NC0003433_J15070080 Report_20150902

Lab
DUI E Analytical Laboratory APagel1aof35
ENERGY
Order Number:
Project Name:
Customer Name(s):
Customer Address:
Lab Contact:
Report Authorized By:
(Signature)
Program Comments:
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
J15070080
CAPE FEAR - AB GW ASSESSMENT WATER
Tim Hunsucker, Chris Suttell, Kathy Webb, John Toepfer
Mary Ann Ogle Phone: [phone]
✓/
mary.ogle@duke-
energy.com
2015.07.13.13 15:05:41-04'00' Date:
Mary Ann Ogle
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
7/13/2015
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Collection
Sample ID Plant/Station Date and Time
Collected By
Sample Description
2015022043
Cape Fear
01-Jul-15 10:25 AM
Illegible
MW-10
2015022046
Cape Fear
01-Jul-15 12:12 PM
Illegible
MW-11
2015022047
Cape Fear
01-Jul-15 8:10 AM
Illegible
Filter Blank
2015022048
Cape Fear
01-Jul-15 8:10 AM
Illegible
Equipment Blank
4 Total Samples
Analytical Lab
Page 2 of 35

Analytical Lab
Page 3 of 35
Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals 0 Yes ❑ No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes 0 No
All laboratory QA/QC requirements are acceptable. 0 Yes ❑ No
Report Sections Included:
E%-'] Job Summary Report
❑� Sample Identification
Technical Validation of Data Package
❑� Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
❑d Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
❑� Chain of Custody
❑� Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Mary Ann Ogle Date: 7/13/2015

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15070080
Site: MW-10
Collection Date: 01-Jul-15 10:25 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
M2 0.01
INORGANIC IONS BY IC
Chloride
23
mg/L
1
Sulfate
610
mg/L
10
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.008
mg/L
0.005
Barium (Ba)
0.028
mg/L
0.005
Boron (B)
0.892
mg/L
0.05
Iron (Fe)
2.54
mg/L
0.01
Manganese (Mn)
11.7
mg/L
0.005
Strontium (Sr)
1.40
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
158
mg/L
0.1
Magnesium (Mg)
50.9
mg/L
0.005
Potassium (K)
2.72
mg/L
0.1
Sodium (Na)
34.6
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.027
mg/L
0.005
Barium (Ba)
0.029
mg/L
0.005
Boron (B)
0.922
mg/L
0.05
Iron (Fe)
2.80
mg/L
0.01
Manganese (Mn)
12.5
mg/L
0.005
Strontium (Sr)
1.46
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015022043
Matrix: GW WW
Analytical Lab
Page 4 of 35
DF
Method
Analysis Date/Time
Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
07/06/2015 10:31
LSTARLI
10
EPA 300.0
07/07/2015 21:49
BGN9034
100
EPA 300.0
07/07/2015 21:49
BGN9034
1
EPA 245.1
07/07/2015 12:46
ACPAYNE
1
EPA 245.1
07/07/2015 13:09
ACPAYNE
1
EPA 200.7
07/06/2015 10:32
FCJORDA
1
EPA 200.7
07/06/2015 10:32
FCJORDA
1
EPA 200.7
07/06/2015 10:32
FCJORDA
1
EPA 200.7
07/06/2015 10:32
FCJORDA
1
EPA 200.7
07/06/2015 10:32
FCJORDA
1
EPA 200.7
07/06/2015 10:32
FCJORDA
1
EPA 200.7
07/06/2015 10:32
FCJORDA
10
EPA 200.7
07/06/2015 12:44
FCJORDA
1
EPA 200.7
07/06/2015 12:44
FCJORDA
1
EPA 200.7
07/06/2015 12:44
FCJORDA
1
EPA 200.7
07/06/2015 12:44
FCJORDA
1
EPA 200.7
07/07/2015 10:46
MHH7131
1
EPA 200.7
07/07/2015 10:46
MHH7131
1
EPA 200.7
07/07/2015 10:46
MHH7131
1
EPA 200.7
07/07/2015 10:46
MHH7131
1
EPA 200.7
07/07/2015 10:46
MHH7131
1
EPA 200.7
07/07/2015 10:46
MHH7131
1
EPA 200.7
07/07/2015 10:46
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15070080
Site: MW-10
Collection Date: 01-Jul-15 10:25 AM
Analyte
Result
Units Qualifiers
RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
19.8
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
3.49
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
21.0
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
3.55
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
0.366
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
1100
mg/L
25
Total Carbon
TOC
1.0
mg/L
0.1
TOTAL SUSPENDED SOLIDS
TSS
< 5
mg/L
5
Sample #: 2015022043
Matrix: GW WW
Analytical Lab
Page 5 of 35
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
07/07/2015 10:15
JAHERMA
1
EPA 200.8
07/07/2015 10:15
JAHERMA
1
EPA 200.8
07/07/2015 10:15
JAHERMA
1
EPA 200.8
07/07/2015 10:15
JAHERMA
1
EPA 200.8
07/07/2015 10:15
JAHERMA
1
EPA 200.8
07/07/2015 10:15
JAHERMA
1
EPA 200.8
07/07/2015 10:15
JAHERMA
1
EPA 200.8
07/07/2015 10:15
JAHERMA
1
EPA 200.8
07/07/2015 10:15
JAHERMA
1
EPA 200.8
07/07/2015 10:15
JAHERMA
1
EPA 200.8
07/07/2015 10:15
JAHERMA
1
EPA 200.8
07/07/2015 10:15
JAHERMA
1
EPA 200.8
07/07/2015 10:15
JAHERMA
1
EPA 200.8
07/07/2015 08:01
JAHERMA
1
EPA 200.8
07/07/2015 08:01
JAHERMA
1
EPA 200.8
07/07/2015 08:01
JAHERMA
1
EPA 200.8
07/07/2015 08:01
JAHERMA
1
EPA 200.8
07/07/2015 08:01
JAHERMA
1
EPA 200.8
07/07/2015 08:01
JAHERMA
1
EPA 200.8
07/07/2015 08:01
JAHERMA
1
EPA 200.8
07/07/2015 08:01
JAHERMA
1
EPA 200.8
07/07/2015 08:01
JAHERMA
1
EPA 200.8
07/07/2015 08:01
JAHERMA
1
EPA 200.8
07/07/2015 08:01
JAHERMA
1
EPA 200.8
07/07/2015 08:01
JAHERMA
1
EPA 200.8
07/07/2015 08:01
JAHERMA
Vendor Method V_SHEALY
Vendor Method V_ELE1
1 SM2540C 07/06/201514:58 AGIBBS5
1 SM5310C/EPA9060A 07/06/201513:39 TJA7067
1 SM2540D 07/06/2015 08:00 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15070080
Site: MW-11
Collection Date: 01-Jul-15 12:12 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
22
mg/L
1
Sulfate
200
mg/L
5
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.006
mg/L
0.005
Barium (Ba)
0.058
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
2.75
mg/L
0.01
Manganese (Mn)
0.792
mg/L
0.005
Strontium (Sr)
0.532
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
53.5
mg/L
0.01
Magnesium (Mg)
36.9
mg/L
0.005
Potassium (K)
0.486
mg/L
0.1
Sodium (Na)
48.5
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.076
mg/L
0.005
Barium (Ba)
0.059
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
3.81
mg/L
0.01
Manganese (Mn)
0.912
mg/L
0.005
Strontium (Sr)
0.535
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015022046
Matrix: GW WW
Analytical Lab
Page 6 of 35
DF Method Analysis Date/Time Analyst
Vendor Method V_SHEALY
1
EPA 353.2
07/06/2015 10:35
LSTARLI
10
EPA 300.0
07/07/2015 22:07
BGN9034
50
EPA 300.0
07/07/2015 22:07
BGN9034
1
EPA 245.1
07/07/2015 12:48
ACPAYNE
1
EPA 245.1
07/07/2015 13:02
ACPAYNE
1
EPA 200.7
07/06/2015 10:36
FCJORDA
1
EPA 200.7
07/06/2015 10:36
FCJORDA
1
EPA 200.7
07/06/2015 10:36
FCJORDA
1
EPA 200.7
07/06/2015 10:36
FCJORDA
1
EPA 200.7
07/06/2015 10:36
FCJORDA
1
EPA 200.7
07/06/2015 10:36
FCJORDA
1
EPA 200.7
07/06/2015 10:36
FCJORDA
1
EPA 200.7
07/06/2015 12:51
FCJORDA
1
EPA 200.7
07/06/2015 12:51
FCJORDA
1
EPA 200.7
07/06/2015 12:51
FCJORDA
1
EPA 200.7
07/06/2015 12:51
FCJORDA
1
EPA 200.7
07/07/2015 10:50
MHH7131
1
EPA 200.7
07/07/2015 10:50
MHH7131
1
EPA 200.7
07/07/2015 10:50
MHH7131
1
EPA 200.7
07/07/2015 10:50
MHH7131
1
EPA 200.7
07/07/2015 10:50
MHH7131
1
EPA 200.7
07/07/2015 10:50
MHH7131
1
EPA 200.7
07/07/2015 10:50
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15070080
Site: MW-11
Collection Date: 01-Jul-15 12:12 PM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
4.50
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
0.372
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
1.03
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
4.23
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
0.867
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
550
mg/L
25
Total Carbon
TOC
5.8
mg/L
0.2
TOTAL SUSPENDED SOLIDS
TSS
5.0
mg/L
5
Sample #: 2015022046
Matrix: GW WW
Analytical Lab
Page 7 of 35
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
07/07/2015 10:35
JAHERMA
1
EPA 200.8
07/07/2015 10:35
JAHERMA
1
EPA 200.8
07/07/2015 10:35
JAHERMA
1
EPA 200.8
07/07/2015 10:35
JAHERMA
1
EPA 200.8
07/07/2015 10:35
JAHERMA
1
EPA 200.8
07/07/2015 10:35
JAHERMA
1
EPA 200.8
07/07/2015 10:35
JAHERMA
1
EPA 200.8
07/07/2015 10:35
JAHERMA
1
EPA 200.8
07/07/2015 10:35
JAHERMA
1
EPA 200.8
07/07/2015 10:35
JAHERMA
1
EPA 200.8
07/07/2015 10:35
JAHERMA
1
EPA 200.8
07/07/2015 10:35
JAHERMA
1
EPA 200.8
07/07/2015 10:35
JAHERMA
1
EPA 200.8
07/07/2015 09:11
JAHERMA
1
EPA 200.8
07/07/2015 09:11
JAHERMA
1
EPA 200.8
07/07/2015 09:11
JAHERMA
1
EPA 200.8
07/07/2015 09:11
JAHERMA
1
EPA 200.8
07/07/2015 09:11
JAHERMA
1
EPA 200.8
07/07/2015 09:11
JAHERMA
1
EPA 200.8
07/07/2015 09:11
JAHERMA
1
EPA 200.8
07/07/2015 09:11
JAHERMA
1
EPA 200.8
07/07/2015 09:11
JAHERMA
1
EPA 200.8
07/07/2015 09:11
JAHERMA
1
EPA 200.8
07/07/2015 09:11
JAHERMA
1
EPA 200.8
07/07/2015 09:11
JAHERMA
1
EPA 200.8
07/07/2015 09:11
JAHERMA
Vendor Method V_SHEALY
Vendor Method V_ELE1
1 SM2540C 07/06/201514:58 AGIBBS5
2 SM5310C/EPA9060A 07/06/201513:39 TJA7067
1 SM2540D 07/06/2015 08:00 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15070080
Site: Filter Blank
Collection Date: 01-Jul-15 8:10 AM
Analyte
Result
Units
Qualifiers RDL
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
0.006
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015022047
Matrix: GW WW
Analytical Lab
Page 8 of 35
DF
Method
Analysis Date/Time
Analyst
1
EPA 245.1
07/07/2015 13:11
ACPAYNE
1
EPA 200.7
07/06/2015 10:39
FCJORDA
1
EPA 200.7
07/06/2015 10:39
FCJORDA
1
EPA 200.7
07/06/2015 10:39
FCJORDA
1
EPA 200.7
07/06/2015 10:39
FCJORDA
1
EPA 200.7
07/06/2015 10:39
FCJORDA
1
EPA 200.7
07/06/2015 10:39
FCJORDA
1
EPA 200.7
07/06/2015 10:39
FCJORDA
1
EPA 200.8
07/07/2015 10:56
JAHERMA
1
EPA 200.8
07/07/2015 10:56
JAHERMA
1
EPA 200.8
07/07/2015 10:56
JAHERMA
1
EPA 200.8
07/07/2015 10:56
JAHERMA
1
EPA 200.8
07/07/2015 10:56
JAHERMA
1
EPA 200.8
07/07/2015 10:56
JAHERMA
1
EPA 200.8
07/07/2015 10:56
JAHERMA
1
EPA 200.8
07/07/2015 10:56
JAHERMA
1
EPA 200.8
07/07/2015 10:56
JAHERMA
1
EPA 200.8
07/07/2015 10:56
JAHERMA
1
EPA 200.8
07/07/2015 10:56
JAHERMA
1
EPA 200.8
07/07/2015 10:56
JAHERMA
1
EPA 200.8
07/07/2015 10:56
JAHERMA

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15070080
Site: Equipment Blank
Collection Date: 01-Jul-15 8:10 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
< 0.1
mg/L
0.1
Sulfate
< 0.1
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
UNDIGESTED METALS BY lCP
Calcium (Ca)
0.015
mg/L
0.01
Magnesium (Mg)
< 0.005
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
< 0.05
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015022048
Matrix: GW WW
Analytical Lab
Page 9 of 35
DF Method Analysis Date/Time Analyst
Vendor Method V_SHEALY
1 EPA 353.2
07/06/2015 10:37
LSTARLI
1 EPA 300.0
07/07/2015 20:20
BGN9034
1 EPA 300.0
07/07/2015 20:20
BGN9034
1 EPA 245.1
07/07/2015 12:50
ACPAYNE
1 EPA 200.7
07/06/2015 12:55
FCJORDA
1 EPA 200.7
07/06/2015 12:55
FCJORDA
1 EPA 200.7
07/06/2015 12:55
FCJORDA
1 EPA 200.7
07/06/2015 12:55
FCJORDA
1 EPA 200.7
07/07/2015 10:55
MHH7131
1 EPA 200.7
07/07/2015 10:55
MHH7131
1 EPA 200.7
07/07/2015 10:55
MHH7131
1 EPA 200.7
07/07/2015 10:55
MHH7131
1 EPA 200.7
07/07/2015 10:55
MHH7131
1 EPA 200.7
07/07/2015 10:55
MHH7131
1 EPA 200.7
07/07/2015 10:55
MHH7131
1 EPA 200.8
07/07/2015 09:18
JAHERMA
1 EPA 200.8
07/07/2015 09:18
JAHERMA
1 EPA 200.8
07/07/2015 09:18
JAHERMA
1 EPA 200.8
07/07/2015 09:18
JAHERMA
1 EPA 200.8
07/07/2015 09:18
JAHERMA
1 EPA 200.8
07/07/2015 09:18
JAHERMA
1 EPA 200.8
07/07/2015 09:18
JAHERMA
1 EPA 200.8
07/07/2015 09:18
JAHERMA
1 EPA 200.8
07/07/2015 09:18
JAHERMA
1 EPA 200.8
07/07/2015 09:18
JAHERMA
1 EPA 200.8
07/07/2015 09:18
JAHERMA
1 EPA 200.8
07/07/2015 09:18
JAHERMA
1 EPA 200.8
07/07/2015 09:18
JAHERMA
METHANE - (Analysis Performed by Shealy Labs
Methane (CH4) Complete
Vendor Method V_SHEALY

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15070080
Site: Equipment Blank
Collection Date: 01-Jul-15 8:10 AM
Analyte Result Units Qualifiers RDL DF
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete
TOTAL DISSOLVED SOLIDS
TDS < 25 mg/L 25 1
Total Carbon
Sample #: 2015022048
Matrix: GW WW
Analytical Lab
Page 10 of 35
Method Analysis Date/Time Analyst
Vendor Method
V_ELE1
SM2540C 07/06/201514:58 AGIBBS5
TOC 0.226 mg/L 0.1 1 SM5310C/EPA9060A 07/06/201513:39 TJA7067
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L 5 1 SM2540D 07/06/2015 08:00 AGIBBS5
Qualifiers:
M2 Matrix spike recovery was Low: the associated Laboratory Control Spike (LCS) was acceptable.

Analytical Lab
Page 11 of 35
Element One inc.
6319-D Carolina Beach Rd.
Wilmington, NC 28412
(Tone: 910 793-0128
Fax: [phone]
[e-mail]
REPORT OF ANALYSES
Duke Energy
July 8, 2015
Laboratory Services
Client Project Name AB GW Assessment water (wells) Cape Fear
13339 Hagers Ferry Road Bid.
MG03A Client Project Number J15070080
Huntersville, NC 28078
PO Number
Sample Matrix GW WW
Sample Type Grab
Date Received
07/07/2015
Date Analyzed 07/07/2015
Method SM 4500 S2_ D
Time Received
1647
Delivered by FedEx
Received by
PDS
eOne ID Duke Energy ID
Parameter Result Unit Dil
DL Date
Time
Sampled
Sampled
25259-1
Equipment Blank
Sulfide
< 0.1
mg/L 1
0.1
07/01/15
0810
25259-2"
MW-10
Sulfide
< 0.2
mg/L 2
0.1
07/01/15
1025
25259-3
MW-11
Sulfide
< 0.1
mg/L 1
0.1
07/01/15
1212
"Sample spike recovery outside of QA limits of 85-115%; dilution necessary to meet laboratory QA limits.
Ken Smith, Laboratory Director
25259 Duke Report Packet Compiled by�AS
NC Certifications: DW 37788 and DWQ DENR 604

Analytical Lab
Page 12 of 35
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e ementOne SAMPLE SUBMISSION FORM
TAT 5 BD
Hold Time Expiration 07.08.15 @ 0810
Client: Duke Energy
LIMS No J15070080
Project ID HF Lee
Analytical Lab
Lab Ilyge
12g2tq
Analysis Due Date
07.07.15
Report Due Date
07.10.15
Date Rec:
07.07.15
Time Rec:
1647
Rec By
PDS
H >9 Ye No
I Tem <_ 6°C Yes No
Ref. Method:
SM4500 S2 D
If No, Record
I If No, Record
Sample Identification & Collection Information
Lab ID Client ID Collection Date Collection Time Analysis Requested
1 Equipment Blank 07.01.15 0810 ulfi' e
2 MW-10 07.01.15 1025
3 MW-11 07.01.15 1212
NOTE for Sulfide The MS/MSD spike should approximate 2 to 3 times the sample concentration. If no sulfide detected
at 100 pg/L spike the sample to render the final spike concentration at — 500 pg/L

Analytical Lab
Page 14 of 35
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
Na2S•9H2O Lot #
40721
UNITS OF ANSWER
ug/mL
DETECTION LIMIT u
1.000
CLIENT:
Lab ID#
Duke
25259
SPK LEVEL u
MAX ALIQUOT
5
10.00
Date:
07/08/15
STANDARD conc(ppm)
X
Time Analysis Begun
17;00
Cal Std Lot: SD-17-3
10
Time Analysis Ended
18:30
QC Std Lot: SD-17-4
10
Analyst:
KAM
STD ABSORPTION
Y
X
Y
e.00
ug STD
SOLUTION
STD
ABS
°'°°
°.
0e00
0.00
100
2.50
5.00
7.50
10.00
0.000
0.094
0.226io
0.430
0.61
0.773
T 100
Y500
04M
�--�-2.50
0100
0
Q0 000 2m 400 600 aee 000 200
x
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL PREP
ANALYZED VOL in mL
Sloe 0.07741978+
Correlation 0.998213974'
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
1 0.0000
10
10
10
<
0
Std. B. 1.00
0.098
0.8156
10
10
10
<
81.56%
1
Std. B. 2.50
0.229
2.6052
10
10
10
0.261
104.21 %
2.5
Std. B. 5.00
0.432
5.3784
10
10
10
0.538
107.57%
5
Std. B. 7.50
0.617
7.9057
10
10
10
0.791
105.41 %
7.5
Std. B. 10.00
0.765
9.9276
10
10
10
0.993
99.28%
10
LRB
-0.001
0.0000
10
10
10
<
0
LRB SPK
0.446
5.5697
10
10
10
0.557
112%
5.0
QC
0.451
5.6380
10
10
10
0.564
113%
5.0
25259-1
-0.002
0.0000
10
10
10
0.542
25259-1 s k
0.435
5.4194
10
10
10
108%
5.0
25259-2
-0.002
0.0000
10
10
10
<
25259-2 s k
0.315
3.7801
10
10
10
0.378
76%
5.0
25259-3
0.001
-0.5096
10
10
10
< 0.1
25259-3 dup
0.002
-0.4959
10
10
10
25259-3 s k
0.361
1 4.4085
10
10
10
0.441
88%
5.0
25259-2
0.000
0.0000
10
10
5
1.002
25259-2 s k
0.405
5.0096
10
10
5
100%
5.0
Blank
0.000
0.0000
10
10
10
<
QC
0.449
5.6107
10
10
10
0.561
112%
5.0
Submitted for QA/QC- Date: 07/07/15
By: (Print)
KAM
(sign):
l�

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
Project Name: AB GW Assessment Water - Cape Fear
Project Number:J15070080
Lot Number:QG07015
Date Completed:07/13/2015
I&e /� 4"e�
Grant Wilton
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Shealy Environmental Services, Inc. Page: 1 of 10
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Duke Energy
Lot Number: QG07015
Project Name: AB GW Assessment Water - Cape Fear
Project Number: J15070080
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 10
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QG07015
Project Name: AB GW Assessment Water - Cape Fear
Project Number: J15070080
Sample Number Sample ID Matrix Date Sampled Date Received
001 2015022043 Aqueous 07/01/20151025 07/07/2015
002 2015022046 Aqueous 07/01/20151212 07/07/2015
003 2015022048 Aqueous 07/01/2015 0810 07/07/2015
(3 samples)
Shealy Environmental Services, Inc. Page: 3 of 10
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SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QG07015
Project Name: AB GW Assessment Water - Cape Fear
Project Number: J15070080
Sample Sample ID Matrix Parameter Method Result Q Units Page
001
2015022043
Aqueous
Alkalinity
SM 2320B-
120
mg/L
5
001
2015022043
Aqueous
Bicarbonate Alkalinity
SM 2320B-
120
mg/L
5
001
2015022043
Aqueous
Methane
RSK - 175
17
ug/L
6
002
2015022046
Aqueous
Alkalinity
SM 2320B-
160
mg/L
7
002
2015022046
Aqueous
Bicarbonate Alkalinity
SM 2320B-
160
mg/L
7
002
2015022046
Aqueous
Methane
RSK - 175
460
ug/L
8
(6 detections)
Shealy Environmental Services, Inc. Page: 4 of 10
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QG07015-001
Description: 2015022043 Matrix: Aqueous
Date Sampled:07/01/2015 1025 Project Name: AB GW Assessment Water -
Date Received:07/07/2015 Project Number: J15070080
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 (Alkalinity) SM 2320B-2011 1 07/10/2015 1159 HMA 79330
1 (Bicarbonate ) SM 2320B-2011 1 07/10/2015 1159 HMA
1 (Carbonate Al) SM 2320B-2011 1 07/10/2015 1159 HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
120
10
mg/L
2
Bicarbonate Alkalinity
SM 2320B-20
120
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QG07015-001
Description: 2015022043 Matrix: Aqueous
Date Sampled:07/01/2015 1025 Project Name: AB GW Assessment Water -
Date Received:07/07/2015 Project Number: J15070080
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 07/08/2015 1237 DCS 79090
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 17 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QG07015-002
Description: 2015022046 Matrix: Aqueous
Date Sampled:07/01/2015 1212 Project Name: AB GW Assessment Water -
Date Received:07/07/2015 Project Number: J15070080
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 (Alkalinity) SM 2320B-2011 1 07/10/2015 1205 HMA 79330
1 (Bicarbonate ) SM 2320B-2011 1 07/10/2015 1205 HMA
1 (Carbonate Al) SM 2320B-2011 1 07/10/2015 1205 HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
160
10
mg/L
2
Bicarbonate Alkalinity
SM 2320B-20
160
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QG07015-002
Description: 2015022046 Matrix: Aqueous
Date Sampled:07/01/2015 1212 Project Name: AB GW Assessment Water -
Date Received:07/07/2015 Project Number: J15070080
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 07/08/2015 1255 DCS 79090
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 460 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QG07015-003
Description: 2015022048 Matrix: Aqueous
Date Sampled:07/01/2015 0810 Project Name: AB GW Assessment Water -
Date Received:07/07/2015 Project Number: J15070080
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 (Alkalinity) SM 2320B-2011 1 07/10/2015 1227 HMA 79330
1 (Bicarbonate ) SM 2320B-2011 1 07/10/2015 1227 HMA
1 (Carbonate Al) SM 2320B-2011 1 07/10/2015 1227 HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
2
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QG07015-003
Description: 2015022048 Matrix: Aqueous
Date Sampled:07/01/2015 0810 Project Name: AB GW Assessment Water -
Date Received:07/07/2015 Project Number: J15070080
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 07/08/2015 1336 DCS 79090
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: QG07015
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Inorganic non-metals - MB
Sample ID: QQ79330-001 Matrix: Aqueous
Batch:79330
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 07/10/20151146
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QG07015
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Inorganic non-metals - LCS
Sample ID: QQ79330-002 Matrix: Aqueous
Batch:79330
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 95 1 95 90-110 07/10/20151152
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QG07015
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Inorganic non-metals - MS
Sample ID: QG07015-002MS Matrix: Aqueous
Batch:79330
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 160 100 240 1 75 70-130 07/10/20151214
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QG07015
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Inorganic non-metals - MSD
Sample ID: QG07015-002MD Matrix: Aqueous
Batch:79330
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Alkalinity 160 100 250 1 85 4.0 70-130 20 07/10/20151222
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QG07015
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane - MB
Sample ID: QQ79090-001 Matrix: Aqueous
Batch:79090
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 07/08/20151051
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QG07015
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane - LCS
Sample ID: QQ79090-002 Matrix: Aqueous
Batch:79090
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 110 1 74 70-130 07/08/20151009
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QG07015
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Methane - LCSD
Sample ID: QQ79090-003 Matrix: Aqueous
Batch:79090
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 110 1 74 0.69 70-130 30 07/08/20151024
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QG07015
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
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DactiunentHumber:F-AD-01 R lu�Daia:ftrlY7fl
Rini ion Number 17 Effx$ve 1rige. #U`34li
Sample Receipt Checklist (SRC.)
Client: Cooler luspccled h r:'date: r , �-r�c „ Lot 0.
Means of rcxipt: D SESI D Clicnt ❑ UP Q 1?fix [I Airbome hxp ZOT11e17
Yea
No
I. Were custody seals pTesent on the oaolc-?
Yes LJ
I No
NAE�
If cuglody seals wm preamt, wem they intsct and uab„t,kcn?
Cu lr--r ID.r )dginal tempentm upon receipt Ueri (ouriruled) tempmWxre upen rfteipt
_ f "S_'AI I', 1 c / . / . K,C 1 I "C I '1C
Mtflwd: ❑ Temperature Blank Against Battles TR Cmmn IDD: lit Gun Cmection P r:g,e °
1~ tfluA of 000lant2rWet lee ❑ Blue Tee ❑ Dry Ice j None
Yes ❑
N;r ❑
No 0-l'i4A7,14,
NA
3. If temperature of wiy cwler cxomded 6_0V. was Proect Il &mges notified?
FM notiGed by SRC, phone, nate (circle erne), other -
(For coolers re ccivcd via comme<rerdal courier, Phis arc to lrc notifled
im=gtcl ,
Yes
❑
is the ccrrn_mercia rnl.rief's packing Aip attached to this form?
5. Were proper (reel' shed.1rm&ted folled? -
Sa Warc &quipks rclin uisli.cd by client to C4mnrcreial cQvrter'?
Yes
ZI
nfo ❑
Ye1;
o
NA
°cs
No El
6. J Were yam lc TDs 'isted rot: the CDC'.?
7. Were .sam le IT s 1ilvd mall sample. contai
S. Was Collection elate & time listed an the 6 C?
Yes
liar
Yes 77
l4_t ❑
Yes
No ❑
9 _ Was w1leclurn date & time listed on all sample containers?
'es
Nia ❑
IT Did all container I*e] information (ID, date, time) a 1-ee with the COC?
Ycs
Pto El
11. Wore tests to be perfonned listed rin the C:OC?
Yes
No ❑
12. Did all lei arrive in the proper containers fnr tmoh legit?
k'1z,
No []
13. Did all wntaiAers arrive in 92212condition unlbtokca, lids oni etc_)?
Yes
Nn D
14. Was lauaw si m 1c vi3lume available`
Yes {]
Noy
15_ Were all samples received within 'A the bolding time cv 49 hu=, whichever
comes first?
16. Were xnv samples camai=s missin ?
Ycs
No
Ye fi ❑
No
17, Were there any_r=xum;s sam 1cs not t steci on COC? _
1 K W'em bubbles presemi ;, caestre" ('A'or 6arrn in drarnerer in -any VGA vials?
Ycs ❑
Nc E�
,lass ]
Yes ®
No 0
NA
19, Were all mt;Lals;' ,Gd'I-IW, nutrient samples received at a pH of <2?
Yes ❑
No ❑
NA
20. W= ail e, ide author sulfide s les received at ar >12?
YGs ❑
Nc, ❑
NA V
21. Were. all appticahl�e h'H3r T ;1�rcya�id�°phcmo14�0.2mgOL) �sarrrple� free 0
residual cblorinc?
Yes ❑
No ❑
NA
22. W= collcctim tcmpciramm documented on the 00C for NC saran les?
Yes ❑
No
NA (
23. Were client re marks,+relluests (ix, rcquastcd dilutions} 14+ S 41SD desiguatbas,
etc- -- oorractl' transcribed f-om the COC into the came t &mTlDn in LJMS'?
Yes ❑
Nto
24, Was the quote number used taken from the container label?
Sample Ptre+teirvataan (Nlwt be completed for cosy° sample(.) inctwTectly przserved or vs tth headspacc.)
Samplc(s) were received incorrectly preset'~`ml snd were adjusted
accardin I • in sample r iviia with St } T1NO3,nC1,NEi0i4) u* SIB #
S le s Vr'et'e ter:civecl %frith babbics ---fi mm In diameter.
Sacra lc s were received with TFtC >412 mkVL (If," 21 is No M
SC Drinking Water Crrsj ect Sample(s) pH N'ttilicd to be > 2 by Daie:
Sam l s we= not rcucived al, a pH of-2 and were adjusted accord ° using SR-4
Sample labels applied by ' G��c-ram Vunfwd tly, > ►gate; 1
CoTumunt`S:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

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