WQ0039924_Permit Application_20180401

za•
Water Resources
ENVIRONMENTAL QUALITY
April 16, 2018
JUSTIN DAWKINs — PLANT MANAGER
VON DREHLE CORPORATION
126 FIRST ST.
CORDOVA, NORTH CAROLINAi28330
Dear Mr. Dawkins:
ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
LINDA CULPEPPER
Interim Director
Subject: Acknowledgement of
Application No. WQ0039924
von Drehle Corporation DCAR
Residuals Management System
Richmond County
The Water Quality Permitting Section acknowledges receipt of your permit application and
supporting documentation received on April 16, 2018. Your application package has been assigned the
number listed above, and the primary reviewer is Troy Doby.
Central and Regional Office staff will perform a detailed review of the provided application, and
may contact you with a request for additional information. To ensure maximum efficiency in processing
permit applications, the Division of Water Resources requests your assistance in providing a timely and
complete response to any additional information requests.
Please note. that processing standard review permit applications may take as long as 60 to 90 days
after receipt of a complete application. If you have any questions, please contact
Troy Doby at [phone] [e-mail].
Sincerely,
Nathaniel D. Thornburg, Supervisor
Division of Water Resources,
cc:rations "Section__
Permit File WQ0039924
---"`Nothing Compares.,..
State of North Carolina I Environmental Quality I Water Resources I Water Quality Permitting I Non -Discharge Permitting
1617 Mail Service Center I Raleigh, North Carolina 27699-1617
919-807-6332

BRANCH RESIDUALS & SOILS, LLC
8646 W. Market St.' Suite 111 Greensboro, NC 27409
PHONE [phone] • Fax [phone]
I
April 12, 2018
1. North Carolina Department of Environment and Natural Resources
Division of Water Resources/Aquifer Protection Section
Land Application Unit
1636 Mail Service Center
Raleigh, North Carolina 27699-1636
- _ Attention: Mr. Nathaniel Thornburg
Reference: NEW PERMIT FOR THE DISTRIBUTION OF RESIDUAL SOLIDS
von Drehle Corporation — Cordova Facility
Cordova, North Carolina
BR&S Job No. 2014-110
Dear Mr. Thornburg:
Branch Residuals & Soils, LLC is under contract with the von Drehle Corporation to prepare a new
distribution permit. von Drehle has and will continueIo operate WQ0005135:for the land, application of
Class B residual solids. Both these permits cover the same Fiber Clay residual solids: Permit WQ0005135 .
should remain active, for app lications to their current land and in case there comes.A time when Class A
' pathogen. standards can not be met. .The generated Fiber Clay has no domestic input but is derived from:
woody sources that are known to have interference with fecal coliform values (Klebsiella sp.). Based on
- the false positive interferences With the fecal coliform testing procedures, von Drehle will be performing
_ - Salmonella testing. Currently there are no labs certified to perform this test in the North Carolina. Due to
- the holding time requirement (8 hours), it will be impossible .to meet this requirement. von Drehle will
make appropriate efforts to. collect samples so that holding. time . is kept to a minimum. Distribution
avenues will include ' application in' accordance with soil- lime requirements, distribution as a soil
amendment (either alone or in concert with other products), distributed to facilities that may blend soil
amendments and mulch, and as a daily landfill cover.
Please contact me immediately if you require additional infonnation or have questions in the review of .
the permit application.
i
Since y,
G
RobertT. Branch, L. S. S.
Project Manager
cc: Mr. Cluis Fowler = von Drehle Corporation — Cordova Facility
I

EXPLANATION - , AMOUNT /�
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GREENSBORO NC 27409-9447 lot
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TABLE OF CONTENTS
Section No. Title
I DISTRIBUTION OF RESIDUAL SOLIDS APPLICATION FORM
II RESIDUALS SOURCE CERTIFICATION ATTACHMENT — FIBER CLAY
Vicinity Map
Process Flow Diagram and Narrative
Justification of Residuals Production Rate
Sampling Plan
Residual Analytical Reports
III MANAGEMENT PLAN
Overview of Process and Residual Solids Handling
Distribution Methods for Reuse
Transportation and Logistics
Monitoring and Recordkeeping
Leachate Collection
IV VON DREHLE CORDOVA FIBER CLAY
LABEL AND PRODUCT INFORMATION SHEET
V VON DREHLE CORDOVA FIBER CLAY
RESIDUALS RECEIPT FORM
VI SPILL CONTROL PLAN
VII APPLICATION RATES

SECTION I
DISTRIBUTION OF RESIDUAL SOLIDS APPLCIATION FORM

State of North Carolina
Department of Environmental Quality
Division of Water Resources
D�lAsion of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted the Applicant shall submit one original and two conies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit website
General — This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent)
residuals under 15A NCAC 02T .1100.
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Distribution of Class A Residuals (FORM: DCAR 06-16):
Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do
not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
0 The project name should be consistent on the plans, specifications, etc.
The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate
person may be designated as the signing official if.a delegation letter is provided from a person who meets the criteria in 15A
NCAC 02T .0106(b).
Q If this project is for a modification of an existing permit, submit one copy of the existing permit.
Q Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to
operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units.
B. Application Fee (New and Major Modification Application Packages)
Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental
Quality (NCDEQ).
Facility Classification
New Permit I Major Modification I
Major (residuals permitted for distribution >— 3,000 dry tons/year)
F $1,310
$395
Minor (residuals permitted for distribution < 3,000 dry tons/year) 1 $810
$245
I - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage;
adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted.
There is no fee for minor permit modifications.
C. Cover Letter (All Application Packages)
M List all items included in the application package, as well as a brief description of the requested permitting action.
RECEIVEDINCDEQIDWR
APR 16 2018
Non -Discharge
Permitting Unit
INSTRUCTIONS FOR FORM: DCAR 06-16
Page 1 of 3

D. Program Information (All Application Packages)
Provide a narrative explaining the following:
How the materials will be handled and transported from where the residuals were produced to where it will be treated.
How the residuals will be processed/treated (attach process flow diagram).
i
How leachate collection will be handled.
Where the residuals will be stored until processed.
How the final product will be distributed (packaging, bulk, etc.)
What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the
limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause
contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality.
® Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed.
Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the
person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following
information:
Name and address of the person who prepared the residual that is sold or given away.
A statement that application of the residuals to the land shall be in accordance with the instructions on the label or
information sheet.
A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered.
Z A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored
residuals into any surface waters.
Information on all applicable setbacks in accordance with 15A NCAC 02T .1108(b).
Z A statement that the residuals shall be applied at agronomic or recommended rates for intended uses.
E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units)
El Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 15A
NCAC 02T .1104(a). Specifications for standard equipment may only be omitted for municipalities with approved standard
- -1
specifications, but use of the standard specifications must be noted on each sheet of the plans.
D Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the
residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and
natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals
treatment and storage units. Depict minimum separations required in 15A NCAC 02T .1108(a) on the plans.
,] Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units:
description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity
of the finalproduct in accordance with 15A NCAC 02T .1104(a)(2)(B), including leakage and pressure testing as appropriate.
Q Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR
CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and'
specifications may be labeled with the phrase: FINAL DESIGN — NOT RELEASED FOR CONSTRUCTION.
F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units)
Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T
.1104(a).
G. Environmental Assessments (May be Required - See 15A NCAC 1C .0300)
Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include
information on any mitigating factor(s) from the Environmental Assessment. (EA) that impact the construction of the residuals
treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for
the construction of the subject facilities.
INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3

W
H. Operation and Maintenance Plan (New and Renewal Application Packages)
For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan.
Submit the O&M Plan in accordance with 15A NCAC 02T .1110 and include at a minimum:
Operational functions; describe the operation of the program to show what operations are necessary for the program to function
and by whom the functions are to be conducted.
Maintenance schedules; may include equipments calibration, maintenance of signs, etc.
Safety measures; may include safety training program, manuals, signs, etc.
Spill response plan; including control, containment, remediation, emergency contact information, etc.
Inspection plan including the following information;
Names and titles of personnel responsible for conducting the inspections.
•Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected
location(s) and inspection frequency are representative of the residuals management program.
Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event
that noncompliance is observed.
Sampling and monitoring plan including the following information;
Names and titles of personnel responsible for conducting the sampling and monitoring.
Detailed description of monitoring procedures including parameters to be monitored.
Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow,
and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling
plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet
pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual
sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected
by cold temperatures.
ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL
SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
WATER QUALITY PERMITTING SECTION
NON -DISCHARGE PERMITTING UNIT
By U.S. Postal Service:
1617 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1617
TELEPHONE NUMBER: [phone]
By Courier/Special Delivery:
512 N. SALISBURY STREET
RALEIGH, NORTH CAROLINA 27604
FAX NUMBER: [phone]
INSTRUCTIONS FOR FORM: DCAR 06-16
Page 3 of 3

J
State of North Carolina
Department of Environmental Quality
_W
ivlslon of Water Resources 15A
of Water Resources
esou�`s 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
D
FORM: DCAR 06-16
s
I. APPLICANT INFORMATION:
1. Applicant's name: Von Drehle Corporation
Applicant type: 0 Individual JZ Corporation Q General Partnership Q Privately -Owned Public Utility
[] Federal ❑ State d Municipal Q County
Signature authority's name per 15A NCAC 02T .0106: Justin Dawkins Title: 'Plant Manaeei
Applicant's mailing address: {126-First.Street
City: Co'rd6ua State: NC Zip:
Telephone number: (910) " 6-9131 Email Address: Justin dawltinsr7a vondrehle.com
2. Consultant's name: Branch Residuals'& Soils: LLC License Number (for P.E.): i . `
Affiliation: El On Staff Z Retained (Firm: ) RECF'V79. 1N00EQIDWR
Consultant's mailing address:'8646 West<Market Street-.Suilte'1:1-et
APR 1 6 2018
City: Greensboro State: NC Zip:
r_, r- - Non -Discharge
Telephone number: 336) 510-.0340 Email Address: bbrarich06ranchrs.com Permitting Unit
3. Fee submitted: K 1`31:0:00 (See Instruction B)
II. PERMIT INFORMATION:
1. Application is for (check all that apply): 0 new, Q modified, Q renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: i.
Date of most -recently issued permit:
- Date of most -recently certified Attachment A (if different than the permit):
III. FACILITY INFORMATION:
1. Name of residuals processing facility: win .Drehle"Corporation- Cordova
City: 'Cordova State: NC Zip:
Coordinates: Latitude: M- $_5' 2.'" Longitude: N.0 449' 42"
Datum: kXD'83 Level of accuracy: (1'
Method of measurement: +Ulan
County where facility is located: Richmond
2. Facility contact (person familiar with residuals preparation):
Name: Chris"fowler Title: and Apphcation ORC
Mailing address: 16 Fir 2st, Street
City::Cordova State: NC Zip: 2833S0-, .. 1
Telephone number: (9 b) 410- 19 31 E-mail address: chris:fowlernaivondrehle.c m
FORM: DCAR 06-16
Pagel of 3

Ir
3. Is the residual process facility also the generator? Yes; [] No
If No, please specify delivery frequency and quantity of residual to be processed:_i
T_ 4. Length of residuals storage at facility: 9 days (Note: the Division requires minimum 30 days storage in units that are separate
{ from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
1. Specify how these residuals will be distributed:
I '
[] sold or given away in bags or other containers; [] lawn (bulk); El home garden (bulk);
other (explain); See Attached 9yl aee nt'Plan
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
2. Complete the following if residuals are to be mixed with other materials:
Type of Materials
Amounts to be added
er 1.0 dry ton of residuals (dry ton
None
None
3. Approximate amounts of the residuals received and processed at the facility: 22:500 dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: 22.5.00 dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): Residuals are kept on small storage. load' pr-ior.to'loadmg onto trucks
6. Does the facility have a stormwater management plan?, IN Yes; El No
Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: 'Due_to %o solids;
�e.wateris riot -generated; rainwater.rewets solids.
V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
G Complete and submit the attached Residuals Source Certification and all associated documentation.
! Residuals Source
Certification
FORM: DCAR 06-16 Page 2 of 3

Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units)
attest that this application for
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package
may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed
this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
0 Yes F� No, Explain; t
I, Justin Dawkins Plant Manager
-, (Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for von Drehle Corporation — Cordova NC Facility
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this "application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature: ���717 �T/�. Date: T�
FnRNr- nrau 06-16 Page 3 of 3

0
SECTION II
RESIDUALS SOURCE CERTIFICATION ATTACHMENT - FIBER CLAY

R-.00p,
Dlvlslon of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applicant shall submit one original and two conies of the application and
supporting documentation
_ For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit
General - This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 11-15):
-� ❑ Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
_. ❑ For new or renewed permits, submit a separate certification for each source facility.
❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
❑ Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Residuals Source -Generating Facility Information:
❑ For each source facility, attach the following:
❑ Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for
_ Residuals Land Application Permits".
❑ Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated,treated, processed, and stored at the facility.
❑ Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8.
_ Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the
permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or
disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing.
❑ Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure
that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector
attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to
- be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
❑ For each source facility, attach the following:
❑ Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
❑ Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach
analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities.
INSTRUCTIONS FOR FORM: RSC 06-16
Page I of 1

L _J - - --� j �___j L _j -- � ' --- - I -- -- ) - - - ` I- - I ` - -_j — - — _ J
RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name: von Drehle Corporation, Cordova, NC facility
Status Maximum Dry Tons Per Year
Facility Permit Holder Facility Name County Permit Number
Code Current b Proposed
N Von Drehle Corporation Cordova, NC Richmond 0 16,499
a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (Le, not applicable to new facility).
SUMMARY FOR FORM: RSC 06-16 Page 1

Divlslon of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: von Drehle Corporation
2. Facility permit holder is: Q Federal, [] State, [j Local Government, or 0 Private.
Facility permit issued by: [] Div. of Water Resources, n Div. of Environmental Health,
or [] Other (explain: =.
3. Facility contact person and title: Chris Fowler, Land Application ORC
Complete mailing address: 126 First Street
City: Cordova
Telephone number: 910) 410-9131
4. Facility physical address: 126 First Street
City: Cordova State: NC
Coordinates: Latitude: 34' 55' 2.73"
State: NC Zip: 28330 --.-'
E-mail address: chris.fowler(i,vondrehle.com
Datum: NAD 83
Method of measurement: Man
Zip:28330;
Longitude: 790 49' 42.77"
Level of accuracy: 1'
FORM: RSC 06-16
5. Purpose of the facility:
[] treatment of municipal wastewater, (] treatment of 100% domestic wastewater,
[] treatment of potable water, 10 treatment of 100% industrial wastewater,
[j treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: = % industrial and = % domestic)
(] other (explain: = ).
6. Does the facility have an approved pretreatment program: 0 Yes No
7. Facility permitted/design flow: 0.395 MGD and facility average daily flow: 0.272 MGD
8. Average amount of residuals being generated at this facility 27,500 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: Separation and Belt Press
Type and volume of residuals storage (i.e., outside of residuals treatment units): Storage pad 150 cubic yArds
H. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
n 40 CFR Part 503 or JE 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
r] Biological Non -Biological
FORM: RSC 06-16 Page 1 of
i
5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: [] yes no.
If yes, list the number(s): =
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: U yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well
as those for corrosivity, ignitability, and reactivity:
Laboratory: Microbac and Date of analysis: February 7.2017
Passed corrosivity test: S yes ❑ no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: ED yes [] no. Flashpoint: Non OF (> 140°F)
Passed reactivity test: M yes ❑no. HCN: <9.98 mg/kg (<250) & H2S: <100 mg/kg (<500)
TCLP Parameter
Limit
(mgfi)
Result
(Mg/7)
TCLP Parameter
Limit
(Mg/7)
Result
(mgq)
Arsenic
5.0
<1.00
Hexachlorobenzene
0.13
<0.05
Barium
100.0
0.272
Hexachloro-1,3-Butadiene
0.5
<0.05
Benzene
0.5
<0.05
Hexachloroethade
3.0
<0.05
Cadmium
1.0
<0.10
Lead
5.0
<1.00
Carbon Tetrachloride
0.5
<0.05
Lindane
0.4
<0.0005
Chlordane
0.03
<0.01
Mercury
0.2
<0.002
Chlorobenzene
100.0
<0.05
Methoxychlor
10.0
<0.0005
Chloroform
6.0
<0.05
Methyl Ethyl Ketone
200.0
<0.05
Chromium
5.0
<0.20
Nitrobenzene
2.0
<0.05
in -Cresol
200.0
<0.05
Pentachlorophenol
100.0
<0.05
o-Cresol
200.0
<0.05
Pyridine
5.0
<0.05
p-Cresol
200.0
<0.05
Selenium
1.0
<0.50
Cresol
200.0
<0.15
Silver
5.0
<0.10
2,4-D
10.0
<0.02
Tetrachloroethylene
0.7
<0.05
1,4-Dichlorobenzene
7.5
<0.05
Toxaphene
0.5 _
<0.01
1,2-Dichloroethane
0.5
<0.05
Trichloroethylene
0.5
<0.05
1,1-Dichloroethylene
6.7
<0.05
2,4,5-Trichlorophenol
400.0
<0.05
2,4-Dinitrotoluene
0.13
<0.05
2,4,6-Trichlorophenol
2.0
<0.05
Endrin
0.02
<0.0005
2,4,5-TP (Silvex)
1.0
<0.02
Heptachlor and its Hydroxide
0.008
<0.0005
Vinyl Chloride
0.2
<0.05
FORM: RSC 06-16 Page 2 of 5

i
I
4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate
the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
- -� a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Microbac and Date of analysis: February 19, 2018
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mg1kg)
Monthly Average
Concentration Limits
(Class A Only)
(mgl'kg)
Result
(mg1kg)
Arsenic
75
41
0.0200
Cadmium
85
39
0.0010
Copper
4,300
1,500
8.0600
Lead
840
300
0.7860
Mercury
57
17
0.5500
Molybdenum
75
n/a
1.4700
Nickel
420
420
0.0010
Selenium
100
100.
0.0100
Zinc
7,500
2,800
30.1000
b. For Surface Disposal Unit (landf:'ll): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: = and Date of analysis:
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
�] > 0 but < 25
30
200
210
r] >_ 25 but < 50
34
220
240
[] >_ 50 but < 75
39
260
270
E] > 75 but < 100
46
300
320
�] >_ 100 but < 125
53
360
390
>_ 125
62
450
420
Result (mg/kg)
IFORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 45 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
- Laboratory: Microbac and Date of analysis: February 19, 2018
Parameter
Result
(mg1kg)
Aluminum
1,010.00
Ammonia -Nitrogen
77.90
Calcium
191,000.00
Magnesium
1,780.00
Nitrate -Nitrite Nitrogen
0.75
pH (Standard Unit)
7.80
Phosphorus
0.62
Potassium
69.70
Sodium
956.00
Total Kjeldahl Nitrogen
813.00
c. Using the results listed in Item 11. 5b. above, calculate the sodium adsorption ration (SAR): 0.40
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and
conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 0.40 %. This
rate is a (check one): default value, or C] actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (11') Year PAN
Five -Year
Maximum Adjusted PAN
(mg1kg)
(mgAg)
Surface
334
481
Injection/Incorporation
373
520
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: =
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
}
a. For Distribudon/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
— or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
Alternative 1 [15A NCAC 02T. 1 106(b)(3)(A)] - Time/Temperature Compliance.
❑ Alternative 2 [15A NCAC 02T. 1 106(b)(3)(B)] - Alkaline Treatment.
❑ Alternative 3 [15A NCAC 02T. 1 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 4 [15A NCAC 02T. 1 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: [] composting, ❑ heat drying, heat treatment,
j thermophilic aerobic digestion, H beta ray irradiation,
gamma ray irradiation, or n pasteurization.
b. For Land Application of Class B:
Alternative 1 [15A NCAC 02T.1106(c)(1)] -Fecal Colifoim Density Demonstration.
[] Alternative 2 [15A NCAC 02T.1106(c)(2)] -Process to Significantly Reduce Pathogens (PSRP).
Specify one: aerobic digestion, ❑ air drying, ❑ anaerobic digestion,
- ❑ composting, or ❑ lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
❑ Select One of the Class B or Equivalent PathogenReduction Alternatives in Item II. 7b. above.
[] Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)].
C] Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
❑
Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
f
I
Alternative 2 [15A NCAC 02T.1107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
[]
Alternative 3 [15A NCAC 02T.1107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
[]
Alternative 4 [15A NCAC 02T. 1 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T.1107(a)(6)] - Alkaline Stabilization.
C]
Alternative 7 [15A NCAC 02T. 1 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T.1107(a)(8)] - Drying of Unstabilized Residuals.
Alternative 9 [15A NCAC 02T.1107(a)(9)] - Injection.
Alternative 10 [15A NCAC 02T.I 107(a)(10)] - Incorporation.
❑
Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T. 1 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
-- Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur
when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

Vicinity Map

I
4_­
74
Von Drehle Corpo'ration
Ist—
ii
c
-@nch.
Gapel,earBranch�
SCALE: .1 in:= 1,500 ft- Von Drohle Corporation
Distribiltioii of Fiber, Clay' Site
I CHECKED BY: RTB-
Vicinit
Cordova, North Carolina y
DkAWN B
BRAWCA
'RTB -Map
Si '�. RESIDUALS
SOILS
LL irojici No.' 2014-:1,10
c.1
DATE: M�/201;

Process Flow Diagram and Narrative

FIBER CLAY PROCESS NARRATIVE
Recycled paper in bales is released and placed in the pulping process. There, mixed with water, the
recycled paper is reduced to pulp. The pulp is sent through a de -trashing system, where large
metals and plastics such as plastic bags or soda cans are removed. These large rejects are deposited
in an indoor pit to be removed to landfill. From here, the accepted material is sent to a holding
chest where it is fed into the pulp cleaning and screening system. The first stage of the cleaning
and screening system is responsible for the removal of dense contaminants such as glass and small
metal pieces such as staples. The next stage is the coarse screening stage which removes smaller
plastics that are slightly larger than .06 inches in diameter; these plastics, as well as the glass and
small metals, are ultimately deposited in the previously mentioned indoor pit. Following this
stage is the centrifugal forward cleaning stage. In this stage, lighter, but still relatively dense
particles, such as sand and dirt, are separated by centrifugal force from pulp and ultimately rejected
to the mill sump. The final stage of cleaning and screening is the fine screening stage.
In the fine screening stage, very small (slightly larger than. 005 inches), light contaminants s u ch
a s s t i c k i e s, ink particles and smaller dirt particles are removed and ultimately sent to the mill
sump as well. From the mill sump, these rejected solids are sent to a Krofta DAF clarifier where
they are coagulated, floated and skimmed off the surface and sent to a belt press where it is
dewatered to approximately 40% solids and deposited onto the fiber clay pad outside. The
^� accepted material from the fine screening stage is sent to a Variosplit washing system where
ti
through a dewatering process of the pulp, very fine ash and fiber fines are removed. These rejects
are sent to a Tauro DAF clarifier where they are removed in a similar fashion as with the Krofta
I and sent to the belt press to be dewatered and deposited on the fiber clay pad. Accepted pulp
from the washing stage is sent to a screw press for further dewatering, and the pulp is then fed
into a high temperature dispersion system, where any remaining small contaminants such as dirt
and stickies are pulverized to a size smaller than what can be seen with the human eye.
The pulp is also mixed with a bleaching agent at high temperature and is sent to a bleaching tower
to allow the bleaching process to take place and increase pulp brightness. The pulp is then mixed
with water and diluted to 5% solids and sent to the paper machines. At the paper machines, the
pulp is applied to a press felt, while simultaneously being dewatered with a poly wire belt; a
sheet of paper is formed, which is pressed, dried and rolled up to be shipped. In this process, more
ash and fines are removed and are ultimately sent to a Megacell DAF clarifier where, as with the
other DAF units, a fiber clay blanket is formed, sent to the belt press and then the fiber clay pad.

von Drehle Paper Process Flowchart
Bails inPulper
Dump accepts Detrasher
Tank Scavenger
accepts rejects
Screen
Greene
'eed Tank
accepts
HD
rejects
Cleaner
accepts
Coarse re, cts
Screen
[rejects
accepts
entrifuaall rejects _1 Mill
Cleaners
#accep,.5
✓anospu
rejects
Tauro
Washer
DAF
accepts
accepts
Screw
rejects
H2O to
Press
WW Ches
accepts
Bleach
Tower
Water
IDrum I
Screen
Tailings
Pit
accepts
Krofta
DAF
accepts
Water to
City or
return to Process
4DAF
Landfill
Sludge rejects Land App
Press or
Landfill
T
Product

The water from each of these DAF units is generally re -used in the process, with the excess being
discharged to the City of Rockingham wastewater treatment system.
Following is the process flow schematic diagram for the water and solids in von Drehle Corporation
Cordova's Paper Process.

Justification of Residuals Production Rate

JUSTIFICATION OF RESIDUALS PRODUCTION RATE
von Drehle Corporation produces approximately 27,500 dry.tons of the Fiber Clay annually. Since
a portion of this will be sent to permit WQ0005135 and a portion will be covered under this permit,
it will not be necessary to have the total production listed under either these permits. von Drehle will
also request application of this residual in South Carolina. von Drehle requests the limit be set at
16,499 dry tons.

Sampling Plan

J
FIBER CLAY SAMPLING PLAN
von Drehle Fiber Clay is transported by conveyor from the belt presses to the storage pad in the back
at von Drehle's facility in Cordova. Fiber Clay will be distributed by placement onto sealed trailers that
will be routed to one of several marketing sites, non-specific receiver sites or to the landfill as daily
cover.
Based on the amount of residual to be distributed, von Drehle Fiber Clay will be sampled bi-monthly
from the belt presses. Representative samples of von Drehle Fiber Clay will be collected and
composited prior to the beginning of the preceding bi-monthly cycle so that data will be made available
prior to that distribution period. Seven independent grab samples will be collected for Salmonella or
fecal analysis. These samples will be immediately placed on ice and delivered to a lab certified in the
testing protocol. Since there are no labs that are certified for the state of North Carolina for the
Salmonella testing, at.a minimum this lab has certification such as Nation Environmental Laboratory
Accreditation Conference (NELAC). If at an any point, North Carolina has a lab that becomes
accredited and is close enough to meet the necessary hold times, they will be used. All samples will be
sent to qualified laboratories that are familiar with the environmental sample preparation and standards
required. Annually, a residuals solid sample will be analyzed for toxicity characteristics leaching
procedure (TCLP). TCLP parameters are listed below:
Arsenic
Cadmium .
Chlorobenzene
o-Cresol
Cresol
1,2-Dichloroethane
Endrin
Hexachloroethane
Lindane
Methyl ethyl ketone
Pyridine
Tetrachloroethylene
2,4, 5 -Trichlorophenol
Vinyl chloride
Barium
Benzene
Carbon tetrachloride
Chlordane
Chloroform
Chromium
m-Cresol
p-Cresol
2, 4-D
1,4-Dichlorobenzene
1,1-Dichloroethylene
2,4-Dinitrotoluene
Hexacblorobenzene
Heptachlor (and its hydroxide)
Lead
Hexachloro-1,3-butadiene
Mercury
Methoxychlor
Nitrobenzene
Pentachlorophenol
Selenium
Silver
Toxaphene
Trichloroethylene
2,4,6-Trichlorophenol
2,4,5-TP (Silvex)

Bi-monthly (once every two months, prior to the end of the preceding two month period,) a composite
Fiber Clay residual solid sample will be collected and analyzed for: Cadmium, Copper, Lead, Nickel,
i Zinc, Aluminum, Ammonia — Nitrogen, Nitrate -Nitrite, Nitrogen, % Total Solids, pH, Phosphorus,
Potassium, TKN, and Calcium Carbonate Equivalency (CCE). From this information, the Plant
Available Nitrogen (PAN) and Agricultural Lime Equivalency (ALE) will be calculated. This will
be the basis for the application rates that will be used in the next monitoring period and changes will
be made to the product label to reflect the most recent analytical data.

Residual Analytical Reports

nC BIOLOGICAL CONSULTING SERVICES
OF NORTH FLORIDA, INC.
July 24, 2014
Mr. Robert Branch
Branch Residuals and Soils
8646 W. Market St.
Suite 111
Greensboro, NC 27409
RE: Salmonella spp. and Fecal Coliform analysis final report for samples 1, 2, 3, 4, 5,
and 6; BCS IDs: 1407216-221. Project ID: VonDrehle 2014-10.
Dear Mr. Branch;
We have completed the Salmonella spp. and Fecal Coliform analysis on the samples
that were received at our laboratory on July 16, 2014, The samples were analyzed for
the presence of Salmonella spp. as per EPA 1682. The samples were also analyzed for
Fecal Coliform as per EPA1681. The method is the EPA equivalent of Standard Method
9221 E (APHA, 2012) for the analysis of biosolids for fecal coliforms. ,
Following, you will find our report on the results of the analysis. Should you have any
questions, please do not hesitate to contact me.
Sincerely;
c
George Lukasik, Ph.D.
Laboratory Director
PAGE 1 OF 4
BCS LABORATORIES - GAINESVILLE
4609 NW 6TH STREET, BLDG A, GAINESVILLE, FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH LABORATORY #E82924, EPA# FLO 1 147
FILE: BRANCH RESIDUALS AND SOILS 07 15 2014 BCS 1407216-221.DOCX
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
O �N ACCC9O
�s

Client:
Project:
Ahalwsis Parameter;
Receipt Date/Time:
Analysis Minimum Detection Limit:
Practical Quantification Limit:
Branch Residuals and Soils
Von Drehle 2014-10
July 16, 201_4 @ 11.30; 7.61 C
1.0 mpn (cfu) / weight analyzed
1.0 mpn.(cfu) / weight analyzed
Salmonella Most
Probable Number/ 4
Data
Sample ID
Sampling
Analysis Start
Analysis Stop
Dry Weight
Analysis
BCS Sample #
Date/Time
Date/Time
Date/Time
(%)
Results / ml
grams dry weight
Qualifier*
1
07/15/2014
07/16/2014
07/19/2014
40.5%
0.07
0.69
Q
BCS #1407216
10:25
12:24
14:00
2
07/15/2014
07/16/2014
07/19/2014
o
45.0 /o
None Detected
None Detected
U' Q
BCS #1407217
10:29
12:46
14:00
<0.06
<0.6
3 ,
07/15/2014
07/16/2014
07/19/2014
o
43.5 /o
None Detected
None Detected
U' Q
BCS #1407218
10:42
12:56
14:00
<0.06
<0.6
4
07/15/2014
07/16/2014
07/22/2014
44.7%
0.07
0.64
Q
BCS #1407219
10:45
13:13
13:30
5
07/15/2014
07/16/2014
07/19/2014
o
49'2 /0
None Detected
None Detected
U' Q
BCS #1407220
10:51
13:27
14:00
<0.06
<0.5
6
07/15/2014
07/16/2014
07/19/2014
49 6%
None Detected
None Detected
U, Q
BCS #1407221
10:55
13:32
14:00
<0.06
<0.5
*Data Qualifier:' ;indicates_thatahe_anal-yte_was_analyzed-for but not detected at the indicated_limii of detection I; indicates that the reported value is between the
laboratory method detection limits and the laboratory practical quantitation limit. L; indicates Off -scale high -actual value know to be greater than value given, and ,C2
• i_ndi.cates_that_the sample_was_held_beyondhe_stan a�dindicated holding time of 24 hours.�
PAGE 2 OF 4
BCS LABORATORIES - GAINESVILLE
4609 NW 6TH STREET, BLDG A, GAINESVILLE, FLORIDA 32609
TEL.. [phone], Fax. [phone]
WWW.MICRO BIOSERVICES:COM
FL DOH LABORATORY #E82924, EPA# FLO 1 147
FILE: BRANCH RESIDUALS AND SOILS 07 15 2014 BCS 1407216-221.DOCX
THIS REPORT SHALL NOT SE 'REPRODUCED. EXCEPT IN FULL. WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
10 ACCp17
O�
tiO
�. x

Client:
Project:
Ana y_sic Paramete
Receipt Date/Time:
Analysis Minimum Detection Limit:
Practical Quantification Limit:
Branch Residuals and Soils
Von Drehle 2014-10
(EP
(Fecal Coli rm (FCj in Bid- — lids; EPA 1681 i4/625/R92/0:13)`TSNT9v221E
July 16, 2014 @ 11:30; 7.60 C
-1.0 mpn (cfu) / weight analyzed
1.0 mpn (cfu) / weight analyzed
FC MPN / gram
Data
Sample ID
Sampling
Analysis Start
Analysis Stop
Dry Weight
FC MPN/ml
BCS Sample #
Date/Time
Date/Time
Date/Time
(oho)
dry weight
Qualifier*
1
07/15/2014
07/16/2014
07/17/2014
40.5%
5,422
1.3 x 104
Q
BCS #1407216
10:25
12:24
13:30
2
07/15/2014
07/16/2014
07/17/2014
45.0%
2,398
5.3 x 103
Q
BCS #1407217
10:29
12:46
13:30
3
07/15/2014
07/16/2014
07/17/2014
43.5%
5,422
1.2 x 104
Q
BCS #1407218
10:42
12:56
13:30
4 •
07/15/2014
07/16/2014
07/17/2014
44.7%
2,781
6.2 x 103
Q
BCS #1407219
10:45
13:13
13:30
5
07/15/2014
07/16/2014
07/17/2014
49.2%
239,800
4.9 x 105
Q
BCS #1407220
10:51
13:27
13:30
1
6
07/15/2014
07/16/2014
07/17/2014
49.6%
221,200
4.5 x 105
Q
BCS #1407221
10:55
13:32
13:30
* Data Qualifier: U; indicates that the •analyte was analyzed for but not detected at the indicated limit of detection. I; indicates that the reported value is between the
laboratory method detection limits and the laboratory_ practical quantitation limit. L; indicates Off -scale high -actual value know to be greater than value given, and
indicates_that_the_sample_was_held.beyond_the_standard iindicated holding time of 24 hours.
PAGE 3OF4
BCS LABORATORIES - GAINESVILLE
4609 NW 6TH STREET, BLDG A, GAINESVILLE, F.LORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH LABORATORY #E82924, EPA# FLO 1 147
FILE: BRANCH RESIDUALS AND SOILS 07 15 2014 BCS 1407216-221.DOCX
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUTTHE WRITTEN CONSENT OF BCS LABORATORIES
,p ACCOq

Client:
Project:
Analysis Parameter:
Receipt Date/Time:
Branch Residuals and Soils
Von Drehle 2014-10
Salmonella in Biosolids; Method EPA 1682 (EPA/625/R92/013)
Fecal Coliform in Biosolids; EPA 1681 (EPA/625/R92/013) / SM 95221 E
July 16, 2014 @ 11:30; 7.61 C .
I certify that I have personally examined and am familiar with the, information submitted herein. Based on my inquiry of those
individuals immediately responsible for obtaining the information, I believe the submitted information is true, accurate, and
complete. The above results relate only the collected and referenced sample(s) and to their condition at the time of process.
The analysis results are not indicative or representative of a process. Sampling and field data information was submitted by the
client. The analysis and presented results in this report meet the requirements of The NELAC Institute (TNI), ISO 17025, and
the State of Florida Department of Public Health's Laboratory Certification Program, as applicable unless otherwise noted.
c
Signature of Laboratory Director/Authorized Rep
Date:
July 24, 2014
PAGE 4 OF 4
BCS LABORATORIES - GAINESVILLE
4609 NW 6TH STREET, BLDG A, GAINESVILLE, FLORIDA.32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH LABORATORY #E82924, EPA# FLO 1 147
FILE: BRANCH RESIDUALS AND SOILS 07 15 2014 BCS 1407216-221.DOCX
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUTTHE WRITTEN CONSENT OF BCS LABORATORIES
- S�� �N-ACCp9�qY
f

G Inc. BIOLOGICAL CONSULTING SERVICES
OF NORTH FLORIDA, INC.
{
July 13, 2017
Robert Branch
Branch Residuals and Soils
8646 W. Market St. Suite 111
Greensboro NC 27409
336-510-0340
[e-mail]
Client ID: VD-1, VD-2, VD-3, VD-4, VD-5, VD-6, VD-7
BCS ID: 1707029, 1707030, 1707031, 1707032, 1707033, 1707034, 1707035
Dear Robert Branch,
We have completed the analysis of the submitted samples as outlined below.
Project Name: N/A
Analysis Method
Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited)
Following, you will find our report on the results of the analysis conducted on the referenced samples.
Should you have any questions, please do not hesitate to contact me.
Sincerely, ��JJ
r Bonnie Mull, MPH
Laboratory Operations Manager
Page 1 of 8
Final Report BCS ID 1707029,1707030, 1707031, 1707032, 1707033, 1707034, 1707035
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
LABORATORY
���c0 ACCREDITATION
`�' BUREAU mo+.d.
n ACCREDITEDesonm7*2e is

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: N/A
Client Sample ID: VD-1
Sample Date/Time: July 06, 2017 14:40
BCS Sample ID: 1707029 Sample Description: Soil
Date Received: July 07, 2017 10:05 Amount Submitted:250ml bottle % Solids: 41.4
Amount Analyzed: 30.00 g Receipt Temperature: 6.8 deg C Preserved: Yes
Analysis Start: July 07, 2017 14:15 Analysis Stop Date: July 13, 2017 12:58
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 150.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
- I
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: N/A
Client Sample ID: VD-2 Sample Date/Time: July 06, 2017 14:41
BCS Sample ID: 1707030 Sample Description: Soil
Date Received: July 07, 2017 10:05 Amount Submitted:250ml bottle % Solids: 38.4
Amount Analyzed: 30.00 g Receipt Temperature: 6.8 deg C Preserved: Yes
Analysis Start: July 07, 2017 14:15 Analysis Stop Date: July 13, 2017 12:58
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 2 of 8
Final Report BCS ID 1707029, 1707030, 1707031, 1707032, 1707033, 1707034, 1707035
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
rl! I LABORATORY
PDO
ACCREDITATION
BUREAU
�`. ACCREDITEDnoozcl—' -/

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: N/A
Client Sample ID: VD-3
Sample Date/Time: July 06, 2017 14:44
BCS Sample ID: 1707031 Sample Description: Soil
Date Received: July 07, 2017 10:05 Amount Submitted:250ml bottle % Solids: 41.0
Amount Analyzed: 30.00 g Receipt Temperature: 6.8 deg C Preserved: Yes
Analysis Start: July 07, 2017 14:15 Analysis Stop Date: July 13, 2017' 12:58
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 150.6 Salmonella MPN/4 dry grams
4nalysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: N/A
Client Sample ID: VD-4
Sample Date/Time: July 06, 2017 14:46
BCS Sample ID: 1707032 Sample Description: Soil
Date Received: July 07, 2017 10:05 Amount Submitted:250ml bottle % Solids: 37.2
Amount Analyzed: 30.00 g Receipt Temperature: 6.8 deg C Preserved: Yes
Analysis Start: July 07, 2017 14:15 Analysis Stop Date: July 13, 2017 12:58
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
4nalysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting unit.
Page 3 of 8
Final Report BCS ID 1707029, 1707030, 1707031, 1707032, 1707033, 1707034, 1707035
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
00 LABORATORY
ACCREDITATION
BUREAU .a.wew J
ACCREDITEDrsonim I

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: N/A
Client Sample ID: VD-5
Sample Date/Time: July06, 2017 14:53
BCS Sample ID: 1707033 Sample Description: Soil
Date Received: July 07, 2017 10:05 Amount Submitted:250ml bottle % Solids: 43.7
Amount Analyzed: 30.00 g Receipt Temperature: 6.8 deg C Preserved: Yes
Analysis Start: July 07, 2017 14:15 Analysis Stop Date: July 13, 2017 12:58
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: .50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: N/A
Client Sample ID: VD-6
Sample Date/Time: July 06, 2017 14:56
BCS Sample ID: 1707034 Sample Description: Soil
Date Received: July 07, 2017 10:05 Amount Submitted:250ml bottle % Solids: 40.5
Amount Analyzed: 30.00 g Receipt Temperature: . 6.8 deg C Preserved: Yes
Analysis Start: July 07, 2017 14:15 Analysis Stop Date: July 13, 2017 12:58
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: 150.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
4nalysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting unit!
Page 4 of 8
Final Report BCS ID 1707029,1707030, 1707031, 1707032, 1707033, 1707034, 1707035
BCS LABORATORIES, INC. -- GAINESVIL.LE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 6&03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
�""'""�• LABORATORY
ACCREDITATION
BUREAU
ACCREDf7EDisonicno:
_ S Ii^"a

Client: Branch Residuals and Soils
_ Analysis: Salmonella
Project Name: N/A
Client Sample ID: VD-7 Sample Date/Time: July 06, 2017 14:54
BCS Sample ID: 1707035 Sample Description: Soil
Date Received: July 07, 2017 10:05 Amount Submitted:250ml bottle % Solids: 41.2
Amount Analyzed: 30.00 g Receipt Temperature: 6.8 deg C' Preserved: Yes
Analysis Start: July 07, 2017 14:15 Analysis Stop Date: July 13, 2017 12:58
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as perthe method's standard reporting units
Page 5 of 8
Final Report BCS ID 1707029, 1707030, 1707031, 1707032,1707033, 1707034, 1707035
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
LABORATORY
ACCREDITATION
�fcls BUREAU a a...
rn1; ACCREDITEDrsonrcnoz

Client: Branch Residuals and Soils
Project: N/A
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes:
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Page 6 of 8
Final Report BCS ID 1707029, 1707030, 1707031, 1707032,1707033, 1707034, 1707035
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
f TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 6&03950, EPA# FLO 1 147
_ THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
�'"'"' %• LABORATORY
J4 1' ACCREDITATION
BUREAUaJ
ACCREDITEDamic»oe

I certify that I have examined I am familiar with the information submitted herein. The results pertain only to
analyzed sample(s) associated identifier #(s). Based on my inquiry of the individuals responsible for the
analysis, I believe the data to be true, accurate, complete. Sampling field data was obtained from submitted
documents. The analysis was authorized commissioned by the client. The resulting data are representative of
the analysis conducted on the material/samples/articles provided by the client (or client's representative)
it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate
method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS
Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any
sample, batch, source, or the process they are derived from. Quality assurance controls were performed as
outlined in the method and as per Good Laboratory Practices. The analysis results presented in this report
meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH
Environmental Laboratory Certification Program, as applicable unless otherwise noted.
o��]
Signature of Laboratory Director/Authorized Rep. Date.. July 13, 2017
Page 7 of 8
Final Report BCS ID 1707029, 1707030, 1707031, 1707032, 1707033, 1707034, 1707035
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 6&03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN -CONSENT OF BCS LABORATORIES
LABORATORY
LaACCREDITATION
BUREAU a�a...
"'•;� ACCREDITEDrsonreneze 7

DATA QUALIFIER CODES
SYMBOL MEANING _
_B I Results based on counts outside the acceptable range
Sample received without prior notification or delayed delivery. Analysis performed outside of
?associated method required QC data set (1 QC data set per 20 samples per 168 hours). _
I _ Value. is between the laboratory method detection limit & laboratory practical quantitation limit_
J1 The sample matrix Interfered with the ability to make any accurate determination. T
J2 i No Quality Control- criteria exist for the component.
J3_ ;The data are questionable because of improper laboratory or field protocols.
JL f Off scale high. Actual value is known to be greater than value given_ _ _... ---- ---- -
i Presumptive evidence for the presence of material. There is an indication that the analyte is present, j
N Ibut the confirmation requirement was not met. i
0 _ iSampled, but analysis not performed. —
Q -Sample held beyond the accepted- holding time.
Indicates that the compound was analyzed for but not detected. The specified component was not
U ;!detected. The reported value is the method detection limit.
V ;Analyte was detected in both sample and associated method blank. Data may not be accurate. ;
Y ,The laboratory analysis was from an improperly preserved sample. The data may not be accurate.
iToo many colonies present (TNTC)• the numeric value given represents the upper end of the value that i
Z I
can be determined based on the volume.
7 ;Data .are rejected and should not be used. QC data for analyte did not meet acceptance criteria. }
Presence or absence of analyte could not be confirmed. l
** : Not reported due to interference.
A I BCS d n is not currently accredited for this analyte. —_
..._. -- _ _ ___._..__
# _ ;BCS Lab specific qualifier. See laboratory analysis
Page 8 of 8
Final Report BCS ID 1707029, 1707030, 1707031, 1707032, 1707033, 1707034, 1707035
BCS LABORATORIES, INC. — GAINESVI.LLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
LABORATORY
��. ACCREDITATION i
,ram, BUREAU
.^ ACCREDITEDwmcno�
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CHAIN OF CUSTODY'.RECORD
BCB Laboratories
www.microbioservir.es.com 4609 NW 6th street, Building A'
FL DOH Laboratory #E82924, EPA# FL01147'" Gainesville, FL 32609
Tel. [phone], Fax. [phone]
Client Name and Address:
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Project Manager; Facility/Site: Cow,(
Telephone Number: 334, 9M,16-a3 40 faxNo.: Report7o:�-
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inc. BIOLOGICAL CONSULTING SERVICES
OF NORTH FLORIDA, INC.
August 29, 2017
Robert Branch
Branch Residuals and Soils
8646 W. Market St. Suite 111
Greensboro NC 27409
336-510-0340
[e-mail]
Client ID: VD-1, VD-2, VD-3, VDA, VD-5, VD-6, VD-7
BCS ID: 1708221, 1708222, 1708223, 1708224, 1708225, 1708226, 1708227
Dear Robert Branch,
We have completed the analysis of the submitted samples as outlined below.
Project Name: 2014-110
Anal sis IMethod
Salmonella JEPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited)
Following, you will find our report on the results of the analysis conducted on the referenced samples.
Should you have any questions, please do not hesitate to contact me.
Sincerely,
Bonnie Mull, MPH
Laboratory Operations Manager
Page 1 of 8
Final Report BCS ID 1708221,1708222, 1708223, 1708224, 1708225, 1708226, 1708227
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
LABORATORY
ACCREDITATION
BUREAU aM bnWMH
'„ ' Q ACCREDITED.,

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: VD-1
Sample Date/Time: August 23, 2017 13:42
BCS Sample ID: 1708221 Sample Description: Biosolids
Date Received: August 24, 2017 9:45 Amount Submitted:250 mL bottle % Solids: 43.2
Amount Analyzed: 30.00 g Receipt Temperature: 2.5 deg C Preserved: Yes
Analysis Start: August 24, 2017 10:30 Analysis Stop Date: August 29, 2017 11:40
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: VD-2 Sample Date/Time: August 23, 2017 13:44
BCS Sample ID: 1708222 Sample Description: Biosolids
Date Received: August 24, 2017 9:45 Amount Submitted:250 mL bottle % Solids: 39.8
Amount Analyzed: 30.00 g Receipt Temperature: 2.5 deg C Preserved: Yes
Analysis Start: August 24, 2017 10:30 Analysis Stop Date: August 29, 2017 11:40
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 150.7- Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting unit
- Page 2 of 8
Final Report BCS ID 1708221, 1708222, 1708223, 1708224, 1708225, 1708226, 1708227
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
LABORATORY
ACCREDITATION
BUREAU .« J
ACCREDITEDeswrcim

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: VD-3 Sample Date/Time: August 23, 2017 13:40
BCS Sample ID: '1708223 Sample Description: Biosolids
Date Received: August 24, 2017 9:45 Amount Submitted:250 mL bottle % Solids: 39.4
Amount Analyzed: 30.00 g Receipt Temperature: 2.5 deg C Preserved: Yes
Analysis Start: August 24, 2017 10:30 Analysis Stop Date: August 26, 2017 9:02
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: :90.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: VD-4 Sample Date/Time: August 23, 2017 13:47
BCS Sample ID: 1708224 Sample Description: Biosolids
Date Received: August 24, 2017 9:45 Amount Submitted:250 mL bottle % Solids: 41.7
Amount Analyzed: 30.00 g Receipt Temperature: 2.5 deg C Preserved: Yes
Analysis Start: August 24, 2017 10:30 Analysis Stop Date: August 29, 2017 11:40
Analyst: Wei -yea Hsu, M.S. - Qualifier: U
Primary Value: <_0.07 Salmonella MPN/ml-sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 3 of 8
Final Report BCS ID 1708221, 1708222, 1708223, 1708224, 1708225, 1708226, 1708227
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN_ CONSENT OF BCS LABORATORIES
,'' " LABORATORY
ACCREDITATION
�—� BUREAU
•tia`'�° -,^ n ACCRED1TED"ECI M
I :

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: VD-5
Sample Date/Time: August 23, 2017 13:49
BCS Sample ID: 1708225 Sample Description: Biosolids
Date Received: August 24, 2017 9:45 Amount Submitted:250 mL bottle % Solids: 34.5
Amount Analyzed: 30.00 g Receipt Temperature: 2.5 deg C Preserved: Yes
Analysis Start: August 24, 2017 10:30 Analysis Stop Date: August 29, 2017 11:40
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.8 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's .
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: 2014-110
Client Sample ID: VD-6
Sample Date/Time: August 23, 2017 13:35
BCS Sample ID: 1708226 Sample Description: Biosolids
Date Received: August 24, 2017 9:45 Amount Submitted:250 mL bottle % Solids: 40.1
Amount Analyzed: 30.00 g Receipt Temperature: 2.5 deg C Preserved: Yes
Analysis Start: August 24, 2017 10:30 Analysis Stop Date: August 29, 2017 11:40
Analyst: Wei -yea Hsu, M.S. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.6 Salmonella MPN/4 dry grams
4nalysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 4 of 8
^ Final Report BCS ID 1708221, 1708222, 1708223, 1708224, 1708225, 17 08226,1708227
BCS LABORATORIES, INC. -- GAINESVILLE .
i 4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
Il TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
LABORATORY
ACCREDITATION
BUREAU »a•.•
% � ` ACCREDITEDwmcvP2.

Client: Branch Residuals and Soils
Analysis: Salmonella
P-roject Name: 2014-110
Client Sample ID: VD-7 Sample Date/Time: August 23, 2017 13:53
BCS Sample ID: 1708227 Sample Description: Biosolids
Date Received: August 24, 2017 9:45 Amount Submitted:250 mL bottle % Solids: 38.7
Amount Analyzed: 30.00 g Receipt Temperature: 2.5 deg C Preserved: Yes
Analysis Start: August 24, 2017 10:30 Analysis Stop Date: August 29, 2017 11:40
Analyst: Wei -yea Hsu, M.S. Qualifier: U
�. Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes:. Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 5 of 8
') ! Final Report BCS ID 1708221, 1708222, 1708223, 1708224, 1708225, 1708226, 1708227
_ BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 6&03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
LABORATORY
ACCREDITATION
�+[D
BUREAUaJr�ACCREDITEDtsonccvu.,
^�

ti
i
Client: Branch Residuals and Soils
Project: 2014-110
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
- Report Notes: Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
-1
Page 6 of 8
Final Report BCS ID 1708221, 1708222, 1708223, 1708224, 1708225, 1708226, 1708227
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
LABORATORY
ACCREDITATION
t BUREAU .aJ
'-/ n ACCRED1TEDwici !

I certify that I have examined I am familiar with the information submitted herein. The results pertain only to
analyzed sample(s) associated identifier #(s). Based on my inquiry of the individuals responsible for the
analysis, I believe the data to be true, accurate, complete. Sampling field data was obtained from submitted
documents. The analysis was authorized commissioned by the client. The resulting data are representative of
l the analysis conducted on the material/samples/articles provided by the client (or client's representative)
it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate
I
method, however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS
Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any
sample, batch, source, or the process they are derived from. Quality assurance controls were performed as
outlined in the method and as per Good Laboratory Practices. The analysis results presented in this report
meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DQH
Environmental Laboratory Certification Program, as applicable unless otherwise noted.
Signature of Laboratory Director/Authorized Rep.
Date.
. August ust 29, 2017
Page 7 of 8
Final Report BCS ID 1708221,1708222, 1708223, 1708224, 1708225, 1708226, 1708227
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTENCONSENT OF BCS LABORATORIES
LABORATORY
ACCREDITATION
BUREAU
ACCRED1TEDnoerc»0:: _
> w•r„i.a,a"

DATA QUALIFIER CODES
SYMBOL
_
MEANING
B
Results based on counts outside the acceptable range.
Sample received without prior notification or delayed delivery. Analysis performed outside of
X
_
associated method required QC data set (1 QC data set per 20 samples per 168 hours)_
I
Value is between the laboratory method detection limit & laboratory practical quantitation limit.
J1
,The sample matrix interfered with the ability to make any accurate determination.
'No Quality Control criteria exist for the component__
J_2_ —
13
The data are questionable because of improper laboratory or field protocols.
L
Y1
Off scale high. Actual value is known to be greater than value given.
Presumptive evidence for the presence of material. There is an indication that the analyte is present,
N I
but the confirmation requirement was not met.
0 ISampled, but analysis not performed.
Q 'Sample held beyond the accepted holding time.
II Indicates that the compound was analyzed for but not detected. The specified component was not
detected. The reported value is the method detection limit_
V ;Analyte was detected in both sample and associated method blank. Data may not be accurate
Y !The laboratory analysis was from an improperly preserved sample_ The data may not be accurate. I
;Too many colonies present (TNTC); the numeric value given represents the upper end of the value that
Z
i can be determined based on the volume.
7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria.
— _ ? Presence or absence of analyte could not be confirmed.
**
Not reported due to interference.
I BCS is not currently accredited for this analyte.
_A
#_ BCS Lab specific qualifier. See laboratory analysis notes.
Page 8 of 8
? Final Report BCS ID 1708221, 1708222, 1708223, 1708224,1708225, 1108226,1708227
t
BCS LABORATORIES, INC. -- GAINE:SVILLE
4609 NW 6TH STREET.-STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# FLO 1 147
') THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
II" - LABORATORY
ACCREDITATION
BUREAU
: - z ACCREDITEDimk??0215

CHAIN OF CUSTODY RECORD BCS 'Laboratories
www.microbioservices.com 4609 NW 6th Street, Building A
FL DOH Laboratory#E82924, EPA#FL01147 Gainesville, FL 32609
( �11 Tel. [phone], Fax. [phone]
Client Name and Address: �;ZA va,� 1<e6.'J,J5 S S�; `5 44-s���k, �j� �r7'° I Compliance Monitoring? Yes❑ No
City/State2ip: G2e-c.t5 �na;- A(C Z _7gD 9 Report To: Sj(-.e
Project Manager: Qo h,.v - &A", Email: h b O-A. off. (2 6 erA,,,iC�-
Telephone Number: Fax No.: 33& 5-10-0341 Quote #:
Sampler Name: (Print) Project ID: ZDJC(-ilk
Sampler Signature: , Invoice To: Sr4
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08/24/2017 9:45
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I
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UPS
Postal
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Date
Time
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ywwobsfA-t. Ptzta E11VT
< ,

Inc. BIOLOGICAL CONSULTING SERVICES
OF NORTH FLORIDA, INC.
December 19, 2017
Robert Branch
Branch Residuals and Soils.
8646 W..Market St. Suite 111
Greensboro NC 27409
336-510-0340
[e-mail]
Client ID: VD-1, VD-2, VD-3, VD-4, VD-5, VD-6, VD-7
BCS ID: 1712079, 1712080, 1712081, 1712082, 1712083, 1712084, 1712085
Dear Robert Branch,
We have completed the analysis of the submitted samples as outlined below.
Project Name: Cordova NA
Anal sis _ Method
Salmonella JEPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited)
Following, you will find our report on the results of the analysis conducted on the referenced samples.
Should you have any questions, please do not hesitate to contact me.
Sincerely, �J
Bonnie Mull, MPH
Laboratory Operations Manager
Page l of.8
Final Report BCS ID 1712079, 1712080, 1712081, 1712082, 1712083, 1712084, 1712085
l
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], I'Ax. [phone]
WWW.MICROBIOSERVICES.COM
_ FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# F'L.O 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
LABORATORY '
ACCREDITATION _
BUREAUd J
ACCREDITEDRwnacnoz:

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova NA
Client Sample ID: VD-1
Sample Date/Time: December 11, 2017 14:05
BCS Sample ID: 1712079 Sample Description: Biosolids
Date Received: December 12, 2017 10:40 Amount Submitted:100ml bottle % Solids: 34.8
Amount Analyzed: 30.10 g Receipt Temperature: 1.9 deg C Preserved: Yes
Analysis Start: December 12, 2017 11:10 Analysis Stop Date: December 15, 2017 9:55
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova NA
Client Sample ID: VD-2
Sample Date/Time: December 11, 2017 14:07
BCS Sample ID: 1712080 Sample Description: Biosolids
Date Received: December 12, 2017 10:40 Amount Submitted:100ml bottle % Solids: 34.5
Amount Analyzed: 30.08 g Receipt Temperature: 1.9 deg C Preserved: Yes
Analysis Start: December 12,. 2017 11:10 Analysis Stop Date: December 15, 2017 9:55
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: 50.07 Salmonella MPN/mL sample analyzed
Secondary Value: :50.8 Salmonella MPN/4 dry grams
4nalysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
l
i
Page 2 of 8
Final Report BCS ID 1712079, 1712080, 1712081, 1712082, 1712083, 1712084, 1712085
i
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
_ FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# FLO 1 147
~� THIS REPORT SHALL NOT BE REPRODUCED; EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
LABORATORY
_ I BUREEAUITATION
�00
,��, ACCREDI7EDismic �,

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova NA
Client Sample ID: VD-3
Sample Date/Time: December 11, 2017 14:10
BCS Sample ID: 1712081 Sample Description: Biosolids
Date Received: December 12, 2017 10:40 Amount Submitted:100ml bottle % Solids: 37.4
Amount Analyzed: 30.07 g Receipt Temperature: 1.9 deg C Preserved: Yes
Analysis Start: December 12, 2017 11:10 Analysis Stop Date: December 15, 2017 9:55
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: <_0.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova NA
Client Sample ID: VD-4 Sample Date/Time: December 11, 2017 14:12
BCS Sample ID: 1712082 Sample Description: Biosolids
Date Received: December 12, 2017 10:40 Amount Submitted:100ml bottle % Solids: 36.5
Amount Analyzed: 30.09 g Receipt Temperature: 1.9 deg C Preserved: Yes
Analysis Start: December 12, 2017 11 10 Analysis Stop Date: December 15, 2017 9:55
Analyst: Greta Pallack, B.A. Qualifier:, U
Primary Value: 50.07 Salmonella MPN/ml- sample analyzed
Secondary Value: :50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting unit:
Page 3 of 8
Final Report BCS ID 1712079, 1712080, 1712081, 1712082, 1712083, 1712084, 1712085
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
LABORATORY ov
ACCREDITATION
BUREAU;4, ACCREDITEDnoncJ7021

Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: - Cordova NA
Client Sample ID: VD-5
Sample Date/Time: December 11, 2017, 14:14
BCS Sample ID: 1712083 Sample Description: Biosolids
Date Received: December 12, 2017 10:40 Amount Submitted:100mi bottle % Solids: 36.7
Amount Analyzed: 30.10 g Receipt Temperature: 1.9 deg C Preserved: Yes
Analysis Start: December 12, 2017 11:10 Analysis Stop Date: December 19, 2017 15:30
Analyst: Greta Pallack, B.A. Qualifier: None
Primary Value: 0.21 Salmonella MPN/mL sample analyzed
Secondary Value: 2.3 Salmonella MPN/4 dry.grams
Analysis Notes: None
Client: Branch Residuals and Soils
Analysis: Salmonella
Project Name: Cordova NA
r Client Sample ID: VD-6 Sample Date/Time: December 11, 2017 14:16
BCS Sample ID: 1712084 Sample Description: Biosolids
Date Received: December 12, 2017 10:40 Amount Submitted:100ml bottle % Solids: 36.4
Amount Analyzed: 30.10 g Receipt Temperature: 1.9 deg C Preserved: Yes
Analysis Start: ' December 12, 2017 11:10 Analysis Stop Date: December 14, 2017 10:15
Analyst: Greta Pallack, B.A. Qualifier: U
Primary Value: :50.07 Salmonella MPN/mL sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 4 of 8
Imo' Final Report BCS ID 1712079, 1712080, 1712081, 1712082, 1712083, 1712084, 1712085
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH-#E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
LABORATORY
ACCREDITATION
BUREAU
ACCRED1TEDnwEc,7o2i J
i

Client: Branch Residuals and Soils
— Analysis: Salmonella
Project Name: Cordova NA
Client Sample ID: VD-7 Sample Date/Time: December 11, 2017 14:18
BCS Sample ID: 1712085 Sample Description: Biosolids
Date Received: December 12, 2017 10:40 Amount Submitted:100ml bottle % Solids: 36.1
Amount Analyzed: 30.10 g Receipt Temperature: 1.9 deg C Preserved: Yes
Analysis Start: December 12, 2017 11:10 Analysis Stop Date: December 14, 2017 10:15
Analyst: Greta Pallack, B.A. Qualifier: U
r
Primary Value: :50.07 Salmonella MPN/ml- sample analyzed
Secondary Value: 50.7 Salmonella MPN/4 dry grams
u Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's
detection limit for the amount of sample analyzed as per the method's standard reporting units
Page 5 of 8
Final Report BCS ID 1712079,1712080, 1712081, 1712082,1712083, 1712084,1712085
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH.#E82924, ISO%IEC 17025:2005 L2422 (L-A-B), PA DEP# 6&03950, EPA# FLO1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
LABORATORY
ACCREDITATION
,�lSCI� BUREAU .-,�dJ
�" �� ACCREDITEDawics?.

Client: Branch Residuals and Soils
-- Project: Cordova NA
Method Detection Limit: 1 microorganism/ unit weight or volume analyzed
Practical Quantitation Limit: 1 microorganism/ unit weight or volume analyzed
Report Notes: Custody Seal Condition: Not Present
Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt
as per the described analytical methodology. End of report notes.
Page 6 of 8
Final Report BCS ID 1712079,1712080, 1712081, 1712082, 1712083, 1712084, 1712085
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 6&03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
LABORATORY
ACCREDITATION i
BUREAU ,QdJ
"'; a ACCREDITEDswicim..

I certify that I have examined I am familiar with the information submitted herein. The results pertain only to
analyzed sample(s) associated identifier #(s). Based on my inquiry of the individuals responsible for the
analysis, I believe the data to be true, accurate, complete. Sampling field data was obtained from submitted
documents. The analysis was authorized commissioned by the client. The resulting data are representative of
the analysis conducted on the material/samples/articles provided by the client (or client's representative)
it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate
method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS
Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any
sample, batch, source, or the process they are derived from. Quality assurance controls were performed as
outlined in the method and as per Good Laboratory Practices. The analysis results presented in this report
meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH
Environmental Laboratory Certification Program, as -applicable unless otherwise noted.
Signature of Laboratory Director/Authorized Rep.
]u�
Date: December 19, 2017
Page-7 of 8
! Final Report BCS ID 1712079,1712080, 1712081,1712082, 1712083, 1712084, 1712085
BCS LABORATORIES, INC. -- GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAX. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
0 , "„ — LABORATORY
ACCREDITATION
BUREAU
t ^ ACCREDITED ismic im.

DATA QUALIFIER CODES_
SYMBOL
MEANING
B
' based on counts outside the acceptable range.
_Results
(Sample received without prior notification or delayed delivery. Analysis performed outside of
X
yassociated method required QC data set (1 QC data set per 20 samples per 168 hours).
(Value Is between the laboratory method detection limit & laboratory practical quantitation limit_
—J1 'The sample matrix interfered with the ability to make any accurate determination.0
_J2
J3
No Quality Control criteria exist for the components
(The data are questionable because of improper laboratory or field protocols.,.—.---,---. —�
_ L
` Off scale high. Actual value is known to be greater than value given
i Presumptive evidence for the presence of material. There is an Indication that the analyte is present,
N
I but the confirmation requirement was not met.
0._._
_
but analysis not performed
Q
.;Sampled,
Sample held beyond the accepted holding time. j
Indicates that the compound was analyzed for but not detected. The specified component was not
U
detected. The reported value is the method detection limiter 1
V
!Analyte was detected In both sample and associated method blank_ Data maynotbe accurate.
Y
1The laboratory analysis was from an improperly preserved sample The data may not be accurate. 1
;Too many colonies. present (TNTC); the numeric value given represents the upper end of the value that
Z
I can be determined based on the volume.
7
'Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. j
Presence or absence of analyte could not be confirmed.
**
Not reported due to interference.
^
BCS is not currently accredited for this analyte.
#
? BCS Lab specific qualifier. See laboratory analysis notes.
Page 8 of 8
Final Report BCS ID 1712079, 1712080, 1712081, 1712082, 1712083, 1712084, 1712085
BCS LABORATORIES, INC. — GAINESVILLE
4609 NW 6TH STREET. STE. A. GAINESVILLE. FLORIDA 32609
TEL. [phone], FAx. [phone]
WWW.MICROBIOSERVICES.COM
FL DOH #E82924, ISO/IEC 17025:2005 L2422 (L-A-B), PA DEP# 68-03950, EPA# FLO 1 147
THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES
""'""�• LABORATORY
ACCREDITATION -
-� BUREAU,« J
ACCREDITEDwlic»o�

i
CHAIN OF CUSTODY RECORD BCS Laboratories
' www.microbloservices.com 4609 NW 6th street, Building A
1^c FL DOH Laboratory #E82924, EPA# FI-01147 Gainesville, FL 32609
Tel. [phone], Fax. [phone]
Client Name and Address: 31FA1c.k� 5+ I h vI S �U r S Compliance Monitoring? 0 Yes❑ No
City/State/Zip: C12e t?,43 & ax, A-/ c Z "q0 Project ID: yo ►`I �i2e�(P
Project Manager: 26bsn-4 Facility/Site: (o2J,)JA /d
Telephone Number: Fax No.: Report To:
Sampler Name: (Print) V4e,,F, Fe'4 Email: G--
Sampler Signature: ' J Invoice To: 004
Branch Residuals and Soils
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1712095
12112/2017 10:40
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12/12J2017 10:40
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_ VD-6
17120134
12/12/2017 10:40
Laboratory Comments:
S Postal DHL FEDEX Other: Temp. @ recp't: / 1 i / °C
UP T
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Date Time IR- Corrected for
Custody Seal: Intact Broken
Presence of visabld ice Y
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�� Hold Time
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Page: 1 of 1
Report Number: 18-080-0230
Account Number: 46368
Send To: Branch Residuals and Soils LLC
Bob Branch
8646 West Market Street
Suite 111
Greensboro, NC 27409
Lab Number: 59303
Sample Id : Von Drehle
Waypoint-(D
ANALYTICAL
Project: Von Drehle
REPORT OF ANALYSIS
Total Solids *
38.20 382000
Moisture *
61.79
;pH *'
'7,6
Calcium Carbonate Equivalent
40.10 401000
Comments:
NC CERT#257
CCE, SULFUR AND ORGANIC NITROGEN
NOT FOR COMPLIANCE PURPOSES.
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 * Fax [phone]
www.waypointanalytical.com
Date Sampled:
Date Received: 03/21/2018 00:00
Date Reported: 03/29/2018
100.0
BW1
03/21/201814:00
SM-2540G
100.0
SW1
03/21/201814:00
SM-2540G
1.0
JM
03/22/2018 08:15
9045D
2500
R D
03/26/2018 12:30
AOAC 955.01
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of ourclients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Pof« r 60w r/
Pauric McGroary
Agronomist

i
�MICROBAC°
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8A0774
- Von Drehle Corporation Project Name: Residuals Sample - 60 day
Mr. Chris Fowler Project / PO Number: N/A
126 First Street Received: 01/26/2018
Cordova, NC 28330 Reported: 02/19/2018
Case Narrative
Report amended on February 19, 2018 for work order KBA0774 that was originally reported on February 16, 2018 to removed PCB results.
Analytical Testing Parameters
Client Sample ID: Residual from Paper Plant
Sample Matrix: Solid Collected By: Marin
Lab Sample ID: K8A0774-01 Collection Date: 01/26/2018 11:56
Method: Calculation
Plant Available Nitrogen
Method: EPA 300.0, Rev. 2.1 (1993)
Nitrate as N
Nitrite as N
Method: SM 2540 G-2011
- % Solids
Method: SM 4500 H+B-2011 (Non -Aqueous)
pH at 25 °C
Method: SM 4500 NH3 C-2011
Ammonia as N
Wet Chemistry
Method: Calculation
Sodium Adsorption Ratio, SAR
Method: SM 4500 P F-2011
Result
RL
Units
Note
Prepared
Analyzed
Lab
260
mg/kg
02/16/18 1640
02/16/18 1645
FAY
<0.0250
0.0250
mg/kg
01/26/18 1534
01/29/18 1430
FAY
<0.500
0.500
mg/kg
01/26/18 1534
01/29/18 1430
FAY
45.0
1.00
%
01131/181349
FAY
7.8
1.0
pH Units
H
01/29/18 1200
FAY
77.9
0.100
mg/kg
Y
01/30/18 0934
FAY
Result
RL
Units
Note
Prepared
Analyzed
Lab
0.420
mg/kg
02/16/18 1640
02/16/18 1645
FAY
Phosphorus, Total (as P)
0.62
0.25
mg/kg
Metals
Result
RL
Units Note Prepared
Method: EPA 200.7 Rev 4.41994
Aluminum
1010
2.46
mg/kg
Arsenic
<0.020
0.020
mg/kg
Cadmium
<0.001
0.001
mg/kg
Calcium
191000
0.983
mg/kg
_ Copper
8.06
0.005
mg/kg
Lead
0.786
0.003
mg/kg
Magnesium
1780
0.983
mg/kg
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920
p I www.microbac.com
02/02/18 1411 FAY
Analyzed Lab
02/14/18 0942
FAY
02/14/18 0942
FAY
02/14/18 0942
FAY
02/14/18 0942
FAY
02/14/18 0942
FAY
02/14/18 0942
FAY
02/14/18 0942
FAY
Page 1 of 4

Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8A0774
Client Sample ID: Residual from Paper Plant
Sample Matrix: Solid Collected By: Marin
Lab Sample ID: K8A0774-01 Collection Date: 01/26/2018 11:56
Metals
Result
RL
Units
Note Prepared Analyzed
Lab
- Molybdenum
1.47
0.001
mg/kg
02/14/18 0942
FAY
Nickel
<0.001
0.001
mg/kg
02/14/18 0942
FAY
Potassium
69.8
1.97
mg/kg
02/14/18 0942
FAY
Selenium
<0.010
0.010
mg/kg
02/14/18 0942
FAY
Sodium
956
4.92
mg/kg
02/16/181007 02116/181506
FAY
Zinc
30.1
0.010
mg/kg
02/14/18 0942
FAY
Analyses Subcontracted
to: ECI
Result
RL
Units
Note Prepared Analyzed
Method: SM 4500-N org B
02/15/18 0000
Total Kjeldahl Nitrogen 813 mg g
Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley
Mercury Result RL Units Note Prepared Analyzed
Method: SVV7471A
_. Mercury, Total <0.550 0.550 mg/kg DRY 02/05/18 0733 02/05/18 1227
PCB SOLID
Result
RL
Units Note
Prepared
Analyzed
Method:8082A
Aroclor-1016
<38.4
'38.4
ug/kg DRY
01/31/18 0903
01/31/18 1737
Aroclor-1221
<38.4
38.4
ug/kg DRY
01/31/18 0903
01/31/18 1737
' Aroclor-1232
<38.4
38.4
ug/kg DRY
01/31/18 0903
01/31/18 1737
;Aroclor-1242
3
38.4
ug/kg DRY
01/31/18 0903
01/31/18 1737
Aroclor-1248
jnrjtP\
<38.4
38A
ug/kg DRY
01/31/18 0903
01/31/18 1737
_ Aroclor-1254
WEB EGA-
<38.4
38.4
ug/kg DRY
01/31/18 0903
01/31/18 1737
Aroclor-1260
�ci /r
<38.4
38.4 ug/kg DRY
01/31/18 0903
01/31/18 1737
Surrogate: 2,4,5,6-Tetrachloro-m-Xylene
69.9
Limit: 29-133
% Rec
01/31/18 0903
01/31/18 1737
Surrogate: Decachlorobiphenyl
44.6
Limit: 60-125 % Rec
01/31/18 0903
01/31/18 1737
Percent Solids
Result
RL
Units Note
Prepared
Analyzed
- Method: D2216
Percent Solids
44.6
1.00
weight %
02/02/18 0735
Laboratory
FAY: Microbac Laboratories, Inc. - Fayetteville
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, INC 28306 1910.864.1920 p I www.microbac.com Page 2 of 4

i
(D)MICROBAC°
Microbac Laboratories, Inc. - Fayetteville
j CERTIFICATE OF ANALYSIS
K8A0774
{ Definitions
I *: Surrogate or spike compound out of range
H: Analyte was prepared and/or analyzed outside of the analytical method holding time
MDL: Minimum Detection Limit
RL: Reporting Limit
�Y: This analyte is not on the laboratory's current scope of accreditation.
i Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11
North Carolina DENR NPDES
Report Comments
Reviewed and Approved By:
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted. '
The data and information on this, and other accompanying documents, represents Bonnie K. Sanders
only the sample(s) analyzed. This report is incomplete unless all pages indicated Senior Project Manager
in the footnote are present and an authorized signature is included.
[e-mail]
02/19/201811:18
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 3 of 4

-j -- ----! ---� _ �
0
Fayetteville Division 2592 Hope Mills Road - Fayetteville, NC 28306 [phone] / F" ' --- rn
MC R max` - * K8A0774* a r:
CHAIN OF CUSTODY RECORD IIIG�GI���II�WNI�tl���l�
CLIENT NAME&ADDRESS:
VonDrehle Corp.
126 First Street
Cordova, NC 28330
PO#
PROJECT/LOCATION:
Cordova - 60-dayseries
#OF
B
o
T
T
L
E
s
TYPE
OF
ANALYSIS
PRESERVATION CODE
rE
E
I(M)
1 -
�E
C
2
Q
!E
�
U
E
Q�
a
o
U
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Z'
O
c
N
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o
(1).
Q
Z
Cn
d
Z1
Zv
y;
o,
m-'.
l=t
I—:
j
'
—
' o
Q
o
m
d`;
CODE: A = None
B = HNO3 (pH<2) + c4"C
C = H2SO4 (pH<2) + <4'C
D = NaOH + <4°C
E = ZN Acetate + <4°C
F= HCI
CONTACT PERSON:
Mr. Chris Fowler
PHONE:
910-410-9131
SAMPLER:
J. MARI N
DATE / METHOD OF SHIPMENT:
Microbac
LAB ID #
SAMPLE TYPE
DATE
TIME
COMP
cRa6
pH
D.O.
TEMP'C
RES.
CHLORIN
Residual from paper plant
«
��
X
2
4
A
A
A
A
A
A
A
A
A
A
L,
1
A
A
A
A
A
A
A
I A
A
JA-
I/
Reli ulahed by:
1
Dyateqq /�-� / G
/ (ice—` D
�
Lie
Receiv by: I ature)
_ 2
Date
Time
Rel quished by:
Date
Time
Received by: (Signature)
Date
Time
7 3
4
Relinquished by:
Date I
Time •
Received by: (Signature)
Date
Time
5
6
Comments or Special Hazards:

M I C R 0 B A C
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8A0694
Project Description
Residuals Sample -Annual
For:
Mr. Chris Fowler
Von Drehle Corporation
126 First Street
Cordova, NC 28330
Bonnie K. Sanders
Senior Project Manager
Wednesday, February 7, 2018
Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of
your report was completed by Microbac Laboratories, Inc. - Fayetteville. If you have any questions, comments, or require
further assistance regarding this report, please contact your service representative listed above.
I certify that all test results meet all of the requirements of the accrediting authority listed within this report. All results for soil
samples are reported on a'dry-weight' basis unless specified otherwise. Analytical results for water and wastes are reported on
a'as received' basis unless specified otherwise. A statement of uncertainty for each analysis is available upon request. This
laboratory report shall not be reproduced, except in full, without the written approval of Microbac Laboratories. The reported
results are related only to the samples analyzed as received.
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com
Page 1 of 8

Von Drehle Corporation
Mr. Chris Fowler
126 First Street
Cordova, NC 28330
ICI ICROBAC°
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8A0694
Project Name: Residuals Sample - Annual
Project / PO Number: 2030767
Received: 01/24/2018
Reported: 02/07/2018
Sample Summary Report
Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received
Residual from paper plant. K8A0694-01 Solid Grab 01/24/18 11:45 01/24/18 14:50
i
I
Page 2 of 8

0MICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8A0694
Analytical Testing Parameters
Client Sample ID: Residual from paper plant
Sample Matrix: Solid Collected By: Marin
Lab Sample ID: K8A0694-01 Collection Date: 01/24/2018 11:45
Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley
Result RL Units Note Prepared Analyzed
-_' Method: SW9045
Corrosivity pH 8.58 UNITS 01/26/18 1508
Temperature At Determination (C) 17.2 UNITS 01/26/18 1508
8270 TC
Result
RL Units
Note
Prepared
Analyzed
Method: SW8270C
1,4-Dichlorobenzene
<50.0
50.0 ug/L
01/30/18 1430
01/31/18 1013
_ 2,4,5-Trichlorophenol
<50.0
50.0 ug/L
01/30/18 1430
01/31/18 1013
2,4,6-Trichlorophenol
<50.0
50.0 ug/L
01/30/18 1430
01/31/18 1013
2,4-Dinitrotoluene
<50.0
50.0 ug/L
01/30/18 1430
01/31/18 1013
Hexachlorobenzene
<50.0
50.0 ug/L
01/30/18 1430
01131/181013
Hexachlorobutadiene
<50.0
50.0 ug/L
01/30/18 1430
01/31/18 1013
Hexachloroethane
<50.0
50.0 ug/L
01/30/18 1430
01/31/18 1013
m-,p-Cresol
<50.0
50.0 ug/L
01/30/18 1430
01/31/18 1013
"- Nitrobenzene
<50.0
50.0 ug/L
01/30/18 1430
01/31/18 1013
j o-Cresol
<50.0
50.0 ug/L
01/30/18 1430
01/31/18 1013
Pentachlorophenol
<250
250 ug/L
01/30/18 1430
01/31/18 1013
_- Pyridine
<250
250 ug/L
01/30/18 1430
01/31/18 1013
Surrogate: 2,4,6-Tdbromophenol 97.0
Limit: 10-123 % Rec
01/30/18 1430
01/31/18 1013
Surrogate: 2-Fluorobiphenyl
81.6
Limit: 43-11.6 % Rec
01/30/18 1430
01/31/18 1013
Surrogate: 2-Fluorophenol
49.7
Limit: 21-100 % Rec
01/30/18 1430
01/31/16 1013
Surrogate: Nitrobenzene-d5
73.0
Limit: 35-114 % Rec
01/30/18 1430
01/31/18 1013
Surrogate: p-Terphenyl-d14
90.7
Limit: 33-141 % Rec
01/30/18 1430
01/31/18 1013
Surrogate: Phenol-d5
33.7
Limit: 10-94 % Rec
01/30/18 1430
01/31/18 1013
Ignitability of Solids
Result
RL Units
Note
Prepared
Analyzed
Method: 1030
Bumrate - 1030
<2.20
2.20 mm/sec
01/30/18 1140
Mercury
Result
RL Units
Note
Prepared
Analyzed
I Method: SW7470A
Mercury
<0.00200
0.00200 mg/L
01/30/18 0957
01/31/18 1133
Metals by 6010
Result
RL Units
Note
Prepared
Analyzed
Method: SW6010C
Arsenic, TCLP
<1.00
1.00 mg/L
01/30/18 1029
01/31/18 1353
Barium, TCLP
0.272
0.100 mg/L
01/30/18 1029
01/31/18 1353
Microbac
Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I
www.microbac.com
Page 3 of 8

�MICR®BAc"
Microbac Laboratories,` Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8A0694
Client Sample ID: Residual from paper plant
Sample Matrix: Solid Collected By: Marin
Lab Sample ID: K8A0694-01 Collection Date: 01/24/2018 11:45
Metals by 6010
Result
RL
Units
Note Prepared
Analyzed
Cadmium, TCLP
<0.100
0.100
mg/L
01/30/18 1029
01/31/18 1353
Chromium, TCLP
<0.200
0.200
mg/L
01/30/18 1029
01/31/18 1353
Lead, TCLP
<1.00
1.00
mg/L
01/30/18 1029
01/31/18 1353
j Silver, TCLP
<0.100
0.100
mg/L
01/30/18 1029
01/31/18 1353
Metals by 6020
Result
RL
Units
Note Prepared
Analyzed
Method: SW6020A
TCLP
<0 500
0 500
mg/L
01/30/18 1029
01/31/18 1549
- Selenium,
Reactivity, Cyanide
Result
RL
Units
Note
Prepared
Analyzed
Method: SW9014
Reactivity, Cyanide
<9.98
9.98
mg/kg
01/31/18 1520
Sulfide (Reacitivity)
Result
RL
Units
Note
Prepared
Analyzed
Method: SW9034
- Reactivity, Sulfide
<100
100
mg/kg
01/31/18 1700
TCLP HERBICIDES
Result
RL
Units
Note
Prepared
Analyzed
Method: SW8151A
2 4-D
<20.0
20.0
ug/L
01/31/18 1213
02/01/18 2006
2,4,5-TP (Silvex)
<2.00
2.00
ug/L
01/31/18 1213
02/01/18 2006
( Surrogate: 2,4-Dichlorophenylacetic acid
41.3
Limit: 20-144
% Rec
01/31/18 1213
02/01/18 2005
TCLP Pesticides
Result
RL
Units
Note
Prepared
Analyzed
Method: SW8081B
' Endrin
<0.500
0.500
ug/L
01/30/18 1215
02/02/18 0520
Lindane
<0.500
0.500
ug/L
01/30/18 1215
02/02/18 0520
Methoxychlor
<0.500
0.500
ug/L
01/30/18 1215
02/62/18 0520
Toxaphene
<10.0
10.0
ug/L
01/30/18 1215
02/02/18 0520
Chlordane
<10.0
10.0
ug/L
01/30/18 1215
02/02/18 0520
Heptachlor
<0.500
0.500
ug/L
01/30/18 1215
02/02/18 0520
Heptachlor Epoxide
<0.500
0.500
ug/L
01/30/18 1215
02/02/18 0520
alpha Chlordane
<0.500
0.500
ug/L
01/30/18 1215
02/02/18 0520
gamma Chlordane
<0.500
0.500
ug/L
01/30/18 1215
02/02/18 0520
Surrogate: 2,4,5,6-Tetrachloro-m-xylene
53.3
Limit: 20-180
% Rec
01/30/18 1215
02/02/18 0520
Surrogate: Decachlorobiphenyl
20.1
Limit: 25-140
% Rec
01/30/18 1215
02/02/18 0520
Volatile Organics
Result
RL
Units
Note
Prepared
Analyzed
Microbac Laboratories, Inc.
2692 Hope Mills Rd I Fayetteville, NIC 28306 1910.864.1920 p I www.microbac.com Page 4 of 8

VMICROBAC@
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8A0694
Client Sample ID: Residual from paper plant
Sample Matrix: Solid Collected By: Marin
Lab Sample ID: K8A0694-01 Collection Date: 01/24/2018 11:45
Volatile Organics
Result
RL Units
Method: SW8260B
1,1-Dichloroethene
<50.0
50.0 ug/L
1,2-Dichloroethane
<50.0
50.0 ug/L
Benzene
<50.0
50.0 ug/L
Carbon tetrachloride
<50.0
50.0 ug/L
Chlorobenzene
<60.0
50.0 ug/L
Chloroform
<50.0
50.0 ug/L
Methyl Ethyl Ketone
<100
100 ug/L
- Tetrachloroethene
<50.0
50.0 ug/L
Trichloroethene
<50.0
50.0 ug/L
Vinyl chloride
<100
100 ug/L
Surrogate: 1,2-Dichloroethane-d4
101
Limit: 80-120 % Rec
Surrogate: 4-Bromofluorobenzene
103
Limit: 86-115 % Rec
Surrogate: Dibromofluoromethane
97.8
Limit: 86-118 % Rec
Surrogate: Toluene-d8
99.9
Limit: 88-110 % Rec
Note Prepared
Analyzed
01/31/18 1655
01/31/18 1655
01/31/18 1655
01/31/18 1655
01/31/18 1655
01/31/18 1655
01/31/18 1655
01/31/18 1655
01/31/18 1655
01/31/18 1655
01/31/18 1655
01/31/18 1655
01/31/18 1655
01/31/18 1655
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 5 of 8

(&MICROBAC ®R
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8A0694
Batch Quality Control Summary
Analyses Subcontracted to: Microbac Laboratories, Inc. - Ohio Valley
Spike Source %REC RPD
Metals by 6020 Result RL Units Level Result %REC Limits RPD Limit Notes
Batch WG647253 - METHOD - SW6020A
BLK (WG646865-02) Prepared: 01/30/2018 Analyzed: 01/31/2018
Selenium, TCLP ND 0.0500 mg/L - U
BS (WG646865-03) Prepared: 01/30/2018Analyzed: 01/31/2018
Selenium, TCLP 0.237 0.0500 mg/L 94.9 80-120 20
Spike Source %REC RPD
Reactivity, Cyanide Result RL Units Level Result %REC Limits RPD Limit Notes
Batch WG646993 - SW7.33 - SW9014
BS (WG646993-01) Prepared: Analyzed: 01/31/2018
Reactivity, Cyanide ND 100 mg/kg 4.96 .5-110 50 U
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 8

VMICROBAC@
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K8A0694
Laboratory
FAY: Microbac Laboratories, Inc. - Fayetteville
Definitions
*: Surrogate or spike compound out of range
J: [Undefined]
IVIDL: Minimum Detection Limit
RL: Reporting Limit
_ RPD: Relative Percent Difference
U. Not detected at or above adjusted sample detection limit
Cooler Receipt Log
Cooler ID: Default Cooler Temp: 4.1 °C
Cooler Inspection Checklist
Custody Seals Intact and/or No Evidence of Tampering Yes
COC/Labels Agree Yes
Received on Ice (or not required) Yes
Containers Intact
Preservation Correct (or not required)
Project Requested Certification(s)
Microbac Laboratories, Inc. - Fayetteville
11 North Carolina DENR NPDES
Yes
Yes
Report Comments
Reviewed and Approved By:
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted. ���\�" �► VY
The data and information on this, and other accompanying documents, represents Bonnie K. Sanders
only the sample(s) analyzed. This report is incomplete unless all pages indicated Senior Project Manager
in the footnote are present and an authorized signature is included.
[e-mail]
02/07/2018 12:26
Microbac Laboratories, Inc.
2692 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 7 of 8

Fayetteville Division 2592 Hope Mills Road - Fayetteville, NC 28306 [phone]
I C B A. `" : Y, *K8A0694*
r
.. II�QNIdVI�VB�V�V�e�l�
'CHAIN OF:CUSTODY RECORD
CLIENT NAME BADDRESS:
VonDrehle Corp.
126 First Street
Cordova, NC. 28930
POO
PROJECTILOCATION:
Cordova - Yearly
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CONTACT PERSON:
Mr: Chris Fowler
PHONE
940-410-9131
AMPLER
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DATE l METHOD OF SHIPMENT:
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Page 8 of 8

SECTION III
MANAGEMENT PLAN

MANAGEMENT PLAN
von Drehle Corporation produces Fiber Clay from its Cordova, North Carolina facility as a bi-product
' of paper towel production using recycled paper. These residual solids are produced by non -biological
processes that separate clay non -suitable fibers out during the production processes. Plastics are also
separated and are sent to the land fill and are not to be considered as part of this Class A permit
application. These residuals have no domestic contribution. This facility has a Class B land
application permit (WQ0005135) for these same residual solids. Von Drehle .desires to have both
Class A and B permits in effect as a backup should von Drehlebe unable to meet Class A standards.
Based on the pathogen testing and the nb-biological nature of the treatment process, vector attraction
NoN —
reduction testing is not required.
von Drehle wishes to distribute their Fiber Clay in the following ways:
• Use as a landfill daily cover,
• Admixture for composts, soil amendments, and potting soils, and
• As a replacement for commercial lime (or most limiting application factor) on nonspecific
agricultural receiver sites.
For direct application, von Drehle Corporation or it's assigned representative will identify local
landowners and/or other property as receiver sites. Application made to all sites will be based on the
ability of the crop and the land to properly assimilate the residual solids. Application thickness of the
application rate, percent solids of the residuals applied, the type, whether the field can or will be
incorporated, thickness of the vegetative cover, and the lime requirement of the soil will be
predominant application factors. The nitrogen needs of the crop will be secondary since it is expected
that additional nitrogen will need to be applied to correct the carbon -nitrogen ratio to all the proper
growth of the crop. von Drehle, . plans to take all of these into account to be conservative and will
distribute these residuals based on the most restrictive of these application rates.
For uses of these residuals in other processes other than direct application, von Drehle makes no claim
for their consistency or properties. Use by other entities will be without their responsibility to
determine and accept as is, with no liability or other implication to von Drehle Corporation.
1

Overview of Process and Residual Solids handling
1
11

Overview of Process and Residual Solids Handling
i
von Drehle Corporation Cordova facility is located at 126 First Street in Richmond County, North
Carolina. This facility produces, approximately 22,500 dry tons of Fiber Clay annually through
separation and fractionation processes from their feed stock recycled paper. The processes remove all
tplastics which are sent to the landfill. The majority of the recycled paper is repulped for von Drehle's
paper making process. The clay and short fibers that are separated out in the various screening and
1 fractionation processes are run through a belt press and Fiber Clay is made. Fiber Clay is a product
' of non -biological processes and has no domestic contribution.
' Fiber Clay can be placed in sealed trucks have three potential types of destinations:
• To a landfill for use as daily cover,
• To an offsite blending operation for the inclusion in composts, soil amendments, and potting
soils or
• As a replacement for commercial lime (or most limiting application factor) on nonspecific
agricultural receiver sites.

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Distribution Methods for Reuse
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Distribution Methods for Reuse
The Fiber Clay may be distributed in the following manner:
• Use as a landfill daily cover,
• Admixture for composts, soil amendments, and potting soils, and
• As a replacement for commercial lime on nonspecific agricultural receiver sites.
For direct, application to nonspecific receiver sites, von Drehle Corporation or its assigned
representative will identify local landowners and/or other property as receiver sites. Application made
to all sites will be based on the ability of the crop and the land to properly assimilate the residual
solids. Application thickness of the application rate, percent solids of the residuals applied, and the
type and thickness of the vegetative cover will be the determining factors. These materials have very
little nitrogen value so application will be based on:
• application thickness or
• lime needs of the soil.
whichever of these accounts for the most restrictive application rate.
Application thickness of the application rate; percent solids of the residuals applied, the type, whether
the field can or will be incorporated, thickness of the vegetative cover, and the lime requirement of
the soil will be predominant application factors. The nitrogen needs of the crop will be secondary
since it is expected that additional nitrogen (above what is required for crop growth) will need to be
applied to correct the carbon -nitrogen ratio to all the proper growth of the crop. von Drehle, plans to
take all of these into account to be conservative and will distribute these residuals based on the most
restrictive of these application rates.
For other distribution points regarding the use of this residual in other processes or as admixtures, von
Drehle makes no claim for their consistency or properties. Use by other entities will be without their
responsibility to determine and accept as is with no implication to von Drehle.

Transportation and Logistics
8

Transportation and Logistics
von Drehle Corporation Fiber Clay will be loaded into sealed sludge trailers. These trailers will be
routed to various points for distribution, land application to nonspecific receiver sites, or sent a landfill
as daily cover. Trucks will travel on major traffic routes to the application and or distribution sites.
Individuals, agencies, or companies wishing to receive either of the von Drehle Fiber Clay will be,
issued a product information sheet, the most recent copy of the analytical information, and Product
Receipt Form. The product information sheet will specify the buffer requirements for von Drehle's
Fiber Clay as well as application restrictions. Each Product Receipt Form will document:
Amount of Fiber Clay received,
• The name, address and telephone number of the person who prepared the Fiber Clay,
• The name, address and telephone number of the person distributing/land applying the
residuals,
• A description of the processes that generated the residuals,
• A summary of the results from the most recent residuals sampling event,
• ' A .summary of the type and volume of residuals distributed/land applied per acre,
• A summary of the nutrients land applied per acre, and
• A list of recommendations to the recipient of the residual regarding field use,'soil testing,
pH adjustment, and other relevant agronomic information.
Both the Product Label and the Product Receipt Form will be required to ensure receipt of this
information and for the removal volume. Copies of this information will be retained by the von Drehle
Cordova and will be available for review upon request
The distribution receiver, the land applier, and the site receiver will be instructed as to the proper use
of this material as listed below:
• Applications should be made in accordance with approved application standards.
• Application shall not be made to land that is flooded, frozen, or snow covered.
• Application and storage must be performed to prevent runoff from the application or
storage site to any surface water.

• Buffer or "no application" zones as described in the approved permit and Product
Information Sheet.
• Applications must not be applied so thick as to cover existing vegetation.
• Additional nitrogen may need to be applied to offset nitrogen. deficient symptoms due to
improper carbon to nitrogen ratio.

Monitoring and Recordkeeping

1
Monitoring and Recordkeeping
The von Drehle Corporation Cordova facility requests that the Fiber Clay (Fiber Clay) be monitored
bi-monthly for residuals analysis based on the amount of these residuals expected to be distributed.
A set of seven (7) fecal or Salmonella analyses will be performed prior to the end of the preceding bi-
monthly period. A TCLP analysis will be performed once per permit cycle. Fiber Clay samples will
- be collected and delivered to a laboratory qualified to analyze residual solids and that is familiar with
routine environmental sample preparation and standards.
Records pertinent to the successful management of the land applications program will be maintained
for the benefit of the farm operator, DWR, land applicator, and permittee. These records will contain
at a minimum:
• Source of the residuals,
• Type of the residuals,
• Date of the residual application/ distribution receiver,
• Information regarding the location of the residual application / distribution receiver (i.e. field
owner name, address, and telephone number, approximate field location, and field number)
• Method of application / intended distribution,
• Weather conditions (if applicable),
• . Soil conditions (if applicable),
• Type of crop or crops to be grown on the field or type of distribution receiver and intended
use,
• Volume or weight of residuals applied to the field or provided to distribution receiver,
• Annual totals of dry tons per acre of residuals, annual pounds of plant available nitrogen, and
' annual pounds of phosphorus applied to the. field or annual total of dry tons given to
__ distribution receiver if distributed as a non -land application alternative.

Each year an annual summary of the activities of the program will be prepared and delivered to the
appropriate agencies and participants on or before the 1 st of March. The Fiber Clay annual summary
will include:
1.
A) Summary of the Fiber Clay,
B) Volume/Weight of the distributed amount of Fiber Clay,
C) Name of the receiver of the distributed Fiber Clay,
D) Intended use(s) of the Fiber Clay,
E) Volume/Weight of other Amendments or Bulking Agents,
F) Annual totals of dry tons/acre of the Fiber Clay,
G) pounds of plant available nitrogen (PAN), phosphorus, and lime applied from the
Fiber Clay, if distributed to non-specific receiver sites and
H) pounds of nitrogen needed to offset organic carbon applied through Fiber Clay.
2. Bi-monthly - nutrients and metals will be analyzed of Aluminum, Ammonia, Arsenic,
Cadmium, Calcium, Copper, Lead, Magnesium, Mercury, Molybdenum, Nickel,
Nitrate -Nitrite, Zinc, % Total Solids, CCE, pH, Phosphorus, Potassium, TKN, Selenium,
and Sodium will be collected and analyzed by a qualified laboratory. From this
information, the Plant Available Nitrogen (PAN) will be calculated. If land application
occurs at a frequency of less than bi-monthly, nutrient and metal analyses will be
required for each distribution event.
3. Once a permit cycle a Toxicity Characteristics Leaching Procedure (TCLP) analysis with
ignitability, reactivity, and corrosivity of the von Drehle Fiber Clay will be collected and
analyzed by a qualified laboratory.

11
Leachate Collection

Leachate Collection
No provision is made for leachate collection since the residuals are not designed to undergo any
mixing with other productions on -site. The storage padat the facility is sloped to the back to the
drainage feature. Below the drainage feature is a screen to capture any solids that are washed to the
drain.
Once these residuals have been transported to the potential application sites or for other uses, the fiber
clay can be stockpiled in a covered facility or covered on the ground similar to other Class A products.
Once covered this material will remain covered until the time of application.

SECTION IV
VON DRHLE CORDOVA FIBER CLAY LABEL
AND PRODUCT INFORMATION SHEET

The von Drehle Corporation Cordova
Fiber Clay Label
Produced By Preparer
von Drehle Corporation Chris Fowler [phone]
Wastewater Treatment Plant 126 First Street
Cordova, North Carolina 28330 Cordova, North Carolina 28330
For information on this product contact von Drehle Corporation
Cordova, NC facility at [phone]
Fiber Clay from the von Drehle Corporation Cordova NC are the clay and short fibers excluded from the repulping
process of recycled paper production. The generated residuals have no domestic source percentage and are an exceptional
quality residual solid that is permitted for bulk distribution.
IApproved used for von Drehle Fiber Clay:
• Amendment for creation of soil mixture to be further distributed to the public,
• Amendment for compost to be further distributed to the public,
{ • Use as a daily landfill cover,
• Application to potential receiver sites for use as a soil amendment or replacement for agricultural lime.
' Provisions for application are listed below.
Provisions for Application
Application ofvon Drehle Fiber Clay are prohibited except in accordance with the provisions specified in theApplication
Information Sheet. Application must conform to standards identified in Permit WQOOxxxxx (Class A Permit No) and
include but are not limited to:
Maximum slope for the land application of these residuals is 10 % for surface applications and 18% for subsurface
applications
Distance
Buffer Items (feet)
Public or private water supply source, waters classified as SA or SB, and any Class I or Class II impounded
reservoir used as a source of drinking water for both surface and subsurface methods 100
Surface waters (intermittent streams, perennial streams, perennial surface water bodies and wetlands) 25
Surface water diversions (ephemeral streams, ditches, groundwater lowering ditches, or waterways) 0
Application can not occur to:
• adversely affect a threatened or endangered species or it's critical habitat,
• within the 100-year flood plain unless solids are incorporated within a 24-hour period,
• cause prolonged nuisance conditions,
• create conditions where runoff will occur,
• within the 100-year flood plain unless solids are incorporated within a 24-hour period, or
• during a measureable rainfall event or 24-hours following a 0.5 inch cumulative rainfall event (over 24-hours).

Application Information Sheet von Drehle Fiber Clay
1. von Drehle Fiber Clay shall not be applied to flooded, frozen, or snow-covered areas.
2. Application and storage of von Dreble Fiber Clay must be conducted in such,a way as to prevent runoff or
erosion from the application or storage site to any surface water.
_ 3. Applications of von Drehle Fiber Clay must not be applied so thick as to cover existing vegetation. Application
that is made to sites with less than 50 percent ground cover should be incorporated unless incorporation will result
in violation of other federal program.
4. Applications of von Dreble Fiber Clay shall be applied uniformly at a rate equal to amount that can be
adequately assimilated into the soil through incorporation, will not smother any current living crop on the surface
of the soil if material will not be incorporated, or the agronomic rate of the crop as specified by the permit and
the most recent residual analysis, or the lime requirement of the soil and most recent residuals analysis; whichever
is most limiting.
5. An acceptable soil pH (greater than 6.0) see appropriate state extension service for crop specific optimal soil pH
on individual receiver sites. The soil pH should be verified annually with a soil sample with recommendations.
These recommendations should be.followed as they relate to optimal crop growth, monitoring and adjustment of
the exchangeable sodium percentage, potential for calcium and magnesium deficiency, as well as other relevant
agronomic information. Additional fertilizer, lime, or other nutrients may need to be added as directed by the soil
sample results.
6. Applications and loading rates of von Dreble Fiber Clay shall be applied at rates that comply with realistic yield
expectations based on the soil series and crops found at: http://nutrients.soil.ncsu.edu/yields/
von Drehle Corporation Cordova Fiber Clay
Annroximatelv Contain:
45.00
Percent Solids
0.67
Plant Available Nitrogen surface land a lied ounds per dry ton
0.75
Plant Available Nitrogen (incorporated or injected) pounds per dry ton
0.003
Phosphate 205pounds per dry ton
0.17
1 Potash Opounds per dry ton
802
Liming agent pounds per dry, ton
7.8
pH of Fiber Clay
See von Drehle Corporation Cordova WWTP for a copy of the most recent residuals analysis
and loading rates.

SECTION V
WON DREHLE FIBER CLAY RECEIPT FORM

VON DREHLE CORPORATION CORDOVA
FIBER CLAY RECEIPT FORM
I , (printed name) have received wet
tons of von Drehle Corporation Cordova Fiber Clay, a von Drehle Fiber Clay product label,
and a copy of the most recent analysis of the product. I have read these documents and agree
to adhere to the directions specified on the Application Information Sheet and the Product
Label. My intended use of this product is
Contact Information:
Name
Address
City, State, Zipcode
Phone Number
Email Address
Signature of Receiver
Date of Receipt

SECTION VI
SPILL CONTROL PLAN

SPILL CONTROL PLAN
VON DREHLE CORPORATION CORDOVA
FIBER CLAY
CORDOVA, NORTH CAROLINA
In the case of a spill, the following actions shall be taken immediately:
1. Halt the source of the spill: Damaged truck or trailer tank unit.
2. Contain spill: Use straw bales to form a barrier. Straw hay bales can be obtained from
several sources for this purpose. Soil near the site can also be used to form a barrier for
containment.
3. Clean up: Use residual solids application equipment to recover as much of the material as
possible. After the application equipment has recovered as much material as possible, it
will be land applied as per operation plan.
4. Final Clean up: Any unrecoverable material will be scraped and swept from the road
-� surface and incorporated into an adjacent tillable area.
5. Notification: As soon as possible after a spill occurs notify:
A. von Drehle Corporation - [phone]
B. Department of Environment and Natural Resources
Fayetteville Regional Office at [phone] or appropriate regional office
C. The appropriate County Sheriffs Department
D. Fire Department if assistance is required for washdown
6. Management of clean-up efforts: The ORC or applicator shall take immediate charge of
-1 the clean-up activities. Additional labor will be requested from the treatment plant and
other departments as needed.
7. Reporting: Within 5 days of notifications, a written report will be prepared detailing the
cause of the spill, all actions taken in response to the spill, and proposed actions to be taken
to ensure spill.does not recur..

SECTION VII
APPLICATION RATES

APPLICATION RATES
Prior to a distribution event, a private land owner will contact von Drehle Corporation Cordova to
initiate an application. This land owner will indicate the type of crop to be grown and the size of the
field to have the residuals distributed. A recent soil sample will be needed to determine lime
requirements.
A recent sample of Fiber Clay generated from von Drehle Corporation Cordova will be used to
calculate the application rates for the crop based on the soil liming needs and the crop and soil
assimilation characteristics. Prior to the distribution event, the potential receiver sites will be
reviewed to insure the crop has been identified correctly and the field size is correct. Soils data will
be checked at that time. Application rates will be determined based on the solids content of the
residuals, the height of the crop on the receiver site, smothering potential of the crop, the lime
requirement of the soil, lime requirements of the soils analysis, and nitrogen needs of the crop to be
grown.
Application rates will be limited based on either: application thickness, lime needs of the soil, or
nitrogen needs of the crop; whichever of the three accounts .for the most restrictive application rate.
w' Based on my knowledge of potential receiver sites, application thickness should be no more than 3
wet tons per acre if it is to be spread on the surface of the soil with an actively growing crop and.no
more than 10 wet tons per acre if the residual is to be incorporated, depending on the percent solids
of the residuals. The incorporated amount may be further reduced if the incorporation equipment fail
to properly turn the residual under depending on slope, cover, soil assimilation. Application should
not occur at a rate that the residuals may experience runoff or erosion from the receiver site. Re-
application of sites will be based on these same factors. If there are questions concerning an individual
application rate for a receiver site, consult a licensed soil scientist.
Application of Fiber Clay has been shown to create an imbalance in the soil carbon to nitrogen ratio.
This is particularly important as it relates to specific time periods in a crop's growth cycle. It may
be necessary to apply additional nitrogen to achieve the crop results. The application rates listed

below outline the lime -added values from the following applications. At this point application rates
should be limited to about one ton of lime per acre (5 wet tons per acre).
Wet Tons/
Acre
Dry Tons/
Acre. , .
PAN
#/Acre
Lime
Tons/Acre
1
0.45
0.30
0.18
2
0.90
0.60
0.36
3
1.35
0.90
0.54
4
1.80
1.20
0.72
• 5
2.25
1.50
0.90
6
2.70
1.80
1.08
7
3.15
2.10
1.26
8
3.60
2.40
1.44
9
4.05
2.70
1.62
10
4.50
3.00
1.80
11
4.95
3.30
1.98
12
5.40
3.60
2.17
13
5.85
3.90
2.35
14
6.30
4.21
2.53
15
6.75
4.51
2.71
16
7.20
4.81
2.89
17
7.65
5.11
3.07
18
8.10
5.41
3.25
19
8.55
5.71
3.43
20
9.00
6.01
3.61