WQ0009267_Monitoring - 09-2023_20231121

Monitoring Report Submittal
Permit Number#*
Name of Facility:*
Month: * September
Report Information
Type *
Revised - GW-59
WQ0009267
City of Jacksonville WWTF
Confirmation Email Address: *
Name of Submitter: *
Signature:
Date of submittal:
Initial Review
Year:* 2023
Upload Document*
WQ0009267 September 2023 GW-59 REVISED 5.08MB
MW Report, VOCs Attached.pdf
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
[e-mail]
Amy Palaschak
11 /21 /2023
This will be filled in automatically
Reviewer: Wanda.Gerald

Is the project number correct?* W00009267
Is the monitoring report accepted?* Yes NO
Regional Office* Wilmington
Reviewer: _anonymous
Review Date: 11/22/2023

GW-59A COMPLIANCE REPORT' FORM Permit #_WQ0009267
(Submit one each monitoring period with GW-59 forms.)
1
Enter date monitoring results were due. (10/31/2023) Will this monitoring report (GW-59 and GW-59A) be
YES
NO
submitted after the established due date?
2
Was any required information missing on the GW-59 report forms?
YES
NO
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
Report was previously submitted online and rejected by [e-mail] on
11/07/2023 for "In correct—BIan k—and_or—year". The sample date on GW-59 for MW 8 has been
updated and all GW-59 forms are included in this resubmittal.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance.
4
Are any monitored constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells
individually with constituent(s) and concentrations) exceeding standards in the space provided below:
MW 3 — VOCs — Toluene 12.3 ug/L, p-Isopropyltoluene 24.0 ug/L
MW 14 — VOCs — Toluene 1.05 ug/L
MW 10 — TDS 575 mg/L
5
For the constituents identified in question 4 above, have standards been exceeded previously for the same
YES
NO
constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space
provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample
collection date for each occurrence (for the last two years).
MW3—12/2022 (Toluene 10.6 ug/L, p-Isopropyltoluene 18.8 ug/L), 3/2023 (Toluene 13.7 ug/L,
p-Isopropyltoluene 21.5 ug/L, Chloromethane 0.73 ug/L), 612023 (Toluene 19.5 ug/L, p-Isopropyltoluene
65.7)
MW10 — all TDS — 912021 (675 mg/L), 12/2021 (633 mg/L), 312022 (607.5 mg/L), 612022 (577 mg/L), 912022
(560.5 mg/L), 12/2022 (660 mg/L), 3/2023 (618.5 mg/L), 6/2023 (604.5)
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE
IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact
the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this groundwater
YES
NO
quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to
question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the
impact the waste disposal system is having at the review and compliance boundaries surrounding this facility.
Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties.
Discussed reoccurring issues with Helen Perez, NC DEQ and Geoff Kegley, NC DEQ at facility
inspection August 15, 2023. Placement of monitoring wells do not appear to be located at review or
compliance boundaries. NC DEQ recommends that we evaluate well locations and submit change
requests in the future permit modification.
g
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form
with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report (Compliance Report GW-59A) is true and complete to the best of my knowledge
11/16/2023
Signatui f Permittee(or Authorized Agent) Date
G W-59A 12/8/2003

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Please Print Clearly or Type
Facility Name: City of Jacksonville Land Treatment System
Permit Name (if different):
Facility Address: 716 Firetower Road
Jacksonville NC 28540 County Onslow
(City; (State) (Zip)
Contact Person: Amy Palaschak Telephone#: [phone]
Well Location/Site Name MW-1 No. of wells to be sampled: 17
PERMIT Number: Expiration Date: 7/31/2029
Non -Discharge W00009267 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
WELL ID NUMBER (from Permit): MW-1 Date sample collected: 9/28/2023
Well Depth: 16.6 ft. Well Diameter: 2 in.
Depth to Water Level 82546: 5.1 ft. below measuring point Screened Interval: 3 ft. to 13 ft.
Measuring Point is 3.2 ft. above land surface Relative M.P. Elevation: 1.9 ft.
Volume of water pumped/bailed before sampling: 5.52 gallons
Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
FIELD ANALYSES:
pH 00400: 5 units
Spec. Cond. 00094:
Odor 00085:
Appearance
(LABORATORY INFORMATION
Date sample analyzed: 9/28/2023 Laboratory Name: 1. Jacksonville 2. Environmental Chemists
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
Coliform: MF Fecal 31616
<1
/100mL
Nitrate (NO3) as N 00620 <0.02
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
(Note: Use MPN method for highly turbid samples)
Orthophosphate70507
issolved Solids:Total 70300
112
mg/L
Al -Aluminum 01105
pH (Lab) 00403
5.04
units
Ba - Barium 01007
TOC 00680
10.2
mg/L
Ca - Calcium 00916
Chloride 00940
53
mg/L
Cd - Cadmium 01027
Arsenic 01002
ug/L
Chromium: Total 01034
Grease and Oils 00552
mg/L
Cu - Copper 01042
Phenol 32730
ug/L
Fe - Iron 01045
Sulfate 00945
18
mg/L
Hg - Mercury 71900
pecific Conductance 00095
µMhos
K - Potassium 00937
Total Ammonia 00610
<0.2
mg/L
Mg - Magnesium 00927
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
TKN as N 00625
mg/L
Ni - Nickel 01067
mg/L
mg/L
mg/L
mg/L
mg/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
Pb - Lead 01051
Zn - Zinc 01092
Temp. 000l o: 21.3 °C
µMhos
Certification No. 1. 128 2. 94
ug/L
mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ® Yes (1) ❑ No (0)
VOC 7873 , method # SM 6200C
, method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
If WELL
WAS
DRY at
time of
sampling,
check
here:❑

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH,,NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
(City( (State)
(Zip)
X Spray Field El Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-2
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-2
Date sample collected: 9/27/2023
FIELD ANALYSES:
WAS
Well Depth: 17.0 ft.
Well Diameter: 2 in.
pH 0040o: 5.4 units Temp. 000lo: 24.2 oC
DRY at
Depth to Water Level 82546: 5 ft. below measuring point Screened Interval: 3 ft. to
13 ft. Spec. Cond, 00094: µMhos
time of
sampling,
Measuring Point is 2.4 ft. above land surface
Relative M.P. Elevation: 2.6 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
5.76
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 9/27/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.08
ni Pb - Lead 01051 uglL
Coliform: MF Fecal 31616 23
1100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 262
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 5.4
units
Ba - Barium 01007
ug1L
TOC 00680 16.6
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 57
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 12
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs. mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aqent) Name and Title - Please print or Noe
GW-59 Rev.8/2013
re of PermlttiMeUr Authorized Agent)
(Date)
10/31 /2023

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT S NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone_ 919-807-6306
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
icty) (stale)
(zlp)
X Spray Field 0 Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-3
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-3
Date sample collected: 9/27/2023
FIELD ANALYSES:
WAS
Well Depth: 17.0 ft.
Well Diameter: 2 in.
pH 0040o: 4.9 units Temp. 000lo: 25.4 °C
DRY at
Depth to Water Level 82546: 4.7 ft. below measuring point Screened Interval: 3 ft. to
13 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 3.2 ft. above land surface
Relative M.P. Elevation: 1.5 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
5.90
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 9/27/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 73
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 4.87
units
Ba - Barium 01007
ug/L
TOC 00680 2.7
mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 10
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.812013
Authorized Aqent)
(Date)
10/31 /2023

SUBMIT FORM ON YELLOW PAPER ONLY
• .
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• •
•
1617 MAIL SERVICE CENTER, RALLEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print
Clearly or Type
PERMIT Number: Expiration Date: _ 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
(city) (State)
(Zip)
X Spray Field El Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-4
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-4
Date sample collected: 9/27/2023
FIELD ANALYSES:
WAS
Well Depth: 16.0 ft.
Well Diameter: 2 in.
pH 00400: 4.9 units Temp. 000lo: 29.7 oC
DRY at
Depth to Water Level 82546: 4.4 ft. below measuring point Screened Interval: 5.8 ft. to
14 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.68 ft. above land surface
Relative M.P. Elevation: 1.72 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
5.57
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 9/27/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N oo615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 229
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 4.91
units
Ba - Barium 01007
ug/L
TOC 00680 1.3
mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 51
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
uglL
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 42
mg/L
Hg - Mercury 71900
ug1L Lab Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia oo6lo <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
IUVV-0:1 K@V. olzu IJ

SUBMIT FORM ON YELLOW PAPER ONLY
•
DEPARTMENT OF ENVIRONMENT S NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
161' MAIL SERVICE CENTER, RALEIGH,:NC 276994617 Phone: [phone]
FACILITY INFORMATION
Please Print
Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
Permit Name (if different):
NPDES Other
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
(city; (State)
(zip)
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-5
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-5
Date sample collected: 9/27/2023
FIELD ANALYSES:
WAS
Well Depth: 18.1 ft.
Well Diameter: 2 in.
pH 00400: 5.2 units Temp. 000lo: 22.5 °C
DRY at
Depth to Water Level 82546: 5.8 ft. below measuring point Screened Interval: 5 ft. to
15 ft. Spec. Cond. 00094: µMhos
time of
sampling,check
Measuring Point is 2.57 ft. above land surface
Relative M.P. Elevation: 3.23 ft.
Odor 00085:
Volume of water pumped/bailed before sampling:
5.90
gallons
Appearance
here:
❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ElNO
LABORATORY INFORMATION
Date sample analyzed: 9/27/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 35
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 5.16
units
Ba - Barium 01007
ug/L
TOC 00680 <0.5
mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 10
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 000lo <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address: 716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
;cty, (state) t7_1pi
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-6
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-6
Date sample collected: 9/26/2023
FIELD ANALYSES:
WAS
Well Depth: 16.8 ft.
Well Diameter: 2 in.
pH 00400: 5.6 units Temp. 000lo: 31 °C
DRY at
Depth to Water Level 82546: 4 ft. below measuring point Screened Interval: 3.5 ft. to
14 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.65 ft. above land surface
Relative M.P. Elevation: 1.35 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 6.14
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 9/26/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615 0.11
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 392 mg/L
Al -Aluminum oilo5
mg/L
pH (Lab) oo403 5.62 units
Ba - Barium 01007
ug/L
TOC oo66o 6.9 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 52 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 21 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095 µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia omio <0.2 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625 mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.8/2013
(or Authorized Aqent)
(Date)
10/31 /2023

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH,;NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
(City) (staiej
Zip;
X Spray Field Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-7
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-7
Date sample collected: 9/26/2023
FIELD ANALYSES:
WAS
Well Depth: 15.0 ft.
Well Diameter: 2 in.
pH 0040o: 4.7 units Temp. 000ic 30.5 °C
DRY at
Depth to Water Level 82546: 3 ft. below measuring point Screened Interval: 2.5 ft. to
13 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: 0 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
5.76
gallons
Appearance
here:
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 9/26/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <02
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 256
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 4.67
units
Ba - Barium 01007
ug/L
TOC oomo 9
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 55
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 56
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.8/2013
(or Authorized Agent)
(Date)
10/31 /2023

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or Type
Facility Name:
Permit Name (if different):
Facility Address:
Jacksonville
(city)
of Jacksonville Land Treatment
716 Firetower Road
NC 28540 County Onslow
(State) (ZIP)
Contact Person: Amy Palaschak Telephone#: [phone]
Well Location/Site Name MW-8 No. of wells to be sampled: 17
PERMIT Number: Expiration Date: 7/31/2029
Non -Discharge WQ0009267 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-8
Date sample collected:
9/25/2023
FIELD ANALYSES:
WAS
Well Depth: 12.1 ft.
Well Diameter:
2 in.
pH 0040o: 4.6 units Temp. 000lo: 31.8 °C
DRY at
Depth to Water Level 82546: 8.1 ft. below measuring point Screened Interval:
3 ft. to 9 ft.
Spec. Cond. 00094: µMhos
time of
sampling,check
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation:
5.1 ft.
Odor 00085:
Volume of water pumped/bailed before sampling: 1.92
gallons
Appearance
here:
❑
Samples for metals were collected unfiltered: X YES
❑ NO and field acidified: X
YES El NO
Date sample analyzed:
9/25/2023
Laboratory Name: 1. Jacksonville
2. Environmental Chemists Certification No.
1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L
Pb - Lead 01051
ug/L
Coliform: MF Fecal 31616
<1
/100mL
Nitrate (NO3) as N 00620 0.02
mg/L
Zn - Zinc 01092
mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly
turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
)issolved Solids:Total 70300
198
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403
4.6
units
Ba - Barium 01007
ug/L
TOC oomo
3.2
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940
<5
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
99
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ® Yes (1)
❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 7673 method #
SM 6200C
Total Ammonia 00610
<0.2
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.8/2013
(or Authorized Agent)
11 /16/2023

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone. [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
iCiq) (State;
izip1
X Spray Field Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-9
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-9
Date sample collected: 9/25/2023
FIELD ANALYSES:
WAS
Well Depth: 14.0 ft.
Well Diameter: 2 in.
pH 00400: 3.88 units Temp. 000lo: 29.7 °C
DRY at
Depth to Water Level 82546: 8.1 ft. below measuring point Screened Interval: 7 ft. to
11 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.55 ft. above land surface
Relative M.P. Elevation: 5.55 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
2.83
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 9/25/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.03
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 221
mg/L
Al -Aluminum ol1o5
mg/L
pH (Lab) 00403 3.88
units
Ba - Barium 01007
ug/L
TOC o068o 2.8
mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 8
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 97
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia oo610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen: NH3 as N: Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aqent) Name and Title- Please print or type
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
• .
DEPARTMENT OF ENVIRONMENT 8, NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
• • •
•
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Dater 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
(city) (State)
(Zip)
X Spray Field El Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-10
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-10
Date sample collected: 9/25/2023
FIELD ANALYSES:
WAS
Well Depth: 30.1 ft.
Well Diameter: 2 in.
pH 00400: 6.5 units Temp. 000lo 30.7 °C
DRY at
Depth to Water Level 82546: 8.1 ft. below measuring point Screened Interval: 17 ft. to
27 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.9 ft. above land surface
Relative M.P. Elevation: 5.2 ft.
Odor 000m:
check
Volume of water pumped/bailed before sampling:
10.56
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 9/25/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved
and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.05
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 1.36
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 575
mg/L
AI -Aluminum 01105
mg/L
pH (Lab) 00403 6.46
units
Ba - Barium 01007
ug/L
TOC 00680 1.9
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 14
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 156
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia o0610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone_ 919-807-6306
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
(City) (State)
[Zip)
X Spray Field El Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-11
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-11
Date sample collected: 9/28/2023
FIELD ANALYSES:
WAS
Well Depth: 22.2 ft.
Well Diameter: 2 in.
pH 0040o: 4.5 units Temp. 000lr 21 °C
DRY at
Depth to Water Level 82546: 11 ft. below measuring point Screened Interval: 5 ft. to
20 ft. Spec. Cond. 00094: µMhos
time of
sampling,check
Measuring Point is 2.25 ft. above land surface
Relative M.P. Elevation: 8.25 ft.
Odor 000m:
Volume of water pumped/bailed before sampling:
5.62
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 9/28/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.51
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 32
mg/L
Al - Aluminum o11o5
mg/L
pH (Lab) 00403 4.54
units
Ba - Barium 01007
ug/L
TOC 00680 <0.5
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 <5
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: — mg/L Effluent Total VOCs: - mg/L VOC Removal%
1 cerfdy that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Wally Hansen - Public Services Director
Permittee (or Authorized Aqent) Name and Title - Please print or tvoe
Authorized Aqentl (Date)
10/31 /2023
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
ON •
MIDEPARTMENTOF
ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH,NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print
Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
(Citgi (State,
(Zlp)
X Spray Field El Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-12
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-12
Date sample collected: 9/28/2023
FIELD ANALYSES:
WAS
Well Depth: 18.3 ft.
Well Diameter: 2 in.
pH 00400: 5.6 units Temp. 000lo: 30.1 °C
DRY at
Depth to Water Level 82546: 5.2 ft. below measuring point
Screened Interval: 5 ft. to
15 ft. Spec. Cond. 00094: µMhos
time of
sampling,check
Measuring Point is 3.04 ft. above land surface
Relative M.P. Elevation: 2.16 ft.
Odor 000s5:
Volume of water pumped/bailed before sampling:
6.29
gallons
Appearance
here:
❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 9/28/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N o0615 0.07
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 149
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 5.57
units
Ba - Barium 01007
ug/L
TOC 00680 28.3
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 8
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 8
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <02
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aqent) Name and Title - Please print or tvAe
GW-59 Rev.8/2013
Authorized Agent)
(Date)
10/31 /2023

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH,'NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
(cty) (state)
(ZIP1
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-13
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other.,
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-13
Date sample collected: 9/25/2023
FIELD ANALYSES:
WAS
Well Depth: 23.2 ft.
Well Diameter: 2 in.
pH 00400: 4.7 units Temp. 000l( 30 °C
DRY at
Depth to Water Level 82546: 15 ft. below measuring point Screened Interval: 10.5 ft. to
23.2 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.75 ft. above land surface
Relative M.P. Elevation: 11.75 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
4.18
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 9/25/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.04
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P oo665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 68
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 4.67
units
Ba - Barium 01007
ug/L
TOC 00680 1.3
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 20
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 0.3
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aqentl Name and Title - Please Drint or tme
GW-59 Rev.8/2013
(or Authorized Aqent)
(Date)
10/31 /2023

SUBMIT FORM ON YELLOW PAPER ONLY
• .
.
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
� �
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617IMAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Dater 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge W00009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
cit,l ;state,
(ZIP)
X Spray Field Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-14
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-14
Date sample collected: 9/25/2023
FIELD ANALYSES:
WAS
Well Depth: 17.9 ft.
Well Diameter: 2 in.
pH 00400: 4.8 units Temp. 000lo: 28.5 °C
DRY at
Depth to Water Level 82546: 11 ft. below measuring point Screened Interval: 5 ft. to
15 ft. Spec. Cond. 00094: µMhos
time of
sampling,check
Measuring Point is 3.2 ft. above land surface
Relative M.P. Elevation: 8 ft.
Odor 00085:
Volume of water pumped/bailed before sampling:
3.22
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 9/25/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead oimi ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.04
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 68
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) oo403 4.83
units
Ba - Barium 01007
ug/L
TOC omw 13.4
mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 11
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 1.29
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: — mg/L Effluent Total VOCs: mg/L VOC Removal%
certify that, to the best of my knowledge and belief, the information submitted in this report is true; accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a
DWR-certified laboratory. > I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Wally Hansen - Public Services Director
Permittee (or Authorized Aoent) Name and Title -Please print or type
(or Authorized Aoent)
(Date)
10/31 /2023
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
• .
. DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
I G M
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617'MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]'
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
'City) (State)
(ZIP)
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-15
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MWA5
Date sample collected: 9/27/2023
FIELD ANALYSES:
WAS
Well Depth: 15 ft.
Well Diameter: 2 in.
pH 0040o: 4.7 units Temp. 000lo: 25.6 °C
DRY at
Depth to Water Level 82546: 3.2 ft. below measuring point Screened Interval: 5 ft. to
15 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.9 ft. above land surface
Relative M.P. Elevation: 0.3 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
5.66
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 9/27/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 1.13
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 117
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 4.69
units
Ba - Barium 01007
ug/L
TOC 00680 1.5
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 52
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
uglL (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia o0610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.8/2013
(or Authorized Aqent)
(Date)
10/31 /2023

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617iMAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]r
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC
23540 County Onslow
❑ Lagoon ❑ Remediation: Infiltration Gallery
;City) (6ta+ei
(ZIP)
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-16
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-16
Date sample collected: 9/28/2023
FIELD ANALYSES:
WAS
Well Depth: 25 ft.
Well Diameter: 2 in.
pH 00400: 4.5 units Temp. 000lo: 21.2 °C
DRY at
Depth to Water Level 82546: 8.4 ft. below measuring point Screened Interval: 15 ft. to
20 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.4 ft. above land surface
Relative M.P. Elevation: 6 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
7.97
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 9/28/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <4
/100mL
Nitrate (NO3) as N 00620 0.24
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids -.Total 70300 69
mg/L
Al - Aluminum o11o5
mg/L
pH (Lab) oo403 4.52
units
Ba - Barium 01007
ug/L
TOC 00680 2.3
mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 32
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 13
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia o0610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese o1o55
ii method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please print or tviDe
GW-59 Rev.8/2013
of perm (or Authorized Aqent)
(Date)
10/31 /2023

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Dater 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
(city) (State)
iziP'
X Spray Field El Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-17
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-17
Date sample collected: 9/28/2023
FIELD ANALYSES:
WAS
Well Depth: 25 ft.
Well Diameter: 2 in.
pH 00400: 4.5 units Temp. 000lo 25.1 °C
DRY at
Depth to Water Level 82546: 5.8 ft. below measuring point Screened Interval: 15 ft. to
20 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 1.9 ft. above land surface
Relative M.P. Elevation: 3.9 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
9.22
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 9/28/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <10
/100mL
Nitrate (NO3) as N 00620 0.04
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 90
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) oo403 4.51
units
Ba - Barium 01007
ug/L
TOC omm 0.9
mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 38
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 12
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia o0610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N: Ammonia Nitrogen, Total)
Mn - Manganese o1 o55
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please print or tvpe
(or Authorized Aqent)
10/31 /2023
GW-59 Rev.8/2013

F-77 Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab;' Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoio environmentalchemists.com
City of Jacksonville
Date of Report: Oct 09, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-22274
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
23-54252 Site: MW-8
9/25/2023
12:20 PM Water AP/ML/LC
Test
Method
Results
Date Analyzed
Sulfate
EPA 300.0, Rev. 2.1, 1993
99 mg/L
09/29/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
3.2 mg/L
09/27/2023
Chloride
SM4500 CI E-2011
< 5 mg/L
09/29/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,1,1-Trichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
1,1,2-Trichloroethane
SW 846 Method 8260015030E
<0.5 pg/L
09/28/2023
1,1-Dichloroethane
SW 846 Method 826OD/5030B
<0.5 pg/L
09/28/2023
1,1-Dichloroethene
SW 846 Method 8260DIS0306
<0.5 pg/L
09/28/2023
1, 1 -Dichloropropene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,2,3-Trichlorobenzene
SW 646 Method 826OD15030B
<0.5 pg/L
09/28/2023
1,2,3-Trichloropropane
SW 846 Method 82BOD15030B
<0,5 pg/L
09/28/2023
1,2,4-Trichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
<1 pg/L
09/28/2023
1,2-Dibromoethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,2-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
1,2-Dichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,2-Dichloropropane
SW 846 Method 8260015030E
<0.5 pg/L
09/28/2023
1,3,5-Trimethylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,3-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
1,3-Dichloropropane
SW 846 Method 82BOD15030B
<0.5 pg/L
09/28/2023
1 4-Dichlorobenzene
SW 846 Method 8260D150306
<0 5 pg/L
09/28/2023
2,2-Dichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
2-Chlorotoluene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
4-Chlorotoluene
SW 846 Method 8260015030B
<0.5 pg/L
09/28/2023
Report # 2023-22274
Page 1 of 15

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
- 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info-, environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Oct 09, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-22274
Project ID: Monitoring Wells
Benzene
SW 846 Method 826OD/50308
<0.5 pg/L
09/28/2023
Bromobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
09/28/2023
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 tag/L
09/28/2023
Bromodichloromethane
SW 846 Method 826oD/50308
<0.5 pg/L
09/28/2023
Bromoform
SW 846 Method 826OD/50308
<0.5 tag/L
09/28/2023
Bromomethane
SW 846 Method 828oD15030B
<0.5 pg/L
09/28/2023
Carbon tetrachloride
SW 846 Method 826oD/5030B
<0.5 pg/L
09/28/2023
Chlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
09/28/2023
Chloroethane
SW 846 Method 826OD/5030B
<0.5 pg/L
09/28/2023
Chloroform
SW 846 Method 826OD/5030B
<0.5 pg/L
09/28/2023
Chloromethane
SW 846 Method 826OD/5030B
<0.5 pg/L
09/28/2023
CIS-1,2-Dichloroethene
SW 846 Method 826OD/5030B
<0.5 pg/L
09/28/2023
cis-1,3-Dichloropropene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Dibromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Dibromomethane
SW 846 Method 826OD/5030B
<0.5 pg/L
09/28/2023
Dichlorodifluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Ethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Hexachlorobutadiene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Isopropylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
M+P Xylene
SW 846 Method 8260D15030B
<1.0 pg/L
09/28/2023
Methylene chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Naphthalene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
n-Propylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
ortho-Xylene
SW 846 Method 826OD/5030B
<0.5 pg/L
09/28/2023
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
sec -Butyl benzene
<,�v 748 Method u26OD/- + c
<0.5 pg/L
09/28/2023
Styrene
SW 846 Method 826OD/5030B
<0.5 pg/L
09/28/2023
tert-Butylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
09/28/2023
Tetrachloroethene
SW 846 Method 8260D150308
<0.5 pg/L
09/28/2023
Report 9 2023-22274
Page 2 of 15

envirochem
ANALYTICAL 8 CONSULTING CHEMISTS
F"0007' -:O"qql
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info, it environmentalchemists.com
City of Jacksonville
Date of Report: Oct 09, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-22274
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260DJ5030B
<0.5 pg/L
09/28/2023
Trans-1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Trans-1 ,3-dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Trichloroethene
SW 846 Method 8280D15030B
<0.5 pg/L
09/28/2023
Trichlorofluoromethane
SW 846 Method 8280D15030B
<0.5 pg/L
09/28/2023
Vinyl chloride
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Nitrate Nitrogen (Cale
Nitrite Nitrogen EPA 353 2, Rev 2.0, 1993 < 0.02 mg/L 09/26/2023
Nitrate+Nitrite-Nitrogen EPA 353 2, Rev 2 0,1993 0.02 mg/L 09/28/2023
Nitrate Nitrogen Subtraction Method 0.02 mg/L 10/04/2023
Report # 2023-22274 Page 3 of 15

envirochem
ANALYTICAL & CONSULTING CHEMISTS
City of Jacksonville
Post Office Box 128
Jacksonville NC 28541
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Oct 09, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-22274
Project ID: Monitoring Wells
Lab ID Sample ID:
23-54259 Site: MW-9
Test
Collect Date/Time
9/25/2023 12:32 PM
Method
Matrix Sampled by
Water AP/MULC
Results Date Analyzed
Sulfate
EPA 300.0, Rev 2 1, 1993
97 mg/L
09/29/2023
Total Organic Carbon (TOC)
SM 5310 8-2014
2.8 mg/L
09/27/2023
Chloride
SM4500 CI E-2011
8 mg/L
09/29/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,1,1-Trichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,1,2-Trichloroethane
SW B46 Method 8260D/503013
<0.5 pg/L
09/28/2023
1,1-Dichloroethane
SW 846 Method 8260D150306
<0.5 pg/L
09/28/2023
1,1-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1, 1 -Dichloropropene
SW 846 Method 82BOD/5030a
<0.5 pg/L
09/28/2023
1,2, 3-Trichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,2,3-Trichooropropane
SW B46 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,2,4-Trichlorobenzene
SW 646 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8269D/5030B
<1 pg/L
09/28/2023
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,2-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
1,2-Dichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,2-Dichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
1,3,5-Trimethyl benzene
SW 846 Method 8260015030B
<0.5 pg/L
09/28/2023
1,3-Dichlorobenzene
SW 846 Method 82600/50308
<0.5 pg/L
09/28/2023
1,3-Dichloropropane
SW 846 Method 82600150308
<0.5 pg/L
09/28/2023
1 4-Dichlorobenzene
SW B46 Method 8260D15030B
<0.5 pg/L
09/28/2023
2,2-Dichloropropane
SW 846 Method 8260D150308
<0.5 pg/L
09/28/2023
2-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
4-Chlorotoluene
SW 846 Method 826OD/5030B
<0.5 pg/L
09/28/2023
Report # 2023-22274 Page 4 of 15

F00"07 -71 Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infon environmentalchemists.com
City of Jacksonville
Date of Report: Oct 09, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-22274
Project ID: Monitoring Wells
Benzene
SW 846 Method 826OD150308
<0.5 pg/L
09/28/2023
Bromobenzene
SW 846 Method 8260D150308
<0.5 pg/L
09/28/2023
Bromochloromethane
SW 846 Method 8260D150308
<0.5 pg/L
09/28/2023
Bromodichloromethane
SW 846 Method 8260D/50308
<0.5 pg/L
09/28/2023
Bromoform
SW 848 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Bromomethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Carbon tetrachloride
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Chlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Chloroethane
SW 846 Method 826001503GB
<0.5 pg/L
09/28/2023
Chloroform
SW 846 Method 8260015030E
<0.5 pg/L
09/28/2023
Chloromethane
SW 846 Method 8260015030E
<0.5 pg/L
09/28/2023
cis-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
cis-1,3-Dichloropropene
SW 846 Method 82600/5030B
<0.5 pg/L
09/28/2023
Dibromochloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Dibromomethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Dichlorodifluoromethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Ethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Hexachlorobutadiene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Isopropylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
M+P Xylene
SW 846 Method 826OD15030B
<1.0 pg/L
09/28/2023
Methylene chloride
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Naphthalene
SW 846 Method 8260D/50308
<0.5 pg/L
09/28/2023
n-Butylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
09/28/2023
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
ortho-Xylene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
sec-B utyl benzene
SW 646 Method 8260D/, , ,.;b
<0.5 pg/L
09/28/2023
Styrene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
tert-Butylbenzene
SW 846 Method 8280D/5030B
<0.5 pg/L
09/28/2023
Tetrachloroethene
SW B46 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Report #:. 2023-22274
Page 5 of 15

F"107 Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info;a environmentalchemists.com
City of Jacksonville
Date of Report: Oct 09, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-22274
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260DIS030B
<0.5 pg/L
09/28/2023
Trans-1,2-Dichloroethene
SW 846 Method 826OD150308
<0.5 pg/L
09/28/2023
Trans- 1, 3-d ich loropropene
SW 846 Method 8260DIS030B
<0.5 pg/L
09/28/2023
Trichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Trichlorofluoromethane
SW 846 Method 8260DIS030B
<0.5 pg/L
09/28/2023
Vinyl chloride
SW 846 Method 8260DI5030B
<0.5 Ng/L
09/28/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353 2, Rev. 2 0, 1993 < 0,02 mg/L 09/26/2023
Nitrate+ N itrite-N itrogen EPA 353 2, Rev. 2.0, 1993 0.03 mg/L 09/28/2023
Nitrate Nitrogen Subtraction Method 0.03 mg/L 10/04/2023
Report # 2023-22274 - Page 6 of 15

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
4710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoia.environmentalchemists com
City of Jacksonville
Date of Report: Oct 09, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-22274
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-54260 Site: MW-10
9/25/2023
12:40 PM Water AP/MULC
Test
Method
Results
Date Analyzed
Sulfate
EPA 300 0 Rev 21 1993
156 mg/L
09/29/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
1.9 mg/L
09/27/2023
Chloride
SM4500 CI E-2011
14 mg/L
09/29/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,1,1-Trichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,1,2-Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,1-Dichloroethane
SW 846 Method 826OD150308
<0.5 pg/L
09/28/2023
1,1-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,1-Dichloropropene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,2,3-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,2,3-Trichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
1,2,4-Trichlorobenzene
SW 845 Method 82BOD15030B
<0.5 pg/L
09/28/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
<1 pg/L
09/28/2023
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,2-Dichlorobenzene
SW 846 Method 82600/5030B
<0.5 pg/L
09/28/2023
1,2-Dichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
1,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,3-Dichlorobenzene
SW 846 Method 82BOD160308
<0.5 pg/L
09/28/2023
1,3-Dichloropropane
SW 846 Method 8260015030B
<0.5 pg/L
09/28/2023
1 4-Dichlorobenzene
SW 846 Method 826OD15030B
<0 5 pg/L
09/28/2023
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
2-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
4-Chlorotoluene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Report # 2023-22274
Page 7 of 15

roop"--- -71 Environmental Chemists, Inc.
• 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Oct 09, 2023
Customer PO M
Customer ID: 08110015
Report M 2023-22274
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D15030B
<0 5 pg/L
09/28/2023
Bromobenzene
SW 846 Method 8260D15030B
<0 5 pg/L
09/28/2023
Bromochloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Bromodichloromethane
SW 845 Method 8260D15030B
<0.5 pg/L
09/28/2023
Bromoform
SW 846 Method 826oD15030B
<0 5 pg/L
09/28/2023
Bromomethane
SW 846 Method 826OD750308
<0 5 pg/L
09/28/2023
Carbon tetrachloride
SW 846 Method 82BOD750308
<0.5 pg/L
09/28/2023
Chlorobenzene
SW 845 Method 8260D15030B
<0 5 pg/L
09/28/2023
Chloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Chloroform
SW 846 Method 8260015030B
<0.5 pg/L
09/28/2023
Chloromethane
SW 846 Method 82600150309
<0.5 pg/L
09/28/2023
cis-1,2-Dichloroethene
SW 846 Method 82600/5030B
<0.5 pg/L
09/28/2023
cis-1, 3-Dich loropropene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Dibromochloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Dibromomethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Dichlorodifluoromethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Ethylbenzene
SW 846 Method 82600/50308
<0.5 pg/L
09/28/2023
Hexachlorobutadiene
SW 846 Method 826oD150308
<0.5 pg/L
09/28/2023
lsopropylbenzene
SW 846 Method 82600/50308
<0.5 pg/L
09/28/2023
M+P Xylene
SW 845 Method 8260D15030B
<1.0 pg/L
09/28/2023
Methylene chloride
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Naphthalene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
n-Butylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
n-Propylbenzene
SW 846 Method 8260D1503013
<0.5 pg/L
09/28/2023
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
p-Isopropyltoluene
SW 846 Method 8260D1503013
<0.5 pg/L
09/28/2023
sec-Butylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Styrene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
tert-Butyl benzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Tetrachloroethene
SW 846 Method 6260015030E
<0.5 pg/L
09/28/2023
Report #: 2023-22274
Page 8 of 15

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
City of Jacksonville
Date of Report: Oct 09, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-22274
Project ID: Monitoring Wells
Toluene
SW 846 Method 826GD15030B
<0.5 pg/L
09/28/2023
Trans-1,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Trans- 1,3-dichloropropene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Trichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Trichlorofluoromethane
SW 846 Method 82600150308
<0.5 pg/L
09/28/2023
Vinyl chloride
SW 846 Method 8260D/50308
<0.5 pg/L
09/28/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2. Rev 2 0, 1993
< 0.02 mg/L
09/26/2023
Nitrate+ N itrite-N itrogen
EPA 353.2, Rev 2 0,1993
0.05 mg/L
09/28/2023
Nitrate Nitrogen
Subtraction Method
0.05 mg/L
10/04/2023
Report # 2023-22274 Page 9 of 15

-77
pp"w'".
Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
Lk,® 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info't:envtronmentalchemists com
City of Jacksonville
Date of Report: Oct 09, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-22274
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-54261 Site: MW-13
9/25/2023
1:25 PM Water AP/MULC
Test
Method
Results
Date Analyzed
Sulfate
EPA 300.0, Rev 2.1, 1993
<5 mg/L
09/29/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
1.3 mg/L
09/27/2023
Chloride
SM4500 a E-2011
20 mg/L
09/29/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,1,1-Trichloroethane
SW B46 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
1,1,2-Trichloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
09/28/2023
1,1-Dichlorcethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,1-Dichloroethene
SW 846 Method 8260D150308
<0.5 pg/L
09/28/2023
1,1-Dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
09/28/2023
1,2,3-Trichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
1,2,3-Trichloropropane
SW 846 Method 826oD/5030B
<0.5 pg/L
09/28/2023
1,2,4-Trichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 826aD/5030B
<1 pg/L
09/28/2023
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0,5 pg/L
09/28/2023
1,2-Dichlorobenzene
SW 846 Method 826OD15030B
<0,5 pg/L
09/28/2023
1,2-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,2-Dichloropropane
SW 846 Method 8260015030E
<0.5 pg/L
09/28/2023
1,3,5-Trimethylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
09/28/2023
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1 4-Dichlorobenzene
SW 846 Method 8260D15030B
<0 5 pg/L
09/28/2023
2,2-Dichloropropane
SW 846 Method 8260D/50308
<0.5 pg/L
09/28/2023
2-Chlorotoluene
SW 846 Method 8260D/50308
<0.5 pg/L
09/28/2023
4-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Report #: 2023-22274
Page 10 of 15

-71
Environmental Chemists, Inc.
• 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab i Fax
`` 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Oct 09, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-22274
Project ID: Monitoring Wells
Benzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Bromodichloromethane
SW 846 Method 828oD/5030B
<0.5 pg/L
09/28/2023
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Chloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
cis- 1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
cis-1,3-Dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Dibromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Dibromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Dichlorodifluoromethane
SW 846 Method 826oD/5030B
<0.5 pg/L
09/28/2023
Ethylbenzene
SW 846 Method 825OD15030B
<0.5 pg/L
09/28/2023
Hexachlorobutadiene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Isopropylbenzene
SW 846 Method 8260D/50306
<0.5 pg/L
09/28/2023
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
09/28/2023
Methylene chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Naphthalene
SW 846 Met,.od 8260D15030B
<0.5 pg/L
09/28/2023
n-Butylbenzene
SW 846 Method 826OD150308
<0.5 pg/L
09/28/2023
n-Propylbenzene
SW 846 Method 826OD150308
<0.5 pg/L
09/28/2023
ortho-Xylene
SW 846 Method 82601)r5030B
<0.5 pg/L
09/28/2023
p-Isopropyitoluene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
sec-Butylbenzene
SW 846 Method 826013/5030B
<0.5 pg/L
09/28/2023
Styrene
SW 846 Method 8260D15030B
<0.5 pg/L
0b/28/2023
tert-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Tetrachloroethene
SW 846 Method 826oD/6030B
<0.5 pg/L
09/28/2023
Report #:: 2023-22274
Page 11 of 16

iw
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info a environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Oct 09, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-22274
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Trans-1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Trans-1,3-dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Trichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2. Rev. 2.0, 1993
< 0.02 mg/L
09/26/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.04 mg/L
09/28/2023
Nitrate Nitrogen
Subtraction Method
0.04 mg/L
10/04/2023
r
Report # 2023-22274 Page 12 of 15

• •
ANALYTICAL 8 CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
info,a environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC 28541
Attention:
Date of Report: Oct 09, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-22274
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-54262 Site: MW-14
9/25/2023
1:42 PM Water AP/MULC
Test
Method
Results
Date Analyzed
Sulfate
EPA 300.0, Rev, 2.1, 1993
<5 mg/L
09/29/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
13.4 mg/L
09/27/2023
Chloride
SM4500 ci E-2011
11 mg/L
09/29/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
1,1,1-Trichloroethane
SW 845 Method 82BOD15030B
<0.5 pg/L
09/28/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,1,2-Trichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,1-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,1-Dichloroethene
SW 846 Method 82GOD15030B
<0.5 pg/L
09/28/2023
1,1-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,2,3-Trichlorobenzene
SW 846 Method 82600150308
<0.5 pg/L
09/28/2023
1,2,3-Trichloropropane
SW 846 Method 8260D15030B
<Q,5 pg/L
09/28/2023
1,2,4-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,2,4-Trimethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
<1 pg/L
09/28/2023
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,2-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
1,2-Dichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,2-Dichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1, 3-Dichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,3-Dichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,4-Dichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
2,2-Dichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
2-Chlorotoluene
SW 846 Method 82601D150308
<0.5 pg/L
09/28/2023
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Report #. 2023-22274 Page 13 of 15

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoaa environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Oct 09, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-22274
Project ID: Monitoring Wells
Benzene
SW 846 Method 8280D15030B
<0.5 pg/L
09/28/2023
Bromobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Bromochloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Bromodichloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Bromoform
SW 846 Method 826OD15030B
<0.5 lag/L
09/28/2023
Bromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Carbon tetrachloride
SW 846 Method 8260D150308
<0.5 pg/L
09/28/2023
Chlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Chloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
cis- 1,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
cis-1,3-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Dibromochloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Dibromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Dichlorodifluoromethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Ethylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Hexachlorobutadiene
SW 846 Method 826OD150306
<0.5 pg/L
09/28/2023
Isopropylbenzene
SW 846 Method 82BOD15030B
<0.5 pg/L
09/28/2023
M+P Xylene
SW 846 Method 826OD15030B
<1.0 pg/L
09/28/2023
Methylene chloride
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Naphthalene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
n-Butylbenzene
SW B46 Method 8260D15030B
<0.5 pg/L
09/28/2023
n-Propylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
ortho-Xylene
SW 846 Method 826OD/5030B
<0.5 pg/L
09/28/2023
p-Isopropyltoluene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
sec-Butylbenzene
SW 846 Method 8260D/503 q
<0.5 pg/L
09/28/2023
Styrene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
tert-Butylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Tetrachloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Report 4:: 2023-22274
Page 14 of 15

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
tw 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Oct 09, 2023
Customer PO #:
Customer ID: 08110015
Report #, 2023-22274
Project ID: Monitoring Wells
Toluene
SW 846 Method 8280D/50306
1.05 pg/L
09/28/2023
Trans-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Trans-1,3-dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Trichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Trichlorofluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Vinyl chloride
SW 846 Method 8260D/5030B
<0,5 pg/L
09/28/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev 2 0, 1993
< 0.02 mg/L
09/26/2023
Nitrate+ N itrite-N itrogen
EPA353.2, Rev 20 1993
0.04 mg/L
09/28/2023
Nitrate Nitrogen
Subtraction Method
0.04mg/L
10/04/2023
Comment:
Reviewed by:
Report #. 2023-22274 Page 15 of 15

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Date: 9�a� O Report Number: _ 2023-aD ccD
Receipt of sample:
ECHEM Pickup Client Delivery ❑ JUPS ❑ FeclEx ❑ Other ❑
❑ YES 10 NO
N N/A 1. Were custody seals present on the cooler?
❑ YES 10 NO
N N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt a °C Corrected temperature upon receipt °C
How temperature taken:
❑ Temperature Blank 0 Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
N YES ❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
N YES ❑ NO
4. Were proper custody procedures (relinquished/received) followed?
0 YES
❑ NO
5. Were sample ID's listed on the COC?
0 YES
❑ NO
6. Were samples ID's listed on sample containers?
N YES
❑ NO
7. Were collection date and time listed on the COC?
N YES
❑ NO
8. Were tests to be performed listed on the COC?
N YES
❑ NO
9. Did samples arrive in proper containers for each test?
0 YES
❑ NO
10. Did samples arrive in good condition for each test?
N YES
❑ NO
11. Was adequate sample volume available?'
❑O YES
❑ NO
12. Were samples received within proper holding time for requested tests?
YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES ❑ NO 118.
Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked
at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
(Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s)
were received incorrectly preserved and were adjusted accordingly
by adding (circle one):
H2SO4 HNO3 HCl NaOH
Time of preservation:
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately
for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s)
were received with headspace
COMMENTS:
DOC. QA.002 Rev ]

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F -77 "17
Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info(a,.environmentalchemists.com
City of Jacksonville
Date of Report: Oct 09, 2023
Post Office Sox 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report M 2023-22412
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-54606 Site: MW-6
9/26/2023
1:55 PM Water MULC
Test
Method
Results
Date Analyzed
Sulfate
EPA 300 0 Rev 21 1993
21 mg/L
09/29/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
6.9 mg/L
09/27/2023
Chloride
SM4500 C1 E-2011
52 mg/L
09/29/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 µg/L
09/28/2023
1,1,1-Trichloroethane
SW B46 Method 8260DIS030B
<0.5 µg/L
09/28/2023
1,1,2,2-Tetrach loroethane
SW 846 Method 8260D/5030B
<0.5 lig/L
09/28/2023
1,1,2-Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1, 1 -Dich loroethane
SW 846 Method 8260D/50308
<0.5 µg/L
09/28/2023
1,1-Dichloroethene
SW 846 Method 8260D15030B
<0.5 µg/L
09/28/2023
1,1-Dich loropropen e
SW 846 Method 826OD16030B
<0.5 µg/L
09/28/2023
1,2,3-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 µg/L
09/28/2023
1,2,3-Trichloropropane
SW 846 Method 8260D15030B
<0.5 µg/L
09/28/2023
1,2,4-Trichlorobenzene
SW 846 Method 82600/5030B
<0.5 µg/L
09/28/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260DIS030B
<0.5 µg/L
09/28/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D150308
<1 pg/L
09/28/2023
1,2-Dibromoethane
SW 846 Method 826OD15030B
<0.5 µg/L
09/28/2023
1,2-Dichlorobenzene
SW 846 Method 8260D15030B
<0.5 µg/L
09/28/2023
1,2-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 µg/L
09/28/2023
1,2-Dichloropropane
SW 846 Method 8260D15030B
<0.5 µg/L
09/28/2023
1,3,5-Trimethyl benzene
5W 846 Method 826OD15030B
<0.5 µg/L
09/28/2023
1,3-Dichlorobenzene
SW 846 Method 8260D15030B
<0.5 µg/L
09/28/2023
1,3-Dichloropropane
SW 846 Method 8260D15030B
<0.5 µg/L
09/28/2023
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 µg/L
09/28/2023
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 µg/L
09/28/2023
2-Chlorotoluene
SW 846 Method 82BOD/503oB
<0.5 µg/L
09/28/2023
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 µg/L
09/28/2023
Report #.. 2023-22412
Page 1 of 9

[en7virochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infoia�environmentalchemists.com
City of Jacksonville
Date of Report: Oct 09, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-22412
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Bromobenzene
SW 846 Method 82BOD150308
<0.5 pg/L
09/28/2023
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Bromoform
SW 846 Method 82BOD15030B
<0.5 pg/L
09/28/2023
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Chlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Chloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
cis- 1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
cis- 1,3-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Dibromochloromethane
SW 846 Method 826oD/5030B
<0.5 pg/L
09/28/2023
Dibromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Dichlorodifluoromethane
SW 846 Method 6260D/5030B
<0.5 pg/L
09/28/2023
Ethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Isopropylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
09/28/2023
Methylene chloride
SW 846 Method 826oD15030B
<0.5 pg/L
09/28/2023
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
n-Propylbenzene
SW 846 Method 826OD150308
<0.5 pg/L
09/28/2023
ortho-Xylene
SW 846 Method 826OD150308
<0.5 pg/L
09/28/2023
p-Isopropyltoluene
SW 846 Method 826OD150306
<0.5 pg/L
09/28/2023
sec-BuMbenzene
SW 846 Method 82601)1_ . -',Ijb
<0.5 pg/L
09/28/2023
Styrene
SW 846 Method 8260015030E
<0.5 pg/L
09/28/2023
tert-Butyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Tetrachloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Report p:: 2023-22412
Page 2 of 9

[envirochem]
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
infoiu,environmentalchemists.com
City of Jacksonville
Date of Report: Oct 09, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-22412
Project ID: Monitoring Wells
Toluene
SW 846 Method 82BOD150308
<0.5 pg/L
09/28/2023
Trans-1,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Trans- 1,3-dichloropropene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Trichioroethene
SW 846 Method 8260D150303
<0.5 pg/L
09/28/2023
Trichlorofluoro methane
SW 846 Method 8260D/50308
<0.5 pg/L
09/28/2023
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA353.2. Rev. 20, 1993 0.11 mg/L 09/27/2023
Nitrate+Nitrite-Nitrogen EPA 353.2. Rev. 2.0, 1993 < 0.02 mg/L 10/02/2023
Nitrate Nitrogen Subtraction Method <0.02 mg/L 10/04/2023
Report # 2023-22412 Page 3 of 9

F-77 Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
® 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
City of Jacksonville Date of Report: Oct 09, 2023
Post Office Box 128 Customer PO M
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report M 2023-22412
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-54607 Site: MW-7 9/26/2023 11:59 AM Water MULC
Test _ Method Results Date Analyzed
Sulfate
EPA 300.0, Rev, 2 1, 1993
56 mg/L
09/29/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
9.0 mg/L
09/27/2023
Chloride
SM4500 CI E-2011
55 mg/L
09/29/2023
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1, 1, 1 -Trichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,1,2-Trichloroethane
SW 846 Method 8260D15030B
<0, 5 pg/L
09/28/2023
1,1-Dichloroethane
SW 846 Method 8260D150306
<0.5 pg/L
09/28/2023
1,1-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,1-Dichloropropene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,2,3-Trichlorobenzene
SW 646 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,2,3-Trichooropropane
SW 846 Method 8260015030E
<0.5 pg/L
09/28/2023
1, 2, 4-Trichlorobenzene
SW 846 Method 8280D150308
<0, 5 pg/L
09/28/2023
1,2,4-Trimethylbenzene
SW 846 Method 826OD16030B
<0.5 pg/L
09/28/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 826OD150308
<1 pg/L
09/28/2023
1,2-Dibromoethane
SW 846 Method 8260DIS0308
<0.5 pg/L
09/28/2023
1,2-Dichlorobenzene
SW 846 Method 8260015030E
<0.5 pg/L
09/28/2023
1,2-Dichloroethane
SW 846 Method 82600/5030B
<0.5 pg/L
09/28/2023
1,2-Dichloropropane
SW 846 Method 8260015030E
<0.5 pg/L
09/28/2023
1,3,5-Trimethylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,4-Dichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
2,2-Dichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
2-Chlorotoluene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Report*: 2023-22412 Page 4 of 9

F"17— --"RI Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL_ & CONSULTING CHEMISTS infoiti�environmentalchemists.com
City of Jacksonville
Date of Report: Oct 09, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-22412
Project ID: Monitoring Wells
Benzene
SW 646 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Bromobenzene
SW 846 Method 8260D1503013
<0.5 pg/L
09/28/2023
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Chlorobenzene
SW 846 Method 828OD15030B
<0.5 pg/L
09/28/2023
Chloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Chloroform
SW 846 Method 826oW5030B
<0.5 pg/L
09/28/2023
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
cis-1, 2-D ich loroethene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
cis-1, 3-D ich loropropene
SW 846 Method 828aD/50308
<0.5 pg/L
09/28/2023
Dibromochloromethane
SW 846 Method 826OD150308
<0.5 pg/L
09/28/2023
Dibromomethane
SW 846 Method 826oW50308
<0.5 pg/L
09/28/2023
Dichlorodifluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Ethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Hexachlorobutadiene
SW 846 Method 828UD150308
<0.5 pg/L
09/28/2023
Isopropylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
M+P Xylene
SW 846 Method 8260D15030B
<1.0 pg/L
09/28/2023
Methylene chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Naphthalene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
n-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
n-Propylbenzene
SW 846 Meth A 8260D/5030B
<0.5 pg/L
09/28/2023
ortho-Xylene
SW 846 Method 8260D/50308
<0.5 pg/L
09/28/2023
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
sec-Butyibenzene
�•* % 846 Method 6260/5 _ _ e'
<0.5 pg/L
09/28/2023
Styrene
SW 846 Method 826oD/50308
<0.5 pg/L
09/28/2023
te rt-Bu tyl benzene
SW 846 Method 826oD/50308
<0.5 pg/L
09/28/2023
Tetrachloroethene
SW sas Me" 826OD15030B
<0.5 pg/L
09/28/2023
Report #: 2023-22412
Page 5 of 9

F705� -
6envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910,392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(cz environmentalchemists.com
City of Jacksonville
Date of Report: Oct 09, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention-
Report #: 2023-22412
Project ID: Monitoring Wells
Toluene
SW 846 Method 6260D/5030B
<0.5 pg/L
09/28/2023
Trans-1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Trans-1,3-dichloropropene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2, Rev 2.0. 1993 < 0.02 mg/L 09/27/2023
Nitrate+Nitrite-Nitrogen EPA 353.2, Rev 2.0, 1993 < 0.02 mg/L 10/02/2023
Nitrate Nitrogen Subtraction Method <0.02 mg/L 10/04/2023
Report # 2023-22412 Page 6 of 0

ANALYTICAL & CONSULTING CHEMISTS
F00017-71
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(a�environmentalchemists.com
City of Jacksonville
Date of Report: Oct 09, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-22412
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-54608 Site: MW-12
9/26/2023
1:08 PM Water ML/LC
Test
Method
Results
Date Analyzed
Sulfate
EPA 300 0, Rev 2 1 1993
8 mg/L
09/29/2023
Total Organic Carbon (TOC)
SM 5310 8-2014
28.3 mg/L
09/27/2023
Chloride
SM4500 C1 E-2011
8 mg/L
09/29/2023
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D 5030E
<0.5 pg/L
09/28/2023
1, 1, 1-Trichloroethane
SW 846 Method 8260Dr5030s
<0.5 pg/L
09/28/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D 50308
<0.5 pg/L
09/28/2023
1,1,2-Trichloroethane
SW 846 Method 826OD150308
<0.5 pg/L
09/28/2023
1,1-Dichloroethane
SW 846 Method 82600150308
<0.5 pg/L
09/28/2023
1,1-Dichloroethene
SW 846 Method 82600150306
<0.5 pg/L
09/28/2023
1,1-Dichloropropene
SW 846 Method 82600150308
<0.5 pg/L
09/28/2023
1,2,3-Trichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
1,2,3-Trichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
1,2,4-Trichlorobenzene
SW 846 Method 8260DIS030B
<0.5 pg/L
09/28/2023
1,2,4-Trimethylbenzene
SW 846 Method 82600/5030B
<0.5 pg/L
09/28/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 82600/5030B
<1 pg/L
09/28/2023
1,2-Dibromoethane
SW 846 Method 8260015030E
<0.5 pg/L
09/28/2023
1,2-Dichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
1,2-Dichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
1,2-Dichloropropane
SW 846 Method 8260015030E
<0.5 pg/L
09/28/2023
1,3,5-Trimethylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
09/28/2023
1,3-Dichlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
09/28/2023
1,3-Dichloropropane
SW 846 Method MOD/50308
<0.5 pg/L
09/28/2023
1,4-Dichlorobenzene
SW 646 Method 8260D/50308
<0.5 pg/L
09/28/2023
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
4-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Report #:: 2023-22412
Page 7 of 9

r- envirochem
iMi
ANALYTICAL & CONSULTING CHEMISTS
City of Jacksonville
Post Office Box 128
Jacksonville NC 28541
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Oct 09, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-22412
Project ID: Monitoring Wells
Benzene
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Bromobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Bromochloromethane
SW 846 Method 8260D150308
<0.5 pg/L
09/28/2023
Bromodichloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Bromoform
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Bromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
09/28/2023
Carbon tetrachloride
SW 846 Method 82BOD150306
<0.5 pg/L
09/28/2023
Chlorobenzene
SW 846 Method 8260D150308
<0.5 pg/L
09/28/2023
Chloroethane
SW 846 Method 826oD/50308
<0.5 pg/L
09/28/2023
Chloroform
SW 846 Method 82600/50308
<0.5 pg/L
09/28/2023
Chloromethane
SW 846 Method 8260U50308
<0.5 pg/L
09/28/2023
cis-1,2-Dichloroethene
SW 846 Method 8260Dr50308
<0.5 pg/L
09/28/2023
cis-1,3-Dichloropropene
SW 846 Method 82600+50308
<0.5 pg/L
09/28/2023
Dtbromochloromethane
SW 846 Method 8260D 50308
<0.5 pg/L
09/28/2023
Dibromomethane
SW 846 Method 8260D 50308
<0.5 pg/L
09/28/2023
DichlorodiflUOfomethane
SW 846 Method 8260D+50308
<0.5 pg/L
09/28/2023
Ethylbenzene
SW 846 Method 82600 50308
<0.5 pg/L
09/28/2023
Hexachlorobutadiene
SW 846 Method 8260D+50308
<0.5 pg/L
09/28/2023
1sopropylbenzene
SW 846 Method 8260U50306
<0.5 pg/L
09/28/2023
M+P Xylene
SW 846 Method 8260U5030B
<1.0 pg/L
09/28/2023
Methylene chloride
SW 846 Method 82BOD15030B
<0.5 pg/L
09/28/2023
Naphthalene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
09/28/2023
ortho-Xylene
SW 846 Method 8280D/5030B
<0.5 pg/L
09/28/2023
p-Isopropyltoluene
SW 846 Method 826oD/50308
<0.5 pg/L
09/28/2023
sec-Butylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
09/28/2023
Styrene
SW 846 Method 8260DIS030B
<0.5 pg/L
09/28/2023
tert-Butylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Tetrachloroethene
SW &46 Method 82600/50308
<0.5 pg/L
09/28/2023
Report #- 2023-22412
Page 8 of 9

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info;a environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Oct 09, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-22412
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Trans- 1,2-Dichloroethene
Sw846Me" e26=50308
<0.5 pg/L
09/28/2023
Trans- 1,3-dichloropropene
SW 846 Method 826oD/5030B
<0.5 pg/L
09/28/2023
Trichloroethene
SW 846 Method e26ODr5030B
<0.5 pg/L
09/28/2023
Trichlorofluoromethane
SW 846 Method 826oD/5030B
<0,5 pg/L
09/28/2023
Vinyl chloride
SW 846 Method 8260D15030B
<0.5 pg/L
09/28/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev 2 0, 1993
0.07 mg/L
09/27/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev 2.0, 1993
< 0.02 mg/L
10/02/2023
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
10/04/2023
Comment:
�n a
^n . /--A`n ` n
Reviewed by:
Report # 2023 22412 Page 9 of 9

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Client: C��i1 C� W�l Date: Report Number: _ 2023- 2Apti
Receipt of sample: ECHEM Pickup Client Delivery ❑
1UPS 17 FeclEx ❑ Other ❑
❑ YES
10 NO
1 N N/A
I,. Were custody seals present on the cooler?
❑ YES
113 NO
IN N/A
12. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank N Against Bottles
I Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
N YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
N YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
N YES
❑ NO
S. Were sample ID's listed on the COC?
N YES
❑ NO
6. Were samples ID's listed on sample containers?
N YES
❑ NO
7. Were collection date and time listed on the COC?
N YES
❑ NO
8. Were tests to be performed listed on the COC?
N YES
❑ NO
9. Did samples arrive in proper containers for each test?
N YES
❑ NO
10. Did samples arrive in good condition for each test?
N YES
❑ NO
11. Was adequate sample volume availableT
N YES
❑ NO
12. Were samples received within proper holding time for requested tests?
YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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F"07— Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
© 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
s 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
City of Jacksonville
Date of Report: Oct 25, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-22604
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-55114 Site: MW-2
9/28/2023
12:42 PM Water MULC
Test
Method
Results
Date Analyzed
Sulfate
EPA 300.0, Rev 2.1. 1993
12 mg/L
10/02/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
16.6 mg/L
10/03/2023
Chloride
SM4500 CI E-2011
57 mg/L
09/29/2023
1,1,1,2-Tetrach loroethane
SW 846 Method 8260D/5030B
<0,5 pg/L
10/05/2023
1,1,1-Trichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
10/05/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D 5030B
<0.5 pg/L
10/05/2023
1,1,2-Trichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
1, 1 -Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
1,1-Dichloroethene
SW B46 Method 82BOD15030B
<0 5 pg/L
10/05/2023
1,1-Dichloropropene
SW 846 Method 8260D/5030B
<0 5 pg/L
10/05/2023
1,2,3-Trichlorobenzene
SW 846 Method 826OD150303
<0.5 pg/L
10/05/2023
1,2,3-Trichloropropane
SW 846 Method8260D/50308
<0 5 pg/L
10/05/2023
1,2,4-Trichlorobenzene
SW 846 Method 8260D15030B
<0 5 pg/L
10/05/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
10/05/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 826OD15030B
<1 pg/L
10/05/2023
1,2-Dibromoethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
1,2-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
1,2-Dichloroethane
SW 846 Method 8260D15030B
<0 5 pg/L
10/05/2023
1,2-Dichloropropane
SW 846 Method 8260D 5030E
<0.5 pg/L
10/05/2023
1,3,5-Trimethylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
10/05/2023
1,3-Dichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
10/05/2023
1, 3-Dichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
10/05/2023
1,4-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
2,2-Dichloropropane
SW 846 Method 826GD15030B
<0.5 pg/L
10/05/2023
2-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
4-Chlorotoluene
SW 846 Method 826oD/5030B
<0.5 pg/L
10/05/2023
Report #- 2023-22604
Pagel of 24

77 Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
® 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
611, 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Date of Report: Oct 25, 2023
City of Jacksonville
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-22604
Project ID: Monitoring Wells
Benzene
SW 846 Method 826oD/5030B
<0.5 pg/L
10/05/2023
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Bromodichloromethane
SW 846 Method 826oD/5030B
<0.5 pg/L
10/05/2023
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Carbon tetrachloride
SW 646 Method 8280D/5030B
<0.5 pg/L
10/05/2023
Chlorobenzene
SW 646 Method 8260D/50308
<0.5 pg/L
10/05/2023
Chloroethane
SW B46 Method 826OD15030B
<0.5 pg/L
10/05/2023
Chloroform
SW 846 Method 8260D15030B
<0.5 pg/L
10/05/2023
Chloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
cis-1,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
10/05/2023
cis-1,3-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Dibromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
Dibromomethane
SW 846 Method 8260D/50308
<0.5 pg/L
10/05/2023
Dichlorodifluoromethane
SW 846 Method 8260D 5030E
<0.5 pg/L
10/05/2023
Ethylbenzene
SW 846 Method 8260D 5030E
<0.5 pg/L
10/05/2023
Hexachlorobutadtene
SW 846 Method 8260D5030B
<0.5 pg/L
10/05/2023
Isopropylbenzene
SW 846 Method 8260D 5030B
<0.5 pg/L
10/05/2023
M+P Xylene
SW 846 Method 826OD150308
<1.0 pg/L
10/05/2023
Methylene chloride
SW 846 Method 8260U50306
<0.5 pg/L
10/05/2023
Naphthalene
SW 846 Method 8260D15030B
<0.5 pg/L
10/05/2023
n-Butyibenzene
SW 846 Method 8260D15030B
<0.5 pg/L
10/05/2023
n-Propylbenzene
SW 846 Method 8260D 50308
<0.5 pg/L
10/05/2023
ortho-Xylene
SW 846 Method 8260D 5030E
<0.5 pg/L
10/05/2023
p-Isopropyltoluene
SW 846 Method 8260D.5030B
<0.5 pg/L
10/05/2023
sec-Butylbenzene
SW 846 Method 8280D/5030B
<0.5 pg/L
10/05/2023
Styrene
SW 846 Method 82BOD15030B
<0.5 pg/L
10/05/2023
tert-Butylbenzene
SW 846 Method 826GO15030B
<0.5 pg/L
10/05/2023
Tetrachloroethene
SW 646 Method 828OD15030B
<0.5 pg/L
10/05/2023
Report #- 2023-22604
Page 2 of 24

F"I", -- 77
ANALYTICAL & CONSULTING CHEMISTS
City of Jacksonville
Post Office Box 128
Jacksonville NC 28541
Attention.
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Oct 25, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-22604
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Trans-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Trans- 1,3-dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353 2, Rev 2 0, 1993
0.08 mg/L
09/28/2023
Nitrate+Nitrite-Nitrogen
EPA 3532 Rev 2 0,1993
0.07 mg/L
10/03/2023
Nitrate Nitrogen
Subtraction Method
<0.02mg/L
10/11/2023
Report tt 2023-22604 Page 3 of 24

—.-Oqql
Environmental Chemists,
Inc.
•
6602 Windmill Way,
Wilmington, NC 29405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown
Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
-
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
info;a!environmentalchemists.com
City of Jacksonville
Date of Report: Oct 25, 2023
Post Office Sox 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-22604
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
23-55115 Site: MW-3
9/28/2023
11-50 AM Water MULC
Test
Method
Results Date Analyzed
Sulfate
EPA 300 0 Rev 2 1, 1993
<5 mg/L
10/02/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
2.7 mg/L
10/03/2023
Chloride
SM4500 Q E-2011
10 mg/L
09/29/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 8260D�5030B
<0.5 pg/L
10/04/2023
1, 1, 1 -Trichloroethane
SW 846 Method 8260D,5030B
<0.5 pg/L
10/04/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D. 5o OB
<0.5 pg/L
10/04/2023
1,1,2-Trichloroethane
SW 846 Method 82601)�50306
<0.5 pg/L
10/04/2023
1, 1 -Dich loroethane
SW 846 Method 826oD/50308
<0.5 pg/L
10/04/2023
1,1-Dichloroethene
SW 846 Method 826OD/5030B
<0.5 pg/L
10/04/2023
1,1-Dichloropropene
SW 846 Method 82BOD15030B
<0.5 pg/L
10/04/2023
1,2,3-Trichlorobenzene
SW 846 Method 8280D/50306
<0.5 pg/L
10/04/2023
1,2,3-Trichloropropane
SW 845 Method 8260DIS030B
<0.5 pg/L
10/04/2023
1,2,4-Trichlorobenzene
SW 846 Method 826OD150308
<0.5 pg/L
10/04/2023
1,2,4-Trimethylbenzene
SW 646 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260015030B
<1 pg/L
10/04/2023
1,2-Dibromoethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,2-Dichlorobenzene
SW 846 Method 8260DI5030B
<0.5 pg/L
10/04/2023
1,2-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,2-Dichloropropane
SW 846 Method 826OD/50308
<0.5 pg/L
10/04/2023
1,3,5-Trimethyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1, 3-Dichlorobenzene
SW 846 Method 826OD150308
<0.5 pg/L
10/04/2023
1,3-Dichloropropane
SW B46 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,4-Dichlorobenzene
SW 846 Method 8260015030B
<0.5 pg/L
10/04/2023
2,2-Dichloropropane
SW 846 Method 82BOD15030B
<0.5 pg/L
10/04/2023
2-Chlorotoluene
SW 846 Method 826ODI5030B
<0,5 pg/L
10/04/2023
4-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Report # 2023-22604
Page 4 of 24

envirochem
ANALYTICAL & CONSULTING CHEMISTS
F"00— -- —. -00441
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Rowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville
Date of Report: Oct 25, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-22604
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Bromobenzene
SW 846 Method 8260DI5030B
<0.5 pg/L
10/04/2023
Bromochloromethane
SW 846 Method 8260D/50306
<0.5 pg/L
10/04/2023
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
10/0412023
Bromomethane
SW 846 Method 8260D16030B
<0.5 pg/L
10/04/2023
Carbon tetrachloride
SW 846 Method 8280D/5030B
<0.5 pg/L
10/04/2023
Chlorobenzene
SW 846 Method 82BOD150308
<0.5 pg/L
10/04/2023
Chloroethane
SW 846 Method 82BOD15030B
<0.5 pg/L
10/04/2023
Chloroform
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Chloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
cis-1,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
cis-1,3-Dichloropropene
SW 846 Method 8260015030E
<0.5 pg/L
10/04/2023
Dibromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Dibromomethane
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Dichlorodifluoromethane
SW 846 Method 8260D150308
<0.5 pg/L
10/04/2023
Ethylbenzene
SW 846 Method 8260D150308
<0.5 pg/L
10/04/2023
Hexachlorobutadiene
SW 846 Method 8260D/50308
<0.5 pg/L
10/04/2023
Isopropylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
10/04/2023
Methylene chloride
SW 846 Method 8280D/50308
<0.5 pg/L
10/04/2023
Naphthalene
SW 846 Method 8260D/50308
<0.5 pg/L
10/04/2023
n-Butylbenzene
SW 846 Method 8260DIS030B
<0.5 pg/L
10/04/2023
n-Propylbenzene
SW 846 Method 8260015030B
<0.5 pg/L
10/04/2023
ortho-Xylene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
p-Isopropyltoluene
SW 846 Method 826oDI50308
24.0 pg/L
10/04/2023
sec-Butylbenzene
SW 846 Method 82BOD150308
<0.5 pg/L
10/04/2023
Styrene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
tert-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Tetrachloroethene
SW 846 Method 8260D150308
<0.5 pg/L
10/04/2023
Report #:: 2023-22604
Page 5 of 24

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville
Date of Report: Oct 25, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention.
Report #: 2023-22604
Project ID: Monitoring Wells
Toluene
SW 846 Method 826oD/5030B
12.3 pg/L
10/04/2023
Trans- 1,2-Dichloroethene
SW 846 Method 826oD/5030B
<0.5 pg/L
10/04/2023
Trans- 1,3-dichloropropene
SW 846 Method 8260Dl5030B
<0.5 pg/L
10/04/2023
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Trichlorofluoromethane
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Vinyl chloride
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353 2, Rev 2 0, 1993 < 0.02 mg/L 09/28/2023
Nitrate+Nitrite-Nitrogen EPA 3532 Rev 2 0, 1993 < 0.02 mg/L 10/03/2023
Nitrate Nitrogen Subtraction Method <0.02mg/L 10111/2023
Report # 2023-22604 Page 6 0f 24

envirochem
O
ANALYTICAL & CONSULTING CHEMISTS
City of Jacksonville
Post Office Box 128
Jacksonville NC 28541
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab; Fax
[e-mail]
Date of Report: Oct 25, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-22604
Project 1D: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-55116 Site: MW-4
9/28/2023
10:54 AM Water ML/LC
Test
Method
Results Date Analyzed
Sulfate
EPA 300.0. Rev 2 1, 1993
42 mg/L
10/02/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
1.3 mg/L
10/03/2023
Chloride
SM4500 CE E-2011
51 mg/L
09/29/2023
1, 1, 1,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,1,1-Trichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 826OD16030B
<0.5 pg/L
10/04/2023
1,1,2-Trichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
1,1-Dichloroethane
SW 845 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,1-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,1-Dichloropropene
SW 846 Method 82BOD15030B
<0.5 pg/L
10/04/2023
1,2,3-Trichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,2,3-Trichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,2,4-Trichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,2,4-Trimethyl benzene
SW 846 Method 826OD150306
<0.5 pg/L
10/04/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 826OD15030B
<1 pg/L
10/04/2023
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,2-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1, 2-Dichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
1,2-Dichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1, 3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1, 3-Dichloropropane
SW 846 Method 8260D150308
<0.5 pg/L
10/04/2023
1,4-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
2,2-Dichloropropane
SW 846 Method 826oW503013
<0.5 pg/L
10/04/2023
2-Chlorotoluene
SW 846 Method 826oD15030B
<0.5 pg/L
10/04/2023
4-Chlorotoluene
SW 846 Method 8260D150308
<0.5 pg/L
10/04/2023
Report #:: 2023-22604
Page 7 of 24

F"00, -- -."'047 Environmental Chemists, Inc.
envirochem j 6602 Windmill Way, Wilmington, NC 29405 . 910.392.0223 Lab . 910.392.4424 Fax
© 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
s 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Date of Report: Oct 25, 2023
City of Jacksonville
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-22604
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Bromobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
10/04/2023
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Bromoform
SW 846 Method 8260D/50308
<0.5 pg/L
10/04/2023
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Chlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Chloroethane
SW 846 Method 8260150308
<Q.5 pg/L
10/04/2023
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
cis-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
cis-1,3-Dichloropropene
SW 846 Method 82600150308
<0.5 pg/L
10/04/2023
Dibromochloromethane
SW 846 Method 826oD150306
<0.5 pg/L
10/04/2023
Dibromomethane
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Dichlorodifluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Ethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Hexachlorobutadiene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Isopropylbenzene
SW 846 Method 826oD/5030B
<0.5 pg/L
10/04/2023
M+P Xylene
SW 846 Method 8260D15030B
<1.0 pg/L
10/04/2023
Methylene chloride
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Naphthalene
SW 846 Method 8280D/5030B
<0.5 pg/L
10/04/2023
n-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
n-Propylbenzene
SW 846 Method 8260DIS030B
<0.5 pg/L
10/04/2023
ortho-Xylene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
p-Isopropyltoluene
SW 846 Method 82BOD15030B
<0.5 pg/L
10/04/2023
sec-Butylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
10/04/2023
Styrene
SW 846 Method 8260D/50308
<0.5 pg/L
10/04/2023
tert-Butyl benzene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Tetrachloroethene
SW 845 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Report # 2023.22604
Page 8 of 24

rooww' 7 77
ISMI
ANALYTICAL & CONSULTING CHEMISTS
City of Jacksonville
Post Office Box 128
Jacksonville NC 28541
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
info;a:environmentalchemists.com
Date of Report: Oct 25, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-22604
Project ID: Monitoring Wells
Toluene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Trans-1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 ug/L
10/04/2023
Trans- 1,3-dichloropropene
SW 846 Method 8260D/5030B
<0.5 gg/L
10/04/2023
Trichloroethene
SW 846 Method 8260D,5030B
<0.5 pg/L
10/04/2023
Trichlorofluoromethane
SW 846 Method 8260D 5030E
<0.5 pg/L
10/04/2023
Vinyl chloride
SW 846 Method 8260D 50308
<0.5 pg/L
10/04/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA353.2, Rev 20 1993
< 0.02 mg/L
09/28/2023
Nitrate+Nitrite-Nitrogen
EPA 353 2, Rev 2 o 1993
< 0.02 mg/L
10/03/2023
Nitrate Nitrogen
Subtraction Method
<0.02mg/L
10/11/2023
Report # 2023-22604 page 9 of 24

envirochem
40
ANALYTICAL & CONSULTING CHEMISTS
City of Jacksonville
Post Office Box 128
Jacksonville
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Oct 25, 2023
Customer PO #:
NC 28541 Customer ID: 08110015
Report #: 2023-22604
Project ID: Monitoring Wells
Lab ID Sample ID:
23-55117 Site: MW-5
Test
Sulfate
Total Organic Carbon (TOC)
Chloride
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1, 1,2-Trichloroeth a ne
1,1-Dichloroethane
1, 1 -Dich loroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethyibenzene
1, 2-Dibromo-3-Ch loropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1, 3, 5-Tri methylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Collect Date/Time Matrix
9/28/2023 9:32 AM Water
Method
EPA 300.0, Rev. 2.1, 1993
SM 5310 B-2014
SM4500 CI E-2011
SW 846 Method 8260D/50308
SW 846 Method 8260D15030B
SW 846 Method 8260D15030B
SW 846 Method 8260015030B
SW 846 Method 8260D15030B
SW 846 Method 826OD150308
SW 846 Method 826OD15030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D150308
SW 846 Method 826OD15030B
SW 846 Method 826OD15030B
SW 846 Method 826OD15030B
SW 846 Method 8260D/50308
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5o3OB
SW 846 Method 8280D/50308
SW 846 Method 82600/503013
SW 846 Method 8260D15030B
SW 846 Method 8260D150308
SW 846 Method 8260D/5030B
Results
Sampled by
MULC
Date Analyzed
<5 mg/L
10/02/2023
<0.5 mg/L
10/03/2023
10 mg/L
09/29/2023
<0.5 pg/L
10/04/2023
<0.5 pg/L
10/04/2023
<0.5 pg/L
10104/2023
<0.5 pg/L
10/04/2023
<0.5 pg/L
10/04/2023
<0.5 pg/L
10/04/2023
<0.5 pg/L
10/04/2023
<0.5 pg/L
10/04/2023
<0.5 pg/L
10/04/2023
<0.5 pg/L
10/04/2023
<0.5 pg/L
10/04/2023
<1 pg/L
10/04/2023
<0.5 pg/L
10/04/2023
<0.5 pg/L
10104/2023
<0.5 pg/L
10/04/2023
<0.5 pg/L
10/04/2023
<0.5 pq/L
10/04/2023
<0.5 pg/L
10/04/2023
<0.5 pg/L
10/04/2023
<0.5 pg/L
10/04/2023
<0.5 pg/L
10/04/2023
<0.5 pg/L
10/04/2023
<0.5 pg/L
10/04/2023
Report # 2023-22604 Page 10 of 24

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910-392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville Date of Report: Oct 25, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-22604
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Bromochloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Bromodichloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Bromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Carbon tetrachloride
SW 846 Method 8280/5030B
<0.5 pg/L
10/04/2023
Chlorobenzene
SW 848 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Chloroethane
SW 846 Method 826OD/5030B
<0.5 pg/L
10/04/2023
Chloroform
SW 846 Method 826oa/5030B
<0.5 pg/L
10104/2023
Chloromethane
SW 846 Method 8266D/5030B
<0.5 pg/L
10/04/2023
cis-1,2-Dichloroethene
SW 846 Method 8260D150308
<0.5 pg/L
10/04/2023
cis-1,3-Dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Dibromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Dibromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Dichlorodifluoromethane
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Ethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Isopropylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
10/04/2023
Methylene chloride
SW 846 Method 82600/5030B
<0.5 pg/L
10/04/2023
Naphthalene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
n-Butylbenzene
SW 846 Method 8260D/50306
<0.5 pg/L
10/04/2023
n-Propylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
ortho-Xylene
SW 846 Method 8260D/50308
<0.5 pg/L
10/04/2023
p-Isopropyltoluene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
sec-Butylbenzene
SW 846 Method 826oD/5030B
<0.5 pg/L
10/04/2023
Styrene
SW 848 Method 8260D/5030B
<0.5 pg/L
10/04/2023
tert-Butylbenzene
SW 846 Method 8260D/50306
<0.5 pg/L
10/04/2023
Tetrachloroethene
SW 848 Method 826OD16030B
<0.5 pg/L
10/04/2023
Report #:: 2023-22604
Page 11 of 24

F0100-7 _747
40
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Oct 25, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-22604
Project ID: Monitoring Wells
Toluene
SW 846 Method 82600/5030B
<0.5 pg/L
10/04/2023
Trans-1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Trans- 1,3-dichloropropene
SW 846 Method8260D/5030B
<0.5pg/L
10/04/2023
Trichloroethene
SW 846 Method 8260D/5030B
<0,5 pg/L
10/04/2023
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Vinyl chloride
SW 846 Method 82BOD15030B
<0.5 pg/L
10/04/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
< 0.02 mg/L
09/28/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
< 0.02 mg/L
10/03/2023
Nitrate Nitrogen
Subtraction Method
<0.02mg/L
10/11/2023
Report #:: 2023-22604 Page 12 of 24

SM
ANALYTICAL & CONSULTING CHEMISTS
F"10- -- _747
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville
Date of Report: Oct 25, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention.-
Report #: 2023-22604
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-55118 Site: MW-15
9/28/2023
1:56 PM Water MULC
Test
Method
Results
Date Analyzed
Sulfate
EPA 300.0, Rev. 2.1, 1993
<5 mg/L
10/02/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
1.5 mg/L
10/03/2023
Chloride
SM4500 CI E-2011
52 mg/L
09/29/2023
1, 1, 1,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1, 1, 1 -Trichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,1,2-Trichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,1-Dichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
1,1-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,1-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,2,3-Trichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,2,3-Trichooropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,2,4-Trichlorobenzene
SW 846 Method 826oD/5030B
<0.5 pg/L
10/04/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
<1 pg/L
10/04/2023
1,2-Dibromoethane
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
1,2-Dichlorobenzene
SW 846 Method 826OD150308
<0.5 pg/L
10/04/2023
12-Dichloroethane
SW 846 Method 8260015030E
<0.5 pg/L
10/04/2023
1,2-Dichloropropane
SW 846 Method 82600/5030B
<0,5 pg/L
10/04/2023
1, 3, 5-Trimethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,3-Dichlorobenzene
SW 845 Method 8260D/50308
<0.5 pg/L
10/04/2023
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
4-Chlorotoluene
SW 846 Method 826OD150308
<0.5 pg/L
10/04/2023
Report #:: 2023-22604
Page 13 of 24

--71
envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville Date of Report: Oct 25, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-22604
Project ID: Monitoring Wells
Benzene
SW 846 Method 826oD/5030B
<0.5 pg/L
10/04/2023
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Bromodichloromethane
SW 846 Method 826OD150308
<0.5 pg/L
10/04/2023
Bromoform
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Bromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Carbon tetrachloride
SW 846 Method 8260D/50308
<0.5 pg/L
10/04/2023
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Chloroethane
SW 846 Method 826=5030B
<0.5 pg/L
10/04/2023
Chloroform
SW 846 Method 82600150308
<0.5 pg/L
10/04/2023
Chloromethane
SW 846 Method 826OD150308
<0.5 pg/L
10/04/2023
cis-1,2-Dichloroethene
SW 846 Method 8260016030E
<0.5 pg/L
10/04/2023
cis- 1,3-Dichloropropene
SW 846 Method 826oD/5030B
<0.5 pg/L
10/04/2023
Dibromochloromethane
SW 846 Method 8260D/503oB
<0.5 pg/L
10/04/2023
Dibromomethane
SW 846 Method B26OD15030B
<0.5 pg/L
10/04/2023
Dichlorodifluoromethane
SW 846 Method 82600/5030B
<0.5 pg/L
10/04/2023
Ethylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
10/04/2023
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Isopropylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
M+P Xylene
SW 846 Method 8260/5030B
<1.0 pg/L
10/04/2023
Methylene chloride
SW 846 Method 8260D150306
<0.5 pg/L
10/04/2023
Naphthalene
SW 846 Method 826oD/5030B
<0.5 pg/L
10/04/2023
n-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pq/L
10/04/2023
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
ortho-Xylene
SW 846 Method 8280D150308
<0.5 pg/L
10/04/2023
p-Isopropyitoluene
SW 846 Method 8260D/50308
<0.5 pg/L
10/04/2023
sec -Butyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Styrene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
tert-Butylbenzene
SW 846 Method 8260D150308
<0.5 pg/L
10/04/2023
Tetrachloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Report # 2023.22604
Page 14 of 24

Environmental Chemists, Inc.
• 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
® 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28W . 910.347.5843 Lab/Fax
ANALYTICAL 8r CONSULTING CHEMISTS [e-mail]
City of Jacksonville
Date of Report: Oct 25, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-22604
Project ID: Monitoring Wells
Toluene
SW 846 Method 826oD/5030B
<0.5 pg/L
10/04/2023
Trans-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Trans-1,3-dichloropropene
SW 846 Method 8280D/5030B
<0.5 pg/L
10/04/2023
Trichloroethene
SW 846 Method 826OD150303
<0.5 pg/L
10/04/2023
Trichlorofluoromethane
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Vinyl chloride
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Nitrate Nitrogen (Calc)
!Nitrite Nitrogen
EPA353.2, Rev. 2.0, 1993
< 0.02 mg/L
09/28/2023
Nitrate+Nitrite-Nitrogen
EPA353.2, Rev. 2.0, 1993
1.13 mg/L
10/03/2023
Nitrate Nitrogen
Subtraction Method
1.13mg/L
10/11/2023
Report #• 2023-22604 Page 15 of 24

-,""7
Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
40 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
City of Jacksonville
Date of Report: Oct 25, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-22604
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
23-55119 Site: MW-11
9/28/2023
8:30 AM Water ML/LC
Test
Method
Results
Date Analyzed
Sulfate
EPA 300.0, Rev 2 1, 1993
<5 mg/L
10/02/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
<0.5 mg/L
10/03/2023
Chloride
SM4500 ci E-2011
< 5 mg/L
09/29/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 82600/5030B
<0.5 pg/L
10/04/2023
1,1,1-Trich loroethane
SW 846 Method 8280015030E
<0.5 pg/L
10/04/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260015030E
<0.5 pg/L
10/04/2023
1,1,2-Trichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,1-Dichloroethane
SW 846 Method 8260DIS030B
<0.5 pg/L
10/04/2023
1,1-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
1,1-Dichloropropene
SW 846 Method 8260D/50300
<0.5 pg/L
10/04/2023
1,2,3-Trichlorobenzene
SW 846 Method MOD15030B
<0.5 pg/L
10/04/2023
1,2,3-Trichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,2,4-Trichlorobenzene
SW 846 Method 82600/5030B
<0.5 pg/L
10/04/2023
1,2,4-Trimethyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8280D15030B
<1 pg/L
10/04/2023
1,2-Dibromoethane
SW 846 Method 828OD15030B
<0.5 pg/L
10/04/2023
1,2-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,2-Dichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,2-Dichloropropane
SW 846 Method 826OD16030B
<0.5 pg/L
10/04/2023
1,3,5-Trimethylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
10/04/2023
1, 3-Dichlorobenzene
SW 846 Method MODIS030B
<0.5 pg/L
10/04/2023
1,3-Dichloropropane
SW 846 Method 82600/5030B
<0.5 pg/L
10/04/2023
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
2-Chlorotoluene
SW 846 Method 8260DIS0308
<0.5 pg/L
10/04/2023
4-Chlorotoluene
sw 846 Method 8260015030E
<0.5 pg/L
10/04/2023
Report #: 2023-22604
Page 16 of 24

Environmental Chemists, Inc.
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville Date of Report: Oct 25, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-22604
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Bromobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Bromochloromethane
SW 845 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Bromomethane
SW 846 Method 826OD150308
<0.5 pg/L
10/04/2023
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Chloroethane
SW 846 Method 826OD/5030B
<0.5 pg/L
10/04/2023
Chloroform
SW 846 Method 8260D/6030B
<0.5 pg/L
10/04/2023
Chloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
cis- 1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
cis-1,3-Dichloropropene
SW 846 Method 8260DIS030B
<0.5 pg/L
10/04/2023
Dibromochloromethane
SW 846 Method 6260DIS030B
<0.5 pg/L
10/04/2023
Dibromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Dichlorodifluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Ethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Hexachlorobutadiene
SW 846 Method 82BOD/5030B
<0.5 pg/L
10/04/2023
Isopropylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
10/04/2023
Methylene chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Naphthalene
SW 846 Method 826oD/5D306
<0.5 pg/L
10/04/2023
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
n-Propyibenzene
SW 846 Method 826oD/5030B
<0.5 pg/L
10/04/2023
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
p-Isopropyltoluene
SW 846 Method 8260D/50308
<0.5 pg/L
10104/2023
sec-Butylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
10/04/2023
Styrene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
tert-Butyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Tetrachloroethene
SW 846 Method 82BOD/5030B
<0.5 pg/L
10/04/2023
Report # 2023-22604
Page 17 of 24

-�7
Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
© 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
s 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
City of Jacksonville
Date of Report: Oct 25, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-22604
Project ID: Monitoring Wells
Toluene
SW 648 Method 8260DIS0308
<0.5 pg/L
10/04/2023
Trans- 1,2-Dichloroethene
SW 846 Method 8260DIS030B
<0.5 pg/L
10/04/2023
Trans- 1,3-dichloropropene
SW 846 Method 8260Dl503013
<0.5 pg/L
10/04/2023
Trichloroethene
SW 846 Method 826OD15030B
<0.5 ug/L
10/04/2023
Trichlorofluoromethane
SW 848 Method 826OD15030B
<0,5 ug/L
10/04/2023
Vinyl chloride
SW 846 Method 8260D15030B
<0,5 ug/L
10/04/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 3532. Rev. 2.0, 1993
< 0.02 mg/L
09/28/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.51 mg/L
10/03/2023
Nitrate Nitrogen
Subtraction Method
0.51 mg/L
10/11/2023
Report tt: 2023-22604 Page 18 of 24

ANALYTICAL & CONSULTING CHEMISTS
F"0007-7"ql
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville Date of Report: Oct 25, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-22604
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-55120 Site: MW-1 9/28/2023 9:45 AM Water ML/LC
Test Method Results Date Analyzed
Sulfate
EPA 300.0. Rev. 2.1, 1993
18 mg/L
10/02/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
10.2 mg/L
10/03/2023
Chloride
SM4500 C1 E-2011
53 mg/L
09/29/2023
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
1, 1, 1 -Trichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,1,2,2-Tetrach loroethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,1,2-Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,1-Dichloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
10/04/2023
1,1-Dichloroethene
SW 846 Method 8260D/50308
<0.5 pg/L
10/04/2023
1,1-Dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
10/04/2023
1,2,3-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,2,3-Trichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,2,4-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,2,4-Trimethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 826OD15030B
<1 pg/L
10/04/2023
1,2-Dibromoethane
SW 846 Method 82600/5030B
<0.5 pg/L
10/04/2023
1,2-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,2-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,2-Dichloropropane
SW 846 Method 826oD/5030B
<0.5 pg/L
10/04/2023
1,3,5-Trimethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10104/2023
1,3-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
2,2-Dichloropropane
SW 846 Method 826OD150308
<0.5 pg/L
10/04/2023
2-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
4-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Report #. 2023-22604 Page 19 of 24

F"07- I
envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowser -town Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
info@envi ronmen talchemists. com
City of Jacksonville
Date of Report: Oct 25, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-22604
Project ID: Monitoring Wells
Benzene
SW 846 Method 82600150308
<0.5 pg/L
10/04/2023
Bromobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Bromochloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Bromodichloromethane
SW 846 Method 8260DY5030B
<0.5 pg/L
10/04/2023
Bromoform
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Bromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Carbon tetrachloride
SW 846 Method 826oD15030B
<0.5 pg/L
10104/2023
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Chloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Chloroform
SW 846 Method 826OD15030B
<0.5 pg/L
10/0412023
Chloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
cis- 1,2-Dichloroethene
SW 846 Method 8260015030E
<0.5 pg/L
10/04/2023
cis- 1,3-Dichloropropene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Dibromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Dibromomethane
SW 845 Method 8260D15030B
<0.5 pg/L
10/04/2023
Dichlorodifluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Ethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
10104/2023
1sopropylbenzene
SW 846 Method 8280D/5030B
<0.5 pg/L
10/0412023
M+P Xylene
SW 846 Method 8260w5mm
<1.0 pg/L
10/04/2023
Methylene chloride
SW 846 Method 8260015030E
<0.5 pg/L
10/04/2023
Naphthalene
SW 846 Method 82BOD15030B
<0.5 pg/L
10/04/2023
n-Butylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
n-Propylbenzene
SW 846 Method 8260D/50308
<0.5 pq/L
10/04/2023
ortho-Xylene
SW 846 Method 8280D/5030B
<0.5 pg/L
10/04/2023
p-Isopropyltoluene
SW 846 Method 8280D/5030B
<0.5 pg/L
10104/2023
sec-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Styrene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
tert-Butylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Tetrachloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Report #. 2023-22604
Page 20 of 24

777 Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
® 710 Rowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoi'u environmentalchemists.com
City of Jacksonville
Date of Report: Oct 25, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-22604
Project ID: Monitoring Wells
Toluene
SW 846 Method 8280D/5030B
<0.5 pg/L
10/04/2023
Trans- 1,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Trans- 1,3-dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Tnchlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
< 0.02 mg/L
09/28/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
< 0.02 mg/L
10/03/2023
Nitrate Nitrogen
Subtraction Method
<0.02mg/L
10/11/2023
Report p 2023-22604 Page 21 of 24

F""� -- 7ql
SM
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville
Date of Report: Oct 25, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-22604
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-55121 Site: MW-16
9/28/2023
11:30 AM Water ML/LC
Test
Method
Results
Date Analyzed
Sulfate
EPA 300.0, Rev. 2.1. 1993
13 mg/L
10/02/2023
Total Organic Carbon (TOC)
SM 5310 8-2014
2.3 mg/L
10/03/2023
Chloride
SM4500 C1 E-2011
32 mg/L
09/29/2023
1, 1, 1,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1, 1, 1-Trichloroethane
SW 846 Method 82BOD150308
<0.5 pg/L
10/04/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
10/04/2023
1,1,2-Trich loroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,1-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,1-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,1-Dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,2,3-Trichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
1,2,3-Trichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
1,2,4-Trichlorobenzene
SW 646 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,2,4-Trimethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260015030B
<1 pg/L
10/04/2023
1,2-Dibromoethane
SW 846 Method 82e0D/50308
<0.5 pg/L
10/04/2023
1,2-Dichlorobenzene
SW 846 Method 826OD16030B
<0.5 pg/L
10/04/2023
1,2-Dichloroethane
SW 846 Method 8260D/5039B
<0.5 pg/L
10/04/2023
1,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
1,3,5-Trimethyl benzene
SW 846 Method 8260D/50308
<0.5 pg/L
10/04/2023
1, 3-Dichlorobenzene
SW 846 Method 826OD150308
<0.5 pg/L
10/04/2023
1,3-Dichloropropane
SW 846 Method 826OD160308
<0.5 pg/L
10/04/2023
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
2,2-Dichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
4-Chlorotoluene
SW 846 Method 826OD150308
<0.5 pg/L
10/04/2023
Report #.-. 2023-22604
Page 22 of 24

Environmental Chemists, Inc.
IL envirochem
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
info@envi ronmentalchemists.com
City of Jacksonville Date of Report: Oct 25, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-22604
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D/50308
<0.5 pg/L
10/04/2023
Bromobenzene
SW 846 Method 826013/5030B
<0.5 pg/L
10/04/2023
Bromochloromethane
SW 846 Method 826oD/5030B
<0.5 pg/L
10/04/2023
Bromodichloromethane
SW 846 Method 826OD150303
<0.5 pg/L
10/04/2023
Bromoform
SW 846 Method 8260D/50308
<0.5 pg/L
10/04/2023
Bromomethane
SW 846 Method 8260D1503GB
<0.5 pg/L
10/04/2023
Carbon tetrachloride
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Chloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Chloroform
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Chloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
cis-1,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
cis-1,3-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Dibromochloromethane
SW 846 Method MOD15030B
<0.5 pg/L
10/04/2023
Dibromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Dichlorodifluoromethane
SW 846 Method 8260D150308
<0.5 pg/L
10/04/2023
Ethylbenzene
SW 846 Method 82600/5030B
<0.5 pg/L
10/04/2023
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Isopropylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
M+P Xylene
SW 846 Method 8260D15030B
<1.0 pg/L
10/04/2023
Methylene chloride
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Naphthalene
sW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
n-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
p-Isopropyltoluene
SW 846 Method 82500/5030B
<0.5 pg/L
10/04/2023
sec -Butyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Styrene
SW 846 Method 626OD15030B
<0.5 pg/L
10/04/2023
tert-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Tetrachloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Report M 2023-22604
Page 23 of 24

0
ANALYTICAL & CONSULTING CHEMISTS
F"'50' -- 71
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville
Post Office Box 128
Jacksonville NC 28541
Attention:
Date of Report: Oct 25, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-22604
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260015030B
<0.5 pg/L
10/04/2023
Trans- 1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
10/04/2023
Trans- 1,3-dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Trichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
10/04/2023
Trichlorofluoromethane
SW 846 Method 8260D/50300
<0.5 pg/L
10/04/2023
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
10/04/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0. 1993
< 0.02 mg/L
09/28/2023
Nitrate+ N itrite-N itrogen
EPA 353.2, Rev. 2.0. 1993
0.24 mg/L
10/03/2023
Nitrate Nitrogen
Subtraction Method
0.24 mg/L
10/11/2023
Comment:
Reviewed by: Koj,-Au,
Report # 2023-22604 Page 24 of 24

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Client: F Date: C Report Number: _ 2023- a d
Receipt of sample: ECHEM Pickup Client Delivery O
JUPS ❑ FeclEx ❑ Other ❑
❑ YES
❑ NO
❑x N/A
1. Were custody seals present on the cooler?
❑ YES
ID NO
IN N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank 0 Against Bottles
IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
O YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
❑x YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed?
x❑ YES ❑ NO 5. Were sample ID's listed on the COC?
l YES ❑ NO 6. Were samples ID's listed on sample containers?
1XI YES ❑ NO 7. Were collection date and time listed on the COC?
I] YES ❑ NO 8. Were tests to be performed listed on the COC?
Z YES
❑ NO
9. Did samples arrive in proper containers for each test?
0 YES
❑ NO
10. Did samples arrive in good condition for each test?
O YES
❑ NO
11. Was adequate sample volume availableT
Z YES
❑ NO
12. Were samples received within proper holding time for requested tests?
YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
❑ YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCl NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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ANALYTICAL & CONSULTING CHEMISTS
F"00- -- -:O"qql
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910,392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
info(& environment alchemists. com
City of Jacksonville
Date of Report: Oct 25, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-22671
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-55260 Site: MW-17
9/28/2023
2:26 PM Water DT/CB
Test
Method
Results
Date Analyzed
Sulfate
EPA 300 0 Rev 2 1. 1993
12 mg/L
10/02/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
0.9 mg/L
10/03/2023
Chloride
SM4500 CI E-2011
38 mg/L
10/06/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 8260D, winB
<0.5 pg/L
10/05/2023
1,1,1-Trichloroethane
SW 846 Method 8260D50303
<0.5 pg/L
10/05/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D 5o30B
<0.5 pg/L
10/05/2023
1,1,2-Trichloroethane
SW 846 Method 8260Dr5030B
<0.5 pg/L
10/05/2023
1,1-Dichloroethane
SW 846 Method 8260D150308
<0.5 pg/L
10/05/2023
1,1-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
1,1-Dichloropropene
SW 846 Method 8260D15030B
<0.5 pg/L
10/05/2023
1,2,3-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
1,2,3-Trichloropropane
SW 846 Method 826OD/5030B
<0.5 pg/L
10/05/2023
1,2,4-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
1, 2-Dibromo-3-Chloropropane
SW 848 Method 826OD/50306
<1 pg/L
10/05/2023
1,2-Dibromoethane
SW 846 Method 8260D/50308
<0.5 pg/L
10/05/2023
1,2-Dichlorobenzene
SW 846 Method 8260DIS030B
<0.5 pg/L
10/05/2023
1,2-Dichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
1,2-Dichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
1,3,5-Trimethylbenzene
SW 846 Method 82BOD/5030B
<0.5 pg/L
10/05/2023
1, 3-Dichlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
10/05/2023
1,3-Dichloropropane
SW 848 Method 8260D/50306
<0.5 pg/L
10/05/2023
1,4-Dichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
10/05/2023
2,2-Dichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
10/05/2023
2-Chlorotoluene
SW 846 Method 8260D15030B
<0.5 pg/L
10/05/2023
4-Chlorotoluene
SW 846 Method 82GOD15030B
<0.5 pg/L
10/05/2023
Report M. 2023-22671
Page 1 of 3

F"�' -- 77 Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
® 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
City of Jacksonville
Date of Report: Oct 25, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-22671
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D/50308
<0.5 pg/L
10/05/2023
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Bromodichloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Bromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
Carbon tetrachloride
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
Chlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
10/05/2023
Chloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Chloroform
SW 846 Method 8260D/50308
<0.5 pg/L
10/05/2023
Chloromethane
SW 845 Method 8260D/50308
<0.5 pg/L
10/05/2023
cis- 1,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
10/05/2023
cis-1,3-Dichloropropene
SW 846 Method 828OD15030B
<0.5 pg/L
10/05/2023
Dibromochloromethane
SW 646 Method 8260DIS030B
<0.5 pg/L
10/05/2023
Dibromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
Dichlorodifluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
Ethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
Hexachlorobutadiene
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
Isopropylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
10/05/2023
Methylene chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Naphthalene
SW 846 Method 8280D15030B
<0.5 pg/L
10/05/2023
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
n-Propylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
10/05/2023
ortho-Xylene
SW 846 Method 82BOD15030B
<0.5 pg/L
10/05/2023
p-lsopropyltoluene
SW 846 Method 8280DIS030B
<0.5 pg/L
10/05/2023
sec-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
Styrene
SW 846 Method 8260D15030B
<0.5 pg/L
10/05/2023
tert-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Tetrachloroethene
SW 846 Method 8260D/50308
<0.5 pg/L
10/05/2023
Report #:: 2023-22671
Page 2 of 3

F"W"" -- —1 -,"7
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
info.ia environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Oct 25, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-22671
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Trans- 1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Trans- 1,3-dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
10/05/2023
Trichlorofluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
Vinyl chloride
SW 846 Method 826OD15030B
<0.5 pg/L
10/05/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
< 0.02 mg/L
09/29/2023
Nitrate+Nitrite-Nitrogen
EPA 3532, Rev. 2.0, 1993
0.04 mg/L
10/03/2023
Nitrate Nitrogen
Subtraction Method
0.04 mg/L
10/12/2023
Comment: t 1 _
_ _ r _
Reviewed by:
Report # 2023-22671 Page 3 of 3

Sample Receipt Checklist
6602 Windmill Wa)
Wilmington, NC 2840�
910.392,0223
Client- -,~(r i NzDate: dal J Report Number: J' Z2Lo J
o sample E iiElVl Pickup ❑ — -. — ---
�c ILi iJU PJ/A 1. Were cus
1 YES
❑ fV0 N`/A 2. if custody
Original temperature upon receipt -:R, I `'C
ody seals present on the cooler?
sears were present, were they intact/unbroken?
!;�oti/ temperature
talon:
o Lorrected temperature upon receipt
em
❑ Temperature Elan;
IR Gun ID:
Thomas
Against Bottles
Traceable SIN 210886869
YES
❑
NO
lR Gun Correction Factor `C: 0.0
YES
❑
NO
- If temperature of cooler exceeded 6 C, was Project Mgr./QA notified?
4. Were proper custody
YES
❑
NO
procedures (relinquished/received) followed?
5. Were sample ID's Usted on the COC?
YES
YES
❑
❑
NO
6. Were samples ID's listed on sample containers?
YES
❑
NO
7. Were collection date and time listed on the COC?
YES
O
NO
8. Were tests to be performed listed on the COC?
YES
❑
NO
NO
9. Did samples arrive in proper containers for each test?
YES
❑
10. Did samples arrive in good condition for each test?
YES
❑
NO
11. Was adequate sample volume available?'
YES
❑
NO
NO
12. Were samples received within proper holding time for requested tests?
❑
YES
O
13. Were acid preserved samples received at a pH of <2a
YES
❑
NO
14. Were cyanide samples received at a pH >12?
NO
15. Were sulfide samples received at a pH >9?
OYES
YES
—
❑
[�
NO
NO
16 Were Phi NH3/ TKN
/ r�ol rereived at a chlorire residual of <0.5 m/L?
❑
YES
O
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples am checked for Chlorine at time of analysis a• d recorded o�i the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrect)
Sample(s) Y preserved or with headspace}
were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
:Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify custome- service immediately for incorrectly preserved samples. obtain a new sample or
notify the state lab if directed to ana-yzed by the customer. Who was notified, date and time:
Volatiles Samples)
were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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