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WQ0001817_Monitoring - 03-2023_20231110 (2)
Monitoring Report Submittal ................................................... Permit Number#* WQ0001817 Name of Facility:* Albemarle Utility Company Month: * March Report Information Type * Revised - NDMR, NDAR-1, NDAR-2, NDMLR Revised - GW-59 Year:* 2023 Upload Document* March NDMR & NDAR-1 2023 Revised.pdf 9.3MB PDF Only March GW-59 2023 Revised.pdf 15.25MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address: * danny.perry@albemarleplantation.com Name of Submitter: * Danny S Perry Signature: a�a�rirJ S� t tf Date of submittal: 11/10/2023 This will be filled in automatically Initial Review Reviewer: Wanda.Gerald Is the project number correct?* WQ0001817 Is the monitoring report accepted?* Yes No Regional Office* Washington Reviewer: _anonymous Review Date: 11/14/2023 SUBMIT FORM ON, OW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Facility Name: Albemarle Utility Comapany Permit Name (if different): Facilitv Address: 862 Holiday Island RD N.0 27944 County Perqimans act Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 Location/Site Name: North of Holding Lagoon No. of wells to be sampled: 10 DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 PERMIT Number: Expiration Date: 05-31-2025 Non -Discharge WQ0001817 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): MW -1 Date sample collected: 3/23/2023 Well Depth: 20 ft. Well Diameter: 2 in. Depth to Water Level 82546:15.0 ft. below measuring point Screened Interval: -5 ft. to Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5.0 gallons Samples for metals were collected unfiltered: ❑ YES N NO and field acidified: El YES ® NO -20 ft. FIELD ANALYSES: pH 00400: 6.2 units Temp. o001o: 16.7 °C Spec. Cond. 00094: µ Odor 00085: None Appearance Tan If WELL WAS DRY at time ofMhos sampling, check here: ❑ LABORATORY INFORMATION Date sample analyzed:3/23/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.07 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.03 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 239 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.2 units Ba - Barium 01007 ug/L TOC 00680 5.3 mg/L Ca - Calcium 00916 mg/L Chloride 00940 12 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Signature of GW-59 Rev.06-07-2018 r ° ` Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ` 910.392.0223 Lab � 910.392.4424 Fax 710 Sowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5M3 Lab/Fax ANALYTICAL S CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Apr 05, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report M 2023-05799 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14596 Site: MW-1 3/23/2023 10:00 AM Water Jay Baker Test Method _ Results Date Analyzed Color Color Tan 03/23/2023 Depth to water, ft. Depth to Water, Ft. 15,0 feet 03/23/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/23/2023 Odor Qualitative None 03/23/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 239 mg/L 03/24/2023 Temperature SM 2550 B-2010 16.7 C 03/23/2023 pH SM 4500 H B-2011 6.2 units 03/23/2023 Total Organic Carbon (TOC) SM 5310 B-2014 5.3 rng/L 03/24/2023 Fecal Coliform SM9222D-2015MF <1 Colonies/100ml- 03/23/2023 Chloride SW500 Ci E-2011 12 mg/L 03/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev 2 0, 1993 0.07 mg/L 03/23/2023 Nitrate+Nitrite-Nitrogen EPA 3532,Rev 2.0, 1993 0,10mg/L 03/27/2023 Nitrate Nitrogen subtraction Method 0.03 mg/L 04/04/2023 Report # . 2023-05799 Page 1 of 10 SUBMIT FORM 01 LOW PAPER ONLY Mail original ROUNDWATER QUALITY MONITORING: and 1 copy to: OMPLIANCE REPORT FORM icility Name: Albemarle Utility Company armit Name (if different): _ icility Address: 862 Holid Hertford Island Rd NC act Person: Danny Shelton Perry ORC Location/Site Name: East of Baffle Lagoon Please Print Clearly or Type 27944 County Perquimans Telephone#: 252-426-1007 No. of wells to be sampled: 10 DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 PERMIT Number: Expiration Date: 05-31-2025 Non -Discharge WQ0001817 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER (from Permit): MW-2 Date sample collected: 3/23/2023 Well Depth: 12 ft. Well Diameter: 2 in. Depth to Water Level 82546: 4.5 p ft. below measuring point Screened Interval: -2 ft. to -12 ft. Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5.0 gallons Samples for metals were collected unfiltered: ❑ YES © NO and field acidified: ❑ YES ® NO FIELD ANALYSES: pH 00400: 5.3 units Temp. 000lo: 15.5 °C Spec. Cond. 000sa: µ Mhos Odor 00085: none Appearance Tan If WELL WAS DRY at time of sampling,check here:❑ LABORATORY INFORMATION Date sample analyzed:3/23/2023 Laboratory Name: Environment Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.10 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 colonies /100ml- Nitrate (NO3) as N 00620 0.05 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 251 mg/L Al - Aluminum of im mg/L pH (Lab) 00403 5.3 units Ba - Barium 01007 ug/L TOC oo68o 31.2 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 14 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) ipecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 < 0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Lamb Corporate Secretary Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.06-07-2018 envirochem ANALYTICAL 8 CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ° 910.347.5843 Lab/Fax in fo(2.,envi ronmen talchemists.com Albemarle Utility Date of Report: Apr 05, 2023 862 Holiday Island Road Customer PO #: Hertford NC 279" Customer ID: 09110024 Attention: Report #: 2023-05799 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14597 Site: MW-2 3/23/2023 10A 0 AM Water Jay Baker Test Method Results Date Analyzed Color Color Tan 03/23/2023 Depth to water, ft. Depth to water, Ft. 4.5 feet 03/23/2023 Ammonia Nitrogen EPA 350.1, Rev 2.0, 1993 < 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/23/2023 Odor aualitabve None 03/23/2023 Total Dissolved Solids (TDS) SM 2540 c-2015 251 mg/L 03/24/2023 Temperature SM 2550 B-2010 15.5 C 03/23/2023 pH SM 4500 H B-2011 5.3 units 03/23/2023 Total Organic Carbon (TOC) SM 5310 B-2014 31.2 mg/L 03/30/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/23/2023 Chloride SM4500 Cl E-2011 14 mg/L 03/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2, Rev. 2.0, 1993 0.10 mg/L 03/23/2023 Nitrate+Nitrite-Nitrogen EPA 3532, Rev. 2.0, 1993 0.15 mg/L 03/27/2023 Nitrate Nitrogen Subtracton Method 0.05 mg/L 04/04/2023 Report #:. 2023-05799 Page 2 of 10 SUBMIT FORM 01\ LOW PAPER ONLY DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon g ❑Remediation: Infiltration Gallery M Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: South East of Spray field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 3 Date sample collected: 3/23/2023 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 5.8 units Temp. 000lo: 1 5.4 °C DRY at Depth to Water Level 82546: 7.0 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec. Cond. 00094: µMhos time of 3 sampling,check Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor 00085: none Volume of water pumped/bailed before sampling: 1 gallons Appearance Tan/Grey here:❑ Samples for metals were collected unfiltered: ❑ YES N NO and field acidified: ❑ YES M NO LABORATORY INFORMATION Date sample analyzed:3/23/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.05 mg/L Pb - Lead o1051 ug/L Coliform: MF Fecal 31616 4 colonies /100mL Nitrate (NO3) as N 00620 0.68 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 951 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 5.8 units Ba - Barium 01007 ug/L TOC 00680 22.3 mg/L Ca - Calcium 00916 mg/L Chloride oo94o < 5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%, GW-59 Rev.06-07-2018 envirochem 4 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab * 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 1 910.347,5843 Lab/Fax info@environmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Date of Report: Apr 05, 2023 Customer PO #: Customer ID: 09110024 Report #: 2023-06799 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14598 Site: MW-3 3/23/2023 10:20 AM Water Jay Baker Test Method Results Date Analyzed Color Color Tan/Grey 03/23/2023 Depth to water, ft. Depth to water, Ft. 7.0 feet 03/23/2023 Ammonia Nitrogen EPA 350,1, Rev. 2.0, 1993 < 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Bailed before sampling 1(Dry) gallons 03/23/2023 Odor Qualitative None 03/23/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 951 mg/L 03/24/2023 Temperature SM 2550 B-2010 15.4 C 03/23/2023 pH SM 4500 H B-2011 5.8 units 03/23/2023 Total Organic Carbon (TOC) SM 5310 B-2014 22.3 mg/L 03/30/2023 Fecal Coliform SM 9222 D•2015 MF 4 Colonies/100ml- 03/23/2023 Chloride SM4500 Cl E-2011 < 5 mg/L 03/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 3532. Rev 20, 1993 0.05 mg/L 03/23/2023 Nitrate+ N itrite-N itrogen EPA353.2, Rev 20, 1993 0.73 mg/L 03/27/2023 Nitrate Nitrogen Subtraction Method 0.68 mg/L 04/04/2023 Report M 2023-05799 Page 3 of 10 SUBMIT FORM ON , DW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Icility Name: Albemarle Utility Company ,rmit Name (if different): Icility Address: 862 Holiday Island Rd Hertford NC 27944 or Type County Perquimans act Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 Location/Site Name: South West of Spray field No. of wells to be sampled: 10 WELL ID NUMBER (from Permit): MW - 4 Date sample collected: 3/23/2023 Well Depth: 12 ft. Well Diameter: 2 in. Depth to Water Level 82546:7.0 ft. below measuring point Screened Interval: -2 ft. Measuring Point is 3 ft. above land surface Relative M.P. Elevation: Volume of water pumped/bailed before sampling: 4.0 gallons Samples for metals were collected unfiltered: ❑ YES 0 NO and field acidified: ❑ YES LI DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 PERMIT Number: Expiration Date: 05-31-2025 Non -Discharge WQ0001817 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: to -12 ft. ft. NO FIELD ANALYSES: pH oo400: 5.9 units Spec. Cond. 00094: Odor 00085: Appearance Tan/Grey If WELL Temp. 000lo: 15.4 °C DRY at µMhos time of none Date sample analyzed:3/23/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.07 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 174 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 5.9 units Ba - Barium 01007 ug/L TOC 00680 20.8 mg/L Ca - Calcium 00916 mg/L _ Chloride oo94o < 5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) ipecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Lamb - Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 Environmental Chemists, Inc. envirochem6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab 1 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 b 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 , 910.347.5843 Labs Fax ANALYTICAL & CONSULTING CHEMISTS inforuienvironmentalchemistscom Albemarle Utility Date of Report: Apr 05, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-05799 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14599 Site: MW-4 3/23/2023 10:30 AM Water Jay Baker Test Method Results Date Analyzed Color Color fan/Grey 03/23/2023 Depth to water, ft. Depth to water, Ft 7.0 feet 03/23/2023 Ammonia Nitrogen EPA 350.1, Rev 2.0. 1993 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Bailed before sampling 4.0 gallons 03/23/2023 Odor Qualitative None 03/23/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 174 mg/L 03/24/2023 Temperature SM 2550 B-2010 15.4 C 03/23/2023 pH SM 4500 H B-2011 5.9 units 03/23/2023 Total Organic Carbon (TOC) SM 5310 B-2014 20.8 mg/L 03/30/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 03/23/2023 Chloride SM4500 CI E-2011 < 5 mg/L 03/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2 Rev. 2 0. 1993 0.07 mg/L 03/23/2023 Nitrate+Nitrite-Nitrogen EPA 353 2 Rev. 2 D, 1993 0.07 mg/L 03/27/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/04/2023 Report # 2023-05799 Page 4 of 10 SUBMIT FORM OI LOW PAPER ONLY Mail original! GROUNDWATER QUALITY MONITORING: and 1 copy to: COMPLIANCE REPORT FORM Please Print Clearly or Type Icility Name: Albemarle Utility Company ;rmit Name (if different): Icility Address: 862 Holiday Island Rd Hertford NC 27944 County Perquimans act Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 Location/Site Name: South West of Sprayfield No. of wells to be sampled: 10 L ID NUMBER (from Permit): MW - 5 Date sample collected: 3/23/2023 Depth: 15 ft. Well Diameter: 2 in. i to Water Level 82546: 9.1 ft. below measuring point Screened Interval: 12 ft. wring Point is 3 ft. above land surface Relative M.P. Elevation: ne of water pumped/bailed before sampling: 5.0 gallons )les for metals were collected unfiltered: ❑ YES E NO and field acidified: ❑ YES L1 DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 PERMIT Number: Expiration Date: 05-31-2025 Non -Discharge WQ0001817 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery K Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: to 2 ft. ft. 7,1no FIELD ANALYSES: pH 00400: 6.0 units Spec. Cond. 00094: Odor 00om: Temp. 000lo: 15.4 oC uMhos None Appearance Grey/ Tan Date sample analyzed:3/23/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.03 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 3.71 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 6.0 units Ba - Barium 01007 ug/L TOC 00680 5.2 mg/L Ca - Calcium 00916 mg/L _ Chloride 00940 81 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) ipecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% If WELL DRY at time of sampling, check here: El GW-59 Rev.06-07-2018 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392,4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS inforu;environmentalchemists.com Albemarle Utility Date of Report: Apr 05, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-05799 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14600 Site: MW-5 3/23/2023 10:40 AM Water Jay Baker Test Method Results Date Analyzed Color Color Grey/Tan 03/2312023 Depth to water, ft. Depth to Water. Ft. 9.1 feet 03/23/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0.1993 < 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Baited before sampting 5.0 gallons 03/23/2023 Odor Qualitative None 03/23/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 371 mg/L 03/24/2023 Temperature SM 2550 8-2010 15A C 03/23/2023 pH SM4500 H B-2011 6.0 units 03/23/2023 Total Organic Carbon (TOC) SM 5310 B-2014 5.2 mg/L 03/30/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/23/2023 Chloride SM4500 Cl E-2011 81 mg/L 03/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 Rev, 2 0 1993 0.03 mg/L 03/23/2023 Nitrate+ N itrite-Nitrogen EPA 353.2, Rev 2 0 1993 0.04 mg/L 03/27/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/0412023 Report #: 2023-05799 Page 5 of 10 SUBMIT FORM ON SOW PAPER ONLY GROUNDWATER QUALITY MONITORING: • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-25-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC Permit Name (if different): NPDES Other Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED ❑E Lagoon ❑ Remediation: Infiltration Gallery Hertford NC 27944 County Perquimans M Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: West Of Spray Field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 6 Date sample collected: 3/23/2023 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 5.9 units Temp. oo010: 1 5.7 °C DRY at Depth to Water Level 82546: 8.7 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: none sampling,check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Grey here:❑ Samples for metals were collected unfiltered: ❑ YES E NO and field acidified: ❑ YES ® NO LABORATORY INFORMATION Date sample analyzed:3/23/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.08 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 715 mg/L All - Aluminum of lo5 mg/L pH (Lab) 00403 5.9 units Ba - Barium 01007 ug/L TOC 00680 6.0 mg/L Ca - Calcium 00916 mg/L _ Chloride 00940 213 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH. as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.06-07-2018 envirochem 6� w ANALYTICAL & CONSULTING CHENMSTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392,4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info@environmentalchemists.com Albemarle Utility Date of Report: Apr 05, 2023 862 Holiday Island Road Customer PO 0: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-05799 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14601 Site: MW-6 3/23/2023 10:50 AM Water Jay Baker Test Method Results Date Analyzed Color color Grey 03/23/2023 Depth to water, ft. Depth to Water. Ft. 8.7 feet 03/23/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0. 1993 < 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Balled before sampling 5.0 gallons 03/23/2023 Odor Qualitative None 03/23/2023 Total Dissolved Solids (TDS) SM 2540 C-205 715 mg/L 03/24/2023 Temperature SM 2550 B-201 a 15.7 C 03/23/2023 pH SM4500 H B-2011 5.9 units 03/23/2023 Total Organic Carbon (TOC) SM 5310 B-2014 6.0 mg/L 03/30/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/23/2023 Chloride SM4500 C1 E-2011 213 mg/L 03/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev 2 0, 1993 0.08 mg/L 03/23/2023 Nitrate+Nitrite-Nitrogen EPA 353.2. Rev 2 0, 1993 0.06 mg/L 03/27/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/04/2023 Report #:: 2023-05799 Page lS of 10 SUBMIT FORM OI LOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Albemarle Utility Company Permit Name (if different): Facility Address: 862 F Hertford Please Print Island Rd NC 27944 act Person: Danny Shelton Perry ORC Location/Site Name: West of Baffle lagoon or Type County Perquimans Telephone#: 252-426-1007 No. of wells to be sampled: 10 DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 PERMIT Number: Expiration Date: 05-31-2025 Non -Discharge WQ0001817 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED N Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: WELL ID NUMBER (from Permit): MW - 7 Date sample collected: 3/23/2023 Well Depth: 16.9 ft. Well Diameter: 2 in. Depth to Water Level 82546: 4.0 ft. below measuring point Screened Interval: 11.9 ft. to 16.9 ft. Measuring Point is 2•5 ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5.0 gallons Samples for metals were collected unfiltered: ❑ YES M NO and field acidified: ❑ YES M NO FIELD ANALYSES: pH 00400: 6.4 units Temp. 000lo: 14.0 °C Spec. Cond. 00094: µMhos Odor 00085: none Appearance Red/Tan WAS DRY at time of sampling, check here:❑ LABORATORY INFORMATION Date sample analyzed:3/23/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.05 mg/L Pb - Lead oio51 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 301 mg/L Al - Aluminum olim mg/L pH (Lab) 00403 6.4 units Ba - Barium 01007 ug/L TOC 00680 19.3 mg/L Ca - Calcium 00916 mg/L _ Chloride 00940 40 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 < 0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Lamb - Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 '77 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab 1 910.392.4424 Fax ® 710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ° 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Apr 05, 2023 862 Holiday Island Road Customer PO 0: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-05799 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14602 Site: MW-7 3/23/2023 9:50 AM Water Jay Baker Test Method Results Date Analyzed Color Color Red/Tan 03/23/2023 Depth to water, ft. Depth to Water, Ft. 4.0 feet 03/23/2023 Ammonia Nitrogen EPA 350,1, Rev. 2.0, 1993 < 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/23/2023 Odor Qualitative None 03/23/2023 Total Dissolved Solids (TDS) SM 2540 c-2015 301 mg/L 03/24/2023 Temperature SM 2550 B-2010 14.0 C 03/23/2023 pH SM 45Co H B-2011 6.4 units 03/23/2023 Total Organic Carbon (TOC) SM 5310 B.2014 19.3 mg/L 03/30/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/23/2023 Chloride SM4500 CI E-2011 40 mg/L 03/24/2023 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353 2, Rev. 2.0, 1993 0.05 mg/L 03/23/2023 Nitrate+Nitrite-Nitrogen EPA 3532. Rev 2.0, 1993 < 0.02 mg/L 03/27/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/04/2023 Report # 2023-05799 Page 7 of W SUBMIT FORM ON "-'LOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Albemarle Utility Company Permit Name (if different): Facility Address: 862 Holiday Island Rd Hertford NC Contact Person: Danny Shelton Perry ORC Well Location/Site Name: East of Spray Field Please Print Clearly or 27944 County Perquimans Telephone#: 252-426-1007 No. of wells to be sampled: 10 DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER. IURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 PERMIT Number: Expiration Date: 05-31-2025 Non -Discharge WQ0001817 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 8 Date sample collected: 3/23/2023 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH oo400: 5-8 units Temp. 000lo: 1 5.5 °C DRY at Depth to Water Level 82546: 5.0 ft. below measuring point Screened Interval: 5 ft. to 15 ft. Spec. Cond. 000sa: µMhos of timesampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: none check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan here: El Samples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified: ❑ YES ® NO Date sample analyzed:3/2312023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 _ PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.03 mg/L Pb - Lead olo51 ug/L Coliform: MF Fecal 31616 3 colonies /100mL Nitrate (NO3) as N 00620 0.09 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 405 mg/L Al - Aluminum oil o5 mg/L pH (Lab) 00403 5.8 units Ba - Barium 01007 ug/L TOC 00680 6.8 mg/L Ca - Calcium 00916 mg/L Chloride 00940 141 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron olo45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 < 0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.06-07-2018 F""' -- 77 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 , 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info4'-,znvironmentalchemists com Albemarle Utility Date of Report: Apr 05, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-05799 Project ID: Monitoring Wells Lab ID Sample 1D: Collect Date/Time Matrix Sampled by 23-14603 Site: MW-8 3/23/2023 11:05 AM Water Jay Baker Test Method Results Date Analyzed Color Color Clear/Tan 03/23/2023 Depth to water, ft. Depth to water. Ft. 5.0 feet 03/23/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0,1993 < 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/23/2023 Odor Qualitative None 03/23/2023 Total Dissolved Solids (TDS) SM 2540 c-2015 405 mg/L 03/24/2023 Temperature SM 2550 B-2010 15.5 C 03/23/2023 pH SM 4500 H B-2011 5.8 units 03/23/2023 Total Organic Carbon (TOC) SM 5310 B-2014 6.8 mg/L 03/24/2023 Fecal Coliform SM 9222 D-2015 MF 3 Colonies/100m L 03/23/2023 Chloride SM4500 Cl E-2011 141 mg/L 03/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0. 1993 0.03 mg/L 03/23/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 0.12 mg/L 03/27/2023 Nitrate Nitrogen Subtraction Method 0,09 mg/L 04/04/2023 Report M: 2023-05798 Page 8 of 10 SUBMIT FORM OP LOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Print Clearly or Type Facility Name: Albemarle Utility Company Permit Name (if different): Facility Address: 862 Holiday Island Rd Hertford NC 27944 County Perquimans act Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 Location/Site Name: West of Spray Field No. of wells to be sampled: 10 DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 PERMIT Number: Expiration Date: 05-31-2025 Non -Discharge WQ0001817 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED X Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 9 Date sample collected: 3/23/2023 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.3 units Temp. 000lo: 1 5.0 °C DRY at Depth to Water Level 82546: 6.4 ft. below measuring p g point Screened Interval: 4 ft. to 14 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: none check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan here:❑ Samples for metals were collected unfiltered: ❑ YES M NO and field acidified: ❑ YES © NO Date sample analyzed:3/23/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.02 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 8 colonies /100mL Nitrate (NO3) as N 00620 0.03 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 85.0 mg/L Al - Aluminum o11o5 mg/L pH (Lab) 00403 6.3 units Ba - Barium 01007 ug/L TOC 00680 4.1 mg/L Ca - Calcium 00916 mg/L _ Chloride 00940 5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) >pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Lamb - Corporate Secretary Permittee (or Authorized Apent) Name and Title - Please print or type GW-59 Rev.06-07-2018 enviroehe-m ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Albemarle Utility Date of Report: Apr 05, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-05799 Project 1D: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14604 Site: MW-9 3/23/2023 11:35 AM Water Jay Baker Test Method Results Date Analyzed Color color Clearlran 03/23/2023 Depth to water, ft. Depth to Water, Ft. 6.4 feet 03/23/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/23/2023 Odor Qualitative None 03/23/2023 Total Dissolved Solids (TDS) SM 2540 c-2015 85.0 mg/L 03/24/2023 Temperature SM 2550 B-2010 15.0 C 03/23/2023 pH SM 4500 H B-2011 6.3 units 03/23/2023 Total Organic Carbon (TOC) SM 5310 B-2014 4.1 mg/L 03/24/2023 Fecal Coliform SM 9222 D•2015 MF 8 Colonies/100mL 03/23/2023 Chloride SM4500 Cl E-2011 5 mg/L 03/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0. 1993 0.02 mg/L 03/23/2023 Nitrate+Nitrite-Nitrogen EPA 353.2. Rev. 2.0, 1993 0.05 mg/L 03/27/2023 Nitrate Nitrogen Subtraction Method 0.03 mg/L 04/04/2023 Report 0 2023-05799 Page 9 of 10 SUBMIT FORM ON Vim' LOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Albemarle Utility Company Permit Name (if different): Facility Address: 862 Holiday Island Rd Hertford N.C. Please Print Clearly or 27944 County Perquimans act Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 Location/Site Name: South of Spray Field No. of wells to be sampled: 10 DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER. )URCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 PERMIT Number: Expiration Date: 05-31-2025 Non -Discharge WQ0001817 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-10 Date sample collected: 3/23/2023 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH oo400: 6.0 units Temp. 000lo: 1 6.3 °C DRY at Depth to Water Level 82546: 9.0 ft. below measuring point Screened Interval: 5 ft. to 14 ft. Spec. Cond. 00094: µMhos time of sampling,check Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Tan here:❑ Samples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified: ❑ YES K NO Date sample analyzed:3/23/2023 Laboratory Name: Environmental Chemists„ Inc PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.02 Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 0.16 Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 )issolved Solids:Total 70300 415 mg/L Al - Aluminum of lo5 pH (Lab) 00403 6.0 units Ba - Barium 01007 TOC 00680 1.5 mg/L Ca - Calcium 00916 Chloride oo94o 152 mg/L Cd - Cadmium 01027 Arsenic 01002 ug/L Chromium: Total olo34 Grease and Oils 00552 mg/L Cu - Copper 01042 Phenol 32730 ug/L Fe - Iron 01045 Sulfate 00945 mg/L Hg - Mercury 71900 Specific Conductance 00095 µMhos K - Potassium 00937 Total Ammonia 00610 <0•2 mg/L Mg - Magnesium 00927 (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) _ Mn - Manganese 01055 TKN as N 00625 mg/L Ni - Nickel 01067 mg/L mg/L mg/L mg/L mg/L ug/L mg/L ug/L ug/L mg/L ug/L ug/L mg/L mg/L ug/L ug/L Pb - Lead o1o51 Zn - Zinc 01092 Certification No. 94 ug/L mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 method # method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Lamb Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 Environmental Chemists, Inc. • 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab � 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255•A Wilmington Highway, Jacksonville, NC 28540 - 910.347,5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infoia,:environmentalchemists.com Albemarle Utility Date of Report: Apr 05, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-05799 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14605 Site: MW-10 3/23/2023 11:20 AM Water Jay Baker Test Method Results Date Analyzed Color Color Tan 03/23/2023 Depth to water, ft. Depth to water, Ft. 9.0 feet 03/23/2023 Ammonia Nitrogen EPA 350.1, Rev 2.0, 1993 < 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/23/2023 Odor Qualitative None 03/23/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 415 mg/L 03/24/2023 Temperature SM 2550 B-2010 16.3 C 03/23/2023 pH SM 4500 M B-2011 6.0 units 03/23/2023 Total Organic Carbon (TOC) SM 5310 B-2014 1.5 mg/L 03/24/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100mL 03/23/2023 Chloride SM4500 C1 E-2011 152 mg/L 03/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2, Rev 2.0, 1993 0.02 mg/L 03/23/2023 Nitrate+Nitrite-Nitrogen EPA 353.2. Rev. 2.0, 1993 0.18 mg/L 03/27/2023 Nitrate Nitrogen Subtraction Method 0.16 mg/L 04/04/2023 Comment: { -. Reviewed by: fi"� ✓ Report t1:: 2023-05799 Page 10 of 10 GW-59A COMPLIANCE REPORT FORM Permit #Wi%,� 001) / 3 I (Submit one each monitoring period with GW-59 forms.) 1 Enter date monitoring results were due. ( 1Y -30 .Z31 Will this monitoring report (GW-59 and GW-59A) YES be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES NO IF the answer to question 1 or 2 is "YES'; list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YE NO identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is "NO'; skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: Z-.Pki 1 it 70 5 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YE NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is `NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentrations) reported, and sample collection for each occurrence (for the last two years). -�date —S - 4 ci C 1-) -cj S b -oit— Are the monitoring wells listed in section 5 located at or beyond the review boundary? YE NO If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES'; describe those actions in the space provided below. If the answer to question 7 is "NO'; contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report is true and complete to the best of my knowledge. �GW--59�A)) Oignature of ermittee (or Authorized Agent) nate GW-59A 12/8/2003 0to P4 �i -- $7,9 67 -6 3 /0 Y�r o 7/ 5- i—c uj PH 3 57, :9 6, 2, -57 S> 7 L d D -5-7 w LC* Lam: PH 37 z__Ll, "-c: P 4: 45 jvt Ale) ,evil