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HomeMy WebLinkAboutWQ0034380_Monitoring - 07-2023_20230815WAYNEt SANDERff TOGETHER, WE MAKE CHICKEN AMAZING Certified Mail #7021 2720 0000 4465 1766 August 9, 2023 Division of Water Quality Information Processing -14Q Szs Unit r►�+� 1617 Mail Service Center 44, Raleigh, NC 27699-1617 Re: Sanderson Farms, Inc. Q Kinston, Lenoir County Permit No. WQ0034380 Please find attached the original and (1) copy Compliance Monitoring Forms (GW-59) for each well and the GW-59A Compliance Report Form that are required three times a year. If you need further information, please contact me at (601) 426-1572. Sincerely, Stephanie Shoemaker Sr. Director of Environmental, Regulatory and Permitting Wayne -Sanderson Farms, LLC CC: David May, Regional Supervisor Division of Water Quality Aquifer Protection Section 943 Washington Square Mall Washington, NC 27889 Certified Mail #7021 2720 0000 4465 1773 waynesandersonfarms. com SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Pnnt Clearly or Type PERMIT Number: Expiration Date: Facility Name: Sanderson Farms WWTF Non -Discharge WQ0034380 UIC Permit Name (if different): same NPDES Other Facility Address: 2081 Sanderson Way Kinston NC 28504 TYPE OF PERMITTED OPERATION BEING MONITORED 2081 Sanderson Way Kinston NC 285t1$"" County Lenoir ❑ Lagoon ❑ Remediation: Infiltration Gallery - 0 Spray Field ❑ Remediation: Contact Person: Joseph Franklin Telephone#: 252-902-8906 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Sanderson Farms WWTF WW Irrigation System No. of wells to be sampled: Eight (8) ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-1 Date sample collected: 7/25/2023 FIELD ANALYSES: WAS Well Depth: 20 ft. Well Diameter: 2 in. pH 00400: 5.2 units Temp. 000lo: 20.9 °C DRY at Depth to Water Level 82546: 11.58 ft. below measuring point Screened Interval: 5 ft. to 20 ft. Spec. Cond. 000sa: µMhos time ofsampling, Measuring Point is 3.11 ft. above land surface Relative M.P. Elevation: 48.31 ft. Odor 00085: none check Volume of water pumped/bailed before sampling: 10 gallons Appearance cloudy here: ❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 7/26/2023-8/8/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. #94/#37729 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.13 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.45 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.19 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 7030o 38 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 0068o 3.8 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 8 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 0.4 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.05-02-2017 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: Facility Name: Sanderson Farms WWTF Non -Discharge W00034380 UIC Permit Name (if different): same NPDES Other Facility Address: 2081 Sanderson Way Kinston NC 28504 TYPE OF PERMITTED OPERATION BEING MONITORED 2081 Sanderson Way Kinston NC 28564°" County Lenoir ❑ Lagoon ❑ Remediation: Infiltration Gallery ■❑ Spray Field ❑ Remediation: Contact Person: Joseph Franklin Telephone#: 252-902-8906 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Sanderson Farms WWTF WW Irrigation System No. of wells to be sampled: Eight (8) ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-2 Date sample collected: 7/25/2023 FIELD ANALYSES: WAS Well Depth: 20 ft. Well Diameter: 2 in. pH 00400: 5.9 units Temp. 000lo: 24.2 °C DRY at Depth to Water Level 82546: 4.17 ft. below measuring point Screened Interval: 5 ft. to 20 ft. Spec. Cond. 00094: µM time ofhos sampling, Measuring Point is 3.83 ft. above land surface Relative M.P. Elevation: 42.63 ft. Odor 00085: none check Volume of water pumped/bailed before sampling: 10 gallons Appearance clear here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 7/26/2023-8/8/2023 Laboratory Name: Environmental Chemists, Inc. Certification No. #94/#37729 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.06 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.23 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 7030o 346 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 36.1 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 99 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3as N: Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.05-02-2017 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: Facility Name: Sanderson Farms WWTF Non -Discharge W00034380 UIC Permit Name (if different): same NPDES Other Facility Address: 2081 Sanderson Way Kinston NC 28504 TYPE OF PERMITTED OPERATION BEING MONITORED 2081 Sanderson Way Kinston NC 28564`' County Lenoir ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: Contact Person: Joseph Franklin Telephone#: 252-902-8906 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Sanderson Farms WWTF WW Irrigation System No. of wells to be sampled: Eight (8) ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-3 Date sample collected: 7/25/23 FIELD ANALYSES: WAS Well Depth: 20 ft. Well Diameter: 2 in. pH oo400: 6.08 units Temp. 000lo: 24.4 °C DRY at Depth to Water Level 82546: 5.0 ft. below measuring point Screened Interval: 5 ft. to 20 ft. Spec. Cond. 00094: µMhos time ofsampling, Measuring Point is 3•02 ft. above land surface Relative M.P. Elevation: 40.92 ft. Odor 00085: none check Volume of water pumped/bailed before sampling: 10 gallons Appearance clear here: ❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 7/26/23-8/8/23 Laboratory Name: Environmental Chemists, Inc. Certification No. #94/#37729 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 0.06 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 1.05 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.23 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 7030o 233 mg/L Al - Aluminum o11o5 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 0068o 8.0 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 84 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOC& mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.05-02-2017 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: • • • • INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: Facility Name: Sanderson Farms WWTF Non -Discharge WQ0034380 UIC Permit Name (if different): same NPDES Other Facility Address: 2081 Sanderson Way Kinston NC 28504 TYPE OF PERMITTED OPERATION BEING MONITORED 2081 Sanderson Way Kinston NC 28504"" County Lenoir ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: Contact Person: Joseph Franklin Telephone#: 252-902-8906 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Sanderson Farms WWTF WW Irrigation System No. of wells to be sampled: Eight (8) ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-4 Date sample collected: 7/25/23 FIELD ANALYSES: WAS Well Depth: 20 ft. Well Diameter: 2 in. pH 0040o: 6.24 units Temp. 000lo: 24.7 °C DRY at Depth to Water Level 82546: 4.75 ft. below measuring point Screened Interval: 5 ft. to 20 — ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 2.95 ft. above land surface Relative M.P. Elevation: 36.05 ft. Odor 00085: none check Volume of water pumped/bailed before sampling: 10 gallons Appearance clear here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 7/26/23-8/8/23 Laboratory Name: Environmental Chemists, Inc. Certification No. #94/#37729 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.04 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.14 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.48 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 7030o 460 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 0068o 45.1 mg/L Ca - Calcium 00916 mg/L Chloride 00940 110 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 2.0 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3as N. Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Paul Billingsley, VP of Development and Engineering Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.05-02-2017 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: Facility Name: Sanderson Farms WWTF Non -Discharge WQ0034380 UIC Permit Name (if different): same NPDES Other Facility Address: 2081 Sanderson Way Kinston NC 28504 TYPE OF PERMITTED OPERATION BEING MONITORED 2081 Sanderson Way Kinston NC 28564`°' County Lenoir ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: Contact Person: Joseph Franklin Telephone#: 252-902-8906 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Sanderson Farms WWTF WW Irrigation System No. of wells to be sampled: Eight (8) ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-6 Date sample collected: 7/25/23 FIELD ANALYSES: WAS Well Depth: 11 ft. Well Diameter: 2 in. pH oo4o0: 6.6 units Temp. 000lo: 26.2 °C DRY at Depth to Water Level 82546: 7.67 ft. below measuring point Screened Interval: 6 ft. to 11 ft. Spec. Cond. 000sa: [Mhos time ofsampling, Measuring Point is 3.04 ft. above land surface Relative M.P. Elevation: 40.34 ft. Odor 00085: none check Volume of water pumped/bailed before sampling: 10 gallons Appearance clear here: ❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 7/26/23-8/8/23 Laboratory Name: Environmental Chemists, Inc. Certification No. #94/#37729 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.05 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 4.19 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 8.31 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 703oo 267 mg/L Al - Aluminum oilo5 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 10.3 mg/L Ca - Calcium 00916 mg/L Chloride 00940 125 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N, Ammonia Nitrogen, Total) Mn - Manganese 01o55 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.05-02-2017 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: Facility Name: Sanderson Farms WWTF Non -Discharge WQ0034380 UIC Permit Name (if different): same NPDES Other Facility Address: 2081 Sanderson Way Kinston NC 28504 TYPE OF PERMITTED OPERATION BEING MONITORED 2081 Sanderson Way Kinston NC 28564`=` County Lenoir ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: Contact Person: Joseph Franklin Telephone#: 252-902-8906 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Sanderson Farms WWTF WW Irrigation System No. of wells to be sampled: Eight (8) ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-7 Date sample collected: 7/25/23 FIELD ANALYSES: WAS Well Depth: 16 ft. Well Diameter: 2 in. pH ooaoo: 6.73 units Temp. 000lo: 25.3 °C DRY at Depth to Water Level 62546: 5.25 ft. below measuring point Screened Interval: 6 ft. to 16 ft. Spec. Cond. 000sa: µMhos time ofsampling, Measuring Point is 2.33 ft. above land surface Relative M.P. Elevation: 36.28 ft. Odor 00085: none check Volume of water pumped/bailed before sampling: 10 gallons Appearance clear here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 7/26/23-8/8/23 Laboratory Name: Environmental Chemists, Inc. Certification No. #94/#37729 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.47 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 1.50 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 150 mg/L All - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 0.9 mg/L Ca - Calcium 00916 mg/L Chloride 00940 16 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen. NH3as N, Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.05-02-2017 SUBMIT FORM ON YELLOW PAPER ONLY • . DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: Facility Name: Sanderson Farms WWTF Non -Discharge WQ0034380 UIC Permit Name (if different): same NPDES Other Facility Address: 2081 Sanderson Way Kinston NC 28504 TYPE OF PERMITTED OPERATION BEING MONITORED 2081 Sanderson Way Kinston NC 28504"' County Lenoir ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: Contact Person: Joseph Franklin Telephone#: 252-902-8906 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Sanderson Farms WWTF WW Irrigation System No. of wells to be sampled: Eight (8) ❑ Water Source Heat Pump ❑ Other: (from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-8 Date sample collected: 7/25/23 FIELD ANALYSES: WAS Well Depth: 12.7 ft. Well Diameter: 2 in. pH 00000: 5.65 units Temp. 000lo: 25.5 °C DRY at Depth to Water Level 82546: 5.25 ft. below measuring point Screened Interval: 2.7 ft. to 12.7 ft. Spec. Cond. 000sa: µMhos time ofsampling, Measuring Point is 3.34 ft. above land surface Relative M.P. Elevation: 38.39 ft. Odor 00085: none check Volume of water pumped/bailed before sampling: 10 gallons Appearance clear here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 7/26/23-8/8/23 Laboratory Name: Environmental Chemists, Inc. Certification No. #94/#37729 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.03 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 5.34 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.12 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 703oo 292 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 0068o 8.8 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 94 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3as N. Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Paul Billingsley, VP of Development and Engineering Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.05-02-2017 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearty or Type PERMIT Number: Expiration Date: Facility Name: Sanderson Farms WWTF Non -Discharge WQ0034380 UIC Permit Name (if different): same NPDES Other Facility Address: 2081 Sanderson Way Kinston NC 28504 TYPE OF PERMITTED OPERATION BEING MONITORED 2081 Sanderson Way Kinston NC 285'04°' County Lenoir ❑ Lagoon ❑ Remediation: Infiltration Gallery A Spray Field ❑ Remediation: Contact Person: Joseph Franklin Telephone#: 252-902-8906 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Sanderson Farms WWTF WW Irrigation System No. of wells to be sampled: Eight (8) ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-9 Date sample collected: 7/25/23 FIELD ANALYSES: WAS Well Depth: 12.5 ft. Well Diameter: 4 in. pH 00000: 5.98 units Temp. 000lo: 27.3 °C DRY at Depth to Water Level 82546: 3.58 ft. below measuring point Screened Interval: 2.5 ft. to 12.5 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 2.85 ft. above land surface Relative M.P. Elevation: 37.18 ft. Odor 00085: none check Volume of water pumped/bailed before sampling: 10 gallons Appearance clear here: ❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 7/26/23-8/8/23 Laboratory Name: Environmental Chemists, Inc. Certification No. #94/#37729 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 4.36 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.08 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 703oo 392 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 0068o 8.3 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 78 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.05-02-2017 GW-59A COMPLIANCE REPORT FORM Permit # WQ00343R0 (Submit one each monitoring period with GW-59 forms.) 1 Enter date monitoring results were due. ( ) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? X 2 Was any required information missing on the GW-59 report forms? YES NO IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance X 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is "NO", skip to section 8, if the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below. Monitoring Well 44 - Ammonia Nitrogen is 1.5 mg/L. 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? X If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). Monitoring Well 94 - Ammonia Nitrogen 2.0 mg/L November 2021; March 2023 Ammonia Nitrogen 2.0 mg/L 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? if the answer to question 7 is "YES", describe those actions in the space provided below. X If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. Will contact Randy Sipe at Washington Regional Office. g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Comp ancee RReepport GW-59A) is true and complete to the best of my knowledge. / `T - O Z Signature of Permittee (or Authorized Agent) at GW-59A 12/8/2003 k envirochem ANALYTICAL & CONSULTING CHEMISTS FF"07 _77 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 4 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/ Fax info;, a. environmentalchemists com Sanderson Farms -Kinston Date of Report: Aug 08, 2023 2081 Sanderson Way Customer PO #: Kinston NC 28504 Customer ID: 13100004 Attention: Report #: 2023-16029 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-39575 Site: MW-1 7/25/2023 10:46 AM Water Tim Carrell & Terry Summers Test Ammonia Nitrogen Total Dissolved Solids (TDS) Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Chloride Nitrate Nitrogen (Calc) Method EPA 350.1, Rev 20, 1993 SM 2540 C-2015 SM 4500 P (F-H)-2011 SM 5310 8-2014 SM 9222 0-2015 MF SM4500 CI E-2011 Results Date Analyzed 0.4 mg/L 07/26/2023 38 mg/L 07/26/2023 0.19 mg/L 08/07/2023 3.8 mg/L 07/27/2023 <1 Colonies/100mL 07/25/2023 8 mg/L 07/28/2023 Nitrite Nitrogen EPA 353.2, Rev. 2.0 1993 0.13 mg/L 07/25/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0.1993 0.58 mg/L 08/01/2023 Nitrate Nitrogen Subtraction Method 0.45 mg/L 08/08/2023 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-39576 Site: MW-2 7/25/2023 10-27 AM Water Tim Carrell & Terry Summers Test Method Results Date Analyzed Ammonia Nitrogen Total Dissolved Solids (TDS) Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Chloride Nitrate Nitrogen (Calc) EPA 350.1. Rev. 2.0, 1993 SM 2540 C-2015 SM 4500 P (F-H)-2011 SM 5310 B-2014 SM 9222 D-2015 MF SM4500 CI E-2011 0.2 mg/L 07/26/2023 346 mg/L 07/26/2023 0.23 mg/L 08/07/2023 36.1 mg/L 07/27/2023 <1 Colonies/100mL 07/25/2023 99 mg/L 07/28/2023 Nitrite Nitrogen EPA 353.2, Rev. 2.0 1993 0.06 mg/L 07/25/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev, 2.0, 1993 0.06 mg/L 08/01/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 08/08/2023 Report M: 2023.16029 Page 1 of 4 ropp- _- 77 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Sanderson Farms -Kinston Date of Report: Aug 08, 2023 2081 Sanderson Way Customer PO #: Kinston NC 28504 Customer ID: 13100004 Attention: Report #: 2023-16029 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-39577 Site: MW-3 7/25/2023 9:15 AM Water Tim Carrell & Terry Summers Test Method Results Date Analyzed Ammonia Nitrogen EPA 350.1, Rev, 2.0, 1993 < 0.2 mg/L 07/26/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 233 mg/L 07/26/2023 Total Phosphorus SM 4500 P ;F-H;.-2011 0.23 mg/L 08/07/2023 Total Organic Carbon (TOC) SM 5310 a-2014 8.0 mg/L 07/27/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 07/25/2023 Chloride SM4500 C E-2011 84 mg/L 07/28/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2. Rev 2 0. 1993 0.06 mg/L 07/25/2023 Nitrate+N itrite-Nitrogen EPA 353.2, Rev 2 0, 1993 1,11 mg/L 08101 /2023 Nitrate Nitrogen Subtraction Method 1.05 mg/L 08/08/2023 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-39578 Site: MW-4 7/25/2023 9:08 AM Water Tim Carrell & Terry Summers Test Method Results Date Analyzed Ammonia Nitrogen EPA 350.1, Rev 2 0, 1993 2.0 mg/L 07/27/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 460 mg/L 07/26/2023 Total Phosphorus SM 4500 P (F-H)-2011 0.48 mg/L 08/07/2023 Total Organic Carbon (TOC) SM 5310 8-2014 45.1 mg/L 07/27/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 07/25/2023 Chloride SM4500 Ci E-2011 110 mg/L 07/28/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2, Rev. 2 0, 1993 0.04 mg/L 07/25/2023 Nitrate+Nitrite-Nitrogen EPA 353 2, Rev. 2 0,1993 0.18mg/L 08/01/2023 Nitrate Nitrogen Subtraction Method 0.14mg/L 08/08/2023 Report X 2023-16029 Page 2 of 4 ! . ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392-4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info:a environmentalchemists.com Sanderson Farms -Kinston Date of Report: Aug 08, 2023 2081 Sanderson Way Customer PO #: Kinston NC 28504 Customer ID: 13100004 Attention. Report #: 2023-16029 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-39579 Site: MW-6 7/25/2023 10:05 AM Water Tim Carrell & Terry Summers Test Method Results Date Analyzed Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 07/27/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 267 mg/L 07/26/2023 Total Phosphorus SM 4500 P (F-H)-2011 8.31 mg/L 08/07/2023 Total Organic Carbon (TOC) SM 5310 B-2014 10.3 mg/L 07/27/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 07/25/2023 Chloride SM4500 C1 E-2011 125 mg/L 07/28/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2. Rev 2 0.1993 0.05 mg/L 07/25/2023 Nitrate+Nitrite-Nitrogen EPA 353 2, Rev. 2 0, 1993 4.24 mg/L 08/01 /2023 Nitrate Nitrogen Subtraction Method 4.19 mg/L 08/08/2023 Lab ID Sample ID: Collect Daterrime Matrix Sampled by 23-39580 Site: MW-7 7/25/2023 10:12 AM Water Tim Carrell & Terry Summers Test Method Results Date Analyzed Ammonia Nitrogen Total Dissolved Solids (TDS) Total Phosphorus Total Organic Carbon (TOC) Fecal Coliform Chloride Nitrate Nitrogen (Calc) Nitrite Nitrogen N itrate+N itrite-Nitrogen Nitrate Nitrogen EPA 350.1. Rev. 2 0, 1993 SM 2540 C-2015 SM 4500 P (F-H)-2011 SM 5310 B-2014 SM 9222 D-2015 MF SM4500 CI E-2011 EPA 353 2, Rev 2 0, 1993 EPA 353 2, Rev. 2 0, 1993 Subtraction Method < 0.2 mg/L 07/27/2023 150 mg/L 07/26/2023 1.50 mg/L 08/07/2023 0.9 mg/L 07/27/2023 <1 Colonies/100mL 07/25/2023 16 mg/L 07/28/2023 < 0.02 mg/L 0.47 mg/L 0.47 mg/L 07/25/2023 08101 /2023 08/08/2023 Report V 2023-16029 Page 3 of 4 envirochem ANALYTICAL & CONSULTING CHEMISTS Sanderson Farms -Kinston 2081 Sanderson Way Kinston NC 28504 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab a 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax infoia environmentalchemists com Date of Report: Aug 08, 2023 Customer PO M Customer ID: 13100004 Report #: 2023-16029 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-39581 Site: MW-8 7/25/2023 9:46 AM Water Tim Carrell & Terry Summers Test Method Results Date Analyzed Ammonia Nitrogen EPA3501 Rev 20.1993 < 0.2 mg/L 07/27/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 292 mg/L 07/26/2023 Total Phosphorus SM 4500 P (F-H)-2011 0.12 mg/L 08/07/2023 Total Organic Carbon (TOC) SM 5310 B-2014 8.8 mg/L 07/27/2023 Fecal Coliform SM 9222 D-201 5 MF <1 Colonies/100ml- 07/25/2023 Chloride SM4500 CI E-2011 94 mg/L 07/28/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0 1993 0.03 mg/L 07/25/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev 2.0 1993 5.37 mg/L 08/01/2023 Nitrate Nitrogen Subtraction Method 5.34 mg/L 08/08/2023 Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-39582 Site: MW-9 7/25/2023 9:37 AM Water Tim Carrell & Terry Summers Test Method Results Date Analyzed Ammonia Nitrogen EPA 350.1, Rev 2 0. 1993 < 0.2 mg/L 07/27/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 392 mg/L 07/26/2023 Total Phosphorus SM 4500 P (F-H).2011 0.08 mg/L 08/07/2023 Total Organic Carbon (TOC) SM 5310 B-2014 8.3 mg/L 07/27/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 07/25/2023 Chloride SM4500 C) E-2011 78 mg/L 07/28/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev 2 0.1993 < 0.02 mg/L 07/25/2023 Nitrate+Nitrite-Nitrogen CPA353.2, Rev 20, 1993 4.36 mg/L 08/01/2023 Nitrate Nitrogen Subtraction Method 4.36 mg/L 08/08/2023 Comment: Reviewed by: i r Report #.: 2023.16329 Page 4 of 4 Environmental Chemist, Inc., Wilmington, NC Lab #94 Sample Receipt Checklist 6602 Windmill Way Wilmington, NC 28405 910.392.0223 Client:_Se,, hr^,-,,,3 Date: 3 Report Number: _ 2023- ) Receipt of sample: ECHEM Pickup Client Delivery ❑ UPS ❑ FeclEx ❑ Other ❑ ❑ YES ❑ NO � IN 1. Were custody seals present on the cooler? ❑ YES ❑ NO ❑O N/A 2. If custody seals were present, were they intact/unbroken? Original temperature upon receipt °C Corrected temperature upon receipt How temperature taken: ❑ Temperature Blank Ox Against Bottles IR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0 9 YES ❑ NO 3. if temperature of cooler exceeded 6°C, was Project Mgr./QA notified? ❑x YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO S. Were sample ID's listed on the COC? YES ❑ NO 6. Were samples ID's listed on sample containers? 7. Were collection date and time listed on the COC? 21 YES ❑ NO ❑x YES ❑ NO 8. Were tests to be performed listed on the COC? x❑ YES ❑ NO 9. Did samples arrive in proper containers for each test? O YES NO NO 10. Did samples arrive in good condition for each test? O YES ❑ NO 11. Was adequate sample volume available?' 12. Were samples received within proper holding time for requested tests? 9 YES ❑ NO YES ❑ NO 13. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES ❑ NO 15. Were sulfide samples received at a pH >9? BYES ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCl NaOH Time of preservation: if more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified. date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 "C i :alep :AS paAiaoaa :AS pa.laA118o wesaa :paloafab :paldao3v :O, paAlaoaa U04m ainle.ladwal all Z '6 awlLa 4 :AS pan, lLaleq :ftf3 payslnbullab JalsuWl 9 9 d 0 9 9 d 0 9 9 d 0 9 9 d 0 9 9 �yC IA :JopO d 0 9 9 ,,�J ? J0103 d Wi0plo0 leoad X 9 9 ,r :(plag) 4 d 0 001 X 9 9 :pal!e8 suolle9 d d lelol `£ON '£HN X J 9 (� :aaleM of Ul ad d 0 Sal'ZON'apuol40 X 9 9 LL /dGZ 1 :IIaM uljoliuovy, d 0 ! 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