NC0088838_Correspondence_20151222

SFRSC
Chemical Solutions
a division of Radiator Specialty Company
December 22, 2015
Central Files
North Carolina Department of Environment
and Natural Resources
Division of Water Quality
Water Quality Section
1617 Mail Service Center
Raleigh, North Carolina 27699
RE: November 2015 Discharge Monitoring Report
Radiator Specialty Company
Indian Trail, Union County, North Carolina
Permit No. NCO088838
Dear Sirs:
Radiator Specialty Company (RSC) respectfully submits for your review, two
copies of its November Discharge Monitoring Report (DMR) as required by Part II
Section D.(2) of National Pollutant Discharge Elimination System (NPDES) Permit No.
NC0088838.
On August 5, 2014, Mr. Ron Berry of the North Carolina Department of
Environment and Natural Resources Division of Water Quality contacted RSC via email
to discuss RSC's NPDES Permit Number NCO088838 renewal. The new permit will
require RSC to sample its effluent for 1,4-Dioxane with a reporting concentration of 80
µg/L. The current analytical method utilized by RSC, Standard Method 624, does not
target 1,4-Dioxane. As a result, in an August 11, 2014 telephone conversation, Mr. Ron
Berry authorized RSC to immediately implement a change in the analytical procedure
defined in the permit from EPA Method 624 to SW-846 Method 8260 to target 1,4-
Dioxane. RSC implemented this analytical method change during the August 2014
monthly sampling event to collect and evaluate 1,4-Dioxane analytical results.
The Method Reporting Limit for SW-846 Method 8260 is 150 jig/L. Prism
Laboratories, Inc. has indicated that a normal Method Detection Limit for SW-846
Method 8260 is 10.6 µg/L. Should 1,4-doxane be detected in the effluent sample at a
concentration between the permit limit and 150 µg/L, the result would be reported as a
"J" value.
600 Radiator Road — Indian Trail, NC 28079-5225 — Telephone: [phone] — Fox: 704-684-1975 — www.rscbrands.com

Central Files
December 22, 2015
Page 2
The analytical results associated with the November 24, 2015 sample indicated
the presence of 1,4-Dioxane at an estimated (J value) concentration of 97 micrograms per
liter (ug/L). RSC proposes to confirm these results utilizing the analytical data associated
with the December effluent sample collected on December 15, 2015. These results will
be presented in the December DMR to be submitted in January 2016.
Radiator Specialty Company appreciates the North Carolina Department of
Environment and Natural Resources cooperation and assistance in this matter. If you
have any questions or require additional information, please call me at [phone].
Sincerely,
Radiator Specialty Company
Stuart A. Kerkhoff
Operator in Responsible Charge
NPDEMNOVEMQER20I S.DOC

EFFLUENT
NPDES PERMIT NO. NCO088838 DISCHARGE NO._001_ MONTH —November— YEAR_2015
FACILITY NAME Radiator Specialty Company CLASS_C_ COUNTY —Union —
CERTIFIED LABTORY (1) CERTIFICATION NO.
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC)_ Stuart Kerkhoff GRADE_PC-1 CERTIFICATION NO._993806_
PERSON(S) COLLECTING SAMPLES ORC PHONE_(704) 684-1815
CHECK BOX IF ORC HAS CHANGED NO FLOW / DISCHARGE FROM SITE "
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
BY THIS SIGNATURE. I CERTIFY TIiATTHIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
MR
MUM
©MMn©
mn©
_E'
©_-_
lcrmn©
®IMM®MIMMM
lmmnm
mm-_
m_-_
m'
EMM"
mIMMM©
momn©
mEMM©IMIMMMM
m_-_
m_-_MEMnm
mmOMM
®=3=©
m_-©
mIMMU®
m_-_
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J: Detected but below the Reporting Limit, therefore, result is an estimated concentration (CLP J-Flag).
DWQ Form MR-I.I (11/04)

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable) .
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the
permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations."
Stuart Kerkhoff
Permittee (Please print or type)
/2
Signature of Permittee*** Date
(Required unless submitted electronically)
600 Radiator Road, Indian Trail, NC 28079 [phone] [e-mail] 10/31/2013
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2) Certification No.
Certified Laboratory (3)
Certified Laboratory (4)
Certified Laboratory (5)
PARAMETER CODES
Certification No.
Certification No.
Certification No.
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/was and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and. as a result. there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
'Signature of Permittee: if signed by other than the permitter. then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
Page 2

NC Certification No. 402 Case Narrative
Full -Service Analytical 8
Environmental Solutions
AlkaLw
SC Certification No. 99012
NC Drinkinq Water Con No. 37735 12/09/2015
VA Certification No. 460211
DoD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-B Accredited Certificate No. L2307
Radiator Specialty Co Project: NPDES Monthly
Stuart Kerkhoff
600 Radiator Rd. Lab Submittal Date: 11/24/2015
Indian Trail, NC 28079 Prism Work Order: 5110484
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are Flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
V�e� a_. ?�_
RobbiA.Jones
President/Project Manager
Data Qualifiers Key Reference:
DEC 15 2015 [
Reviewed By Robbi A. Jones
President/Project Manager
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced,except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road -P.O. Box 240543 - Charlotte. NC 26224-0543
Phone: [phone]- Toll Free Number: 1.8001529.6364-Fax: [phone] Page 1 0f 6

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IN Rk ISM I Full -Service Analytical &
Environmental Solutions
LABORATORIES INC
Sample Receipt Summary
12/09/2015
Prism Work Order: 5110484
Client Sample ID
Lab Sample 1D
Matrix
Date Sampled
Date Received
Outfall 001
5110484-01
Water
11 /24/15
11 /24/15
Samples were received in good condition at 2.3 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Tall Free Number: 1-8001529.6364 - Fax: [phone] Page �R6

r
Laboratory Report
ismFutl-Service Analytical 8 Environmental Solutions12/09/2015
Radiator Specialty Co Project: NPDES Monthly Client Sample ID: Outfall 001
Attn: Stuart Kerkhoff Prism Sample ID: 5110484-01
600 Radiator Rd. Prism Work Order: 5110484
Indian Trail, NC 28079 Sample Matrix: Water Time Collected: 11/24/15 08:19
Time Submitted: 11/24/15 15:05
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Total Suspended Solids
BRL
mg/L
2.6
0.80
1
ISM 2540 D
11/25/15 11:40
EGC
P5K0532
Volatile Organic Compounds by GC/MS
1,1,1-Trichloroethane
BRL
ug/L
4.0
0.061
1
8260B
12/3/15 21:19
KDM
P51.0081
1,4-Oloxane
97 j
ug/L
150
14
1
8260B
1213115 21:19
KDM
P51-0081
Tetrachloroethylene
0.80 J
ug/L
3.0
0.098
1
8260B
1213115 21:19
KOM
P51-0081
Vinyl chloride
BRL
ug/L
2.0
_ 0.097
- 1 _
8260B
12/3/15 21:19
KDM
P5L0081
Dibromofluoromethane 107 % 75-129
Toluene-d8 95 /0 77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] Toll Free Number:1-8001529-6364 - Fax: [phone] Page 3.of 6

LWIR
Ism
Full -Service Analytical &
I Environmental Solutions
ADO[MC
Radiator Specialty Co Project: NPDES Monthly
Attn: Stuart Kerkhoff
600 Radiator Rd.
Indian Trail, NC 28079
Volatile Organic Compounds by GC/MS - Quality Control
Level II QC Report -
12/9/15
Prism Work Order: 5110484
Time Submitted: 11/24/2015 3:05:00PM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P51-0081 - 5030B
Blank (1351-0081-131-K1)
------ --- ------ - ---.. .
-
Prepared & Analyzed: 12/03/15
,1,1-Trichlorcethane
BRL
4.0
ug/L
1,4-Oioxane
BRL
150
ug/L
Tetrachloroethylene
BRL
3.0
ug/L
Vinyl chloride
BRL
2.0
ug/L
Surrogate: Dibromonuoromethane
52.3
ug/L
50.00 105
75-129
Surrogate: Toluene-d8
48.2
ug/L
50.00 96
77-123
LCS (PSL0081_BS1) __- - -�
- -
Prepared & Analyzed: 12/03/15
1.1,1-Trichlorcethane
22.2
4.0
ug/L
20.00 111
-
75-136
1,4-Dioxane
1.00E9
150
ug/L
200.0 NR
70-130
Tetrachloroethylene
19.7
3.0
ug/L
20.00 99
80-129
Vinyl chloride
23.8
2.0
ug/L
20.00 119
57-141
Surrogate: Dibrornonuoromethane
52.0
u92
50.00 104
75-129
Surrogate: Toluene-0
49.2
ug/L
50.00 98
77-123
LCS Dup (1251-0081-13SD1)
Prepared & Analyzed: 12/03/15
1,1,1- dchloroethane
21.2
4.0
ug/L
20.00 106
75-136 5
20
1,4-Oioxane
1.00E9
150
ug/L
200.0 NR
70-130 0
20
Tetrachloroethylene
19.2
3.0
ug/L
20.00 96
80-129 2
20
Vinyl chloride
23.9
2.0
ug/L
20.00 120
57-141 0.4
20
Surrogate: Dibromonuorornethane
50.8
ug/L
50.00 102
75-129
Surrogate: Toluene-d8
48.1
ug/L
50.00 96
77-123
This report should not be reproduced. except in its entirety. without the written consent of Prism Laboratories. Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number:1-8001529.6364 - Fax: [phone] :4:of G P� 8,=
9...

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'nAnalyticalI Environmental SolutionsVLABORIIORIM WC.
Radiator Specialty Co
Attn: Stuart Kerkhoff
600 Radiator Rd.
Indian Trail, NC 28079
General Chemistry Parameters - Quality Control
Analyte
Project: NPDES Monthly
Level II QC Report
12/9115
Prism Work Order: 5110484
Time Submitted: 11/24/2015 3:05:00PM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P51<0532 - NO PREP
Blank (P5K0532-BLK1) _...___ _ ...... Prepared 8 Analyzed: 11/25/15
Total Suspended Solids BRL 5.0 mg/L
LCS (PSK0532-BS1) Prepared & Analyzed: 11/25/15
Total Suspended Solids 490 5.0 mg/L 477.0 103 90-110
Sample Extraction Data
Prep Method: 5030E
Lab Number Batch Initial Final Date/rime
5110484-01 P51-0081 10 mL 10 mL 12/03/15 8:08
This report should not be reproduced, except in its entirety. without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 _ 11
Phone: [phone] - Toll Free Number: 1.8001529-6364 - Fax: [phone] ` Add '.A . r,.3

PR I S M I Full -Service Analytical AT Environmental Solutions
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449 Springbrook Road • Charlotte, NC 28217
Phone [phone] Fax: [phone]
Client Company Name: 'Lt �,c.4o! S, YL; A /L, L
Report To/Contact Name: _S-h4R E-
Reporting Address: G CJU i2r�ri14, 1) A
Email Address: 3 k,
EDD Type: PDF ✓Er
Site Location Name:
Site Location Physical
CLIENT I DATE
SAMPLE DESCRIPTION I COLLECTED
TIME
COLLECTED
MILITARY
HOURS
Sampler's Signature Z( LCL� /(}p
Upon relinquishing, this Chain of Cuslo
subalitted In writing to the Prism Projet: M
elinq, is it Sy. ( Ignatyrr I
ReIvWished By: (Slgnatury
RP nq etl By. (Signature)
Mellrod of ShipmanL NOTE: A L SAMPLE CO LER ;
SAMPLES ARE NOT ACCEPTED
OFed F. ❑IIP6 nu....n n_:.._-_.
MATRIX
(SOIL,
WATER OR
SLUDGE)
W
CHAIN OF CUSTODY RECORD
PAGE!/IOF / QUOTE s TO ENSURE PROPER BILLINGI
Project Name: I� ��I I� L
Short Hold Analysis: (Yes) UST Project: (Yes) (�
*Please ATTACH any project specific reporting (QC LEVEL 1 II III IV)
provisions and/or QCgqRequire mgnts 1
Invoice To: _ .Ai G L i'y {�c, L 7 `
Address: t"0 ,i ,.c ,r R,I
Purchase Order No./Billing Reference 75.0 —L 3 0O7
Requested Due Date O i Day 112 Days ❑ 3 Days O 4 Days ❑ 5 Days
"Working Days" O 6-9 Days G13iandard 10 days O RushPle-Work Must Be
Samples received after 14:00 will be processed next business day.
pproved
Turnaround time Is based on business days. excluding weekends and holidays.
(SEE REVERSE FOR TERMS S CONDRIONS REGARDING SERVICES
RENDERED BY PRISM LABORATORIES. INC. TO CLIENT)
SAMPLE CONTAINER AN
PRESERVA• (-J
'TYPE NO. If
TIVES Lj ,
SEE BELOW
VOA
VOA
'_ I Sampled By (Print Name) -) t(Av e f
authorization for Prism to proceed with the a
There will be charges for any changes after
LABORATORY.
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Samples INTACT upon arrival?
Received ON WET ICE?
PROPER PRESERVATIVES nulicalo-tn
Received WIl IIIN I IOLDING Nf/.CS4
CUSTODY SEALS INTACT?
VOLATILES ,e:'u WiOUT HEADSPA!:'_v
PROPER CONTAINERS u,.,sJ7
TEMP: Thrni. 10 vA T--.7 .,,. ....
1''S NO N!A
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification: NELAC_ DoD_ FL_ NC
SC_ OTHER N/A
Water Chlorinated: YES_ NOS
Sample Iced Upon Collection: YES ZNO_
U
&!2L IAffiliation
as requested above. Any changes must be
s have been Initialized.
/
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PRISM
/ REMARKS Lqg
ID NO.
Comments:
F irld No, Fce•
P II i19c•
❑ C SC
❑ NC El
❑ NC ❑ SC
❑ NC ❑ SC
..r+olc:
❑ NC ❑ SC
ncKA:
CERCLA
LANDFILL
OTHER:
❑
❑
❑
❑ NC
❑ SC
CI NC ❑ SC
❑ NC ❑ SC
❑ NC ❑ SC
'CONTAINER TYPE CODES: A = Amber
❑
C = Clear G= Glass
❑ ❑
P = Plastic; TL = Teflon -Lined Cap
❑ O
VOA = Volatile Organics Analysis (Zero Head Space)