NC0003433_J15060657report_20150902

Lab
DUI E Analytical Laboratory APagel1aof49
ENERGY
Order Number:
Project Name:
Customer Name(s):
Customer Address:
Lab Contact:
Report Authorized By:
(Signature)
Program Comments:
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
J15060657
CAPE FEAR - AB GW ASSESSMENT WATER
Tim Hunsucker, Chris Suttell, Kathy Webb, John Toepfer
Mary Ann Cale Mary Ann OgPC'one: 980-875-5274
2015.07.02
13:54:57-04'00' Date:
Mary Ann Ogle
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
7/2/2015
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Collection
Sample ID Plant/Station Date and Time
Collected By
Sample Description
2015020184
Cape Fear
18-Jun-15 10:35 AM
Illegible
MW-5BR
2015020185
Cape Fear
17-Jun-15 4:28 PM
Illegible
CMW-1
2015020186
Cape Fear
18-Jun-15 9:45 AM
Illegible
ERB-38 (GW)
2015020188
Cape Fear
18-Jun-15 9:45 AM
Illegible
Filter Blank
4 Total Samples
Analytical Lab
Page 2 of 49

Analytical Lab
Page 3 of 49
Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals 0 Yes ❑ No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes 0 No
All laboratory QA/QC requirements are acceptable. 0 Yes ❑ No
Report Sections Included:
E%-'] Job Summary Report
❑� Sample Identification
Technical Validation of Data Package
❑� Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
❑d Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
❑� Chain of Custody
❑� Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Mary Ann Ogle Date: 7/2/2015

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060657
Site: MW-5BR
Collection Date: 18-Jun-15 10:35 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.019
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
23
mg/L
1
Sulfate
71
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
1.21
mg/L
0.005
Barium (Ba)
0.036
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
0.136
mg/L
0.005
Zinc (Zn)
0.010
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
45.0
mg/L
0.01
Magnesium (Mg)
0.910
mg/L
0.005
Potassium (K)
2.17
mg/L
0.1
Sodium (Na)
27.7
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
1.21
mg/L
0.005
Barium (Ba)
0.037
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.039
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
0.135
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015020184
Matrix: GW WW
Analytical Lab
Page 4 of 49
DF Method Analysis Date/Time Analyst
Vendor Method V_SHEALY
1
EPA 353.2
06/26/2015 11:08
LSTARLI
10
EPA 300.0
06/23/2015 18:38
BGN9034
10
EPA 300.0
06/23/2015 18:38
BGN9034
1
EPA 245.1
06/19/2015 14:26
ACPAYNE
1
EPA 245.1
06/19/2015 15:07
ACPAYNE
1
EPA 200.7
06/22/2015 11:07
FCJORDA
1
EPA 200.7
06/22/2015 11:07
FCJORDA
1
EPA 200.7
06/22/2015 11:07
FCJORDA
1
EPA 200.7
06/22/2015 11:07
FCJORDA
1
EPA 200.7
06/22/2015 11:07
FCJORDA
1
EPA 200.7
06/22/2015 11:07
FCJORDA
1
EPA 200.7
06/22/2015 11:07
FCJORDA
1
EPA 200.7
06/22/2015 13:26
FCJORDA
1
EPA 200.7
06/22/2015 13:26
FCJORDA
1
EPA 200.7
06/22/2015 13:26
FCJORDA
1
EPA 200.7
06/22/2015 13:26
FCJORDA
1
EPA 200.7
06/26/2015 13:26
FCJORDA
1
EPA 200.7
06/26/2015 13:26
FCJORDA
1
EPA 200.7
06/26/2015 13:26
FCJORDA
1
EPA 200.7
06/26/2015 13:26
FCJORDA
1
EPA 200.7
06/26/2015 13:26
FCJORDA
1
EPA 200.7
06/26/2015 13:26
FCJORDA
1
EPA 200.7
06/26/2015 13:26
FCJORDA

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060657
Site: MW-5BR
Collection Date: 18-Jun-15 10:35 AM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
5.27
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
6.22
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
14.1
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
1.07
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
6.56
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
14.4
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
RADIOLOGICAL - (Analysis Performed by GEL)
Vendor Parameter
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS 220 mg/L 25
Total Carbon
TOC 0.769 mg/L 0.1
Sample #: 2015020184
Matrix: GW WW
Analytical Lab
Page 5 of 49
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/26/2015 19:04
SLS2560
1
EPA 200.8
06/26/2015 19:04
SLS2560
1
EPA 200.8
06/26/2015 19:04
SLS2560
1
EPA 200.8
06/26/2015 19:04
SLS2560
1
EPA 200.8
06/26/2015 19:04
SLS2560
1
EPA 200.8
06/26/2015 19:04
SLS2560
1
EPA 200.8
06/26/2015 19:04
SLS2560
1
EPA 200.8
06/26/2015 19:04
SLS2560
1
EPA 200.8
06/26/2015 19:04
SLS2560
1
EPA 200.8
06/26/2015 19:04
SLS2560
1
EPA 200.8
06/26/2015 19:04
SLS2560
1
EPA 200.8
06/26/2015 19:04
SLS2560
1
EPA 200.8
06/26/2015 19:04
SLS2560
1
EPA 200.8
06/26/2015 21:15
SLS2560
1
EPA 200.8
06/26/2015 21:15
SLS2560
1
EPA 200.8
06/26/2015 21:15
SLS2560
1
EPA 200.8
06/26/2015 21:15
SLS2560
1
EPA 200.8
06/26/2015 21:15
SLS2560
1
EPA 200.8
06/26/2015 21:15
SLS2560
1
EPA 200.8
06/26/2015 21:15
SLS2560
1
EPA 200.8
06/26/2015 21:15
SLS2560
1
EPA 200.8
06/26/2015 21:15
SLS2560
1
EPA 200.8
06/26/2015 21:15
SLS2560
1
EPA 200.8
06/26/2015 21:15
SLS2560
1
EPA 200.8
06/26/2015 21:15
SLS2560
1
EPA 200.8
06/26/2015 21:15
SLS2560
Vendor Method
V_SHEALY
Vendor Method v GEL
Vendor Method V_ELE1
1 SM2540C 06/22/201514:30 AGIBBS5
1 SM5310C/EPA9060A 06/28/2015 09:30 GHUTCHI

Analytical Lab
Certificate of Laboratory Analysis Page 6 of 49
This report shall not be reproduced, except in full.
Order # J15060657
Site: MW-5BR Sample #: 2015020184
Collection Date: 18-Jun-15 10:35 AM Matrix: GW WW
Analyte Result Units Qualifiers RDL DF Method Analysis Date/Time Analyst
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L 5 1 SM2540D 06/22/2015 07:54 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060657
Site: CMW-1
Collection Date: 17-Jun-15 4:28 PM
Analyte Result Units Qualifiers RDL DF
RADIOLOGICAL - (Analysis Performed by GEL)
Vendor Parameter Complete
Sample #: 2015020185
Matrix: GW WW
Analytical Lab
Page 7 of 49
Method Analysis Date/Time Analyst
Vendor Method
v GEL

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060657
Site: ERB-38 (GW)
Collection Date: 18-Jun-15 9:45 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
< 0.1
mg/L
0.1
Sulfate
< 0.1
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
UNDIGESTED METALS BY lCP
Calcium (Ca)
< 0.01
mg/L
0.01
Magnesium (Mg)
< 0.005
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
< 0.05
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
0.264
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015020186
Matrix: GW WW
Analytical Lab
Page 8 of 49
DF Method Analysis Date/Time Analyst
Vendor Method V_SHEALY
1 EPA 353.2
06/26/2015 11:10
LSTARLI
1 EPA 300.0
06/23/2015 21:05
BGN9034
1 EPA 300.0
06/23/2015 21:05
BGN9034
1 EPA 245.1
06/19/2015 14:28
ACPAYNE
1 EPA 200.7
06/22/2015 13:30
FCJORDA
1 EPA 200.7
06/22/2015 13:30
FCJORDA
1 EPA 200.7
06/22/2015 13:30
FCJORDA
1 EPA 200.7
06/22/2015 13:30
FCJORDA
1 EPA 200.7
06/26/2015 13:30
FCJORDA
1 EPA 200.7
06/26/2015 13:30
FCJORDA
1 EPA 200.7
06/26/2015 13:30
FCJORDA
1 EPA 200.7
06/26/2015 13:30
FCJORDA
1 EPA 200.7
06/26/2015 13:30
FCJORDA
1 EPA 200.7
06/26/2015 13:30
FCJORDA
1 EPA 200.7
06/26/2015 13:30
FCJORDA
1 EPA 200.8
06/26/2015 21:36
SLS2560
1 EPA 200.8
06/26/2015 21:36
SLS2560
1 EPA 200.8
06/26/2015 21:36
SLS2560
1 EPA 200.8
06/26/2015 21:36
SLS2560
1 EPA 200.8
06/26/2015 21:36
SLS2560
1 EPA 200.8
06/26/2015 21:36
SLS2560
1 EPA 200.8
06/26/2015 21:36
SLS2560
1 EPA 200.8
06/26/2015 21:36
SLS2560
1 EPA 200.8
06/26/2015 21:36
SLS2560
1 EPA 200.8
06/26/2015 21:36
SLS2560
1 EPA 200.8
06/26/2015 21:36
SLS2560
1 EPA 200.8
06/26/2015 21:36
SLS2560
1 EPA 200.8
06/26/2015 21:36
SLS2560
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4) Complete Vendor Method V_SHEALY

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060657
Site: ERB-38 (GW)
Collection Date: 18-Jun-15 9:45 AM
Analyte Result Units Qualifiers RDL DF
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete
TOTAL DISSOLVED SOLIDS
TDS < 25 mg/L 25 1
Total Carbon
Sample #: 2015020186
Matrix: GW WW
Analytical Lab
Page 9 of 49
Method Analysis Date/Time Analyst
Vendor Method
V_ELE1
SM2540C 06/22/201514:30 AGIBBS5
TOC 0.153 mg/L 0.1 1 SM5310C/EPA9060A 06/28/2015 09:30 GHUTCHI
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L 5 1 SM2540D 06/22/2015 07:54 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060657
Site: Filter Blank
Collection Date: 18-Jun-15 9:45 AM
Analyte
Result
Units
Qualifiers RDL
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.017
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
0.311
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015020188
Matrix: GW WW
Analytical Lab
Page 10 of 49
DF
Method
Analysis Date/Time
Analyst
1
EPA 245.1
06/19/2015 15:09
ACPAYNE
1
EPA 200.7
06/22/2015 11:11
FCJORDA
1
EPA 200.7
06/22/2015 11:11
FCJORDA
1
EPA 200.7
06/22/2015 11:11
FCJORDA
1
EPA 200.7
06/22/2015 11:11
FCJORDA
1
EPA 200.7
06/22/2015 11:11
FCJORDA
1
EPA 200.7
06/22/2015 11:11
FCJORDA
1
EPA 200.7
06/22/2015 11:11
FCJORDA
1
EPA 200.8
06/26/2015 19:26
SLS2560
1
EPA 200.8
06/26/2015 19:26
SLS2560
1
EPA 200.8
06/26/2015 19:26
SLS2560
1
EPA 200.8
06/26/2015 19:26
SLS2560
1
EPA 200.8
06/26/2015 19:26
SLS2560
1
EPA 200.8
06/26/2015 19:26
SLS2560
1
EPA 200.8
06/26/2015 19:26
SLS2560
1
EPA 200.8
06/26/2015 19:26
SLS2560
1
EPA 200.8
06/26/2015 19:26
SLS2560
1
EPA 200.8
06/26/2015 19:26
SLS2560
1
EPA 200.8
06/26/2015 19:26
SLS2560
1
EPA 200.8
06/26/2015 19:26
SLS2560
1
EPA 200.8
06/26/2015 19:26
SLS2560

Analytical Lab
Page 11 of 49
Gernert One Inc.
6319-D Caroiina (beach Rd.
@4Viimington, NC 28412
(Phone: [phone]
[tau: 910 792-6853
[e-mail]
REPORT OF ANALYSES
Duke Energy June 25, 2015
Laboratory Services Client Project Name AB GW Assessment Cape Fear
13339 Hagers Ferry Road Bld. MG03A Client Project Number J15060657
Huntersville, NC 28078 PO Number
Sample Matrix GW WW Sample Type Grab Date Received 06/22/2015
Date Analyzed 06/24/2015 Method SM 4500 S2_ D Time Received 1455
Delivered by FedEx
eOne ID Duke Energy ID Parameter Result Unit Dil
25149-1 MW-5BR
25149-2 ERB-38 (GW)
Sulfide < 0.1 mg/L 1
Received by JRC
DL Date Time
Sampled Sampled
0.1 06/18/15 1035
Sulfide < 0.1 mg/L 1 0.1 06/18/15 0945
Ken Smith, Laboratory Director
25149 Duke Report Packet Compiled by05
NC Certifications: DW 37788 and DWQ DENR 604

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elernentOne SAMPLE SUBMISSION FORM
TAT 5 BD
Hold Time Expiration 6.25.15 @ 0945
Client: Duke Energy
LIMS No J15060657
Project ID Cape Fear
Analytical Lab
Lab r,e 1 Z5149
Analysis Due Date 06.24.15
Report Due Date 06.26.15
Date Rec:
06.22.15
Time Rec:
1455
Rec By
J RC
H >9 Y No Temps 60C es No Ref. Method:
If No, Record If No, Record SM4500 S2 D
b-ample Identification $ Collection Information
Lab ID
Client ID
Collection Date
Collection Time
Analysis Requested
1
MW-5BR _
06.18.15
1035
ulfi
2
ERB-38 (GW)
06.18.15
0945
i
NOTE for Sulfide The MS/MSD spike should approximate 2 to 3 times the sample concentration. If no sulfide detected
at 100 pg/L spike the sample to render the final spike concentration at — 500 Ng/L
Lab Communications
All AB Groundwater Assessment jobs need a RL of 0.1
_ Per Email 5 Day TAT
SS Page 1 of 1 Prep By / Date K G ` )`&1'
SS by�--C% Labeled By / Date Z 3
6/23/2015 0:30:39 AM ID Verification By /Dat W(� • 1

Analytical Lab
Page 14 of 49
METHOD:
SM 4500 S2-_D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
ug/mL
DETECTION LIMIT u
1.000
CLIENT:
Duke
SPK LEVEL_WM
5
Lab ID#
25149 / 151 / 153
Na2S•9H2O Lot #
40721 lCal
1
JSTD
MAX ALIQUOT
10.00
Date:
06/24/15
STANDARD conc(ppm)
X
Time Analysis Begun
13:45
Std Lot: SD-12-1
10
Time Analysis Ended
15:30
QC Std Lot: SD-12-2
10
Analyst:
KAM
ABSORPTION
Y
X
0.9W
0.6m
ug STD
SOLUTION
rAB
°'W
08°0O.5W1.00
0.00
2.50
5.00
7.50
10.00
0.230
0.444
0.624
0.799
04M
0300
02W
o,W
°0°um 2.m A.W 6.00 am mm 12M
X
I
SAMPLE SAMP
I.D. ABS
R
ug PER ALI in mL PREP
ALIQUOT ANALYZED VOL in mL
Sloe <0.079973626;
ALI in mL RESULTS
TAKEN ug/mL
Correlation 0.998400337'
LESS THAN SPIKE
% SPK REC LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.098
0.8009
10
10
10
<
80.09%
1.0
Std, B. 2.50
0.236
2.6255
10
10
10
0.263
105.02%
2.5
Std. B. 5.00
0.447
5.4153
10
10
10
0.542
108.31 %
5.0
Std. B. 7.50
0.637
7.9275
10
10
10
0.793
105.70%
7.5
Std. B. 10.00
0.820
10.3470
10
10
10
1.035
103.47%
10.0
LRB
0.000
0.0000
10
10
10
<
0.0
LRB SPK
0.445
5.3889
10
10
10
0.539
108%
5.0
QC
0.440
5.3228
10
10
10
0.532
106%
5.0
25149-1
0.002
-0.4684
10
10
10�0
1:
25149-1 s k
0.426
5.1377
10
10
10
0.514
103%
5.0
25149-2
0.002
-0.4684
10
10
10
25149-2 dup
0.001
-0.4816
10
10
10
< 0.1
25149-2 s k
0.437
5.2831
10
10
10
0.528
106%
5.0
25151-6
0.016
-0.2833
10
10
10<0.1'
25151-6 s k
0.408
4.8997
10
10
10
0.490
98%
5.0
25151-7
0.002
-0.4684
10
10
10
n o-l�,
25151-7 s k
0.431
5.2038
10
10
10
0.520
104%
5.0
25151-8
0.009
-0.3758
10
10
10
< {
25151-8 s k
0.439
5.3095
10
10
10
0.531
106%
5.0
25151-9
0.002
-0.4684
10
10
10�,
25151-9 spk
0.437
5.2831
10
10
10
0.528
106%
5.0
25153-1
0.003
-0.4552
10
10
10
25153-1 s k
0.428
5.1641
10
10
10
0.516
103%
5.0
25153-2
0.035
-0.0321
10
10
10
<
25153-2 s k
0.292
3.3659
10
10
10
0.337
67%
5.0
25153-3
0.003
-0.4552
10
10
10ti,
25153-3 s k
0.436
5.2699
10
10
10
0.527
105%
5.0
Blank
0.000
0.0000
10
10
10
<
QC
0.440
5.3228
10
10
10
0.532
106%
5
Submitted for QA/QC-
Date: 06/24/15
By: (Print)
KAM
(sign):
/"Oe
Page 1 of 2

Analytical Lab
Page 15 of 49
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
ug/mL
1.000
DETECTION LIMIT u
CLIENT:
Duke
SPK LEVELLuM
5
Lab ID#
25149 / 151 / 153
Na2S•9H20 Lot #
40721
MAX ALIQUOT
10.00
Date:
06/24/15
STANDARD conc(ppm)
X
Time Analysis Begun
13:45
Cal Std Lot: SD-12-1
10
Time Analysis Ended
15:30
QC Std Lot: SD-12-2
10
Analyst:
KAM
STD ABSORPTION
Y
X
Y
0800
ug STD
SOLUTION
STD
ABS
0100
0.00
1.00
2.50
5.00
77.50
.50
10.00
0.000
0.094
0.230
0.444
0.624
0.799
0510
0570
--'°°
°°°°
---350
0.
o mo
o.too
0.0
200 aoo &W am loan uoo
X
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
x
ALI in mL PREP
ANALYZED VOL in mL
Sloe 0.079973626
Correlation 0,998400337
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.098
0.8009
10
10
10
<
80.09%
1.0
Std, B. 2.50
0.236
2.6255
10
10
10
0.263
105.02%
2.5
Std. B. 5.00
0.447
5.4153
10
10
10
0.542
108.31 %
5.0
Std. B. 7.50
0.637
7.9275
10
10
10
0.793
105.70%
7.5
Std. B. 10.00
0.820
10,3470
10
10
10
1.035
103.47%
10.0
LRB
0.000
0.0000
10
10
10
<
0.0
LRB SPK
0.445
5.3889
10
10
10
0.539
108%
5.0
QC
0.440
5.3228
10
10
10
0.532
106%
5.0
25153-2
0.020
-0.2304
10
10
5
25153-2 spk
0.377
4.4898
10
10
5
0.898
90%
5.0
Blank
0.000
0.0000
10
10
10
1 <
QC
0.438
5.2963
10
10
10
0.530
106%
5.0
Submitted for QA/QC-
Date: 06/24/15
By: (Print)
KAM (sign):
00
l�
Page 2 of 2

® Laboratories LLc
nalytical Lab
,_ age 16 of 49
a member of The GEL Group IN'.
June 29, 2015
Mary Ann Ogle
Duke Energy Analytical Laboratory
13339 Hagers Ferry Road
Mail Code: MGO3A2
Huntersville, North Carolina 28078
Re: AB GW Assessment Water
Work Order: 375519
SDG: J15060657
Dear Mary:
P4 Box 30712 Charleston. SC 29417
2040 Sange Road Chad eston.SC29407
P 843 556.8171
F 843.76Gi.1178
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the
sample(s) we received on June 22, 2015. This original data report has been prepared and reviewed in accordance
with GEL's standard operating procedures.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs
on time every time. We trust that you will find everything in order and to your satisfaction. If you have any
questions, please do not hesitate to call me at [phone], ext. 4443.
Sincerely,
Lindsay Fabra
Project Manager
Purchase Order: 1142110
Enclosures
gel.com
Page 1 of 11
problem solved

Analytical Lab
Page 17 of 49
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis Report
for
DUP0002 Duke Energy
Client SDG: J15060657 GEL Work Order: 375519
The Qualifiers in this report are defined as follows:
* A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a Tracer compound
** Analyte is a surrogate compound
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the Certificate of Analysis.
The designation ND, if present, appears in the result column when the analyte concentration is not detected above
the limit as defined in the 'U' qualifier above.
This data report has been prepared and reviewed in accordance with GEL Laboratories LLC
standard operating procedures. Please direct any questions to your Project Manager, Lindsay Fabra.
Reviewed by
JU,&Y ,
Page 2 of 11

Analytical Lab
GEL LABORATORIES LLC Page 18of49
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis
Company:
Duke Energy Analytical Laboratory
Address :
13339 Hagers Ferry Road
Mail Code: MG03A2
Huntersville, North Carolina 28078
Contact:
Mary Ann Ogle
Project:
AB GW Assessment Water
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
2015020184
375519001
Water
18-JUN-15 10:35
22-JUN-15
Client
Report Date: June 29, 2015
Project: DUKE00225
Client ID: DUP0002
Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method
Metals Analysis-ICP-MS
SW846 3010A/6020A Liquid "As Received"
Uranium-238 U 9.30E-06
0.000067
0.0002
ug/mL
1
SKJ 06/25/15
1431 1487792 1
Uranium-233 U 0.00
0.00001
0.00005
ug/mL
1
SKJ 06/25/15
1627 1487792 2
Uranium-234 U 0.00
0.00001
0.00005
ug/mL
1
Uranium-236 U 1.00E-06
0.00001
0.00005
ug/mL
1
Rad Gas Flow Proportional Counting
GFPC, Ra228, Liquid "As Received"
Radium-228 U -1.64
1.79
3.00
pCi/L
AXM6 06/26/15
1124 1487751 3
Rad Radium-226
Lucas Cell, Ra226, liquid "As Received"
Radium-226 U 0.351
0.567
1.00
pCi/L
CXP3 06/29/15
0730 1488322 4
The following Prep Methods were performed:
Method Description
Analyst
Date
Time Prep Batch
SW846 3010A SW 846 3010 Acid Digestion
JXM5
06/23/15
1100
1487791
The following Analytical Methods were performed:
Method Description Analyst Comments
1 SW846 3010A/6020A
2 SW846 3010A/6020A
3 EPA 904,0/SW846 9320 Modified
4 EPA 903.1 Modified
Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits
Barium-133 Tracer GFPC, Ra228, Liquid "As Received" 96.1 (15%-125%)
Notes:
Page 3 of 11

Analytical Lab
GEL LABORATORIES LLC Page 19of49
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis
Company:
Duke Energy Analytical Laboratory
Address :
13339 Hagers Ferry Road
Mail Code: MG03A2
Huntersville, North Carolina 28078
Contact:
Mary Ann Ogle
Project:
AB GW Assessment Water
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
2015020185
375519002
Water
17-JUN-15 16:28
22-JUN-15
Client
Report Date: June 29, 2015
Project: DUKE00225
Client ID: DUP0002
Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method
Metals Analysis-ICP-MS
SW846 3010A/6020A Liquid "As Received"
Uranium-238 U 0.0000661
0.000067
0.0002
ug/mL
1
SKJ 06/25/15
1439 1487792 1
Uranium-233 U 0.00
0.00001
0.00005
ug/mL
1
SKJ 06/25/15
1636 1487792 2
Uranium-234 U 0.00
0.00001
0.00005
ug/mL
1
Uranium-236 U 1.00E-06
0.00001
0.00005
ug/mL
1
Rad Gas Flow Proportional Counting
GFPC, Ra228, Liquid "As Received"
Radium-228 U -0.309
1.35
3.00
pCi/L
AXM6 06/26/15
1124 1487751 3
Rad Radium-226
Lucas Cell, Ra226, liquid "As Received"
Radium-226 0.570
0.511
1.00
pCi/L
CXP3 06/29/15
0730 1488322 4
The following Prep Methods were performed:
Method Description
Analyst
Date
Time Prep Batch
SW846 3010A SW 846 3010 Acid Digestion
JXM5
06/23/15
1100
1487791
The following Analytical Methods were performed:
Method Description Analyst Comments
1 SW846 3010A/6020A
2 SW846 3010A/6020A
3 EPA 904,0/SW846 9320 Modified
4 EPA 903.1 Modified
Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits
Barium-133 Tracer GFPC, Ra228, Liquid "As Received" 93.4 (15%-125%)
Notes:
Page 4 of 11

Analytical Lab
Page 20 of 49
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
QC Summary
Duke Energy Analytical Laboratory
13339 Hagers Ferry Road
Mail Code: MG03A2
Huntersville, North Carolina
Contact: Mary Ann Ogle
Workorder: 375519
Report Date: June 29, 2015
Page 1 of 3
Parmname
NOM
Sample
Qual
QC
Units
RPD%o
REC%
Range Anlst
Date Time
Metals Analysis - ICPMS
Batch 1487792
QC1203342284
375519001
DUP
Uranium-233
U
ND
U
ND
ug/mL
N/A
SKJ
06/25/1516:29
Uranium-234
U
ND
U
ND
ug/mL
N/A
Uranium-236
U
ND
U
ND
ug/mL
N/A
Uranium-238
U
ND
U
ND
ug/mL
N/A
06/25/1514:32
QC1203342283
LCS
Uranium-238
0.0496
0.0555
ug/mL
112
(80%-120%)
06/25/1514:24
QC1203342287
LCS
Uranium-233
0.0005
0.000517
ug/mL
103
(80%-120%)
06/25/1516:21
Uranium-234
0.00055
0.000543
ug/mL
98.7
(80%-120%)
Uranium-236
0.005
0.00575
ug/mL
115
(80%-120%)
QC1203342282
MB
Uranium-233
U
ND
ug/mL
06/25/1516:19
Uranium-234
U
ND
ug/mL
Uranium-236
U
ND
ug/mL
Uranium-238
U
ND
ug/mL
06/25/1514:23
QC1203342285
375519001
MS
Uranium-238
0.0496
U
ND
0.0557
ug/mL
112
(75%-125%)
06/25/1514:34
QC1203342288
375519001
MS
Uranium-233
0.0005
U
ND
0.000529
ug/mL
106
(75%-125%)
06/25/1516:30
Uranium-234
0.00055
U
ND
0.000557
ug/mL
101
(75%-125%)
Uranium-236
0.005
U
ND
0.00589
ug/mL
118
(75%-125%)
QC1203342286
375519001
SD1LT
Uranium-233
U
ND
U
ND
ug/L
N/A
06/25/1516:31
Page 5 of 11

Analytical Lab
Page 21 of 49
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
QC Summary
Workorder: 375519
Page 2 of 3
Parmname
NOM Sample
Qual
QC
Units
RPD% REC%
Range Anlst Date Time
Metals Analysis - ICPMS
Batch 1487792
Uranium-234
U ND
U
ND
ug/L
N/A
Uranium-236
U ND
U
ND
ug/L
N/A
(0%-10%) SKJ 06/25/1516:31
Uranium-238
U ND
U
ND
ug/L
N/A
(0%-10%) 06/25/1514:35
Rad Gas Flow
Batch 1487751
QC1203342157 375519002 DUP
Radium-228 U -0.309 U 0.914 pCi/L N/A N/AAXM6 06/26/1511:24
QC1203342158 LCS
Radium-228 30.7 33.8 pCi/L 110 (75%-125%) 06/26/1511:24
QC1203342156 MB
Radium-228 U -0.42 pCi/L 06/26/1511:24
Rad Ra-226
Batch 1488322
QC1203343639 375516001 DUP
Radium-226 0.651
0.893 pCi/L 31.3
(0% - 100%) CXP3 06/29/15 08:05
QC1203343641 LCS
Radium-226 24.7
25.1 pCi/L
102 (75%-125%) 06/29/15 08:40
QC1203343638 MB
Radium-226 U
0.474 pCi/L
06/29/15 08:05
QC1203343640 375516001 MS
Radium-226 124 0.651
118 pCi/L
95 (75%-125%) 06/29/15 08:05
Notes:
The Qualifiers in this report are defined as follows:
** Analyte is a Tracer compound
< Result is less than value reported
> Result is greater than value reported
BD Results are either below the MDC or tracer recovery is low
E %difference of sample and SD is >10%. Sample concentration must meet flagging criteria
FA Failed analysis.
FB Mercury was found present at quantifiable concentrations in field blanks received with these samples.
Data associated with the blank are deemed
invalid for reporting to regulatory agencies
H Analytical holding time was exceeded
Page 6of11

Analytical Lab
Page 22 of 49
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
QC Summary
Workorder: 375519
Parmname NOM Sample Qual QC Units RPD%o REC'%
Page 3 of 3
Range Anlst Date Time
J Value is estimated
K Analyte present. Reported value may be biased high. Actual value is expected to be lower.
L Analyte present. Reported value may be biased low. Actual value is expected to be higher.
M M if above MDC and less than LLD
M REMP Result > MDC/CL and < RDL
N Metals --The Matrix spike sample recovery is not within specified control limits
N/A RPD or %Recovery limits do not apply.
N1 See case narrative
ND Analyte concentration is not detected above the detection limit
NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
R Sample results are rejected
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma Spectroscopy --Uncertain identification
UJ Gamma Spectroscopy --Uncertain identification
UL Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.
X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Y Other specific qualifiers were required to properly define the results. Consult case narrative.
^ RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
h Preparation or preservation holding time was exceeded
N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable.
^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than
five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the
RL is used to evaluate the DUP result.
* Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the QC Summary.
Page 7 of 11

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Analytical Lab
Page 23 of 49
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Page 8 of 11

Analytical Lab
Page 24 of 49
Laboratories LLc
SAMPLE RECEIPT & REVIEW FORM
Client:
SDG/AWCOC/Work Order:
Received By:
Date Received: /
Suspected Hazard Information
B
o *If Net Counts > 100cpm on samples not marked "radioactive", contact the Radiation Safety Group for further
>
Z investigation.
COC/Samples marked as radioactive?
Maximum Net Counts Observed* (Observed Counts - Area Background Counts):
Classified Radioactive H or III by RSO?
If yes, Were swipes taken of sample containers < action levels?
COC/Samples marked containing PCBs?
Package, COC, and/or Samples marked as
beryllium or asbestos containing?
If yes, samples are to be segregated as Safety Controlled Samples, and opened by the GEL Safety Group.
Shipped as a DOT Hazardous?
IIazatd Class Shipped: UN#:
Samples identified as Foreign Soil?
Sample Receipt Criteria
z z
Comments/Qualifiers (Required for Non -Conforming Items)
Shipping containers received intact
Circle Applicable:
1
and sealed?
Seals broken Damaged container Leaking container Other (describe)
Samples requiring cold preservation
Preservation Method* Ice bags Blue ice Dryice! None Other (describe)
2
within (0 < 6 dog. C)?*
all temperatures are recorded in Celsius
Daily check performed and passed on
Temperature Device Serial 0:
2a
IR temperature gun?
Secondary Temperature Device Serial if (If Applicable): �04 �33 �2
3
Chain of custody documents included
with shipment?
Circle Applicable:
4
Sample containers intact and sealed?
Seals broken Damaged container Leaking container Other (describe)
Samples requiring chemical
Sample ID's, containers affected and observed pH:
5
preservation at proper pH?
If Preservation added Lotth
Do Low Level Perchlorate samples
Sample ID's and containers affected:
6
(EPA 6850) have headspaee as
required?
VOA vials flee of headspace (defined
Sample ID's and containers affected:
?
as < 6mm bubble)?
(If yes, immediately deliver to Volatiles laboratory)
8
Are Encore containers present?
Samples received within holding
ID's and tests affected:
9
time?
10
Sample ID's on COC match ID's on
Sample to's and containers affected:
bottles?
Date & time on COC match date &
Sample ID's affected:
11
time on bottles?
Number of containers received match
Sample ID's affected:
12
number indicated on COC?
Are sample containers identifiable as
13
GEL provided?
14
COC form is properly signed in
relinquished/received sections?
Circle Applicable:
FedEx. Air FedEx Ground UPS Feld Services Courier Other
15
Carrier and tracking number.
Comments (Use Continuation Fonn if needed):
PM (or PMA) review: Initials 110b7 Date U j;7Aj j(,;- Page of / GL-CHL-SR-001 Rev 1
Page 9 of 11 I

Analytical Lab
Page 25 of 49
List of current GEL Certifications as of 29 June 2015
State
Certification
Alaska
UST-110
Arkansas
88-0651
CLIA
42DO904046
California
2940 Interim
Colorado
SC00012
Connecticut
PH-0169
Delaware
SC000122013-10
DoD ELAP/ ISO17025 A2LA
2567.01
Florida NELAP
E87156
Foreign Soils Permit
P330-12-00283, P330-12-00284
Georgia
SC00012
Georgia SDWA
967
Hawaii
SC000122013-10
Idaho Chemistry
SC00012
Idaho Radiochemistry
SC00012
Illinois NELAP
200029
Indiana
C—SC-01
Kansas NELAP
E-10332
Kentucky SDWA
90129
Kentucky Wastewater
90129
Louisiana NELAP
03046 (A133904)
Louisiana SDWA
LA150001
Maryland
270
Massachusetts
M—SCO 12
Michigan
9976
Mississippi
SC000122013-10
Nebraska
NE—OS-26-13
Nevada
SC000122014-1
New Hampshire NELAP
2054
New Jersey NELAP
SCO02
New Mexico
SC00012
New York NELAP
11501
North Carolina
233
North Carolina SDWA
45709
Oklahoma
9904
Pennsylvania NELAP
68-00485
Plant Material Permit
PDEP-12-00260
S.Carolina Radchem
10120002
South Carolina Chemistry
10120001
Tennessee
TN 02934
Texas NELAP
T104704235-15-10
Utah NELAP
SC000122015-17
Vermont
VT87156
Virginia NELAP
460202
Washington
C780
West Virginia
997404
Page 10 of 11

Analytical Lab
There are no "Data Exception Reports" associated with this analytical rePOO.26 of 49
Page 11 of 11

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
Project Name: AB GW Assessment Water - Cape Fear
Project Number:J15060657
Lot Number:QF20017
Date Completed:06/29/2015
Grant Wilton
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
*QF20017*
Shealy Environmental Services, Inc. Page: 1 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Duke Energy
Lot Number: QF20017
Project Name: AB GW Assessment Water - Cape Fear
Project Number: J15060657
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QF20017
Project Name: AB GW Assessment Water - Cape Fear
Project Number: J15060657
Sample Number Sample ID Matrix Date Sampled Date Received
001 2015020184 Aqueous 06/18/20151035 06/20/2015
002 2015020186 Aqueous 06/18/2015 0945 06/20/2015
(2 samples)
Shealy Environmental Services, Inc. Page: 3 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES,
INC.
Executive Summary
Duke Energy
Lot Number: QF20017
Project Name: AB GW Assessment Water - Cape Fear
Project Number: J15060657
Sample Sample ID
Matrix Parameter Method Result Q
Units
Page
001 2015020184
Aqueous Alkalinity SM 2320B-
53
mg/L
5
001 2015020184
Aqueous Bicarbonate Alkalinity SM 2320B-
22
mg/L
5
001 2015020184
Aqueous Carbonate Alkalinity SM 2320B-
25
mg/L
5
(3 detections)
Shealy Environmental Services, Inc. Page: 4 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF20017-001
Description: 2015020184 Matrix: Aqueous
Date Sampled:06/18/2015 1035 Project Name: AB GW Assessment Water -
Date Received:06/20/2015 Project Number: J15060657
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/26/2015 1910
HMA 78167
1
(Bicarbonate ) SM 2320B-2011
1 06/26/2015 1910
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/26/2015 1910
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
53
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
22
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
25
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF20017-001
Description: 2015020184 Matrix: Aqueous
Date Sampled:06/18/2015 1035 Project Name: AB GW Assessment Water -
Date Received:06/20/2015 Project Number: J15060657
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/27/2015 1358 DCS 78294
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF20017-002
Description: 2015020186 Matrix: Aqueous
Date Sampled:06/18/2015 0945 Project Name: AB GW Assessment Water -
Date Received:06/20/2015 Project Number: J15060657
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/26/2015 1947
HMA 78168
1
(Bicarbonate ) SM 2320B-2011
1 06/26/2015 1947
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/26/2015 1947
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF20017-002
Description: 2015020186 Matrix: Aqueous
Date Sampled:06/18/2015 0945 Project Name: AB GW Assessment Water -
Date Received:06/20/2015 Project Number: J15060657
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/27/2015 1409 DCS 78294
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 8 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: QF20017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MB
Sample ID: QQ78167-001 Matrix: Aqueous
Batch:78167
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 06/26/20151621
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF20017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - LCS
Sample ID: QQ78167-002 Matrix: Aqueous
Batch:78167
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 98 1 98 90-110 06/26/20151627
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF20017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MS
Sample ID: QF20017-001 MS Matrix: Aqueous
Batch:78167
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 53 100 73 N 1 20 70-130 06/26/20151916
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF20017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MSD
Sample ID: QF20017-001 MD Matrix: Aqueous
Batch:78167
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Alkalinity 53 100 74 N 1 22 2.0 70-130 20 06/26/20151921
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF20017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MB
Sample ID: QQ78168-001 Matrix: Aqueous
Batch:78168
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 06/26/20151935
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF20017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - LCS
Sample ID: QQ78168-002 Matrix: Aqueous
Batch:78168
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 98 1 98 90-110 06/26/20151941
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF20017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MS
Sample ID: QF20017-002MS Matrix: Aqueous
Batch:78168
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity ND 100 90 1 90 70-130 06/26/20151953
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF20017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MSD
Sample ID: QF20017-002MD Matrix: Aqueous
Batch:78168
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Alkalinity ND 100 94 1 94 4.8 70-130 20 06/26/2015 2000
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF20017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ78294-001 Matrix: Aqueous
Batch:78294
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 06/27/20151228
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF20017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ78294-002 Matrix: Aqueous
Batch:78294
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 120 1 79 70-130 06/27/20151156
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF20017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ78294-003 Matrix: Aqueous
Batch:78294
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 110 1 73 8.5 70-130 30 06/27/20151218
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF20017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
W
g 4 Imo` M
rim
a s
I L
Q
k ! 14ieesuai�h}
' i ■1 ems ullde w
1i I
Shealv
w' P01:42089-- I Y
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OFMCI
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't k
PM
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
151 only Ern itownraual. Scr ikes, try--
Ilwx:umarre NuruU-r. F-AD-016
RevisiemHuniur I
Sample Reczeipt Checklist. ('SRC.)
Client: . Goolor inspected by1datu- � + f5 I,�,Ir #:
Page1ofII
Replaces Date: 11,9NO 4
Eff�Qtive elate: M130lI5
Means ofrece(pt: ❑ SESI ❑ Client ❑ UF'S ❑ FedEx ❑ Airborne E.xp ft Other
Yea
No
1. Were custody weals resetrt trt the caole ?
Yes ❑
I Na
Ej
I IOTA
1 If t:45tod seals were rew-nt, wcro tho7j.inlact and unbtiokerk?
Cooler I) Original temperature upon receipt+Deri'ved (oorrected) temperature upon receipt
Method' f-emperatura Plank ❑ Against Battles IR Gun ID: 111 Gun Correction Fn tar: 0 °C
Method of coolant; [rf Wet Ice ELBIUO Ice L1 U Ice ❑ None
Yr<s ❑
NQ El
NA
3. If temure pentof any lol.er excccded 6.0'1,2, was Pnu cc:t Manager notified?
PM notified by SR.C, phone, note (circle one), other.
(For coolers received via commercial u=ricx, Phis are to be notified
irxil,lrediat>e.l .
Yes ❑
o ❑
NA
d- Is the c�ommerci.el courier's packingslipattached to this farm?
Yes
No F7
i, Wem r+)er custodyprocedures (relin ui3lrerYreaived followed't
Ycs ❑
o ❑
NA
5a Were samples rel iniquished by client to cor=crcial coo icr? Y_
Yes
o 1
6. Were sample Ilys listed on the CDC?
Yes
'o ❑
7. Were saris le IDs listed can all sample containers?
YIZ
No ❑
8. W@s colleWon cute& time listed on the C ?
YesQfNc,
Q 1
9. Wu collection date & time listed un A Nano lu ocutaiines's?
Yesff ffLNQ
❑
10, Did all container label informatioa fD date time a re, v4ith the COC?
yes0
k"ra ❑
I I . Nero tests to be pzrfbrmed listed on the COC?
Yet Ea
No ❑
12. Did all sawn les arrive in the proper containers for eaeh teSv-
Yes
€r
13, f]id all containers arrive in good condition unbroken lids M etc, ?
Y
Nei ❑
14. WA& adegune sam le votutne available?
Yes ❑
No E
IS - Were all samples received within- '42 the holding time or 48 hours, whichever
come,% first?
yet ❑
No
16. W= aay samples confainem inismn ?
Yes Ll
No
No
17. Were there Uly c-e$5 SamR!s not listed Dn COC?
Yes ❑
NA ❑
13. WfTe babbles Eesent >" ea-FiFe}° ('A"or 6mm in diameter) in any VOA i7a15?
Yes ❑
No ❑
NA
19. Were all 1l1etaIS/0 G/FMN {nutrient saniples received at a pH of <2"
Yes ❑
No ❑
W40
M Wen all c aide and/or sulfide sam lcs reccivocl at a pH >12?
Yes ❑
No ❑
NA
21, Were all applicable NH3aKN:cyatside:�phcn.ol (<)0,2mprL) C mplcs tiee of
residual chlori=7
Yes ElNo
❑
NAO
62. M"crtwUectir)n ten r$tufes documcFtcd on thin COC far NC saris les?
❑
Yesetc.-.
No❑
Nr
-2. '4W41re client remarks#rcgsiests (i.e- requested dilutions, MS 'ISD designatiom,
carrectl trartscribli from the t t(' into Ghe irilriCnt sC>ctiO]S in r"Inw15'?
Yes ❑
140
24. VWaN tilt: quote number used talkela from the container label?
Sample 1Prese.r►ition (Must tie conlpletead l'or any samplc{s) incormody preserved or with headspace-)
Saurglc(s) _ wcrc received incor=ily p -e5mrcd and were adjusllc
accordingly in sty le receivlti with (H2S()q.HNOl ,HCLNaOH) using SR 0
Sam le(s, were re( e6ved with bubbles > 6 rum in diameter.
Saul le 5) were recejved withTRC,>41.2 m ±L(if#21 ie-N9
SC Drinking 'Water Pmjcet $amp le(s) pH vcri ficd to be ? 2 by /ate:
Sam le s were not received atH of rI and w= ad'asled arccardingly using SR
- -- e
Sauip�le labels appliud by! Verified by:
commcnts:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

---- Duke Enemy _._.
Aaa"rat lrbors"
Chain of Cwkody I.
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