NC0003433_J15060163 Report_20150902

Lab
DUI E Analytical Laboratory APagel1aof39
ENERGY
Order Number:
Project Name:
Customer Name(s):
Customer Address:
Lab Contact:
Report Authorized By:
(Signature)
Program Comments:
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
J15060163
CAPE FEAR - AB GW ASSESSMENT WATER
Tim Hunsucker, Chris Suttell, Kathy Webb, John Toepfer
Mary Ann Ogle
Mary Ann Ogle
Phone: [phone]
� Mary Ann Ogle
2015.06.23 Date:
14:07_42_-04'00'
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
6/23/2015
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Collection
Sample ID Plant/Station Date and Time
Collected By
Sample Description
2015017400
Cape Fear
03-Jun-15 9:05 AM
JH Gilmer II
ERB-36(GW)
2015017401
Cape Fear
03-Jun-15 10:55 AM
JH Gilmer II
MW-6BR
2015017402
Cape Fear
03-Jun-15 11:30 AM
JH Gilmer II
MW-18S
2015017403
Cape Fear
03-Jun-15 9:05 AM
JH Gilmer II
Filter Blank
4 Total Samples
Analytical Lab
Page 2 of 39

Analytical Lab
Page 3 of 39
Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals 0 Yes ❑ No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes 0 No
All laboratory QA/QC requirements are acceptable. 0 Yes ❑ No
Report Sections Included:
E%-'] Job Summary Report
❑� Sample Identification
Technical Validation of Data Package
❑� Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
❑d Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
❑� Chain of Custody
❑� Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Mary Ann Ogle Date: 6/23/2015

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060163
Site: ERB-36(GW)
Collection Date: 03-Jun-15 9:05 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.011
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
< 0.1
mg/L
0.1
Sulfate
1.1
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
UNDIGESTED METALS BY lCP
Calcium (Ca)
0.063
mg/L
0.01
Magnesium (Mg)
< 0.005
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
< 0.05
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.009
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Analytical Lab
Page 4 of 39
Sample #: 2015017400
Matrix: GW WW
DF Method Analysis Date/Time Analyst
Vendor Method V_SHEALY
1 EPA 353.2
06/08/2015 10:51
LSTARLI
1 EPA 300.0
06/09/2015 01:42
BGN9034
1 EPA 300.0
06/09/2015 01:42
BGN9034
1 EPA 245.1
06/05/2015 13:45
ACPAYNE
1 EPA 200.7
06/10/2015 10:38
MHALL3
1 EPA 200.7
06/10/2015 10:38
MHALL3
1 EPA 200.7
06/10/2015 10:38
MHALL3
1 EPA 200.7
06/10/2015 10:38
MHALL3
1 EPA 200.7
06/08/2015 12:33
MHALL3
1 EPA 200.7
06/08/2015 12:33
MHALL3
1 EPA 200.7
06/08/2015 12:33
MHALL3
1 EPA 200.7
06/08/2015 12:33
MHALL3
1 EPA 200.7
06/08/2015 12:33
MHALL3
1 EPA 200.7
06/08/2015 12:33
MHALL3
1 EPA 200.7
06/08/2015 12:33
MHALL3
1 EPA 200.8
06/08/2015 20:17
SLS2560
1 EPA 200.8
06/08/2015 20:17
SLS2560
1 EPA 200.8
06/08/2015 20:17
SLS2560
1 EPA 200.8
06/08/2015 20:17
SLS2560
1 EPA 200.8
06/08/2015 20:17
SLS2560
1 EPA 200.8
06/08/2015 20:17
SLS2560
1 EPA 200.8
06/08/2015 20:17
SLS2560
1 EPA 200.8
06/08/2015 20:17
SLS2560
1 EPA 200.8
06/08/2015 20:17
SLS2560
1 EPA 200.8
06/08/2015 20:17
SLS2560
1 EPA 200.8
06/08/2015 20:17
SLS2560
1 EPA 200.8
06/08/2015 20:17
SLS2560
1 EPA 200.8
06/08/2015 20:17
SLS2560
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4) Complete Vendor Method V_SHEALY

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060163
Site: ERB-36(GW)
Collection Date: 03-Jun-15 9:05 AM
Analyte Result Units Qualifiers RDL DF
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete
TOTAL DISSOLVED SOLIDS
TDS < 25 mg/L 25 1
Total Carbon
Sample #: 2015017400
Matrix: GW WW
Analytical Lab
Page 5 of 39
Method Analysis Date/Time Analyst
Vendor Method
V_ELE1
SM2540C 06/08/201514:28 AGIBBS5
TOC 0.323 mg/L 0.1 1 SM5310C/EPA9060A 06/09/201513:48 GHUTCHI
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L 5 1 SM2540D 06/08/2015 09:02 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060163
Site: MW-6BR
Collection Date: 03-Jun-15 10:55 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.011
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
250
mg/L
5
Sulfate
39
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.008
mg/L
0.005
Barium (Ba)
0.714
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
0.417
mg/L
0.005
Strontium (Sr)
0.892
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
97.7
mg/L
0.01
Magnesium (Mg)
32.5
mg/L
0.05
Potassium (K)
4.15
mg/L
0.1
Sodium (Na)
94.1
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.082
mg/L
0.005
Barium (Ba)
0.757
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.116
mg/L
0.01
Manganese (Mn)
0.475
mg/L
0.005
Strontium (Sr)
0.907
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015017401
Matrix: GW WW
Analytical Lab
Page 6 of 39
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
06/08/2015 10:52
LSTARLI
50
EPA 300.0
06/09/2015 08:49
BGN9034
10
EPA 300.0
06/09/2015 08:49
BGN9034
1
EPA 245.1
06/05/2015 14:06
ACPAYNE
1
EPA 245.1
06/11/2015 10:34
ACPAYNE
1
EPA 200.7
06/05/2015 10:54
MHALL3
1
EPA 200.7
06/05/2015 10:54
MHALL3
1
EPA 200.7
06/05/2015 10:54
MHALL3
1
EPA 200.7
06/05/2015 10:54
MHALL3
1
EPA 200.7
06/05/2015 10:54
MHALL3
1
EPA 200.7
06/05/2015 10:54
MHALL3
1
EPA 200.7
06/05/2015 10:54
MHALL3
1
EPA 200.7
06/10/2015 09:27
MHALL3
10
EPA 200.7
06/10/2015 09:27
MHALL3
1
EPA 200.7
06/10/2015 09:27
MHALL3
1
EPA 200.7
06/10/2015 09:27
MHALL3
1
EPA 200.7
06/08/2015 12:37
MHALL3
1
EPA 200.7
06/08/2015 12:37
MHALL3
1
EPA 200.7
06/08/2015 12:37
MHALL3
1
EPA 200.7
06/08/2015 12:37
MHALL3
1
EPA 200.7
06/08/2015 12:37
MHALL3
1
EPA 200.7
06/08/2015 12:37
MHALL3
1
EPA 200.7
06/08/2015 12:37
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060163
Site: MW-6BR
Collection Date: 03-Jun-15 10:55 AM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
4.73
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
0.362
ug/L
0.2
Vanadium (V) Low Level
1.88
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
4.57
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
2.19
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
790
mg/L
25
Total Carbon
TOC
0.653
mg/L
0.1
TOTAL SUSPENDED SOLIDS
TSS
< 5
mg/L
5
Sample #: 2015017401
Matrix: GW WW
Analytical Lab
Page 7 of 39
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/21/2015 21:04
SLS2560
1
EPA 200.8
06/21/2015 21:04
SLS2560
1
EPA 200.8
06/21/2015 21:04
SLS2560
1
EPA 200.8
06/21/2015 21:04
SLS2560
1
EPA 200.8
06/21/2015 21:04
SLS2560
1
EPA 200.8
06/21/2015 21:04
SLS2560
1
EPA 200.8
06/21/2015 21:04
SLS2560
1
EPA 200.8
06/21/2015 21:04
SLS2560
1
EPA 200.8
06/21/2015 21:04
SLS2560
1
EPA 200.8
06/21/2015 21:04
SLS2560
1
EPA 200.8
06/21/2015 21:04
SLS2560
1
EPA 200.8
06/21/2015 21:04
SLS2560
1
EPA 200.8
06/21/2015 21:04
SLS2560
1
EPA 200.8
06/08/2015 20:21
SLS2560
1
EPA 200.8
06/08/2015 20:21
SLS2560
1
EPA 200.8
06/08/2015 20:21
SLS2560
1
EPA 200.8
06/08/2015 20:21
SLS2560
1
EPA 200.8
06/08/2015 20:21
SLS2560
1
EPA 200.8
06/08/2015 20:21
SLS2560
1
EPA 200.8
06/08/2015 20:21
SLS2560
1
EPA 200.8
06/08/2015 20:21
SLS2560
1
EPA 200.8
06/08/2015 20:21
SLS2560
1
EPA 200.8
06/08/2015 20:21
SLS2560
1
EPA 200.8
06/08/2015 20:21
SLS2560
1
EPA 200.8
06/08/2015 20:21
SLS2560
1
EPA 200.8
06/08/2015 20:21
SLS2560
Vendor Method
V_SHEALY
Vendor Method V_ELE1
1 SM2540C 06/08/201514:28 AGIBBS5
1 SM5310C/EPA9060A 06/09/201513:48 GHUTCHI
1 SM2540D 06/08/2015 09:02 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060163
Site: MW-18S
Collection Date: 03-Jun-15 11:30 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
29
mg/L
1
Sulfate
180
mg/L
5
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
0.008
mg/L
0.005
Boron (B)
0.173
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
0.118
mg/L
0.005
Strontium (Sr)
0.090
mg/L
0.005
Zinc (Zn)
0.013
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
10.5
mg/L
0.01
Magnesium (Mg)
10.4
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
121
mg/L
0.5
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.325
mg/L
0.005
Barium (Ba)
0.010
mg/L
0.005
Boron (B)
0.180
mg/L
0.05
Iron (Fe)
0.288
mg/L
0.01
Manganese (Mn)
0.137
mg/L
0.005
Strontium (Sr)
0.093
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015017402
Matrix: GW WW
Analytical Lab
Page 8 of 39
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
06/08/2015 10:54
LSTARLI
10
EPA 300.0
06/09/2015 09:25
BGN9034
50
EPA 300.0
06/09/2015 09:25
BGN9034
1
EPA 245.1
06/05/2015 13:59
ACPAYNE
1
EPA 245.1
06/11/2015 10:37
ACPAYNE
1
EPA 200.7
06/05/2015 10:58
MHALL3
1
EPA 200.7
06/05/2015 10:58
MHALL3
1
EPA 200.7
06/05/2015 10:58
MHALL3
1
EPA 200.7
06/05/2015 10:58
MHALL3
1
EPA 200.7
06/05/2015 10:58
MHALL3
1
EPA 200.7
06/05/2015 10:58
MHALL3
1
EPA 200.7
06/05/2015 10:58
MHALL3
1
EPA 200.7
06/10/2015 09:35
MHALL3
1
EPA 200.7
06/10/2015 09:35
MHALL3
1
EPA 200.7
06/10/2015 09:35
MHALL3
10
EPA 200.7
06/10/2015 09:35
MHALL3
1
EPA 200.7
06/08/2015 12:41
MHALL3
1
EPA 200.7
06/08/2015 12:41
MHALL3
1
EPA 200.7
06/08/2015 12:41
MHALL3
1
EPA 200.7
06/08/2015 12:41
MHALL3
1
EPA 200.7
06/08/2015 12:41
MHALL3
1
EPA 200.7
06/08/2015 12:41
MHALL3
1
EPA 200.7
06/08/2015 12:41
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060163
Site: MW-18S
Collection Date: 03-Jun-15 11:30 AM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
8.15
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
0.876
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
1.63
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
450
mg/L
25
Total Carbon
TOC
0.481
mg/L
0.1
TOTAL SUSPENDED SOLIDS
TSS
6.0
mg/L
5
Sample #: 2015017402
Matrix: GW WW
Analytical Lab
Page 9 of 39
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/21/2015 20:43
SLS2560
1
EPA 200.8
06/21/2015 20:43
SLS2560
1
EPA 200.8
06/21/2015 20:43
SLS2560
1
EPA 200.8
06/21/2015 20:43
SLS2560
1
EPA 200.8
06/21/2015 20:43
SLS2560
1
EPA 200.8
06/21/2015 20:43
SLS2560
1
EPA 200.8
06/21/2015 20:43
SLS2560
1
EPA 200.8
06/21/2015 20:43
SLS2560
1
EPA 200.8
06/21/2015 20:43
SLS2560
1
EPA 200.8
06/21/2015 20:43
SLS2560
1
EPA 200.8
06/21/2015 20:43
SLS2560
1
EPA 200.8
06/21/2015 20:43
SLS2560
1
EPA 200.8
06/21/2015 20:43
SLS2560
1
EPA 200.8
06/08/2015 20:26
SLS2560
1
EPA 200.8
06/08/2015 20:26
SLS2560
1
EPA 200.8
06/08/2015 20:26
SLS2560
1
EPA 200.8
06/08/2015 20:26
SLS2560
1
EPA 200.8
06/08/2015 20:26
SLS2560
1
EPA 200.8
06/08/2015 20:26
SLS2560
1
EPA 200.8
06/08/2015 20:26
SLS2560
1
EPA 200.8
06/08/2015 20:26
SLS2560
1
EPA 200.8
06/08/2015 20:26
SLS2560
1
EPA 200.8
06/08/2015 20:26
SLS2560
1
EPA 200.8
06/08/2015 20:26
SLS2560
1
EPA 200.8
06/08/2015 20:26
SLS2560
1
EPA 200.8
06/08/2015 20:26
SLS2560
Vendor Method
V_SHEALY
Vendor Method V_ELE1
1 SM2540C 06/08/201514:28 AGIBBS5
1 SM5310C/EPA9060A 06/09/201513:48 GHUTCHI
1 SM2540D 06/08/2015 09:02 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060163
Site: Filter Blank
Collection Date: 03-Jun-15 9:05 AM
Analyte
Result
Units
Qualifiers RDL
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
0.006
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015017403
Matrix: GW WW
Analytical Lab
Page 10 of 39
DF
Method
Analysis Date/Time
Analyst
1
EPA 245.1
06/11/2015 10:39
ACPAYNE
1
EPA 200.7
06/05/2015 11:02
MHALL3
1
EPA 200.7
06/05/2015 11:02
MHALL3
1
EPA 200.7
06/05/2015 11:02
MHALL3
1
EPA 200.7
06/05/2015 11:02
MHALL3
1
EPA 200.7
06/05/2015 11:02
MHALL3
1
EPA 200.7
06/05/2015 11:02
MHALL3
1
EPA 200.7
06/05/2015 11:02
MHALL3
1
EPA 200.8
06/21/2015 21:11
SLS2560
1
EPA 200.8
06/21/2015 21:11
SLS2560
1
EPA 200.8
06/21/2015 21:11
SLS2560
1
EPA 200.8
06/21/2015 21:11
SLS2560
1
EPA 200.8
06/21/2015 21:11
SLS2560
1
EPA 200.8
06/21/2015 21:11
SLS2560
1
EPA 200.8
06/21/2015 21:11
SLS2560
1
EPA 200.8
06/21/2015 21:11
SLS2560
1
EPA 200.8
06/21/2015 21:11
SLS2560
1
EPA 200.8
06/21/2015 21:11
SLS2560
1
EPA 200.8
06/21/2015 21:11
SLS2560
1
EPA 200.8
06/21/2015 21:11
SLS2560
1
EPA 200.8
06/21/2015 21:11
SLS2560

Analytical Lab
Page 11 of 39
E�ernent One Inc,
6319-D Carolina Beach Rd.
Wilmington, NC 28412
(Phone: [phone]
Fax: [phone]
[e-mail]
REPORT OF ANALYSES
Duke Energy
June 11, 2015
Laboratory Services
Client Project Name AB GW Assessment Cape Fear
13339 Hagers Ferry Road Bld. MG03A
Client Project Number
J15060163
Huntersville, NC 28078
PO Number
Sample Matrix GW WW
Sample Type
Grab
Date Received
06/04/2015
Date Analyzed 06/05/2015
Method
SM 4500 S2- D
Time Received
1620
Delivered by Fed Ex
Received by
LLB
eOne ID Duke Energy ID
Parameter
Result Unit Dil
DL Date
Sampled
Time
Sampled
24974-1 ERB-36 (GW)
Sulfide
< 0.1 mg/L 1
0.1 06/03/15
0905
24974-2 MW-66R
Sulfide
< 0.1 mg/L 1
0.1 06/03/15
1055
24974-3 MW-18S
Sulfide
< 0.1 mg/L 1
0.1 06/03/15
1130
Ken Smith, Laboratory Director
24974 Duke Report Packet Compiled by�
NC Certifications: DW 37788 and DWQ DENR 604

Analytical Lab
Page 12 of 39
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e ementOne SAMPLE SUBMISSION FORM
TAT 7 BD
Hold Time Expiration 06.10.15 @ 0905
Client: Duke Energy
LIMS No J15060163
Project ID Cape Fear
Analytical Lab
Lab I Gage Y4614
Analysis Due Date 06.09.15
Report Due Date 06.15.15
Date Rec:
06.04.15
Time Rec:
1620
Rec By
LLB
H >9 Yes No
<_
Tem 6°C Y No
Ref. Method:
SM4500 S2 D
If No, Record
If No, Record
Sample Identification & Collection Information
Lab ID Client ID _ Collection Date Collection Time Anal sis Requested-
1 ERB-36 (GW) 06.03.15 0905
2 M_W-6BR 06.03.15 105_5
.....w. 3 MW-18S 06.03.1.5 1130
ide
NOTE for Sulfide The MS/MSD spike should approximate 2 to 3 times the sample concentration. If no sulfide detected
at 100 pg/L spike the sample to render the final spike concentration at — 500 pg/L
Lab Communications
......... _ _ .......... ... ....... _........ ... ._.__.
All AB Groundwater Assessment jobs need a RL of 0.1
SS Pagel f Prep By / Date Y\A/-` 6'
SS by Labeled By / Date .,4624 S
6/5/2015 9. 8:27 AM ID Verification By /Date I'G4r1 5 I S

Analytical Lab
Page 14 of 39
METHOD:
SM 4500 S2- D
ELEMENT ASSAY:
Sulfide
CLIENT:
Duke
Lab ID#
24968/ 969/ 970/ 971/ 972/ 973/`
Date:
06/05/15
Time Analysis Begun
12:25
Time Analysis Ended
16:30
ug'iiU
SOLUTION
0.00
1.00
2.50
5.00
7.50
10.00
y
STD
ABS
0.0 00
0.099
0.228
0.425
X
10
10
Y
0.613
a.uo z.00 a.ao a.ro a.ao 10,00 12.00
0.780� x jl
ELEMENT ONE
Spectrophotometer UNITS OF ANSWER
Wavelength 664 DETECTION LIMIT u
SPK LEVEL u
MAX ALIQUOT
Na2S•9H2O Lot # STANDARD conc(ppm)
40721 lCal Sid Lot: WC2-86-1
QC Std Lot: WC2-86-2
STD ABSORPTION
An*.;,
.,
Sloe 0.077758044
Correlation0.898636362.
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
u /mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.100
0.8627
10
10
10
<
86.27%
1.0
Std. B. 2.50
0.232
2.6418
10
10
10
0.264
105.67%
2.5
Std. B. 5.00
0.428
5.2836
10
10
10
0.528
105.97%
5.0
Std. B. 7.50
0.625
7.9388
10
10
10
0.794
105.85%
7.5
Std. B. 10.00
0.779
10.0144
10
10
10
1.001
100.14%
10.0
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.433
5.3509
10
10
10
0.535
107%
5.0
QC
0.438
5.4183
10
10
10
0.542
108%
5.0
24968-1
0.005
-0.4178
10
10
10
24968-1 s k
0.429
5.2970
10
10
10
0.530
106%
5.0
24968-2
0.000
0.0000
10
10
10
24968-2 dup
0.006
-0.4043
10
10
10
< 0.1
24968-2 s k
0.451
5.5936
10
10
10
0.559
112%
5.0
24968-3
-0.002
0.0000
10
10
10
I
24968-3 s k
0.398
4.8792
10
10
10
0.488
98%
5.0
24968-4
0.006
-0.4043
10
10
10
24968-4 s k
0.439
5.4318
10
10
10
0.543
109%
5.0
24968-5
0.003
-0.4447
10
10
10
24968-5 s k
0.429
5.2970
10
10
10
0.530
106%
5.0
24968-6
-0.002
0.0000
10
10
10
01
24968-6 s k
0.404
4.9601
10
10
10
0.496
99%
5.0
24968-7
0.103
0.9031
10
10
10
<
24968-7 s k
0.498
6.2270
10
10
10
0.623
125%
5.0
24968-8
0.006
-0.4043
10
10
10
24968-8 s k
0.401
4.9196
10
10
10
0.492
98%
5.0
24968-9
0.004
-0.4312
10
10
10
24968-9 s k
0.407
5.0005
10
10
10
0.500
100%
5.0
Blank
0.000
0.0000
10
10
10
<
QC
0.436
5.3914
10
10
10
0.539
108%
5.0
Submitted for QA/QC-
Date: 06/05/15
By: (Print)
KAM
(sign):
Page 1 of 7

Analytical Lab
Page 15 of 39
METHOD:
SM 4500 S2= D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
ull
DETECTION LIMIT u
1000
CLIENT:
Duke
SPK LEVEL u
5
Lab ID#
24968/ 969/ 970/ 971/ 1a72/ 973/ 974/ 975 MAX ALIQUOT
06/05/15 Na2S•9H2O Lot # STANDARD conc(ppm)
12:25 1 40721 Cal Std Lot: WC2-86-1
16:30 QC Std Lot: WC2-86-2
KAM STD ABSORPTION
Y
10.00
Date:
X
Time Analysis Begun
10
Time Analysis Ended
10
Analyst:
Y
X
ug STD
STD
SOLUTION
ABS
0.00
0.000
1.00
0.099
2.50
0.228
5.00
750
0.425
0613
4.00 e.00 am 10.00 ».ee
10.00 0.780 x
Sloe 0.077756044
Correlation 0.998636362
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in ni
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
u /mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.100
0.8627
10
10
10
<
86.27%
1.0
Std. B. 2.50
0.232
2.6418
10
10
10
0.264
105.67%
2.5
Std. B. 5.00
0.428
5.2836
10
10
10
0.528
105.67%
5.0
Std. B. 7.50
0.625
7.9388
10
10
10
0.794
105.85%
7.5
Std. B. 10.00
0.779
10.0144
10
10
10
1.001
100.14%
10.0
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.433
5.3509
10
10
10
0.535
107%
5.0
QC
0.438
5.4183
10
10
10
0.542
5.0
24968-10
-0.001
0.0000
10
10
10
24968-10 s k
0.400
4.9062
10
10
10
0.491
98%
5.0
24969-1
0.018
-0.2425
10
10
10;0.
77,7
24969-1 du
0.015
-0.2830
10
10
10
< 0.1
24969-1 s k
0.450
5.5801
10
10
10
0.558
112%
5.0
24969-2
0.032
-0.0538
10
10
10.01
24969-2 s k
0.451
5.5936
10
10
10
0.559
112%
5.0
24969-3
-0.002
0.0000
10
10
1001
24969-3 s k
0.437
5.4049
10
10
10
0.540
108%
5.0
24969-4
0.156
1.6175
10
10
10'.:12
24969-4 s k
0.571
7.2109
10
10
10
0.721
112%
5.0
24969-5
0.860
11.1062
10
10
10
1.111
24969-5 s k
1.147
14.9744
10
10
10
1.497
77%
5.0
24969-6
0.043
0.0944
10
10
10
<
24969-6 s k
0.472
5.8766
10
10
10
0.588
118%
5.0
24969-7
0.002
-0.4582
10
10
10
0-
24969-7 s k
0.418
1 5.1488
10
10
10
0.515
103%
5.0
24969-8
0.068
0.4314
10
10
10
<
24969-8 s k
0.487
6.0788
10
10
10
0.608
122%
5.0
Blank
-0.001
0.0000
10
10
10
<
QC
0.436
5.3914
10
10
10
0.539
1084
5.0
Submitted for QA/QC Date: 06/05/15
By: (Print)
KAM
(sign): `
Page 2 of 7

Analytical Lab
Page 16 of 39
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length'664
UNITS OF ANSWER
ug/mL
DETECTION LIMIT u
1.000
CLIENT:
Duke
SPK LEYELiuM
5
Lab ID#
24968/ 969/ 970/ 971/ 972/ 973/ 974/ 975
06/05/15
1225
16:30
KAM
Na2S•9H2O Lot #
40721
MAX ALIQUOT
10.00
Date:
STANDARD conc(ppm)
X
Time Analysis Begun
Cal Std Lot: WC2-86-1
_
10
Time Analysis Ended
QC Std Lot: WC2-86-2
10
Analyst:
STD ABSORPTION
Y
X
Y
ug STD
SOLUTION
STD
ABS
0.00
1.00
2.50
5.00
7.50
10.00
0.000
am
--
-- -- ---j------
-
0.099
o.
-
-
�
-sue
0.228
0.425
0100
---- ---------
0.613
0.780
- ------ -- -
°00 u.00 z.°o aoo a.°o a°o law u°o
x
�^�
;,
Sloe 0.077756044
Correlation 0.9986363621
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.100
0.8627
10
10
10
<
86.27%
1.0
Std. B. 2.50
0.232
2.6418
10
10
10
0.264
105.67%
2.5
Std. B. 5.00
0.428
5.2836
10
10
10
0.528
105.67%
5.0
Std. B. 7.50
0.625
7.9388
10
10
10
0.794
105.85%
7.5
Std. B. 10.00
0.779
10.0144
10
10
10
1.001
100.14%
10.0
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.433
1 5.3509
10
10
10
0.535
107%
5.0
QC
0.438
5.4183
10
10
10
0.542
5.0
24969-9
0.004
-0.4312
10
10
10
c:0;1
24969-9 s k
0.360
4.3670
10
10
10
0.437
87%
5.0
24969-10
0.004
-0.4312
10
10
10
41
24969-10 s k
0.430
5.3105
10
10
10
0.531
106%
5.0
24969-11
0.000
0.0000
10
10
10
dr1,
24969-11 du
-0.001
0.0000
10
10
10
< 0.1
24969-11 s k
0.431
5.3240
10
10
10
0.532
106%
5.0
24970-1
0.059
0.3101
10
10
10
<
24970-1 s k
0.208
2.3183
10
10
10
0.232
46%
5.0
24970-2
0.022
-0.1886
10
10
10
<
24970-2 s k
0.206
2.2914
10
10
10
0.229
46%
5.0
24970-3
0.566
7.1436
10
10
10
0.714
24970-3 s k
0.847
10.9310
10
10
10
1.093
76%
5.0
24970-4
0.022
-0.1886
10
10
10
24970-4 s k
0.429
5.2970
10
10
10
0.530
106%
5.0
24970-5
0.002
1 -0.4582
10
10
10.t`
24970-5 s k
0.433
5.3509
10
10
10
,
0.535
107%
5.0
24971-1
0.008
-0.3773
10
10
10"41
24971-1 s k
0.397
4.8657
10
10
10
0.487
97%
5.0
Blank
-0.001
0.0000
10
10
10
<
QC
0.436
5.3914
10
10
10
0.539
108% 1
5.0
Submitted for QA/QC Date: 06/05/15
By: (Print)
KAM
gig
(sign): '
Page 3 of 7

Analytical Lab
Page 17 of 39
METHOD:
SM 4500 S2- D
ELEMENT ASSAY:
Sulfide
CLIENT:
Duke
Lab ID#
249681969/ 970/ 971/ 972/ 973f
Date:
06/05/15
Time Analysis Begun
12:25
Time Analysis Ended
16:30
Analyst:
KAM.
X
Y
ug STD
STD
SOLUTION
ABS
0.00
0.000
1.00
0.099
2.50
0.228
5.00
7 50
0.425
0 613
ELEMENT ONE
Wave Length'664 "r- 1 CV 1 1UN Luw i u
SPK LEVEL u
MAX ALIQUOT
Na2S•9H2O Lot # STANDARD conc(ppm)
40721 Cal Std Lot: WC2-86-1
QC Std Lot: WC2-86-2
STD ABSORPTION
• 0.00 200 400 8,00 8.00 10.00 12M
10.00 0.780 x
�0
� ,..:.�. -
d.:.:
.. •.
Sloe 0.077756044
Correlation 0.998636362
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.100
0.8627
10
10
10
<
86.27%
1.0
Std. B. 2.50
0.232
2.6418
10
10
10
0.264
105.67%
2.5
Std. B. 5.00
0.428
5.2836
10
10
10
0.528
105.67%
5.0
Std. B. 7.50
0.625
7.9388
10
10
10
0.794
105.85%
7.5
Std. B. 10.00
0.779
10.0144
10
10
10
1.001
100.14%
10.0
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.433
1 5.3509
10
10
10
0.535
107%
5.0
QC
0.438
5.4183
10
10
10
0.542
5.0
24971-2
0.008
-0.3773
10
10
10
<f 1
24971-2 s k
0.395
4.8388
10
10
10
0.484
97%
5.0
24971-3
0.009
-0.3638
10
10
10
24971-3 s k
0.409
5.0275
10
10
10
0.503
101%
5.0
24972-1
0.014
-0.2965
10
10
10,p,1
24972-1 s k
0.364
4.4209
10
10
10
0.442
88%
5.0
24972-2
0.028
-0.1078
10
10
10�f
24972-2 dup
0.034
-0.0269
10
10
10
< 0.1
24972-2 s k
0.360
4.3670
10
10
10
0.437
87%
5.0
24972-3
0.001
-0.4717
10
10
10
24972-3 s k
0.430
5.3105
10
10
10
0.531
106%
5.0
24973
0.008
-0.3773
10
10
10
<
24973 s k
0.016
-0.2695
10
10
10
<
-5%
5.0
24974-1
0.000
0.0000
10
10
10.
24974-1 s k
0.432
5.3375
10
10
10
0.534
107%
5.0
24974-2
0.004
-0.4312
10
10
10
'�,) 4
24974-2 s k
0.389
4.7579
10
10
10
_->
0.476
95%
5.0
24974-3
O.00D
0.0000
10
10
10
c Q 1
24974-3 s k
0.366
4.4479
10
10
10
0.445
89%
5.0
Blank
0.000
0.0000
10
10
10
<
QC
0.435
5.3779
1 10
10
10
0.538
108%
5.0
Submitted for QA/QC- Date: 06/05/15
By: (Print)
KAM
(sign):
Page 4 of 7

Analytical Lab
Page 18 of 39
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
g
UNITS OF ANSWER
ug/mL
DETECTION LIMIT u
SPK LEVEL u
1.000
5
CLIENT:
Duke
Lab ID#
24968/ 969/ 970/ 971/972/ 973/ 974/ 975 MAX ALIQUOT
06/05/15 Na2S•9H2O Lot # STANDARD conc(ppm)
12:25 40721 Cal Std Lot: WC2-86-1
16:30 QC Std Lot: WC2-86-2
KAM _ STD ABSORPTION
Y o�
10.00
Date:
X
Time Analysis Begun
10
Time Analysis Ended
10
Analyst:
Y
X
ug STD
SOLUTION
STD1
a -
ABS
°`°°
0.00
1.00
2.50
5.00
7.50
10.00
0.000
°.
- - -
-- --
- -
-- m
0.099
04M
-----
----
----
-z�
090D
0.228
°.
:a
-,°�
0.425
°.,w
-- -
--- ----
---
-
---
----
--
0.613°.�
0.780
,�.�
SAMP
ABS
Sloe 0.077756044
Correlation 0.998636362
SAMPLE
I.D.
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.100
0.8627
10
10
10
<
86.27%
1.0
Std. B. 2.50
0.232
2.6418
10
10
10
0.264
105.67%
2.5
Std. B. 5.00
0.428
5.2836
10
10
10
0.528
105.67%
5.0
Std. B. 7.50
0.625
7.9388
10
10
10
0.794
105.85%
7.5
Std. B. 10.00
0.779
10.0144
10
10
10
1.001
100.14%
10.0
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.433
5.3509
10
10
10
0.535
107%
5.0
QC
0.438
1 5.4183
10
10
10
0.542
5.0
24975-1
0.014
-0.2965
10
10
10
0,1
24975-1 s k
0.375
4.5692
10
10
10
0.457
91 %
5.0
24975-2
0.002
-0.4582
10
10
10R
s
1
24975-2 s k
0.422
5.2027
10
10
10
0.520
104%
5.0
24975-3
0.054
1 0.2427
10
10
10
<
24975-3 s k
0.469
5.8362
10
10
10
0.584
117%
5.0
24975-4
0.006
-0.4043
10
10
10
01
24975-4 dup
0.003
-0.4447
10
10
10
< 0.1
24975-4 s k
0.361
4.3805
10
10
10
0.438
88%
5.0
24975-5
0.382
4.6636
10
10
10:466
24975-5 s k
0.767
9.8527
10
10
10
0.985
104%
5.0
24975-6
0.029
-0.0943
10
10
101
24975-6 s k
0.432
5.3375
10
10
10
0.534
107%
5.0
24975-7
0.025
-0.1482
10
10
10
<:01
24975-7 s k
0.438
5.4183
10
10
10
0.542
108%
5.0
24975-8
0.000
0.0000
10
10
10
f1
24975-8 s k
0.425
5.2431
10
10
10
0.524
105%
5.0
24975-9
-0.002
0.0000
10
10
10�
,
24975-9 s k
0.425
5.2431
10
10
10
0.524
105%
5.0
Blank
0.001
0.0000
10
10
10
<
QC
0.434
5.3644
10
10
10
0.536 1
1074
Submitted for QA/QC- Date: 06/05/15
By: (Print)
KAM
OA.0
(sign): C�
Page 5 of 7

Analytical Lab
Page 19 of 39
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
a/mL
DETECTION LIMu
ITSPK
1.000
CLIENT:
Duke
LEVEL u
5
Lab ID#
24968/ 969/ 970/ 971/ 972/ 973/ 974/ 975
06/05/15
12:25
16:30
KAM
Y
MAX ALIQUOT
Na2S•9H2O Lot # STANDARD co_nc(ppm)
40721 Cal Std Lot: WC2-86-1
QC Std Lot: WC2-86-2
STD ABSORPTION
10.00
_ X
10
10
Y
Date:
Time Analysis Begun
Time Analysis Ended
Analyst:
X
ug STD
STD
SOLUTION
ABS
0.00
0.000
1.00
0.099
2.50
0.228
5.00
7 50
0.425
0.613 o.00 2.00 e.m loco ,i W
10.00 0.780 X
Sloe 0.077756044
Correlation 0.998636362
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
u /mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.100
0.8627
10
10
10
<
86.27%
1.0
Std. B. 2.50
0.232
2.6418
10
10
10
0.264
105.67%
2.5
Std. B. 5.00
0.428
5.2836
10
10
10
0.528
105.67%
5.0
Std. B. 7.50
0.625
7.9388
10
10
10
0.794
105.85%
7.5
Std. B. 10.00
0.779
10.0144
10
10
10
1.001
100.14%
10.0
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.433
5.3509
10
10
10
0.535
107%
5.0
QC
0.438
5.4183
10
10
10
0.542
5.0
24968-7
0.058
0.2966
10
10
5
G0.
24968-7 s k
0.455
5.6475
10
10
5
1.129
113%
5.0
24969-5
0.458
5.6879
10
10
5
24969-5 s k
0.809
10.4188
10
10
5
2.084
95%
5.0
24969-6
0.022
-0.1886
10
10
5<.1
u ,
24969-6 s k
0.445
5.5127
10
10
5
1.103
110%
5.0
24969-8
0.031
-0.0673
10
10
5
e 0 x
24969-8 s k
0.445
5.5127
10
10
5
1.103
110%
5.0
24970-1
0.058
0.2966
10
10
5
<
24970-1 s k
0.285
3.3562
10
10
5
0.671
67%
5.0
24970-2
0.024
-0.1617
10
10
5
<
24970-2 s k
0.309
3.6796
10
10
5
0.736
74%
5.0
24970-3
0.631
8.0196
10
10
5
1.604
24970-3 s k
0.865
11.1736
10
10
5
2.235
63%
5.0
24973
0.013
1 -0.3099
10
10
5
<
24973 s k
0.092
0.7548
10
10
5
<
15%
5.0
24975-3
0.030
-0.0808
10
10
5b
F.
24975-3 s k
0.453
5.6205
10
10
5
1.124
112%
5.0
24969-5
0.186
2.0218
10
10
2
1.011
24969-5 s k
0.604
7.6557
10
10
2
3.828
113%
5.0
Blank
0.000
0.0000
10
10
10
<
QC
0.434
5.3644
10
10
10
0.536
107%
5.0
Submitted for QA/QC-
Date: 06/05/1.5
By: (Print)
KAM
(sign):
Page 6 of 7

Analytical Lab
Page 20 of 39
METHOD:
SM 4500 S2- D
ELEMENT ASSAY:
Sulfide
CLIENT:
Duke
Lab ID#
24968/ 969/ 970/ 971/ 972/ 973/`!
Date:
06/05/15
Time Analysis Begun
12:25
Time Analysis Ended
16:30
Analyst:
KAM
X
Y
ug STD
STD
SOLUTION
ABS
0.00
0.000
1.00
0.099
2.50
0.228
5.00
750
0.425
0 613
ELEMENT ONE
Spectrophotometer UNITS OF ANSWER
Wave Length 664 DETECTION LIMIT(ug)
SPK LEVEL u
MAX ALIQUOT
Na2S•9H2O Lot # STANDARD conc(ppm)
40721 1 Cal Std Lot: WC2-86-1
QC Std Lot: WC2-86-2
STD ABSORPTION
X
10
sm
71
• 2.Oo Y.00 &W 800 low Mw
10.00 0.780 x
onion 101-0001Q-
.,
Sloe 0.077756044
Correlation 0.898636382
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.100
0.8627
10
10
10
<
86.27%
1.0
Std. B. 2.50
0.232
2.6418
10
10
10
0.264
105.67%
2.5
Std. B. 5.00
0.428
5.2836
10
10
10
0.528
105.67%
5.0
Std. B. 7.50
0.625
7.9388
10
10
10
0.794
105.85%
7.5
Std. B. 10.00
0.779
10.0144
10
10
10
1.001
100.14%
10.0
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.433
5.3509
10
10
10
0.535
107%
5.0
QC
0.438
5.4183
10
10
10
0.542
5.0
24970-1
0.033
-0.0404
10
10
2
0 '
24970-1 s k
0.373
4.5422
10
10
2
2.271
91 %
5.0
24970-2
0.016
-0.2695
10
10
20,.�.
24970-2 s k
0.370
4.5018
10
10
2
2.251
90%
5.0
24970-3
0.302
3.5853
10
10
2
1.:iJ3 n
24970-3 s k
0.675
8.6127
10
10
2
4.306
101 %
5.0
24973
0.004
-0.4312
10
10
2
<
24973 s k
0.161
1.6849
10
10
2
0.842
34%
5.0
24973
0.003
-0.4447
10
10
1
<
24973 s k
0.244
2.8035
10
10
1
2.804
56%
5.0
24973
0.002
-0.4582
10
10
0.5
<
24973 s k
0.308
3.6662
10
10
0.5
7.332
73%
5.0
24973
0.000
0.0000
10
10
0.25
4 0
24973 s k
0.354
4.2862
10
10
0.25
17.145
86%
5.0
Blank
0.000
1 0.0000
10
10
10
<
QC
0.434
5.3644
10
1 10
1 10
1 0.536
1 107%
1 5.0
Submitted for QA/QC-
Date: 06/05/15
By: (Print)
KAM
0
(sign): /-
/ C-Z
Page 7 of 7

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
Project Name: AB GW Assessment Water - Cape Fear
Project Number:J15060163
Lot Number:QF04079
Date Completed:06/10/2015
Grant Wilton
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
*QF04079*
Shealy Environmental Services, Inc. Page: 1 of 10
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Duke Energy
Lot Number: QF04079
Project Name: AB GW Assessment Water - Cape Fear
Project Number: J15060163
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QF04079
Project Name: AB GW Assessment Water - Cape Fear
Project Number: J15060163
Sample Number Sample ID Matrix Date Sampled Date Received
001 2015017400 Aqueous 06/03/2015 0905 06/04/2015
002 2015017401 Aqueous 06/03/20151055 06/04/2015
003 2015017402
(3 samples)
Aqueous 06/03/20151130 06/04/2015
Shealy Environmental Services, Inc. Page: 3 of 10
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SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QF04079
Project Name: AB GW Assessment Water - Cape Fear
Project Number: J15060163
Sample Sample ID
Matrix Parameter Method Result Q
Units
Page
002
2015017401
Aqueous Alkalinity SM 2320B-
160
mg/L
7
002
2015017401
Aqueous Bicarbonate Alkalinity SM 2320B-
160
mg/L
7
002
2015017401
Aqueous Methane RSK - 175
18
ug/L
8
003
2015017402
Aqueous Alkalinity SM 2320B-
100
mg/L
9
003
2015017402
Aqueous Bicarbonate Alkalinity SM 2320B-
100
mg/L
9
(5 detections)
Shealy Environmental Services, Inc. Page: 4 of 10
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QF04079-001
Description: 2015017400 Matrix: Aqueous
Date Sampled:06/03/2015 0905 Project Name: AB GW Assessment Water -
Date Received:06/04/2015 Project Number: J15060163
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/09/2015 1823
HMA 76878
1
(Bicarbonate ) SM 2320B-2011
1 06/09/2015 1823
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/09/2015 1823
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 10
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Methane
Client: Duke Energy Laboratory ID: QF04079-001
Description: 2015017400 Matrix: Aqueous
Date Sampled:06/03/2015 0905 Project Name: AB GW Assessment Water -
Date Received:06/04/2015 Project Number: J15060163
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/08/2015 1423 DCS 76780
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 10
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QF04079-002
Description: 2015017401 Matrix: Aqueous
Date Sampled:06/03/2015 1055 Project Name: AB GW Assessment Water -
Date Received:06/04/2015 Project Number: J15060163
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/09/2015 1829
HMA 76878
1
(Bicarbonate ) SM 2320B-2011
1 06/09/2015 1829
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/09/2015 1829
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
160
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
160
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 10
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF04079-002
Description: 2015017401 Matrix: Aqueous
Date Sampled:06/03/2015 1055 Project Name: AB GW Assessment Water -
Date Received:06/04/2015 Project Number: J15060163
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/08/2015 1434 DCS 76780
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 18 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 8 of 10
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF04079-003
Description: 2015017402 Matrix: Aqueous
Date Sampled:06/03/2015 1130 Project Name: AB GW Assessment Water -
Date Received:06/04/2015 Project Number: J15060163
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/09/2015 1834
HMA 76878
1
(Bicarbonate ) SM 2320B-2011
1 06/09/2015 1834
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/09/2015 1834
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
100
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
100
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 of 10
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF04079-003
Description: 2015017402 Matrix: Aqueous
Date Sampled:06/03/2015 1130 Project Name: AB GW Assessment Water -
Date Received:06/04/2015 Project Number: J15060163
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/08/2015 1445 DCS 76780
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 10 of 10
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: QF04079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - Ii
Sample ID: QQ76878-001 Matrix: Aqueous
Batch:76878
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 06/09/20151742
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF04079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - LCS
Sample ID: QQ76878-002 Matrix: Aqueous
Batch:76878
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 95 1 95 90-110 06/09/20151748
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF04079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ76780-001 Matrix: Aqueous
Batch:76780
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 06/08/20151346
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF04079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ76780-002 Matrix: Aqueous
Batch:76780
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 50 44 1 87 70-130 06/08/20151319
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF04079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ76780-003 Matrix: Aqueous
Batch:76780
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 50 44 1 88 1.1 70-130 30 06/08/20151331
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF04079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Document N-F-AD-016 ReptaeesDate.1LMIA
RcvivionN4etabfr 1? i�frmliMRntixov3WI5
Sample Rjm6pt Checklist ( RQ
Clitnt: r.p 'CV1-W1' — Ci)okr ItLspccicd byldatc:l r-., I Lot #, C ! 0
Meaty of oceipt, [2r SI~SI [] Clieat ❑ UPS 0 Fe t 0 Airborne Exp ❑ Other
-1
Yes
-.No
ZI
1. Were cusWdy seals pre=t on t% coolers'
Yes
Ll
I JNo
Lj
I NA
1 If cmtody scads wets sal, were they i nteut and unbroken?
Cboler `91nal teMcraturc upon r ipV)Derlved (correeted) temperature Mann rcccipt.
h+le#hod: Temperature Blank ❑ Agaiwt Mottles IR Gun ID; IR Gun m�r+ctiun Factor: �.� IT
h+lethc�d cualan#. Wet Ice ❑Blue Ice Dt Ice ❑ Pone
Yes ❑
(_] IA
Y
3. If tunaperaturc ofany cooler exceeded 6.0°C, was Project Manager autificd?
PM4 rll�tified by SRC, plrorw, uote (oi.role oue), other:
or ocolers re i*red viaa wumnemal courier, PMs are to be notified
=ja -
Yes ❑
Nn
❑ hrA
_
4- Is the commercial courier's packing slip attachDd to this fin?
Yes
No
13,
Were prom custody pTocedmosreign-ni&ed/recei d followed?
Yes ❑
Q
i NA
Sa Wes+e lea relinqislted b cliieat t� eammercial courier`
6. Wcrc sample IDs listed on the C UC;7
Yes
[
Yes
U
7, Were sample 13Ds listed Dti all sample, c&ulitaltlm?
Ycs
No
8. Wag collection date & time listed on the COG?
Yes
o
®
9- Was collection date & time listed on all sample container?
Yes
a
10. Did all container label information (ED, date, tune) a be With Che C0C.'
Yea
140
❑
11. Wcr: c Q sty tt, Ise erforrt,l litite�l on the Cf1C?
12- Did all sa, les arrive in thopuper containers for eadl test?
Yes
a
Yea
Nc
1„1. Did all coWainers arrive in good condition u broken lids can etc.)?
Yes
o
14- Nara adequate sam le voluma available`
Yes
a ❑
11
15 Were all samples received 1w+ithin'/2 the holding tune or 49 hours, Whichever
comes first?
Yes
a
ifs. Wc= any samples comWpers msFi ?
YrJA
140
0,
V. Were there an excess samples not IkLed b17 COO
18. Were bul3Wes prescm ea -site" '%"rar 6mm in di=L10 in an 'tiT(j L vials'
Yes ❑
lio
KA ❑
Yes
o ❑
iU27
19, Were all n taWQ*)CflE++L+nu#rienl samples received at a pH of «?
Yes
a ❑
NA
20. Were all cyanide ainder sulfide samples received at a pH ?12?
Yes ❑
u ❑
NA
21. Were all applicable 1NH3tTKl*1lcyamide.'phtnol (-<0.2mg/L) samples free of
residual chlorine?
Y'cs ❑
MNEI
NA 121
22- Were collection temperai=s documcntcd cm the COC for NC: samples'
Yes ❑
a ❑
NA Er
23- Were cliimt tema 'reyucsts (i.e. requested dilutions, KJSIMSD clrsignatiaus,
etc. -,)correctly transcribed from the COC into the comment eeclkm in UMS?
Yes
a
24. Was the ante uuinber -asod taken from the contamu label's
SaWple
--
ervati6on (bust be completed for any smmplc#sj incorrectly pre:9erved or with kadspam-)
ple(s
atccordsn
were received intorrcctly presem-ed atld Were adjust
in &=plVrcc4:dvinS w4 HzSOa,HNI?i}HCI NaO using SR #
aa I s
' were reoeivtd with bulpbles >6 mm In dlametur,
tample(O
were reDeiveci with TRC -0.2 2#L if *21 is No
Dri
sample(s
g Water Projea Sartiple(s) pH veri6adto be> 2 by Dat :
wem nmt rmeived at a pE of < 2 and %ere a4justcd aocardiz Lain SF #
Sample l
a lied by: Verified by, haute:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

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