day
11 B. Sis (2-Chlom-
ethyl) Ether
(111-44-4)
X
< 20
< 0.027
1
ugll
Ibs/day
128. Ills (2-Chl rain,
pIAryOEtMr1102-60-1)
X
<20
<0.027
1
ug/1
Ibs/day
13B. 81s (2-Elt yl.
—
hexYl) Phthalate
I1I7d1-7)
< 10
< 0.013
1
ugll
Ibs/day
148.`4-Bromo-
phw(y(I Phenyl
stn«11101aB-3)
X
< 20
< 0.027
1
ug/l
Ibs/day
166 Butyl Benzyl
Phlete 186-08-7
tlg
X
< 20
< 0.027
1
ugll
Ibslday
'188 3C soro-
a1 rol,
X
< 20
< 0.027
1
ugll
Ibs/day
f%
pitanv
-Ma)
X
< 20
< 0.027
1
ug/I
Ibs/day
H15.chryss is
t21841+)
X
< 10
< 0.013
1
ugll
Ibs/day
19B..OWanzo a )
w3-70-3t
X
< 10
< 0.013
1
ug/l
Ibs/day
208. 1,2-Dlchloro-
al.ane (96-5a1)
X
< 10
< 0.013
1
ugll
Ibs/day
218. 1,3Diehlpto-
anzeM (541-73-1
X
< 10
< 0.013
1
ug/1
Ibs/day
EPA Form 2510-2C (8•90)
PAGE V-6 CONTINUE ON PAGE V-7

CONTINUED FROM PACE VA
1. POLLUTANT
AND CAS
x. MARK 'X•
3. EFFLUENT
6. UNITS
S. INTAKE (opfionelJ
NUMBER e... �- - e. MAXIMUM DAILY VALUE
`eiwr
b. MAXIM M
/ eVol
Ey D/�y VALVE
C.LONG T� M
(!
//g�yypp VALUE
!f/eVeiMblfl o`w ii.•.r PI III u
OC/MS FRACTION a
-RASE/NEUTRAL
LLANALL-
yeES
e. CONCEry-
TR^TION b. MAes
G TERM b
O. LONG .ryO,OF
ANAL-
i'I`
III
oVellebl[�
COMPOUNDS (eonllneed,•
Yscs
'qlL. 1,44Dkhloro-
?sVIma 086-46-7 X < 1.0 < 0.0013
$$8 3,3'•Dkhbr
1
ug/1 Ibs/day
( X < 40 < 0.054
1
ug/1 Ibs/day
p4Q.:. EMI
184-W2)
X
< 10
< 0.013
1
ug/1
Ibs/day
Byi
X
< 10
< 0.013
1
Ug/1
Ibs/day
X
< 10
< 0.013
1
ug/1
Ibs/day
27,6; 2,4Dinitro-
X
wIyM1'.(t2t-14-2)
< 10
< 0.013
1
ug/I
Ibs/day
281L2,6-Dlnitro-
X
wliMIMI (60o-20-2)
< 10
< 0.013
1
ug/I
Ibs/day
29B. P(-NOctyl
t1 na
(Ir 7.8 fe40t
X
< 20
< 0.027
1
ug/I
Ibs/day
308; 1,2-Wpheny4
hydieglrw (a Ago•
baiuene) (122-BB-7
X
< 20
< 0.027
Ibs/day
1
u /I
9
31 &� FlDonntMne
X
(2054")
< 10
< 0.013
1
ug/I
Ibs/day
328. Fluorens
X
�Bsa37)
< 10
< 0.013
1
ug/f
Ibs/day
(U8:741) =
X
< 10
< 0.013
1
ug/1
Ibs/day
348. N...
ellidrolwtediene
(87 BB 31
X
< 10
< 0.013
1
ug/1
Ibslday
368. e
cnIop toddle e
(77-47entediene
(n 47 4)
x
< 40
< 0.054
1
ug/I
Ibs/day
368. NeAechloro-
ethelw (67-72-1)
X
< 10
< 0.013
37B. indent,
--
1
Ug/1
Ibslday
(1.2.3-ad) Pyrene
(193.39-5)
X
< 10
< 0.013
1
ugll
Ibs/day
388. Iwphorone
(78-69-1)
X
< 20
< 0.027
1
ug/I
Ibs/day
H 820-3jNaphthalene
X
< 10
< 0.013
1
ug/I
Ibslday
40B(9B . 3) benzene
y
A
< 10
< 0.013
1
ug/1
ibs/day
41B. N-Nltro-
todimethylemine
(62-78-9)
X
< 20
< 0.027
42B. N-Nibowdl-
1
Ug/1
Ibs/day
N 621-84-7 -ProPYlemine
X
< 20
< 0.027
1
ug/1
Ibs/day
EPA Form 3510-2C
/E.onl
CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
F. [.POLLUTANT x. MwgK 'x'
AND CAS
3. EFFLUENT
4. UNITS
5. INTAKE (ilptwwf)
NUMBER r Lea- c ea'
Lai
L MAXMIUM DAILY VALUC •MAXI M 00 O�Y VALUE 0.LONG Tp,pM 1(p�i VALUE
NO.OF
aVC(IaL a (1/aYa1�001aJ ;A-0
a. LONG TERM h.MO.OF
fl/eaalbelel u�w- iiri♦ wa
a' CONCFN' L MA53
TR ATION
LANAI'
1') °
lalr
Ian. wa
Irl
c o..0 r.rw •naw
la).
1"
PI w•
ANAL-
YSES
GC/MS FRACTION - BASE/NEUTRAL
COMPOUNDS Nmtinued)a
TMATPDN IaI YSES
43B. N-NKro-
mdlphenylamine
X
< 20
< 0.027
1
(85368)
ug/I
Ibs/day
e5-01-8 unthnm
X
< 20
< 0.027
1
ugll
Ibs/day
45B. POoo)
X
< 20
< 0.027
1
ugll
Ibslday
468. 1,2,4- TrF
°1h1Qre°!iEe e
X
< 20
< 0.027
1
ug/I
Ibs/day
GCRAFRACTION - PESTICIDES
P Aayr�
j �?
X
< 0.05
< 0.00007
1
ug/I
Ibs/day
2p,.
2r o611D
44
X
< 0.05
< 0.00007
1
ugll
Ibs/day
a1127)
X
< 0.05
< 0.00007
1
ug/I
Ibslday
4V:'y•BNC
(66.69-9)
X
< 0.05
< 0.00007
1
ugll
Ibs/day
(3194")
X
< 0.10
< 0.00013
1
ug/I
Ibs/day
6P. Chlordene
(57-74-9)
X
<0.50
< 0.00067
1
ug/I
Ibslday
16o-93 2)
X
< 0.10
< 0.00013
1
ug/i
Ibs/day
SP. 4,4'-DOE
(72-55-9)
X
< 0.10
< 0.00013
1
ug/I
Ibs/day
9P. 4,4'-DDD
(72-54-8)
X
< 0.10
< 0.00013
1
ug/I
Ibslday
1 OP. Dleldrin
(Bo 67-1)
X
< 0.10
< 0.00013
1
ugll
Ibslday
I IP. a -Endow Men
(115-29-7)
X
< 0.10
< 0.00013
1
ug/I
Ibs/day
t2P.0-Endomlten
1115-29-7)
X
< Q.10
< 0,00013
1
ug/I
Ibslday
13P. Endomitan
SoMate
(1031-073)
X
< 0.10
< 0.00013
1
ug/I
Ibs/day
14P. Endrin
(72.2")
X
< 0.06
< 0.00008
1
ug/I
Ibslday
ISP. Endrin
Aldehyde
(7421-93-4)
X
< 0.10
< 0.00013
1
ug/I
Ibs/day
16P. Heptachlor
(78-443)
X
< 0.05
< 0.00007
1
ug/l
Ibs/day
EPA Form aaly-2C ie-iv)
CONTINUE ON PAGE V-9

EPA I.O. NUMBER (copy from item 1 Or Form 1) OUTFALL NUMBER
CONTINUED FROM PACE V-B Llcrnne7400enn
- VJJYV VYVJ UUI
L POLLUTANT 2. MARK X. 3. EFFLUENT
AND CAS
4. UNITS
NUMBER T G w�- we- t. MAXIMUM DAILY VALUE MAXI Ma a o Y VALUE C.LONG TE/1M /�ypG VA UE
N R SG, d. No. OF
��e
5. INTAKE (Jprion4l)
e.
(1/oVOIWDIe
(17 auell.Dle/ u:w iinr 1�1
ew ANAL-w• 1�1 r coxcew�ixw ♦rox Irl r wow Irl r. YSES
L CONCEN.
TRATION MASS
LONG TERM b. NO.Op
Irl c ANALco"cE-
OC/MS FRACTION — PESTICIDES (Conitnoed)•
Irlrwp VSEs
17P. H"P hl.,
EPDXId. X < 0.80 < 0.0011 1
(102"7.3)
ug/I Ibslday
(53iess1.9)
X
< 1.0
< 0.0013
1
ug/I
Ibs/day
IOP. PCB-1254
X
(11097-69-1)
< 1.0
< 0.0013
1
ug/i
Ibslday
20P. PCB-1221
%<
----
(11104-28-2)
< 1.0
< 0.0013
1
ug/I
Ibs/day
11141 %sit
X
< 1.0
< 0.0013
1
ug/I
Ibs/day
ze-6j B
X
12672
< 1.0
< 0.0013
1
u /I
9
Ibs/day
23P. PCB-1260
X
(11090-82-5)
< 1.0
< 0.0013
1
ug/I
Ibs/day
6X
< 1.0
< 0.00131Tox<
R674---iisi
han.1-35.2> %<
< 1.0 < 0.0013
1
ug/1
Ibs/day
:PA Form 9510-20 (9-90)

EPA I.D. NUMBER (copy from Item 1 Of Form 1)
PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of
this information on separate sheets (use the same formed instead of completing these pages.
SEE INSTRUCTIONS.
NCDO53488409
V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page J of Form 2-Cl
OUT FA LL NO
002
PART A - You must provide the results of at least one analysis for every pollutant in this table.
Complete one table for each outfall. See instructions for additional details.
2. EFFLUENT
3. UNITS
4. INTAKE (optional)
1. POLLUTANT
a. MA%IMUM DAILY VALUE
- MAXI M ]0
avai1la
OAY VALUE
e
C•
• V LU
(sDeci{v (f blank)
a. LONG
TERM
aTNATION
b. MASS
I avar a
I�)
t
(a) r
d. NO. OF
ANALYSES
b NO. OF
ANALYSES
Irl
(aj r^fe
conca:�in wr�on
ia) r^ea
(�)
(r) r
a Biochemical
Oxygen Demand
(DOD)
2.0
6.41
1
mg/L
Ibslday
b. Chemical
Demand
77
247
1
mg/L
Ibslday
Oxygen
c. Total Organic
Carbon (TOC)
7.2
23.1
1
mg/L
Ibs/day
Total oTs
d.T
d. l Suspended
Solids S
18
57.65
1
mg/L
Ibs/day
e. Ammonia (as N)
1
mg1L
Ibslday
1, F bw
VALUE
VALUE
VALUE
VALUE
0.384
0,176
0.093
50
MGD
a. Temperature
VALUE
VALUE
VALUE
VALUE
(winter)
20.2
15.6
12.4
25
°C
_
h. TempNature
VALUE
VALUE
VALUE
VALUE
(aammer)
30.4
28.7
25.5
25
°C
MINIMUM
MAXIMUM
MINIMUM
MAXIMUM
i.PH
6.4
7.2
6.4
7.2
50
STANDARD UNITS
PART 8 - Mark "X" in column 2-a for each pollutant you know or have reason to believe is present. Mark " X-in column 2-b for each pollutant you believe to be absent. If you mark column 2a for any pollutant
which is limited either directly, or indirectly but expressly, in an afNuerd limitations guideline, you must provide the results of at least one analysis for that pollutant. For otherpollutants for which you mark
column 2s, you must provide quantitative data wan explartation of their presence in your discharge.
Complete one table for each outfall. Seethe instructions for additional details and requirements.
I. POLLUT-
Z. MARK 'X'
3. EFFLUENT
4. UNITS
S. INTAKE (optional)
ANT AND
CAB No.
e, V`.
b`V:
`ecnr
• MAXIMUM DAILY VALUE
b. MAXI M ]
y
1/aW
p/� Y VALUE
elC
C. N
T M VALUE
/t /�y
1/aV011aO l?
a
e. LONG TERM
AVERAGE VALUE
NO.
(1/auoaabR)
ANAL
a. CONCEN.
TRATION
b. MA55
ANA
'
lal rwaa
la) rep
I'
Conce NrwwTow
wwTow
°encanrwwrlon
la) rwaa
YSES
conce.rwwnon
Ia) rwu
YSES
a. Bromide
(24959-67-9)
X
b. Chlorine,
Total Residual
X
a Color
X
< 25
NIA
1
ADMI
N/A
d. Facal
Coliform
X
a. Fluoride
(15984-48.6)
X
0.14
0.188
1
mg/L
Ibslday
f. Nhreta—
Nhrhe(MN)
X
0.42
1.35
1
mg/L
Ibs/day
EPA Form 3S10-2C (8-90) PAGE V-1 CONTINUE ON REVERSE

ITEM V-0 CON71NLIEO FROM Farrar?
iy >. .. .....
T AND
'VAS NO.
(IlaPaBabA)
ol.Nhro9anr
Tg1�I organic
(4a 11
3. ARK N�X.
.�i. �,»`-
iii. ai«•
X
3. EFFLUENT
a• MAXINUM DAILY VALU[ •MAXI M f0 p/ty yALU[ 0. p ny A
[N+a/b4ie /mt11W4 4ANA�-
4. UNITS
&CONC[N- e. MAss
TRATION
5. IN T AKE(optim,W)
�oqG T[ q
AV[R AGC VATU[ NO. OF
ANAL-
co»c ae.w wno» (0 • YSEs
,
•,ox
(al N.0
cowcxxiw
I,Ix
Vales
R OP and
OnM
L PhD4hOIV9
X
5.2
16.65
1
mglL
Ibslday
fa. p), TotN
(7723-14.0)
X
< 0.10
< 0.32
1
mglL
Ibslday
I. RadiPActiuky
11)'Alpha,
Total
X
(2) Saw,
Total.
v
A
(3) Radium,
Total
X
141 Radium
226, Total
X
k. Suff w
(a. SO )
(14808t798
X
18
57.6
1
mg/L
Ibslda y
SUMIde
(.8)
X
m. SU1
(ca SO3)
(14265-45.3)
X
n. Surfactant.
X
< 0.10
< 0.32
1
mg/L
Ibslday
o. Aluminum,
Total
(7429.90.5)
x
P. ar um,
Total
(7440.39-3)
p- Boron,
X
0.025
0.08
1
mg/L
Ibs/day
Total
(7440.42-8)
r. MO
X
0.054
0.17
1
mg/L
Ibslday
Total
(7440.48-4)
�F
X
a Iron, Total
(743989.6)
X
0.97
3.1
1
mg/L
Ibslday
t. Maanealum,
Total
(7439-95-4)
. Molybdenum,
X
3.3
10.6
1
mg/L
Ibslday
Tow]
(7439-98-7)
X
V. an0an1 ,
Total
(7439-96.5)
X
0.092
0.29
1
mg/L
Ibslday
w. Tin, Total
(1440-31.5)
X
c. Titanium,
Total
(7440-32-6) X
FDA P.— 1cm_1n .
PACE v_e
PACE
- CONTINUE ON PAGE VV •3

EPA 1.0, NUMBER (copy from Item 1 o/Form 1)
OUTFALL NUMBER
NCDO53488409
002
CONTINUED FROM PAGE 3 OF FORM 2-C
PARTC- If you area primary industry and this outfell contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions for. "X"
you must test Mark incolumn
2-a for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. It are not required
you to mark column 2-a (secondary industries, nonprocess
wastewater ourtalls, end nonrequired GC/MS fractions/, mark' X" in column 2-b for each pollutant you know or have reason believe "X"
to is present. Mark in column 2-c for each pollutant you
believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must the results
provide
of at least one analysis for that pollutant If you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, 2.4
acrylonitrile,
dinitrophenol, or 2-methyl-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that discharge in
you
concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you mus! either submit at least one analysis or briefly describe the reasons the is expected to
pollutant
be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table /a//7 pages) for each outfell. See instructions for additional details and requirements.
I. POLLUTANTLz. MARNx•3.
EFFLUENTAND CAS
4. UNITS
3. INTAKE (optioal)
opt /1 yp
NUMBER T ��i �� a.MAXIMUMDAILY VALUE b.MAXI Mellebr yYALUE C.LONGT OIb01 VALUE d NO.OF
bl lab1
a. LONG TERM
ANAL-
aualbak) - iiwi ei'!r aonu:iwwnow lal«wee UI (.1. Iq P)..ee vsEs
a' CONC[N- b. MAss
TRATION
b. NO.OF
ANA4(U
pl concxn-
coecanrwwnon cmcenrnwnon
METALS, CYANIDE, AND TOTAL PHENOLS
I
ww non b r VSE54
1 M. Antimony,
Total (7440-36-0)
X
2M. Areenle, Tout
(7440-38-2)
X
3M. Beryllium,
Total, 7440-41.7)
X
4M. Cadmlum,
Total (7 AAn 43-9)
X
SM. Chromium,
Tau] (74411 47.31
X
f74/6aP8)TOW
X
7111. LfttToW
(7439-92-11
X
SM. Mercury, Total
(7439-97-6)
X
9M. Nickel. Tout
(744"2.0).
X
_
10M. Wei,Wm,
Tau) (7782-49-21
X
11 W 411ver, Tool -
(744(>•27�q
X
/2M. Thelllum,
Ton( (7440.28-0)
X
13M.--Zlne, Total
(7440-666)
X
0.015
0.02
mg/L
Ibs/day
14M. Cyanide,
Tout (57-12.61
X
IBM. Phenols,
Tout
X
DIOXIN
2,3,7,11-Ter s, DESCRIBE RESULTS
chlgodibenxo-P-
X
Dicain (178a-01-e)
EPA Fortin 3619-2C (11-90) PAGE V-3 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
f. El"IME r A Nr
AND CAS
NUMBER Ii��'
tl/aue[e6te/ wi,i- �iwr
e
aa.- AMA%IMUM DAILY VALUE
ii. w�� 1•I rwe.
x a ♦wwtmn
3.
MART Mw1a
eewaex.w w.,ex
..
EFFLUENT
WVVALUE
1.1 rwe.
GLDNGT MAA��(tpp VA [
euailaDle
I�1
enneaxv u�ox 1•I '•wu
d No. OF
ANAL-
YSES
4. UNITS
�. CONCEN-
TRATION
h MAs[
S. INTAKE
A. LONG
(optional)
TERM
b. NO.o1
wNw4
YSES
OC/64B FRACTION —VOLATILE
IV. Aeroteln
(107-028)
COMPOUNDS
X
1�l eoxur
I.) rw.e
2V. Acrylonitrlle
(107-13-1)
X
3V. Benzene
(7143-2)
4V. 81e (Chloro-
methyl) Ether
(54288.1
X
X
5V. Sromoform
(75.26-2)
6V. C.rbon
X
'
Tetrechlorlde
(56-23-5)
X
-
7V. ChImobenieM
(108-90-7)
8V. Chlorodl-
bromomethane
(124418-1)
X
X
8V. Chloroethene
(75-00-3)
10V. 2Chioro-
X
ethyWinyl Ether
(110-758)
X
i IV. Chloroform
(6746-3)
12V. Dichlom.
bromomethene
(75.27-4)
13V. Dichloro-
dllluorom"t,.n.i
(75-718)
X
X
X
14V. 1,1.Dlohluro-
ethane (75-34-3)
X
15V. 1,2-Dlehloro.
etheM (107-M2)
X
16V. 1,1-Dichloro-
ethylene (75.35-4)
X
17V. 1,2-01chloro-
Propene 17647-5)
X
16V. 13)id4ao-
PAV/Wm(W2.764)
X
18V. EthYlberraene
(100.41.4)
X
20V. Methyl
Bromide (7483-8)
X
21 V. Methyl
Chloride (7487.3) X
EPA- Form 3510-2C (E•90)
.......
CONTINUE ON PAGE V-;

CONTINUFn FRIW PAG. v.A
4,POLLUTANT S. MARK'X'
AND CAS ]. EFFLUENT
NUMBER ,moo• n.aa- ,��� L MAXIMUM DAILY VALUE 'MAXI OM OD /IY VA UE C.LONG T M Ayp . VALUE
Yp N C NO.OF
�. UNITS
5. INTAKE (opriona)J
yypyOOy
::N-
(uauN)e6R) auw. • aiwY wiA ANA4
Id rAaa
ACONC[N• n MAss
F. LONG TERM o.NO.OF
wvew cowun•nwnor Irl rwaa wcsnrwoww Irl rwaa YSEE
OCJMS FRACTION —VOLATILE COMPOUNDS (eonNnu[d)
TRATION
(d [owcaw. Irl rwas YEEE
22V. Methyl[M
-
ChlSrWe (75-09-2)
x
23V.:, t,l,i,3-TwE-
ifIE11E
X .
(794
(79J4:5)
24V. T4tr[ehloro
"I4M (127-18-41
X
25V. Tolua*
410048-3)
X
28V. 1,2-TrEnr
Olehloro[thylEM
X
,
(156 0-5)
27V. 1,1,1-Trl-
chlotowthEM
V
A
(7145.8)
28V. 1,1,2-Trl-
chloroethEM
X
(79-0DS)
29V. Trichloro-
[thYIEM (79-01-6)
x
30V. Trlchloro-
11UOrORNthSM
V
(7&59.4)
A
31 V. V inyy1
X
Chlor" (75-014)
OCAU FRACTION — ACID COMPOUNDS
IA.2-Chloroph"o
(911474)
X
2A. 2,4-DKMoro-
"ol (12683-2)
X
'
3A. 2,4.)4MthyI-
PhMWl(10547-9)
�(
o-0
CtMal(534.5
Crgol l534-52-1)
X
SA.2,4Dlnitro•
Phenol (51-28-5)
X
8A. 2-Ni"phenol
(88.754)
�(
7A 4Nltrophonol
(100-02.7)
X
BA. P-Chloro-M-
Cm01159-50-7)
�(
�A;P4nt�ehbro-
p*IMr10[(574651
X
-10A:.PhEMI
f1,11�45y.2)..
X
T/i-
_ i.
X
Yes
EPA Form 3510_9C
rE-go
PAGE
v_c
__
_ _
1- "'i - ---- ' CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
I.POLLUTANT a. MAPH X. 3. EFFLUENT AND CAS
NUMBER L MAXIMUM DAILY VALUE B. MAXIM M SO DAY VALUE GLONc TEpM eypp VALUE
(I/ouelleblr) viw ii:T suer eua a r (./aaallanifl' .1 ND.oi
I.. lal r Id _ AnA4
GC/MS FNACTIO lal 'I
N— BASE/NEUTR.LCOMPOUNDS ATJO�(')" rscs
4. UNITS
a. CONC[N-
TRATION b. MASS
S. INTAKE (uplimmf/
a Lonc TERM b. NO. OF
An
I'l� Dlr V5E5
B. Acenaphthene
(83-32-9)
X
28. Acenephtylene
(208-968)
X'
'
38. Anthrecene
(120-12.7)
X
4B. BentlClne
'---
(9287-5)
X
58. Bento (4)
Anthr c.ne
56-55-3)
X
66. Benro (a)
PyreM (50.328)
X
7B. 3,4.Benro.
fluorenthen,
(20649-2)
X
-
80. Banzo (rhl)
Pwylene
(19 f •242)
X
as. servo (k)
Fluoranth.na
(207-08-9)
X
1 OB. BM (2-Chlonu
Mary) Methane
(11t-9t-1)
X
11 B. BIa (2-Chloro-
ethyl) Ethw
(111�4-q
X
128. 6h j2-Chk iw
pgrrOEthw(102-50.1)
X
135. 84 (2-Ethyl-
hesYl) Phthalate
(11741-7)
X
phy�jfl Phenpq PiHm l
yl
ithM'(10165-3)
-15Bi.Butyl
X
ll r yl
11170 Bleb (8588-7
X
I106AL4bro-
"
X
SOW yl
M3)
X
'?l86 GMyrrle
Y218,e1.a1
X
19 lllbeMo a 1
:AntMeeeM
(53-70-3)
X
206. 1,2-Okhloro-
be1DeM(95-50-1)
X
210. I,3-DlchJoro-
b.mr (541-731
X
EPA Form 5510.2C (9-90) PAGE V-6 CONTINUE ON PAGE V-7

CONTINUED FROM PAGE V.6
I. POLLUTANT
T. MARN •X'
AND CAS
NUMBER
•�� �` ��" <<�i'
`wiirt
]. EFFLUENT
a. MA%IMUM pA1L1 VALUE b. MAXI M ]O p/+Y VALUE C.LONG TE M .1yp VALUE
apa 4 (1 eVnllYbl[� LL NO OF
4. UNITS
S. INTAKE (iPrionol/
(//auoiloblc)
uu- Kiwi+
a. CONCEN
4. LONG TERM b. NO.OF
�,� 1d u•
COMPOUNDS (ton Nnuad,•
hI
wcz«'.Iw..,o.
Id .•
ANw L-
yscs
OC/MS FRACTION-
BASEINEUTRAL
TRATION b MAST
1,1 wNw4
1+I .. rscs
1,}Dlchloro-
-.fie.'
, am (106.464
X
-338:3,3'-Dbhlor
'�1834iF11'-' -
X
OkthYl
X
J"44 21
-Butyl
-
X
2,4-Dlnii ro
tp� ,121.14-2)
X
"28B:Z,6DInhYo-
t.Z(W&2D.2)
X
2811. DI-N-OcWI
Phow"Its
X
(117.84-0)
308: 1.2-Dlphonyl.
hydmlm (m Azo-
X
bsnzene)(122E67
311L Flu4nnthana
(206-44-0)
X
32B. Fluorana
(eaa�a-7)
X
33& Ascodgwobinioni
IM&7.4-.1).,.
�(
34B. Hsu
ehlorobuudlana
X
(8168.31
358. Haxachloro-
CYOl ntadlsne
X
(77-47-4)
368. Hexachloro-
othene (67.72.1)
X
376. Indano
--
(1,2,3-td) Pyrons
X
(193.39-6)
38B. Iwphorons
(78-59-1)
X
39B. NEPhthslana
(91-20-3)
�(
408. Nhrobanzana
(98-95-3)
X
41 B. N-N Itro.
wdlmathYlamTne
X
(52-75-9)
42B. N-NlVowdi-
N-Propy1 mina
X
62164-7
_
VISA
" "+ `^""" CONTINUE ON REVERSE

CONTINUED FROM TNF FRONT
UTANT z. MARK 'X 3. EFFLUENT CAS
BER • ����' ww' A. MAXIMUM DAILY VALUC •MAXI f u 1U p/aY VALUE C.LONG TF.pM /�ypG VALUC
lbb4/ 'r filar pl<I7"',L-fONCEN..
(l 'ANAS
COMPOUNDS(con tinued)vsE
FPhemnth�e
4. UNITS
eTRAT10N b. MASS
i. IN TgKE /eprinnaf)
LONG TERMiex•
(,Ic bANAOrRACTION—wBASEMEUTRAL
I:1 .. usesro-
l4mine
nthrene
X
488. pyreni
(12Pu0-0)
�(
t.2.4. Trl-
awrep ;e�e X
RClM�FRACTION - PESTICIDES
». A�1`ln _
(�'�4� X
(#1PalFt- )
X
3P• P�-.B9NC
(31985'7) X
4P: -9NC
(68439:-9)
X
6P. 3-1iHC
(319-86-8)
X
.
8P. Chlordane
(57-74.9)
X
7P. 4,4'-DDT
(50-293)
X
8P. 4,4'-DDE
(72a5.9)
X
9P. 4,4'-ODD
(72-548)
X
I OP. Dbldrin
(60-87-1)
X
1/P. 0-Endowlfen
(115-29.7)
X
12P. P-Endow Kan
(115-29-71
X
I3P. Endowifan
Sut(aw
(1031-07-0)
X
14P. Endrtn
(72-20-9)
y
A
16P. Entlrin
Altlahyda
(]421-93-41
X
16P. Nepischlpr
(76443) X
EPA Fore 3510.2C (6.901
PAMP
v-a
CONTINUE ON PAGE V-9
aW

EPA 1.0. NUMBER (Copy from Item I of Foam I/ OUTFACE NUMBER
CONTINUED FROM PAGE V-A hlrnneawoo wnn
VUL
I. POLLUTANT"or
3. EFFLUENT
AND CAS {I o /�
NUMBER. MAXIM VM OAILY VALUE • MAXI VWnllepk) VALUEC.LONGTERMurf. VALU d NO.OF
'I 61e
4. UNITS
5. INTAKE (,IPNona!/
1I ollaG 1 ANAL.
I�
(a) rwsaDI
• CONCEN-
b. MASS
e. LONG TERMOfewllebUj b. NO.OF
.Lexr.ATlex (a) r.n I'I (d rww• YSES
GC/MS FRACTIONnoed)17P.
TRATION
xxcex AN L-
YS
H"chlorEpoxide(102437-3)
?BP. PCB-1242
(53469-21-9)
19P. PC13-1254
(11097-69-1)
X
20P. PCB-1221
---
(11104-28.2)
X
.
21P. PCB-1232
(11141-16-5)
X
22P. PCB-1248
-
(12672-29.6)
X
23P. PCB-1260
—
--
(11098-82.6)
X
24P. PCB-1016
(1267411-2)
X
25P. Toxyhene
�F
(8001-35-2) v
:PA Form 3510.2C (5.90)

EPA Form 2C
Additional/Supplementary Information
Performance Fibers, Inc.

Item H. A.
Water Flow Line Drawing

A
Discharge
NO. 002
(113 GPD)
113
Stem a
Boi
14
Compressor
and Steam
Condensate
Storm
Water
Air Dryer
HAW
RIVER
v
1261 8
4
Overflow Fire _(
v Pond ol
33 A
v A
Q�
MR
Potable
4Wa2
Oa Mist
1.5 Alr P011utlon
Control
System
1.0 Oil
Pre -Treatment
— 0 WATER D.
--fl EVAPORATION --0•
—b STEAM—�
IN OIL
0.2
Alum
4.7
6 Settling
Pmd
� 4.e
1.0
5.75
000Bnp
to
Towers
827
ran,
Beam
t1
TW-1, 4. S. a
Cleaning
23.3
10
1.0
.
Was7j:tWA�DsnCfan
`03.05 GPD)
Tr
i 0.25
`Y
Concentrated
Oil Emulsion
"Stopped Off -aft
PERFORMANCE FIBERS, INC.
NEW HILL, CHATHAM
COUNTY
NORTH CAROLINA
NPDES Permit No. NC0001899
Distha ge
N0. 001
,(82 GPD)
NOTE: Flows are listed in units
of thousands of gallons.

Item II. B. Outfall Descriptions
Outfall 001
Performance Fiber's Moncure, North Carolina facility operates a 0.244-MGD wastewater
treatment facility with the following components and with final discharge through Outfall 001 to
the Haw River:
• Sanitary Flow Bar Screen and Grinder
• Process Wastewater Bar Screen
• Neutralization Chamber
• Aeration Basin
• Clarifier
• Sludge Drying Bed
• Optional Polishing Pond
• Chlorine Gas Disinfection
• Chlorine Contact Chamber.
Two separate pipelines transport process and sanitary waste to the wastewater treatment plant.
Process wastewater comes primarily from non -process cooling tower blowdown with smaller
contributions from the following: steam condensate, regenerated water from water softeners,
demineralizer blowdown, water rinse from polyester parts cleaning operations, stormwater from
raw material handling areas, finish oil pretreatment (ultrafiltration permeate), beam cleaning and
manufacturing building floor drains.
Sanitary wastewater comes primarily from plant restrooms, cafeteria, and custodial sinks. The
plant has a separate sanitary collection system that flows to a lift station. Sanitary waste is
blended in a comminutor, or the comminutor may be bypassed in the event of a mechanical
failure and the flow would be directed through a bar screen. From the lift station, the sanitary
influent is pumped directly into the aeration basin.
The process wastewater flows into a lift station adjacent to the sanitary lift station. It is then
pumped into a 1,200 gallon neutralization/mixing basin at the north end of the aeration basin. A
mixer provides thorough mixing to keep settleable solids in suspension and to aid in the
dispersion of pH control chemicals. A pH probe is used to measure influent pH and transmits a
signal to the pH analyzer/controller. The pH controller regulates the speed of a sulfuric acid
pump, which is used to control pH. The mixing basin then discharges through a 6" pipe into the
aeration basin.
The aeration basin has a capacity of 650,000 gallons and contains four surface aerators to
introduce oxygen into the water and provide mixing horsepower.
Water from the aeration basin overflows a weir into a 20' diameter clarifier. The clarifier is
designed with a surface overflow rate of 440 gallons/ftz/day. A liquid coagulant is added to the
water as it flows from the aeration basin to the clarifier to aid in solids settling. The clarifier is
equipped with surface and bottom sweep arms. The surface sweep arm directs floating solids to a
scum pit. The bottom sweep rakes sludge to be recycled or wasted. Sludge pumps remove settled
solids from the bottom of the clarifier and either pump the recycled sludge back to the aeration
basin or waste it to the sludge drying beds.

Clarifier overflow can be valved to a one -million gallon capacity polishing pond for additional
solids removal or directly into the chlorine contact chamber. Thus, overflow form the clarifier,
water from the polishing pond, or a blended flow from both structures enters a 9' X 37' X 3'
chlorine contact chamber that is designed for a minimum of 30 minutes contact time at a flow rate
of 90 gpm. The chlorinators located in the wastewater treatment plant lab building are manually
controlled and the chlorination room is equipped with a chlor-alert alarm system. Chlorine is
supplied to the chlorinators through scale -mounted 150 lb. cylinders. Chlorine recirculation
pumps transfer water from the effluent end of the chlorine contact chamber and supplies the
diluted water through the chlorine injector. The chlorinated water is returned through a
submerged diffuser to the influent end of the contact chamber.
Effluent flow from the chlorine contact chamber is measured before it enters an underground
pipeline that discharges directly into the Haw River.
Outfall 002
Stormwater, steam condensate, air dryer condensate, and fire pond overflow discharge through
Outfall 002 to Shaddox Creek. The drainage system which reports to Outfall 002 includes a
system of baffles and weirs designed to contain accidental spills of oil. In an emergency, flow
can be contained in a holding pond and pumped to a storage or pumped to the process sewer.

Item III. A & B. Production
On November 5, 1987 EPA issued regulations establishing effluent limitations for the Organic
Chemicals, Plastics, and Synthetic Fibers (OCPSF) industrial category. Provisions of Subpart C
(414.31) and Subpart I (414.90) Direct Discharge Point Sources That Use End -of -Pipe Biological
Treatment are applicable to process wastewater discharges from the manufacture of polyester
fiber and resin. OCPSF effluent guidelines are not expressed in terms of production. No metal -
bearing waste streams or cyanide -bearing waste streams listed in Appendix A to Part 414 exist in
the manufacture of polyester fiber and resin.

Item V. A-C.
Characteristics listed in Item V reflect data from January 1, 2005 - January 25, 2006. For some
parameters, testing was conducted throughout the year, while other parameters were tested
annually. One time testing was conducted for most of the parameters.

Item VI.
The following is a list of Item V-C pollutants that are present on the plant site. None of these
materials are used as a raw material or intermediate and none of these materials are manufactured
as a product or a by-product of the manufacturing process. The list may not be exhaustive, as
some commercial products are considered proprietary by the manufacturer and their specific
composition is not known to us. In addition, some new materials may be obtained in the future
that contain one or more of the listed chemicals and whose composition may not be known to us.
Pollutant
Use on Site
Antimony
Lab Reagent
Chromium
Lab Reagent
Copper
Lab Reagent
Lead
Lab Reagent
Mercury
Lab Reagent, Instrumentation
Nickel
Lab Reagent
Silver
Lab Rea ent Electrical Equipment
Zinc
Lab Reagent
Phenols
Lab Reagent
Carbon Tetrachloride
Lab Reagent
Chloroform
Lab Reagent
Dichlorodifluoromethane
Lab Reagent, Refrigerant, Leak Checks
1 1 2 2-Tetrachloroethane
Lab Reagent
Tetrachloroeth lene
Solvent
Toluene
Lab Reagent
1 1 1-Trichloruethane
Solvent
Trichloroeth lene
Solvent
Phenol
Lab Reagent
Dichlorobenzene
Lab Reagent
1 2 4-Trichlorobenzene
Electrical Equipment
PCB
Electrical Equipment

W A7F9
0
ww� —{
ee� �
January 31, 2006
Mr. Charles E. Powell, Jr. REM
Environmental Engineer
Performance Fibers, Inc.
338 Pea Ridge Road
New Hill, NC 27562
Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Alan W. Klimek, P.E. Director
Division of Water Quality
r
Subject: Receipt of permit renewal application
NPDES Permit NC0001899
Performance Fibers, Inc.
Chatham County
Dear Mr. Powell:-
The NPDES Unit received your permit renewal application on January 30, 2006. A member of the
NPDES Unit will review your application. They will contact you if additional information is required to
complete your permit renewal. You should expect to receive a draft permit approximately 30-45 days before
your existing permit expires. The requirements in your existing permit will remain in effect until the
permit is renewed (or the Division takes other action).
If you have any additional questions concerning renewal of the subject permit, please contact me at
[phone], extension 520.
Sincerely,
Frances Candelaria
Point Source Branch
cc: CENTRAL FILES
Raleigh Regional Office/Surface Water Protection
NPDES Unit
cw
No-'`o'i Caro ' a
a r1
North Carolina Division of Water Quality 1617 Mail Service Center Raleigh, NC 276994617 Phone [phone] Customer Service
Internet h2o.enrstate.nc.us 512 N. Salisbury St. Raleigh, NC 27604 FAX [phone]
An Equal Opportunity/Affirmative Action Employer— 50% Recycled/10% Post Consumer Paper

Performance f'
January 27, 2006
Mr. Charles H. Weaver, Jr.
NC Department of Environment & Natural Resources
Division of Water Quality
NPDES Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Subject: NPDES Permit Renewal Application
Performance Fibers, Inc.
New Hill, Chatham County, North Carolina
Permit # NC0001899
Dear Mr. Weaver:
J N 3 1 2006
Performance Fibers is requesting renewal of its NPDES Permit (NPDES Permit No. 0001899) per Federal
Regulations 40 CFR 122.41, and North Carolina Regulations (15A NCAC 2H.0105(e)). The permit would
continue to allow Performance Fibers to discharge water from two outfalls into receiving waters designated
as the Haw River and Shaddox Creek in the Cape Fear River Basin. Enclosed are three (3) signed copies of
the EPA Application for Permit to Discharge Wastewater for Existing Manufacturing, Commercial,
Mining, and Silviculural Operations (FORM 2C) and EPA FORM 1 (General Information).
Performance Fibers New Hill, North Carolina facility has not made any operational or process changes that
impact the wastewater treatment plant since the last NPDES permit application. Since there has not been a
significant change in hydraulic or organic loading on the wastewater treatment plant, Performance Fibers
requests that the NPDES effluent limitations and monitoring requirements remain the same as those in the
existing permit.
At this time there are only two changes anticipated at the wastewater treatment facility in the next five (5)
years. One is to add a second sludge drying bed and the second is to add a pumping station at the polishing
pond so water can be pumped back to the aeration basin. The return of polishing pond water would
improve treatment plant performance during low influent flow situations. Performance Fibers understands
that any planned change could result in the need to submit for a minor or major permit modification and
Performance Fibers would consult with the NPDES Unit prior to such a change.
In order to expand on the enclosed narrative description of our outfalls (Item II-B.) and our wastewater
treatment process, Performance Fibers manages sludge generated from our "wasting sludge" process as
follows: Sludge that is wasted from the biological system is pumped to a sand drying bed where the water
drains through the sand into a collection system that leads to a sump. The sump is equipped with an
automatic level control switch and the water is returned directly to the aeration basin. Once the sludge is
dried, it is shoveled off the bed into a metal dumpster and transported to the following landfill:
Brunswick Waste Management Facility, LLC
107 Mallard Crossing Road
Lawrenceville, Virginia 23868
[phone]
338 PEA RIDGE ROAD I NEW HILL, NC 27362 1 TEL [phone]
w u•u, p e rfo rin a n e e fi b e r s. t om

Performance re *Fibers
Pursuant to telephone conversations with Ms. Toya Fields, NPDES Permit Unit, the information contained
in Form 2C, Item V is not complete, as Performance Fibers is awaiting receipt of analytical results for a
certain number of these pollutants. Pollutants for which analyses are pending are noted on the Form for
each Outfall. Performance Fibers expects to received analytical results within the next 30 days and as
discussed, when results are received from the certified laboratory, these results will be submitted to the
NPDES Permit Unit. In addition as discussed in our telephone conversations, Form 3 is not included in this
submission package, as it is not required as part of this application. Similarly, we also understand that
Form 5 is not required, as this is a renewal application, and Form 5 is a requisite item for proposed
facilities.
Performance Fibers continues its membership in the Upper Cape Fear River Basin Association and
renewed signature of membership in March of 2005. Performance Fibers understands that pursuant to the
memorandum of agreement between NC DENR and the Upper Cape Fear River Basin Association, that any
instream monitoring requirements specified in the new permit will be waived as long as Performance Fibers
remains a member of UCFRBA. This agreement should be described in the effluent limitations and
monitoring requirements section of the new permit.
Performance Fibers is most appreciative of the telephone assistance of the NPDES Permit Unit in
preparation of this submission package. If we can provide any further information or should you have any
questions regarding this submission, please contact me at [phone].
Sincerely,
(3U0 :;-: P0 "to
Charles E. Powell, Jr., REM
Environmental Engineer
Enclosures: -EPA FORM 1- General Information
-EPA FORM 1-Item XI- Topographic Map
-EPA FORM 2C-Application for Permit to Discharge Wastewater, Existing
Manufacturing, Commercial, Mining and Silvicultural Operations
-Water Flow Line Drawing
-Wastewater Treatment Process Description-Outfall 001 and Outfal1002
-List of Item V-C pollutants
With Enclosures
cc: B. Ferree
G. Gardner
D. Peterson -W/O Enclosures
D. Stidham- W/O Enclosures
338 PEA RIDGE ROAD I NEW HILL, NC 27562 1 TEL [phone]
uwu.perJormnu a/ibers.eom

Please print or type in the unshaded areas oni
(rill -in areas are spaced for elite type, i. e., 12 c tersfnch
For Approved. OD 3. 2040-0086. Approval expires 5-31-92
FORM
U.S. ENVIRONMENTAL PROTECTION AGENCY
I. EPA I.D. NUMBER
EPAe GENERAL INFORMATION
NCD053488409 TfA U
F
Consolidated Permits Program
GENERAL
(Read the "General Instructions"before starting.)
1
2 13 14 15
LABEL ITEMS
GENERAL INSTRUCTIONS
If a preprinted label has been provided,
I. EPA I.D. NUMBER
affix It in the designated space. Review the
information carefully; If any of it is
III. FACILITY NAME
incorrect cross through it and enter the
correct data in the aropriate fill-in area
pp
below. Also, if any of a data is
preprinted
absent (the area to the Is of the label
V. FACILITY PLEASE PLACE LAE1ELAI THIS SPACE
a ace list the information that should
it in
PPear) please provide it in the proper fill-
in below. If label is
MAILING LIST
arearsi the complete
and correct need Items
you not complete
1, III, V, and VI(excep[ VI-B which must be
Complete
VI. FACILITY
if�noplabel hasbeenroved tootthhe
LOCATION
instructions for detailed item descriptions
and for the legal authorization under which
this data is collected.
II. POLLUTANT CHARACTERISTICS
INSTRUCTIONS: Complete A through J to determine whether you need to submit any permit application fortes
to the EPA. If you answer "yes" to any
questions, you must submit this form and the supplemental from listed in the parenthesis following the question.
Mark "X" in the box in the third column if
the supplemental form is attached. If you answer "no" to each question, you need not submit any of these forms.
You may answer "no" if your activity is
excluded from permitrequirements; see Section C of the instructions. See also, Section D of the instructions
for definitions of bold-faced terms.
MARK "X"
MARK "X"
SPECIFIC QUESTIONS
SPECIFIC QUESTIONS
FORM
FORM
YES
NO
ATTACHED
YES
�
ATTACHED
s this facility a publicly owned treatment works
B. Does or will this facility (either existing or
which results In a discharge to waters of the
❑
M
Elproposed)
induce a concentrated animal
❑
®
❑
U.S.? (FORM 2A)
feeding operation or aquatic animal
-
production facility which results in a discharge
to waters of the U.S.? (FORM 28)
16
17
18
19
20
21
C. Is this facility which currently results in
®
❑
®
D. Is this proposal facility (other than Nose described
❑
®
❑
discharges to waters of the U.S. other than
in A or B above) which will result in a discharge
those described ILA or B above? FORM 2C
to waters of the U.S.7 FORM 2D
22
23
24
25
26
27
E. Does or will th,a facility treat, store, or ispose of
F. Do you or will you inlect 'Iis facility mdustnal or
hazardous wastes? (FORM 3)
®
❑
❑
municipal effluent below the lowermost stratum
❑
®
❑
containing, within one quarter mile of the well
bore, underground sources of drinking water?
(FORM 4)
26
29
1 30
31
32
33
G. Do you or will you inject at this facility any
H. Do you or will you inject at this acidity fluids for
produced water other fluids which are brought to
the surface In connection with conventional oil or
❑
®
❑
special processes such as mining of suffer by the
Fresch process, solution mining of minerals, in
❑
®
❑
natural gas production, inject fluids used for
situ combustion of fossil fuel, or recovery of
enhanced recovery of al or natural gas, or inject
geothermal energy? (FORM 4)
fluids for storage of liquid hydrocarbons?
FORM 4
34
35
36
37
38
39
1. s this facility a proposed stationary source s this facility a proposed stationary source
which is one of the 28 industrial categories listed which is NOT one of the 28 industrial categories
in instructions M El El El®
El
the and which will potentially emit listed in the instructions and which will potentially
100 tons per year of any air pollutant regulated emit 250 tons per year of any air pollutant
under the Clean Air Act and may affect or be regulated under the Clean Air Act and may affect
44 45
located in an attainment areal FORM 5 40 41 42 or be located in an attainment are? FORM 5 43
III. NAME OF FACILITY
o SKIP Performance Fibers, Inc.
1
15 1 16-29 30 69
IV. FACILITY CONTACT
A NAME & TITLE last, first, & title B. PHONE area code & no.
D Powell, Charles, Environmental Engineer 919 545 3154
2
15 1 16 45 1 46 48 49 51 52 55
V. FACILITY MAILING ADDRESS
A. STREET OR P.O. BOX
s 338 Pea Ridge Road
15 1 16 45
B. CITY OR TOWN C. STATE D. ZIP CODE
wl NC 27562
E4
16 1 16 40 41 42 47 51
VI. FACILITY LOCATION
A. STREET, ROUTE NO. OR OTHER SPECIFIC IDENTIFIER
6 338 Pea Ridge Road
15 1 16 45
B. COUNTY NAME
Chatham
48 70
C. CITY OR TOWN
D. STATE
E.
F. COUNTY CODE
New Hill
NC
27019
r5l
8
15
16 40
41 42
47
1 52 54
EPA FORM 3510-1 (8-90)
101ZI I Ialof 1DhI RWA31 R )of

CONTINUED FROM THE FRONT
VII. SIC CODES 4-digit, in order of .....
A FIRST B. SECOND
C
2824
(sPec�Y)
7 2821
(specify)
e
Manmade Organic Fibers, except
s
Plastics, Materials, Synthetic Resins, and
6 79
,e 7
celluosfc
Nonvulcanizable Elastomers
C. THIRD D. FOURTH
i (specify) (specify)
A
15
15 16 18 19
Vlll. OPERATOR INFORMATION
A. NAME B. Is the name listed in Item
o Performance Fibers, Inc. VIII-A also the owner?
JB
® YES ❑ NO
18 1 19 55
C. STATUS OF OPERATOR Enter the appropriate letter into the answer box; if "Omer. * specify.)
D. PHONE area code & no.
F = FEDERAL M = PUBLIC (other than federal or state)
P
(specify)
c
919
542
2200
A
S = STATE O = OTHER (specify)
58
18 18
79 21
22 25
P=PRIVATE
75
E. STREET OR PO BOX
338 Pea Ridge Road
26 55
F. CITY OR TOWN
G. STATE H. ZIP CODE IX. INDIAN LAND
kBc
New Hill
NC 27562 Is the facility located on Indian lands?
42 42 47 51 YE ® NO
It
75 18 40
X. EXISTING ENVIRONMENTAL PERMITS
A NPDES (Discharges to Surface Water
0. PSD Air Emissions from Proposed Sources
s P ° 02657T27
75 18 1 77 1 18 38
NC0001899
9
N
15
18
17 18 30
B. UIC (Underground Injection of Fluids
E. OTHER s
(Specify)
WTP Alum Residuals
Land Application
c
T
I
°
1
°
WQ0023197
s
u
s
+s
76
77
76 30
a
75
n
79 30
1
Program Permit
C. RCRA Hazardous Wastes E. OTHER (specify) (Specify)
c R ' NCO053488409-R1 9 T ° NC5000100 NPDES Stormwater
15 16 17 18 30 15 18 17 18 30 Permit
X1. MAP
Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must
show the outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of its
hazardous waste treatment, storage, or disposal facilities, and each well where it injects fluids underground. Include all springs,
rivers and other surface water bodies in the map area. See instructions for precise requirements.
XII. NATURE OF BUSINESS rDvide a brief description)
A chemical plant engaged in the manufacture of industrial synthetic polyester fiber and organic polyester resin.
XIII. CERTIFICATION see instructions
1 certify under penalty of law that I have personally examined and am familiar with the information submitted in this application and
all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information contained in
the application, I believe that the information is true, accurate and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fine and im riso ent.
A. NAME & OFFICIAL TITLE (type orprint) B. SIGNATURE
C. DATE SIGNED
Don Peterson, Plant Manager J
t ( l C
COMMENTS FOR OFFICIAL USE ONLY
c
C
15
16 55
EPA FORM 3510-1 (8-90)

EPA FORM 1
Item XI.
Topographic Map
Performance Fibers, Inc.

SITE
_ y
- ',^n:.; �+• 1. !j AS �P/� .
Outfa11001
-/[:e+'I ;. nL-,Pcsu' '�! 1)Llililll O02
Ab
`mac-
I /
QtWitter
IV
IA
,
0
0 VA
0.3 0.6 0.9 1.2 1.5 km - -
0 0.7 0.4 0.6 0.8 1 ni
Map center is 350 37' 12"N, 79' 02' 41"W (WG584/NAD83)
Moncure quadrangle M 8.527
Projection is UTM Zone 17 NAD83 Datum G=1.139
Performance Fibers, Inc
Moneure, Chalhum Count`•, NC
EPA Form 1, Item XI

Form
A 1.0. NUM BER(COPY from Item O 'Orm IJ OMB It to
MaaM prim or type in the unshaded areas only. NCD053488409 Approval expires 8-31-98.
FORM U.S. EN V IRORMENTAL PROTECTION AGENCY
2C ��EPA APPLICATION NFORPERMITTODISCHARGE WASTEWATER
EXISTING MANUFACTURING, COMMERCIAL, MINING AND SILVICULTURAL OPERATIONS
NPDES Consolidated Permits Program
1. OUTFALL LOCATION
For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving waterA..
NVMtARLL
D. LATITUDE
C. LONGITUDE
D. RECEIVING WATER (.Mm )
YIM.
!. a.C.
001
35
37
01
79
03
25
Haw River
002
35
37
00
79
02
36
Shaddox Creek
II. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES
and treatment units labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showin
flows between intake, operatloro, treatment units, and outfalls. If a Water balance cannot be determined (ay., /or certain mining activides),
pictorial description of the nature and amount of any source of Water and any collection or treatment measures.
A. Attach a line drawing showing the rater flow through the facility. Indicate Sources of Intake Water, operations contributing wastewater to the7FROM
B. For each outfall, provide a description of: 11 All operations contributing wastewater to the effluent, including prucissa wastewater, sanitary w
cooling water, and stoml water runoff; (2) The average flow contributed by each operation; and 13) The treatment received by the wastewater.
on additional sheets if necessary.
1. OUT-
E. OPKRATION(S) CONTRIBUTING FLOW
S. TREATMENT
FALLN
(list)
a. OPERATION (list)
. AVERAGE FLOW
Onclud• units)
a. DESCRIPTION
. LIST CO
TABLE SC.t
001
See additional information for complete 001 c
ascription
Firepond Overflow
33,000 GPD
Discharge to Surface Water
4-A
002
Stormwater Runoff
78,500 GPD
Oil Baffles and Weirs, Discharge to Surface Water
1.H
4-A
Steam and HVAC Condensate
1,000 GPD
Discharge to Surface Water
4-A
Air Dryer
500 GPD
Discharge to Surface Water
4-A
FICIAL USE ONLY eatfluent ry sL )
EPA Form 3510-2C (R-Mi PAGE 1 OF 4 LUNunut LIN Nave Nac

CONTINUED FROM THE fR
C. Except for storm runoff, leeks, or wills, are anyWe discharges described in Items 11-A or B intermitten sessonal?
❑YES (complete the following table) ® NO (ao to Section Ill)
3. FREQUENCY
4. FLOW
I.OUTFALL
2. OPERATION(])
a. DAYS
b. MONTHS
a. FLOW RATE
4 TOTAL VOLUME
NUMBER
CONTRIBUTING FLOW
ISR WEEK
PER YEAR
(in rned)
(specify with units)
t DUR-
1. LDxe TawM
e. MwaIYVM
OMO Ta nY
r. Mw..MVM
isI
ilt
(specfy
(specify
ATION
we rase)
werag.)
•v wwoa
D• v
wvawwoa
u v
(in day.)
III. PRODUCTION
A. Does an effluent
guideline limitation promulgated by EPA under
Section 304
of the Clean
Water Act apply
to your facility?
® Yes
(Complete Item III-B) Refer to Supplementary
Information
❑ NO (to to
Section IV)
B. Am the limitations in the applicable effluent guideline expressed in terms of production (or other meauJm of Operation)?
DYES (complete Item III-C) ®NO (so to Section IV)
C. If you answered "yes" to item 111-B, list the quantity which represents an actual measurement of your level of production, expressed in the terms
and units
used in the applicable effluent guideline, and indicate the affected outfalls.
1VERAGE DAILY PRODUCTION
2. AFF6CTBD
a, aV NNTItY wets Dw•
n. UNITe OF M......
C. owaRwTlox, wwooecq MwTa wlw� aTc.
(specify)
OUTFALLS
(tilt out/al! numbers)
NIA
IV. IMPROVEMENTS
A. Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operation of waste-
water treatment equipment or practices or any other environmental programs which may effect the discharges described in this application? This includes,
but is not limited to, permit conditions, administrative or enforcement orders, enforcement compliance schedule letters, stipulations, court orders, and grant
or loan conditions. YES (Complete Me following table) ❑ ®ND (so to Item IVB)
1. IDENTIFICATION OF CONDITION,
E. AFFECTED OVTFALLE
4. IF'A
M
AGREEMENT, ETC.
]. BRIEF DESCRIPTION OF PROJECT
T.
y
a. xo.
4 woad ow pwxwwe•
ulwio
,idTio
B. OPTIONAL: You may attach additional sheets desatbing any additional water pollution control programs (or other environmental projects which may affect
Your diseharya) ,you now Aaw underway of which. VW plan. Indicate whether each program is now underway or planned, and indicate your actual or
Planned schedules for
fx)rlatluCtlOn, ❑MARK "Xw IY-DEaCRI"ION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
EB♦ e
.. TYrm 3510-2C (Rev. 2-BO) PAGE 2 OF 4 CONTINUE ON PAGE 3

CONTINUED FROM PAGE 2 1
EPA I.D fMBER(copy from Item l or LOrm 11 I •
WINTAKE AND EFFLUENT CHARACTERISTICS
A, B, & C: See instructions before proceeding — Complete one set of tables for each outfell — Annotate the outfatl number in the space provided.
NOTE: Tables V-A, V-8, and V-C are included on separate sheets numbered V-1 through V-9.
D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions, which you know or have reason to believe is discharged or may be
discharged from any outfell. For every pollutant you list, briefly describe the reasons you believe it to be present and report any analytical data in your
possession.
I. POLLUTANT
3. SOURCE
1.POLLUTANT
g. SOURCE
Acetaldehyde Cresol
Possible process by-product
Used in QC lab
Crotonaldehyde
Possible process by-product
Cyclohexane
Used in QC Lab
Xylene
Used in QC Lab
VI. POTENTIAL DISCHARGES
NOT COVERED BY ANALYSIS
a substance or acomponent of a substancewhich youcurrently use or manufacture
as an intermediate or final product or
Is anypollutant listed in Item V-C
byproduct)
®YES (list all such Pollutants below) ❑No (go
to (fern VLB)
Antimony
Phthalate Esters (Possible process by-product)
(Refer to Supplementary Information)
EPA Form 3510-2C (8-90) PAGE 3 OF 4 CONTINUE ON REVERSI

CONTINUED FROM THE FRONT AM
f' -I
VII, BIOLOGICAL TOXICITY TESTING DATA ss
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made owanyof your discharges or on a
receiving water in relation to your discharge within the last 3 years?
® YES (Identify the test(,) and describe their purposes below) ❑ No (go to Section VIIf)
Chronic Toxicity at Discharge 001 and
Acute Toxicity at Discharge 002
per monitoring requirements of NPDES permit.
IIILONTRACT ANALYSIS INFORMATION
Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
® YES (list the name, address, and telephone number of and pollutants ❑ NO (go to Section IX)
analysed by, each such laboratory or firm below)
A. NAME
S. ADDRESS
C. NE
area code a no.
0. POLLUTANTS ANALYZED
diet
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
[phone]
Huntersville, NC 28078
ext. 236
Tritest, Inc.
6701 Conference Drive
Roger Thomas
Raleigh, NC 27607
(919) 8344984
NC WIN Cert #067
NCIDW Cert #37731
IX. CERTIFICATION
l certify under penahy of law that this document end ell attachments were prepared under my direction or supervision in accordance with a system designed to
assure that qualified personnel properlygether and evaluate the information submitted. Based on my inquiry of the parson orpersons who menage the system or
those persons directlyresponsible forgathering the information, the information submitted is, to thebest of myknowledge andbelief, true, accurate, andcomplete.
If am aware that there are significant pene#ies for submitting false information, including the possibility of fine and imprisonment for knowing violations.
A. NAME S OFFICIAL TITLE (type Or print)
B. PHONE NO. (area CUde Q n0,)
C. SIGNATURE
D. DATE SIGNED
PAGE 4 OF 4
EPA Form 3510-2C (8-90)

EPA I.D. NUMBER (COPY from Item I of Form 1)
PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of
this information on separate sheets (use the same format) instead of completing these pages.
NCD053488409
SEE INSTRUCTIONS. v
OUTFALL NO
V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form?-Cl 0 )i
PART A - You must provide the results of at least one analysis for every pollutant in )this table. Complete one table for each outfall. See instructions for additional details.
2. EFFLUENT '.
3. UNITS
4. INTAKE (Optional)
I. POLLUTANT
(epeclfY if blank)
a. MAXIMUM DAILY VALVE
•MAXI as a
wal?ag%
Y VALUE
e.
I sea
LU
a e L-OFYSES
[. LONG
TERM
a CONCEN-
TRATION
Iz MASS
SES
ANALI.YSES
III
Isl wwaa
Iml
..... nrn wner,
la) wwaa
cone [:��wwnen
III wwas
MA
one [eiw.rion
OI ..wsa
a. Blochemical
Oxygen Demand
8.34
5.6
3.3
2.2
2,4
1.6
52
mg/L
Ibslday
(BOD)
b. Chemical
Oxygen Demand
(COD)
a Total Organic
Carbon (TOC)
d. Total Suspended
sodas (Tss)
7.5
5.8
6.8
4.5
.12
3.0
52
mg/L
Ibslday
e. Ammonia (w N)
VALUE
VALUE
VALUE
VALUE
t. Flow
0161
0.105
0.080
365
MGD
9. Temperature
VALUE
VALUE
VALUE
VALUE
(winter)
20.5
17.2
13.1
365
oC
h Temperature
VALUE
VALUE
VALUE
VALUE
(summer)
30.3
26.3
24.2
365
°C
MINIMUM
MAXIMUM
MINIMUM
MAXIMUM
1. PH
6.8
8.3
6.6
8.3
365
STANDARD UNITS
PART 8 - Mark "X" in column 2-a for each pollutant you know or he" reason to befieve is present. Mark "X" in column 2-b for each pollutant you believe to be absent. If you mark column 2a for any pollutant
which is limited eitherdireetly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark
column 2a, you must provide quantitative data "an explanation of their presence in your discharge. Complete one table for each outfall. Seethe instructions for additional details and requirements.
I. POLLUT-
Z. MARK •X•
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
ANT AND
a, ec-cb.
ea
e. MAXIMUM DAILY VALUE
b. MAXI M a
Wa0601t
Y VALUC
c.LONG TF M # b f� VALUE
j(�oaal(ap aJ
dNO. O
a. L NG T
AV ERAGE VALUE
NO
CAS NO.
(U auoBobla)
eva
iw a-
uwr
wv[
e.
)stir
ANAL-
USES
a. CONCE N-
TR ATION
b. MAss
ANAL
YSES
Ii) wwfa
la) wwff
(i) w
Ial wua
...... rwwnen
one aw�rnwnow
eonc[nfnwrlon
a. Bromide
$
(24959-67-9)
X
Is. Chlorine,
Total Residual
X
< 1.0
< 1.0
< 1.0
< 1.0
< 1.0
< 1.0
365
mg/L
Ibs/day
a Color
X
d. Fecal
Collform -
X
1200
1200
370
12
#I100 ml
a. Fluoride
(16984.48.8)
X
f.
Nltrib (asko (W NI
X
EPA Form 8510.20 8.90 * PAGE V-1 CONTINUE ON REVERSE
� ) Awaiting Receipt of Analytical Results

ITEM -B CONTINUED
FROM
FRONT
�.AGLLUT-.
2. MARK •X•
S. EFFLUENT
4. UNITS
5. INTAKE (optional)
NT AND
•,CAB NO.
a� n
b. ae-
�i
a. MAXIMUM DAILY VALUE
,MAXI M
Walb64
Sp pA Y VA UC
o.
aVO1bD
Ay VALUE
tl. NO.OF
a TERM
AJER AGE VALUE
(//ewLoD4)
...c
unt
�a
ianr
_
a.CONC 6H-
TRATION
b. MASS
NO.Of
ANAL-
1') "�tt
,
convnrw.non
cone enrnAnon
la) N
conunrw.nen
Iz) rwst
YSES
conceerwnrmn
Ixl NA..
YSES
B NlDogan,
Total Organic
x
(4i N)
A. Oil and
Grevee
X
13.4
9.4
7.1
5.5
6
4
52
mg/L
Ibs/day
1. Phosphorus
(as P), Total
(7723-14-0)
X
2.1
1.6
1.6
1.3
1.3
.9
25
mg/L
Ibs/day
I. Radioactivity
(1) Alpha,
TOUT
X
(2) Beta,
Total„
X
LF
13) Radium,
Total
X
14) Redlum
226, Total
X
k. Sulfate
(- Sod)
X
$
(14BgB-79A)
1. WIWI,
oa S)
X
m.5u he
(as S03)
(14265-45-3)
X
n. Surtactantt
X
.A.
o. Aluminum,
Total
(]429-90.5)
X
P. Barium,
Total
39-3)
y
(7440
Q. Boron,
Total
X
(740—b-4t 8)
r,
Total
X
17440-48-41
a. Iron, Total
(7439-89-6)
X
t. Magneium,
Total
439-95
. Molybdenum,
Total
X
(7439-96 7)
Y. arlgalleae.
Total
(7439-96.6)
X
w. Tin, Total
U44031-5)
X
x. Titanium,
Total
X
(7440.32-6) 1
EPA Form 3510.2C (8.90) * Awaiting Receipt of Analytical Results 1. Y-4 CONTINUE ON PAGE V -3

EPA I.O. N(COPY from Item I Of FOM I)
OUTFALL NUMBER
NCDO53488409
001UMBER
CONTINUED FROM PAGE 3 OF FORM 2-C
PARTC- If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you musttest for. Mark "X" in column
2-a for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary Industries, nonprocess
wastewater ouvalls, and nonrequired GC/MS fractions), mark "X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you
believe is absent. If you mark column 2a for any pollutant, you must provide the resulis of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results
of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolain, acrylonitrile, 2,4
dinitrophenol, or 2-methyl-4, 6 dinitrophenoi, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in
concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to
be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (all7 pages) for each outfall. See instructions for additional details and requirements.
I. POLLUTANT
Z. MARK •X•
3. EFFLUENT
4. UNITS
S. INTAKE (optional)
NUMBER
t{T
No
4{'
,t t
Gat"
...
a. MAXIMUM DAILY VALUE
b. MAXI M SO
as
SI Y W ALOE
a e
4LONG T M
8ad
AVR yALUE
1 NO.OF
{' CONCEN-
a. LONG
ERA
TERM
E
b, NO.OF
(lfauoliobie)
aY�A•
{iNT
)ENT
ANAL-
YSE$
TRATION
b. MASS
ANAL-
Y$E$4
CONCt M1It......
Ill MA{{
.ONO {N1TRNT,OM
tr) MI,FS
CO MC{NTIR .{TION
(1) MA..
II7RA IONN
Ill MA{{
METALS, CYANIDE, AND TOTAL PHENOLS
1M. Antimony,
Total 17440-36-0)
X
*
1
Ug/1
Ibs/day
2M. Arsenic, Total
(7440-38-2)
X
*
1
ug/1
Ibs/day
3M. Beryllium,
Total, 7440.41-7)
X
*
1
ug/1
Ibs/day
Totall(7 m440-43-9)
X
*
1
ug/1
Ibs/day
SM. Chromium,
Total (7440-47-3)
X
*
1
ug/1
Ibs/day
am. ciaper, (7sta6)T01°
X
*
1
ug/l
Ibs/day
7M. 1.0114 TOW
(743a92-11
X
*
1
ug/1
Ibs/day
SM. Mercury, Total
(7439,97.6)
X
*
1
ugll
Ibs/day
SM. NkscN, Total .
(74apo2-0)
X
*
1
u9/l
Ibs/day
I OM. selenium,
Total (77e2-49-2)
X
*
1
ug/I
Ibs/day
111 M. S11aar, Total'
(744.0.22.4)
X
*
1
Ug/1
Ibs/day
12M. Thalllum,
Total(7440-28-0)
X
*
1
ug/1
Ibs/day
13M.'Zinc, Total
17440-66-61
X
*
1
Ug/1
Ibs/day
14W Cvanlda,
Total (57-12-5)
X
*
1
Ug/1
Ibs/day
Tool PMnols,
X
*
1
Ug/1
Ibs/day
DIOXIN
*4
EPA Form 3610.2C (5-90) PAGE V-3
* Awaiting Receipt of Analytical Results

1. POLLUTANT 1 2,:MARX •Xv 3. EFFLUENT
AND CAE
4. UNITE
6. INTAKE (optional)
NUMBER r;o• n BE 'v 9- e. MAXIMUM DAILY VALUE MAXI M DAY VALVE ALONG T M e�(p .VALUE
�iwe• OVa LY y�yyp,e d NO.OF
e. LONG TERM
hA
wa-
(1)avdhtble) ev�w- eewr ie�-r cowcaniwwr.ow (altos 1�) (ri two 11 ANAL-
.eoecaxrwwnox wnox la1 two USES
eTRATION bLMAE/
Ao. Lf
h�w�t1ONw' lai twee YiEi
OC/MB FRACTION - VOLATILE COMPOUNDS
IV. Aerohin
(107 o2a)
X
*
1
ug/I
lb/day
2V. Acrylonitrlle
(107-13.1)
X
< 10.0
0
1
ug/I
lb/day
3V. Benzene
171."2)
X
< 1.0
0
`•
1
ug/1
lb/day
4V. Bb (Chloro-
methyl) Ether
X
(542-88-1)
1
ug/l
lb/day
V. (6 6-26 2) oform
X
1
ug/l
lb/day
6V. Cerbon
ti23-5)ritle
X
< 1.0
0
1
ug/I
lb/day
7V. Chlorobenzene
(108.90-7)
X
< 1.0
0
1
ug/l
lb/day
6V. Chlorodl-
bromormthene
y
it
/�
1
ug/l
lb/day
9V. Chlormthem
(75-00-3)
X
< 2.0
0
1
ug/l
lb/day
I OV. 2-Chtoro.
ethyNlnyl Ether
X
(110.7")
1
ug/1
lb/clay
11 V. Chloroform
(87-66-3)
X
< 5.0
0
1
ug/l
lb/day
12V. Dichloro.
bromomethem
x
yr
(75-27-4)
1
ug/I
lb/day
13V. Oichloro
dtfluoromathom
X
(75-71-8)
1
ug/1
lb/day
14V. 1,1.Dichlcro.
athem (75-34-3)
X
< 1.0
0
1
ugfl
lb/day
16V. 1,2-Dkhloro-
.them (107-W2)
X
< 1.0
0
1
ug/I
lb/day
16V. 1,1-01chlom-
athylem (76.35-4)
X
< 1.0
0
1
ug/I
lb/day
17V. 1,2-Dlchloro.
orOmne (76-87-5)
X
< 1.0
0
1
ugh
lb/day
19V. IA4)W llere-
WgWWR(612-76E)
X
< 1.0
0
ug/1
1
lb/day
19V. Ethylbenzem
-
(100-41-4)
X
< 1.0
0
1
ug/I
lb/'day
20V. Methyl
-
Bromide (7483-9)
X
1
u9/1
lb/day
21V. Methyl
Chloride (74-87.3) X
< 2.0
0
1
ug/I
lb/day
.24w_ ra_anf
ern rvnw ��.� ♦�-r PAGE V-4
* Awaiting Receipt of Analytical Results
CONTINUE ON PAGE Of

. l Nev.. rnUNl rAur V V
1. POLLUTANT
AND CAS
2. MARK
3. EFFLUENT
4. UNITS
5. INTAKE /optional)
NUMBER _
����
vi
vi-
L MAXIMUM DAILY VALUE
,MAXI M
aVa
Y VALUE
c.LONG T M
aUa110D1f
y1(pp
�1 VALUE
d NO.OF
+. CONC[N-
.. LONG
TERM
b. NO.OF
(1/Wallable)
+u`w-
�ii,`.i
-
•: hr
ANAL-
YSES
TR ATtOM
tt MA1i
ANAL-
uses
w��i, (•) rwa
hr
(al rAlw
��Iw
(r) wnu
(,) <owc+w-
l.l �+••
OCM8 FRACTION — VOLATILE COMPOUNDS (tontlnuad)
cngr e176Ae-2)
X
< 1.0
0
1
ug/I
Ibslday
23V 11,1,2,2-T.—
chkwo.al.n4
X
*
1
ugll
Ibs/day
(7034-5)
24V. T.tr.ehloro-
.myl« (127-18-4
X
< 1.0
0
1
ug/l
Ibs/day
25V. TOlu4n.
(108483)
X
< 1.0
p
1
ug/I
Ibs/day
26V. 1,2-Trans-
DldNorotthyl4n.
X
< 1.0
0
1
ug/I
Ibslday
(16660-5)
27V. 1,1,1-Trl-
0
chlb hs.
X
< 1.0
1
ug/l
Ibs/day
28V. 1,1,2-Trl-
cbloro hans
X
< 1.0
0
1
ugll
Ibs/day
(79-M5)
29V. Trichloro-
.thyl.M (79-01-6)
X
< 1.0
0
1
ug/I
Ibslday
30V. Trichioro-
tluoromothans
X
1
ug/I
Ibs/day
(75-693)
cn o'rW: �75.01-4)
X
< 2.0
0
1
ug/I
Ibs/day
OCMB FRACTION — ACID COMPOUNDS
tA, 2Chloropheno
(95.57-8)
X
< 10
0
1
ug/I
Ibs/day
2A. 2,4.Dlchloro-
ptteltoi (120-83-2)
X
< 10
0
1
ugll
Ibs/day
3A, 2,4-Di"thyl-
pharool (1�7-9)
X
< 10
0
1
ugll
Ibs/day
4A: 4,8-Dinitro-0-
Cr4.ol (634-52-1)
X
< 50
0
1
ug/I
Ibs/day
GA. Dinitr . 1161-28-5
X
< 50
0
1
ug/I
Ibslday
8 tropn.nol
(8 75-5
X
< 10
0
1
ug/I
Ibs/day
7A. 4-Nltroph•nol
(100-02-7)
X
< 10
0
1
Ug/I
Ibs/day
Crr..ol(5960-7)
X
*
1
ug/I
Ibs/day
9A[ P4nwhlwr
plwtol f87-8616)
X
*
1
ug/l
Ibs/day
lQA phttnol
(ta�a6-z)
X
<10
0
1
ug/l
Ibs/day
Trl-
r1
X
*
1
ug/I
Ibs/day
EPA Form 3510.2C (8-90) * A..,nr PAGE V-5 CONTINUE ON REVERSE

1. POLLUTANT 2. MARx 'x' 3. EFFLUENT
AND CAS
4. UNITS
S. INTAKE /nptiorlalJ
NUMBER •' �+ b ', i- a ae- •. MA%IMUM DAILY VALU¢ b. MAXI M �p p/�Y VALUE c.LONG TIE e�[ �i VALU!
♦rave OUpllebl¢ (/ '+ 6�J d NO.OF
1 pee O C
S. LONG TERM b. NO.OF
(IJ •eellaDle iia- •nw- AN
1 onlw- un+ asw+ cows aeiwwnoe 121 rwaa 1.1 1+1� 1�1
ncaxrxwnox oxc[x+xwnow Id rwaa YSlL
a. CONCEN. b. MASS
TRATION
ANAL-
hiw ai l+l Nwaa NAL
GCMG FRACTION — BASEMEUTRAL COMPOUNDS
owx
(83-32 9))ephthane
X
<10
0
1
ug/1
Ibs/day
28. Acenephtylene
(208-86-8)
X
< 10
0
1
ug/1
Ibs/day
3B. Anthrwene
1120-12-7)
X
<10
0
1
ug/I
Ibs/day
1
Ug/I
Ibs/day
58. Benzo (•)
Anthrwena
6636-3)
< 10
0
-
1
Ug/l
Ibs/day
68. Benzo (.)
6B. Be (60.328)
X
< 10
0
1
ug/1
Ibs/day
78. 3,4-Banzo-
fluorinthene
< 10
- 0
(20549-2)
1
ug/I
Ibs/day
8B. Benzo (!hi)
X
*
(101-2�4--2)
1
ug/I
Ibs/day
911-8•tlz0 (h)
Fluoranthana
--
12o7.OB-B1
< 10
0
1
ug/l
Ibs/day
10B. Bh (2-Chloro
Mathana
X
eMezy)
(111.81-n
1
Ug/I
Ibs/day
11 B. Biz (2-Chlom
lthY,111liitaj
%�
*
1
ug/I
Ibs/day
12B. So 2-chbvi o-
X
*
NW4EOW(102-Bat)
1
ug/l
Ibs/day
138. Bie (2-8thy1-
lu=y2) Phthalate
(117-81-7)
< 10
0
1
ug/l
lbs/day
-141L 4-Bromo-
erl
;th"' 01.6a-3)
X
*
1
ug/I
Ibs/day
PWh*Butyl aerayl
'Phttwlev
X
*
-68-7
(86-08-7
1
ug/I
Ibs/day
i188r2Chlom-
o
X
*
1
ug/I
Ibs/day
w17jBc.pthl6ro-
72-3)
X
*
1
Ug/l
Ibs/day
188. Cihrysiwa
M1841-9)
X
<10
0
1
ug/l
Ibs/day
188:.DWanzo a, )
(53-70-3)
X
<10
0
1
ug/I
Ibs/day
206. 1,2.Oichiorc-
b.nz• (9"0-1)
X
<10
0
1
Ug/I
Ibs/day
baru•rI•(fiat-78-t
be8ori3-Dleh73-
X
<10
0
1
Ug/l
Ibs/day
EPA Form 3510-2C (8-80) PAGE V-6 CONTINUE ON PAGE V-7
* Awaiting Receipt of Analytical Results

GVN 1INUEU I-HOM PAGE V-6
1. POLLUTANT z. MARK W 3. EFFLUENT
AND CAS
4- UNITS
S. INTAKE (optional)
b. MAXI M 8 Y VALUE ALONG T M .VALUE NUMBER ere tr bet" •t' a. MAXIMUM DAILY VALUE /� aVa/�ay ge
rn" cvx r..eNt OVaI b (I p( d NO.OF
D. LONG TERM b. ".AIIOF
(1/eValleblef OV�w- iin� ♦ Ir) ANAL-
tonc enrwwnow III uwq once wriwwnow Iil uwfr <anctrvrl"when (xl'"^tt YSES
e. CONCEM
tx MASS
TRATION
(r) toner n- Ix) uwf• YSES
OC/MS FRACTION _ BASEMEUTRAL COMPOUNDS (continue&
rwwnon
Benzne
(I 46-lor
benzene (1DB-46-7
X
< 1.0
0
1
ug/I
Ibs/day
-2.18: 3.7-Dkhlor
°vlow,1W
X
*
1
Ugh
Ibs/day
241L 014thyl
POthiLl.2a)
X
< 10
0
1
Ug/l
Ibs/day
2eZ Dln ethyl
-
', el:
X
<10
0
1
ug/I
Ibs/day
Butyl
zj':.
X
< 10
0
1
ug/1
Ibs/day
$Ze.o
toluane no(1(12121hY
.14-2)
X
< 10
Q
1
ug/I
Ibs/day
288
tw1usn °006-20-2)
x
< 10
0
1
ug/I
Ibs/day
298: pw-ocwl
(1-1h 77444.0)
X
*
1
Ug/I
Ibs/day
308. 1.2-Owhenyl-
be eIMi22.687
X
1
ug/I
Ibs/day
(206-44)i-0) uoranth.ne
X
< 10
0
1
ug/I
lbs/day
328. Fluorene
tega3-7)
X
< 10
0
1
ug/l
Ibs/day
11i�74 p,
X
< 10
0
1
Ug/l
Ibs/day
34B. Hexe•
chlowbutadlene
(87-68-3)
X
< 10
0
1
ug/I
Ibs/day
368. Hexachloro-
`77 � melene
X
*
1
ug/l
Ibs/day
368. Hexachlwo-
emane (67.72.1)
X
< 10
0
1
ug/I
Ibs/day
376. Indeno
(193-39-5) rang
X
< 10
0
1
ug/I
Ibs/day
388. Iwphorone
(78-59-1)
X
1t
1
ug/I
Ibs/day
(9 8 Naphthalene
X
< 10
1
ug/I
lbs/day
(98 96--3) bentene
X
< 10
0
1
ug/I
Ibs/day
41 B. N-N Itro.
—
wdimethylamine
%�
*
(62-78-9)
1
Ug/l
Ibs/day
420. N-Nltrowdi-
N-Propylem ine
621�47
%�
'�
1
ug/l
Ibs/day
EPA Form 3510-2C (8-90) * PAGE V-7
Awaiting Receipt of Analytical Results
CONTINUE ON REVERSE

CONTINUFn Funu TUF vc, wT
1. POLLUTANT z. Mwwx •x• 3. EFFLUENT
4,
AND CAS
UNITS
6. INTAKE /oprimin!)
NUMBER Tear to ee- G [e- 9, MAXIMUM DAILY VALUE MAXI M )D p/IY VALUE C.LONO TpjiM /�y@ VALUE
,wn leve •Ieve eu a 1 NO.OF
e. LONG TERM
(q eyalfaVb gp'
(rleu•ibblc/ �`w- [wr awr cows [w�iwwnow (fl wwa ANAL
w1iwwnan Ir) I+I N TSES
• CONCEN- b. MASS
TRATION
b. NO. OF
(,) cowce w- wNAL-
cowu canc[hrlwwn ow
GC/W FRACTION—SASE/NEUTRAL COMPOUNDS (continued)[
III M MSAL
43B. N•Nltro-
X
*
(aodIphenylemine
1
ug/1
Ibs/day
. Ph nenthnne
BJ
X
< 10
0
1
ug/I
Ibs/day
(12i-o%.o)e
X
<10
1
ug/I
Ibs/day
468. 1,2,4 - Trl-
Lo
°a1or0'
X
<2.0
ug/I
)Gn•
1
Ibs/day
OCAESiRACTION
. PFSTICInFit
f.
(309- 2)
X
yt
1
ug/I
Ibs/day
2P. a-SHC
(31994�)
X
1
ug/I
Ibs/day
*
79
X
1
ug/I
Ibs/day
((68$yyYs)C
X
1
ug/I
Ibs/day
OP. S-eHC
*
(31941")
X
1
ug/1
Ibs/day
OP. Chlordene
(67-744)
X
*
1
ug/I
Ibs/da Y
iso-sea)
x
1
ug/I
Ibs/day
BP. 4,4'-DDE
(72-66-9)
X
1
ugh
Ibs/day
9P. 4,4'-ODD
(72-648)
X
*
1
ug/I
Ibs/day
1 OP. Dleldrin
(60-57-1)
X
*
1
ug/I
Ibs/day
11 P. a-EndewHen
1115.29-7)
X
*
1
ug/I
Ibs/day
12P. 0-Endowlfen
*
(115-29-7)
X
1
ug/l
Ibs/day
13P. Endoeulfen
3utlete
(1031-0781
X
1
ug/l
Ibs/day
14P. Endrin
i72-208)
X
*
1
ug/I
Ibs/day
I6P. Endrin
-
dehyder
7142193-4)
X
*
-_
1
ug/I
Ibs/day
17 P. Heptechior
X
*
1
ug/I
Ibs/day
PA Form 3510-2C (8-90) PAGE V-B
* Awaiting Receipt of Analytical Results
Ulil

bNTINVED FROM PAGE V-S
NCD053488409
001
1. POLLUTANT
x. MARK •X•
3. EFFLUENT
4. UNITS
S. INTAKE'p a naval
NUMBER
Ttfr
wt'
a��vf'
0. MAXIMUM
DAILY VALUE
MAXINVM 7fl
DAY VALUE
a.LON6 TEpaM
Ay F VALUE
S NO.OF
a. LONG
TERM
b. NO. OF
(1/available)
ou`w-
ifnr
fever
ANAL-
YSES
CONCE_
�TRAT ON
b. MASS
ANAL
YSES
I')
eo«eenrwwnow
(a) ywfs
(�1
oo«et«r«canon
(a) rwfs
(�1
o«tf«v.now
lel aa•M
1�� ca^clue'
Ia) rwu
GCAIIS FRACTION —PESTICIDES
(continued)
17P. Hapnehlor
kts
(im4 57-3)
X
*
1
ug/I
Ibs/day
42
(53+es z1-9)
X
*
1
ug/l
Ibs/day
19P. PCB-1254
01097-69-1)
X
*
1
Ug/I
Ibs/day
201'. PCB-1221
X
*
ugll
111104-28.2)
1
lbs/day
21P. PCB-1232
X
*
(11141.1a-S)
1
ug/I
Ibs/day
112672 z9-6i a
X
*
-
ug/I
1
Ibs/da Y
l09"2-6) u
X
*
—
1
Ug/I
Ibs/da Y
24P. PCB-1016
:12674.11-2)
X
*
1
Ug/l
Ibs/day
taoaP.ol-3s-2T=haas
:)
x
*
1
u9/I
Ibs/day
PAGE V-9
Form 3510-2C (8-%0)

EPA I.D. NUMBER (cop), from Item I of Form 1)
PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of
this information on separate sheets (use the same format) instead of completing these pages. NCO053488409
SFF INSTRIICTIr1NS
OUTF"ALL NO
V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-0002
PART A - You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
Z. EFFLUENT
3. UNITS
4. INTAKE (optional)
t. POLLUTANT
(epeeify If blank)
a. MAXIMUM DAILY VALUE
. MAXIM M 9.0 p/�1Y VALUE
I aVal4aSIC
c LU
I OVar a P d. NO. OF
a. LONG
TERM
4 NO, OF
a. CONCEN-
TRATION
b. MASS
ANALYSES
1.) NA,.
Dr
pl N.
ANALYSES
lil
lal .w„
a. alochemical
Oxygen Demand
*
Ibs/day
(BDD/
b. Chemical
Oxygen Demand
(COD)
C. Total Organic
Carbon (TOC)
d. Total Suspended
Solid, (TSS)
e. Ammonia (a, N)
VALUE
VALUE
VALUE
VALUE
t, Flow
0.384
0.176
0.093
50
MGD
g. Temperature
VALUE
VALUE
VALUE
VALUE
(winter)
20.2
15.6
12.4
25
0�
h. Tempef1111re
VALUE
VALUE
VALUE
VALUE
(summer)
30.4
28.7
25.5
25
eC
MINIMUM
MAXIMUM
MINIMUM
MAXIMUM
i.PH
64
72
64
7.2
50
STANDARD UNITS
PART 8 - Mark'"X" in column 2-a for each pollutant you know or have reason to believe is present. Mark "X" in column 2-b for each pollutant you believe to be absent. If you mark column 2a for any pollutant
which is limited either directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark
column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall, Seethe instructions for additional details and requirements.
1. POLLUT-
x. MARK •X'
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
ANT AND
a, ae,
b. ex
e. MAXIMUM DAILY VALUE
b. MAXI UM eg
ape
DrV VALUE
a
c.LONG TERM AY G. VALUE
(Il aaatlab e/
dNO. O
a. L NG TERM
AV ERAGE VALUE
b. NO
CAS NO.
aANAL-. CONCEN
TRATION(IJ
bMw55
Anll
O1'
xl
oNc eTa ATioN
CONccnN
available)
YSE5
YSEB
a. Bromide
(24959-67-9)
X
b. Chlorine,
Tout R"Idual
X
c. Color
v
A
d. Fecal
collform
X
a. Fluoride
(169e4-49a)
X
0.14
0.188
1
mg/L
Ibs/day
f. Musts—
N wife file N)
X
PAGE V-1 CONTINUE ON REVERSE
EPA Form 3510.2C (6-110) * Awaiting Receipt of Analytical Results

ITEM V-8 CONTINUED
FRt7M
FRONT
LWT-
_. MARK •%•
!. EFFLUENT
4. UNITS
5. INTAKE (npNmlaq
T AND
'CAB NO.
a. aa- b.eo
eVc u
. MAx1 M f Y Vw Uc a A-
MAItIMYM GAILY VALYc aa�� LUE
BANAL
�,pp�
(1f1aaLabie)
iin`T iwT
LCONCEN- b. MASS
TRATION
V.RL NO.OF
Aell AGE VALUE ANAI-
IT) NA{{
,
COMCi XTw11T10
COXC{NTwwT10M
1t) Nw{�
COXO{X1w wT10X
(+I Mwf{
YEEE
cowc{XTwwT,oX I.1 Nw�• VSEE
0.:NItttl9an,
Tghl Organic
y
!a{ N(
A
.N Qil and
'Or�Ma
X
4
PPT o
-
(aa P), au
X
(7723140)l
1• Redlooctivlty
(I)Alpha,
"
Total
�(
(2) Seta,
Total.
X
y[
(3) Radium,
.
Tout
X
(4) Radium
— —
226, Total
X
it. Su ate
(aa SO4)
x
lk
114808-79-8
I. Sulfide
(aa Sl
X
M.Su fe
(as S03)
(14265-45.3)
X
n. Surfactant,.
X
o. Aluminum,
Total
X
(7429.90-5)
P. ar um,
Total
(7440.39-3)
x
o. ron,
Total
X
(7440-42.8)
r. Cobalt,
Tout
(7440.48-4)
a Iron, Total
(7439.89-6)
t- Mafnalum,
Total
(7439.95-4)
U. Molybdenum,
Tx
Tout
(7439.98.7)V.
en9emw,
Toul(7439-96.6)Tin,
Tout
(1440-31-5)
x. Titanium,
Tout
x
17440.32.6)
EPA Form 3510.2C (8.90) * Awaiting Receipt of Analytical Results FAoc V-4 CONTINUE ON PAGE V.3

EFA I.D. NUM DER (COPY from ftem 1 OJ Form 1)
OU TFALL NUMBER
NCDO53488409
002
CONTINUED FROM PAGE 3 OF FORM 2-C
PARTC- Ifyouareaprimaryy industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractionsyou must test for. Mark •'X"in column
2-a for all such GINS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess
wastewater oude//s, andnonrequired GC/MS fractions), mark "X" in Column 2•b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you
believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results
of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4
dinitrophenol, or 2-methyl-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to believe that you discharge in
concentrations of 100ppb orgreater.Otherwise, for pollutants for which you markcolumn 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant isexpected to
be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (a//7 pages) for each outfall. See instructions for additional details and requirements.
t. POLLUTANT
2. MARK •X'
3. EFFLUENT
4. UNITS
5. INTAKE (optionO
AND CAS
NUMBER
1NOt
❑ ya.
C Cos•
a. MAXIMUM DAILY VALUE
b. MAXI M apo
auaOab%
pp Y'VALUE
C.LONG T M i�yypp VALUE
4uwND1aCONCEW
d NO.OF
a. LONG
ER
TERM
E
b. NO.OF
(it available)
waw
w
iirwi
lava
si�,T
ANAL-
vse3
aTRATION
b. MASS
ANAL-
YSESa
11)
UI nwss
Ix1MAss
L1 Nwas
I�iw,'nonw
(�) M
eowcew.wwTo..
CONC.HVRAr,
cewe)w AT,ow
METALS, CYANIDE, AND TOTAL PHENOLS
1M. Antimony,
Tout (7440-36-0)
X
2M. Arsenic, Total
(7440-38-2)
X
3M. Beryllium,
Total, 7440.41.7)
X
4M. Cadmium,
X
Total(7440-43-9)
SM. Chromium,
Total (744047.3)
X
am. Caliper, Tool
08)
A9
p444s
X
711A. Lost Tout
(7439-92-11
X
SM. Mercury, Tout
(743"7-6)
X
9M. Nickel, Total .
(744602-0)
X
16M. Selenlum,
Total:(7782-49-2)
X
. 11 U. Sl Ivw, Total .
(7440.22.4)
X
12M. Thelllum,
Tout (7440.28-0)
X
13M.'Zinc, Total
(7440-64-6)
X
0.015
0.02
mg/L
Ibs/day
14M. Cyanide,
Total(57-12•5)
X
IBM. Phanols,
X
--
Total
DIOXIN
2,3,7.8-Tatra-
DESCRIBE RESULTS
cldgadlbenzo-P-
X
0bot4+ (T764.01.6)
EPA Form 3610.2C (8-90) PAGE V-3 CONTINUE ON REVERSE

1. POLLUTANT
AND CAS
a..MARK •A•
3. EFFLUENT
4• UNITS
S. INTAKE (optional)
NUMBER
' of
ti a<
`e
y-'
`ai
a. MAXIMUM DAILY VALUH
. MAXI M b
aaa
DAY VALUE
/labM
c.LONG T M IfYR VALUE
ae <
a1bCI
d NO.OF
e. LONGTERM
AVERA
L NO.01
(Jl oedlaD!<)
ewuu-
ova
U.-
Hi
ANAL-
_
eTRAT ON
b. MASS
ANAL-
U)
([) rwn
ICI
la) rwu
lien rvcan-
corvcwnrwwnox
corvcaxiw.noN
coece Ni)nwnoN
h) rwsa
YSES
en
1[I rwaa
YSES
OCA43 FRACTION — VOLATILE COMPOUNDS
IV. Acroleln
(107-02-8)
X
2V. Aerylonitrlle
(107-13-1)
3V. Benzene
(71.43-2)
X
[
4V. Bla
methyl) Ether
EtheEthe.1)
X
(542$8
5V. Bromoform
(75-25-2)
X
6V. Carbon
Tetrachloride
y
(56-23-5)
A
7 V. Chlorobanzene
(108-90-7)
X
8 V. Chlorodi.
bromomathane
y
A
(12448-1)
9V. Chloroethene
(75-00-3)
X
10V. 2-Chloro-
sthyNlnyl Ether
x
(11 D-75$)
11 V. Chloroform
(67-66-3)
X
12V. Dichloro.
bromomathane
x
(75-27-4)
13V. Dichloro-
dlfluoromethane
x
(75-71-8)
14V. 1,1-Dichloro-
ethane (75-34-3)
y
/�
15V. 1,2.Dichloro-
etheM(107-06-2)
X
16V. 1,1.Dlchloro-
eMylene (75-35-4)
X
17V. 1,2-Dichloro-
propane (78-87-5)
X
16V. 1,3-Didduo-
prapylene(542-75-8)
X
19V. Ethyibonzeno
(100-41<)
X
20V. Mathyl
Bromide (74-83-9)
X
21 V. Methyl
Chloride (74$7.3)
X
EPA Form 3011M2b (e-r) PAGE V-4 CONTINUE ON PAGE V-'.

.V rinUeu rnVN ^Or u-
1. POLLUTANT
z. MwwN •x•
77
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
AND CAS
NUMBER
♦• T
t\ Ve
C e`.
L MAXIMUM DAILY VALUE
b. MAXI M
ouo
p Y VALUE
S%
c.LONG T pM
ilaua4a��e
VALUE
d NO OF
a. LONG
TERM
b. NO.Or
(if oudWbls)
o".'w.
ii.`.i
aY
ei�T
ANAL-
YSES
e. eONCEN-
TRATION
D MASS
ANAL'
YSES
1�1, ITI Nwee
c oxcenrwxno..
LI
lal rover
oxe ei.T)w.nox
la) v
(�� coxc aw-
lal Roves
�OCIAAS FRACTION — VOLATILE COMPOUNDS (continued)
22V. Methylene
x
Chloride (76-09-2)
23V:. 11,2,2-Tetr►
eh *
bro
X .
(79.34.5)
24V. Teirachloro-
X
ethyNm (127-18-4)
25V. Toluene
x
(106488.3)
26V. 1,2-Trend
Dlchlorocthylene
X
'
(156.6(")
27V. 1,1,1-Tri-
chlorcethane
X
(71-55-6)
28V. 1,1,2-Tn-
chloroethane
X
(79-DO-5)
29V. Trichloro.
e hylene (79-01-6)
X
30V. Trlchloro.
iluorometham
X
(75.89-4)
31V. Vinyyl
x
Chloride (75-014)
GC/MS FRACTION — ACID COMPOUNDS
IA. 2-ChlorophenP
x
(95-57-8)
2A. 2,4-Dichloro.
phenol(120-83-2)
x
3A. 2,4-Dimethyl-
phenol(105-67-9)
X
4A. 4,6-D1n1tro-0-
Creeol(534-52-1)
X
5A.-2.401nitro-
Phenol (51-28.5)
x
GA. 2-Nitrophanol
(88.75-5)
X
7A. 4-Nltrophenol
(100.02-7)
X
GA. P-Chloro-M-
Creeol(59-50.7)
x
9A; Pentechloro-
phwio1(87-86-5)
x
' 70A:.Phenol
x
AI *Td-
:oli 1
X
l
EPA Form 351D-2C (8-00) PAGE V-5 CONTINUE ON REVERSE

I.
PAND CABNT
2. MARK W
3, EFFLUENT
4. UNITS
5. INTAKE /+rplinnal)
NUMBER
TriT
aa'
se
C ee-
a. MAXIMUM DA14V VALUE
0. MAXIM M 9,�
aUal
DAV VALUE
a ¢
C.40NG T�RM
I aaa
R`6Pf• °"`�E
a 8
4 NO.OF
e. LONG
TERM
(it available)
eirie-
ve
aireiT
,1
A-
ANAL-
e. CDNC[N-
TRATIONUI
b. MASS
b. NO.OF
ANAv
1.1 III "+wea
l+l x.es
I1
1+1
coxc axtwwaoe
coxc aeixwn ox
c="cexrxwnox
rev
VSES
coxc as
TwwT,ax
1+1Nve
rs[s
GC/MS FRACTION— SASE/NEUTRAL
COMPOUNDS
18. Acensphthene
(83-32.9)
X
28. Aaanaphtylene
(208-96-e)
X.
38. Anthracene
X
1120-12-7)
46. Senzid In*
X
-------
(92-87-5)
58. Benzo (a)
Anthrecens
X
_
b6-b5-3)
6B. Benzo (a)
X
Pyrene (M325)
76. 3,4•Benzo-
-
HuorEnthens
X
(206.89.2)
so, Benzo ON)
PerYlelle
X
191.24.2)
as.:Benzo (k)
Fluorenthene
X
4207-08-9)
10e. ale (2-Chloro
wthoxy) Methane
X
(111-91-t)
110. Ills(2-Chloro-
ethyl) Ether
X
(111-"4)
126. Bs 12-C"bro
X
proPAEMw(102-60.1)
138. BIB (2-Ethyl-
haxyl) Phthelete
X
(117-61-7)
,146. 4-Bromo-
.yyhelljtt Phenyl
X
1Eth4,(101.86-3)
165. Butyl Benzyl
--
PhNwlm (85-66-7
X
166-2Chloro-
hthalmw
X
14
178.Chlo{O-
ePfw6 B)PhenV1
X
Ether f7OO5-72-3)
185. Chry"ne
1218.01-9)
X
198: AIbenzo (a.h)
-
Anthm"ne
X
153-70-3)
20B. 1,2-0ichloro-
benzena(95.50-1)
X
218. 1,3-Dichloro-
benzans
X
(541-73-1
EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7

Gum I INULU hHum PAUL Vi
1. POLLUTANT z. MARK'X 13. EFFLUENT
AND CAS
d. UNITS
5. INTAKE (up tinno!/
b. MAXI M ]o pA Y VALUE C.LONG T M .VALUE
NUMBER et„�T 4 [[- �'• a. MAXIM VM DAILY VALUE ��� d No
4Ve1
a. LONGTERM
ev[ 1 aea o ¢ .OF
(t/OUGIIObIf a ANAL-
1 OVu- PI
ii.+ir ai:T Irl NA++ 111 ..w++ 14 �•++ YSES
a' CDNCE N' b. MASS
TRATION
A b NO.OF
(,I ocxcex. ANAL-
conc[w�iwwno.. oxc [.1.iwwnow
OC/M6 FRACTION —BASE/NEUTRAL COMPOUNDS (continued,
x Ton 1+1 rwu USES
32.B. 1,4Dlchloro-
p0=sna (106-46.7
X
738:3.7-01chlor
b dn
X
248.10NShyl
VaIa,thyl
X
pm -Butyl
Z7,8..$4Dlnit
WIu4M_(t21.14-42)
X
289. 2.6-Dlnitr -
tolusne (50640-21
X
29B. OI-N-Octyl
Phthah"
X
(117-84-0)
308. 1.2-Oiphenyl•
hydrezim(as Aso-
X
bekstne)(/22-66-7
31 IL Fluorenthene
(206-44-0)
X
328. Flu"*
(86-73-7)
X
HaschWabommma
, (�118.744) .
X
34B. Hexa-
chlorobutWiens
X
(B7.88.3)
36B. Hexechloro-
cyclopsntsdlsne
X
(77-47-4)
368. Hexechloro-
ethens (67.72-1)
X
378.Indeno
(1,2,3.cd) Pyrene
X
(193-39-5)
38B. Itophorone
(76-59-1)
X
39B. Naphthalene
(91.20-3)
X
40B. Nltrobanzens
X
(98.95-3)
41B. N-Nitro-
zodimethylemine
X
(62-75-9)
428. N-NIVo+odi-
N-Propylamine
X
621-64-7
EPA Form 3510-2C (8-N) PAGE V-7 CONTINUE ON REVERSE

CONTINUFn FRrtaa TMF FRr1111T
!. POLLUTANT I 2. MARK •X• I3. EFFLUENT
4. UNITS
AND CAS
6. INTAKE (aprionol)
NUMBER *aar h aa- G aa- a, MAXIMUM DAILY VALUE . MAXI M ]yy pp//��Y VALUE C.LONG TCjrM /�y@(i VALUE
un uava OVallaclf (//OVC110618J Q NO.OF
a. LONG TERM
�Na
ANAL
(I(auairNwaf Ni (a)wu
C5tahleJ
TRATION
O.OF
b_ rHAL
+YSES
cnncawswnnow
+coec ew I+) r+
YSE$
GC/MS FRACTION — SASE/NEUTRAL COMPOUNDS (continued)
aanoA
436. N-Nkro-
sodlpMAYlamine
y
(B&3Q6)
A
448. Phenanthrene
166-018)
�(
458. Pyre:
(129-00-0)
A
460. 1,2,4 - Tri-
chlorOhMlaane
v
OCAiPRACTION — PESTICIDESA
(309-M2)
X
2P, a-SHC
(319434-6)
X
3P. B C
(31 7)
X
4P. yy BNC
(68-o9.9)
X
5P. S-8NC
(3194188)
X
8P. Chlordane
(57.748)
X
7P. 4,4'-DDT
(50-2")
X
BP. 4,4•-DDE
172-55-9)
X
9P. 4,4'-ODO
(72-6")
X
10P. Dleldrin
(60467-1)
x
11P. 0-Endowlfan
(115-29-7)
X
12P. Q-Endowlfan
(115-29-7)
X
131P. Endowlfen
3ulfala
(1031-078)
X
W. Endrin
[72.208)
X
top. Endrin
4ldehyde
X
;7421-93-4)
I6P. Heptachlor
!76-448)
X
7A Form 3510-2C (8.90) PAGE V-8 CONTINUE ON PAGE V 9

XINTINUED FROM PAGE V-8
NCDO53488409
002
1. POLLUTANT
i. MwRlc'x•
3. EFFLUENT
4. UNITS
S. INTAKE (�xplional)
NUMBER
"•'
b. •a' �a•-
a
a. MAXIMUM
DAILY vALU6
. MAXI M io
OYY7/0b1f
p/:Y VALUE
C.LONG TgpM
(f/pua&b/B)
/�yp�e A
d NO.OF
a. LONG
TERM
(I/auaiWble)
ina
o�`w-
eve
iinr veer
a. CONCEN.
TRATION
b. MASS
b.NO OF
e;
11
1.) Nwvv
1•) "xwv
conc ewrwwnan
«c an1iwwrmw
co«cew.r
Id w. vv
YSES
(�'w owcen-
wno«
Ixl wwu
YSES
GC/MS FRACTION —PESTICIDES (continued)
17P. H"chlor
EpoxMa
X
(1024-57-3)
18P. PCB-1242
(53460.21-9)
x
19P. PCB-1254
X
(11097.69-1)
20P. PCB-1221
--_
(11104-28-2)
x
21P. PCB-1232
(11141-16-6)
X
22P. PCB-1248
x
-
(12672-29.6)
t3P. PCB-1260
1109482-5)
X
14P. PCB-1016
.12674-11-2)
X
15P. Toxaphane
x
:8001-35-2)
PAGE V-9
Form 3510-2C (B-90)

EPA Form 2C
Additional/Supplementary Information
Performance Fibers, Inc.

Item II. A.
Water Flow Line Drawing

Discharge
NO. 002
(113 GPD)
Air
Compressor
and Steam
Condensate
Srm
Wattoer
Air Dryer
HAW
RIVER
261 I 8
Overflow Fire 01
33 Pond v
0
220
Potable Alum
Water Settling
Treatment 5 Pond
1215
5
Process
1.5 Oil Mist
Air Pollution
Control 1,1
System
1.0 Oil
—r Pre -Treatment -
0 WATER i
---E> EVAPORATION --�
—► STEAM
--.� OIL
0.2
_ Polishing 4.7
v 4.9 Pond
Cooling 10 i.0 6.75
Towers 62.7 Sanitary Beam a
TN!-1. 4. 5.6 Cleaning
23.3 10 1.0
wastewater Cl'
�(83.05 GPD) Tr e,tm nt Disinfection
77.3
j 0.25
W
Concentrated
Oil Emulsion
,Shipped Off -site
J(:HtMA I IU OF
FLOW
PERFORMANCE FIBERS, INC.
NEW HILL, CHATHAM
COUNTY
NORTH CAROLINA
NPOES Permit No. NC0001899
Discharge
NO. 001
v (82 GPD)
NOTE. Flows are listed in units
of thousands of gallons.

Item Il. B. Outfall Descriptions
Outfall 001
Performance Fiber's Moncure, North Carolina facility operates a 0.244-MGD wastewater
treatment facility with the following components and with final discharge through Outfall 001 to
the Haw River:
• Sanitary Flow Bar Screen and Grinder
• Process Wastewater Bar Screen
• Neutralization Chamber
• Aeration Basin
• Clarifier
• Sludge Drying Bed
• Optional Polishing Pond
• Chlorine Gas Disinfection
• Chlorine Contact Chamber.
Two separate pipelines transport process and sanitary waste to the wastewater treatment plant.
Process wastewater comes primarily from non -process cooling tower blowdown with smaller
contributions from the following: steam condensate, regenerated water from water softeners,
demineralizer blowdown, water rinse from polyester parts cleaning operations, stormwater from
raw material handling areas, finish oil pretreatment (ultrafiltration permeate), beam cleaning and
manufacturing building floor drains.
Sanitary wastewater comes primarily from plant restrooms, cafeteria, and custodial sinks. The
plant has a separate sanitary collection system that flows to a lift station. Sanitary waste is
blended in a comminutor, or the comminutor may be bypassed in the event of a mechanical
failure and the flow would be directed through a bar screen. From the lift station, the sanitary
influent is pumped directly into the aeration basin.
The process wastewater flows into a lift station adjacent to the sanitary lift station. It is then
pumped into a 1,200 gallon neutralization/mixing basin at the north end of the aeration basin. A
mixer provides thorough mixing to keep settleable solids in suspension and to aid in the
dispersion of pH control chemicals. A pH probe is used to measure influent pH and transmits a
signal to the pH analyzer/controller. The pH controller regulates the speed of a sulfuric acid
pump, which is used to control pH. The mixing basin then discharges through a 6" pipe into the
aeration basin.
The aeration basin has a capacity of 650,000 gallons and contains four surface aerators to
introduce oxygen into the water and provide mixing horsepower.
Water from the aeration basin overflows a weir into a 20' diameter clarifier. The clarifier is
designed with a surface overflow rate of 440 gallons/ftZ/day. A liquid coagulant is added to the
water as it flows from the aeration basin to the clarifier to aid in solids settling. The clarifier is
equipped with surface and bottom sweep arms. The surface sweep arm directs floating solids to a
scum pit. The bottom sweep rakes sludge to be recycled or wasted. Sludge pumps remove settled
solids from the bottom of the clarifier and either pump the recycled sludge back to the aeration
basin or waste it to the sludge drying beds.

Clarifier overflow can be valved to a one -million gallon capacity polishing pond for additional
solids removal or directly into the chlorine contact chamber. Thus, overflow form the clarifier,
water from the polishing pond, or a blended flow from both structures enters a 9' X 37' X 3'
chlorine contact chamber that is designed for a minimum of 30 minutes contact time at a flow rate
of 90 gpm. The chlorinators located in the wastewater treatment plant lab building are manually
controlled and the chlorination room is equipped with a chlor-alert alarm system. Chlorine is
supplied to the chlorinators through scale -mounted 150 lb. cylinders. Chlorine recirculation
pumps transfer water from the effluent end of the chlorine contact chamber and supplies the
diluted water through the chlorine injector. The chlorinated water is returned through a
submerged diffuser to the influent end of the contact chamber.
Effluent flow from the chlorine contact chamber is measured before it enters an underground
pipeline that discharges directly into the Haw River.
Outfa11002
Stormwater, steam condensate, air dryer condensate, and fire pond overflow discharge through
Outfall 002 to Shaddox Creek. The drainage system which reports to Outfall 002 includes a
system of baffles and weirs designed to contain accidental spills of oil. In an emergency, flow
can be contained in a holding pond and pumped to a storage or pumped to the process sewer.

Item III. A & B. Production
On November 5, 1987 EPA issued regulations establishing effluent limitations for the Organic
Chemicals, Plastics, and Synthetic Fibers (OCPSF) industrial category. Provisions of Subpart C
(414.31) and Subpart 1(414.90) Direct Discharge Point Sources That Use End -of -Pipe Biological
Treatment are applicable to process wastewater discharges from the manufacture of polyester
fiber and resin. OCPSF effluent guidelines are not expressed in terms of production. No metal -
bearing waste streams or cyanide -bearing waste streams listed in Appendix A to Part 414 exist in
the manufacture of polyester fiber and resin.

Item V. A-C.
Characteristics listed in Item V reflect data from January 1, 2005 - January 25, 2006. For some
parameters, testing was conducted throughout the •year, while other parameters were tested
annually. One time testing was conducted for most of the parameters.
For all of the pollutants marked with an asterisk (*), sampling has occurred and Performance
Fibers is awaiting receipt of the analytical results from the certified laboratory. When the results
are received, Item V will be completed in full and submitted to DWQ.

Item VI.
The following is a list of Item V-C pollutants that are present on the plant site. None of these
materials are used as a raw material or intermediate and none of these materials are manufactured
as a product or a by-product of the manufacturing process. The list may not be exhaustive, as
some commercial products are considered proprietary by the manufacturer and their specific
composition is not known to us. In addition, some new materials may be obtained in the future
that contain one or more of the listed chemicals and whose composition may not be known to us.
Pollntant
Use on Site
Antimony
Lab Reagent
Chromium
Lab Reagent
Copper
Lab Reagent
Lead
Lab Reagent
Mercury
Lab Reagent, Instrumentation
Nickel
Lab Reagent
Silver
Lab Reagent, Electrical Equipment
Zinc
Lab Reagent
Phenols
Lab Reagent
Carbon Tetrachloride
Lab Reagent
Chloroform
Lab Reagent
Dichlorodifluoromethane
Lab Reagent, Refrigerant, Leak Cheeks
1,1,2,2-Tetrachloroethane
Lab Reagent
Tetrachloroeth lene
Solvent
Titanium Chelate
Catalyst
Toluene
Lab Reagent
1, 1, 1 -Trichloroethane
Solvent
Trichloroeth lene
Solvent
Phenol
Lab Reagent
Dichlorobenzene
Lab Reagent
1,2,4-Trichlorobenzene
Electrical Equipment
PCB
Electrical Equipment