NC0038377_J15030202 Report_20150902

DUE Analytical Laboratory Page 1 of 113
ENERGY
Order Number:
Project Name:
Customer Name(s):
Customer Address:
Lab Contact:
Report Authorized By:
(Signature)
Program Comments:
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
J15030202
AB GW ASSESSMENT SOIL
Tim Hunsucker, Jerry Wylie, Kathy Webb, John Toepfer
Margaret Galvin -Karr Phone: [phone]
i V _ marge.galvin-karr@duke-
RGY IX" energy.com 2015.04.08 14:47:26 -04-00, Date:
Margaret Galvin -Karr
Please contact the Program Manager (Margaret Galvin -Karr) with any questions regarding this report.
Data Flags & Calculations:
4/6/2015
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Page 2 of 113
Sample ID Plant/Station
Collection
Date and Time Collected By
Sample Description
2015006511
MAYO STEAM
03-Mar-15 3:24 PM
illegible
SB-2 (0.5-2.0)
2015006512
MAYO STEAM
03-Mar-15 3:52 PM
illegible
SB-2 (11.0-12.5)
2015006513
MAYO STEAM
03-Mar-15 3:58 PM
illegible
SB-2EB
2015006514
MAYO STEAM
04-Mar-15 10:15 AM
illegible
SB-5 (1.0-2.0)
2015006515
MAYO STEAM
04-Mar-15 10:25 AM
illegible
SB-5 (2.3-3.3)
2015006516
MAYO STEAM
04-Mar-15 11:10 AM
illegible
SB-5(8.0-9.0)
2015006517
MAYO STEAM
04-Mar-15 10:02 AM
illegible
SB-5EB
2015006518
MAYO STEAM
04-Mar-15 1:10 PM
illegible
SB-6 (1.0-2.0)
2015006519
MAYO STEAM
04-Mar-15 12:39 PM
illegible
SB-6EB
2015006520
MAYO STEAM
04-Mar-15 2:47 PM
illegible
SB-3 (5.0-6.0)
2015006521
MAYO STEAM
04-Mar-15 3:05 PM
illegible
SB-3 (17.0-18.5)
2015006522
MAYO STEAM
04-Mar-15 2:16 PM
illegible
SB-3EB
2015006523
MAYO STEAM
04-Mar-15 4:25 PM
illegible
S13-1 (1.0-2.0)
2015006524
MAYO STEAM
04-Mar-15 4:45 PM
illegible
SB-1 (13.5-14.5)
2015006525
MAYO STEAM
04-Mar-15 5:30 PM
illegible
SB-1 EB
15 Total Samples

Page 3 of 113
Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals Yes No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes No
All laboratory QA/QC requirements are acceptable. (] Yes ❑ No
Report Sections Included:
L� Job Summary Report
❑ Sample Identification
n Technical Validation of Data Package
6 Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
LVI Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
6 Chain of Custody
LVI Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: DBA Account Date: 4/6/2015

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030202
Site: SB-2 (0.5-2.0)
Collection Date: 03-Mar-15 3:24 PM
Analyte Result Units Qualifiers RDL DF
PERCENT SOLIDS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
DIONEX ANIONS BY VENDOR - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
PH IN SOIL - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
TOTAL ORGANIC CARBON IN SOILS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
Page 4 of 113
Sample #: 2015006511
Matrix: SOIL
Method Analysis Date/Time Analyst
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030202
Site: SB-2 (11.0-12.5)
Collection Date: 03-Mar-15 3:52 PM
Analyte Result Units Qualifiers RDL DF
PERCENT SOLIDS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
DIONEX ANIONS BY VENDOR - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
PH IN SOIL - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
TOTAL ORGANIC CARBON IN SOILS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
Page 5 of 113
Sample #: 2015006512
Matrix: SOIL
Method Analysis Date/Time Analyst
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE

Certificate of Laboratory Analysis Page 6 of 113
This report shall not be reproduced, except in full.
Order # J15030202
Site: SB-2EB
Collection Date: 03-Mar-15 3:58 PM
Analyte Result Units Qualifiers RDL DF
METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
Sample #: 2015006513
Matrix: SOIL
Method Analysis Date/Time Analyst
Vendor Method V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030202
Site: SB-5 (1.0-2.0)
Collection Date: 04-Mar-15 10:15 AM
Analyte Result Units Qualifiers RDL DF
PERCENT SOLIDS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
DIONEX ANIONS BY VENDOR - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
PH IN SOIL - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
TOTAL ORGANIC CARBON IN SOILS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
Page 7 of 113
Sample #: 2015006514
Matrix: SOIL
Method Analysis Date/Time Analyst
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030202
Site: SB-5 (2.3-3.3)
Collection Date: 04-Mar-15 10:25 AM
Analyte Result Units Qualifiers RDL DF
PERCENT SOLIDS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
DIONEX ANIONS BY VENDOR - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
PH IN SOIL - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
SPLP LEACHATE - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
TOTAL ORGANIC CARBON IN SOILS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
Page 8 of 113
Sample #: 2015006515
Matrix: SOIL
Method Analysis Date/Time Analyst
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030202
Site: SB-5(8.0-9.0)
Collection Date: 04-Mar-15 11:10 AM
Analyte Result Units Qualifiers RDL DF
PERCENT SOLIDS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
DIONEX ANIONS BY VENDOR - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
PH IN SOIL - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
SPLP LEACHATE - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
TOTAL ORGANIC CARBON IN SOILS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
Page 9 of 113
Sample #: 2015006516
Matrix: SOIL
Method Analysis Date/Time Analyst
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030202
Site: SB-5EB
Collection Date: 04-Mar-15 10:02 AM
Analyte Result Units Qualifiers RDL DF
METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
Page 10 of 113
Sample #: 2015006517
Matrix: SOIL
Method Analysis Date/Time Analyst
Vendor Method V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030202
Site: SB-6 (1.0-2.0)
Collection Date: 04-Mar-15 1:10 PM
Analyte Result Units Qualifiers RDL DF
PERCENT SOLIDS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
DIONEX ANIONS BY VENDOR - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
PH IN SOIL - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
TOTAL ORGANIC CARBON IN SOILS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
Page 11 of 113
Sample #: 2015006518
Matrix: SOIL
Method Analysis Date/Time Analyst
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030202
Site: SB-6EB
Collection Date: 04-Mar-15 12:39 PM
Analyte Result Units Qualifiers RDL DF
METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
Page 12 of 113
Sample #: 2015006519
Matrix: SOIL
Method Analysis Date/Time Analyst
Vendor Method V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030202
Site: SB-3 (5.0-6.0)
Collection Date: 04-Mar-15 2:47 PM
Analyte Result Units Qualifiers RDL DF
PERCENT SOLIDS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
DIONEX ANIONS BY VENDOR - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
PH IN SOIL - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
TOTAL ORGANIC CARBON IN SOILS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
Page 13 of 113
Sample #: 2015006520
Matrix: SOIL
Method Analysis Date/Time Analyst
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030202
Site: SB-3 (17.0-18.5)
Collection Date: 04-Mar-15 3:05 PM
Analyte Result Units Qualifiers RDL DF
PERCENT SOLIDS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
DIONEX ANIONS BY VENDOR - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
PH IN SOIL - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
SPLP LEACHATE - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
TOTAL ORGANIC CARBON IN SOILS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
Page 14 of 113
Sample #: 2015006521
Matrix: SOIL
Method Analysis Date/Time Analyst
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030202
Site: SB-3EB
Collection Date: 04-Mar-15 2:16 PM
Analyte Result Units Qualifiers RDL DF
METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
Page 15 of 113
Sample #: 2015006522
Matrix: SOIL
Method Analysis Date/Time Analyst
Vendor Method V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030202
Site: SB-1 (1.0-2.0)
Collection Date: 04-Mar-15 4:25 PM
Analyte Result Units Qualifiers RDL DF
PERCENT SOLIDS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
DIONEX ANIONS BY VENDOR - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
PH IN SOIL - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
TOTAL ORGANIC CARBON IN SOILS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
Page 16 of 113
Sample #: 2015006523
Matrix: SOIL
Method Analysis Date/Time Analyst
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030202
Site: SB-1 (13.5-14.5)
Collection Date: 04-Mar-15 4:45 PM
Analyte Result Units Qualifiers RDL DF
PERCENT SOLIDS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
DIONEX ANIONS BY VENDOR - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
PH IN SOIL - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
SPLP LEACHATE - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
TOTAL ORGANIC CARBON IN SOILS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
Page 17 of 113
Sample #: 2015006524
Matrix: SOIL
Method Analysis Date/Time Analyst
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE

Certificate of Laboratory Analysis Page 18 of 113
This report shall not be reproduced, except in full.
Order # J15030202
Site: SB-1 EB
Collection Date: 04-Mar-15 5:30 PM
Analyte Result Units Qualifiers RDL DF
METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
Sample #: 2015006525
Matrix: SOIL
Method Analysis Date/Time Analyst
Vendor Method V_PACE

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P36g01qrwy.,k�e. Suite 100
Huntersville, INC 28078
[phone]
March 30, 2015
Program Manager
Duke Energy
13339 Hagers Ferry Road
Bldg.7405 MG30A2
Huntersville, NC 28078
RE: Project: J 15030202
Pace Project No.: 92240158
Dear Program Manager:
Enclosed are the analytical results for sample(s) received by the laboratory on March 06, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
HORIZON Database Administrator
Enclosures
cc: Marge Galvin -Karr, Duke Energy
Program Manager, Duke Energy
Rodney Wilke, Duke Energy
p«FO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
lqe� ��� without the written consent of Pace Analytical Services, Inc..
BRAT,
Page 1 of 94

lacmnalyfica(
www.pacelabs.com
Pace Analytical Services, Inc.
PgB99aO�ar&y.11e. Suite 100
Huntersville, NC 28078
[phone]
Project: J15030202
Pace Project No.: 92240158
Minnesota Certification IDs
1700 Elm Street SE Suite 200, Minneapolis, MN 55414
A21-A Certification #: 2926.01
Alaska Certification #: UST-078
Alaska Certification #MN00064
Alabama Certification #40770
Arizona Certification #: AZ-0014
Arkansas Certification #: 88-0680
California Certification #: 01155CA
Colorado Certification #Pace
Connecticut Certification #: PH-0256
EPA Region 8 Certification #: 8TMS-L
Florida/NELAP Certification #: E87605
Guam Certification #:14-008r
Georgia Certification #: 959
Georgia EPD #: Pace
Idaho Certification #: MN00064
Hawaii Certification #MN00064
Illinois Certification #: 200011
Indiana Certification#C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky Dept of Envi. Protection - DW #90062
Kentucky Dept of Envi. Protection - WW #:90062
Louisiana DEQ Certification #: 3086
Louisiana DHH #: LA140001
Maine Certification #: 2013011
Maryland Certification #: 322
Michigan DEPH Certification #: 9909
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Green Bay Certification IDs
1241 Bellevue Street, Green Bay, WI 54302
Florida/NELAP Certification #: E87948
Illinois Certification #: 200050
Kentucky Certification #: 82
Louisiana Certification #: 04168
Minnesota Certification #: 055-999-334
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
CERTIFICATIONS
Minnesota Certification #: 027-053-137
Mississippi Certification #: Pace
Montana Certification #: MT0092
Nevada Certification #: MN_00064
Nebraska Certification #: Pace
New Jersey Certification #: MN-002
New York Certification #: 11647
North Carolina Certification #: 530
North Carolina State Public Health #: 27700
North Dakota Certification #: R-036
Ohio EPA#: 4150
Ohio VAP Certification #: CL101
Oklahoma Certification #: 9507
Oregon Certification #: MN200001
Oregon Certification #: MN300001
Pennsylvania Certification #: 68-00563
Puerto Rico Certification
Saipan (CNMI) #:MP0003
South Carolina #:74003001
Texas Certification #: T104704192
Tennessee Certification #: 02818
Utah Certification #: MN000642013-4
Virginia DGS Certification #: 251
Virginia/VELAP Certification #: Pace
Washington Certification #: C486
West Virginia Certification #: 382
West Virginia DHHR #:9952C
Wisconsin Certification #: 999407970
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification #: 2958
New Jersey Certification #: FL765
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FLO1264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Washington Certification #: C955
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
North Dakota Certification #: R-150
South Carolina Certification #: 83006001
Texas Certification #: T104704529-14-1
US Dept of Agriculture #: S-76505
Wisconsin Certification #: 405132750
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
Pggc0 Sirpyl'y. Suite 100
Huntersville, NC 28078
[phone]
Project: J15030202
Pace Project No.: 92240158
Asheville Certification IDs
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
CERTIFICATIONS
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y S09r6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: J15030202
Pace Project No.: 92240158
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92240158001
2015006511
Solid
03/03/1515:24
03/06/15 14:15
92240158002
2015006512
Solid
03/03/1515:52
03/06/15 14:15
92240158003
2015006514
Solid
03/04/1510:15
03/06/15 14:15
92240158004
2015006518
Solid
03/04/1513:10
03/06/15 14:15
92240158005
2015006520
Solid
03/04/1514:47
03/06/15 14:15
92240158006
2015006523
Solid
03/04/1516:25
03/06/15 14:15
92240158007
2015006515
Solid
03/04/1510:25
03/06/15 14:15
92240158008
2015006516
Solid
03/04/1511:10
03/06/15 14:15
92240158009
2015006521
Solid
03/04/1515:05
03/06/15 14:15
92240158010
2015006524
Solid
03/04/1516:45
03/06/15 14:15
92240158011
2015006513
Water
03/03/1515:58
03/06/15 14:15
92240158012
2015006517
Water
03/04/1510:02
03/06/15 14:15
92240158013
2015006519
Water
03/04/1512:39
03/06/15 14:15
92240158014
2015006522
Water
03/04/1514:16
03/06/15 14:15
92240158015
2015006525
Water
03/04/1517:30
03/06/15 14:15
92240158016
2015006515 SPLP
Water
03/04/15 10:25
03/06/15 14:15
92240158017
2015006516 SPLP
Water
03/04/15 11:10
03/06/15 14:15
92240158018
2015006521 SPLP
Water
03/04/15 15:05
03/06/15 14:15
92240158019
2015006524 SPLP
Water
03/04/15 16:45
03/06/15 14:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
PA OzSIWYINe. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
J15030202
92240158
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92240158001
2015006511
EPA 6010
TAP
16
PASI-0
EPA 6020
CRT
8
PASI-O
EPA 7471
TAP
1
PASI-O
ASTM D2974-87
GPW
1
PASI-O
EPA 9045
MAB
1
PASI-A
EPA 9056
AIS
2
PASI-O
EPA 9056
AIS
1
PASI-O
EPA 9060
TJJ
6
PASI-G
92240158002
2015006512
EPA 6010
TAP
16
PASI-0
EPA 6020
CRT
8
PASI-O
EPA 7471
TAP
1
PASI-O
ASTM D2974-87
GPW
1
PASI-O
EPA 9045
MAB
1
PASI-A
EPA 9056
AIS
2
PASI-O
EPA 9056
AIS
1
PASI-O
EPA 9060
TJJ
6
PASI-G
92240158003
2015006514
EPA 6010
TAP
16
PASI-0
EPA 6020
CRT
8
PASI-O
EPA 7471
TAP
1
PASI-O
ASTM D2974-87
GPW
1
PASI-O
EPA 9045
MAB
1
PASI-A
EPA 9056
AIS
2
PASI-O
EPA 9056
AIS
1
PASI-O
EPA 9060
TJJ
6
PASI-G
92240158004
2015006518
EPA 6010
TAP
16
PASI-0
EPA 6020
CRT
8
PASI-O
EPA 7471
TAP
1
PASI-O
ASTM D2974-87
GPW
1
PASI-O
EPA 9045
MAB
1
PASI-A
EPA 9056
AIS
2
PASI-O
EPA 9056
AIS
1
PASI-O
EPA 9060
TJJ
6
PASI-G
92240158005
2015006520
EPA 6010
TAP
16
PASI-0
EPA 6020
CRT
8
PASI-O
EPA 7471
TAP
1
PASI-O
ASTM D2974-87
GPW
1
PASI-O
EPA 9045
MAB
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 5 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y RGA,16fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
J15030202
Pace Project No.:
92240158
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
EPA 9056
AIS
2
PASI-O
EPA 9056
AIS
1
PASI-O
EPA 9060
TJJ
6
PASI-G
92240158006
2015006523
EPA 6010
TAP
16
PASI-0
EPA 6020
CRT
8
PASI-O
EPA 7471
TAP
1
PASI-O
ASTM D2974-87
GPW
1
PASI-O
EPA 9045
MAB
1
PASI-A
EPA 9056
AIS
2
PASI-O
EPA 9056
AIS
1
PASI-O
EPA 9060
TJJ
6
PASI-G
92240158007
2015006515
EPA 6010
TAP
16
PASI-0
EPA 6020
CRT
8
PASI-O
EPA 7471
TAP
1
PASI-O
ASTM D2974-87
GPW
1
PASI-O
EPA 9045
MAB
1
PASI-A
EPA 300.0
AES2
1
PASI-A
EPA 353.2
DMN
1
PASI-A
SM 4500-CI-E
DMN
1
PASI-A
EPA 9056
AIS
2
PASI-O
EPA 9056
AIS
1
PASI-O
EPA 9060
TJJ
6
PASI-G
92240158008
2015006516
EPA 6010
TAP
16
PASI-0
EPA 6020
CRT
8
PASI-O
EPA 7471
TAP
1
PASI-O
ASTM D2974-87
GPW
1
PASI-O
EPA 9045
MAB
1
PASI-A
EPA 300.0
AES2
1
PASI-A
EPA 353.2
DMN
1
PASI-A
SM 4500-CI-E
DMN
1
PASI-A
EPA 9056
AIS
2
PASI-O
EPA 9056
AIS
1
PASI-O
EPA 9060
TJJ
6
PASI-G
92240158009
2015006521
EPA 6010
TAP
16
PASI-0
EPA 6020
CRT
8
PASI-O
EPA 7471
TAP
1
PASI-O
ASTM D2974-87
GPW
1
PASI-O
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 6 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3690Ar6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project: J15030202
Pace Project No.: 92240158
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
EPA 9045
MAB
1
PASI-A
EPA 300.0
AES2
1
PASI-A
EPA 353.2
DMN
1
PASI-A
SM 4500-CI-E
DMN
1
PASI-A
EPA 9056
AIS
2
PASI-O
EPA 9056
AIS
1
PASI-O
EPA 9060
TJJ
6
PASI-G
92240158010
2015006524
EPA 6010
TAP
16
PASI-0
EPA 6020
CRT
8
PASI-O
EPA 7471
TAP
1
PASI-O
ASTM D2974-87
GPW
1
PASI-O
EPA 9045
MAB
1
PASI-A
EPA 300.0
AES2
1
PASI-A
EPA 353.2
DMN
1
PASI-A
SM 4500-CI-E
DMN
1
PASI-A
EPA 9056
AIS
2
PASI-O
EPA 9056
AIS
1
PASI-O
EPA 9060
TJJ
6
PASI-G
92240158011
2015006513
EPA 6020A
RJS
24
PASI-M
EPA 7470
DM
1
PASI-M
92240158012
2015006517
EPA 6020A
RJS
24
PASI-M
EPA 7470
DM
1
PASI-M
92240158013
2015006519
EPA 6020A
RJS
24
PASI-M
EPA 7470
DM
1
PASI-M
92240158014
2015006522
EPA 6020A
RJS
24
PASI-M
EPA 7470
DM
1
PASI-M
92240158015
2015006525
EPA 6020A
RJS
24
PASI-M
EPA 7470
DM
1
PASI-M
92240158016
2015006515 SPLP
EPA 6020A
TT3
24
PASI-M
EPA 7470
DM
1
PASI-M
92240158017
2015006516 SPLP
EPA 6020A
TT3
24
PASI-M
EPA 7470
DM
1
PASI-M
92240158018
2015006521 SPLP
EPA 6020A
TT3
24
PASI-M
EPA 7470
DM
1
PASI-M
92240158019
2015006524 SPLP
EPA 6020A
TT3
24
PASI-M
EPA 7470
DM
1
PASI-M
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 7 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3Sy RGAr6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
Project: J15030202
Pace Project No.: 92240158
Lab Sample ID Client Sample ID
Method Parameters
SUMMARY OF DETECTION
Result Units Report Limit Analyzed
92240158001
2015006511
EPA 6010
Aluminum
10200
mg/kg
8.0
03/17/15 09:54
EPA 6010
Barium
65.7
mg/kg
0.80
03/17/15 09:54
EPA 6010
Beryllium
0.52
mg/kg
0.40
03/17/15 13:53
D3
EPA 6010
Boron
16.3J
mg/kg
19.9
03/17/15 13:53
D3
EPA 6010
Calcium
227
mg/kg
39.9
03/17/15 09:54
EPA 6010
Chromium
12.9
mg/kg
2.0
03/17/15 13:53
D3
EPA 6010
Copper
22.8
mg/kg
2.0
03/17/15 13:53
D3
EPA 6010
Iron
18300
mg/kg
3.2
03/17/15 09:54
EPA 6010
Magnesium
2420
mg/kg
39.9
03/17/15 09:54
EPA 6010
Manganese
365
mg/kg
2.0
03/17/15 13:53
D3
EPA 6010
Nickel
1.7
mg/kg
0.40
03/17/15 09:54
EPA 6010
Potassium
2020
mg/kg
79.8
03/17/15 09:54
EPA 6010
Strontium
4.3
mg/kg
0.80
03/17/15 09:54
EPA 6010
Zinc
27.3
mg/kg
1.6
03/17/15 09:54
EPA 6020
Arsenic
1.9
mg/kg
1.6
03/17/15 11:51
D3
EPA 6020
Cadmium
0.13J
mg/kg
0.19
03/17/15 11:51
D3
EPA 6020
Cobalt
6.4
mg/kg
1.6
03/17/15 11:51
D3
EPA 6020
Lead
7.5
mg/kg
1.6
03/17/15 11:51
D3
EPA 6020
Selenium
1.3J
mg/kg
1.6
03/17/15 11:51
D3
EPA 6020
Vanadium
44.8
mg/kg
1.6
03/17/15 11:51
D4
EPA 7471
Mercury
0.020
mg/kg
0.012
03/17/15 13:27
ASTM D2974-87
Percent Moisture
35.5
%
0.10
03/16/15 15:26
EPA 9045
pH at 25 Degrees C
5.3
Std. Units
0.10
03/12/15 15:55
EPA 9060
Total Organic Carbon
3450
mg/kg
928
03/13/15 10:12
EPA 9060
Total Organic Carbon
3640
mg/kg
929
03/13/15 10:17
EPA 9060
Total Organic Carbon
3880
mg/kg
922
03/13/15 10:23
EPA 9060
Total Organic Carbon
4020
mg/kg
935
03/13/15 10:29
EPA 9060
Mean Total Organic Carbon
3750
mg/kg
929
03/13/15 10:12
EPA 9060
RSD%
6.7
%
03/13/15 10:12
92240158002
2015006512
EPA 6010
Aluminum
5930
mg/kg
6.1
03/17/15 09:59
EPA 6010
Barium
31.3
mg/kg
0.61
03/17/15 09:59
EPA 6010
Beryllium
0.39
mg/kg
0.061
03/17/15 09:59
EPA 6010
Boron
7.8
mg/kg
3.1
03/17/15 09:59
EPA 6010
Calcium
22.2J
mg/kg
30.7
03/17/15 09:59
EPA 6010
Chromium
10.8
mg/kg
0.31
03/17/15 09:59
EPA 6010
Copper
5.5
mg/kg
0.31
03/17/15 09:59
EPA 6010
Iron
10300
mg/kg
2.5
03/17/15 09:59
EPA 6010
Magnesium
1070
mg/kg
30.7
03/17/15 09:59
EPA 6010
Manganese
69.4
mg/kg
0.31
03/17/15 09:59
EPA 6010
Molybdenum
0.89
mg/kg
0.61
03/17/15 09:59
EPA 6010
Nickel
0.91
mg/kg
0.31
03/17/15 09:59
EPA 6010
Potassium
800
mg/kg
61.5
03/17/15 09:59
EPA 6010
Sodium
30.9J
mg/kg
61.5
03/17/15 09:59
EPA 6010
Strontium
1.1
mg/kg
0.61
03/17/15 09:59
EPA 6010
Zinc
14.9
mg/kg
1.2
03/17/15 09:59
EPA 6020
Arsenic
1.5
mg/kg
1.2
03/17/15 11:53
D3
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y 91*r6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
Project: J15030202
Pace Project No.: 92240158
Lab Sample ID Client Sample ID
Method Parameters
SUMMARY OF DETECTION
Result Units Report Limit Analyzed Qualifiers
92240158002
2015006512
EPA 6020
Cobalt
1.6
mg/kg
1.2
03/17/15 11:53
EPA 6020
Lead
4.8
mg/kg
1.2
03/17/15 11:53
EPA 6020
Selenium
0.85J
mg/kg
1.2
03/17/15 11:53
EPA 6020
Vanadium
23.8
mg/kg
1.2
03/17/15 11:53
ASTM D2974-87
Percent Moisture
19.2
%
0.10
03/16/15 15:27
EPA 9045
pH at 25 Degrees C
6.0
Std. Units
0.10
03/12/15 15:55
EPA 9060
Total Organic Carbon
386J
mg/kg
743
03/13/15 11:32
EPA 9060
Total Organic Carbon
387J
mg/kg
747
03/13/15 11:38
EPA 9060
RSD%
5.2
%
03/13/15 11:25
92240158003
2015006514
EPA 6010
Aluminum
5320
mg/kg
34.0
03/17/15 13:58
EPA 6010
Barium
47.1
mg/kg
3.4
03/17/15 13:58
EPA 6010
Beryllium
0.36
mg/kg
0.34
03/17/15 13:58
EPA 6010
Calcium
313
mg/kg
170
03/17/15 13:58
EPA 6010
Copper
11.1
mg/kg
1.7
03/17/15 13:58
EPA 6010
Iron
8280
mg/kg
13.6
03/17/15 13:58
EPA 6010
Magnesium
1940
mg/kg
170
03/17/15 13:58
EPA 6010
Manganese
406
mg/kg
1.7
03/17/15 13:58
EPA 6010
Potassium
1730
mg/kg
340
03/17/15 13:58
EPA 6010
Strontium
4.2
mg/kg
3.4
03/17/15 13:58
EPA 6010
Zinc
36.3
mg/kg
6.8
03/17/15 13:58
EPA 6020
Arsenic
1.8
mg/kg
1.4
03/17/15 11:56
EPA 6020
Cadmium
0.12J
mg/kg
0.16
03/17/15 11:56
EPA 6020
Cobalt
2.8
mg/kg
1.4
03/17/15 11:56
EPA 6020
Lead
5.4
mg/kg
1.4
03/17/15 11:56
EPA 6020
Selenium
1.9
mg/kg
1.4
03/17/15 11:56
EPA 6020
Vanadium
6.8
mg/kg
1.4
03/17/15 11:56
ASTM D2974-87
Percent Moisture
26.5
%
0.10
03/16/15 15:29
EPA 9045
pH at 25 Degrees C
6.0
Std. Units
0.10
03/12/15 15:55
EPA 9060
Total Organic Carbon
503J
mg/kg
816
03/13/15 11:49
EPA 9060
Total Organic Carbon
573J
mg/kg
813
03/13/15 11:55
EPA 9060
Total Organic Carbon
484J
mg/kg
823
03/13/15 12:01
EPA 9060
Total Organic Carbon
445J
mg/kg
819
03/13/15 12:06
EPA 9060
Mean Total Organic Carbon
502J
mg/kg
818
03/13/15 11:49
EPA 9060
RSD%
10.6
%
03/13/15 11:49
92240158004
2015006518
EPA 6010
Aluminum
2510
mg/kg
6.4
03/17/15 10:07
EPA 6010
Barium
54.8
mg/kg
0.64
03/17/15 10:07
EPA 6010
Beryllium
0.17
mg/kg
0.064
03/17/15 10:07
EPA 6010
Boron
2.9J
mg/kg
3.2
03/17/15 10:07
EPA 6010
Chromium
0.74
mg/kg
0.32
03/17/15 10:07
EPA 6010
Copper
13.1
mg/kg
0.32
03/17/15 10:07
EPA 6010
Iron
3920
mg/kg
2.6
03/17/15 10:07
EPA 6010
Magnesium
816
mg/kg
32.1
03/17/15 10:07
EPA 6010
Manganese
192
mg/kg
0.32
03/17/15 10:07
EPA 6010
Nickel
0.55
mg/kg
0.32
03/17/15 10:07
REPORT OF LABORATORY ANALYSIS
D3
D3
D3
D3
D3
D3
D3
D3
D3
D3
D3
D3
D3
D3
D3
D3
D3
D3
D3
D3
D3
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3Sy RGAr6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
Project: J15030202
Pace Project No.: 92240158
Lab Sample ID Client Sample ID
Method Parameters
SUMMARY OF DETECTION
Result Units Report Limit Analyzed
92240158004
2015006518
EPA 6010
Potassium
801
mg/kg
64.2
03/17/15 10:07
EPA 6010
Sodium
67.2
mg/kg
64.2
03/17/15 10:07
EPA 6010
Strontium
4.1
mg/kg
0.64
03/17/15 10:07
EPA 6010
Zinc
14.7
mg/kg
1.3
03/17/15 10:07
EPA 6020
Arsenic
1.2J
mg/kg
1.3
03/17/15 12:05
EPA 6020
Cobalt
2.5
mg/kg
1.3
03/17/15 12:05
EPA 6020
Lead
4.2
mg/kg
1.3
03/17/15 12:05
EPA 6020
Selenium
0.901
mg/kg
1.3
03/17/15 12:05
EPA 6020
Vanadium
2.7
mg/kg
1.3
03/17/15 12:05
ASTM D2974-87
Percent Moisture
20.3
%
0.10
03/16/15 15:29
EPA 9045
pH at 25 Degrees C
5.9
Std. Units
0.10
03/12/15 15:55
EPA 9060
RSD%
4.7
%
03/13/15 12:11
92240158005
2015006520
EPA 6010
Aluminum
5030
mg/kg
5.3
03/17/15 10:12
EPA 6010
Barium
55.2
mg/kg
0.53
03/17/15 10:12
EPA 6010
Beryllium
0.15
mg/kg
0.053
03/17/15 10:12
EPA 6010
Boron
5.7
mg/kg
2.6
03/17/15 10:12
EPA 6010
Calcium
1420
mg/kg
26.4
03/17/15 10:12
EPA 6010
Chromium
20.7
mg/kg
0.26
03/17/15 10:12
EPA 6010
Copper
14.0
mg/kg
0.26
03/17/15 10:12
EPA 6010
Iron
8070
mg/kg
2.1
03/17/15 10:12
EPA 6010
Magnesium
3810
mg/kg
26.4
03/17/15 10:12
EPA 6010
Manganese
348
mg/kg
0.26
03/17/15 10:12
EPA 6010
Molybdenum
1.1
mg/kg
0.53
03/17/15 10:12
EPA 6010
Nickel
7.7
mg/kg
0.26
03/17/15 10:12
EPA 6010
Potassium
2950
mg/kg
52.7
03/17/15 10:12
EPA 6010
Sodium
104
mg/kg
52.7
03/17/15 10:12
EPA 6010
Strontium
11.0
mg/kg
0.53
03/17/15 10:12
EPA 6010
Zinc
30.8
mg/kg
1.1
03/17/15 10:12
EPA 6020
Arsenic
0.64J
mg/kg
1.1
03/17/15 12:07
EPA 6020
Cadmium
0.094J
mg/kg
0.13
03/17/15 12:07
EPA 6020
Cobalt
4.9
mg/kg
1.1
03/17/15 12:07
EPA 6020
Lead
2.4
mg/kg
1.1
03/17/15 12:07
EPA 6020
Vanadium
15.0
mg/kg
1.1
03/17/15 12:07
EPA 7471
Mercury
0.0096
mg/kg
0.0087
03/17/15 13:36
ASTM D2974-87
Percent Moisture
8.5
%
0.10
03/16/15 15:30
EPA 9045
pH at 25 Degrees C
8.6
Std. Units
0.10
03/12/15 15:55
EPA 9060
RSD%
5.0
%
03/13/15 12:35
92240158006
2015006523
EPA 6010
Aluminum
7030
mg/kg
7.0
03/17/15 10:16
EPA 6010
Barium
49.6
mg/kg
0.70
03/17/15 10:16
EPA 6010
Beryllium
0.24
mg/kg
0.070
03/17/15 10:16
EPA 6010
Boron
9.6
mg/kg
3.5
03/17/15 10:16
EPA 6010
Calcium
655
mg/kg
35.0
03/17/15 10:16
EPA 6010
Chromium
15.7
mg/kg
0.35
03/17/15 10:16
EPA 6010
Copper
8.8
mg/kg
0.35
03/17/15 10:16
REPORT OF LABORATORY ANALYSIS
D3
D3
D3
D3
D3
D3
D3
D3
D3
D3
Qualifiers
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 10 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3690Ar6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project:
Pace Project No.:
J15030202
92240158
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
92240158006
2015006523
EPA 6010
Iron
12400
mg/kg
2.8
03/17/15 10:16
EPA 6010
Magnesium
1670
mg/kg
35.0
03/17/15 10:16
EPA 6010
Manganese
104
mg/kg
0.35
03/17/15 10:16
EPA 6010
Nickel
2.5
mg/kg
0.35
03/17/15 10:16
EPA 6010
Potassium
881
mg/kg
70.1
03/17/15 10:16
EPA 6010
Sodium
35AJ
mg/kg
70.1
03/17/15 10:16
EPA 6010
Strontium
6.0
mg/kg
0.70
03/17/15 10:16
EPA 6010
Zinc
14.5
mg/kg
1.4
03/17/15 10:16
EPA 6020
Arsenic
1.2J
mg/kg
1.4
03/17/15 12:10
D3
EPA 6020
Cobalt
3.7
mg/kg
1.4
03/17/15 12:10
D3
EPA 6020
Lead
9.6
mg/kg
1.4
03/17/15 12:10
D3
EPA 6020
Vanadium
28.3
mg/kg
1.4
03/17/15 12:10
D3
EPA 7471
Mercury
0.033
mg/kg
0.011
03/17/15 13:38
ASTM D2974-87
Percent Moisture
30.6
%
0.10
03/16/15 15:31
EPA 9045
pH at 25 Degrees C
6.3
Std. Units
0.10
03/12/15 15:55
EPA 9060
Total Organic Carbon
9710
mg/kg
858
03/13/15 12:56
EPA 9060
Total Organic Carbon
7400
mg/kg
866
03/13/15 13:03
EPA 9060
Total Organic Carbon
7310
mg/kg
866
03/13/15 13:10
EPA 9060
Total Organic Carbon
11800
mg/kg
864
03/13/15 13:15
EPA 9060
Mean Total Organic Carbon
9060
mg/kg
863
03/13/15 12:56
EPA 9060
RSD%
23.8
%
03/13/15 12:56
92240158007
2015006515
EPA 6010
Aluminum
3510
mg/kg
27.1
03/17/15 14:02
D3
EPA 6010
Barium
40.9
mg/kg
2.7
03/17/15 14:02
D3
EPA 6010
Beryllium
0.35
mg/kg
0.27
03/17/15 14:02
D3
EPA 6010
Calcium
189
mg/kg
135
03/17/15 14:02
D3
EPA 6010
Copper
3.9
mg/kg
1.4
03/17/15 14:02
D3
EPA 6010
Iron
6670
mg/kg
10.8
03/17/15 14:02
D3
EPA 6010
Magnesium
1660
mg/kg
135
03/17/15 14:02
D3
EPA 6010
Manganese
393
mg/kg
1.4
03/17/15 14:02
D3
EPA 6010
Potassium
1550
mg/kg
271
03/17/15 14:02
D3
EPA 6010
Strontium
5.2
mg/kg
2.7
03/17/15 14:02
D3
EPA 6010
Zinc
31.6
mg/kg
5.4
03/17/15 14:02
D3
EPA 6020
Arsenic
1.1
mg/kg
1.1
03/17/15 12:12
D3
EPA 6020
Cadmium
0.0911
mg/kg
0.13
03/17/15 12:12
D3
EPA 6020
Cobalt
1.7
mg/kg
1.1
03/17/15 12:12
D3
EPA 6020
Lead
5.5
mg/kg
1.1
03/17/15 12:12
D3
EPA 6020
Selenium
1.2
mg/kg
1.1
03/17/15 12:12
D3
EPA 6020
Vanadium
5.9
mg/kg
1.1
03/17/15 12:12
D3
ASTM D2974-87
Percent Moisture
9.3
%
0.10
03/16/15 15:31
EPA 9045
pH at 25 Degrees C
5.9
Std. Units
0.10
03/12/15 15:55
EPA 300.0
Sulfate
3.1
mg/L
2.2
03/19/15 21:19
EPA353.2
Nitrogen, Nitrate
0.34
mg/L
0.22
03/18/1516:43
B,H1
EPA 9060
Total Organic Carbon
364J
mg/kg
662
03/13/15 13:42
EPA 9060
Total Organic Carbon
443J
mg/kg
663
03/13/15 13:48
EPA 9060
Total Organic Carbon
354J
mg/kg
662
03/13/15 13:53
EPA 9060
Total Organic Carbon
360J
mg/kg
659
03/13/15 13:59
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 11 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3Sy 91�b16fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project:
Pace Project No.:
J15030202
92240158
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed
Qualifiers
92240158007
2015006515
EPA 9060
Mean Total Organic Carbon
380J
mg/kg
661
03/13/15 13:42
EPA 9060
RSD%
11.1
%
03/13/15 13:42
92240158008
2015006516
EPA 6010
Aluminum
1480
mg/kg
5.5
03/17/15 10:25
EPA 6010
Barium
22.2
mg/kg
0.55
03/17/15 10:25
EPA 6010
Beryllium
0.50
mg/kg
0.27
03/17/15 14:06
D3
EPA 6010
Calcium
81.4
mg/kg
27.5
03/17/15 10:25
EPA 6010
Copper
43.8
mg/kg
1.4
03/17/15 14:06
D3
EPA 6010
Iron
5790
mg/kg
2.2
03/17/15 10:25
EPA 6010
Magnesium
368
mg/kg
27.5
03/17/15 10:25
EPA 6010
Manganese
195
mg/kg
1.4
03/17/15 14:06
D3
EPA 6010
Molybdenum
0.36J
mg/kg
0.55
03/17/15 10:25
EPA 6010
Potassium
111
mg/kg
54.9
03/17/15 10:25
EPA 6010
Sodium
46.7J
mg/kg
54.9
03/17/15 10:25
EPA 6010
Strontium
3.1
mg/kg
0.55
03/17/15 10:25
EPA 6010
Zinc
12.3
mg/kg
1.1
03/17/15 10:25
EPA 6020
Arsenic
1.0J
mg/kg
1.1
03/17/15 12:14
D3
EPA 6020
Cobalt
2.2
mg/kg
1.1
03/17/15 12:14
D3
EPA 6020
Lead
11.8
mg/kg
1.1
03/17/15 12:14
D3
EPA 6020
Selenium
0.87J
mg/kg
1.1
03/17/15 12:14
D3
EPA 6020
Vanadium
4.8
mg/kg
1.1
03/17/15 12:14
D3
ASTM D2974-87
Percent Moisture
9.5
%
0.10
03/16/15 15:32
EPA 9045
pH at 25 Degrees C
6.5
Std. Units
0.10
03/12/15 15:55
EPA 300.0
Sulfate
4.1
mg/L
2.2
03/19/15 21:32
EPA353.2
Nitrogen, Nitrate
0.32
mg/L
0.22
03/18/1516:44
B,H1
EPA 9060
RSD%
2.8
%
03/13/15 14:04
92240158009
2015006521
EPA 6010
Aluminum
11800
mg/kg
7.5
03/17/15 10:30
EPA 6010
Barium
51.4
mg/kg
0.75
03/17/15 10:30
EPA 6010
Beryllium
0.26
mg/kg
0.075
03/17/15 10:30
EPA 6010
Boron
12.9
mg/kg
3.8
03/17/15 10:30
EPA 6010
Calcium
208
mg/kg
37.6
03/17/15 10:30
EPA 6010
Chromium
35.6
mg/kg
0.38
03/17/15 10:30
EPA 6010
Copper
15.5
mg/kg
0.38
03/17/15 10:30
EPA 6010
Iron
18100
mg/kg
3.0
03/17/15 10:30
EPA 6010
Magnesium
4250
mg/kg
37.6
03/17/15 10:30
EPA 6010
Manganese
120
mg/kg
0.38
03/17/15 10:30
EPA 6010
Nickel
10.9
mg/kg
0.38
03/17/15 10:30
EPA 6010
Potassium
2410
mg/kg
75.2
03/17/15 10:30
EPA 6010
Sodium
40.9J
mg/kg
75.2
03/17/15 10:30
EPA 6010
Strontium
4.4
mg/kg
0.75
03/17/15 10:30
EPA 6010
Zinc
32.4
mg/kg
1.5
03/17/15 10:30
EPA 6020
Arsenic
1.6
mg/kg
1.5
03/17/15 12:16
D3
EPA 6020
Cobalt
5.2
mg/kg
1.5
03/17/15 12:16
D3
EPA 6020
Lead
8.2
mg/kg
1.5
03/17/15 12:16
D3
EPA 6020
Vanadium
38.4
mg/kg
1.5
03/17/15 12:16
D4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P36gmirpyl'y. Suite 100
Huntersville, NC 28078
[phone]
Project: J15030202
Pace Project No.: 92240158
Lab Sample ID Client Sample ID
Method Parameters
SUMMARY OF DETECTION
Result Units Report Limit Analyzed
92240158009
2015006521
ASTM D2974-87
Percent Moisture
30.3
%
0.10
03/16/15 15:33
EPA 9045
pH at 25 Degrees C
4.9
Std. Units
0.10
03/12/15 15:55
EPA 300.0
Sulfate
4.0
mg/L
2.9
03/19/15 21:46
SM 4500-CI-E
Chloride
26.1
mg/L
7.2
03/19/15 21:09
EPA 9060
Total Organic Carbon
4430
mg/kg
859
03/13/15 14:35
EPA 9060
Total Organic Carbon
2910
mg/kg
863
03/13/15 14:41
EPA 9060
Total Organic Carbon
2580
mg/kg
868
03/13/15 14:47
EPA 9060
Total Organic Carbon
2720
mg/kg
858
03/13/15 14:54
EPA 9060
Mean Total Organic Carbon
3160
mg/kg
862
03/13/15 14:35
EPA 9060
RSD%
27.1
%
03/13/15 14:35
92240158010
2015006524
EPA 6010
Aluminum
4960
mg/kg
6.4
03/17/15 10:47
EPA 6010
Barium
61.5
mg/kg
0.64
03/17/15 10:47
EPA 6010
Beryllium
0.56
mg/kg
0.32
03/17/15 14:11
EPA 6010
Calcium
270
mg/kg
31.8
03/17/15 10:47
EPA 6010
Copper
20.6
mg/kg
1.6
03/17/15 14:11
EPA 6010
Iron
8490
mg/kg
2.5
03/17/15 10:47
EPA 6010
Magnesium
2440
mg/kg
31.8
03/17/15 10:47
EPA 6010
Manganese
678
mg/kg
1.6
03/17/15 14:11
EPA 6010
Potassium
1550
mg/kg
63.6
03/17/15 10:47
EPA 6010
Sodium
40.7J
mg/kg
63.6
03/17/15 10:47
EPA 6010
Strontium
8.3
mg/kg
0.64
03/17/15 10:47
EPA 6010
Zinc
13.2
mg/kg
6.4
03/17/15 14:11
EPA 6020
Arsenic
1.2J
mg/kg
1.3
03/17/15 12:19
EPA 6020
Cobalt
8.9
mg/kg
1.3
03/17/15 12:19
EPA 6020
Lead
2.9
mg/kg
1.3
03/17/15 12:19
EPA 6020
Selenium
1.4
mg/kg
1.3
03/17/15 12:19
EPA 6020
Vanadium
17.8
mg/kg
1.3
03/17/15 12:19
ASTM D2974-87
Percent Moisture
21.6
%
0.10
03/16/15 15:33
EPA 9045
pH at 25 Degrees C
5.5
Std. Units
0.10
03/12/15 15:55
EPA 300.0
Sulfate
3.0
mg/L
2.5
03/19/15 21:59
EPA 353.2
Nitrogen, Nitrate
0.38
mg/L
0.25
03/18/15 16:49
EPA 9060
Total Organic Carbon
433J
mg/kg
768
03/13/15 14:59
EPA 9060
Mean Total Organic Carbon
385J
mg/kg
764
03/13/15 14:59
EPA 9060
RSD%
8.5
%
03/13/15 14:59
92240158011
2015006513
EPA 6020A
Aluminum
46.7
ug/L
10.0
03/13/15 20:24
EPA 6020A
Barium
4.4
ug/L
0.30
03/13/15 20:24
EPA 6020A
Calcium
160
ug/L
40.0
03/13/15 20:24
EPA 6020A
Chromium
5.9
ug/L
0.50
03/13/15 20:24
EPA 6020A
Iron
451
ug/L
50.0
03/13/15 20:24
EPA 6020A
Lead
0.28
ug/L
0.10
03/13/15 20:24
EPA 6020A
Magnesium
17.4
ug/L
10.0
03/13/15 20:24
EPA 6020A
Manganese
6.4
ug/L
0.50
03/13/15 20:24
EPA 6020A
Molybdenum
2.1
ug/L
0.50
03/13/15 20:24
EPA 6020A
Nickel
1.8
ug/L
0.50
03/13/15 20:24
REPORT OF LABORATORY ANALYSIS
D3
D3
D3
D3
D3
D3
D3
D3
D3
H1
Qualifiers
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 13 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y 91*16fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
Project: J15030202
Pace Project No.: 92240158
Lab Sample ID Client Sample ID
Method Parameters
SUMMARY OF DETECTION
Result Units Report Limit Analyzed Qualifiers
92240158011
2015006513
EPA 6020A
Strontium
1.8
ug/L
0.50
03/13/15 20:24
EPA 6020A
Zinc
34.2
ug/L
5.0
03/13/15 20:24
92240158012
2015006517
EPA 6020A
Aluminum
23.0
ug/L
10.0
03/13/15 20:29
EPA 6020A
Barium
1.1
ug/L
0.30
03/13/15 20:29
EPA 6020A
Calcium
136
ug/L
40.0
03/13/15 20:29
EPA 6020A
Chromium
1.3
ug/L
0.50
03/13/15 20:29
EPA 6020A
Iron
139
ug/L
50.0
03/13/15 20:29
EPA 6020A
Lead
0.12
ug/L
0.10
03/13/15 20:29
EPA 6020A
Magnesium
12.2
ug/L
10.0
03/13/15 20:29
EPA 6020A
Manganese
3.5
ug/L
0.50
03/13/15 20:29
EPA 6020A
Molybdenum
0.68
ug/L
0.50
03/13/15 20:29
EPA 6020A
Nickel
0.66
ug/L
0.50
03/13/15 20:29
EPA 6020A
Strontium
1.0
ug/L
0.50
03/13/15 20:29
92240158013
2015006519
EPA 6020A
Aluminum
18.8
ug/L
10.0
03/13/15 20:34
EPA 6020A
Barium
1.0
ug/L
0.30
03/13/15 20:34
EPA 6020A
Calcium
98.9
ug/L
40.0
03/13/15 20:34
EPA 6020A
Chromium
1.9
ug/L
0.50
03/13/15 20:34
EPA 6020A
Iron
173
ug/L
50.0
03/13/15 20:34
EPA 6020A
Lead
0.26
ug/L
0.10
03/13/15 20:34
EPA 6020A
Manganese
4.3
ug/L
0.50
03/13/15 20:34
EPA 6020A
Molybdenum
0.67
ug/L
0.50
03/13/15 20:34
EPA 6020A
Nickel
0.98
ug/L
0.50
03/13/15 20:34
EPA 6020A
Strontium
0.66
ug/L
0.50
03/13/15 20:34
EPA 6020A
Zinc
7.2
ug/L
5.0
03/13/15 20:34
92240158014
2015006522
EPA 6020A
Aluminum
49.3
ug/L
10.0
03/13/15 20:38
EPA 6020A
Barium
2.0
ug/L
0.30
03/13/15 20:38
EPA 6020A
Calcium
132
ug/L
40.0
03/13/15 20:38
EPA 6020A
Chromium
5.1
ug/L
0.50
03/13/15 20:38
EPA 6020A
Copper
1.1
ug/L
1.0
03/13/15 20:38
EPA 6020A
Iron
495
ug/L
50.0
03/13/15 20:38
EPA 6020A
Lead
0.36
ug/L
0.10
03/13/15 20:38
EPA 6020A
Magnesium
16.5
ug/L
10.0
03/13/15 20:38
EPA 6020A
Manganese
7.9
ug/L
0.50
03/13/15 20:38
EPA 6020A
Molybdenum
1.1
ug/L
0.50
03/13/15 20:38
EPA 6020A
Nickel
2.3
ug/L
0.50
03/13/15 20:38
EPA 6020A
Sodium
50.6
ug/L
50.0
03/13/15 20:38
EPA 6020A
Strontium
1.2
ug/L
0.50
03/13/15 20:38
EPA 6020A
Zinc
18.3
ug/L
5.0
03/13/15 20:38
92240158015
2015006525
EPA 6020A
Aluminum
180
ug/L
10.0
03/13/15 20:43
EPA 6020A
Barium
4.8
ug/L
0.30
03/13/15 20:43
EPA 6020A
Calcium
308
ug/L
40.0
03/13/15 20:43
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 14 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3Sy 91116fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
SUMMARY OF DETECTION
Project:
J15030202
Pace Project No.:
92240158
Lab Sample ID
Client Sample ID
Method
Parameters
Result
Units
Report Limit
Analyzed Qualifiers
92240158015
2015006525
EPA 6020A
Chromium
33.7
ug/L
0.50
03/13/15 20:43
EPA 6020A
Copper
4.6
ug/L
1.0
03/13/15 20:43
EPA 6020A
Iron
1360
ug/L
50.0
03/13/15 20:43
EPA 6020A
Lead
0.40
ug/L
0.10
03/13/15 20:43
EPA 6020A
Magnesium
76.3
ug/L
10.0
03/13/15 20:43
EPA 6020A
Manganese
18.7
ug/L
0.50
03/13/15 20:43
EPA 6020A
Molybdenum
4.1
ug/L
0.50
03/13/15 20:43
EPA 6020A
Nickel
4.6
ug/L
0.50
03/13/15 20:43
EPA 6020A
Potassium
109
ug/L
50.0
03/13/15 20:43
EPA 6020A
Sodium
118
ug/L
50.0
03/13/15 20:43
EPA 6020A
Strontium
2.3
ug/L
0.50
03/13/15 20:43
EPA 6020A
Vanadium
4.5
ug/L
1.0
03/13/15 20:43
EPA 6020A
Zinc
12.1
ug/L
5.0
03/13/15 20:43
92240158016
2015006515 SPLP
EPA 6020A
Aluminum
3590
ug/L
10.0
03/27/15 14:25
EPA 6020A
Arsenic
0.76
ug/L
0.50
03/27/15 14:25
EPA 6020A
Barium
34.5
ug/L
0.30
03/27/15 14:25
EPA 6020A
Beryllium
0.27
ug/L
0.20
03/27/15 14:25
EPA 6020A
Boron
9.9
ug/L
5.0
03/27/15 14:25
EPA 6020A
Calcium
966
ug/L
40.0
03/27/15 14:25
EPA 6020A
Chromium
1.7
ug/L
0.50
03/27/15 14:25
EPA 6020A
Copper
1.7
ug/L
1.0
03/27/15 14:25
EPA 6020A
Iron
1270
ug/L
50.0
03/27/15 14:25
EPA 6020A
Lead
1.1
ug/L
0.10
03/27/15 14:25
EPA 6020A
Magnesium
306
ug/L
10.0
03/27/15 14:25
EPA 6020A
Manganese
64.8
ug/L
0.50
03/27/15 14:25
EPA 6020A
Nickel
0.91
ug/L
0.50
03/27/15 14:25
EPA 6020A
Potassium
931
ug/L
50.0
03/27/15 14:25
EPA 6020A
Sodium
2920
ug/L
50.0
03/27/15 14:25
EPA 6020A
Strontium
13.6
ug/L
0.50
03/27/15 14:25
EPA 6020A
Vanadium
1.9
ug/L
1.0
03/27/15 14:25
EPA 6020A
Zinc
5.4
ug/L
5.0
03/27/15 14:25
92240158017
2015006516 SPLP
EPA 6020A
Aluminum
195
ug/L
10.0
03/27/15 14:28
EPA 6020A
Barium
1.7
ug/L
0.30
03/27/15 14:28
EPA 6020A
Boron
72.0
ug/L
5.0
03/27/15 14:28
EPA 6020A
Calcium
202
ug/L
40.0
03/27/15 14:28
EPA 6020A
Chromium
0.90
ug/L
0.50
03/27/15 14:28
EPA 6020A
Iron
73.0
ug/L
50.0
03/27/15 14:28
EPA 6020A
Magnesium
215
ug/L
10.0
03/27/15 14:28
EPA 6020A
Manganese
3.2
ug/L
0.50
03/27/15 14:28
EPA 6020A
Potassium
696
ug/L
50.0
03/27/15 14:28
EPA 6020A
Sodium
5620
ug/L
50.0
03/27/15 14:28
EPA 6020A
Strontium
1.4
ug/L
0.50
03/27/15 14:28
92240158018
2015006521 SPLP
EPA 6020A
Aluminum
132000
ug/L
250
03/27/15 14:46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 15 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
PAROAir6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
Project: J15030202
Pace Project No.: 92240158
Lab Sample ID Client Sample ID
Method Parameters
SUMMARY OF DETECTION
Result Units Report Limit Analyzed Qualifiers
92240158018
2015006521 SPLP
EPA 6020A
Arsenic
12.3
ug/L
2.5
03/27/15 14:31
EPA 6020A
Barium
377
ug/L
1.5
03/27/15 14:31
EPA 6020A
Beryllium
2.6
ug/L
1.0
03/27/15 14:31
EPA 6020A
Boron
75.8
ug/L
25.0
03/27/15 14:31
EPA 6020A
Calcium
2170
ug/L
200
03/27/15 14:31
EPA 6020A
Chromium
269
ug/L
2.5
03/27/15 14:31
EPA 6020A
Cobalt
24.3
ug/L
2.5
03/27/15 14:31
EPA 6020A
Copper
112
ug/L
5.0
03/27/15 14:31
EPA 6020A
Iron
109000
ug/L
250
03/27/15 14:31
EPA 6020A
Lead
62.1
ug/L
0.50
03/27/15 14:31
EPA 6020A
Magnesium
6500
ug/L
50.0
03/27/15 14:31
EPA 6020A
Manganese
250
ug/L
2.5
03/27/15 14:31
EPA 6020A
Molybdenum
2.7
ug/L
2.5
03/27/15 14:31
EPA 6020A
Nickel
48.6
ug/L
2.5
03/27/15 14:31
EPA 6020A
Potassium
5200
ug/L
250
03/27/15 14:31
EPA 6020A
Sodium
4560
ug/L
250
03/27/15 14:31
EPA 6020A
Strontium
38.2
ug/L
2.5
03/27/15 14:31
EPA 6020A
Thallium
0.60
ug/L
0.50
03/27/15 14:31
EPA 6020A
Vanadium
277
ug/L
5.0
03/27/15 14:31
EPA 6020A
Zinc
132
ug/L
25.0
03/27/15 14:31
92240158019
2015006524 SPLP
EPA 6020A
Aluminum
3030
ug/L
10.0
03/27/15 14:34
EPA 6020A
Barium
38.8
ug/L
0.30
03/27/15 14:34
EPA 6020A
Beryllium
0.30
ug/L
0.20
03/27/15 14:34
EPA 6020A
Boron
18.1
ug/L
5.0
03/27/15 14:34
EPA 6020A
Calcium
407
ug/L
40.0
03/27/15 14:34
EPA 6020A
Chromium
1.1
ug/L
0.50
03/27/15 14:34
EPA 6020A
Cobalt
2.5
ug/L
0.50
03/27/15 14:34
EPA 6020A
Copper
4.4
ug/L
1.0
03/27/15 14:34
EPA 6020A
Iron
3140
ug/L
50.0
03/27/15 14:34
EPA 6020A
Lead
0.69
ug/L
0.10
03/27/15 14:34
EPA 6020A
Magnesium
175
ug/L
10.0
03/27/15 14:34
EPA 6020A
Manganese
313
ug/L
0.50
03/27/15 14:34
EPA 6020A
Nickel
0.57
ug/L
0.50
03/27/15 14:34
EPA 6020A
Potassium
414
ug/L
50.0
03/27/15 14:34
EPA 6020A
Sodium
2300
ug/L
50.0
03/27/15 14:34
EPA 6020A
Strontium
12.1
ug/L
0.50
03/27/15 14:34
EPA 6020A
Vanadium
7.0
ug/L
1.0
03/27/15 14:34
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 16 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y RIAr6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 6010
Description: 6010 MET ICP
Client: Duke Energy
Date: March 30, 2015
General Information:
10 samples were analyzed for EPA 6010. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3050 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MPRP/23094
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92239540001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 1157067)
• Aluminum
• Iron
• MSD (Lab ID: 1157068)
• Aluminum
• Iron
R1: RPD value was outside control limits.
• MSD (Lab ID: 1157068)
• Aluminum
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 17 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y RGAr6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 6010
Description: 6010 MET ICP
Client: Duke Energy
Date: March 30, 2015
Analyte Comments:
QC Batch: MPRP/23094
D3: Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
•2015006511 (Lab ID:92240158001)
• Boron
• Beryllium
• Chromium
• Copper
• Manganese
•2015006514 (Lab ID:92240158003)
• Aluminum
• Boron
• Barium
• Beryllium
• Calcium
• Chromium
• Copper
• Iron
• Potassium
• Magnesium
• Manganese
• Molybdenum
• Sodium
• Nickel
• Strontium
• Zinc
•2015006515 (Lab ID:92240158007)
• Aluminum
• Boron
• Barium
• Beryllium
• Calcium
• Chromium
• Copper
• Iron
• Potassium
• Magnesium
• Manganese
• Molybdenum
• Sodium
• Nickel
• Strontium
• Zinc
•2015006516 (Lab ID:92240158008)
• Boron
• Beryllium
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 18 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y 91*r6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 6010
Description: 6010 MET ICP
Client: Duke Energy
Date: March 30, 2015
Analyte Comments:
QC Batch: MPRP/23094
DI Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
•2015006516 (Lab ID:92240158008)
• Chromium
• Copper
• Manganese
•2015006524 (Lab ID:92240158010)
• Boron
• Beryllium
• Chromium
• Copper
• Manganese
• Molybdenum
• Nickel
• Zinc
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 19 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P36RGAr6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 6020
Description: 6020 MET ICPMS
Client: Duke Energy
Date: March 30, 2015
General Information:
10 samples were analyzed for EPA 6020. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3050 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MPRP/23095
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92239540002
M6: Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
• MS (Lab ID: 1157071)
• Antimony
• Arsenic
• Cobalt
• Vanadium
• MSD (Lab ID: 1157072)
• Antimony
• Arsenic
• Vanadium
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 20 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
PW'ArwYINe. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 6020
Description: 6020 MET ICPMS
Client: Duke Energy
Date: March 30, 2015
Analyte Comments:
QC Batch: MPRP/23095
DI Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
•2015006511 (Lab ID:92240158001)
• Arsenic
• Cadmium
• Cobalt
• Lead
• Antimony
• Selenium
• Thallium
•2015006512 (Lab ID:92240158002)
• Arsenic
• Cadmium
• Cobalt
• Lead
• Antimony
• Selenium
• Thallium
• Vanadium
•2015006514 (Lab ID:92240158003)
• Arsenic
• Cadmium
• Cobalt
• Lead
• Antimony
• Selenium
• Thallium
• Vanadium
•2015006515 (Lab ID:92240158007)
• Arsenic
• Cadmium
• Cobalt
• Lead
• Antimony
• Selenium
• Thallium
• Vanadium
•2015006516 (Lab ID:92240158008)
• Arsenic
• Cadmium
• Cobalt
• Lead
• Antimony
• Selenium
• Thallium
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 21 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y 9041bir6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 6020
Description: 6020 MET ICPMS
Client: Duke Energy
Date: March 30, 2015
Analyte Comments:
QC Batch: MPRP/23095
DI Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
•2015006516 (Lab ID:92240158008)
• Vanadium
•2015006518 (Lab ID:92240158004)
• Arsenic
• Cadmium
• Cobalt
• Lead
• Antimony
• Selenium
• Thallium
• Vanadium
•2015006520 (Lab ID:92240158005)
• Arsenic
• Cadmium
• Cobalt
• Lead
• Antimony
• Selenium
• Thallium
• Vanadium
•2015006521 (Lab ID:92240158009)
• Arsenic
• Cadmium
• Cobalt
• Lead
• Antimony
• Selenium
• Thallium
•2015006523 (Lab ID:92240158006)
• Arsenic
• Cadmium
• Cobalt
• Lead
• Antimony
• Selenium
• Thallium
• Vanadium
•2015006524 (Lab ID:92240158010)
• Arsenic
• Cadmium
• Cobalt
• Lead
• Antimony
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 22 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y 904ffiir6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 6020
Description: 6020 MET ICPMS
Client: Duke Energy
Date: March 30, 2015
Analyte Comments:
QC Batch: MPRP/23095
DI Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
•2015006524 (Lab ID:92240158010)
• Selenium
• Thallium
• Vanadium
• MS (Lab ID: 1157071)
• Arsenic
• Cadmium
• Cobalt
• Lead
• Antimony
• Selenium
• Thallium
• MSD (Lab ID: 1157072)
• Arsenic
• Cadmium
• Cobalt
• Lead
• Antimony
• Selenium
• Thallium
D4: Sample was diluted due to the presence of high levels of target analytes.
•2015006511 (Lab ID:92240158001)
• Vanadium
•2015006521 (Lab ID:92240158009)
• Vanadium
• MS (Lab ID: 1157071)
• Vanadium
• MSD (Lab ID: 1157072)
• Vanadium
N2: The lab does not hold TNI accreditation for this parameter.
•2015006511 (Lab ID:92240158001)
• Antimony
•2015006512 (Lab ID:92240158002)
• Antimony
•2015006514 (Lab ID:92240158003)
• Antimony
•2015006515 (Lab ID:92240158007)
• Antimony
•2015006516 (Lab ID:92240158008)
• Antimony
•2015006518 (Lab ID:92240158004)
• Antimony
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 23 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P36904K WeY IN e. Suite100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 6020
Description: 6020 MET ICPMS
Client: Duke Energy
Date: March 30, 2015
Analyte Comments:
QC Batch: MPRP/23095
N2: The lab does not hold TNI accreditation for this parameter.
•2015006520 (Lab ID:92240158005)
• Antimony
•2015006521 (Lab ID:92240158009)
• Antimony
•2015006523 (Lab ID:92240158006)
• Antimony
•2015006524 (Lab ID:92240158010)
• Antimony
• BLANK (Lab ID: 1157069)
• Antimony
• LCS (Lab ID: 1157070)
• Antimony
• MS (Lab ID: 1157071)
• Antimony
• MSD (Lab ID: 1157072)
• Antimony
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 24 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P36904WeYINie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 6020A
Description: 6020A MET ICPMS
Client: Duke Energy
Date: March 30, 2015
General Information:
9 samples were analyzed for EPA 6020A. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3020 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MPRP/52931
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92240320006
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 1917522)
• Aluminum
• Calcium
• Sodium
• MSD (Lab ID: 1917523)
• Aluminum
QC Batch: MPRP/53205
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92242374012
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 1926431)
• Aluminum
• MSD (Lab ID: 1926432)
• Aluminum
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 25 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y 904r6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 6020A
Description: 6020A MET ICPMS
Client: Duke Energy
Date: March 30, 2015
QC Batch: MPRP/53205
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92242374012
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• Iron
R1: RPD value was outside control limits.
• MSD (Lab ID: 1926432)
• Aluminum
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 26 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P369041jWeYINie. Suite100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 7470
Description: 7470 Mercury
Client: Duke Energy
Date: March 30, 2015
General Information:
9 samples were analyzed for EPA 7470. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 7470 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MERP/13071
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92242374012
R1: RPD value was outside control limits.
• MSD (Lab ID: 1926033)
• Mercury
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 27 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3690AWleY.Nie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 7471
Description: 7471 Mercury
Client: Duke Energy
Date: March 30, 2015
General Information:
10 samples were analyzed for EPA 7471. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 7471 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MERP/5474
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92239540004
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 1157679)
• Mercury
• MSD (Lab ID: 1157680)
• Mercury
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 28 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3690*WeYINie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 9045
Description: 9045 pH Soil
Client: Duke Energy
Date: March 30, 2015
General Information:
10 samples were analyzed for EPA 9045. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 29 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3690AWeYINie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 300.0
Description: 300.0 IC Anions, SPLP
Client: Duke Energy
Date: March 30, 2015
General Information:
4 samples were analyzed for EPA 300.0. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 30 of 94

aceAnaiXical
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[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 353.2
Description: 353.2 Nitrogen, NO2/NO3, SPLP
Client: Duke Energy
Date: March 30, 2015
General Information:
4 samples were analyzed for EPA 353.2. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
1-11: Analysis conducted outside the EPA method holding time.
•2015006515 (Lab ID:92240158007)
•2015006516 (Lab ID:92240158008)
•2015006521 (Lab ID:92240158009)
•2015006524 (Lab ID:92240158010)
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
QC Batch: WETA/22256
B: Analyte was detected in the associated method blank.
• BLANK for HBN 256042 [WETA/222 (Lab ID: 1413768)
• Nitrogen, Nitrate
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 31 of 94

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PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: SM 4500-CI-E
Description: 4500 Chloride, SPLP
Client: Duke Energy
Date: March 30, 2015
General Information:
4 samples were analyzed for SM 4500-CI-E. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 32 of 94

aceAnaiXical
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Pace Analytical Services, Inc.
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[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 9056
Description: 9056 IC Anions
Client: Duke Energy
Date: March 30, 2015
General Information:
10 samples were analyzed for EPA 9056. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: WETA/44508
DI Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
•2015006511 (Lab ID:92240158001)
• Chloride
• Sulfate
•2015006512 (Lab ID:92240158002)
• Chloride
• Sulfate
•2015006514 (Lab ID:92240158003)
• Chloride
• Sulfate
•2015006518 (Lab ID:92240158004)
• Chloride
• Sulfate
QC Batch: WETA/44515
DI Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
•2015006521 (Lab ID:92240158009)
• Chloride
• Sulfate
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 33 of 94

aceAnaiXical
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Pace Analytical Services, Inc.
P3y S�05kf�ir6fY.Nie. Suite 100
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[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 9056
Description: 9056 IC Anions
Client: Duke Energy
Date: March 30, 2015
Analyte Comments:
QC Batch: WETA/44515
DI Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
•2015006524 (Lab ID:92240158010)
• Chloride
• Sulfate
QC Batch: WETA/44533
DI Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
•2015006515 (Lab ID:92240158007)
• Chloride
• Sulfate
•2015006516 (Lab ID:92240158008)
• Chloride
• Sulfate
•2015006520 (Lab ID:92240158005)
• Chloride
• Sulfate
•2015006523 (Lab ID:92240158006)
• Chloride
• Sulfate
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 34 of 94

aceAnaiXical
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Pace Analytical Services, Inc.
P3y SMr6fY.Nie. Suite 100
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[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 9056
Description: 9056 IC Anions 48hr
Client: Duke Energy
Date: March 30, 2015
General Information:
10 samples were analyzed for EPA 9056. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
1­13: Sample was received or analysis requested beyond the recognized method holding time.
•2015006511 (Lab ID:92240158001)
•2015006512 (Lab ID:92240158002)
•2015006514 (Lab ID:92240158003)
•2015006515 (Lab ID:92240158007)
•2015006516 (Lab ID:92240158008)
•2015006518 (Lab ID:92240158004)
•2015006520 (Lab ID:92240158005)
•2015006521 (Lab ID:92240158009)
•2015006523 (Lab ID:92240158006)
•2015006524 (Lab ID:92240158010)
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: WETA/44509
DI Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
•2015006511 (Lab ID:92240158001)
• Nitrate as N
•2015006512 (Lab ID:92240158002)
• Nitrate as N
•2015006514 (Lab ID:92240158003)
• Nitrate as N
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 35 of 94

aceAnaiXical
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Pace Analytical Services, Inc.
P3y M,r6fY.Nie. Suite 100
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[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 9056
Description: 9056 IC Anions 48hr
Client: Duke Energy
Date: March 30, 2015
Analyte Comments:
QC Batch: WETA/44509
DI Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
•2015006518 (Lab ID:92240158004)
• Nitrate as N
QC Batch: WETA/44514
DI Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
•2015006521 (Lab ID:92240158009)
• Nitrate as N
•2015006524 (Lab ID:92240158010)
• Nitrate as N
QC Batch: WETA/44534
D3: Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
•2015006515 (Lab ID:92240158007)
• Nitrate as N
•2015006516 (Lab ID:92240158008)
• Nitrate as N
•2015006520 (Lab ID:92240158005)
• Nitrate as N
•2015006523 (Lab ID:92240158006)
• Nitrate as N
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 36 of 94

aceAnaiXical
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Pace Analytical Services, Inc.
P3y 90Ar6fY.Nie. Suite 100
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[phone]
PROJECT NARRATIVE
Project: J15030202
Pace Project No.: 92240158
Method: EPA 9060
Description: Total Organic Carbon Quad
Client: Duke Energy
Date: March 30, 2015
General Information:
10 samples were analyzed for EPA 9060. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 37 of 94

aceAnaiXical
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Pace Analytical Services, Inc.
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[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006511
Lab ID:
92240158001 Collected:
03/03/15 15:24
Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical
Method: EPA 6010
Preparation
Method: EPA
3050
Aluminum
10200
mg/kg
8.0
4.0
1
03/16/15 12:27
03/17/15 09:54
7429-90-5
Barium
65.7
mg/kg
0.80
0.40
1
03/16/15 12:27
03/17/15 09:54
7440-39-3
Beryllium
0.52
mg/kg
0.40
0.20
5
03/16/15 12:27
03/17/1513:53
7440-41-7
D3
Boron
16.3J
mg/kg
19.9
10
5
03/16/15 12:27
03/17/1513:53
7440-42-8
D3
Calcium
227
mg/kg
39.9
19.9
1
03/16/15 12:27
03/17/15 09:54
7440-70-2
Chromium
12.9
mg/kg
2.0
1.0
5
03/16/15 12:27
03/17/1513:53
7440-47-3
D3
Copper
22.8
mg/kg
2.0
1.0
5
03/16/15 12:27
03/17/1513:53
7440-50-8
D3
Iron
18300
mg/kg
3.2
1.6
1
03/16/15 12:27
03/17/15 09:54
7439-89-6
Magnesium
2420
mg/kg
39.9
19.9
1
03/16/15 12:27
03/17/15 09:54
7439-95-4
Manganese
365
mg/kg
2.0
1.0
5
03/16/15 12:27
03/17/1513:53
7439-96-5
D3
Molybdenum
ND
mg/kg
0.80
0.40
1
03/16/15 12:27
03/17/15 09:54
7439-98-7
Nickel
1.7
mg/kg
0.40
0.20
1
03/16/15 12:27
03/17/15 09:54
7440-02-0
Potassium
2020
mg/kg
79.8
39.9
1
03/16/15 12:27
03/17/15 09:54
7440-09-7
Sodium
ND
mg/kg
79.8
39.9
1
03/16/15 12:27
03/17/15 09:54
7440-23-5
Strontium
4.3
mg/kg
0.80
0.40
1
03/16/15 12:27
03/17/15 09:54
7440-24-6
Zinc
27.3
mg/kg
1.6
0.80
1
03/16/15 12:27
03/17/15 09:54
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020
Preparation
Method: EPA
3050
Antimony
ND
mg/kg
1.6
0.80
20
03/16/15 12:27
03/17/1511:51
7440-36-0
D3,N2
Arsenic
1.9
mg/kg
1.6
0.80
20
03/16/15 12:27
03/17/1511:51
7440-38-2
D3
Cadmium
0.13J
mg/kg
0.19
0.096
20
03/16/15 12:27
03/17/1511:51
7440-43-9
D3
Cobalt
6.4
mg/kg
1.6
0.80
20
03/16/15 12:27
03/17/1511:51
7440-48-4
D3
Lead
7.5
mg/kg
1.6
0.80
20
03/16/15 12:27
03/17/1511:51
7439-92-1
D3
Selenium
1.3J
mg/kg
1.6
0.80
20
03/16/15 12:27
03/17/1511:51
7782-49-2
D3
Thallium
ND
mg/kg
1.6
0.80
20
03/16/15 12:27
03/17/1511:51
7440-28-0
D3
Vanadium
44.8
mg/kg
1.6
0.80
20
03/16/15 12:27
03/17/1511:51
7440-62-2
D4
7471 Mercury
Analytical
Method: EPA 7471
Preparation
Method: EPA
7471
Mercury
0.020
mg/kg 0.012
0.0060
1
03/17/15 06:13
03/17/15 13:27
7439-97-6
Percent Moisture
Analytical
Method: ASTM D2974-87
Percent Moisture
35.5
%
0.10
0.10
1
03/16/15 15:26
9045 pH Soil
Analytical
Method: EPA 9045
pH at 25 Degrees C
5.3
Std. Units
0.10
0.10
1
03/12/15 15:55
9056 IC Anions
Analytical
Method: EPA 9056
Chloride
ND
mg/kg
392
196
5
03/13/1516:38
16887-00-6
D3
Sulfate
ND
mg/kg
392
196
5
03/13/1516:38
14808-79-8
D3
9056 IC Anions 48hr
Analytical
Method: EPA 9056
Nitrate as N
ND
mg/kg
39.2
19.6
5
03/13/15 16:38
14797-55-8
D3,H3
Date: 03/30/2015 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 38 of 94

aceAnaiXical
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Pace Analytical Services, Inc.
P3y 90*r6fY.Nie. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006511
Lab ID:
92240158001
Collected:
03/03/15 15:24
Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
Total Organic Carbon Quad
Analytical
Method: EPA 9060
Total Organic Carbon
3450
mg/kg
928
464
1
03/13/15 10:12
7440-44-0
Total Organic Carbon
3640
mg/kg
929
465
1
03/13/15 10:17
7440-44-0
Total Organic Carbon
3880
mg/kg
922
461
1
03/13/15 10:23
7440-44-0
Total Organic Carbon
4020
mg/kg
935
467
1
03/13/15 10:29
7440-44-0
Mean Total Organic Carbon
3750
mg/kg
929
464
1
03/13/15 10:12
7440-44-0
Surrogates
RSD%
6.7
%
1
03/13/15 10:12
Date: 03/30/2015 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 39 of 94

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Pace Analytical Services, Inc.
P3y 90Ar6fY.Nie. Suite 100
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[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006512
Lab ID:
92240158002
Collected:
03/03/15 15:52
Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical
Method: EPA 6010
Preparation
Method: EPA
3050
Aluminum
5930
mg/kg
6.1
3.1
1
03/16/15 12:27
03/17/15 09:59
7429-90-5
Barium
31.3
mg/kg
0.61
0.31
1
03/16/15 12:27
03/17/15 09:59
7440-39-3
Beryllium
0.39
mg/kg
0.061
0.031
1
03/16/15 12:27
03/17/15 09:59
7440-41-7
Boron
7.8
mg/kg
3.1
1.5
1
03/16/15 12:27
03/17/15 09:59
7440-42-8
Calcium
22.2J
mg/kg
30.7
15.4
1
03/16/15 12:27
03/17/15 09:59
7440-70-2
Chromium
10.8
mg/kg
0.31
0.15
1
03/16/15 12:27
03/17/15 09:59
7440-47-3
Copper
5.5
mg/kg
0.31
0.15
1
03/16/15 12:27
03/17/15 09:59
7440-50-8
Iron
10300
mg/kg
2.5
1.2
1
03/16/15 12:27
03/17/15 09:59
7439-89-6
Magnesium
1070
mg/kg
30.7
15.4
1
03/16/15 12:27
03/17/15 09:59
7439-95-4
Manganese
69.4
mg/kg
0.31
0.15
1
03/16/15 12:27
03/17/15 09:59
7439-96-5
Molybdenum
0.89
mg/kg
0.61
0.31
1
03/16/15 12:27
03/17/15 09:59
7439-98-7
Nickel
0.91
mg/kg
0.31
0.15
1
03/16/15 12:27
03/17/15 09:59
7440-02-0
Potassium
800
mg/kg
61.5
30.7
1
03/16/15 12:27
03/17/15 09:59
7440-09-7
Sodium
30.9J
mg/kg
61.5
30.7
1
03/16/15 12:27
03/17/15 09:59
7440-23-5
Strontium
1.1
mg/kg
0.61
0.31
1
03/16/15 12:27
03/17/15 09:59
7440-24-6
Zinc
14.9
mg/kg
1.2
0.61
1
03/16/15 12:27
03/17/15 09:59
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020
Preparation
Method: EPA
3050
Antimony
ND
mg/kg
1.2
0.61
20
03/16/15 12:27
03/17/1511:53
7440-36-0
D3,N2
Arsenic
1.5
mg/kg
1.2
0.61
20
03/16/15 12:27
03/17/1511:53
7440-38-2
D3
Cadmium
ND
mg/kg
0.15
0.074
20
03/16/15 12:27
03/17/1511:53
7440-43-9
D3
Cobalt
1.6
mg/kg
1.2
0.61
20
03/16/15 12:27
03/17/1511:53
7440-48-4
D3
Lead
4.8
mg/kg
1.2
0.61
20
03/16/15 12:27
03/17/1511:53
7439-92-1
D3
Selenium
0.85J
mg/kg
1.2
0.61
20
03/16/15 12:27
03/17/1511:53
7782-49-2
D3
Thallium
ND
mg/kg
1.2
0.61
20
03/16/15 12:27
03/17/1511:53
7440-28-0
D3
Vanadium
23.8
mg/kg
1.2
0.61
20
03/16/15 12:27
03/17/1511:53
7440-62-2
D3
7471 Mercury
Analytical
Method: EPA 7471 Preparation
Method: EPA
7471
Mercury
ND
mg/kg
0.0096
0.0048
1
03/17/15 06:13
03/17/15 13:29
7439-97-6
Percent Moisture
Analytical
Method: ASTM
D2974-87
Percent Moisture
19.2
%
0.10
0.10
1
03/16/15 15:27
9045 pH Soil
Analytical
Method: EPA 9045
pH at 25 Degrees C
6.0
Std. Units
0.10
0.10
1
03/12/15 15:55
9056 IC Anions
Analytical
Method: EPA 9056
Chloride
ND
mg/kg
309
155
5
03/13/1517:00
16887-00-6
D3
Sulfate
ND
mg/kg
309
155
5
03/13/1517:00
14808-79-8
D3
9056 IC Anions 48hr
Analytical
Method: EPA 9056
Nitrate as N
ND
mg/kg
30.9
15.5
5
03/13/15 17:00
14797-55-8
D3,H3
Date: 03/30/2015 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 40 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3Sy Mr6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006512
Lab ID:
92240158002
Collected:
03/03/15 15:52
Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
Total Organic Carbon Quad
Analytical
Method: EPA 9060
Total Organic Carbon
ND
mg/kg
749
375
1
03/13/15 11:25
7440-44-0
Total Organic Carbon
386J
mg/kg
743
371
1
03/13/15 11:32
7440-44-0
Total Organic Carbon
387J
mg/kg
747
373
1
03/13/15 11:38
7440-44-0
Total Organic Carbon
ND
mg/kg
748
374
1
03/13/15 11:44
7440-44-0
Mean Total Organic Carbon
ND
mg/kg
747
373
1
03/13/15 11:25
7440-44-0
Surrogates
RSD%
5.2
%
1
03/13/15 11:25
Date: 03/30/2015 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 41 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y 9%18ir6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006514
Lab ID:
92240158003 Collected:
03/04/15 10:15
Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical
Method: EPA 6010
Preparation
Method: EPA
3050
Aluminum
5320
mg/kg
34.0
17.0
5
03/16/1512:27
03/17/1513:58
7429-90-5
D3
Barium
47.1
mg/kg
3.4
1.7
5
03/16/1512:27
03/17/1513:58
7440-39-3
D3
Beryllium
0.36
mg/kg
0.34
0.17
5
03/16/1512:27
03/17/1513:58
7440-41-7
D3
Boron
ND
mg/kg
17.0
8.5
5
03/16/1512:27
03/17/1513:58
7440-42-8
D3
Calcium
313
mg/kg
170
85.1
5
03/16/1512:27
03/17/1513:58
7440-70-2
D3
Chromium
ND
mg/kg
1.7
0.85
5
03/16/1512:27
03/17/1513:58
7440-47-3
D3
Copper
11.1
mg/kg
1.7
0.85
5
03/16/1512:27
03/17/1513:58
7440-50-8
D3
Iron
8280
mg/kg
13.6
6.8
5
03/16/1512:27
03/17/1513:58
7439-89-6
D3
Magnesium
1940
mg/kg
170
85.1
5
03/16/1512:27
03/17/1513:58
7439-95-4
D3
Manganese
406
mg/kg
1.7
0.85
5
03/16/1512:27
03/17/1513:58
7439-96-5
D3
Molybdenum
ND
mg/kg
3.4
1.7
5
03/16/1512:27
03/17/1513:58
7439-98-7
D3
Nickel
ND
mg/kg
1.7
0.85
5
03/16/1512:27
03/17/1513:58
7440-02-0
D3
Potassium
1730
mg/kg
340
170
5
03/16/1512:27
03/17/1513:58
7440-09-7
D3
Sodium
ND
mg/kg
340
170
5
03/16/1512:27
03/17/1513:58
7440-23-5
D3
Strontium
4.2
mg/kg
3.4
1.7
5
03/16/1512:27
03/17/1513:58
7440-24-6
D3
Zinc
36.3
mg/kg
6.8
3.4
5
03/16/1512:27
03/17/1513:58
7440-66-6
D3
6020 MET ICPMS
Analytical
Method: EPA 6020
Preparation
Method: EPA
3050
Antimony
ND
mg/kg
1.4
0.68
20
03/16/1512:27
03/17/1511:56
7440-36-0
D3,N2
Arsenic
1.8
mg/kg
1.4
0.68
20
03/16/1512:27
03/17/1511:56
7440-38-2
D3
Cadmium
0.12J
mg/kg
0.16
0.082
20
03/16/1512:27
03/17/1511:56
7440-43-9
D3
Cobalt
2.8
mg/kg
1.4
0.68
20
03/16/1512:27
03/17/1511:56
7440-48-4
D3
Lead
5.4
mg/kg
1.4
0.68
20
03/16/1512:27
03/17/1511:56
7439-92-1
D3
Selenium
1.9
mg/kg
1.4
0.68
20
03/16/1512:27
03/17/1511:56
7782-49-2
D3
Thallium
ND
mg/kg
1.4
0.68
20
03/16/1512:27
03/17/1511:56
7440-28-0
D3
Vanadium
6.8
mg/kg
1.4
0.68
20
03/16/1512:27
03/17/1511:56
7440-62-2
D3
7471 Mercury
Analytical
Method: EPA 7471
Preparation
Method: EPA
7471
Mercury
ND
mg/kg
0.011
0.0054
1
03/17/15 06:13
03/17/15 13:31
7439-97-6
Percent Moisture
Analytical
Method: ASTM D2974-87
Percent Moisture
26.5
%
0.10
0.10
1
03/16/15 15:29
9045 pH Soil
Analytical
Method: EPA 9045
pH at 25 Degrees C
6.0
Std. Units
0.10
0.10
1
03/12/15 15:55
9056 IC Anions
Analytical
Method: EPA 9056
Chloride
ND
mg/kg
346
173
5
03/13/1517:22
16887-00-6
D3
Sulfate
ND
mg/kg
346
173
5
03/13/1517:22
14808-79-8
D3
9056 IC Anions 48hr
Analytical
Method: EPA 9056
Nitrate as N
ND
mg/kg
34.6
17.3
5
03/13/15 17:22
14797-55-8
D3,H3
Date: 03/30/2015 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 42 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P36R%-)ir6fyJ,y. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006514
Lab ID:
92240158003
Collected:
03/04/15 10:15
Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
Total Organic Carbon Quad
Analytical
Method: EPA 9060
Total Organic Carbon
503J
mg/kg
816
408
1
03/13/15 11:49
7440-44-0
Total Organic Carbon
573J
mg/kg
813
406
1
03/13/15 11:55
7440-44-0
Total Organic Carbon
484J
mg/kg
823
412
1
03/13/15 12:01
7440-44-0
Total Organic Carbon
445J
mg/kg
819
410
1
03/13/15 12:06
7440-44-0
Mean Total Organic Carbon
502J
mg/kg
818
409
1
03/13/15 11:49
7440-44-0
Surrogates
RSD%
10.6
%
1
03/13/15 11:49
Date: 03/30/2015 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 43 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3Sy 9%1J ir6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006518
Lab ID:
92240158004
Collected:
03/04/15 13:10
Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical
Method: EPA 6010
Preparation
Method: EPA
3050
Aluminum
2510
mg/kg
6.4
3.2
1
03/16/1512:27
03/17/1510:07
7429-90-5
Barium
54.8
mg/kg
0.64
0.32
1
03/16/1512:27
03/17/1510:07
7440-39-3
Beryllium
0.17
mg/kg
0.064
0.032
1
03/16/1512:27
03/17/1510:07
7440-41-7
Boron
2.9J
mg/kg
3.2
1.6
1
03/16/1512:27
03/17/1510:07
7440-42-8
Calcium
ND
mg/kg
32.1
16.1
1
03/16/1512:27
03/17/1510:07
7440-70-2
Chromium
0.74
mg/kg
0.32
0.16
1
03/16/1512:27
03/17/1510:07
7440-47-3
Copper
13.1
mg/kg
0.32
0.16
1
03/16/1512:27
03/17/1510:07
7440-50-8
Iron
3920
mg/kg
2.6
1.3
1
03/16/1512:27
03/17/1510:07
7439-89-6
Magnesium
816
mg/kg
32.1
16.1
1
03/16/1512:27
03/17/1510:07
7439-95-4
Manganese
192
mg/kg
0.32
0.16
1
03/16/1512:27
03/17/1510:07
7439-96-5
Molybdenum
ND
mg/kg
0.64
0.32
1
03/16/1512:27
03/17/1510:07
7439-98-7
Nickel
0.55
mg/kg
0.32
0.16
1
03/16/1512:27
03/17/1510:07
7440-02-0
Potassium
801
mg/kg
64.2
32.1
1
03/16/1512:27
03/17/1510:07
7440-09-7
Sodium
67.2
mg/kg
64.2
32.1
1
03/16/1512:27
03/17/1510:07
7440-23-5
Strontium
4.1
mg/kg
0.64
0.32
1
03/16/1512:27
03/17/1510:07
7440-24-6
Zinc
14.7
mg/kg
1.3
0.64
1
03/16/1512:27
03/17/1510:07
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020
Preparation
Method: EPA
3050
Antimony
ND
mg/kg
1.3
0.63
20
03/16/1512:27
03/17/1512:05
7440-36-0
D3,N2
Arsenic
1.2J
mg/kg
1.3
0.63
20
03/16/1512:27
03/17/1512:05
7440-38-2
D3
Cadmium
ND
mg/kg
0.15
0.075
20
03/16/1512:27
03/17/1512:05
7440-43-9
D3
Cobalt
2.5
mg/kg
1.3
0.63
20
03/16/1512:27
03/17/1512:05
7440-48-4
D3
Lead
4.2
mg/kg
1.3
0.63
20
03/16/1512:27
03/17/1512:05
7439-92-1
D3
Selenium
0.901
mg/kg
1.3
0.63
20
03/16/1512:27
03/17/1512:05
7782-49-2
D3
Thallium
ND
mg/kg
1.3
0.63
20
03/16/1512:27
03/17/1512:05
7440-28-0
D3
Vanadium
2.7
mg/kg
1.3
0.63
20
03/16/1512:27
03/17/1512:05
7440-62-2
D3
7471 Mercury
Analytical
Method: EPA 7471 Preparation
Method: EPA
7471
Mercury
ND
mg/kg
0.0093
0.0046
1
03/17/15 06:13
03/17/15 13:33
7439-97-6
Percent Moisture
Analytical
Method: ASTM
D2974-87
Percent Moisture
20.3
%
0.10
0.10
1
03/16/15 15:29
9045 pH Soil
Analytical
Method: EPA 9045
pH at 25 Degrees C
5.9
Std. Units
0.10
0.10
1
03/12/15 15:55
9056 IC Anions
Analytical
Method: EPA 9056
Chloride
ND
mg/kg
309
154
5
03/13/1517:44
16887-00-6
D3
Sulfate
ND
mg/kg
309
154
5
03/13/1517:44
14808-79-8
D3
9056 IC Anions 48hr
Analytical
Method: EPA 9056
Nitrate as N
ND
mg/kg
30.9
15.4
5
03/13/15 17:44
14797-55-8
D3,H3
Date: 03/30/2015 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 44 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y SHISr6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006518
Lab ID:
92240158004
Collected:
03/04/15 13:10
Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
Total Organic Carbon Quad
Analytical
Method: EPA 9060
Total Organic Carbon
ND
mg/kg
756
378
1
03/13/15 12:11
7440-44-0
Total Organic Carbon
ND
mg/kg
758
379
1
03/13/15 12:17
7440-44-0
Total Organic Carbon
ND
mg/kg
748
374
1
03/13/15 12:23
7440-44-0
Total Organic Carbon
ND
mg/kg
753
377
1
03/13/15 12:29
7440-44-0
Mean Total Organic Carbon
ND
mg/kg
754
377
1
03/13/15 12:11
7440-44-0
Surrogates
RSD%
4.7
%
1
03/13/15 12:11
Date: 03/30/2015 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 45 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y 9%16 1ir6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006520
Lab ID:
92240158005
Collected:
03/04/15 14:47
Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical
Method: EPA 6010
Preparation
Method: EPA
3050
Aluminum
5030
mg/kg
5.3
2.6
1
03/16/1512:27
03/17/1510:12
7429-90-5
Barium
55.2
mg/kg
0.53
0.26
1
03/16/1512:27
03/17/1510:12
7440-39-3
Beryllium
0.15
mg/kg
0.053
0.026
1
03/16/1512:27
03/17/1510:12
7440-41-7
Boron
5.7
mg/kg
2.6
1.3
1
03/16/1512:27
03/17/1510:12
7440-42-8
Calcium
1420
mg/kg
26.4
13.2
1
03/16/1512:27
03/17/1510:12
7440-70-2
Chromium
20.7
mg/kg
0.26
0.13
1
03/16/1512:27
03/17/1510:12
7440-47-3
Copper
14.0
mg/kg
0.26
0.13
1
03/16/1512:27
03/17/1510:12
7440-50-8
Iron
8070
mg/kg
2.1
1.1
1
03/16/1512:27
03/17/1510:12
7439-89-6
Magnesium
3810
mg/kg
26.4
13.2
1
03/16/1512:27
03/17/1510:12
7439-95-4
Manganese
348
mg/kg
0.26
0.13
1
03/16/1512:27
03/17/1510:12
7439-96-5
Molybdenum
1.1
mg/kg
0.53
0.26
1
03/16/1512:27
03/17/1510:12
7439-98-7
Nickel
7.7
mg/kg
0.26
0.13
1
03/16/1512:27
03/17/1510:12
7440-02-0
Potassium
2950
mg/kg
52.7
26.4
1
03/16/1512:27
03/17/1510:12
7440-09-7
Sodium
104
mg/kg
52.7
26.4
1
03/16/1512:27
03/17/1510:12
7440-23-5
Strontium
11.0
mg/kg
0.53
0.26
1
03/16/1512:27
03/17/1510:12
7440-24-6
Zinc
30.8
mg/kg
1.1
0.53
1
03/16/1512:27
03/17/1510:12
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020
Preparation
Method: EPA
3050
Antimony
ND
mg/kg
1.1
0.53
20
03/16/1512:27
03/17/1512:07
7440-36-0
D3,N2
Arsenic
0.64J
mg/kg
1.1
0.53
20
03/16/1512:27
03/17/1512:07
7440-38-2
D3
Cadmium
0.094J
mg/kg
0.13
0.063
20
03/16/1512:27
03/17/1512:07
7440-43-9
D3
Cobalt
4.9
mg/kg
1.1
0.53
20
03/16/1512:27
03/17/1512:07
7440-48-4
D3
Lead
2.4
mg/kg
1.1
0.53
20
03/16/1512:27
03/17/1512:07
7439-92-1
D3
Selenium
ND
mg/kg
1.1
0.53
20
03/16/1512:27
03/17/1512:07
7782-49-2
D3
Thallium
ND
mg/kg
1.1
0.53
20
03/16/1512:27
03/17/1512:07
7440-28-0
D3
Vanadium
15.0
mg/kg
1.1
0.53
20
03/16/1512:27
03/17/1512:07
7440-62-2
D3
7471 Mercury
Analytical
Method: EPA 7471 Preparation
Method: EPA
7471
Mercury
0.0096
mg/kg
0.0087
0.0044
1
03/17/15 06:13
03/17/15 13:36
7439-97-6
Percent Moisture
Analytical
Method: ASTM
D2974-87
Percent Moisture
8.5
%
0.10
0.10
1
03/16/15 15:30
9045 pH Soil
Analytical
Method: EPA 9045
pH at 25 Degrees C
8.6
Std. Units
0.10
0.10
1
03/12/15 15:55
9056 IC Anions
Analytical
Method: EPA 9056
Chloride
ND
mg/kg
272
136
5
03/14/1519:08
16887-00-6
D3
Sulfate
ND
mg/kg
272
136
5
03/14/1519:08
14808-79-8
D3
9056 IC Anions 48hr
Analytical
Method: EPA 9056
Nitrate as N
ND
mg/kg
27.2
13.6
5
03/14/15 19:08
14797-55-8
D3,H3
Date: 03/30/2015 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 46 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
PAR&WYINie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006520
Lab ID:
92240158005
Collected:
03/04/15 14:47
Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
Total Organic Carbon Quad
Analytical
Method: EPA 9060
Total Organic Carbon
ND
mg/kg
660
330
1
03/13/15 12:35
7440-44-0
Total Organic Carbon
ND
mg/kg
651
325
1
03/13/15 12:40
7440-44-0
Total Organic Carbon
ND
mg/kg
659
330
1
03/13/15 12:46
7440-44-0
Total Organic Carbon
ND
mg/kg
656
328
1
03/13/15 12:51
7440-44-0
Mean Total Organic Carbon
ND
mg/kg
657
328
1
03/13/15 12:35
7440-44-0
Surrogates
RSD%
5.0
%
1
03/13/15 12:35
Date: 03/30/2015 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 47 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3Sy 9Wr6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006523
Lab ID:
92240158006 Collected:
03/04/15 16:25
Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical
Method: EPA 6010
Preparation
Method: EPA
3050
Aluminum
7030
mg/kg
7.0
3.5
1
03/16/1512:27
03/17/1510:16
7429-90-5
Barium
49.6
mg/kg
0.70
0.35
1
03/16/1512:27
03/17/1510:16
7440-39-3
Beryllium
0.24
mg/kg 0.070
0.035
1
03/16/1512:27
03/17/1510:16
7440-41-7
Boron
9.6
mg/kg
3.5
1.8
1
03/16/1512:27
03/17/1510:16
7440-42-8
Calcium
655
mg/kg
35.0
17.5
1
03/16/1512:27
03/17/1510:16
7440-70-2
Chromium
15.7
mg/kg
0.35
0.18
1
03/16/1512:27
03/17/1510:16
7440-47-3
Copper
8.8
mg/kg
0.35
0.18
1
03/16/1512:27
03/17/1510:16
7440-50-8
Iron
12400
mg/kg
2.8
1.4
1
03/16/1512:27
03/17/1510:16
7439-89-6
Magnesium
1670
mg/kg
35.0
17.5
1
03/16/1512:27
03/17/1510:16
7439-95-4
Manganese
104
mg/kg
0.35
0.18
1
03/16/1512:27
03/17/1510:16
7439-96-5
Molybdenum
ND
mg/kg
0.70
0.35
1
03/16/1512:27
03/17/1510:16
7439-98-7
Nickel
2.5
mg/kg
0.35
0.18
1
03/16/1512:27
03/17/1510:16
7440-02-0
Potassium
881
mg/kg
70.1
35.0
1
03/16/1512:27
03/17/1510:16
7440-09-7
Sodium
35AJ
mg/kg
70.1
35.0
1
03/16/1512:27
03/17/1510:16
7440-23-5
Strontium
6.0
mg/kg
0.70
0.35
1
03/16/1512:27
03/17/1510:16
7440-24-6
Zinc
14.5
mg/kg
1.4
0.70
1
03/16/1512:27
03/17/1510:16
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020
Preparation
Method: EPA
3050
Antimony
ND
mg/kg
1.4
0.70
20
03/16/1512:27
03/17/1512:10
7440-36-0
D3,N2
Arsenic
1.2J
mg/kg
1.4
0.70
20
03/16/1512:27
03/17/1512:10
7440-38-2
D3
Cadmium
ND
mg/kg
0.17
0.084
20
03/16/1512:27
03/17/1512:10
7440-43-9
D3
Cobalt
3.7
mg/kg
1.4
0.70
20
03/16/1512:27
03/17/1512:10
7440-48-4
D3
Lead
9.6
mg/kg
1.4
0.70
20
03/16/1512:27
03/17/1512:10
7439-92-1
D3
Selenium
ND
mg/kg
1.4
0.70
20
03/16/1512:27
03/17/1512:10
7782-49-2
D3
Thallium
ND
mg/kg
1.4
0.70
20
03/16/1512:27
03/17/1512:10
7440-28-0
D3
Vanadium
28.3
mg/kg
1.4
0.70
20
03/16/1512:27
03/17/1512:10
7440-62-2
D3
7471 Mercury
Analytical
Method: EPA 7471
Preparation
Method: EPA
7471
Mercury
0.033
mg/kg
0.011
0.0057
1
03/17/15 06:13
03/17/15 13:38
7439-97-6
Percent Moisture
Analytical
Method: ASTM D2974-87
Percent Moisture
30.6
%
0.10
0.10
1
03/16/15 15:31
9045 pH Soil
Analytical
Method: EPA 9045
pH at 25 Degrees C
6.3
Std. Units
0.10
0.10
1
03/12/15 15:55
9056 IC Anions
Analytical
Method: EPA 9056
Chloride
ND
mg/kg
362
181
5
03/14/15 20:12
16887-00-6
D3
Sulfate
ND
mg/kg
362
181
5
03/14/15 20:12
14808-79-8
D3
9056 IC Anions 48hr
Analytical
Method: EPA 9056
Nitrate as N
ND
mg/kg
36.2
18.1
5
03/14/15 20:12
14797-55-8
D3,H3
Date: 03/30/2015 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 48 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3Sy 9%1?r6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006523
Lab ID:
92240158006
Collected:
03/04/15 16:25
Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
Total Organic Carbon Quad
Analytical
Method: EPA 9060
Total Organic Carbon
9710
mg/kg
858
429
1
03/13/15 12:56
7440-44-0
Total Organic Carbon
7400
mg/kg
866
433
1
03/13/15 13:03
7440-44-0
Total Organic Carbon
7310
mg/kg
866
433
1
03/13/15 13:10
7440-44-0
Total Organic Carbon
11800
mg/kg
864
432
1
03/13/15 13:15
7440-44-0
Mean Total Organic Carbon
9060
mg/kg
863
432
1
03/13/15 12:56
7440-44-0
Surrogates
RSD%
23.8
%
1
03/13/15 12:56
Date: 03/30/2015 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 49 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y 9%16 ir6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006515
Lab ID:
92240158007
Collected:
03/04/15
10:25
Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA
3050
Aluminum
3510
mg/kg
27.1
13.5
5
03/16/1512:27
03/17/1514:02
7429-90-5
D3
Barium
40.9
mg/kg
2.7
1.4
5
03/16/1512:27
03/17/1514:02
7440-39-3
D3
Beryllium
0.35
mg/kg
0.27
0.14
5
03/16/1512:27
03/17/1514:02
7440-41-7
D3
Boron
ND
mg/kg
13.5
6.8
5
03/16/1512:27
03/17/1514:02
7440-42-8
D3
Calcium
189
mg/kg
135
67.7
5
03/16/1512:27
03/17/1514:02
7440-70-2
D3
Chromium
ND
mg/kg
1.4
0.68
5
03/16/1512:27
03/17/1514:02
7440-47-3
D3
Copper
3.9
mg/kg
1.4
0.68
5
03/16/1512:27
03/17/1514:02
7440-50-8
D3
Iron
6670
mg/kg
10.8
5.4
5
03/16/1512:27
03/17/1514:02
7439-89-6
D3
Magnesium
1660
mg/kg
135
67.7
5
03/16/1512:27
03/17/1514:02
7439-95-4
D3
Manganese
393
mg/kg
1.4
0.68
5
03/16/1512:27
03/17/1514:02
7439-96-5
D3
Molybdenum
ND
mg/kg
2.7
1.4
5
03/16/1512:27
03/17/1514:02
7439-98-7
D3
Nickel
ND
mg/kg
1.4
0.68
5
03/16/1512:27
03/17/1514:02
7440-02-0
D3
Potassium
1550
mg/kg
271
135
5
03/16/1512:27
03/17/1514:02
7440-09-7
D3
Sodium
ND
mg/kg
271
135
5
03/16/1512:27
03/17/1514:02
7440-23-5
D3
Strontium
5.2
mg/kg
2.7
1.4
5
03/16/1512:27
03/17/1514:02
7440-24-6
D3
Zinc
31.6
mg/kg
5.4
2.7
5
03/16/1512:27
03/17/1514:02
7440-66-6
D3
6020 MET ICPMS
Analytical
Method: EPA 6020
Preparation
Method: EPA
3050
Antimony
ND
mg/kg
1.1
0.54
20
03/16/1512:27
03/17/1512:12
7440-36-0
D3,N2
Arsenic
1.1
mg/kg
1.1
0.54
20
03/16/1512:27
03/17/1512:12
7440-38-2
D3
Cadmium
0.0911
mg/kg
0.13
0.065
20
03/16/1512:27
03/17/1512:12
7440-43-9
D3
Cobalt
1.7
mg/kg
1.1
0.54
20
03/16/1512:27
03/17/1512:12
7440-48-4
D3
Lead
5.5
mg/kg
1.1
0.54
20
03/16/1512:27
03/17/1512:12
7439-92-1
D3
Selenium
1.2
mg/kg
1.1
0.54
20
03/16/1512:27
03/17/1512:12
7782-49-2
D3
Thallium
ND
mg/kg
1.1
0.54
20
03/16/1512:27
03/17/1512:12
7440-28-0
D3
Vanadium
5.9
mg/kg
1.1
0.54
20
03/16/1512:27
03/17/1512:12
7440-62-2
D3
7471 Mercury
Analytical
Method: EPA 7471 Preparation
Method: EPA
7471
Mercury
ND
mg/kg
0.0086
0.0043
1
03/17/15 06:13
03/17/15 13:40
7439-97-6
Percent Moisture
Analytical
Method: ASTM
D2974-87
Percent Moisture
9.3
%
0.10
0.10
1
03/16/15 15:31
9045 pH Soil
Analytical
Method: EPA 9045
pH at 25 Degrees C
5.9
Std. Units
0.10
0.10
1
03/12/15 15:55
300.0 IC Anions, SPLP
Analytical
Method: EPA 300.0
Leachate
Method/Date:
EPA 1312; 03/16/15
14:15
Sulfate
3.1
mg/L
2.2
1.1
1
03/19/15 21:19
14808-79-8
353.2 Nitrogen, NO2/NO3, SPLP
Analytical
Method: EPA 353.2
Leachate
Method/Date:
EPA 1312; 03/16/15
14:15
Nitrogen, Nitrate
0.34
mg/L
0.22
0.22
1
03/18/15 16:43
B,H1
4500 Chloride, SPLP
Analytical
Method: SM 4500-CI-E Leachate
Method/Date: EPA 1312; 03/16/15 14:15
Chloride
ND
mg/L
5.5
2.8
1
03/19/15 21:08
16887-00-6
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM
without the written
consent of Pace Analytical Services, Inc..
Page
50 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P369%6rw Y IN e. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006515 Lab ID: 92240158007 Collected: 03/04/15 10:25 Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
9056 IC Anions Analytical Method: EPA 9056
Chloride
ND mg/kg
271
135
5
03/14/15 20:34
16887-00-6 D3
Sulfate
ND mg/kg
271
135
5
03/14/15 20:34
14808-79-8 D3
9056 IC Anions 48hr
Analytical Method: EPA 9056
Nitrate as N
ND mg/kg
27.1
13.5
5
03/14/15 20:34
14797-55-8 D3,1-13
Total Organic Carbon Quad
Analytical Method: EPA 9060
Total Organic Carbon
364J mg/kg
662
331
1
03/13/15 13:42
7440-44-0
Total Organic Carbon
443J mg/kg
663
332
1
03/13/15 13:48
7440-44-0
Total Organic Carbon
354J mg/kg
662
331
1
03/13/15 13:53
7440-44-0
Total Organic Carbon
360J mg/kg
659
330
1
03/13/15 13:59
7440-44-0
Mean Total Organic Carbon
380J mg/kg
661
331
1
03/13/15 13:42
7440-44-0
Surrogates
RSD%
11.1 %
1
03/13/15 13:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc..
Page 51 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3690/t816fY.Ne. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006516
Lab ID:
92240158008
Collected:
03/04/15
11:10
Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3050
Aluminum
1480
mg/kg
5.5
2.7
1
03/16/1512:27
03/17/1510:25
7429-90-5
Barium
22.2
mg/kg
0.55
0.27
1
03/16/1512:27
03/17/1510:25
7440-39-3
Beryllium
0.50
mg/kg
0.27
0.14
5
03/16/1512:27
03/17/1514:06
7440-41-7
D3
Boron
ND
mg/kg
13.7
6.9
5
03/16/1512:27
03/17/1514:06
7440-42-8
D3
Calcium
81.4
mg/kg
27.5
13.7
1
03/16/1512:27
03/17/1510:25
7440-70-2
Chromium
ND
mg/kg
1.4
0.69
5
03/16/1512:27
03/17/1514:06
7440-47-3
D3
Copper
43.8
mg/kg
1.4
0.69
5
03/16/1512:27
03/17/1514:06
7440-50-8
D3
Iron
5790
mg/kg
2.2
1.1
1
03/16/1512:27
03/17/1510:25
7439-89-6
Magnesium
368
mg/kg
27.5
13.7
1
03/16/1512:27
03/17/1510:25
7439-95-4
Manganese
195
mg/kg
1.4
0.69
5
03/16/1512:27
03/17/1514:06
7439-96-5
D3
Molybdenum
0.36J
mg/kg
0.55
0.27
1
03/16/1512:27
03/17/1510:25
7439-98-7
Nickel
ND
mg/kg
0.27
0.14
1
03/16/1512:27
03/17/1510:25
7440-02-0
Potassium
111
mg/kg
54.9
27.5
1
03/16/1512:27
03/17/1510:25
7440-09-7
Sodium
46.7J
mg/kg
54.9
27.5
1
03/16/1512:27
03/17/1510:25
7440-23-5
Strontium
3.1
mg/kg
0.55
0.27
1
03/16/1512:27
03/17/1510:25
7440-24-6
Zinc
12.3
mg/kg
1.1
0.55
1
03/16/1512:27
03/17/1510:25
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020
Preparation
Method: EPA 3050
Antimony
ND
mg/kg
1.1
0.55
20
03/16/1512:27
03/17/1512:14
7440-36-0
D3,N2
Arsenic
1.0J
mg/kg
1.1
0.55
20
03/16/1512:27
03/17/1512:14
7440-38-2
D3
Cadmium
ND
mg/kg
0.13
0.066
20
03/16/1512:27
03/17/1512:14
7440-43-9
D3
Cobalt
2.2
mg/kg
1.1
0.55
20
03/16/1512:27
03/17/1512:14
7440-48-4
D3
Lead
11.8
mg/kg
1.1
0.55
20
03/16/1512:27
03/17/1512:14
7439-92-1
D3
Selenium
0.87J
mg/kg
1.1
0.55
20
03/16/1512:27
03/17/1512:14
7782-49-2
D3
Thallium
ND
mg/kg
1.1
0.55
20
03/16/1512:27
03/17/1512:14
7440-28-0
D3
Vanadium
4.8
mg/kg
1.1
0.55
20
03/16/1512:27
03/17/1512:14
7440-62-2
D3
7471 Mercury
Analytical
Method: EPA 7471 Preparation
Method: EPA 7471
Mercury
ND
mg/kg
0.0093
0.0046
1
03/17/15 06:13
03/17/15 13:42
7439-97-6
Percent Moisture
Analytical
Method: ASTM
D2974-87
Percent Moisture
9.5
%
0.10
0.10
1
03/16/15 15:32
9045 pH Soil
Analytical
Method: EPA 9045
pH at 25 Degrees C
6.5
Std. Units
0.10
0.10
1
03/12/15 15:55
300.0 IC Anions, SPLP
Analytical
Method: EPA 300.0
Leachate
Method/Date:
EPA 1312; 03/16/15
14:15
Sulfate
4.1
mg/L
2.2
1.1
1
03/19/15 21:32
14808-79-8
353.2 Nitrogen, NO2/NO3, SPLP
Analytical
Method: EPA 353.2
Leachate
Method/Date:
EPA 1312; 03/16/15
14:15
Nitrogen, Nitrate
0.32
mg/L
0.22
0.22
1
03/18/15 16:44
B,H1
4500 Chloride, SPLP
Analytical
Method: SM 4500-CI-E Leachate
Method/Date:
EPA 1312; 03/16/15 14:15
Chloride
ND
mg/L
5.5
2.8
1
03/19/15 21:09
16887-00-6
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in
full,
Date: 03/30/2015 02:56 PM
without the written
consent of Pace Analytical Services, Inc..
Page
52 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
PgRoAirpyl,y. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006516 Lab ID: 92240158008 Collected: 03/04/15 11:10 Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
9056 IC Anions Analytical Method: EPA 9056
Chloride
ND mg/kg
272
136
5
03/14/15 20:55
16887-00-6 D3
Sulfate
ND mg/kg
272
136
5
03/14/15 20:55
14808-79-8 D3
9056 IC Anions 48hr
Analytical Method: EPA 9056
Nitrate as N
ND mg/kg
27.2
13.6
5
03/14/15 20:55
14797-55-8 D3,1-13
Total Organic Carbon Quad
Analytical Method: EPA 9060
Total Organic Carbon
ND mg/kg
664
332
1
03/13/15 14:04
7440-44-0
Total Organic Carbon
ND mg/kg
667
333
1
03/13/15 14:17
7440-44-0
Total Organic Carbon
ND mg/kg
662
331
1
03/13/15 14:22
7440-44-0
Total Organic Carbon
ND mg/kg
663
332
1
03/13/15 14:29
7440-44-0
Mean Total Organic Carbon
ND mg/kg
664
332
1
03/13/15 14:04
7440-44-0
Surrogates
RSD%
2.8 %
1
03/13/15 14:04
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc..
Page 53 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
PARO&WYINie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006521
Lab ID:
92240158009
Collected:
03/04/15
15:05
Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA
3050
Aluminum
11800
mg/kg
7.5
3.8
1
03/16/1512:27
03/17/1510:30
7429-90-5
Barium
51.4
mg/kg
0.75
0.38
1
03/16/1512:27
03/17/1510:30
7440-39-3
Beryllium
0.26
mg/kg
0.075
0.038
1
03/16/1512:27
03/17/1510:30
7440-41-7
Boron
12.9
mg/kg
3.8
1.9
1
03/16/1512:27
03/17/1510:30
7440-42-8
Calcium
208
mg/kg
37.6
18.8
1
03/16/1512:27
03/17/1510:30
7440-70-2
Chromium
35.6
mg/kg
0.38
0.19
1
03/16/1512:27
03/17/1510:30
7440-47-3
Copper
15.5
mg/kg
0.38
0.19
1
03/16/1512:27
03/17/1510:30
7440-50-8
Iron
18100
mg/kg
3.0
1.5
1
03/16/1512:27
03/17/1510:30
7439-89-6
Magnesium
4250
mg/kg
37.6
18.8
1
03/16/1512:27
03/17/1510:30
7439-95-4
Manganese
120
mg/kg
0.38
0.19
1
03/16/1512:27
03/17/1510:30
7439-96-5
Molybdenum
ND
mg/kg
0.75
0.38
1
03/16/1512:27
03/17/1510:30
7439-98-7
Nickel
10.9
mg/kg
0.38
0.19
1
03/16/1512:27
03/17/1510:30
7440-02-0
Potassium
2410
mg/kg
75.2
37.6
1
03/16/1512:27
03/17/1510:30
7440-09-7
Sodium
40.9J
mg/kg
75.2
37.6
1
03/16/1512:27
03/17/1510:30
7440-23-5
Strontium
4.4
mg/kg
0.75
0.38
1
03/16/1512:27
03/17/1510:30
7440-24-6
Zinc
32.4
mg/kg
1.5
0.75
1
03/16/1512:27
03/17/1510:30
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020
Preparation
Method: EPA
3050
Antimony
ND
mg/kg
1.5
0.75
20
03/16/1512:27
03/17/1512:16
7440-36-0
D3,N2
Arsenic
1.6
mg/kg
1.5
0.75
20
03/16/1512:27
03/17/1512:16
7440-38-2
D3
Cadmium
ND
mg/kg
0.18
0.090
20
03/16/1512:27
03/17/1512:16
7440-43-9
D3
Cobalt
5.2
mg/kg
1.5
0.75
20
03/16/1512:27
03/17/1512:16
7440-48-4
D3
Lead
8.2
mg/kg
1.5
0.75
20
03/16/1512:27
03/17/1512:16
7439-92-1
D3
Selenium
ND
mg/kg
1.5
0.75
20
03/16/1512:27
03/17/1512:16
7782-49-2
D3
Thallium
ND
mg/kg
1.5
0.75
20
03/16/1512:27
03/17/1512:16
7440-28-0
D3
Vanadium
38.4
mg/kg
1.5
0.75
20
03/16/1512:27
03/17/1512:16
7440-62-2
D4
7471 Mercury
Analytical
Method: EPA 7471 Preparation
Method: EPA
7471
Mercury
ND
mg/kg
0.012
0.0059
1
03/17/15 06:13
03/17/15 13:44
7439-97-6
Percent Moisture
Analytical
Method: ASTM
D2974-87
Percent Moisture
30.3
%
0.10
0.10
1
03/16/15 15:33
9045 pH Soil
Analytical
Method: EPA 9045
pH at 25 Degrees C
4.9
Std. Units
0.10
0.10
1
03/12/15 15:55
300.0 IC Anions, SPLP
Analytical
Method: EPA 300.0
Leachate
Method/Date:
EPA 1312; 03/16/15
14:15
Sulfate
4.0
mg/L
2.9
1.4
1
03/19/15 21:46
14808-79-8
353.2 Nitrogen, NO2/NO3, SPLP
Analytical
Method: EPA 353.2
Leachate
Method/Date:
EPA 1312; 03/16/15
14:15
Nitrogen, Nitrate
ND
mg/L
0.29
0.29
1
03/18/15 16:48
H1
4500 Chloride, SPLP
Analytical
Method: SM 4500-CI-E Leachate
Method/Date: EPA 1312; 03/16/15 14:15
Chloride
26.1
mg/L
7.2
3.6
1
03/19/15 21:09
16887-00-6
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM
without the written
consent of Pace Analytical Services, Inc..
Page
54 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3690 3irwYINe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006521 Lab ID: 92240158009 Collected: 03/04/15 15:05 Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
9056 IC Anions Analytical Method: EPA 9056
Chloride
ND mg/kg
360
180
5
03/13/1516:23
16887-00-6 D3
Sulfate
ND mg/kg
360
180
5
03/13/1516:23
14808-79-8 D3
9056 IC Anions 48hr
Analytical Method: EPA 9056
Nitrate as N
ND mg/kg
36.0
18.0
5
03/13/15 16:23
14797-55-8 D3,1-13
Total Organic Carbon Quad
Analytical Method: EPA 9060
Total Organic Carbon
4430 mg/kg
859
429
1
03/13/15 14:35
7440-44-0
Total Organic Carbon
2910 mg/kg
863
431
1
03/13/15 14:41
7440-44-0
Total Organic Carbon
2580 mg/kg
868
434
1
03/13/15 14:47
7440-44-0
Total Organic Carbon
2720 mg/kg
858
429
1
03/13/15 14:54
7440-44-0
Mean Total Organic Carbon
3160 mg/kg
862
431
1
03/13/15 14:35
7440-44-0
Surrogates
RSD%
27.1 %
1
03/13/15 14:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc..
Page 55 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P36907 WYINe. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006524
Lab ID:
92240158010
Collected:
03/04/15
16:45
Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA
3050
Aluminum
4960
mg/kg
6.4
3.2
1
03/16/1512:27
03/17/1510:47
7429-90-5
Barium
61.5
mg/kg
0.64
0.32
1
03/16/1512:27
03/17/1510:47
7440-39-3
Beryllium
0.56
mg/kg
0.32
0.16
5
03/16/1512:27
03/17/1514:11
7440-41-7
D3
Boron
ND
mg/kg
15.9
7.9
5
03/16/1512:27
03/17/1514:11
7440-42-8
D3
Calcium
270
mg/kg
31.8
15.9
1
03/16/1512:27
03/17/1510:47
7440-70-2
Chromium
ND
mg/kg
1.6
0.79
5
03/16/1512:27
03/17/1514:11
7440-47-3
D3
Copper
20.6
mg/kg
1.6
0.79
5
03/16/1512:27
03/17/1514:11
7440-50-8
D3
Iron
8490
mg/kg
2.5
1.3
1
03/16/1512:27
03/17/1510:47
7439-89-6
Magnesium
2440
mg/kg
31.8
15.9
1
03/16/1512:27
03/17/1510:47
7439-95-4
Manganese
678
mg/kg
1.6
0.79
5
03/16/1512:27
03/17/1514:11
7439-96-5
D3
Molybdenum
ND
mg/kg
3.2
1.6
5
03/16/1512:27
03/17/1514:11
7439-98-7
D3
Nickel
ND
mg/kg
1.6
0.79
5
03/16/1512:27
03/17/1514:11
7440-02-0
D3
Potassium
1550
mg/kg
63.6
31.8
1
03/16/1512:27
03/17/1510:47
7440-09-7
Sodium
40.7J
mg/kg
63.6
31.8
1
03/16/1512:27
03/17/1510:47
7440-23-5
Strontium
8.3
mg/kg
0.64
0.32
1
03/16/1512:27
03/17/1510:47
7440-24-6
Zinc
13.2
mg/kg
6.4
3.2
5
03/16/1512:27
03/17/1514:11
7440-66-6
D3
6020 MET ICPMS
Analytical
Method: EPA 6020
Preparation
Method: EPA
3050
Antimony
ND
mg/kg
1.3
0.64
20
03/16/1512:27
03/17/1512:19
7440-36-0
D3,N2
Arsenic
1.2J
mg/kg
1.3
0.64
20
03/16/1512:27
03/17/1512:19
7440-38-2
D3
Cadmium
ND
mg/kg
0.15
0.076
20
03/16/1512:27
03/17/1512:19
7440-43-9
D3
Cobalt
8.9
mg/kg
1.3
0.64
20
03/16/1512:27
03/17/1512:19
7440-48-4
D3
Lead
2.9
mg/kg
1.3
0.64
20
03/16/1512:27
03/17/1512:19
7439-92-1
D3
Selenium
1.4
mg/kg
1.3
0.64
20
03/16/1512:27
03/17/1512:19
7782-49-2
D3
Thallium
ND
mg/kg
1.3
0.64
20
03/16/1512:27
03/17/1512:19
7440-28-0
D3
Vanadium
17.8
mg/kg
1.3
0.64
20
03/16/1512:27
03/17/1512:19
7440-62-2
D3
7471 Mercury
Analytical
Method: EPA 7471 Preparation
Method: EPA
7471
Mercury
ND
mg/kg
0.010
0.0051
1
03/17/15 06:13
03/17/15 13:51
7439-97-6
Percent Moisture
Analytical
Method: ASTM
D2974-87
Percent Moisture
21.6
%
0.10
0.10
1
03/16/15 15:33
9045 pH Soil
Analytical
Method: EPA 9045
pH at 25 Degrees C
5.5
Std. Units
0.10
0.10
1
03/12/15 15:55
300.0 IC Anions, SPLP
Analytical
Method: EPA 300.0
Leachate
Method/Date:
EPA 1312; 03/16/15
14:15
Sulfate
3.0
mg/L
2.5
1.3
1
03/19/15 21:59
14808-79-8
353.2 Nitrogen, NO2/NO3, SPLP
Analytical
Method: EPA 353.2
Leachate
Method/Date:
EPA 1312; 03/16/15
14:15
Nitrogen, Nitrate
0.38
mg/L
0.25
0.25
1
03/18/15 16:49
H1
4500 Chloride, SPLP
Analytical
Method: SM 4500-CI-E Leachate
Method/Date: EPA 1312; 03/16/15 14:15
Chloride
ND
mg/L
6.4
3.2
1
03/19/15 21:10
16887-00-6
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM
without the written
consent of Pace Analytical Services, Inc..
Page
56 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y 90816fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006524 Lab ID: 92240158010 Collected: 03/04/15 16:45 Received: 03/06/15 14:15 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
9056 IC Anions Analytical Method: EPA 9056
Chloride
ND mg/kg
312
156
5
03/13/1517:27
16887-00-6 D3
Sulfate
ND mg/kg
312
156
5
03/13/1517:27
14808-79-8 D3
9056 IC Anions 48hr
Analytical Method: EPA 9056
Nitrate as N
ND mg/kg
31.2
15.6
5
03/13/15 17:27
14797-55-8 D3,1-13
Total Organic Carbon Quad
Analytical Method: EPA 9060
Total Organic Carbon
433J mg/kg
768
384
1
03/13/15 14:59
7440-44-0
Total Organic Carbon
ND mg/kg
761
381
1
03/13/15 15:05
7440-44-0
Total Organic Carbon
ND mg/kg
768
384
1
03/13/15 15:10
7440-44-0
Total Organic Carbon
ND mg/kg
759
380
1
03/13/15 15:16
7440-44-0
Mean Total Organic Carbon
385J mg/kg
764
382
1
03/13/15 14:59
7440-44-0
Surrogates
RSD%
8.5 %
1
03/13/15 14:59
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc..
Page 57 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P36
Rom r6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006513 Lab ID: 92240158011 Collected: 03/03/15 15:58 Received: 03/06/15 14:15 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
;I➢ZI7c\ri,I=11a 99�r6?
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Sodium
Strontium
Thallium
Vanadium
Zinc
7470 Mercury
Mercury
Date: 03/30/2015 02:56 PM
Analytical Method: EPA 6020A Preparation Method: EPA 3020
46.7
ug/L
10.0
1.2
1
03/13/15 13:04
03/13/15 20:24
7429-90-5
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:24
7440-36-0
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:24
7440-38-2
4.4
ug/L
0.30
0.14
1
03/13/15 13:04
03/13/15 20:24
7440-39-3
ND
ug/L
0.20
0.066
1
03/13/15 13:04
03/13/15 20:24
7440-41-7
ND
ug/L
5.0
1.0
1
03/13/15 13:04
03/13/15 20:24
7440-42-8
ND
ug/L
0.080
0.033
1
03/13/15 13:04
03/13/15 20:24
7440-43-9
160
ug/L
40.0
8.4
1
03/13/15 13:04
03/13/15 20:24
7440-70-2
5.9
ug/L
0.50
0.22
1
03/13/15 13:04
03/13/15 20:24
7440-47-3
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:24
7440-48-4
ND
ug/L
1.0
0.22
1
03/13/15 13:04
03/13/15 20:24
7440-50-8
451
ug/L
50.0
8.0
1
03/13/15 13:04
03/13/15 20:24
7439-89-6
0.28
ug/L
0.10
0.046
1
03/13/15 13:04
03/13/15 20:24
7439-92-1
17.4
ug/L
10.0
2.8
1
03/13/15 13:04
03/13/15 20:24
7439-95-4
6.4
ug/L
0.50
0.14
1
03/13/15 13:04
03/13/15 20:24
7439-96-5
2.1
ug/L
0.50
0.24
1
03/13/15 13:04
03/13/15 20:24
7439-98-7
1.8
ug/L
0.50
0.23
1
03/13/15 13:04
03/13/15 20:24
7440-02-0
ND
ug/L
50.0
8.3
1
03/13/15 13:04
03/13/15 20:24
7440-09-7
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:24
7782-49-2
ND
ug/L
50.0
18.2
1
03/13/15 13:04
03/13/15 20:24
7440-23-5
1.8
ug/L
0.50
0.057
1
03/13/15 13:04
03/13/15 20:24
7440-24-6
ND
ug/L
0.10
0.025
1
03/13/15 13:04
03/13/15 20:24
7440-28-0
ND
ug/L
1.0
0.21
1
03/13/15 13:04
03/13/15 20:24
7440-62-2
34.2
ug/L
5.0
2.5
1
03/13/15 13:04
03/13/15 20:24
7440-66-6
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L 0.20 0.026 1 03/15/1514:30 03/16/1511:04 7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 58 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P36
Ron 16fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006517 Lab ID: 92240158012 Collected: 03/04/15 10:02 Received: 03/06/15 14:15 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
;I➢ZI7c\�i,I=11a 99�r6?
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Sodium
Strontium
Thallium
Vanadium
Zinc
7470 Mercury
Mercury
Date: 03/30/2015 02:56 PM
Analytical Method: EPA 6020A Preparation Method: EPA 3020
23.0
ug/L
10.0
1.2
1
03/13/15 13:04
03/13/15 20:29
7429-90-5
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:29
7440-36-0
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:29
7440-38-2
1.1
ug/L
0.30
0.14
1
03/13/15 13:04
03/13/15 20:29
7440-39-3
ND
ug/L
0.20
0.066
1
03/13/15 13:04
03/13/15 20:29
7440-41-7
ND
ug/L
5.0
1.0
1
03/13/15 13:04
03/13/15 20:29
7440-42-8
ND
ug/L
0.080
0.033
1
03/13/15 13:04
03/13/15 20:29
7440-43-9
136
ug/L
40.0
8.4
1
03/13/15 13:04
03/13/15 20:29
7440-70-2
1.3
ug/L
0.50
0.22
1
03/13/15 13:04
03/13/15 20:29
7440-47-3
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:29
7440-48-4
ND
ug/L
1.0
0.22
1
03/13/15 13:04
03/13/15 20:29
7440-50-8
139
ug/L
50.0
8.0
1
03/13/15 13:04
03/13/15 20:29
7439-89-6
0.12
ug/L
0.10
0.046
1
03/13/15 13:04
03/13/15 20:29
7439-92-1
12.2
ug/L
10.0
2.8
1
03/13/15 13:04
03/13/15 20:29
7439-95-4
3.5
ug/L
0.50
0.14
1
03/13/15 13:04
03/13/15 20:29
7439-96-5
0.68
ug/L
0.50
0.24
1
03/13/15 13:04
03/13/15 20:29
7439-98-7
0.66
ug/L
0.50
0.23
1
03/13/15 13:04
03/13/15 20:29
7440-02-0
ND
ug/L
50.0
8.3
1
03/13/15 13:04
03/13/15 20:29
7440-09-7
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:29
7782-49-2
ND
ug/L
50.0
18.2
1
03/13/15 13:04
03/13/15 20:29
7440-23-5
1.0
ug/L
0.50
0.057
1
03/13/15 13:04
03/13/15 20:29
7440-24-6
ND
ug/L
0.10
0.025
1
03/13/15 13:04
03/13/15 20:29
7440-28-0
ND
ug/L
1.0
0.21
1
03/13/15 13:04
03/13/15 20:29
7440-62-2
ND
ug/L
5.0
2.5
1
03/13/15 13:04
03/13/15 20:29
7440-66-6
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L 0.20 0.026 1 03/15/1514:30 03/16/1511:06 7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 59 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P36
Rom r6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006519 Lab ID: 92240158013 Collected: 03/04/15 12:39 Received: 03/06/15 14:15 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
;I➢ZI7c\ri,I=11 l[99�r 6?
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Sodium
Strontium
Thallium
Vanadium
Zinc
7470 Mercury
Mercury
Date: 03/30/2015 02:56 PM
Analytical Method: EPA 6020A Preparation Method: EPA 3020
18.8
ug/L
10.0
1.2
1
03/13/15 13:04
03/13/15 20:34
7429-90-5
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:34
7440-36-0
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:34
7440-38-2
1.0
ug/L
0.30
0.14
1
03/13/15 13:04
03/13/15 20:34
7440-39-3
ND
ug/L
0.20
0.066
1
03/13/15 13:04
03/13/15 20:34
7440-41-7
ND
ug/L
5.0
1.0
1
03/13/15 13:04
03/13/15 20:34
7440-42-8
ND
ug/L
0.080
0.033
1
03/13/15 13:04
03/13/15 20:34
7440-43-9
98.9
ug/L
40.0
8.4
1
03/13/15 13:04
03/13/15 20:34
7440-70-2
1.9
ug/L
0.50
0.22
1
03/13/15 13:04
03/13/15 20:34
7440-47-3
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:34
7440-48-4
ND
ug/L
1.0
0.22
1
03/13/15 13:04
03/13/15 20:34
7440-50-8
173
ug/L
50.0
8.0
1
03/13/15 13:04
03/13/15 20:34
7439-89-6
0.26
ug/L
0.10
0.046
1
03/13/15 13:04
03/13/15 20:34
7439-92-1
ND
ug/L
10.0
2.8
1
03/13/15 13:04
03/13/15 20:34
7439-95-4
4.3
ug/L
0.50
0.14
1
03/13/15 13:04
03/13/15 20:34
7439-96-5
0.67
ug/L
0.50
0.24
1
03/13/15 13:04
03/13/15 20:34
7439-98-7
0.98
ug/L
0.50
0.23
1
03/13/15 13:04
03/13/15 20:34
7440-02-0
ND
ug/L
50.0
8.3
1
03/13/15 13:04
03/13/15 20:34
7440-09-7
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:34
7782-49-2
ND
ug/L
50.0
18.2
1
03/13/15 13:04
03/13/15 20:34
7440-23-5
0.66
ug/L
0.50
0.057
1
03/13/15 13:04
03/13/15 20:34
7440-24-6
ND
ug/L
0.10
0.025
1
03/13/15 13:04
03/13/15 20:34
7440-28-0
ND
ug/L
1.0
0.21
1
03/13/15 13:04
03/13/15 20:34
7440-62-2
7.2
ug/L
5.0
2.5
1
03/13/15 13:04
03/13/15 20:34
7440-66-6
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L 0.20 0.026 1 03/15/1514:30 03/16/1511:09 7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 60 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3690hrw Y IN e. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006522 Lab ID: 92240158014 Collected: 03/04/15 14:16 Received: 03/06/15 14:15 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
;I➢ZI7c\ri,I=11 l[99�r 6?
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Sodium
Strontium
Thallium
Vanadium
Zinc
7470 Mercury
Mercury
Date: 03/30/2015 02:56 PM
Analytical Method: EPA 6020A Preparation Method: EPA 3020
49.3
ug/L
10.0
1.2
1
03/13/15 13:04
03/13/15 20:38
7429-90-5
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:38
7440-36-0
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:38
7440-38-2
2.0
ug/L
0.30
0.14
1
03/13/15 13:04
03/13/15 20:38
7440-39-3
ND
ug/L
0.20
0.066
1
03/13/15 13:04
03/13/15 20:38
7440-41-7
ND
ug/L
5.0
1.0
1
03/13/15 13:04
03/13/15 20:38
7440-42-8
ND
ug/L
0.080
0.033
1
03/13/15 13:04
03/13/15 20:38
7440-43-9
132
ug/L
40.0
8.4
1
03/13/15 13:04
03/13/15 20:38
7440-70-2
5.1
ug/L
0.50
0.22
1
03/13/15 13:04
03/13/15 20:38
7440-47-3
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:38
7440-48-4
1.1
ug/L
1.0
0.22
1
03/13/15 13:04
03/13/15 20:38
7440-50-8
495
ug/L
50.0
8.0
1
03/13/15 13:04
03/13/15 20:38
7439-89-6
0.36
ug/L
0.10
0.046
1
03/13/15 13:04
03/13/15 20:38
7439-92-1
16.5
ug/L
10.0
2.8
1
03/13/15 13:04
03/13/15 20:38
7439-95-4
7.9
ug/L
0.50
0.14
1
03/13/15 13:04
03/13/15 20:38
7439-96-5
1.1
ug/L
0.50
0.24
1
03/13/15 13:04
03/13/15 20:38
7439-98-7
2.3
ug/L
0.50
0.23
1
03/13/15 13:04
03/13/15 20:38
7440-02-0
ND
ug/L
50.0
8.3
1
03/13/15 13:04
03/13/15 20:38
7440-09-7
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:38
7782-49-2
50.6
ug/L
50.0
18.2
1
03/13/15 13:04
03/13/15 20:38
7440-23-5
1.2
ug/L
0.50
0.057
1
03/13/15 13:04
03/13/15 20:38
7440-24-6
ND
ug/L
0.10
0.025
1
03/13/15 13:04
03/13/15 20:38
7440-28-0
ND
ug/L
1.0
0.21
1
03/13/15 13:04
03/13/15 20:38
7440-62-2
18.3
ug/L
5.0
2.5
1
03/13/15 13:04
03/13/15 20:38
7440-66-6
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L 0.20 0.026 1 03/15/1514:30 03/16/1511:11 7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 61 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3Syy RV16fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006525 Lab ID: 92240158015 Collected: 03/04/15 17:30 Received: 03/06/15 14:15 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
;I➢ZI7c\�i,I=11 l[99�r 6?
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Sodium
Strontium
Thallium
Vanadium
Zinc
7470 Mercury
Mercury
Date: 03/30/2015 02:56 PM
Analytical Method: EPA 6020A Preparation Method: EPA 3020
180
ug/L
10.0
1.2
1
03/13/15 13:04
03/13/15 20:43
7429-90-5
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:43
7440-36-0
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:43
7440-38-2
4.8
ug/L
0.30
0.14
1
03/13/15 13:04
03/13/15 20:43
7440-39-3
ND
ug/L
0.20
0.066
1
03/13/15 13:04
03/13/15 20:43
7440-41-7
ND
ug/L
5.0
1.0
1
03/13/15 13:04
03/13/15 20:43
7440-42-8
ND
ug/L
0.080
0.033
1
03/13/15 13:04
03/13/15 20:43
7440-43-9
308
ug/L
40.0
8.4
1
03/13/15 13:04
03/13/15 20:43
7440-70-2
33.7
ug/L
0.50
0.22
1
03/13/15 13:04
03/13/15 20:43
7440-47-3
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:43
7440-48-4
4.6
ug/L
1.0
0.22
1
03/13/15 13:04
03/13/15 20:43
7440-50-8
1360
ug/L
50.0
8.0
1
03/13/15 13:04
03/13/15 20:43
7439-89-6
0.40
ug/L
0.10
0.046
1
03/13/15 13:04
03/13/15 20:43
7439-92-1
76.3
ug/L
10.0
2.8
1
03/13/15 13:04
03/13/15 20:43
7439-95-4
18.7
ug/L
0.50
0.14
1
03/13/15 13:04
03/13/15 20:43
7439-96-5
4.1
ug/L
0.50
0.24
1
03/13/15 13:04
03/13/15 20:43
7439-98-7
4.6
ug/L
0.50
0.23
1
03/13/15 13:04
03/13/15 20:43
7440-02-0
109
ug/L
50.0
8.3
1
03/13/15 13:04
03/13/15 20:43
7440-09-7
ND
ug/L
0.50
0.25
1
03/13/15 13:04
03/13/15 20:43
7782-49-2
118
ug/L
50.0
18.2
1
03/13/15 13:04
03/13/15 20:43
7440-23-5
2.3
ug/L
0.50
0.057
1
03/13/15 13:04
03/13/15 20:43
7440-24-6
ND
ug/L
0.10
0.025
1
03/13/15 13:04
03/13/15 20:43
7440-28-0
4.5
ug/L
1.0
0.21
1
03/13/15 13:04
03/13/15 20:43
7440-62-2
12.1
ug/L
5.0
2.5
1
03/13/15 13:04
03/13/15 20:43
7440-66-6
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L 0.20 0.026 1 03/15/1514:30 03/16/1511:14 7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 62 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P36R08 6fyJ' ie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006515 SPLP Lab ID: 92240158016 Collected: 03/04/15 10:25 Received: 03/06/15 14:15 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
;T➢Z17c\�iil=11 a
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Sodium
Strontium
Thallium
Vanadium
Zinc
7470 Mercury
Mercury
Date: 03/30/2015 02:56 PM
Analytical Method: EPA 6020A Preparation Method: EPA 3020
3590
ug/L
10.0
1.2
1
03/26/1519:01
03/27/1514:25
7429-90-5
ND
ug/L
0.50
0.25
1
03/26/1519:01
03/27/1514:25
7440-36-0
0.76
ug/L
0.50
0.25
1
03/26/1519:01
03/27/1514:25
7440-38-2
34.5
ug/L
0.30
0.14
1
03/26/1519:01
03/27/1514:25
7440-39-3
0.27
ug/L
0.20
0.066
1
03/26/1519:01
03/27/1514:25
7440-41-7
9.9
ug/L
5.0
1.0
1
03/26/1519:01
03/27/1514:25
7440-42-8
ND
ug/L
0.080
0.033
1
03/26/1519:01
03/27/1514:25
7440-43-9
966
ug/L
40.0
8.4
1
03/26/1519:01
03/27/1514:25
7440-70-2
1.7
ug/L
0.50
0.22
1
03/26/1519:01
03/27/1514:25
7440-47-3
ND
ug/L
0.50
0.25
1
03/26/1519:01
03/27/1514:25
7440-48-4
1.7
ug/L
1.0
0.22
1
03/26/1519:01
03/27/1514:25
7440-50-8
1270
ug/L
50.0
8.0
1
03/26/1519:01
03/27/1514:25
7439-89-6
1.1
ug/L
0.10
0.046
1
03/26/1519:01
03/27/1514:25
7439-92-1
306
ug/L
10.0
2.8
1
03/26/1519:01
03/27/1514:25
7439-95-4
64.8
ug/L
0.50
0.14
1
03/26/1519:01
03/27/1514:25
7439-96-5
ND
ug/L
0.50
0.24
1
03/26/1519:01
03/27/1514:25
7439-98-7
0.91
ug/L
0.50
0.23
1
03/26/1519:01
03/27/1514:25
7440-02-0
931
ug/L
50.0
8.3
1
03/26/1519:01
03/27/1514:25
7440-09-7
ND
ug/L
0.50
0.25
1
03/26/1519:01
03/27/1514:25
7782-49-2
2920
ug/L
50.0
18.2
1
03/26/1519:01
03/27/1514:25
7440-23-5
13.6
ug/L
0.50
0.057
1
03/26/1519:01
03/27/1514:25
7440-24-6
ND
ug/L
0.10
0.025
1
03/26/1519:01
03/27/1514:25
7440-28-0
1.9
ug/L
1.0
0.21
1
03/26/1519:01
03/27/1514:25
7440-62-2
5.4
ug/L
5.0
2.5
1
03/26/1519:01
03/27/1514:25
7440-66-6
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L 0.20 0.026 1 03/26/1519:10 03/27/1512:51 7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 63 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3Sy M16fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006516 SPLP Lab ID: 92240158017 Collected: 03/04/15 11:10 Received: 03/06/15 14:15 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
;T➢Z17c\�iil=11 a
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Sodium
Strontium
Thallium
Vanadium
Zinc
7470 Mercury
Mercury
Date: 03/30/2015 02:56 PM
Analytical Method: EPA 6020A Preparation Method: EPA 3020
195
ug/L
10.0
1.2
1
03/26/1519:01
03/27/1514:28
7429-90-5
ND
ug/L
0.50
0.25
1
03/26/1519:01
03/27/1514:28
7440-36-0
ND
ug/L
0.50
0.25
1
03/26/1519:01
03/27/1514:28
7440-38-2
1.7
ug/L
0.30
0.14
1
03/26/1519:01
03/27/1514:28
7440-39-3
ND
ug/L
0.20
0.066
1
03/26/1519:01
03/27/1514:28
7440-41-7
72.0
ug/L
5.0
1.0
1
03/26/1519:01
03/27/1514:28
7440-42-8
ND
ug/L
0.080
0.033
1
03/26/1519:01
03/27/1514:28
7440-43-9
202
ug/L
40.0
8.4
1
03/26/1519:01
03/27/1514:28
7440-70-2
0.90
ug/L
0.50
0.22
1
03/26/1519:01
03/27/1514:28
7440-47-3
ND
ug/L
0.50
0.25
1
03/26/1519:01
03/27/1514:28
7440-48-4
ND
ug/L
1.0
0.22
1
03/26/1519:01
03/27/1514:28
7440-50-8
73.0
ug/L
50.0
8.0
1
03/26/1519:01
03/27/1514:28
7439-89-6
ND
ug/L
0.10
0.046
1
03/26/1519:01
03/27/1514:28
7439-92-1
215
ug/L
10.0
2.8
1
03/26/1519:01
03/27/1514:28
7439-95-4
3.2
ug/L
0.50
0.14
1
03/26/1519:01
03/27/1514:28
7439-96-5
ND
ug/L
0.50
0.24
1
03/26/1519:01
03/27/1514:28
7439-98-7
ND
ug/L
0.50
0.23
1
03/26/1519:01
03/27/1514:28
7440-02-0
696
ug/L
50.0
8.3
1
03/26/1519:01
03/27/1514:28
7440-09-7
ND
ug/L
0.50
0.25
1
03/26/1519:01
03/27/1514:28
7782-49-2
5620
ug/L
50.0
18.2
1
03/26/1519:01
03/27/1514:28
7440-23-5
1.4
ug/L
0.50
0.057
1
03/26/1519:01
03/27/1514:28
7440-24-6
ND
ug/L
0.10
0.025
1
03/26/1519:01
03/27/1514:28
7440-28-0
ND
ug/L
1.0
0.21
1
03/26/1519:01
03/27/1514:28
7440-62-2
ND
ug/L
5.0
2.5
1
03/26/1519:01
03/27/1514:28
7440-66-6
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L 0.20 0.026 1 03/26/1519:10 03/27/1512:59 7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 64 of 94

aceAnaiXical
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Pace Analytical Services, Inc.
P3Sy Mr6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006521 SPLP Lab ID: 92240158018 Collected: 03/04/15 15:05 Received: 03/06/15 14:15 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
;T➢Z17c\r�il=11 a r 6?
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Sodium
Strontium
Thallium
Vanadium
Zinc
7470 Mercury
Mercury
Date: 03/30/2015 02:56 PM
Analytical Method: EPA 6020A Preparation Method: EPA 3020
132000
ug/L
250
28.8
5
03/26/1519:01
03/27/1514:46
7429-90-5
ND
ug/L
2.5
1.2
1
03/26/1519:01
03/27/1514:31
7440-36-0
12.3
ug/L
2.5
1.2
1
03/26/1519:01
03/27/1514:31
7440-38-2
377
ug/L
1.5
0.70
1
03/26/1519:01
03/27/1514:31
7440-39-3
2.6
ug/L
1.0
0.33
1
03/26/1519:01
03/27/1514:31
7440-41-7
75.8
ug/L
25.0
5.1
1
03/26/1519:01
03/27/1514:31
7440-42-8
ND
ug/L
0.40
0.16
1
03/26/1519:01
03/27/1514:31
7440-43-9
2170
ug/L
200
41.9
1
03/26/1519:01
03/27/1514:31
7440-70-2
269
ug/L
2.5
1.1
1
03/26/1519:01
03/27/1514:31
7440-47-3
24.3
ug/L
2.5
1.2
1
03/26/1519:01
03/27/1514:31
7440-48-4
112
ug/L
5.0
1.1
1
03/26/1519:01
03/27/1514:31
7440-50-8
109000
ug/L
250
40.1
1
03/26/1519:01
03/27/1514:31
7439-89-6
62.1
ug/L
0.50
0.23
1
03/26/1519:01
03/27/1514:31
7439-92-1
6500
ug/L
50.0
14.2
1
03/26/1519:01
03/27/1514:31
7439-95-4
250
ug/L
2.5
0.68
1
03/26/1519:01
03/27/1514:31
7439-96-5
2.7
ug/L
2.5
1.2
1
03/26/1519:01
03/27/1514:31
7439-98-7
48.6
ug/L
2.5
1.2
1
03/26/1519:01
03/27/1514:31
7440-02-0
5200
ug/L
250
41.7
1
03/26/1519:01
03/27/1514:31
7440-09-7
ND
ug/L
2.5
1.2
1
03/26/1519:01
03/27/1514:31
7782-49-2
4560
ug/L
250
91.2
1
03/26/1519:01
03/27/1514:31
7440-23-5
38.2
ug/L
2.5
0.28
1
03/26/1519:01
03/27/1514:31
7440-24-6
0.60
ug/L
0.50
0.12
1
03/26/1519:01
03/27/1514:31
7440-28-0
277
ug/L
5.0
1.1
1
03/26/1519:01
03/27/1514:31
7440-62-2
132
ug/L
25.0
12.5
1
03/26/1519:01
03/27/1514:31
7440-66-6
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L 0.60 0.078 1 03/26/1519:10 03/27/1513:02 7439-97-6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
Page 65 of 94

aceAnaiXical
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Pace Analytical Services, Inc.
P3y M,r6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15030202
Pace Project No.: 92240158
Sample: 2015006524 SPLP Lab ID: 92240158019 Collected: 03/04/15 16:45 Received: 03/06/15 14:15 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
;T➢Z17c\riil=11 a
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Sodium
Strontium
Thallium
Vanadium
Zinc
7470 Mercury
Mercury
Date: 03/30/2015 02:56 PM
Analytical Method: EPA 6020A Preparation Method: EPA 3020
3030
ug/L
10.0
1.2
1
03/26/1519:01
03/27/1514:34
7429-90-5
ND
ug/L
0.50
0.25
1
03/26/1519:01
03/27/1514:34
7440-36-0
ND
ug/L
0.50
0.25
1
03/26/1519:01
03/27/1514:34
7440-38-2
38.8
ug/L
0.30
0.14
1
03/26/1519:01
03/27/1514:34
7440-39-3
0.30
ug/L
0.20
0.066
1
03/26/1519:01
03/27/1514:34
7440-41-7
18.1
ug/L
5.0
1.0
1
03/26/1519:01
03/27/1514:34
7440-42-8
ND
ug/L
0.080
0.033
1
03/26/1519:01
03/27/1514:34
7440-43-9
407
ug/L
40.0
8.4
1
03/26/1519:01
03/27/1514:34
7440-70-2
1.1
ug/L
0.50
0.22
1
03/26/1519:01
03/27/1514:34
7440-47-3
2.5
ug/L
0.50
0.25
1
03/26/1519:01
03/27/1514:34
7440-48-4
4.4
ug/L
1.0
0.22
1
03/26/1519:01
03/27/1514:34
7440-50-8
3140
ug/L
50.0
8.0
1
03/26/1519:01
03/27/1514:34
7439-89-6
0.69
ug/L
0.10
0.046
1
03/26/1519:01
03/27/1514:34
7439-92-1
175
ug/L
10.0
2.8
1
03/26/1519:01
03/27/1514:34
7439-95-4
313
ug/L
0.50
0.14
1
03/26/1519:01
03/27/1514:34
7439-96-5
ND
ug/L
0.50
0.24
1
03/26/1519:01
03/27/1514:34
7439-98-7
0.57
ug/L
0.50
0.23
1
03/26/1519:01
03/27/1514:34
7440-02-0
414
ug/L
50.0
8.3
1
03/26/1519:01
03/27/1514:34
7440-09-7
ND
ug/L
0.50
0.25
1
03/26/1519:01
03/27/1514:34
7782-49-2
2300
ug/L
50.0
18.2
1
03/26/1519:01
03/27/1514:34
7440-23-5
12.1
ug/L
0.50
0.057
1
03/26/1519:01
03/27/1514:34
7440-24-6
ND
ug/L
0.10
0.025
1
03/26/1519:01
03/27/1514:34
7440-28-0
7.0
ug/L
1.0
0.21
1
03/26/1519:01
03/27/1514:34
7440-62-2
ND
ug/L
5.0
2.5
1
03/26/1519:01
03/27/1514:34
7440-66-6
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L 0.60 0.078 1 03/26/1519:10 03/27/1513:04 7439-97-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 66 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3Sy M16fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: MERP/12966 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury
Associated Lab Samples: 92240158011, 92240158012, 92240158013, 92240158014, 92240158015
METHOD BLANK: 1917931 Matrix: Water
Associated Lab Samples: 92240158011, 92240158012, 92240158013, 92240158014, 92240158015
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 03/16/1510:47
LABORATORY CONTROL SAMPLE: 1917932
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 5 5.0 100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1917933 1917934
MS MSD
92240164007 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Mercury ug/L ND 5 5 4.9 4.2 99 85 75-125 15 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc..
Page 67 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y RVr6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: MERP/13071
Analysis Method: EPA 7470
QC Batch Method: EPA 7470
Analysis Description: 7470 Mercury
Associated Lab Samples: 92240158016, 92240158017,
92240158018, 92240158019
METHOD BLANK: 1926030
Matrix: Water
Associated Lab Samples: 92240158016, 92240158017,
92240158018, 92240158019
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Mercury ug/L
ND 0.20
03/27/1512:24
LABORATORY CONTROL SAMPLE: 1926031
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Mercury ug/L
5 4.9
99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1926032 1926033
MS MSD
92242374012
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD RPD Qual
Mercury ug/L ND
5 5 4.2
5.1 83 102 75-125 21 20 R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc..
Page 68 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
PARV16 M.Nie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: MERP/5474 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 92240158001, 92240158002, 92240158003, 92240158004, 92240158005, 92240158006, 92240158007,
92240158008,92240158009,92240158010
METHOD BLANK: 1157677 Matrix: Solid
Associated Lab Samples: 92240158001, 92240158002, 92240158003, 92240158004, 92240158005, 92240158006, 92240158007,
92240158008,92240158009,92240158010
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury mg/kg ND 0.0084 03/17/1512:46
LABORATORY CONTROL SAMPLE: 1157678
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury mg/kg .079 0.081 102 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1157679 1157680
MS MSD
92239540004 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qua]
Mercury mg/kg 0.050 .0988 .0963 0.13 0.12 77 74 80-120 4 20 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc..
Page 69 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3Sy 919r6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: MPRP/23094 Analysis Method: EPA 6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET Solid
Associated Lab Samples: 92240158001, 92240158002, 92240158003, 92240158004, 92240158005, 92240158006, 92240158007,
92240158008,92240158009,92240158010
METHOD BLANK: 1157065 Matrix: Solid
Associated Lab Samples: 92240158001, 92240158002, 92240158003, 92240158004, 92240158005, 92240158006, 92240158007,
92240158008,92240158009,92240158010
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Aluminum
mg/kg
ND
5.0
03/17/15 08:02
Barium
mg/kg
ND
0.50
03/17/15 08:02
Beryllium
mg/kg
ND
0.050
03/17/15 08:02
Boron
mg/kg
ND
2.5
03/17/15 08:02
Calcium
mg/kg
ND
25.1
03/17/15 08:02
Chromium
mg/kg
ND
0.25
03/17/15 08:02
Copper
mg/kg
ND
0.25
03/17/15 08:02
Iron
mg/kg
ND
2.0
03/17/15 08:02
Magnesium
mg/kg
ND
25.1
03/17/15 08:02
Manganese
mg/kg
ND
0.25
03/17/15 08:02
Molybdenum
mg/kg
ND
0.50
03/17/15 08:02
Nickel
mg/kg
ND
0.25
03/17/15 08:02
Potassium
mg/kg
ND
50.1
03/17/15 08:02
Sodium
mg/kg
ND
50.1
03/17/15 08:02
Strontium
mg/kg
ND
0.50
03/17/15 08:02
Zinc
mg/kg
ND
1.0
03/17/15 08:02
LABORATORY CONTROL SAMPLE:
Parameter
1157066
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Aluminum
mg/kg
127
132
103
80-120
Barium
mg/kg
12.7
13.1
103
80-120
Beryllium
mg/kg
1.3
1.2
98
80-120
Boron
mg/kg
127
123
97
80-120
Calcium
mg/kg
637
646
101
80-120
Chromium
mg/kg
12.7
12.8
101
80-120
Copper
mg/kg
12.7
12.6
99
80-120
Iron
mg/kg
127
124
98
80-120
Magnesium
mg/kg
637
648
102
80-120
Manganese
mg/kg
12.7
12.4
97
80-120
Molybdenum
mg/kg
12.7
12.3
96
80-120
Nickel
mg/kg
12.7
12.7
99
80-120
Potassium
mg/kg
637
614
96
80-120
Sodium
mg/kg
637
651
102
80-120
Strontium
mg/kg
12.7
12.4
98
80-120
Zinc
mg/kg
63.7
63.3
99
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc.. Page 70 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3Sy Mr6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1157067
1157068
MS
MSD
92239540001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Aluminum
mg/kg
1440
131
124
2990
2380
1180
756
75-125
23
20 M1,R1
Barium
mg/kg
5.1
13.1
12.4
20.5
18.5
117
108
75-125
10
20
Beryllium
mg/kg
0.033J
1.3
1.2
1.3
1.2
93
96
75-125
2
20
Boron
mg/kg
1.5J
131
124
118
117
89
93
75-125
1
20
Calcium
mg/kg
35.3
657
622
689
668
100
102
75-125
3
20
Chromium
mg/kg
2.0
13.1
12.4
15.2
14.5
101
101
75-125
5
20
Copper
mg/kg
0.96
13.1
12.4
13.8
13.3
98
99
75-125
4
20
Iron
mg/kg
1960
131
124
2320
1960
278
-2
75-125
17
20 M1
Magnesium
mg/kg
43.3
657
622
743
710
107
107
75-125
5
20
Manganese
mg/kg
2.2
13.1
12.4
15.4
14.2
101
97
75-125
8
20
Molybdenum
mg/kg
ND
13.1
12.4
11.2
10.9
85
88
75-125
2
20
Nickel
mg/kg
0.70
13.1
12.4
14.2
13.1
103
100
75-125
8
20
Potassium
mg/kg
33.7J
657
622
669
645
97
98
75-125
4
20
Sodium
mg/kg
ND
657
622
658
636
99
101
75-125
3
20
Strontium
mg/kg
0.29J
13.1
12.4
13.1
12.6
97
99
75-125
4
20
Zinc
mg/kg
3.6
65.7
62.2
67.9
64.2
98
97
75-125
6
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc..
Page 71 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3yy RVr6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: MPRP/23095 Analysis Method: EPA 6020
QC Batch Method: EPA 3050 Analysis Description: 6020 MET SOLID
Associated Lab Samples: 92240158001, 92240158002, 92240158003, 92240158004, 92240158005, 92240158006, 92240158007,
92240158008,92240158009,92240158010
METHOD BLANK: 1157069 Matrix: Solid
Associated Lab Samples: 92240158001, 92240158002, 92240158003, 92240158004, 92240158005, 92240158006, 92240158007,
92240158008,92240158009,92240158010
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Antimony
mg/kg
ND
0.050
03/17/1511:05 N2
Arsenic
mg/kg
ND
0.050
03/17/1511:05
Cadmium
mg/kg
ND
0.0060
03/17/1511:05
Cobalt
mg/kg
ND
0.050
03/17/1511:05
Lead
mg/kg
ND
0.050
03/17/1511:05
Selenium
mg/kg
ND
0.050
03/17/1511:05
Thallium
mg/kg
ND
0.050
03/17/1511:05
Vanadium
mg/kg
ND
0.050
03/17/1511:05
LABORATORY CONTROL SAMPLE:
Parameter
1157070
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
mg/kg
2.5
2.5
99
80-120 N2
Arsenic
mg/kg
2.5
2.7
106
80-120
Cadmium
mg/kg
.25
0.25
99
80-120
Cobalt
mg/kg
2.5
2.7
106
80-120
Lead
mg/kg
2.5
2.5
101
80-120
Selenium
mg/kg
2.5
2.7
108
80-120
Thallium
mg/kg
2.5
2.5
99
80-120
Vanadium
mg/kg
2.5
2.6
103
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1157071
1157072
MS
MSD
92239540002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
mg/kg
ND
2.5
2.5
0.99
0.911
38
34
75-125
20 D3,M6,
N2
Arsenic
mg/kg
3.9
2.5
2.5
5.5
5.7
67
73
75-125
3
20 D3,M6
Cadmium
mg/kg
0.071J
.25
.25
0.33
0.33
103
102
75-125
0
20 D3
Cobalt
mg/kg
9.8
2.5
2.5
11.2
12.8
57
123
75-125
14
20 D3,M6
Lead
mg/kg
3.0
2.5
2.5
5.1
5.6
85
105
75-125
10
20 D3
Selenium
mg/kg
0.83J
2.5
2.5
3.3
3.3
98
100
75-125
2
20 D3
Thallium
mg/kg
0.64J
2.5
2.5
2.9
3.0
94
96
75-125
3
20 D3
Vanadium
mg/kg
32.2
2.5
2.5
30.2
36.6
-84
177
75-125
19
20 D4,M6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc..
Page 72 of 94

aceAnaiXical
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Pace Analytical Services, Inc.
P36gmirpy.,y. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: MPRP/52931 Analysis Method: EPA 6020A
QC Batch Method: EPA 3020 Analysis Description: 6020A Water UPD4
Associated Lab Samples: 92240158011, 92240158012, 92240158013, 92240158014, 92240158015
METHOD BLANK: 1917520 Matrix: Water
Associated Lab Samples: 92240158011, 92240158012, 92240158013, 92240158014, 92240158015
Blank Reporting
Parameter Units Result Limit Analyzed
Aluminum
ug/L
ND
10.0
03/16/15 09:43
Antimony
ug/L
ND
0.50
03/16/15 09:43
Arsenic
ug/L
ND
0.50
03/16/15 09:43
Barium
ug/L
ND
0.30
03/16/15 09:43
Beryllium
ug/L
ND
0.20
03/16/15 09:43
Boron
ug/L
ND
5.0
03/16/15 09:43
Cadmium
ug/L
ND
0.080
03/16/15 09:43
Calcium
ug/L
ND
40.0
03/16/15 09:43
Chromium
ug/L
ND
0.50
03/16/15 09:43
Cobalt
ug/L
ND
0.50
03/16/15 09:43
Copper
ug/L
ND
1.0
03/16/15 09:43
Iron
ug/L
ND
50.0
03/16/15 09:43
Lead
ug/L
ND
0.10
03/16/15 09:43
Magnesium
ug/L
ND
10.0
03/16/15 09:43
Manganese
ug/L
ND
0.50
03/16/15 09:43
Molybdenum
ug/L
ND
0.50
03/16/15 09:43
Nickel
ug/L
ND
0.50
03/16/15 09:43
Potassium
ug/L
ND
50.0
03/16/15 09:43
Selenium
ug/L
ND
0.50
03/16/15 09:43
Sodium
ug/L
ND
50.0
03/16/15 09:43
Strontium
ug/L
ND
0.50
03/16/15 09:43
Thallium
ug/L
ND
0.10
03/16/15 09:43
Vanadium
ug/L
ND
1.0
03/16/15 09:43
Zinc
ug/L
ND
5.0
03/16/15 09:43
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1917521
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Aluminum
ug/L
80
76.9
96
80-120
Antimony
ug/L
80
79.4
99
80-120
Arsenic
ug/L
80
79.0
99
80-120
Barium
ug/L
80
80.7
101
80-120
Beryllium
ug/L
80
82.8
104
80-120
Boron
ug/L
80
81.1
101
80-120
Cadmium
ug/L
80
80.0
100
80-120
Calcium
ug/L
1000
1000
100
80-120
Chromium
ug/L
80
79.9
100
80-120
Cobalt
ug/L
80
80.8
101
80-120
Copper
ug/L
80
77.4
97
80-120
Iron
ug/L
1000
1040
104
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc.. Page 73 of 94

aceAnaiXical
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Pace Analytical Services, Inc.
P3y 906r6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
LABORATORY CONTROL SAMPLE:
1917521
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Lead
ug/L
80
80.9
101
80-120
Magnesium
ug/L
1000
1010
101
80-120
Manganese
ug/L
80
80.3
100
80-120
Molybdenum
ug/L
80
79.5
99
80-120
Nickel
ug/L
80
80.4
100
80-120
Potassium
ug/L
1000
1040
104
80-120
Selenium
ug/L
80
80.6
101
80-120
Sodium
ug/L
1000
988
99
80-120
Strontium
ug/L
80
79.6
100
80-120
Thallium
ug/L
80
79.1
99
80-120
Vanadium
ug/L
80
80.6
101
80-120
Zinc
ug/L
80
78.9
99
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1917522
1917523
MS
MSD
92240320006
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD
RPD Qual
Aluminum
ug/L
168
80
80
359
387
238
274
75-125
8
20 M1
Antimony
ug/L
ND
80
80
80.9
78.9
101
98
75-125
3
20
Arsenic
ug/L
ND
80
80
79.9
78.5
100
98
75-125
2
20
Barium
ug/L
20.0
80
80
103
101
104
101
75-125
2
20
Beryllium
ug/L
ND
80
80
84.1
85.0
105
106
75-125
1
20
Boron
ug/L
138
80
80
232
231
117
117
75-125
0
20
Cadmium
ug/L
ND
80
80
81.1
79.6
101
100
75-125
2
20
Calcium
ug/L
7460
1000
1000
8970
8670
151
122
75-125
3
20 M1
Chromium
ug/L
ND
80
80
81.4
80.3
101
100
75-125
1
20
Cobalt
ug/L
ND
80
80
82.7
81.1
103
101
75-125
2
20
Copper
ug/L
ND
80
80
79.8
79.0
99
98
75-125
1
20
Iron
ug/L
499
1000
1000
1630
1630
113
113
75-125
0
20
Lead
ug/L
0.29
80
80
82.3
81.8
103
102
75-125
1
20
Magnesium
ug/L
2720
1000
1000
3910
3840
118
112
75-125
2
20
Manganese
ug/L
39.8
80
80
123
121
104
102
75-125
2
20
Molybdenum
ug/L
ND
80
80
81.1
79.4
101
99
75-125
2
20
Nickel
ug/L
ND
80
80
82.1
80.0
102
100
75-125
3
20
Potassium
ug/L
1470
1000
1000
2640
2570
117
110
75-125
3
20
Selenium
ug/L
ND
80
80
81.8
80.9
102
101
75-125
1
20
Sodium
ug/L
5770
1000
1000
7190
7000
142
123
75-125
3
20 M1
Strontium
ug/L
47.2
80
80
130
127
103
100
75-125
2
20
Thallium
ug/L
ND
80
80
83.1
82.3
104
103
75-125
1
20
Vanadium
ug/L
ND
80
80
83.2
82.7
103
102
75-125
1
20
Zinc
ug/L
ND
80
80
84.2
84.6
103
104
75-125
0
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc..
Page 74 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y 906r6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: MPRP/53205 Analysis Method: EPA 6020A
QC Batch Method: EPA 3020 Analysis Description: 6020A Water UPD4
Associated Lab Samples: 92240158016, 92240158017, 92240158018, 92240158019
METHOD BLANK: 1926005 Matrix: Water
Associated Lab Samples: 92240158016, 92240158017, 92240158018, 92240158019
Blank Reporting
Parameter Units Result Limit
Analyzed
Aluminum
ug/L
ND
10.0
03/27/1513:48
Antimony
ug/L
ND
0.50
03/27/1513:48
Arsenic
ug/L
ND
0.50
03/27/1513:48
Barium
ug/L
ND
0.30
03/27/1513:48
Beryllium
ug/L
ND
0.20
03/27/1513:48
Boron
ug/L
ND
5.0
03/27/1513:48
Cadmium
ug/L
ND
0.080
03/27/1513:48
Calcium
ug/L
ND
40.0
03/27/1513:48
Chromium
ug/L
ND
0.50
03/27/1513:48
Cobalt
ug/L
ND
0.50
03/27/1513:48
Copper
ug/L
ND
1.0
03/27/1513:48
Iron
ug/L
ND
50.0
03/27/1513:48
Lead
ug/L
ND
0.10
03/27/1513:48
Magnesium
ug/L
ND
10.0
03/27/1513:48
Manganese
ug/L
ND
0.50
03/27/1513:48
Molybdenum
ug/L
ND
0.50
03/27/1513:48
Nickel
ug/L
ND
0.50
03/27/1513:48
Potassium
ug/L
ND
50.0
03/27/1513:48
Selenium
ug/L
ND
0.50
03/27/1513:48
Sodium
ug/L
ND
50.0
03/27/1513:48
Strontium
ug/L
ND
0.50
03/27/1513:48
Thallium
ug/L
ND
0.10
03/27/1513:48
Vanadium
ug/L
ND
1.0
03/27/1513:48
Zinc
ug/L
ND
5.0
03/27/1513:48
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1926006
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Aluminum
ug/L
80
90.1
113
80-120
Antimony
ug/L
80
81.4
102
80-120
Arsenic
ug/L
80
81.9
102
80-120
Barium
ug/L
80
86.1
108
80-120
Beryllium
ug/L
80
81.9
102
80-120
Boron
ug/L
80
84.7
106
80-120
Cadmium
ug/L
80
86.8
108
80-120
Calcium
ug/L
1000
1100
110
80-120
Chromium
ug/L
80
87.4
109
80-120
Cobalt
ug/L
80
85.9
107
80-120
Copper
ug/L
80
85.1
106
80-120
Iron
ug/L
1000
1120
112
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc.. Page 75 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y 90A,16fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
LABORATORY CONTROL SAMPLE:
1926006
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Lead
ug/L
80
85.0
106
80-120
Magnesium
ug/L
1000
1050
105
80-120
Manganese
ug/L
80
89.4
112
80-120
Molybdenum
ug/L
80
84.4
105
80-120
Nickel
ug/L
80
87.2
109
80-120
Potassium
ug/L
1000
1080
108
80-120
Selenium
ug/L
80
82.6
103
80-120
Sodium
ug/L
1000
1080
108
80-120
Strontium
ug/L
80
84.2
105
80-120
Thallium
ug/L
80
88.7
111
80-120
Vanadium
ug/L
80
86.8
108
80-120
Zinc
ug/L
80
87.7
110
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1926431
1926432
MS
MSD
92242374012
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD
RPD Qual
Aluminum
ug/L
57.4
80
80
190
332
166
344
75-125
55
20 M1,R1
Antimony
ug/L
ND
80
80
79.8
80.0
100
100
75-125
0
20
Arsenic
ug/L
ND
80
80
80.6
80.6
101
101
75-125
0
20
Barium
ug/L
2.2
80
80
87.7
86.6
107
105
75-125
1
20
Beryllium
ug/L
ND
80
80
82.7
81.4
103
102
75-125
2
20
Boron
ug/L
ND
80
80
88.3
87.1
108
107
75-125
1
20
Cadmium
ug/L
ND
80
80
87.1
87.1
109
109
75-125
0
20
Calcium
ug/L
102
1000
1000
1170
1200
106
110
75-125
3
20
Chromium
ug/L
1.5
80
80
88.9
87.7
109
108
75-125
1
20
Cobalt
ug/L
ND
80
80
87.1
86.2
109
108
75-125
1
20
Copper
ug/L
1.3
80
80
86.6
85.2
107
105
75-125
2
20
Iron
ug/L
553
1000
1000
1680
1870
113
131
75-125
10
20 M1
Lead
ug/L
0.12
80
80
83.8
82.4
105
103
75-125
2
20
Magnesium
ug/L
29.0
1000
1000
1100
1090
107
106
75-125
0
20
Manganese
ug/L
13.6
80
80
102
101
111
110
75-125
1
20
Molybdenum
ug/L
ND
80
80
83.0
83.2
104
104
75-125
0
20
Nickel
ug/L
1.3
80
80
88.8
87.6
109
108
75-125
1
20
Potassium
ug/L
ND
1000
1000
1100
1100
106
106
75-125
0
20
Selenium
ug/L
ND
80
80
82.9
82.9
104
104
75-125
0
20
Sodium
ug/L
108
1000
1000
1190
1170
108
106
75-125
2
20
Strontium
ug/L
0.95
80
80
84.1
83.3
104
103
75-125
1
20
Thallium
ug/L
ND
80
80
87.8
86.6
110
108
75-125
1
20
Vanadium
ug/L
ND
80
80
85.8
84.6
107
105
75-125
1
20
Zinc
ug/L
26.6
80
80
111
111
106
105
75-125
1
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc..
Page 76 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y 90Ar6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: PMST/3347
Analysis Method:
ASTM D2974-87
QC Batch Method: ASTM D2974-87
Analysis Description:
Dry Weight/Percent Moisture
Associated Lab Samples: 92240158001,
92240158002, 92240158003, 92240158004,
92240158005, 92240158006, 92240158007,
92240158008,92240158009,92240158010
SAMPLE DUPLICATE: 1157598
35178663001
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Percent Moisture
%
23.9
23.3 2
10
SAMPLE DUPLICATE: 1157600
92240158001
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Percent Moisture
%
35.5
35.2 1
10
SAMPLE DUPLICATE: 1157619
92239540004
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
Percent Moisture
%
20.0
19.1 4
10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc.. Page 77 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y 90Ar6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: WET/36142 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 92240158001, 92240158002, 92240158003, 92240158004, 92240158005, 92240158006, 92240158007,
92240158008,92240158009,92240158010
SAMPLE DUPLICATE: 1407673
92240170008 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
pH at 25 Degrees C Std. Units 5.9 5.7 3 10
SAMPLE DUPLICATE: 1407674
92240158003 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
pH at 25 Degrees C Std. Units 6.0 6.1 1 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc.. Page 78 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y 900r6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: WETA/22270
Analysis Method: EPA 300.0
QC Batch Method: EPA 300.0
Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92240158007, 92240158008,
92240158009, 92240158010
METHOD BLANK: 1415171
Matrix: Water
Associated Lab Samples: 92240158007, 92240158008,
92240158009, 92240158010
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Sulfate mg/L
ND 2.0
03/19/1518:22
LABORATORY CONTROL SAMPLE: 1415172
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Sulfate mg/L
20 18.7
94 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1415173 1415174
MS MSD
92239540001
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD RPD Qual
Sulfate mg/L 3.5
24 24 25.8
25.8 93 93 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1415175 1415176
MS MSD
92240158010 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Sulfate mg/L 3.0 25.5 25.5 26.8 26.8 93 93 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc..
Page 79 of 94

aceAnaiXical
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Pace Analytical Services, Inc.
P3y RVr6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: WETA/22256
Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2
Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples: 92240158007, 92240158008,
92240158009, 92240158010
METHOD BLANK: 1413768
Matrix: Water
Associated Lab Samples: 92240158007, 92240158008,
92240158009, 92240158010
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Nitrogen, Nitrate mg/L
0.22 0.020
03/18/15 16:20 B
LABORATORY CONTROL SAMPLE: 1413769
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Nitrate mg/L
2.5 2.5
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1413770 1413771
MS MSD
92239540001
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Nitrate mg/L 0.41
3 3 3.3
3.3 95 95 90-110 0 10 H1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1413772 1413773
MS MSD
92239540002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Nitrate mg/L 0.33 2.9 2.9 3.2 3.2 98 98 90-110 0 10 H1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc..
Page 80 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
P3y 906r6fY.Nie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: WETA/22273
Analysis Method: SM 4500-CI-E
QC Batch Method: SM 4500-CI-E
Analysis Description: 4500 Chloride
Associated Lab Samples: 92240158007, 92240158008,
92240158009, 92240158010
METHOD BLANK: 1415463
Matrix: Water
Associated Lab Samples: 92240158007, 92240158008,
92240158009, 92240158010
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Chloride mg/L
ND 1.0
03/19/15 20:57
LABORATORY CONTROL SAMPLE: 1415464
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Chloride mg/L
20 20.4
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1415465 1415466
MS MSD
92239540003
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD RPD Qual
Chloride mg/L ND
23.9 23.9 24.7
24.6 101 101 90-110 0 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1415467 1415468
MS MSD
92239543006 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Chloride mg/L 5.7J 24.7 24.7 31.0 30.7 102 101 90-110 1 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc..
Page 81 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
Pa89QMr6fy1Ne. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: WETA/44508 Analysis Method: EPA 9056
QC Batch Method: EPA 9056 Analysis Description: 9056 IC Anions
Associated Lab Samples: 92240158001, 92240158002, 92240158003, 92240158004
METHOD BLANK: 1155640 Matrix: Solid
Associated Lab Samples:
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chloride mg/kg ND 50.6 03/13/1512:56
Sulfate mg/kg ND 50.6 03/13/1512:56
LABORATORY CONTROL SAMPLE:
1155641
Parameter
Units
Chloride
mg/kg
Sulfate
mg/kg
MATRIX SPIKE SAMPLE:
1155643
Parameter
Units
Chloride
mg/kg
Sulfate
mg/kg
SAMPLE DUPLICATE: 1155642
Parameter
Chloride
Sulfate
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
504 471 94 80-120
504 466 92 80-120
92239540001 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
ND 500 423 69 80-120 M 1
ND 500 458 78 80-120 M 1
92239540001 Dup
Units Result Result
mg/kg ND ND
mg/kg ND ND
Max
RPD RPD Qualifiers
20
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc.. Page 82 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
Padg"lirpy.,y. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: WETA/44515 Analysis Method: EPA 9056
QC Batch Method: EPA 9056 Analysis Description: 9056 IC Anions
Associated Lab Samples: 92240158009, 92240158010
METHOD BLANK: 1155845 Matrix: Solid
Associated Lab Samples:
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chloride mg/kg ND 48.9 03/13/1515:40
Sulfate mg/kg ND 48.9 03/13/1515:40
LABORATORY CONTROL SAMPLE:
1155846
Parameter
Units
Chloride
mg/kg
Sulfate
mg/kg
MATRIX SPIKE SAMPLE:
1155848
Parameter
Units
Chloride
mg/kg
Sulfate
mg/kg
SAMPLE DUPLICATE: 1155847
Parameter
Chloride
Sulfate
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
500 477 95 80-120
500 480 96 80-120
92240158009 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
ND 717 602 84 80-120
ND 717 610 85 80-120
92240158009 Dup
Units Result Result
mg/kg ND ND
mg/kg ND ND
Max
RPD RPD Qualifiers
20
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc.. Page 83 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
Padg"ifYINe. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: WETA/44533 Analysis Method: EPA 9056
QC Batch Method: EPA 9056 Analysis Description: 9056 IC Anions
Associated Lab Samples: 92240158005, 92240158006, 92240158007, 92240158008
METHOD BLANK: 1156870 Matrix: Solid
Associated Lab Samples:
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chloride mg/kg ND 50.0 03/14/1518:25
Sulfate mg/kg ND 50.0 03/14/1518:25
LABORATORY CONTROL SAMPLE:
1156871
Parameter
Units
Chloride
mg/kg
Sulfate
mg/kg
MATRIX SPIKE SAMPLE:
1156873
Parameter
Units
Chloride
mg/kg
Sulfate
mg/kg
SAMPLE DUPLICATE: 1156872
Parameter
Chloride
Sulfate
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
500 498 100 80-120
500 500 100 80-120
92240158005 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
ND 544 531 98 80-120
ND 544 547 89 80-120
92240158005 Dup
Units Result Result
mg/kg ND ND
mg/kg ND ND
Max
RPD RPD Qualifiers
20
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc.. Page 84 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
Padg ifYINe. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: WETA/44509
Analysis Method:
EPA 9056
QC Batch Method: EPA 9056
Analysis Description:
9056 IC Anions
Associated Lab Samples: 92240158001, 92240158002, 92240158003, 92240158004
METHOD BLANK: 1155644
Matrix: Solid
Associated Lab Samples:
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Nitrate as N
mg/kg
ND 5.1
03/13/15 12:56
LABORATORY CONTROL SAMPLE:
1155645
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Nitrate as N
mg/kg
50.4 47.9
95
80-120
MATRIX SPIKE SAMPLE:
1155647
92239540001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Nitrate as N
mg/kg
ND 50
43.8
85 80-120 H3
SAMPLE DUPLICATE: 1155646
92239540001 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Nitrate as N
mg/kg
ND ND
20 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc.. Page 85 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
Pa89Qffl�116fy f1e. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: WETA/44514
Analysis Method:
EPA 9056
QC Batch Method: EPA 9056
Analysis Description:
9056 IC Anions
Associated Lab Samples: 92240158009, 92240158010
METHOD BLANK: 1155832
Matrix: Solid
Associated Lab Samples:
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Nitrate as N
mg/kg
ND 4.9
03/13/15 15:40
LABORATORY CONTROL SAMPLE:
1155833
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Nitrate as N
mg/kg
50 50.2
100
80-120
MATRIX SPIKE SAMPLE:
1155835
92240158009 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Nitrate as N
mg/kg
ND 71.7
61.0
85 80-120 H3
SAMPLE DUPLICATE: 1155834
92240158009 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Nitrate as N
mg/kg
ND ND
20 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc.. Page 86 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
PaagQm 16fy IN e. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: WETA/44534
Analysis Method:
EPA 9056
QC Batch Method: EPA 9056
Analysis Description:
9056 IC Anions
Associated Lab Samples: 92240158005, 92240158006, 92240158007, 92240158008
METHOD BLANK: 1156874
Matrix: Solid
Associated Lab Samples:
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Nitrate as N
mg/kg
ND 5.0
03/14/15 18:25
LABORATORY CONTROL SAMPLE:
1156875
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Nitrate as N
mg/kg
50 52.2
104
80-120
MATRIX SPIKE SAMPLE:
1156877
92240158005 Spike
MS
MS % Rec
Parameter
Units
Result Conc.
Result
% Rec Limits Qualifiers
Nitrate as N
mg/kg
ND 54.4
55.7
102 80-120 H3
SAMPLE DUPLICATE: 1156876
92240158005 Dup
Max
Parameter
Units
Result Result
RPD
RPD Qualifiers
Nitrate as N
mg/kg
ND ND
20 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc.. Page 87 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
PaagQm 16fy IN e. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15030202
Pace Project No.: 92240158
QC Batch: WETA/27544
Analysis Method: EPA 9060
QC Batch Method: EPA 9060
Analysis Description: 9060 TOC Average
Associated Lab Samples: 92240158001, 92240158002,
92240158003, 92240158004, 92240158005, 92240158006, 92240158007,
92240158008,92240158009,92240158010
METHOD BLANK: 1126431
Matrix: Solid
Associated Lab Samples:
Blank Reporting
Parameter Units
Result Limit Analyzed Qualifiers
Mean Total Organic Carbon mg/kg
ND 600 03/13/15 09:23
LABORATORY CONTROL SAMPLE: 1126432
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Mean Total Organic Carbon mg/kg
120000 112000 93 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1126433 1126434
MS MSD
92240158001
Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Mean Total Organic Carbon mg/kg 3750
9270 9280 13300 13100 104 101 50-150 2 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc..
Page 88 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
Padg"ifYINe. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: J15030202
Pace Project No.: 92240158
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A
Pace Analytical Services - Asheville
PASI-G
Pace Analytical Services - Green Bay
PASI-M
Pace Analytical Services - Minneapolis
PASI-O
Pace Analytical Services - Ormond Beach
ANALYTE QUALIFIERS
B Analyte was detected in the associated method blank.
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
D4 Sample was diluted due to the presence of high levels of target analytes.
H1 Analysis conducted outside the EPA method holding time.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold TN accreditation for this parameter.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
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aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
Padg"WfY.Nie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: J15030202
Pace Project No.: 92240158
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92240158001
2015006511
EPA
3050
MPRP/23094
EPA
6010
ICP/14133
92240158002
2015006512
EPA
3050
MPRP/23094
EPA
6010
ICP/14133
92240158003
2015006514
EPA
3050
MPRP/23094
EPA
6010
ICP/14133
92240158004
2015006518
EPA
3050
MPRP/23094
EPA
6010
ICP/14133
92240158005
2015006520
EPA
3050
MPRP/23094
EPA
6010
ICP/14133
92240158006
2015006523
EPA
3050
MPRP/23094
EPA6010
ICP/14133
92240158007
2015006515
EPA
3050
MPRP/23094
EPA
6010
ICP/14133
92240158008
2015006516
EPA
3050
MPRP/23094
EPA
6010
ICP/14133
92240158009
2015006521
EPA
3050
MPRP/23094
EPA
6010
ICP/14133
92240158010
2015006524
EPA
3050
MPRP/23094
EPA
6010
ICP/14133
92240158001
2015006511
EPA
3050
MPRP/23095
EPA 6020
ICPM/9420
92240158002
2015006512
EPA
3050
MPRP/23095
EPA 6020
ICPM/9420
92240158003
2015006514
EPA
3050
MPRP/23095
EPA 6020
ICPM/9420
92240158004
2015006518
EPA
3050
MPRP/23095
EPA 6020
ICPM/9420
92240158005
2015006520
EPA
3050
MPRP/23095
EPA 6020
ICPM/9420
92240158006
2015006523
EPA
3050
MPRP/23095
EPA 6020
ICPM/9420
92240158007
2015006515
EPA
3050
MPRP/23095
EPA 6020
ICPM/9420
92240158008
2015006516
EPA
3050
MPRP/23095
EPA 6020
ICPM/9420
92240158009
2015006521
EPA
3050
MPRP/23095
EPA 6020
ICPM/9420
92240158010
2015006524
EPA
3050
MPRP/23095
EPA 6020
ICPM/9420
92240158011
2015006513
EPA
3020
MPRP/52931
EPA 6020A
ICPM/23462
92240158012
2015006517
EPA
3020
MPRP/52931
EPA 6020A
ICPM/23462
92240158013
2015006519
EPA
3020
MPRP/52931
EPA 6020A
ICPM/23462
92240158014
2015006522
EPA
3020
MPRP/52931
EPA 6020A
ICPM/23462
92240158015
2015006525
EPA
3020
MPRP/52931
EPA 6020A
ICPM/23462
92240158016
2015006515 SPLP
EPA
3020
MPRP/53205
EPA 6020A
ICPM/23572
92240158017
2015006516 SPLP
EPA
3020
MPRP/53205
EPA 6020A
ICPM/23572
92240158018
2015006521 SPLP
EPA
3020
MPRP/53205
EPA 6020A
ICPM/23572
92240158019
2015006524 SPLP
EPA
3020
MPRP/53205
EPA 6020A
ICPM/23572
92240158011
2015006513
EPA
7470
MERP/12966
EPA 7470
MERC/15051
92240158012
2015006517
EPA
7470
MERP/12966
EPA 7470
MERC/15051
92240158013
2015006519
EPA
7470
MERP/12966
EPA 7470
MERC/15051
92240158014
2015006522
EPA
7470
MERP/12966
EPA 7470
MERC/15051
92240158015
2015006525
EPA
7470
MERP/12966
EPA 7470
MERC/15051
92240158016
2015006515 SPLP
EPA
7470
MERP/13071
EPA 7470
MERC/15183
92240158017
2015006516 SPLP
EPA
7470
MERP/13071
EPA 7470
MERC/15183
92240158018
2015006521 SPLP
EPA
7470
MERP/13071
EPA 7470
MERC/15183
92240158019
2015006524 SPLP
EPA
7470
MERP/13071
EPA 7470
MERC/15183
92240158001
2015006511
EPA
7471
MERP/5474
EPA 7471
MERC/5464
92240158002
2015006512
EPA
7471
MERP/5474
EPA 7471
MERC/5464
92240158003
2015006514
EPA
7471
MERP/5474
EPA 7471
MERC/5464
92240158004
2015006518
EPA
7471
MERP/5474
EPA 7471
MERC/5464
92240158005
2015006520
EPA
7471
MERP/5474
EPA 7471
MERC/5464
92240158006
2015006523
EPA
7471
MERP/5474
EPA 7471
MERC/5464
92240158007
2015006515
EPA
7471
MERP/5474
EPA 7471
MERC/5464
92240158008
2015006516
EPA
7471
MERP/5474
EPA 7471
MERC/5464
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/30/2015 02:56 PM without the written consent of Pace Analytical Services, Inc.. Page 90 of 94

acmnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
Padg"rwyfie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: J15030202
Pace Project No.: 92240158
Lab ID Sample ID QC Batch Method QC Batch
92240158009
2015006521
EPA 7471
MERP/5474
92240158010
2015006524
EPA 7471
MERP/5474
92240158001
2015006511
ASTM D2974-87
PMST/3347
92240158002
2015006512
ASTM D2974-87
PMST/3347
92240158003
2015006514
ASTM D2974-87
PMST/3347
92240158004
2015006518
ASTM D2974-87
PMST/3347
92240158005
2015006520
ASTM D2974-87
PMST/3347
92240158006
2015006523
ASTM D2974-87
PMST/3347
92240158007
2015006515
ASTM D2974-87
PMST/3347
92240158008
2015006516
ASTM D2974-87
PMST/3347
92240158009
2015006521
ASTM D2974-87
PMST/3347
92240158010
2015006524
ASTM D2974-87
PMST/3347
92240158001
2015006511
EPA 9045
WET/36142
92240158002
2015006512
EPA 9045
WET/36142
92240158003
2015006514
EPA 9045
WET/36142
92240158004
2015006518
EPA 9045
WET/36142
92240158005
2015006520
EPA 9045
WET/36142
92240158006
2015006523
EPA 9045
WET/36142
92240158007
2015006515
EPA 9045
WET/36142
92240158008
2015006516
EPA 9045
WET/36142
92240158009
2015006521
EPA 9045
WET/36142
92240158010
2015006524
EPA 9045
WET/36142
92240158007
2015006515
EPA 300.0
WETA/22270
92240158008
2015006516
EPA 300.0
WETA/22270
92240158009
2015006521
EPA 300.0
WETA/22270
92240158010
2015006524
EPA 300.0
WETA/22270
92240158007
2015006515
EPA 353.2
WETA/22256
92240158008
2015006516
EPA 353.2
WETA/22256
92240158009
2015006521
EPA 353.2
WETA/22256
92240158010
2015006524
EPA 353.2
WETA/22256
92240158007
2015006515
SM 4500-CI-E
WETA/22273
92240158008
2015006516
SM 4500-CI-E
WETA/22273
92240158009
2015006521
SM 4500-CI-E
WETA/22273
92240158010
2015006524
SM 4500-CI-E
WETA/22273
92240158001
2015006511
EPA 9056
WETA/44508
92240158002
2015006512
EPA 9056
WETA/44508
92240158003
2015006514
EPA 9056
WETA/44508
92240158004
2015006518
EPA 9056
WETA/44508
92240158005
2015006520
EPA 9056
WETA/44533
92240158006
2015006523
EPA 9056
WETA/44533
92240158007
2015006515
EPA 9056
WETA/44533
92240158008
2015006516
EPA 9056
WETA/44533
92240158009
2015006521
EPA 9056
WETA/44515
92240158010
2015006524
EPA 9056
WETA/44515
Date: 03/30/2015 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical Method
EPA 7471
EPA 7471
Analytical
Batch
MERC/5464
MERC/5464
Page 91 of 94

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
PaagOP, b fYik�e. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: J15030202
Pace Project No.: 92240158
Lab ID
Sample ID
QC Batch Method
QC Batch
92240158001
2015006511
EPA 9056
WETA/44509
92240158002
2015006512
EPA 9056
WETA/44509
92240158003
2015006514
EPA 9056
WETA/44509
92240158004
2015006518
EPA 9056
WETA/44509
92240158005
2015006520
EPA 9056
WETA/44534
92240158006
2015006523
EPA 9056
WETA/44534
92240158007
2015006515
EPA 9056
WETA/44534
92240158008
2015006516
EPA 9056
WETA/44534
92240158009
2015006521
EPA 9056
WETA/44514
92240158010
2015006524
EPA 9056
WETA/44514
92240158001
2015006511
EPA 9060
WETA/27544
92240158001
2015006511
EPA 9060
WETA/27545
92240158002
2015006512
EPA 9060
WETA/27544
92240158002
2015006512
EPA 9060
WETA/27545
92240158003
2015006514
EPA 9060
WETA/27544
92240158003
2015006514
EPA 9060
WETA/27545
92240158004
2015006518
EPA 9060
WETA/27544
92240158004
2015006518
EPA 9060
WETA/27545
92240158005
2015006520
EPA 9060
WETA/27544
92240158005
2015006520
EPA 9060
WETA/27545
92240158006
2015006523
EPA 9060
WETA/27544
92240158006
2015006523
EPA 9060
WETA/27545
92240158007
2015006515
EPA 9060
WETA/27544
92240158007
2015006515
EPA 9060
WETA/27545
92240158008
2015006516
EPA 9060
WETA/27544
92240158008
2015006516
EPA 9060
WETA/27545
92240158009
2015006521
EPA 9060
WETA/27544
92240158009
2015006521
EPA 9060
WETA/27545
92240158010
2015006524
EPA 9060
WETA/27544
92240158010
2015006524
EPA 9060
WETA/27545
Date: 03/30/2015 02:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical Method
Analytical
Batch
Page 92 of 94

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Anions: Cl, Nitrate-N, SO4 Sediment Specific Parameters: %Solids CEC, Particle Size Distribution, Redox Potential