NC0003433_J15050769 Report_20150902

Lab
DUI E Analytical Laboratory APagel1aof411
ENERGY
Order Number:
Project Name:
Customer Name(s):
Customer Address:
Lab Contact:
Report Authorized By:
(Signature)
Program Comments:
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
J15050769
CAPE FEAR - AB GW ASSESSMENT WATER
Tim Hunsucker, Chris Suttell, Kathy Webb, John Toepfer
Mary Ann Ogle
Mary Ann Ogle
Phone: [phone]
Mary Ann Ogle
2015.06.17 Date:
12-L4--5L-04'09
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
6/17/2015
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Collection
Sample ID Plant/Station Date and Time
Collected By
Sample Description
2015016457
Cape Fear
27-May-15 11:15 AM
JH Gilmer II
MW-20BR
2015016458
Cape Fear
27-May-15 12:20 PM
JH Gilmer II
ABMW-3S
2015016459
Cape Fear
27-May-15 4:10 PM
JH Gilmer II
MW-10BR
2015016460
Cape Fear
27-May-15 5:20 PM
JH Gilmer II
ERB-29(GW)
2015016461
Cape Fear
27-May-15 5:20 PM
JH Gilmer II
Filter Blank
5 Total Samples
Analytical Lab
Page 2 of 41

Analytical Lab
Page 3 of 41
Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals 0 Yes ❑ No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes 0 No
All laboratory QA/QC requirements are acceptable. 0 Yes ❑ No
Report Sections Included:
E%-'] Job Summary Report
❑� Sample Identification
Technical Validation of Data Package
❑� Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
❑d Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
❑� Chain of Custody
❑� Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Mary Ann Ogle Date: 6/17/2015

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050769
Site: MW-20BR
Collection Date: 27-May-15 11:15 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
12
mg/L
1
Sulfate
12
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.006
mg/L
0.005
Barium (Ba)
0.136
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.063
mg/L
0.01
Manganese (Mn)
0.124
mg/L
0.005
Strontium (Sr)
0.316
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
25.1
mg/L
0.01
Magnesium (Mg)
6.37
mg/L
0.005
Potassium (K)
1.92
mg/L
0.1
Sodium (Na)
40.0
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.621
mg/L
0.005
Barium (Ba)
0.145
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.730
mg/L
0.01
Manganese (Mn)
0.131
mg/L
0.005
Strontium (Sr)
0.317
mg/L
0.005
Zinc (Zn)
0.006
mg/L
0.005
Sample #: 2015016457
Matrix: GW_WW
Analytical Lab
Page 4 of 41
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
06/01/2015 14:25
LSTARLI
10
EPA 300.0
06/02/2015 22:58
BGN9034
10
EPA 300.0
06/02/2015 22:58
BGN9034
1
EPA 245.1
05/29/2015 14:56
ACPAYNE
1
EPA 245.1
06/03/2015 15:10
ACPAYNE
1
EPA 200.7
06/01/2015 12:42
MHALL3
1
EPA 200.7
06/01/2015 12:42
MHALL3
1
EPA 200.7
06/01/2015 12:42
MHALL3
1
EPA 200.7
06/01/2015 12:42
MHALL3
1
EPA 200.7
06/01/2015 12:42
MHALL3
1
EPA 200.7
06/01/2015 12:42
MHALL3
1
EPA 200.7
06/01/2015 12:42
MHALL3
1
EPA 200.7
06/04/2015 13:17
MHH7131
1
EPA 200.7
06/04/2015 13:17
MHH7131
1
EPA 200.7
06/04/2015 13:17
MHH7131
1
EPA 200.7
06/04/2015 13:17
MHH7131
1
EPA 200.7
06/02/2015 13:55
MHALL3
1
EPA 200.7
06/02/2015 13:55
MHALL3
1
EPA 200.7
06/02/2015 13:55
MHALL3
1
EPA 200.7
06/02/2015 13:55
MHALL3
1
EPA 200.7
06/02/2015 13:55
MHALL3
1
EPA 200.7
06/02/2015 13:55
MHALL3
1
EPA 200.7
06/02/2015 13:55
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050769
Site: MW-20BR
Collection Date: 27-May-15 11:15 AM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
1.43
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
2.30
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
0.826
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
1.57
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
2.55
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
1.61
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
210
mg/L
25
Total Carbon
TOC
0.548
mg/L
0.1
TOTAL SUSPENDED SOLIDS
TSS
11
mg/L
5
Sample #: 2015016457
Matrix: GW_WW
Analytical Lab
Page 5 of 41
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/15/2015 19:41
JAHERMA
1
EPA 200.8
06/15/2015 19:41
JAHERMA
1
EPA 200.8
06/15/2015 19:41
JAHERMA
1
EPA 200.8
06/15/2015 19:41
JAHERMA
1
EPA 200.8
06/15/2015 19:41
JAHERMA
1
EPA 200.8
06/15/2015 19:41
JAHERMA
1
EPA 200.8
06/15/2015 19:41
JAHERMA
1
EPA 200.8
06/15/2015 19:41
JAHERMA
1
EPA 200.8
06/15/2015 19:41
JAHERMA
1
EPA 200.8
06/15/2015 19:41
JAHERMA
1
EPA 200.8
06/15/2015 19:41
JAHERMA
1
EPA 200.8
06/15/2015 19:41
JAHERMA
1
EPA 200.8
06/15/2015 19:41
JAHERMA
1
EPA 200.8
06/06/2015 23:37
SLS2560
1
EPA 200.8
06/06/2015 23:37
SLS2560
1
EPA 200.8
06/06/2015 23:37
SLS2560
1
EPA 200.8
06/06/2015 23:37
SLS2560
1
EPA 200.8
06/06/2015 23:37
SLS2560
1
EPA 200.8
06/06/2015 23:37
SLS2560
1
EPA 200.8
06/06/2015 23:37
SLS2560
1
EPA 200.8
06/06/2015 23:37
SLS2560
1
EPA 200.8
06/06/2015 23:37
SLS2560
1
EPA 200.8
06/06/2015 23:37
SLS2560
1
EPA 200.8
06/06/2015 23:37
SLS2560
1
EPA 200.8
06/06/2015 23:37
SLS2560
1
EPA 200.8
06/06/2015 23:37
SLS2560
Vendor Method
V_SHEALY
Vendor Method V_ELE1
1 SM2540C 06/01/201514:39 AGIBBS5
1 SM5310C/EPA9060A 06/04/201516:19 GHUTCHI
1 SM2540D 06/02/2015 08:15 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050769
Site: ABMW-3S
Collection Date: 27-May-15 12:20 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.016
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
18
mg/L
1
Sulfate
58
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.549
mg/L
0.005
Barium (Ba)
0.643
mg/L
0.005
Boron (B)
0.206
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
2.12
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
236
mg/L
0.1
Magnesium (Mg)
0.072
mg/L
0.05
Potassium (K)
43.5
mg/L
1
Sodium (Na)
67.8
mg/L
0.5
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.537
mg/L
0.005
Barium (Ba)
0.638
mg/L
0.005
Boron (B)
0.205
mg/L
0.05
Iron (Fe)
0.021
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
2.05
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015016458
Matrix: GW_WW
Analytical Lab
Page 6 of 41
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
06/01/2015 14:28
LSTARLI
10
EPA 300.0
06/02/2015 20:17
BGN9034
10
EPA 300.0
06/02/2015 20:17
BGN9034
1
EPA 245.1
05/29/2015 14:59
ACPAYNE
1
EPA 245.1
06/03/2015 15:20
ACPAYNE
1
EPA 200.7
06/01/2015 13:01
MHALL3
1
EPA 200.7
06/01/2015 13:01
MHALL3
1
EPA 200.7
06/01/2015 13:01
MHALL3
1
EPA 200.7
06/01/2015 13:01
MHALL3
1
EPA 200.7
06/01/2015 13:01
MHALL3
1
EPA 200.7
06/01/2015 13:01
MHALL3
1
EPA 200.7
06/01/2015 13:01
MHALL3
10
EPA 200.7
06/04/2015 13:21
MHH7131
10
EPA 200.7
06/04/2015 13:21
MHH7131
10
EPA 200.7
06/04/2015 13:21
MHH7131
10
EPA 200.7
06/04/2015 13:21
MHH7131
1
EPA 200.7
06/02/2015 13:59
MHALL3
1
EPA 200.7
06/02/2015 13:59
MHALL3
1
EPA 200.7
06/02/2015 13:59
MHALL3
1
EPA 200.7
06/02/2015 13:59
MHALL3
1
EPA 200.7
06/02/2015 13:59
MHALL3
1
EPA 200.7
06/02/2015 13:59
MHALL3
1
EPA 200.7
06/02/2015 13:59
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050769
Site: ABMW-3S
Collection Date: 27-May-15 12:20 PM
Analyte
Result
Units Qualifiers
RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
7.96
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
7.79
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
51.0
ug/L
1
Nickel (Ni)
4.51
ug/L
1
Selenium (Se)
1.39
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
2.34
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
1.09
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
8.68
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
8.86
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
56.0
ug/L
1
Nickel (Ni)
5.72
ug/L
1
Selenium (Se)
1.73
ug/L
1
Thallium (TI) Low Level
0.220
ug/L
0.2
Vanadium (V) Low Level
2.53
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
780
mg/L
25
Total Carbon
TOC
6.2
mg/L
0.1
TOTAL SUSPENDED SOLIDS
TSS
8.0
mg/L
5
Sample #: 2015016458
Matrix: GW_WW
Analytical Lab
Page 7 of 41
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/15/2015 19:48
JAHERMA
1
EPA 200.8
06/15/2015 19:48
JAHERMA
1
EPA 200.8
06/15/2015 19:48
JAHERMA
1
EPA 200.8
06/15/2015 19:48
JAHERMA
1
EPA 200.8
06/15/2015 19:48
JAHERMA
1
EPA 200.8
06/15/2015 19:48
JAHERMA
1
EPA 200.8
06/15/2015 19:48
JAHERMA
1
EPA 200.8
06/15/2015 19:48
JAHERMA
1
EPA 200.8
06/15/2015 19:48
JAHERMA
1
EPA 200.8
06/15/2015 19:48
JAHERMA
1
EPA 200.8
06/15/2015 19:48
JAHERMA
1
EPA 200.8
06/15/2015 19:48
JAHERMA
1
EPA 200.8
06/15/2015 19:48
JAHERMA
1
EPA 200.8
06/06/2015 23:41
SLS2560
1
EPA 200.8
06/06/2015 23:41
SLS2560
1
EPA 200.8
06/06/2015 23:41
SLS2560
1
EPA 200.8
06/06/2015 23:41
SLS2560
1
EPA 200.8
06/06/2015 23:41
SLS2560
1
EPA 200.8
06/06/2015 23:41
SLS2560
1
EPA 200.8
06/06/2015 23:41
SLS2560
1
EPA 200.8
06/06/2015 23:41
SLS2560
1
EPA 200.8
06/06/2015 23:41
SLS2560
1
EPA 200.8
06/06/2015 23:41
SLS2560
1
EPA 200.8
06/06/2015 23:41
SLS2560
1
EPA 200.8
06/06/2015 23:41
SLS2560
1
EPA 200.8
06/06/2015 23:41
SLS2560
Vendor Method
V_SHEALY
Vendor Method V_ELE1
1 SM2540C 06/01/201514:39 AGIBBS5
1 SM5310C/EPA9060A 06/04/201516:19 GHUTCHI
1 SM2540D 06/02/2015 08:15 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050769
Site: MW-10BR
Collection Date: 27-May-15 4:10 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.013
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
14
mg/L
1
Sulfate
210
mg/L
5
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.023
mg/L
0.005
Barium (Ba)
0.073
mg/L
0.005
Boron (B)
0.127
mg/L
0.05
Iron (Fe)
0.020
mg/L
0.01
Manganese (Mn)
0.375
mg/L
0.005
Strontium (Sr)
0.949
mg/L
0.005
Zinc (Zn)
0.015
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
81.4
mg/L
0.01
Magnesium (Mg)
13.0
mg/L
0.005
Potassium (K)
2.46
mg/L
0.1
Sodium (Na)
50.5
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.213
mg/L
0.005
Barium (Ba)
0.064
mg/L
0.005
Boron (B)
0.110
mg/L
0.05
Iron (Fe)
0.137
mg/L
0.01
Manganese (Mn)
0.336
mg/L
0.005
Strontium (Sr)
0.941
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015016459
Matrix: GW_WW
Analytical Lab
Page 8 of 41
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
06/01/2015 14:29
LSTARLI
10
EPA 300.0
06/03/2015 08:57
BGN9034
50
EPA 300.0
06/03/2015 08:57
BGN9034
1
EPA 245.1
05/29/2015 15:01
ACPAYNE
1
EPA 245.1
06/03/2015 15:22
ACPAYNE
1
EPA 200.7
06/01/2015 13:28
MHALL3
1
EPA 200.7
06/01/2015 13:28
MHALL3
1
EPA 200.7
06/01/2015 13:28
MHALL3
1
EPA 200.7
06/01/2015 13:28
MHALL3
1
EPA 200.7
06/01/2015 13:28
MHALL3
1
EPA 200.7
06/01/2015 13:28
MHALL3
1
EPA 200.7
06/01/2015 13:28
MHALL3
1
EPA 200.7
06/04/2015 13:34
MHH7131
1
EPA 200.7
06/04/2015 13:34
MHH7131
1
EPA 200.7
06/04/2015 13:34
MHH7131
1
EPA 200.7
06/04/2015 13:34
MHH7131
1
EPA 200.7
06/02/2015 12:32
MHALL3
1
EPA 200.7
06/02/2015 12:32
MHALL3
1
EPA 200.7
06/02/2015 12:32
MHALL3
1
EPA 200.7
06/02/2015 12:32
MHALL3
1
EPA 200.7
06/02/2015 12:32
MHALL3
1
EPA 200.7
06/02/2015 12:32
MHALL3
1
EPA 200.7
06/02/2015 12:32
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050769
Site: MW-10BR
Collection Date: 27-May-15 4:10 PM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
2.42
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
6.04
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
2.91
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
2.49
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
6.57
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
3.34
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
490
mg/L
25
Total Carbon
TOC
0.976
mg/L
0.1
TOTAL SUSPENDED SOLIDS
TSS
9.0
mg/L
5
Sample #: 2015016459
Matrix: GW_WW
Analytical Lab
Page 9 of 41
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/15/2015 19:55
JAHERMA
1
EPA 200.8
06/15/2015 19:55
JAHERMA
1
EPA 200.8
06/15/2015 19:55
JAHERMA
1
EPA 200.8
06/15/2015 19:55
JAHERMA
1
EPA 200.8
06/15/2015 19:55
JAHERMA
1
EPA 200.8
06/15/2015 19:55
JAHERMA
1
EPA 200.8
06/15/2015 19:55
JAHERMA
1
EPA 200.8
06/15/2015 19:55
JAHERMA
1
EPA 200.8
06/15/2015 19:55
JAHERMA
1
EPA 200.8
06/15/2015 19:55
JAHERMA
1
EPA 200.8
06/15/2015 19:55
JAHERMA
1
EPA 200.8
06/15/2015 19:55
JAHERMA
1
EPA 200.8
06/15/2015 19:55
JAHERMA
1
EPA 200.8
06/06/2015 23:59
SLS2560
1
EPA 200.8
06/06/2015 23:59
SLS2560
1
EPA 200.8
06/06/2015 23:59
SLS2560
1
EPA 200.8
06/06/2015 23:59
SLS2560
1
EPA 200.8
06/06/2015 23:59
SLS2560
1
EPA 200.8
06/06/2015 23:59
SLS2560
1
EPA 200.8
06/06/2015 23:59
SLS2560
1
EPA 200.8
06/06/2015 23:59
SLS2560
1
EPA 200.8
06/06/2015 23:59
SLS2560
1
EPA 200.8
06/06/2015 23:59
SLS2560
1
EPA 200.8
06/06/2015 23:59
SLS2560
1
EPA 200.8
06/06/2015 23:59
SLS2560
1
EPA 200.8
06/06/2015 23:59
SLS2560
Vendor Method
V_SHEALY
Vendor Method V_ELE1
1 SM2540C 06/01/201514:39 AGIBBS5
1 SM5310C/EPA9060A 06/04/201516:19 GHUTCHI
1 SM2540D 06/02/2015 08:15 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050769
Site: ERB-29(GW)
Collection Date: 27-May-15 5:20 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
< 0.1
mg/L
0.1
Sulfate
< 0.1
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
UNDIGESTED METALS BY lCP
Calcium (Ca)
0.011
mg/L
0.01
Magnesium (Mg)
< 0.005
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
< 0.05
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Analytical Lab
Page 10 of 41
Sample #: 2015016460
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method V_SHEALY
1 EPA 353.2
06/01/2015 14:35
LSTARLI
1 EPA 300.0
06/02/2015 23:52
BGN9034
1 EPA 300.0
06/02/2015 23:52
BGN9034
1 EPA 245.1
05/29/2015 15:04
ACPAYNE
1 EPA 200.7
06/04/2015 13:29
MHH7131
1 EPA 200.7
06/04/2015 13:29
MHH7131
1 EPA 200.7
06/04/2015 13:29
MHH7131
1 EPA 200.7
06/04/2015 13:29
MHH7131
1 EPA 200.7
06/02/2015 12:36
MHALL3
1 EPA 200.7
06/02/2015 12:36
MHALL3
1 EPA 200.7
06/02/2015 12:36
MHALL3
1 EPA 200.7
06/02/2015 12:36
MHALL3
1 EPA 200.7
06/02/2015 12:36
MHALL3
1 EPA 200.7
06/02/2015 12:36
MHALL3
1 EPA 200.7
06/02/2015 12:36
MHALL3
1 EPA 200.8
06/07/2015 00:04
SLS2560
1 EPA 200.8
06/07/2015 00:04
SLS2560
1 EPA 200.8
06/07/2015 00:04
SLS2560
1 EPA 200.8
06/07/2015 00:04
SLS2560
1 EPA 200.8
06/07/2015 00:04
SLS2560
1 EPA 200.8
06/07/2015 00:04
SLS2560
1 EPA 200.8
06/07/2015 00:04
SLS2560
1 EPA 200.8
06/07/2015 00:04
SLS2560
1 EPA 200.8
06/07/2015 00:04
SLS2560
1 EPA 200.8
06/07/2015 00:04
SLS2560
1 EPA 200.8
06/07/2015 00:04
SLS2560
1 EPA 200.8
06/07/2015 00:04
SLS2560
1 EPA 200.8
06/07/2015 00:04
SLS2560
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4) Complete Vendor Method V_SHEALY

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050769
Site: ERB-29(GW)
Collection Date: 27-May-15 5:20 PM
Analyte Result Units Qualifiers RDL DF
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete
TOTAL DISSOLVED SOLIDS
TDS < 25 mg/L 25 1
Total Carbon
Sample #: 2015016460
Matrix: GW_WW
Analytical Lab
Page 11 of 41
Method Analysis Date/Time Analyst
Vendor Method
V_ELE1
SM2540C 06/01/201514:39 AGIBBS5
TOC 0.327 mg/L 0.1 1 SM5310C/EPA9060A 06/04/201516:19 GHUTCHI
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L 5 1 SM2540D 06/02/2015 08:15 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050769
Site: Filter Blank
Collection Date: 27-May-15 5:20 PM
Analyte
Result
Units
Qualifiers RDL
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
0.055
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015016461
Matrix: GW_WW
Analytical Lab
Page 12 of 41
DF
Method
Analysis Date/Time
Analyst
1
EPA 245.1
06/03/2015 15:24
ACPAYNE
1
EPA 200.7
06/01/2015 13:32
MHALL3
1
EPA 200.7
06/01/2015 13:32
MHALL3
1
EPA 200.7
06/01/2015 13:32
MHALL3
1
EPA 200.7
06/01/2015 13:32
MHALL3
1
EPA 200.7
06/01/2015 13:32
MHALL3
1
EPA 200.7
06/01/2015 13:32
MHALL3
1
EPA 200.7
06/01/2015 13:32
MHALL3
1
EPA 200.8
06/15/2015 20:51
JAHERMA
1
EPA 200.8
06/15/2015 20:51
JAHERMA
1
EPA 200.8
06/15/2015 20:51
JAHERMA
1
EPA 200.8
06/15/2015 20:51
JAHERMA
1
EPA 200.8
06/15/2015 20:51
JAHERMA
1
EPA 200.8
06/15/2015 20:51
JAHERMA
1
EPA 200.8
06/15/2015 20:51
JAHERMA
1
EPA 200.8
06/15/2015 20:51
JAHERMA
1
EPA 200.8
06/15/2015 20:51
JAHERMA
1
EPA 200.8
06/15/2015 20:51
JAHERMA
1
EPA 200.8
06/15/2015 20:51
JAHERMA
1
EPA 200.8
06/15/2015 20:51
JAHERMA
1
EPA 200.8
06/15/2015 20:51
JAHERMA

Analytical Lab
Page 13 of 41
mom
REPORT OF ANALYSES
(EDernent One Inc.
6319-D Carolina Beach Rd.
Wilmington, IBC 28412
Rhone: 910 793-0128
Fax: [phone]
[e-mail]
Duke Energy
June 9, 2015
Laboratory Services
Client Project Name AB GW
Assessment water Cape Fear
13339 Hagers
Ferry Road Bld. MG03A
Client Project Number J15050769
Huntersville, NC 28078
PO Number
Sample Matrix
GW WW
Sample Type Grab
Date Received
05/29/2015
Date Analyzed
06/01/2015
Method
SM 4500 S2- D
Time Received
1645
Delivered by
FedEx
Received by
LLB
eOne ID
Duke Energy ID
Parameter
Result Unit Dil
DL Date
Sampled
Time
Sampled
24897-1
MW-20 BR
Sulfide
< 0.1 mg/L 1
0.1 05/27/15
1115
24897-2
ABMW-3S
Sulfide
< 0.1 mg/L 1
0.1 05/27/15
1220
24897-3
MW-10 BR
Sulfide
< 0.1 mg/L 1
0.1 05/27/15
1610
24897-4
ERB-29 (GW)
Sulfide
< 0.1 mg/L 1
0.1 05/27/15
1720
Ken Sm h, Laboratory Director
24897 Duke Report Packet Compiled byl---�
NC Certifications: DW 37788 and DWQ DENR 604

Analytical Lab
Page 14 of 41
ui
boo
0
4a GJDkJl47uO:) 0 11401 95 o o o o o 0
POAIOGSI(]
(Moleq
16 Mew
1-1
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t IuqwGl3--A)-
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01
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............. .... ...... .....
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----- -----
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Analytical Lab
elementOne SAMPLE SUBMISSION FORM Lab 1bge IrU97
TAT 7 BD
Hold Time Expiration 06.03.15 @ 1115
Client: Duke Energy
LIMS No J15050769
Project ID Cape Fear
Analysis Due Date 06.02.15
Report Due Date 06.09.15
Date Rec:
05.29.15
Time Rec:
0445
Rec By
LLB
H >9 zle
No Tem <_ 6°C a No Ref. Method:
If No, Record I If No, Record SM4500 S2 D
Sample Identification & Collection Information
Lab ID
I Client ID
Collection Date
Collection Time
Analysis Requested
1
MW-20 BR
05/27/15
1115
Sulfid
2
ABMW-3S
05/27/15
1220
ulfi e
3
MW-10 BR
05/27/15
1610
i
4
ERB-29 (GW)
05/27/15
1920
Suff rat -
NOTE for Sulfide
The MS/MSD spike should approximate 2 to 3 times the sample concentration. If no sulfide detected
at 100 pg/L spike the sample to render the final spike concentration at - 500 pg/L
Lab Communications
All AB Groundwater Assessment jobs need a RL of 0.1
SS Pagel of Prep By / Date
SS by Labeled By / Date C-
6/9/2015 2:01:36 PM ID Verification By /Date - /

Analytical Lab
Page 16 of 41
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
u /ml-
1.000
5
DETECTION LIMIT �u
CLIENT:
Duke
SPK LEVELLuca
Lab ID#
24894 / 895 / 896 / 8971898 / 899 MAX ALIQUOT
6/1/15 Na2S•9H2O Lot # STANDARD conc(ppm)
10:00 40721 Cal Std Lot: WC2-85-1
12:50 QC Std Lot: WC2-85-2
KAM STD ABSORPTION
10.00
X
10
10
Y
Date:
Time Analysis Begun
Time Analysis Ended
Analyst:
ug STD
SOLUTION
STD 0. a
°
ABS oxOD
0600
- -- ,
-- - ---
- ----
--- -
- -
e
---------
0.00
1.00
2.50
5,00
7.50
10.00
0.000
0.
0.098
0 °°°
.442
� s oo
0.233
02°0
-
--- 233
0.442
om
0.654
0.835
0.000.00 2W 4.00 e.ao eoo 10.00 1200
x
Sloe 0.083650549
orrelation 0,999259508
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.100
0.9268
10
10
10
<
92.68%
1.0
Std. B. 2.50
0.230
2.5255
10
10
10
0.253
101.02%
2.5
Std. B. 5.00
0.435
5.0466
10
10
10
0.505
100,93%
5.0
Std. B. 7.50
0.623
7.3586
10
10
10
0.736
98.11 %
7.5
Std. B. 10.00
0.817
9.7444
10
10
10
0.974
97.44%
10.0
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.460
5.3541
10
10
10
0.535
107%
5.0
QC
0.454
5.2803
10
10
10
0.528
106%
5.0
24894-1
0.011
1 -0.1677
10
10
10
24894-1 s k
0.411
1 4.7515
10
10
10
0.475
95%
5.0
24894-2
0.000
0.0000
10
10
10
U 1
24894-2 dup
0.004
-0.2538
10
10
10
< 0.1
24894-2 s k
0.452
5.2557
10
10
10
0.526
105%
5.0
24894-3
0.012
-0.1554
10
10
10
0.1
24894-3 s k
0.409
4.7269
10
10
10
0.473
95%
5.0
24894-4
0.003
1 -0.2661
10
10
10
" 5 ,01' ;
24894-4 s k
0.453
5.2680
10
10
10
0.527
105%
5.0
24894-5
0.002
-0.2784
10
10
10
c 01
24894-5 s k
0.449
5.2188
10
10
10
0.522
104%
5.0
24895-1
0.003
-0.2661
10
10
10
24895-1 s k
0.422
4.8867
10
10
10
0.489
98%
5.0
24895-2
0.114
1.0990
10
10
10
24895-2 s k
0.493
5.7599
10
10
10
0.576
93%
5.0
24895-3
0.002
-0.2784
10
10
10"
24895-3 s k
0.400
4.6162
10
10
10
0.462
92%
5.0
24895-4
0.080
0.6809
10
10
10
<
24895-4 s k
0.497
5.8091
10
10
10
0.581
116%
5.0
Blank
0.000
1 0.0000
10
10
10
<
QC
0.456
5.3049
10
10
10
0.530
106% _
5.0
Submitted for QA/QC-
Date: 06/01/15
By: (Print)
KAM
(sign): "
Page 1 of 5 /�

Analytical Lab
Page 17 of 41
METHOD:
SM 4500 S2- D
ELEMENT ASSAY:
Sulfide
CLIENT:
Duke
Lab ID#
24894 / 895 1896 / 897 / 898
Date:
6/1115
Time Analysis Begun
10:00
Time Analysis Ended
12:50
X
Y
ug STD
STD
SOLUTION
ABS
0.00
0.000
1.00
0.098
2.50
0.233
5.00
0.442
7.50
0.654
10.00
0.835
1
X
10
10
ELEMENT ONE
Wave Length 664 - - 1 .,
SPK LEVEL
MAX ALIQU
Na2S•9H2O Lot # STANDARD
40721 Cal Sid Lot:
QC Std Lot:
STD ABSOF
k,..W M....sa `. `• -k
�'+.
Sloe 0.083650549
correlation 0.989259508
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
u /mL
LESS THAN
%o SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.100
0.9268
10
10
10
<
92.68%
1.0
Std. B. 2.50
0.230
2.5255
10
10
10
0.253
101.02%
2.5
Std. B. 5.00
0.435
5.0466
10
10
10
0.505
100.93%
5.0
Std. B. 7.50
0.623
7.3586
10
10
10
0.736
98.11 %
7.5
Sid. B. 10.00
0.817
9.7444
10
10
10
0.974
97.44%
10.0
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.460
5.3541
10
10
10
0.535
107%
5.0
QC
0.454
5.2803
10
10
10
0.528
106%
5.0
24895-5
0.003
-0.2661
10
10
10
24895-5 s k
0.435
5.0466
10
10
10
0,505
101 %
5.0
24895-6
0.005
-0.2415
10
10
100.,1'
24895-6 clup
0.002
-0.2784
10
10
10
< 0.1
24895-6 s k
0.431
4.9974
10
10
10
0.500
100%
5.0
24895-7
0.000
0.0000
10
10
10
<
24895-7 s k
0.347
3.9644
10
10
10
0.396
79%
5.0
24895-8
0.000
0.0000
10
10
10
24895-8 s k
0.446
5.1819
10
10
10
0.518
104%
5.0
24896-1
0.006
-0.2292
10
10
10
E11.
24896-1 s k
0.413
4.7761
10
10
10
0.478
96%
5.0
24896-2
0.000
0.0000
10
10
10
< 0 t
24896-2 s k,
0.435
5.0466
10
10
10
0.505
101 %
5.0
24896-3
0.019
-0.0693
10
10
10s
24896-3 s k
0.417
4.8252
10
10
10
0.483
97%
5.0
24896-4 •
0.003
-0.2661
10
10
10
< 0 1,
24896-4 s k
0.448
5.2065
10
10
10
0.521
104%
5.0
24896-5
0.004
-0.2538
10
10
10
- < 0.,1.
24896-5 s k
0.421
1 4.8744
10
10
10
0.487
97%
5.0
Blank
0.000
0.0000
10
10
10
<
QC
0.456
5.3049
1 10
10
10
0.530
106%
5.0
Submitted for QA/QC- Date: 06/01/15
By: (Print)
KAM
(sj
Page 2 of 5

Analytical Lab
Page 18 of 41
METHOD:
SM 4500 S2- D
ELEMENT ASSAY:
Sulfide
CLIENT:
Duke
Lab ID#
24894 / 895 / 896 / 897 / 898
Date:
6/1 /15
Time Analysis Begun
10:00
Time Analysis Ended
12:50
X
Y
ug STD
STD
SOLUTION
ABS
0.00
0.000
1.00
0.098
2.50
0.233
5.00
0,442
7.50
0.654
10.00
0.835
ELEMENT ONE
Wave Length 664 "" "" "" `
SPK LEVEL u
MAX ALIQUOT
Na2S•9H2O Lot # STANDARD conc(ppjm)
40721 Cal Std Lot: W 2-85-1
QC Std Lot: W 2-85-2
STD ABSORPTION
5
10.00
X
10
10
Y
-ate
--t50
-�150 I
10 ICI
Sloe 0.083650549
orrelation 0.999259508
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
L
°o
SS THAN
SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0,0000
10
10
10
<1
0.0
Std. B. 1.00
0.100
0.9268
10
10
10
<
92.68%
1.0
Std. B. 2.50
0.230
2.5255
10
10
10
0.253
1101.02%
2.5
Std. B. 5.00
0.435
5.0466
10
10
10
0.505
1100.93%
5.0
Std. B. 7.50
0.623
7.3586
10
10
10
0.736
1 98.11 %
7.5
Std. B. 10.00
0.817
9.7444
10
10
10
0.974
97.44%
10.0
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.460
5.3541
10
10
10
0.535
107%
5.0
QC
0.454
5.2803
10
10
10
0.528
106%
5.0
24896-6
0.014
-0.1308
10
10
10
<
24896-6 s k
0.297
3.3495
10
10
10
0.335
67%
5.0
24897-1
0.030
0.0660
10
10
10
24897-1 spk
0.388
4.4686
10
10
10
0.447
89%
5.0
24897-2
0.007
-0.2169
10
10
10
<:0.1
24897-2 dup
0.001
-0.2907
10
10
10
< 0.1
24897-2 s k
0.385
4.4317
10
10
10
0.443
1 89%
5.0
24897-3
0.017
-0.0939
10
10
10
< 01
24897-3 s k
0.417
4.8252
10
10
10
0.483
1 97%
5.0
24897-4
0.005
-0.2415
10
10
10
24897-4 s k
0.452
5.2557
10
10
10
0.526
1 105%
5.0
24898-1
0.005
-0.2415
10
10
10
<Q 1
24898-1 s k
0.403
4.6531
10
10
10
0.465
93%
5.0
24898-2
0.006
-0.2292
10
10
10
a 0,1
24898-2 s k
0.431
1 4.9974
10
10
10
0.500
100%
5.0
24898-3
0.002
-0.2784
10
10
10
�.. . < 4,1" ,
24898-3 s k
0.428
4.9605
10
10
10
0.496
99%
5.0
24898-4
0.006
-0.2292
10
10
10
c'p'1�7-1
1
24898-4 s k
0.396
4.5670
10
10
10
0.457
91 %
5.0
Blank
0.000
0.0000
10
10
10
<
QC
0.456
5.3049
10
10
10
0.530
°
Submitted for QA/QC- Date: 06/01/15
By: (Print)
KAM
(s;
Page 3 of 5

Analytical Lab
Page 19 of 41
METHOD: SM 4500 S2- D ELEMENT ONE
ELEMENT ASSAY: Sulfide Spectrophotometer UNITS OF ANSWER ug/mL
Wave Length 664 DETECTION LIMIT 1,000
CLIENT: Duke SPK LEVEL u 5
Lab ID# 24894 / 895 / 896 / 897 ! 898'/ 899 MAX ALIQUOT 10.00
Date: 6/1/15 Na2S•9H2O Lot # STANDARD conc(pp ) X
Time Analysis Begun 10:00 40721 1 Cal Std Lot: W 2-85-1 10
Time Analysis Ended 12:50 1 QC Std Lot: W 2-85-2 10
Analyst: KAM ISTD ABSORPTION Y
X Y
ug STD STD4 o.'0."" o.M
SOLUTION ABS
0.00 0.000
a �z�
-,�
2.50 0.233 ozao
5.00 0.442 +�
7.50 0.654 00 200 400 6.00 e00 10.00 12.00
10.00 0.835 ! X
Sloe 0.083650549
orrelation 0.999259608
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.100
0.9268
10
10
10
<
92.68%
1.0
Std. B. 2.50
0.230
2.5255
10
10
10
0.253
101.02%
2.5
Std. B. 5.00
0.435
5.0466
10
10
10
0.505
100.93%
5.0
Std. B. 7.50
0.623
7.3586
10
10
10
0.736
98.11 %
7.5
Std. B. 10.00
0.817
9.7444
10
10
10
0.974
97.44%
10.0
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.460
5.3541
10
10
10
0.535
107%
5.0
QC
0.454
5.2803
10
10
10
0,528
106%
5.0
24898-5
0.011
-0.1677
10
10
10
<
24898-5 s k
0.290
3.2634
10
10
10
0.326
65%
5.0
24898-6
0.268
2.9929
10
10
10
0;29
24898-6 s k
0.702
8.3301
10
10
10
0.833
107%
5.0
24898-7
0.003
-0.2661
10
10
10
24898-7 s k
0.413
4.7761
10
10
10
0.478
96%
5.0
24898-8
0.201
1 2.1689
10
10
10
0; 17 .
24898-8 dup
0.187
1.9967
10
10
10
0.200
24898-8 s k
0.572
6.7314
10
10
10
0.673
95%
5.0
24898-9
0.000
0.0000
10
10
10
0:`1
24898-9 s k
0.447
5.1942
10
10
10
0.519
104%
5.0
24899-1
0.013
-0.1431
10
10
10
<
24899-1 s k
0.307
3.4725
10
10
10
0.347
69%
5.0
24899-2
0.005
-0.2415
10
10
10
< m.I
24899-2 s k
0.417
4.8252
10
10
10
0.483
97%
5.0
24899-3
0.013
-0.1431
10
10
10
�`<0,'
24899-3 s k
0.437
5.0712
10
10
10
0.507
101 %
1 5.0
24899-4
0.001
-0.2907
10
10
10^.p.1
24899-4 s k
0.447
5.1942
10
10
10
0.519i
104%
5.0
Blank
0.000
0.0000
10
10
10
<
QC
0.454
5.2803
10
10
10
0,528
106%
5
Submitted for QA/QC-
Date: 06/01/15
By: (Print)
KAM
(s
gn): ..
Page 4 of 5

Analytical Lab
Page 20 of 41
SM 4500 S2- D
:
Sulfide
&Analysis
Duke
24894 / 895 / 896 / 897 1898
611 f15
un
10:00
ugsiu
ELUTION
0.00
1.00
2.50
5.00
7.50
10.00
Y
STD
ABS
Q000
0.098
0.233
0.442
ELEMENT ONE
pectrophotometer UNITS OF ANSWER
DETECTION LIMIT u
Wave Length 664 SPK LEVEL u
MAX ALIQUOT
Na2S•9H2O Lot # STANDARD conc(pp
40721 Cal Std Lot: W
0.654 ow _ z.w
0.835 X
too
SAMPLE SAMP ug PER ALI in MILPREP
I.D. ABS ALIQUOT ANALYZED VOL in mL
Sloe 0.083650549
ALI in mL RESULTS
TAKEN u /mL
Correlation 0.99925950$
,LESS THAN SPIKE
% SPK REC LEVEL
Sid. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
Std. B. 2.50
0.100
0.230
0.9268
2.5255
10
10
10
10
10
10
<
0.253
92.68%
101.02%
1.0
2.5
Std. B. 5.00
0.435
5.0466
10
10
10
0.505
100.93%
5.0
Std. B. 7.50
0.623
7.3586
10
10
10
0.736
98.11 %
7.5
Std, B. 10.00
0.817
9.7444
10
10
10
0.974
97.44%
10.0
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.460
5.3541
10
10
10
0.535
107%
5.0
QC
0.454
5.2803
10
10
10
0.528
106%
5.0
24895-4
0.045
0.2504
10
10
5
<;q 2.
24895-4 s k
0.475 1
5.5385
10
10
5
1.108
111 %
5.0
24895-7
0.000
0.0000
10
10
5;0.2
24895-7 s k
0.458
5.3295
10
10
5
1.066
107%
5.0
24896-6
0.014
-0.1308
10
10
5
< 0.2.
24896-6 s k
0.392
4.5178
10
10
5
0.904
90%
5.0
24898-5
0.005
-0.2415
10
10
5
<'0•.
24898-5 s k
0.375
4.3087
10
10
5
0.862
86%
5.0
24899-1
-0.001
0.0000
10
10
5
<
24899-1 s k
0.366
4.1981
10
10
5
0.840
84%
5.0
24899-1
0.001
1 -0.2907
10
10
2
,c, 0 5
24899-1 s k
0.414
4.7884
10
1 10
2
2.394 96%
5.0
Blank
0.000
0.0000
10
10
10
<
QC
0.455
5.2926
10
10
10
0.529 1
106%
0
Submitted for QA/QC-
Date: 06/01/15
By: (Print)
KAM
(sign):
Page 5 of -5

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
Project Name: AB GW Assessment Water
Project Number:J15050769
Lot Number:QE29067
Date Completed:06/05/2015
Grant Wilton
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
* QE29067*
Shealy Environmental Services, Inc. Page: 1 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Duke Energy
Lot Number: QE29067
Project Name: AB GW Assessment Water
Project Number: J15050769
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QE29067
Project Name: AB GW Assessment Water
Project Number: J15050769
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
2015016457
Aqueous
05/27/20151115
05/29/2015
002
2015016458
Aqueous
05/27/20151220
05/29/2015
003
2015016459
Aqueous
05/27/20151610
05/29/2015
004
2015016460
Aqueous
05/27/20151720
05/29/2015
(4 samples)
Shealy Environmental Services, Inc. Page: 3 of 12
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SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QE29067
Project Name: AB GW Assessment Water
Project Number: J15050769
Sample Sample ID Matrix Parameter Method Result Q Units Page
001
2015016457
Aqueous
Alkalinity
SM 2320B-
140
mg/L
5
001
2015016457
Aqueous
Bicarbonate Alkalinity
SM 2320B-
140
mg/L
5
002
2015016458
Aqueous
Alkalinity
SM 2320B-
600
mg/L
7
002
2015016458
Aqueous
Carbonate Alkalinity
SM 2320B-
280
mg/L
7
002
2015016458
Aqueous
Methane
RSK - 175
160
ug/L
8
003
2015016459
Aqueous
Alkalinity
SM 2320B-
120
mg/L
9
003
2015016459
Aqueous
Bicarbonate Alkalinity
SM 2320B-
120
mg/L
9
003
2015016459
Aqueous
Methane
RSK - 175
13
ug/L
10
(8 detections)
Shealy Environmental Services, Inc. Page: 4 of 12
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QE29067-001
Description: 2015016457 Matrix: Aqueous
Date Sampled:05/27/2015 1115 Project Name: AB GW Assessment Water
Date Received:05/29/2015 Project Number: J15050769
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/02/2015 1632
HMA 76308
1
(Bicarbonate ) SM 2320B-2011
1 06/02/2015 1632
HMA 06/02/2015 1632
1
(Carbonate Al) SM 2320B-2011
1 06/02/2015 1632
HMA 06/02/2015 1632
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
140
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
140
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 12
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Methane
Client: Duke Energy Laboratory ID: QE29067-001
Description: 2015016457 Matrix: Aqueous
Date Sampled:05/27/2015 1115 Project Name: AB GW Assessment Water
Date Received:05/29/2015 Project Number: J15050769
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/03/2015 1601 JJG 76496
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 12
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QE29067-002
Description: 2015016458 Matrix: Aqueous
Date Sampled:05/27/2015 1220 Project Name: AB GW Assessment Water
Date Received:05/29/2015 Project Number: J15050769
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/02/2015 1644
HMA 76308
1
(Bicarbonate ) SM 2320B-2011
1 06/02/2015 1644
HMA 06/02/2015 1644
1
(Carbonate Al) SM 2320B-2011
1 06/02/2015 1644
HMA 06/02/2015 1644
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
600
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
280
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE29067-002
Description: 2015016458 Matrix: Aqueous
Date Sampled:05/27/2015 1220 Project Name: AB GW Assessment Water
Date Received:05/29/2015 Project Number: J15050769
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/03/2015 1625 JJG 76496
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 160 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 8 of 12
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QE29067-003
Description: 2015016459 Matrix: Aqueous
Date Sampled:05/27/2015 1610 Project Name: AB GW Assessment Water
Date Received:05/29/2015 Project Number: J15050769
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/02/2015 1649
HMA 76308
1
(Bicarbonate ) SM 2320B-2011
1 06/02/2015 1649
HMA 06/02/2015 1649
1
(Carbonate Al) SM 2320B-2011
1 06/02/2015 1649
HMA 06/02/2015 1649
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
120
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
120
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE29067-003
Description: 2015016459 Matrix: Aqueous
Date Sampled:05/27/2015 1610 Project Name: AB GW Assessment Water
Date Received:05/29/2015 Project Number: J15050769
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/03/2015 1645 JJG 76496
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 13 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 10 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE29067-004
Description: 2015016460 Matrix: Aqueous
Date Sampled:05/27/2015 1720 Project Name: AB GW Assessment Water
Date Received:05/29/2015 Project Number: J15050769
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/02/2015 1654
HMA 76308
1
(Bicarbonate ) SM 2320B-2011
1 06/02/2015 1654
HMA 06/02/2015 1654
1
(Carbonate Al) SM 2320B-2011
1 06/02/2015 1654
HMA 06/02/2015 1654
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 11 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE29067-004
Description: 2015016460 Matrix: Aqueous
Date Sampled:05/27/2015 1720 Project Name: AB GW Assessment Water
Date Received:05/29/2015 Project Number: J15050769
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/03/2015 1730 JJG 76496
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 12 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29067
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - Ii
Sample ID: QQ76308-001 Matrix: Aqueous
Batch: 76308
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 06/02/20151515
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29067
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - LCS
Sample ID: QQ76308-002 Matrix: Aqueous
Batch: 76308
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 94 1 94 90-110 06/02/20151521
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29067
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ76496-001 Matrix: Aqueous
Batch: 76496
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 06/03/20151449
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29067
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ76496-002 Matrix: Aqueous
Batch: 76496
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 160 1 106 70-130 06/03/20151328
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29067
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ76496-003 Matrix: Aqueous
Batch: 76496
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 150 1 101 4.8 70-130 30 06/03/20151340
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29067
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

sksiy SnvlmnmGnEal Servtces. Inc.
ISacumenr Numbces F-AD-016
Pevmign Nunitmr: 17
Sample Reoeipl Chcrklist (SRC)
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Yes C I NoUNA 1 If custody seals were ese nt were tlic in lHc--I rrkd unbroken?
Gaoler ID/Original temperature upon !=ipvDerived (oorrected) temperature upon rcecipt:
Ik{!e#hnd= ❑Temperaturejilanl{ _ .' gainst Rattles IR Gun ED.- � II1 Cun C.R.orrection Factor,
Mcthud of cauwo7ant: [�Wat Ice BUtie lie ❑ DFY Ice '_bane
- y 3. If temOratune- cdany wokr cxccvded 6.O'DC, was P'rojcct Manager T10tificd?
P nflea by SRC., phone, note (circle c ne), other:
',y4 El`� El` (For calla s received via c=vmiciai courier, PA; a-Te to he, msliiied
Yes LJ I No Lj I NA V 1 4, Is tht mmnercial courier's packi:n Aip attached to [his form?
Yew No Q 1 1 S. Were rAcnavr u&ltjdv grrarrrlurr_q frplinnnigzIr.Prllrrrrivrrll frlllr-mrnA?

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ELEMENTS by WI 10115 (TIR µ}: AS. 84, Cd. Co, Gr, Cu. UU. NI, Pb. an. 94.11 O-U a I'LLi
ELEMENTS by ICP (TEM1= Al, f1a, R. Fs. -Mn, Sr. Zn 4P_Undigoolod Ca, Mg. K. Ha fig by 20.1
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