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HomeMy WebLinkAboutNC0003433_Whole Rock _ XRay Diff 2_20150902SP0112328 FINAL REPORT Multi Element Package COPIES TO Samantha Wilkinson SynTerra CLIENT REFERENCE No: No. SAMPLES MAIN SAMPLE TYPE ABMW-2 AB 0-2 through ABMW-5: AS 0-2 5 CORE Is AMERICAN ASSAY LABORATORIES 1500 GLENDALE AVE. SPARKS, NV USA 89431-5902 Ph.(775) 356-0606 Fax.(775) 356-1413 EMAIL: info@aallabs.com RECEIVED 14-Jul-2015 REPORTED 5-Aug-2015 COMPANY DISCLAIMER :- When small samples are submitted, AAL may process the sample at smaller then specified weights to retain some pulp for quality control reassay. When Values exceed upper limits, AAL will run an Over Range analysis, to establish an accurate value. Additional cost will apply. Due to USDA Soil Quarantine programs - all foreign and some domestic soil material must be decontaminated by drying @ 125c for 48 hours, which will result in loss of Mercury (Hg). NEVADA LEGISLATIVE DISCLAIMER :- The results of this assay were based solely upon the content of the sample submitted. Any decision to invest should be made only after the potential investment value of the claim or deposit has been determined based on the results of assays of multiple samples of geological materials collected by the prospective investor or by a qualified person selected by him and based on an evaluation of all engineering data which is available concerning any proposed project. Nevada State Law NRS 519.130. ANALYSIS A1203 BaO CaO Cr203 Fe203 K20 MgO MnO Na20 P205 Si02 SrO Ti02 V205 As Cd Ce Cc Cu Ga La Me Ni Pb Sb Se METHOD XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR UNIT pet pet pet pet pet pet pet pet pet pet pet pet pet pet ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm LOWER LIMIT 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 1 0.2 1 1 1 2 1 1 1 2 1 1 ANALYSIS Sn W Zn Zr LOI H2O- C S >63 um -63 um.y <2um Quartzlullite�matitelnetite:alciteiiotite METHOD D4A-WR D4A-WR D4A-WR D4A-WR LOI H2O-ILTRA-CILTRA-C ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD UNIT ppm ppm ppm ppm pet pet pet pet pet pet pet pet pet pet pet pet pet LOWER LIMIT 1 1 1 1 0.01 0.01 0.005 0.005 0.01 0.01 0.01 0.1 0.1 0.1 0.1 0.1 0.1 Digitally signed by AMERICAN ASSAY Joshua Zimmerman �Ih4fdipf6CS Date: 2015.08.05 17:31:45-07'00' SIGNATORY ANALYSIS Cover Page AAL-006 SP0112328 AMERICAN ASSAY LABORATORIES FINAL REPORT Is 1500 GLENDALE AVE. SPARKS, NV USA 89431-5902 Ph.(775) 356-0606 Fax.(775) 356-1413 EMAIL: AALLABS@NVBELL.NET Abbreviatior Definition Preparation DIP Sample Destroyed in Preparation DIS Sample Destroyed in Shipment ISS Insufficient Sample Submitte( SDI Sample Diesel Impregnate( SHI Sample Hydraulic Impregnate( SNR Sample Not Receivec Analysis STD - ?? International Reference Material Standar STD - AAL## AAL generated standard material BLANK AAL Laboratory Silica Blan] DTF Data to Folloc, DL Detection Limit of Metho( < or - Lens Than Lower Detection Limit of Metho > Greater than Upper Limit of Metho, N/A Not Analyzec NR Not Reportec (R) column Laboratory repeat weigh, digestion, analysis from original pulp or reject respl D or -D after Sample II Client submitted duplicate rig split sampl -R after Sample II Repeat analysis from original pulp reweigh, digestion and analys: -X after Sample If Repeat analysis from reject resplit, preparation, weigh, digestion and analys ppb Parts per Billion 0.001 ppm = 1 pp ppm Parts per Million 1 ppm = 1 mg/K OPT Troy Ounces per Short Ton(2,000 lbs)(1 ppm= 0.02917 OPT Oz Troy Ounce = 31.103 gram: o Percent 1%=10,000 pp: g Grams lg=0.001 kilogra mg Milligrams lmg=0.001gram Kg Kilograms 1Kg=1000gram ins Pounds llb=0.454kilogra Method FA-PB## Fire Assay Lead Collection - ## sample weight in gran GRAV Gravimetric (Weighed) finis] SF Screen Fire Assay reporting a plus, 2 minus fractions and a head Ca: + ### Plus Fraction (Retained on top of Mesh) ###Screen Siz - ### Minus Fraction (Passed through Mesh) ###Screen Siz CN Cyanide Extractior ORE GRADE 2q sample made to 1000ml volumetric for results > upper limit of meth( Ox-H2SO4 or -HC1 Dilute acid leach for oxide fraction in copper or molybdenum analys: QLA Dilute 10%H2SO4/0.5%Fe2(SO4)3 30C leach for acid soluble copper QLT Dilute 15%H2SO4 30C leach for acid soluble copper SAP Dilute 5%H2SO4/0.5%Fe2(SO4)3 85C leach for acid soluble & chalcocite coppe, D#A Digestion #-2,3 or 4 Acid: 2A=HC1/HNO3 3A-HC1/HNO3/HC104 4A=HC1/HNO3/HF/HC1C HC1 Hydrochloric Acid(37%w/v) Boiling Point 109 HE Hydrofluoric Acid(48%w/v) Boiling Point 108C Extreme Health Hazar HC104 Perchloric Acid(69%w/v) Boiling Point 203C Extreme Fire/Explosion Haza: HNO3 Nitric Acid(69%w/v) Boiling Point 121 H2SO4 Sulfuric Acid(98% w/v) Bailing Point 338 ICP-xB or -x[ ICP-AES and/or ICP-MS analysis using x=2, 3 or 4 acid digestior LiB02-C Lithium Metaborate fusion in Carbon crucibl Na202-C Sodium Peroxide fusion in Carbon crucibl Na202-Zr Sodium Peroxide fusion in Zirconium crucibl Technique AAS Atomic Absorption Spectroscop, ICP-AES Inductively Coupled Plasma Atomic Emission SpectroscoF ICP-MS Inductively Coupled Plasma Mass Spectroscop RG Research Grade (Low detection limit ICP-AES UT Ultra Trace (ICP-AES+ICP-MS analyses XRF-ED or -WE X-Ray Flourescence (-ED = Energy Dispersive) (-WD = Wavelength Dispersiv, XRD X-Ray Diffractior ELTRA-I Carbon & Sulfur infrared detection analyzer inductive heatir ELTRA-P Carbon, Hydrogen & Sulfur infrared detection analyzer resistance furna, LECO-I Nitrogen & Oxygen infra red detection analyzer inductive heatir MW Microwave Digestion ( -PT is at 1500psig and 3000 SG-WD or -HE Specific Gravity-WD=Water Displacement -HP=Helium Pycnometer lg/cm3=62.4lbs/f Definitions Page SP0112328 FINAL REPORT CLIENT SynTerra PROJECT Cape Fear Plant REFERENCE ABMW-2 AB 0-2 through ABMW-5 AB 0-2 REPORTED 5-Aug-2015 A1203 BaO CaO Cr203 Fe203 K20 Mg0 MnO Na20 P205 Si02 Sr0 Ti02 V205 As Cd Ce co Cu XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 1 0.2 1 1 1 SAMPLES Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct PPm PPm PPm PPm PPm ABMW-2 0-2 35.23 0.14 1.20 0.02 6.91 2.08 1.25 0.03 0.04 0.08 44.42 0.16 1.28 0.05 ill 0.3 27 9 52 ABMW-3 0-2 32.49 0.13 1.05 0.04 6.41 2.02 1.18 0.04 0.03 0.07 42.44 0.13 1.23 0.05 138 0.5 29 10 55 ABMW-3 19-20 31.49 0.12 1.80 0.03 7.99 1.80 1.12 0.03 0.04 0.06 36.50 0.18 1.25 0.04 82 0.3 22 7 34 ABMW-4 0-2 29.74 0.13 0.88 0.03 11.62 1.97 1.11 0.03 0.02 0.04 41.87 0.11 1.17 0.04 55 <0.2 14 9 37 ABMW-5 0-2 32.99 0.14 1.55 0.04 9.91 1.96 1.21 0.03 0.03 0.05 44.42 0.14 1.27 0.04 49 0.2 24 13 43 Page 3 of 5 AAL-008 SP0112328 FINAL REPORT CLIENT SynTerra PROJECT Cape Fear Plant REFERENCE ABMW-2 AB 0-2 thrc REPORTED 5-Aug-2015 Ga. La Mo Ni Pb Sb Se Sn W Zn Zr LOI H20- C S Sand >63 um Silt 2-63 um Clay <2um D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR LOI H20- ELTRA-C ELTRA-C Clay XRD Clay XRD Clay XRD 2 1 1 1 2 1 1 1 1 1 1 0.01 0.01 0.005 0.005 0.01 0.01 0.01 SAMPLES PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm PPm Pct Pct Pct Pct Pct Pct Pct ABMW-2 0-2 48 80 14 75 26 3 8 3 3 122 7 6.27 4.639 0.036 29.85 47.31 22.84 ABMW-3 0-2 47 75 7 102 20 3 7 3 7 113 5 10.75 7.633 0.039 26.57 61.20 12.23 ABMW-3 19-20 41 75 13 95 10 <1 8 2 2 81 5 13.65 11.749 0.070 32.58 52.37 15.05 ABMW-4 0-2 23 71 3 71 8 <1 1 1 1 47 5 8.59 6.913 0.032 64.21 29.40 6.39 ABMW-5 0-2 28 84 4 113 17 1 3 2 3 100 8.68 3.477 0.011 38.79 49.05 12.16 Page 4 of 5 AAL-008 SP0112328 FINAL REPORT CLIENT SynTerra PROJECT Cape Fear Plant REFERENCE ABMW-2 AB 0-2 thrc REPORTED 5-Aug-2015 Quartz Mullite Hematite Magnetite Calcite Biotite Clay XRD Clay XRD Clay XRD Clay XRD Clay XRD Clay XRD 0.1 0.1 0.1 0.1 0.1 0.1 SAMPLES Pct Pct Pct Pct Pct Pct ABMW-2 0-2 35.9 56.6 7.2 ABMW-3 0-2 40.8 52.7 6.5 ABMW-3 19-20 33.2 56.9 7.9 2.3 ABMW-4 0-2 41.6 45.1 3.5 2.8 6.4 ABMW-5 0-2 46.2 51.0 2.8 Page 5 of 5 AAL-008 SP0110392 FINAL REPORT Multi Element Package COPIES TO Samantha Wilkinson SynTerra CLIENT REFERENCE No: No. SAMPLES MAIN SAMPLE TYPE ABMW-1 SB 39-41 through AHMW-2 SB 27-28 3 CORE AMERICAN ASSAY LABORATORIES 1500 GLENDALE AVE. SPARKS, NV USA 89431-5902 Ph.(775) 356-0606 Fax.(775) 356-1413 EMAIL: info@aallabs.com RECEIVED 6-Apr-2015 REPORTED 12-May-2015 COMPANY DISCLAIMER :- When small samples are submitted, AAL may process the sample at smaller then specified weights to retain some pulp for quality control reassay. When Values exceed upper limits, AAL will run an Over Range analysis, to establish an accurate value. Additional cost will apply. Due to USDA Soil Quarantine programs - all foreign and some domestic soil material must be decontaminated by drying @ 125c for 48 hours, which will result in loss of Mercury (Hg). NEVADA LEGISLATIVE DISCLAIMER :- The results of this assay were based solely upon the content of the sample submitted. Any decision to invest should be made only after the potential investment value of the claim or deposit has been determined based on the results of assays of multiple samples of geological materials collected by the prospective investor or by a qualified person selected by him and based on an evaluation of all engineering data which is available concerning any proposed project. Nevada State Law NRS 519.130. ANALYSIS A1203 BaO CaO Cr203 Fe203 K20 MgO MnO Na20 P205 Si02 SrO Ti02 V205 As Cd Ce Cc Cu Ga La Me Ni Pb Sb Se METHOD XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR UNIT pet pet pet pet pet pet pet pet pet pet pet pet pet pet ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm LOWER LIMIT 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 1 0.2 1 1 1 2 1 1 1 2 1 1 ANALYSIS Sn W Zn Zr LOI H2O- C S >63 um -63 um.y <2um Quartz Illitedinitelulliteddspar Pyrite METHOD D4A-WR D4A-WR D4A-WR D4A-WR LOI H2O-ILTRA-CILTRA-C ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD UNIT ppm ppm ppm ppm pet pet pet pet pet pet pet pet pet pet pet pet pet LOWER LIMIT 1 1 1 1 0.01 0.01 0.005 0.005 0.01 0.01 0.01 0.1 0.1 0.1 0.1 0.1 0.1 Digitally signed by Joshua AMERICAN ASSAY Zimmerman Iaboraturles 1W Date: 2015.05.12 12:22:49 -07'00' SIGNATORY ANALYSIS Cover Page AAL-006 SP0110392 AMERICAN ASSAY LABORATORIES FINAL REPORT Is 1500 GLENDALE AVE. SPARKS, NV USA 89431-5902 Ph.(775) 356-0606 Fax.(775) 356-1413 EMAIL: AALLABS@NVBELL.NET Abbreviatior Definition Preparation DIP Sample Destroyed in Preparation DIS Sample Destroyed in Shipment ISS Insufficient Sample Submitte( SDI Sample Diesel Impregnate( SHI Sample Hydraulic Impregnate( SNR Sample Not Receivec Analysis STD - ?? International Reference Material Standar STD - AAL## AAL generated standard material BLANK AAL Laboratory Silica Blan] DTF Data to Folloc, DL Detection Limit of Metho( < or - Lens Than Lower Detection Limit of Metho > Greater than Upper Limit of Metho, N/A Not Analyzec NR Not Reportec (R) column Laboratory repeat weigh, digestion, analysis from original pulp or reject respl D or -D after Sample II Client submitted duplicate rig split sampl -R after Sample II Repeat analysis from original pulp reweigh, digestion and analys: -X after Sample If Repeat analysis from reject resplit, preparation, weigh, digestion and analys ppb Parts per Billion 0.001 ppm = 1 pp ppm Parts per Million 1 ppm = 1 mg/K OPT Troy Ounces per Short Ton(2,000 lbs)(1 ppm= 0.02917 OPT Oz Troy Ounce = 31.103 gram: o Percent 1%=10,000 pp: g Grams lg=0.001 kilogra mg Milligrams lmg=0.001gram Kg Kilograms 1Kg=1000gram ins Pounds llb=0.454kilogra Method FA-PB## Fire Assay Lead Collection - ## sample weight in gran GRAV Gravimetric (Weighed) finis] SF Screen Fire Assay reporting a plus, 2 minus fractions and a head Ca: + ### Plus Fraction (Retained on top of Mesh) ###Screen Siz - ### Minus Fraction (Passed through Mesh) ###Screen Siz CN Cyanide Extractior ORE GRADE 2q sample made to 1000ml volumetric for results > upper limit of meth( Ox-H2SO4 or -HC1 Dilute acid leach for oxide fraction in copper or molybdenum analys: QLA Dilute 10%H2SO4/0.5%Fe2(SO4)3 30C leach for acid soluble copper QLT Dilute 15%H2SO4 30C leach for acid soluble copper SAP Dilute 5%H2SO4/0.5%Fe2(SO4)3 85C leach for acid soluble & chalcocite coppe, D#A Digestion #-2,3 or 4 Acid: 2A=HC1/HNO3 3A-HC1/HNO3/HC104 4A=HC1/HNO3/HF/HC1C HC1 Hydrochloric Acid(37%w/v) Boiling Point 109 HE Hydrofluoric Acid(48%w/v) Boiling Point 108C Extreme Health Hazar HC104 Perchloric Acid(69%w/v) Boiling Point 203C Extreme Fire/Explosion Haza: HNO3 Nitric Acid(69%w/v) Boiling Point 121 H2SO4 Sulfuric Acid(98% w/v) Bailing Point 338 ICP-xB or -x[ ICP-AES and/or ICP-MS analysis using x=2, 3 or 4 acid digestior LiB02-C Lithium Metaborate fusion in Carbon crucibl Na202-C Sodium Peroxide fusion in Carbon crucibl Na202-Zr Sodium Peroxide fusion in Zirconium crucibl Technique AAS Atomic Absorption Spectroscop, ICP-AES Inductively Coupled Plasma Atomic Emission SpectroscoF ICP-MS Inductively Coupled Plasma Mass Spectroscop RG Research Grade (Low detection limit ICP-AES UT Ultra Trace (ICP-AES+ICP-MS analyses XRF-ED or -WE X-Ray Flourescence (-ED = Energy Dispersive) (-WD = Wavelength Dispersiv, XRD X-Ray Diffractior ELTRA-I Carbon & Sulfur infrared detection analyzer inductive heatir ELTRA-P Carbon, Hydrogen & Sulfur infrared detection analyzer resistance furna, LECO-I Nitrogen & Oxygen infra red detection analyzer inductive heatir MW Microwave Digestion ( -PT is at 1500psig and 3000 SG-WD or -HE Specific Gravity-WD=Water Displacement -HP=Helium Pycnometer lg/cm3=62.4lbs/f Definitions Page SP0110392 FINAL REPORT CLIENT SynTerra PROJECT : Cape Fear Plant REFERENCE : ABMW-1 SB 39-41 through ABMW-2 SB 27-28 REPORTED :12-May-2015 A1203 BaO CaO Cr203 Fe203 K20 MgO MnO Na20 P205 Si02 SrO Ti02 V205 As Cd Ce Co Cu Ga. La XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 1 0.2 1 1 1 2 1 SAMPLES Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct PPm PPm PPm PPm PPm PPm PPm ABMW-1 SB 39-41 21.08 0.05 0.38 0.04 6.26 1.66 3.28 0.15 1.04 0.26 65.92 <0.01 0.76 0.01 4 <0.2 135 40 16 11 2 ABMW-1 AS 13-15 35.42 0.07 0.94 0.03 3.87 2.08 2.00 0.07 0.22 0.23 41.39 0.02 0.72 <0.01 33 0.4 148 21 137 32 1 ABMW-2 SB 27-28 27.20 0.05 0.31 0.03 3.56 2.70 2.33 0.10 0.17 0.12 31.64 0.01 0.81 0.01 34 <0.2 328 25 91 20 <1 Page 3 of 5 AAL-008 SP0110392 FINAL REPORT CLIENT SynTerra PROJECT : Cape Fear Plant REFERENCE : ABMW-1 SB 39-41 1 REPORTED :12-May-2015 Mo Ni Pb Sb Se Sn W Zn Zr LOI H2O- C S Sand >63 um Silt 2-63 um Clay <2um Quartz Illite D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR LOI H2O- ELTRA-C ELTRA-C Clay XRD Clay XRD Clay XRD Clay XRD Clay XRD 1 1 2 1 1 1 1 1 1 0.01 0.01 0.005 0.005 0.01 0.01 0.01 0.1 0.1 SAMPLES ppm ppm ppm ppm ppm ppm ppm ppm ppm pct pct pct pct pct pct pct pct pct ABMW-1 SB 39-41 7 56 9 <1 <1 1 <1 32 19 2.29 0.63 0.080 <0.005 57.48 28.46 14.06 30.1 6.1 ABMW-1 AB 13-15 3 14 12 6 27 5 3 75 81 10.94 0.29 9.330 0.053 35.48 58.74 5.78 30.1 ABMW-2 SB 27-28 5 43 13 4 1 3 <1 85 53 21.68 1.23 10.296 0.571 79.98 13.12 6.90 17.5 41.4 Page 4 of 5 AAL-008 SP0110392 FINAL REPORT CLIENT SynTerra PROJECT : Cape Fear Plant REFERENCE : ABMW-1 SB 39-41 1 REPORTED :12-May-2015 Kaolinite Mullite Feldspar Pyrite Clay XRD Clay XRD Clay XRD Clay XRD 0.1 0.1 0.1 0.1 SAMPLES pct pct pct pct ABMW-1 SB 39-41 8.0 55.9 ABMW-1 AS 13-15 69.9 ABMW-2 SB 27-28 26.0 13.2 1.9 Page 5 of 5 AAL-008 SP0110873 FINAL REPORT Multi Element Package COPIES TO Samantha Wilkinson SynTerra CLIENT REFERENCE No: No. SAMPLES MAIN SAMPLE TYPE MW-15 SB 35-36 through MW-15: SB 18-19 4 CORE AMERICAN ASSAY LABORATORIES 1500 GLENDALE AVE. SPARKS, NV USA 89431-5902 Ph.(775) 356-0606 Fax.(775) 356-1413 EMAIL: info@aallabs.com RECEIVED 28-Apr-2015 REPORTED 8-Jul-2015 COMPANY DISCLAIMER :- When small samples are submitted, AAL may process the sample at smaller then specified weights to retain some pulp for quality control reassay. When Values exceed upper limits, AAL will run an Over Range analysis, to establish an accurate value. Additional cost will apply. Due to USDA Soil Quarantine programs - all foreign and some domestic soil material must be decontaminated by drying @ 125c for 48 hours, which will result in loss of Mercury (Hg). NEVADA LEGISLATIVE DISCLAIMER :- The results of this assay were based solely upon the content of the sample submitted. Any decision to invest should be made only after the potential investment value of the claim or deposit has been determined based on the results of assays of multiple samples of geological materials collected by the prospective investor or by a qualified person selected by him and based on an evaluation of all engineering data which is available concerning any proposed project. Nevada State Law NRS 519.130. ANALYSIS A1203 BaO CaO Cr203 Fe203 K20 MgO MnO Na20 P205 Si02 SrO Ti02 V205 As Cd Ce Cc Cu Ga La Me Ni Pb Sb Se METHOD XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR UNIT pet pet pet pet pet pet pet pet pet pet pet pet pet pet ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm LOWER LIMIT 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 1 0.2 1 1 1 2 1 1 1 2 1 1 ANALYSIS Sn W Zn Zr LOI H2O- C S >63 um -63 um.y <2um Quartz ldspard oritedinite Illitematiteihibole METHOD D4A-WR D4A-WR D4A-WR D4A-WR LOI H2O-ILTRA-CILTRA-C ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD UNIT ppm ppm ppm ppm pet pet pet pet pet pet pet pet pet pet pet pet pet pet LOWER LIMIT 1 1 1 1 0.01 0.01 0.005 0.005 0.01 0.01 0.01 0.1 0.1 0.1 0.1 0.1 0.1 0.1 SIGNATORY ANALYSIS Digitally signed by Cover Page AMERICAN ASSAY Joshua Zimmerman an.. Date:2015.07.08 17:39:00-07,00, SP0110873 AMERICAN ASSAY LABORATORIES FINAL REPORT Is 1500 GLENDALE AVE. SPARKS, NV USA 89431-5902 Ph.(775) 356-0606 Fax.(775) 356-1413 EMAIL: AALLABS@NVBELL.NET Abbreviatior Definition Preparation DIP Sample Destroyed in Preparation DIS Sample Destroyed in Shipment ISS Insufficient Sample Submitte( SDI Sample Diesel Impregnate( SHI Sample Hydraulic Impregnate( SNR Sample Not Receivec Analysis STD - ?? International Reference Material Standar STD - AAL## AAL generated standard material BLANK AAL Laboratory Silica Blan] DTF Data to Folloc, DL Detection Limit of Metho( < or - Lens Than Lower Detection Limit of Metho > Greater than Upper Limit of Metho, N/A Not Analyzec NR Not Reportec (R) column Laboratory repeat weigh, digestion, analysis from original pulp or reject respl D or -D after Sample II Client submitted duplicate rig split sampl -R after Sample II Repeat analysis from original pulp reweigh, digestion and analys: -X after Sample If Repeat analysis from reject resplit, preparation, weigh, digestion and analys ppb Parts per Billion 0.001 ppm = 1 pp ppm Parts per Million 1 ppm = 1 mg/K OPT Troy Ounces per Short Ton(2,000 lbs)(1 ppm= 0.02917 OPT Oz Troy Ounce = 31.103 gram: o Percent 1%=10,000 pp: g Grams lg=0.001 kilogra mg Milligrams lmg=0.001gram Kg Kilograms 1Kg=1000gram ins Pounds llb=0.454kilogra Method FA-PB## Fire Assay Lead Collection - ## sample weight in gran GRAV Gravimetric (Weighed) finis] SF Screen Fire Assay reporting a plus, 2 minus fractions and a head Ca: + ### Plus Fraction (Retained on top of Mesh) ###Screen Siz - ### Minus Fraction (Passed through Mesh) ###Screen Siz CN Cyanide Extractior ORE GRADE 2q sample made to 1000ml volumetric for results > upper limit of meth( Ox-H2SO4 or -HC1 Dilute acid leach for oxide fraction in copper or molybdenum analys: QLA Dilute 10%H2SO4/0.5%Fe2(SO4)3 30C leach for acid soluble copper QLT Dilute 15%H2SO4 30C leach for acid soluble copper SAP Dilute 5%H2SO4/0.5%Fe2(SO4)3 85C leach for acid soluble & chalcocite coppe, D#A Digestion #-2,3 or 4 Acid: 2A=HC1/HNO3 3A-HC1/HNO3/HC104 4A=HC1/HNO3/HF/HC1C HC1 Hydrochloric Acid(37%w/v) Boiling Point 109 HE Hydrofluoric Acid(48%w/v) Boiling Point 108C Extreme Health Hazar HC104 Perchloric Acid(69%w/v) Boiling Point 203C Extreme Fire/Explosion Haza: HNO3 Nitric Acid(69%w/v) Boiling Point 121 H2SO4 Sulfuric Acid(98% w/v) Bailing Point 338 ICP-xB or -x[ ICP-AES and/or ICP-MS analysis using x=2, 3 or 4 acid digestior LiB02-C Lithium Metaborate fusion in Carbon crucibl Na202-C Sodium Peroxide fusion in Carbon crucibl Na202-Zr Sodium Peroxide fusion in Zirconium crucibl Technique AAS Atomic Absorption Spectroscop, ICP-AES Inductively Coupled Plasma Atomic Emission SpectroscoF ICP-MS Inductively Coupled Plasma Mass Spectroscop RG Research Grade (Low detection limit ICP-AES UT Ultra Trace (ICP-AES+ICP-MS analyses XRF-ED or -WE X-Ray Flourescence (-ED = Energy Dispersive) (-WD = Wavelength Dispersiv, XRD X-Ray Diffractior ELTRA-I Carbon & Sulfur infrared detection analyzer inductive heatir ELTRA-P Carbon, Hydrogen & Sulfur infrared detection analyzer resistance furna, LECO-I Nitrogen & Oxygen infra red detection analyzer inductive heatir MW Microwave Digestion ( -PT is at 1500psig and 3000 SG-WD or -HE Specific Gravity-WD=Water Displacement -HP=Helium Pycnometer lg/cm3=62.4lbs/f Definitions Page SP0110873 FINAL REPORT CLIENT SynTerra PROJECT Cape Fear Plant REFERENCE MW-15 SB 35-36 through MW-15 SB 18-19 REPORTED 8-Jul-2015 A1203 BaO CaO Cr203 Fe203 K20 Mg0 MnO Na20 P205 Si02 Sr0 Ti02 V205 As Cd Ce co Cu XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 1 0.2 1 1 1 SAMPLES Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct PPm PPm PPm PPm PPm MW-15 SB 35-36 16.78 0.06 1.57 <0.01 8.16 1.07 1.23 0.03 0.64 0.95 65.54 <0.01 0.55 0.02 8 <0.2 62 19 45 MW-15 RB 73-74 18.32 0.08 1.15 0.01 7.17 0.91 1.58 0.13 0.74 0.16 64.43 0.01 0.59 0.03 9 <0.2 65 22 43 MW-15 RB 58-59 15.23 0.06 0.43 0.01 5.67 0.69 1.12 0.03 0.82 0.04 71.30 <0.01 0.63 0.02 5 <0.2 58 18 32 MW-15 SB 18-19 8.96 0.05 1.51 <0.01 3.77 1.32 0.68 0.06 1.03 0.06 80.71 0.02 0.59 0.01 2 <0.2 39 21 13 Page 3 of 5 AAL-008 SP0110873 FINAL REPORT CLIENT SynTerra PROJECT Cape Fear Plant REFERENCE MW-15 SB 35-36 thn REPORTED 8-Jul-2015 Ga La Mo Ni Pb Sb Se Sn W Zn Zr LOI H20- C S Sand >63 um Silt 2-63 um Clay <2um D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR LOI H20- ELTRA-C ELTRA-C Clay XRD Clay XRD Clay XRD 2 1 1 1 2 1 1 1 1 1 1 0.01 0.01 0.005 0.005 0.01 0.01 0.01 SAMPLES ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm pct pct pct pct pct pct pct MW-15 SB 35-36 16 30 4 51 16 2 <1 2 <1 88 57 4.77 0.107 <0.005 17.72 74.46 7.82 MW-15 RB 73-74 19 29 2 32 20 1 2 2 <1 118 41 5.47 0.338 0.137 56.40 34.68 8.92 MW-15 RB 58-59 13 26 2 27 18 2 <1 2 <1 88 35 3.68 0.073 <0.005 42.30 53.42 4.28 MW-15 SB 18-19 9 17 1 13 15 <1 1 <1 121 41 26 1.29 0.067 <0.005 74.88 18.98 6.14 Page 4 of 5 AAL-008 SP0110873 FINAL REPORT CLIENT SynTerra PROJECT Cape Fear Plant REFERENCE MW-15 SB 35-36 thn REPORTED 8-Jul-2015 SAMPLES MW-15 SB 35-36 MW-15 RB 73-74 MW-15 RB 58-59 MW-15 SB 18-19 Quartz Feldspar Chlorite Kaolinite Illite Hematite Amphibole Clay XRD Clay XRD Clay XRD Clay XRD Clay XRD Clay XRD Clay XRD 0.1 0.1 0.1 0.1 0.1 0.1 0.1 pct pct pct pct pct pct pct 31.8 10.0 9.8 46.4 2.0 21.1 10.0 5.3 3.4 57.8 25.1 10.3 4.2 4.8 55.6 0.4 54.2 24.4 7.2 3.6 8.4 2.3 Page 5 of 5 AAL-008 SP0111589 FINAL REPORT Multi Element Package COPIES TO Samantha Wilkinson SynTerra CLIENT REFERENCE No: No. SAMPLES MAIN SAMPLE TYPE ABMW-3BR - MW-9BR 4 CORE AMERICAN ASSAY LABORATORIES 1500 GLENDALE AVE. SPARKS, NV USA 89431-5902 Ph.(775) 356-0606 Fax.(775) 356-1413 EMAIL: info@aallabs.com RECEIVED 3-Jun-2015 REPORTED 31-Jul-2015 COMPANY DISCLAIMER :- When small samples are submitted, AAL may process the sample at smaller then specified weights to retain some pulp for quality control reassay. When Values exceed upper limits, AAL will run an Over Range analysis, to establish an accurate value. Additional cost will apply. Due to USDA Soil Quarantine programs - all foreign and some domestic soil material must be decontaminated by drying @ 125c for 48 hours, which will result in loss of Mercury (Hg). NEVADA LEGISLATIVE DISCLAIMER :- The results of this assay were based solely upon the content of the sample submitted. Any decision to invest should be made only after the potential investment value of the claim or deposit has been determined based on the results of assays of multiple samples of geological materials collected by the prospective investor or by a qualified person selected by him and based on an evaluation of all engineering data which is available concerning any proposed project. Nevada State Law NRS 519.130. ANALYSIS A1203 BaO CaO Cr203 Fe203 K20 MgO MnO Na20 P205 Si02 SrO Ti02 V205 As Cd Ce Cc Cu Ga La Me Ni Pb Sb Se METHOD XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR UNIT pet pet pet pet pet pet pet pet pet pet pet pet pet pet ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm LOWER LIMIT 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 1 0.2 1 1 1 2 1 1 1 2 1 1 ANALYSIS Sn W Zn Zr LOI H2O- C S >63 um -63 um.y <2um Quartz �ldspar Illite,liniteilorite:alcite�matitefnetite,lomite METHOD D4A-WR D4A-WR D4A-WR D4A-WR LOI H2O-ILTRA-CILTRA-C ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD UNIT ppm ppm ppm ppm pet pet pet pet pet pet pet pet pet pet pet pet pet pet pet pet LOWER LIMIT 1 1 1 1 0.01 0.01 0.005 0.005 0.01 0.01 0.01 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 Digitally signed by AMERICAN ASSAY Joshua Zimmerman �IabaraIories Date: 2015.07.31 11:50:52-07'00' SIGNATORY ANALYSIS Cover Page AAL-006 S P0111 589 AMERICAN ASSAY LABORATORIES FINAL REPORT Is 1500 GLENDALE AVE. SPARKS, NV USA 89431-5902 Ph.(775) 356-0606 Fax.(775) 356-1413 EMAIL: AALLABS@NVBELL.NET Abbreviatior Definition Preparation DIP Sample Destroyed in Preparation DIS Sample Destroyed in Shipment ISS Insufficient Sample Submitte( SDI Sample Diesel Impregnate( SHI Sample Hydraulic Impregnate( SNR Sample Not Receivec Analysis STD - ?? International Reference Material Standar STD - AAL## AAL generated standard material BLANK AAL Laboratory Silica Blan] DTF Data to Folloc, DL Detection Limit of Metho( < or - Lens Than Lower Detection Limit of Metho > Greater than Upper Limit of Metho, N/A Not Analyzec NR Not Reportec (R) column Laboratory repeat weigh, digestion, analysis from original pulp or reject respl D or -D after Sample II Client submitted duplicate rig split sampl -R after Sample II Repeat analysis from original pulp reweigh, digestion and analys: -X after Sample If Repeat analysis from reject resplit, preparation, weigh, digestion and analys ppb Parts per Billion 0.001 ppm = 1 pp ppm Parts per Million 1 ppm = 1 mg/K OPT Troy Ounces per Short Ton(2,000 lbs)(1 ppm= 0.02917 OPT Oz Troy Ounce = 31.103 gram: o Percent 1%=10,000 pp: g Grams lg=0.001 kilogra mg Milligrams lmg=0.001gram Kg Kilograms 1Kg=1000gram ins Pounds llb=0.454kilogra Method FA-PB## Fire Assay Lead Collection - ## sample weight in gran GRAV Gravimetric (Weighed) finis] SF Screen Fire Assay reporting a plus, 2 minus fractions and a head Ca: + ### Plus Fraction (Retained on top of Mesh) ###Screen Siz - ### Minus Fraction (Passed through Mesh) ###Screen Siz CN Cyanide Extractior ORE GRADE 2q sample made to 1000ml volumetric for results > upper limit of meth( Ox-H2SO4 or -HC1 Dilute acid leach for oxide fraction in copper or molybdenum analys: QLA Dilute 10%H2SO4/0.5%Fe2(SO4)3 30C leach for acid soluble copper QLT Dilute 15%H2SO4 30C leach for acid soluble copper SAP Dilute 5%H2SO4/0.5%Fe2(SO4)3 85C leach for acid soluble & chalcocite coppe, D#A Digestion #-2,3 or 4 Acid: 2A=HC1/HNO3 3A-HC1/HNO3/HC104 4A=HC1/HNO3/HF/HC1C HC1 Hydrochloric Acid(37%w/v) Boiling Point 109 HE Hydrofluoric Acid(48%w/v) Boiling Point 108C Extreme Health Hazar HC104 Perchloric Acid(69%w/v) Boiling Point 203C Extreme Fire/Explosion Haza: HNO3 Nitric Acid(69%w/v) Boiling Point 121 H2SO4 Sulfuric Acid(98% w/v) Bailing Point 338 ICP-xB or -x[ ICP-AES and/or ICP-MS analysis using x=2, 3 or 4 acid digestior LiB02-C Lithium Metaborate fusion in Carbon crucibl Na202-C Sodium Peroxide fusion in Carbon crucibl Na202-Zr Sodium Peroxide fusion in Zirconium crucibl Technique AAS Atomic Absorption Spectroscop, ICP-AES Inductively Coupled Plasma Atomic Emission SpectroscoF ICP-MS Inductively Coupled Plasma Mass Spectroscop RG Research Grade (Low detection limit ICP-AES UT Ultra Trace (ICP-AES+ICP-MS analyses XRF-ED or -WE X-Ray Flourescence (-ED = Energy Dispersive) (-WD = Wavelength Dispersiv, XRD X-Ray Diffractior ELTRA-I Carbon & Sulfur infrared detection analyzer inductive heatir ELTRA-P Carbon, Hydrogen & Sulfur infrared detection analyzer resistance furna, LECO-I Nitrogen & Oxygen infra red detection analyzer inductive heatir MW Microwave Digestion ( -PT is at 1500psig and 3000 SG-WD or -HE Specific Gravity-WD=Water Displacement -HP=Helium Pycnometer lg/cm3=62.4lbs/f Definitions Page SP0111589 FINAL REPORT CLIENT SynTerra PROJECT Cape Fear Plant REFERENCE ABMW-3BR - MW-9BR REPORTED 31-Jul-2015 A1203 BaO CaO Cr203 Fe203 K20 Mg0 MnO Na20 P205 Si02 Sr0 Ti02 V205 As Cd Ce co cu XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 1 0.2 1 1 1 SAMPLES Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct PPm PPm PPm PPm PPm ABMW-3BR 63-64 18.62 0.06 2.07 <0.01 11.95 1.66 1.12 0.07 0.85 0.16 54.37 0.01 0.59 <0.01 6 <0.2 72 15 27 MW-9BR 29-29.5 18.30 0.03 1.92 <0.01 2.59 0.87 0.51 0.05 1.58 0.02 64.95 0.03 0.45 <0.01 2 <0.2 55 7 11 MW-9BR 23.5-24 21.71 0.05 1.05 <0.01 6.23 1.56 1.10 0.03 1.28 0.03 56.09 0.02 0.65 <0.01 3 <0.2 37 12 11 MW-9BR 35-36 19.51 0.04 2.43 <0.01 5.22 0.94 1.17 0.07 1.55 0.11 61.26 0.03 0.60 <0.01 2 0.4 55 14 12 Page 3 of 5 AAL-008 SP0111589 FINAL REPORT CLIENT SynTerra PROJECT Cape Fear Plant REFERENCE ABMW-3BR - MW-91 REPORTED 31-Jul-2015 Ga La Mo Ni Pb Sb Se Sn W Zn Zr LOI H20- C S Sand >63 um Silt 2-63 um Clay <2um D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR LOI H20- ELTRA-C ELTRA-C Clay XRD Clay XRD Clay XRD 2 1 1 1 2 1 1 1 1 1 1 0.01 0.01 0.005 0.005 0.01 0.01 0.01 SAMPLES ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm pct pct pct pct pct pct pct ABMW-3BR 63-64 17 30 4 19 36 5 <1 1 <1 106 66 4.93 0.460 <0.005 17.57 70.50 11.93 MW-9BR 29-29.5 16 22 2 7 17 1 <1 2 3 137 25 2.33 0.340 0.005 44.47 47.52 8.01 MW-9BR 23.5-24 21 16 3 10 19 2 <1 2 1 123 46 3.93 0.029 <0.005 23.52 64.00 12.48 MW-9BR 35-36 19 22 2 12 17 3 <1 2 <1 94 31 2.46 0.071 <0.005 53.27 40.42 6.31 Page 4 of 5 AAL-008 SP0111589 FINAL REPORT CLIENT SynTerra PROJECT Cape Fear Plant REFERENCE ABMW-3BR - MW-91 REPORTED 31-Jul-2015 Quartz Feldspar Illite Kaolinite Chlorite Calcite Hematite Magnetite Dolomite Clay XRD Clay XRD Clay XRD Clay XRD Clay XRD Clay XRD Clay XRD Clay XRD Clay XRD 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 SAMPLES pct pct pct pct pct pct pct pct pct ABMW-3BR 63-64 27.1 8.1 51.5 4.5 2.5 6.5 0.2 MW-9BR 29-29.5 28.1 30.5 6.2 0.9 MW-9BR 23.5-24 23.7 20.7 49.9 3.3 2.4 MW-9BR 35-36 16.2 35.0 39.4 3.6 5.7 Page 5 of 5 AAL-008 SP0112087 FINAL REPORT Multi Element Package COPIES TO Samantha Wilkinson SynTerra CLIENT REFERENCE No: No. SAMPLES MAIN SAMPLE TYPE MW-6BR SB 36-37 through MW-6BR SB 26-27 2 CORE AMERICAN ASSAY LABORATORIES 1500 GLENDALE AVE. SPARKS, NV USA 89431-5902 Ph.(775) 356-0606 Fax.(775) 356-1413 EMAIL: info@aallabs.com RECEIVED 1-Jul-2015 REPORTED 6-Aug-2015 COMPANY DISCLAIMER :- When small samples are submitted, AAL may process the sample at smaller then specified weights to retain some pulp for quality control reassay. When Values exceed upper limits, AAL will run an Over Range analysis, to establish an accurate value. Additional cost will apply. Due to USDA Soil Quarantine programs - all foreign and some domestic soil material must be decontaminated by drying @ 125c for 48 hours, which will result in loss of Mercury (Hg). NEVADA LEGISLATIVE DISCLAIMER :- The results of this assay were based solely upon the content of the sample submitted. Any decision to invest should be made only after the potential investment value of the claim or deposit has been determined based on the results of assays of multiple samples of geological materials collected by the prospective investor or by a qualified person selected by him and based on an evaluation of all engineering data which is available concerning any proposed project. Nevada State Law NRS 519.130. ANALYSIS A1203 BaO CaO Cr203 Fe203 K20 MgO MnO Na20 P205 Si02 SrO Ti02 V205 As Cd Ce Cc Cu Ga La Me Ni Pb Sb Se METHOD XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR UNIT pet pet pet pet pet pet pet pet pet pet pet pet pet pet ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm LOWER LIMIT 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 1 0.2 1 1 1 2 1 1 1 2 1 1 ANALYSIS Sn W Zn Zr LOI H2O- C S >63 um -63 um.y <2um Quartz �ldspar Illited orited omite METHOD D4A-WR D4A-WR D4A-WR D4A-WR LOI H2O-ILTRA-CILTRA-C ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD ay XRD UNIT ppm ppm ppm ppm pet pet pet pet pet pet pet pet pet pet pet pet LOWER LIMIT 1 1 1 1 0.01 0.01 0.005 0.005 0.01 0.01 0.01 0.1 0.1 0.1 0.1 0.1 Digitally signed by AMERICAN ASSAY Joshua Zimmerman �Iahoratcries Date: 2015.08.06 VNEW 12:03:43-07'00' SIGNATORY ANALYSIS Cover Page AAL-006 SP0112087 AMERICAN ASSAY LABORATORIES FINAL REPORT Is 1500 GLENDALE AVE. SPARKS, NV USA 89431-5902 Ph.(775) 356-0606 Fax.(775) 356-1413 EMAIL: AALLABS@NVBELL.NET Abbreviatior Definition Preparation DIP Sample Destroyed in Preparation DIS Sample Destroyed in Shipment ISS Insufficient Sample Submitte( SDI Sample Diesel Impregnate( SHI Sample Hydraulic Impregnate( SNR Sample Not Receivec Analysis STD - ?? International Reference Material Standar STD - AAL## AAL generated standard material BLANK AAL Laboratory Silica Blan] DTF Data to Folloc, DL Detection Limit of Metho( < or - Lens Than Lower Detection Limit of Metho > Greater than Upper Limit of Metho, N/A Not Analyzec NR Not Reportec (R) column Laboratory repeat weigh, digestion, analysis from original pulp or reject respl D or -D after Sample II Client submitted duplicate rig split sampl -R after Sample II Repeat analysis from original pulp reweigh, digestion and analys: -X after Sample If Repeat analysis from reject resplit, preparation, weigh, digestion and analys ppb Parts per Billion 0.001 ppm = 1 pp ppm Parts per Million 1 ppm = 1 mg/K OPT Troy Ounces per Short Ton(2,000 lbs)(1 ppm= 0.02917 OPT Oz Troy Ounce = 31.103 gram: o Percent 1%=10,000 pp: g Grams lg=0.001 kilogra mg Milligrams lmg=0.001gram Kg Kilograms 1Kg=1000gram ins Pounds llb=0.454kilogra Method FA-PB## Fire Assay Lead Collection - ## sample weight in gran GRAV Gravimetric (Weighed) finis] SF Screen Fire Assay reporting a plus, 2 minus fractions and a head Ca: + ### Plus Fraction (Retained on top of Mesh) ###Screen Siz - ### Minus Fraction (Passed through Mesh) ###Screen Siz CN Cyanide Extractior ORE GRADE 2q sample made to 1000ml volumetric for results > upper limit of meth( Ox-H2SO4 or -HC1 Dilute acid leach for oxide fraction in copper or molybdenum analys: QLA Dilute 10%H2SO4/0.5%Fe2(SO4)3 30C leach for acid soluble copper QLT Dilute 15%H2SO4 30C leach for acid soluble copper SAP Dilute 5%H2SO4/0.5%Fe2(SO4)3 85C leach for acid soluble & chalcocite coppe, D#A Digestion #-2,3 or 4 Acid: 2A=HC1/HNO3 3A-HC1/HNO3/HC104 4A=HC1/HNO3/HF/HC1C HC1 Hydrochloric Acid(37%w/v) Boiling Point 109 HE Hydrofluoric Acid(48%w/v) Boiling Point 108C Extreme Health Hazar HC104 Perchloric Acid(69%w/v) Boiling Point 203C Extreme Fire/Explosion Haza: HNO3 Nitric Acid(69%w/v) Boiling Point 121 H2SO4 Sulfuric Acid(98% w/v) Bailing Point 338 ICP-xB or -x[ ICP-AES and/or ICP-MS analysis using x=2, 3 or 4 acid digestior LiB02-C Lithium Metaborate fusion in Carbon crucibl Na202-C Sodium Peroxide fusion in Carbon crucibl Na202-Zr Sodium Peroxide fusion in Zirconium crucibl Technique AAS Atomic Absorption Spectroscop, ICP-AES Inductively Coupled Plasma Atomic Emission SpectroscoF ICP-MS Inductively Coupled Plasma Mass Spectroscop RG Research Grade (Low detection limit ICP-AES UT Ultra Trace (ICP-AES+ICP-MS analyses XRF-ED or -WE X-Ray Flourescence (-ED = Energy Dispersive) (-WD = Wavelength Dispersiv, XRD X-Ray Diffractior ELTRA-I Carbon & Sulfur infrared detection analyzer inductive heatir ELTRA-P Carbon, Hydrogen & Sulfur infrared detection analyzer resistance furna, LECO-I Nitrogen & Oxygen infra red detection analyzer inductive heatir MW Microwave Digestion ( -PT is at 1500psig and 3000 SG-WD or -HE Specific Gravity-WD=Water Displacement -HP=Helium Pycnometer lg/cm3=62.4lbs/f Definitions Page SP0112087 FINAL REPORT CLIENT SynTerra PROJECT Cape Fear Plant REFERENCE MW-6BR SB 36-37 through MW-6BR SB 26-27 REPORTED 6-Aug-2015 A1203 BaO CaO Cr203 Fe203 K20 Mg0 MnO Na20 P205 Si02 Sr0 Ti02 V205 As Cd Ce co Cu XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR XRF-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 1 0.2 1 1 1 SAMPLES Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct Pct PPm PPm PPm PPm PPm MW-6BR SB 36-37 15.12 0.04 2.95 0.02 4.50 0.89 1.08 0.08 1.71 0.06 69.82 0.04 0.57 <0.01 2 <0.2 8 11 12 MW-6BR SB 26-27 16.71 0.04 2.59 0.03 4.80 0.95 1.02 0.09 1.75 0.20 69.28 0.03 0.48 <0.01 2 <0.2 7 9 9 Page 3 of 5 AAL-008 SP0112087 FINAL REPORT CLIENT SynTerra PROJECT Cape Fear Plant REFERENCE MW-6BR SB 36-37 tl REPORTED 6-Aug-2015 Ga La Mo Ni Pb Sb Se Sn W Zn Zr LOI H20- C S Sand >63 um Silt 2-63 um Clay <2um D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR D4A-WR LOI H20- ELTRA-C ELTRA-C Clay XRD Clay XRD Clay XRD 2 1 1 1 2 1 1 1 1 1 1 0.01 0.01 0.005 0.005 0.01 0.01 0.01 SAMPLES ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm ppm pct pct pct pct pct pct pct MW-6BR SB 36-37 14 19 1 9 12 <1 <1 1 <1 76 20 1.98 0.052 <0.005 67.78 25.15 7.07 MW-6BR SB 26-27 15 18 <1 11 11 <1 <1 1 <1 67 16 3.48 0.113 0.009 66.16 24.53 9.31 Page 4 of 5 AAL-008 SP0112087 FINAL REPORT CLIENT SynTerra PROJECT Cape Fear Plant REFERENCE MW-6BR SB 36-37 tl REPORTED 6-Aug-2015 Quartz Feldspar Illite Chlorite Dolomite Clay XRD Clay XRD Clay XRD Clay XRD Clay XRD 0.1 0.1 0.1 0.1 0.1 SAMPLES pct pct pct pct pct MW-6BR SB 36-37 20.3 38.0 39.4 1.2 0.9 MW-6BR SB 26-27 23.6 42.5 30.1 2.3 0.9 Page 5 of 5 AAL-008