WQ0001817_Monitoring - 11-2022_20231027

Monitoring Report Submittal
Permit Number#*
Name of Facility:*
Month: * November
Report Information
Type *
Revised - GW-59
Confirmation Email Address:
Name of Submitter: *
Signature:
Date of submittal:
Initial Review
WQ0001817
Albemarle Utility Company
Year:* 2022
Upload Document*
November 2022 MW's revised.pdf 26.23MB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
[e-mail]
Danny S Perry
Reviewer: Wanda.Gerald
10/27/2023
This will be filled in automatically

Is the project number correct?* WQ0001817
Is the monitoring report accepted?* Yes No
Regional Office* Washington
Reviewer: _anonymous
Review Date: 10/30/2023

SUBMIT FORM ON _ 3W PAPER ONLY
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
..
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 05-31-2025
Facility Name: Albemarle Utility Comapany
Non -Discharge WQ0001817 UIC
NPDES Other
Permit Name (if different):
Facility Address: 862 Holiday Island RD
TYPE OF PERMITTED OPERATION BEING MONITORED
Hertford N.0
27944
County Perqimans
❑■ Lagoon ❑ Remediation: Infiltration Gallery
K Spray Field ❑ Remediation:
Contact Person: Danny Shelton Perry ORC
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: North of Holding Lagoon
No. of wells to be sampled: 10
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW -1
Date sample collected: 11/17/2022
FIELD ANALYSES:
WAS
Well Depth: 20 ft.
Well Diameter: 2 in.
pH 00400: 5.3 units Temp. 000io: 17.6 °C
DRY at
Depth to Water Level 82546:13.3 ft. below measuring point Screened Interval: -5 ft. to
-20 ft. Spec. Cond. 00094: µ
time ofMhos sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
5•0
gallons
Appearance Tan
here:❑
Samples for metals were collected unfiltered: ❑ YES
M NO and field acidified: ❑ YES ® NO
LABORATORY INFORMATION
Date sample analyzed:11/17/2022
Laboratory Name: Environmental Chemists, Inc Certification No. 94
PARAMETERS NOTE: Values should reflect
dissolved
and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.05
mg/L
Pb - Lead o1051 ug/L
Coliform: MF Fecal 31616 <2
/100mL
Nitrate (NO3) as N 00620 0.46
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 320
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 5.3
units
Ba - Barium 01007
uglL
TOC 00680 4.6
mg/L
Ca - Calcium 00916
mg/L
Chloride oo94o 10
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia 00610 <0•2
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total)
Mn - Manganese oio55
ug/L , method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: _
Shayne Lamb Corporate Secretary
Permittee (or Authorized Agent) Name and Title - Please print or type
mg/L Effluent Total VOCs:
yy �mg/AAL+�� VOC Removal%
L- _..... - -
V
GW-59 Rev.06-07-2018

Environmental Chemists, Inc.
envirochem A
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ° 910.392.44:24 1,;1x
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
v
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
into(uenvironmentalcliemists.com
Albemarle Utility
Date of Report: Dec 06, 2022
862 Holiday Island Road
Customer PO #:
Hertford NC 27944
Customer ID: 09110024
Attention:
Report #: 2022-23081
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-56757 Site: MW-1
11/17/2022 11:20 AM Water Jay Baker
Test
Method Results Date Analyzed
Color
color
Tan
11/17/2022
Depth to water, ft.
Depth to water, Ft.
13.3 feet
11/17/2022
Ammonia Nitrogen
EPA350.1, Rev. 2.0,1993
0.2 mg/L
12/01/2022
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
11/17/2022
Odor
Qualitative
None
11/17/2022
Total Dissolved Solids (TDS)
SM 2540 c-2015
320 mg/L
11/19/2022
Temperature
SM 2550 B-2010
17.6 C
11/17/2022
pH
SM 4500 H B-2011
5.3 units
11/17/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
4.6 mg/L
11/29/2022
Chloride
SM4500 CI E-2011
10 mg/L
11/21 /2022
1,1,1,2-Tetrachioroethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
1, 1, 1 -Trichloroethane
SW 846 Method 826OD/5030B
<0, 5 pg/L
11/22/2022
1,1,2,2-Tetrachioroethane
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
1,1,2-Trichloroethane
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/22/2022
1,1-Dichloroethane
SW 846 Method 626OD/5030B
<0.5 pg/L
11/22/2022
1, 1 -Dichloroethene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
1,1-Dichloropropene
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
1,2,3-Trichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11 /22/2022
1,2,3-Trichloropropane
SW 846 Method 826OD150308
<0.5 pg/L
11/22/2022
1,2,4-Trichlorobenzene
SW 846 Method 826OD15030B
<Q 5 pg/L
11/22/2022
1,2,4--Trimethylbenzene
SW 846 Method 8260015030B
<0.5 pg/L
11/22/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,2-Dibromoethane
SW 848 Method 826OD/5030B
<0.5 pg/L
11/22/2022
1,2-Dichlorobenzene
SW 846 Method 82600/5030B
<0,5 pg/L
11/22/2022
1,2-Dichloroethane
SW 846 Method 8260015030E
<0.5 pg/L
11/22/2022
1,2-Dichloropropane
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Page 1 of 32 ..§
Report #. 2022-23081

Environmental Chemists, Inc.
nvirochem 6602 Windmill Way, Wilmington, NC 28405 • 91.0.392.0223 Lab • 91.0.392.4424 Fax
!7:: 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910,347,5843 Lab/Pax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Albemarle Utility
Date of Report: Dec 06, 2022
862 Holiday Island Road
Customer PO #:
Hertford NC
27944
Customer ID: 09110024
Attention:
Report #: 2022-23081
Project ID: Monitoring Wells
1,3,5-Trimethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
1,3-Dichlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
1,3-Dichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
2,2-Dichloropropane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
2-Chlorotoluene
SW 646 Method 8260D/5030B
<0.5 pg/L
11/22/2022
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Benzene
SW 846 Method 8260D/50306
<0.5 pg/L
11/22/2022
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Bromochloromethane
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
Bromodichloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
Bromoform
SW 846 Method 826013/50306
<0.5 pg/L
11/22/2022
Bromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
Carbon tetrachloride
SW 646 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Chlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Chloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
Chloroform
SW 846 Method 826OD/50306
<0.5 pg/L
11/22/2022
Chloromethane
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
cis-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
cis-1,3-Dichloropropene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Dibromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Dibromomethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11 /22/2022
Dichlorodifluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Cthylbenzene
SW 846 Method 8260015030B
<0.5 pg/L
11/22/2022
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Isopropyl benzene
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
M+P Xylene
SW 846 Method 826OD/5030B
<1.0 pg/L
11/22/2022
Methylene chloride
SW 646 Method 8260D/50308
<0.5 pg/L
11/22/2022
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
,'eport # 2022-23081 Page 2 of 32

Environmental Chemists, Inc.
��,.envirochem 16602 Windmill Way, Wilmington, NC 28405 • 91.0.392.0223 Lab • 9.10.392.4424 i-ax
311 710 Bowsertown Road, Manteo, NC 279.54 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Albemarle Utility
862 Holiday Island Road
Hertford NC
Attention:
27944
Date of Report: Dec 06, 2022
Customer PO #:
Customer ID: 09110024
Report #: 2022-23081
Project ID: Monitoring Wells
n-Propylbenzene
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
ortho-Xylene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
sec -Butyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
Styrene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
tert-B utyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Tetrachloroethene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Toluene
SW 846 Method 826013/503013
<0.5 pg/L
11/22/2022
Trans- 1,2-Dichloroethene
SW 846 Method 82600150308
<0.5 pg/L
11/22/2022
Trans- 1,3-dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Trichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
Trichlorofluoromethane
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
Vinyl chloride
SW 845 Method 8260D/5030B
<0.5 pg/L
11 /2212022
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.05 mg/L
11 /18/2022
Nitrate+ Nitrite-N itrogen
EPA353.2, Rev.2.0, 1993
0.51 mg/L
11/22/2022
Nitrate Nitrogen
Subtraction Method
0.46 mg/L
12/05/2022
Report #:: 2022-23081 Page 3 of 32

SUBMIT FORM ON " OW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name: Albemarle Utility Company
Permit Name (if different):
Facility Address: 862 Holiday Island Rd
Hertford NC
)ntact Person: Danny Shelton Perry ORC
ell Location/Site Name: East of Baffle Lagoon
Please Print Clearly or Type
27944
WELL ID NUMBER (from Permit): MW-2
Well Depth: 12 ft.
Depth to Water Level 82546: 4.5 ft. below measuring point
Measuring Point is 3 ft. above land surface
Volume of water pumped/bailed before sampling: 4.0
Samples for metals were collected unfiltered: ❑ YES M
County Perquimans
Telephone#: [phone]
No. of wells to be sampled: 10
Date sample collected: 11 /17/2022
Well Diameter: 2 in.
Screened Interval: -2 ft.
Relative M.P. Elevation:
gallons
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
PERMIT Number:
Expiration Date: 05-31-2025
Non -Discharge WQ0001817
UIC
NPDES
Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑■ Lagoon
❑ Remediation: Infiltration Gallery
❑■ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
to -12 ft.
ft.
NO and field acidified: ❑ YES ® NO
FIELD ANALYSES:
pH 00400: 5.0 units
Spec. Cond. 00094:
Odor 00085: none
Appearance Tan
If WELL
Temp. 000lo: 1 8.3 °C DRY at
uMhos I time of
here:❑
Date sample analyzed: 11 /17/2022
Laboratory Name: Environment Chemists, Inc
Certification No. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.06
mg/L
Pb - Lead olo51 ug/L
Coliform: MF Fecal 31616 <2 colonies
/100mL
Nitrate (NO3) as N 00620 1.33
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 296
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 5.0
units
Ba - Barium 01007
ug/L
TOC 00680 12.8
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 28
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia o0810 0.2
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
, method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs: mg/L
Effluent Total VOCs: mg/L VOC Removal%
Ticertify that, to, the best of my knowledge and belief� the information
DWR-cerfifed laboratory. I am aware that there are significant
submitted
penalties
in this report is true. accurate, and complete, and that the
for submitting false information, including the possilbili�y o fines
laboratory
and imprisonmen�
analytical data was p,oduced using approved methods of analysis by a
for ,nc,,1mg iolations.
a/
Shayne Lamb Corporate Secretary
Permittee (or Authorized Aqent) Name and Title - Please print or type Siqnature of Permittee (oT Authorized Agenta
GW-59 Rev.06-07-2018

[,env rochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab ° 910.392.4424 l ax
710 Howsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax
255-A Wilmington Ifighway, Jacksonville, NC 28540 • 910,347.5843 Lab/Fax
info(a,)environ men talchemists.com
Albemarle Utility Date of Report: Dec 06, 2022
862 Holiday Island Road Customer PO M
Hertford NC 27944 Customer ID: 09110024
Attention: Report M 2022-23081
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-56758 Site: MW-2 11/17/2022 11:35 AM Water Jay Baker
Test Method Results Date Analyzed
Color
Color
Tan
11/17/2022
Depth to water, ft.
Depth to water, Ft.
4.5 feet
11/17/2022
Ammonia Nitrogen
EPA 350.1, Rev. 2 0, 1993
0.2 mg/L
12/01/2022
Gallons bailed before sampling
Gallons Bailed before sampling
4.0 gallons
11/17/2022
Odor
Qualitative
None
11/17/2022
Total Dissolved Solids (TDS)
SM 2540 c-2015
296 mg/L
11/19/2022
Temperature
SM 2550 B-2010
18.3 C
11/17/2022
pH
SM 4500 H B-2011
5.0 units
11/17/2022
Total Organic Carbon (TOC)
SM 5310 6-2014
12.8 mg/L
11/29/2022
Chloride
SM4500 Cl E-2011
28 mg/L
11/21 /2022
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
1, 1, 1 -Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,1,2,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
1,1,2-Trichloroethane
SW 846 Method 82600/5030B
<0.5 pg/L
11 /2212022
1,1-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,1-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1, 1 -Dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
1,2,3-Trichlorobenzene
SW 846 Method 8260D/50308
<0.5 pq/L
11/22/2022
1,2,3-Trichloropropane
SW 846 Method 8260D/50308
<0.5 pg/L
11 /22/2022
,1,2,4-Trichlorobenzene
SW 846 Method 8260D/5030B
<0, 5 pg/L
11/22/2022
1,2,4-Trimethylbenzene
SW 846 Method 826OD150308
<0.5 pg/L
11 /2212022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/50308
<0.5 pg/L
11 /22/2022
1,2-Dibromoethane
SW 846 Method 826OD15030B
<0, 5 pg/L
11/22/2022
1,2-Dichlorobenzene
SW 846 Method 8260D/50306
<0.5 pg/L
11/22/2022
1,2-Dichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
1,2-Dichloropropane
SW 846 Method 8260D/50306
<0.5 pg/L
11/22/2022
Report*: 2022-23081 Page 4 of 32

Environmental Chemists,
—
660zWindmill Way, Wilmington, N[20405 * 910.392.0223Lah ° 910.3e2.24424Fox
r/OoowsermwnRoad, Manun'NC2r95« ^ 252,4735702Luh/;mx
255'AWilmington Highway, Jacksonville, NCz8540 ^ 918347-50433L,b/l'xx
ANALYTICAL uCONSULTING CHEMISTS
io6o@Vcn,i,onmoo/a|u`omio,xzom
Albemarle Utility
Date of Report: Dec O8.2022
862 Holiday Island Road
Customer PO#:
Hertford NC 27944
Customer ID: 09110024
Attention:
Rapmnt#: 2022'23081
Project ID: Monitoring Wells
1.3.5-Trimmthy|benzene
»w»*«Method »es»om«»oa
<0.5pg/L
11/22/2022
1.3-Oioh|orobenzeno
ow**»Method »u«»msoo»o
<0.5pg/L
11/22/2022
1.3'Dich|nnopnopana
uw»^«Method ous»o/«»o»o
<0.5pg/L
11/22/2022
1.4-Oich|onobenzene
owe"«Method »u«»m»»»»o
<0.5pg/L
11/22/2022
2.2-D/ch|oropnopane
»w»^»Method az««mn«oou
°0.5pg/L
11/22/2022
2'Ch|orotV|uene
nw»*»Method mo»om»»»»
<0.5pg/L
11/22/2022
4-Ch|PnobJ|uena
uw«*«Method »:«oom»»»e
^0.5pg/L
11/22/2022
Benzene
«««w^«Method oun»»/5»»»u
<0.5pg/L
11/22/2022
Bnomoba»zena
ew»^oMethod «:m»m««a»o
<0,5pg/L
11/22/2022
Bnumooh|oromathane
aw»eMethod »26Ooa«3mo
<O.Spg/L
11/22/3022
Bnomodich|onomathane
aw8w«Method u2m»om«aoa
<0.5pQ/L
11/22/2022
B»omofurm
mm»*«Method »c««m»»»«»
<05pg/L
11/22/2022
Bromomethone
aw»4«Method »:o»ma«»»e
<0.5pg/L
11/22/2022
Carbon tetrachloride
»w»4*Method »«««na»»»u
x0.5pg/L
11/22/2022
Ch|urobenzene
aw/weMethod «x«»m»«»»e
<0.5pg/L
11/22/2022
Ch}oroeMhane
ewn*«Method »2««om»»«m
<0.5pg/L
11/22/2022
Chloroform
owowMethod aun«m»«a»o
xO.bpg/L
11/22/2022
Ch|oromethene
owmnMethod »z«»om»o»o
<0.5pg/L
11/22Q022
cis- 1.2-Dich|onoetheno
mw»^»Method a2m«c»s»o»e
<0.5Ug/L
11/22/2022
cis- 1.3-Oich|onopnopene
»w8w«Method «2m»nm»o«a
<0.5pg/L
11/22/2022
Dibnomooh|nromethono
»wa*sMethod «a»«m5«»»u
<0.5pg/L
11/22/2022
Dib»omommthane
aw»^«Method oum»m«»u«»
<0.5pg/L
11/22/2022
Oich|orodiOuononmethane
swowsMethod «um«os»»»o
^ <8.5pg/L
11/22/2022
Ethy|banzene
»ww«Method «oo«m»»x»a
«0.6pQ/L
11/22/2022
Hexooh|orobutsdieno
»w»*nMethod «»mmo»mo
«0.5pg/L
11/22/2022
|aopnnpy|benzene
uwm«Method »uo»m»ua»o
<D.Spg/L
11/22/2022
K8+pXy|ene
nw»*«Method »2n»os»a»o
<1 Opg/L
11/22/2022
Methylene chloride
»w»*eMethod »m»om«mo
«05pg/L
11/22/2022
Naphthalene
»w»*»Method »cs»ua»»»u
<0.5pg/L
11/22/2022
n'Buty|benoene
aw»^aMethod «u«»oan»»o
<0.5Ag/L
11/22/2022

a •• a
`M
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 a 910,392.0223 Lab a 910.392.4424 Faix
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, INC 28540 a 910.347.5843 Lab/Fax
[e-mail]
Albemarle Utility
Date of Report: Dec 06, 2022
862 Holiday Island Road
Customer PO #:
Hertford NC
27944
Customer ID: 09110024
Attention:
Report #: 2022-23081
Project ID: Monitoring Wells
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
ortho-Xylene
SW 846 Method 8260015030B
<0.5 pg/L
11 /22/2022
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
sec -Butyl benzene
SW 846 Method 8260D/5030B
<0, 5 pg/L
11/22/2022
Styrene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
tert-Butylbenzene
SW 846 Method 8260D/5030B
<0,5 pg/L
11/22/2022
Tetrachloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022.
Toluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Trans- 1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Trans-1,3-dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Trichloroethene
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
Trichlorofluoromethane
SW 846 Method 826013/50308
<0.5 pg/L
11/22/2022
Vinyl chloride
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 0.06 mg/L 11/18/2022
Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 1.39 mg/L 11/22/2022
Nitrate Nitrogen Subtraction Method 1.33 mg/L 12/05/2022
Report #. 2022-23081 Page 6 or 3 � n-

SUBMIT FORM ON _ DW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Please Print Clearly or Type
Facility Name: Albemarle Utility Company
Permit Name (if different):
Facility Address: 862 Holiday Island Rd
Hertford NC 27944
IContact Person: Danny Shelton Perry ORC
Well Location/Site Name: South East of Spray field
County Perquimans
Telephone#: [phone]
No. of wells to be sampled: 10
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
:RMIT Number: Expiration Date: 05-31-2025
in -Discharge WQ0001817 UIC
'DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑■ Lagoon ❑ Remediation: Infiltration Gallery
N Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): MW - 3 Date sample collected: 11/17/2022
Well Depth: 12 ft. Well Diameter: 2 in.
Depth to Water Level 82546: 8.0 ft. below measuring point Screened Interval: -2 ft. to
Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft.
Volume of water pumped/bailed before sampling: 2 gallons
Samples for metals were collected unfiltered: ❑ YES NO and field acidified: ❑ YES ® NO
-12 ft.
FIELD ANALYSES:
pH 00400: 5.9 units Temp. 00olo: 18.20C
Spec. Cond. 00094: µMhos
Odor 00085: none
Appearance Brown
If WELL
WAS
DRY at
time of
sampling,
check
here:❑
LABORATORY INFORMATION
Date sample analyzed:11/17/2022
Laboratory Name: Environmental Chemists, Inc
Certification No. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.07
mg/L
Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 <10 colonies
/100mL
Nitrate (NO3) as N 00620 0.69
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 1190
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 5.9
units
Ba - Barium 01007
ug/L
TOC 00680 22.2
mg/L
Ca - Calcium 00916
mg/L
Chloride oo94o 9
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 2.3
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total)
Mn - Manganese oio55
ug/L
, method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Shayne Byrum - Corporate Secretary
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.06-07-2018

rip"
,
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Wi.ndm.ill Way, Wilmington, NC 28405 * 910.392.0223 Lab = 910.392.4424 i'D\
710 Bowsertown Road, Manteo, NC '279,54 • 252.473.5702 Lab/Fax
255-A Wilmington IIighway, Jacksonville, NC 28540 ,d 910.347.5843 I-air/fax
info(4ilenviTOT) mentalchelnists.com
Albemarle Utility
Date of Report: Dec 06, 2022
862 Holiday Island Road
Customer PO #:
Hertford NC 27944
Customer ID: 09110024
Attention:
Report #: 2022-23081
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by-
22-56759 Site: MW-3
11/17/2022
11:50 AM Water Jay Baker
Test
Method
Results
Date Analyzed
Color
Color
Brown
11/17/2022
Depth to water, ft.
Depth to Water, Ft.
8, 0 feet
11/17/2022
Ammonia Nitrogen
EPA 350.1, Rev, 2.0, 1993
2.3 mg/L
12/01/2022
(gallons bailed before sampling
Gallons Bailed before sampling
2(dry) gallons
11/17/2022
Odor
Qualitative
None
11/17/2022
- Total Dissolved Solids (TDS)
SM 2540 C-2015
1190 mg/L
11 /19/2022
Temperature
SM 2550 B-2010
18.2 C
11/17/2022
pH
SM 4500 H B-2011
5.9 units
11/17/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
22.2 mg/L
11/29/2022
Chloride
SM4500 Cl E-2011
9 mg/L
11 /21 /2022
1, 1, 1,2-Tetrachloroethane
SW 845 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1, 1, 1 -Trichloroethane
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1, 1, 2-Trichloroethane
SW 846 Method 82600/50308
<0.5 pg/L
11/22/2022
1,1-Dichloroethane
SW 846 Method 8260D/5030B
<0 5 pg/L
11/22/2022
1,1-Dich loroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,1-Dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
1,2,3-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11 /22/2022
1,2,3-Trichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,2,4-Trichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,2-Dichlorobenzene
SW 846 Method 82600/50308
<0.5 pg/L
11/22/2022
1,2-Dichloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
1,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Report #:: 2022-23081
Page 7 of 32

F""07 49 Environmental Chemists, Inc.
• 6602 Windmill Way, Wilmington, NC 28405 x 910.392.0223 Lab k, 910.392.4424
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax"I 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347,5843 Lab/ Fax
ANALYTICAL & CONSULTING CHEMISTS info(iUenvironmen talchemists.com
Albemarle Utility
Date of Report: Dec 06, 2022
862 Holiday Island Road
Customer PO #:
Hertford NC
27944
Customer ID: 09110024
Attention:
Report #: 2022-23081
Project ID: Monitoring Wells
1,3,5-Trimethylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
1,3-Dichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
1, 3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
1 '1 /22/2022
1,4-Dichlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
2,2-Dichloropropane
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
4-Chlorotoluene
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
Benzene
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
Bromobenzene
SW 846 Method 8260DI5030B
<0.5 pg/L
11/22/2022
Bromochloromethane
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
Bromodichloromethane
SW 846 Method 826OD15030B
<Q,5 pg/L
11/22/2022
Bromoform
SW 846 Method 8260015030B
<0.5 pg/L
11/22/2022
Bromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Chlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Chloroethane
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
CIS-1,2-Dichloroethene
SW 846 Method 8260015030B
<0,5 pg/L
11/22/2022
cis-1,3-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Dibromochloromethane
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
Dibromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Dichlorodifluoromethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Ethylbenzene
SW 846 Method 8260015030E
<0.5 pg/L
11/22/2022
Hexachlorobutadiene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2.022
1 sopropyl benzene
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
M+P Xylene
SW 846 Method 826OD150308
<1.0 pg/L
11/22/2022
Methylene chloride
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Report # 2022-23081
Page 8 of 32

Pavirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC: 28405 • 91.0.392.0223 Lab - 910,392.4424 Fax
710 Bowsertown Road, Manteo, NTC 27954 • 252.473.5702 Lab/Pax
255-A Wilmington highway, Jacksonville, NC 28540 . 910.347,5843 Lab/Fax
info(yenvironmentalchemists.com
Albemarle Utility
Date of Report: Dec 06, 2022
862 Holiday Island Road
Customer PO #:
Hertford NC
27944
Customer ID: 09110024
Attention:
Report #: 2022-23081
Project ID: Monitoring Wells
n-Propylbenzene
SW 846 Method 826013/5030B
<0.5 pg/L
11/22/2022
ortho-Xylene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
sec-B utyl benzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Styrene
SW 846 Method 8260D/5030B
<0, 5 pg/L
11/22/2022
tert-Butyl benzene
SW 646 Method 8260D/50308
<0.5 pg/L
11/22/2022
Tetrachloroethene
SW 846 Method 826013/50308
<0.5 pg/L
11/22/2022
Toluene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Trans-1,2-Dichloroethene
SW 846 Method 826013/503013
<0.5 pg/L
11/22/2022
Trans-1,3-dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Vinyl chloride
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
Nitrate Nitrogen (Cale)
Nitrite Nitrogen EPA 353.2, Rev. 2.0. 1993 0.07 mg/L 11/18/2022
Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 0.76mg/L 11/22/2022
Nitrate Nitrogen Subtraction Method 0.69 mg/L 12/05/2022
Report #:: 2022-23081 Page 9 of 32

SUBMIT FORM ON -OW PAPER ONLY
ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
Facility Name: Albemarle Utility Company
Permit Name (if different):
Facility Address: 862 Holiday Island Rd
Hertford NC
or Type
27944 County Perquimans
Contact Person: Danny Shelton Perry ORC Telephone#: [phone]
Well Location/Site Name: South West of Spray field No. of wells to be sampled: 10
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
RMIT Number: Expiration Date: 05-31-2025
n-Discharge WQ0001817 UIC
'DES Other
PE OF PERMITTED OPERATION BEING MONITORED
❑■ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW - 4
Date sample collected: 11/17/2022
FIELD ANALYSES:
WAS
Well Depth: 12 ft.
Well Diameter: 2 in.
pH 00400: 6.0 units Temp. 000lo: 1 5.5 °C
DRY at
Depth to Water Level 82546: 8.2 ft. below measuring point
Screened Interval: -2 ft. to -12 ft.
Spec. Cond. 00094: µ
time ofMhos sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: none
check
Volume of water pumped/bailed before sampling: 3.0 gallons
Appearance Tan
here:
❑
Samples for metals were collected unfiltered: ❑ YES 0 NO
and field acidified: ❑ YES ® NO
Date sample analyzed:11117/2022 Laboratory Name: Environmental Chemists, Inc
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.05
Coliform: MF Fecal 31616
<4 colonies
/100ml-
Nitrate (NO3) as N 00620 0.29
Coliform: MF Total 31504
/100ml-
Phosphorus: Total as P 00665
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
)issolved Solids:Total 70300
232
mg/L
Al - Aluminum 01105
pH (Lab) 00403
6.0
units
Ba - Barium 01007
TOC 00680
32.8
mg/L
Ca - Calcium 00916
Chloride 00940
17
mg/L
Cd - Cadmium 01027
Arsenic 01002
ug/L
Chromium: Total 01034
Grease and Oils 00552
mg/L
Cu - Copper 01042
Phenol 32730
ug/L
Fe - Iron 01045
Sulfate 00945
mg/L
Hg - Mercury 71900
Specific Conductance 00095
µMhos
K - Potassium 00937
Total Ammonia 00610
0.9
mg/L
Mg - Magnesium 00927
(Ammonia Nitrogen; NH3asN;
Ammonia Nitrogen, Total)
Mn - Manganese 01055
TKN as N 00625
mg/L
Ni - Nickel 01067
mg/L
mg/L
mg/L
mg/L
mg/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
Pb - Lead o1o51
Zn - Zinc 01092
Certification No. 94
ug/L
mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes (1) ❑ No (0)
VOC 7873 method #
method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%a
Shayne Lamb - Corporate Secretary
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.06-07-2018

�'enviro7hem
'4N
ANALYTICAL & CONSULTING CHEMISTS
777 0:
Environmental Chemists, Inc;.
6602 Windmill Way, Wilmington, NC: 28405 - 910.392.0223 Lab a 910.392.41:4 i'wl
710 Bowsertown .Road, Manteo, NC 27954 - 252.473.5702 Lab'Fa. ,
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
info(u)environrnentalchemists.corn
Albemarle Utility Date of Report: Dec 06, 2022
862 Holiday Island Road Customer PO #:
Hertford NC 27944 Customer ID: 09110024
Attention: Report #: 2022-23081
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-56760 Site: MW-4 11/17/2022 12:05 PM Water Jay Baker
Test Method
Color
Color
Depth to water, ft.
Depth to Water, Ft
Ammonia Nitrogen
EPA 350.1, Rev. 2 0, 1993
Gallons bailed before sampling
Gallons Bailed before sampling
Odor
Qualitative
Total Dissolved Solids (TDS)
SM 2540 C-2015
Temperature
SM 2550 B-2010
pH
SM 4500 H B-2011
Total Organic Carbon (TOC)
SM 5310 B-2014
Chloride
SM4500 Cl E-2011
1,1,1,2-Tetrach loroethane
SW 846 Method 8260D/5030B
1, 1, 1 -Trichloroethane
SW 846 Method 8260D/5030B
1,1,2,2-Tetrachloroethane
SW 846 Method 826OD/5030B
1,1,2-Trichloroethane
SW 846 Method 826OD/5030B
1,1-Dichloroethane
SW 846 Method 8260D/50308
1, 1 -Dichloroethene
SW 846 Method 826OD/5030B
1,1-Dichloropropene
SW 846 Method 8260D15030B
1,2,3- frichlorobenzene
SW 846 Method 8260D/50308
1, 2, 3-Trich loropropane
SW B46 Method 8260D15030B
1,2,4-Trichlorobenzene
SW 846 Method 8260D15030B
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
1,2-Dibromo-3-Chloropropane
SW 846 Method 826OD/5030B
1,2-Dibromoethane
SW 846 Method 826OD15030B
1,2-Dichlorobenzene
SW 846 Method 8260D/503GB
1,2-Dichloroethane
SW 846 Method 8260D15030B
1,2-Dichioropropane
SW 846 Method 8260D/5030B
Results Date Analyzed
Tan
11/17/2022
8.2 feet
11/17/2022
0.9 mg/L
12/01/2022
3(dry)gallons
11/17/2022
None
11/17/2022
232 mg/L
11/19/2022
15.5 C
11/17/2022
6.0 units
11/17/2022
32.8 mg/L
11/29/2022
17mg/L
11/21/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
/ <0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11 /22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
Report #.: 2022-23081 Page 10 of 32

Environmental Chemists,
Inc.
envirochem i
6602 Windmill Way, Wilmington, NC 28405 1 910.392.0223 Lab A 910.392.4424
Fax
71.0 Bowsertown Road, Manteo, NC 27954 • 252.473,5702 Lab/Fax
sM
255-A Wilmington
Highway Jacksonville, NC 28540 * 910.347.5843 Lab/ Fax
ANALYTICAL & CONSULTING CHEMISTS
in(o(a)environmentalcliemists.corn
Albemarle Utility
Date of Report: Dec 06, 2022
862 Holiday Island Road
Customer PO #:
Hertford NC 27944
Customer ID: 09110024
Attention:
Report #: 2022-23081
Project ID: Monitoring Wells
1,3,5-Trimethylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
2,2-Dichloropropane
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Bromobenzene
SW 846 Method 8260DI50306
<0.5 pg/L
11/22/2022
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Bromodichloromethane
SW 846 Method B260D/5030B
<0.5 pg/L
11/22/2022
Bromoform
SW 845 Method 826ODY5030B
<0.5 pg/L
11/22/2022
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Carbon tetrachloride
SW 846 Method 826ODY50308
<0.5 pg/L
11/22/2022
Chlorobenzene
SW 846 Method 8260D/5030B
<0,5 pg/L
11/22/2022
Chloroethane
SW 846 Method 82600/50308
<0.5 pg/L
11/22/2022
Chloroform
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Chloromethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
cis- 1,2-Dichloroethene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
cis- 1,3-Dichloropropene
SW 846 Method 826ODY50308
<0.5 pg/L
11/22/2022
Dibromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Dibromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Dichlorodifluoromethane
SW 846 Method 8260D15030B
<0.5 pg/L
11/22/2022
Ethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Hexachlorobutadiene
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
1 sopropyl benzene
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
11/22/2022
Methylene chloride
SW 848 Method 82800/5030B
<0.5 pg/L
11/22/2022
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Report #:: 2022-23081
Page 11 of 32

7nv
Environmental Chemists,
Inc.
/
6602 Windmill Way,
Wilmington, NC 28405 • 910.392.0223 Lab ° 910,392.44-14 Fax
71.0 $owsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington
Highway, Jacksonville, NC 28540 • 910.347.5843
Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
info(4,,environmentalchemists.com
Albemarle Utility
Date of Report: Dec 06, 2022
862 Holiday Island Road
Customer PO #:
Hertford NC 27944
Customer ID: 09110024
Attention:
Report #: 2022-23081
Project ID: Monitoring Wells
n-Propylbenzene
SW 846 Method 6260D/5030B
<0.5 pg/L
11/22/2022
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
sec-Butylbenzene
SW 846 Method 826OD16030B
<0.5 pg/L
11/22/2022
Styrene
SW 845 Method 8260D/5030B
<0.5 pg/L
11/22/2022
tert-Butyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Tetrachloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Toluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Trans- 1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Trans-1,3-dichloropropene
SW 646 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Vinyl chloride
SW 846 Method 8260D/5030B
<0,5 pg/L
11/22/2022
Nitrate Nitrogen (Cale)
Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 0.05 mg/L 11/18/2022
Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 0.34 mg/L 11/22/2022
Nitrate Nitrogen Subtraction Method 0.29 mg/L 12/05/2022
Report 2022.23081 Page i 2 oq 32 ��

SUBMIT FORM ON _OW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Please Print Clearly or Type
Facility Name: Albemarle Utility Company
Permit Name (if different):
Facility Address: 862 Holiday Island Rd
Hertford NC 27944 County Perquimans
Contact Person: Danny Shelton Perry ORC
Well Location/Site Name: South West of Sprayfield
Telephone#: [phone]
No. of wells to be sampled: 10
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
:RMIT Number: Expiration Date: 05-31-2025
in -Discharge WQ0001817 UIC
'DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑■ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW - 5
Date sample collected: 11/17/2022
FIELD ANALYSES:
WAS
Well Depth: 15 ft.
Well Diameter: 2 in.
pH 00400: 5.9 units Temp. 000lo: 1 6.0 °C
DRY at
Depth to Water Level 82546: 10.0 ft. below measuring point
p g p
Screened Interval: 12 2
ft. to ft.
Spec. Cond. 000sa: µ Mhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling: 5.0 gallons
Appearance Tan
here:
❑
Samples for metals were collected unfiltered: ❑ YES © NO
and field acidified: El YES (■� NO
ate sample analyzed:11/17/2022 Laboratory Name: Environmental Chemists, Inc
\RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.03
Coliform: MF Fecal 31616
<1 colonies
/100mL
Nitrate (NO3) as N 00620 <0.02
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
solved Solids:Total 70300
423
mg/L
AI - Aluminum of lo5
pH (Lab) 00403
5.9
units
Ba - Barium 01007
TOC 00680
5.8
mg/L
Ca - Calcium oo916
Chloride 00940
106
mg/L
Cd - Cadmium 01027
Arsenic 01002
ug/L
Chromium: Total 01034
Grease and Oils 00552
mg/L
Cu - Copper 01042
Phenol 32730
ug/L
Fe - Iron 01045
Sulfate 00945
mg/L
Hg - Mercury 71900
ecific Conductance 00085
µMhos
K - Potassium 00937
Total Ammonia 00610
<0.2
mg/L
Mg - Magnesium 00927
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn -Manganese oloss
TKN as N 00625
mg/L
Ni - Nickel 01067
mg/L
mg/L
mg/L
mg/L
mg/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
Pb - Lead o1051
Zn - Zinc 01092
Certification No. 94
ug/L
mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes (1) ❑ No (0)
VOC 7873 method #
method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Shayne Lamb -Corporate Secretary �
Permittee (or Authorized Aqent) Name and Title - Please print or type Siqnature of Permittee (M Authorized Agent) -- 'Wte) I
GW-59 Rev.06-07-2018

--
!�nviroichem I
M
ANALYTICAL & CONSULTING CHEMISTS
Albemarle Utility
862 Holiday Island Road
Hertford NC
Attention:
Lab ID Sample ID:
22-56761 Site: MW-5
Test
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 + 910.392.0223 Lab • 910.392.4424 Fa),
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Dec 06, 2022
Customer PO M
27944 Customer ID: 09110024
Report #: 2022-23081
Project ID: Monitoring Wells
Color
Depth to water, ft.
Ammonia Nitrogen
Gallons bailed before sampling
Odor
Total Dissolved Solids (TDS)
Temperature
pH
Total Organic Carbon (TOC)
Chloride
1, 1, 1,2-Tetrachloroethane
1, 1, 1 -Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1, 1 -Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1, 2,4=Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
1.2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichioropropane
Collect Date/Time Matrix
11/17/2022 12:15 PM Water
Method
Color
Depth to Water, Ft.
EPA 350 1, Rev. 2 0, 1993
Gallons Bailed before sampling
Qualitative
SM 2540 C-2015
SM 2550 B-2010
SM 4500 H B-2011
SM 5310 B-2014
SM4500 Cl E-2011
SW 846 Method 8260D/5030B
SW 846 Method 826OD150308
SW 846 Method 8260D/50308
SW 846 Method 826OD15030B
SW 846 Method 8260D/50308
SW 846 Method 8260D/5030B
SW 846 Method 82600/5030B
SW 846 Method 8260D/5030B
SW 846 Method 82600/5030B
SW 846 Method 8260D/5030B
SW 846 Method 82BOD150308
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/50306
SW 846 Method 0260D/5030B
SW 846 Method 8260D/5030B
Results
Sampled by
Jay Baker
Date Analyzed
Tan
11/17/2022
10, 0 feet
11/17/2022
< 0.2 mg/L
12/01 /2022
5.0gallons
11/17/2022
None
11/17/2022
423mg/L
11/19/2022
16.0 C
11/17/2022
5.9 units
11/17/2022
5.8 mg/L
11 /29/2022
106 mg/L
11 /21 /2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
/ <0.5 pg/L
11/22/2022
<0.5pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11 /22/2022
<0.5 pg/L
11/22/2022
Report #:: 2022-23081 Page 13 of 32 ,,

Lienvirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab R 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 * 252.473,5702 Lab/Fay
255-A Wilmington Highway, Jacksonville, NC 28540 11 910.347,5843 Lab/Fax
inf'o(iuenvironmentalchenlists.cont
Albemarle Utility
Date of Report: Dec 06, 2022
862 Holiday Island Road
Customer PO #:
Hertford NC
27944
Customer 1D: 09110024
Attention:
Report #: 2022-23081
Project ID: Monitoring Wells
1,3,5-Trimethylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
1,3-Dichlorobenzene
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
1,3-Dichloropropane
SW 846 Method 826013/50308
<0.5 pg/L
11/22/2022
1,4-Dichlorobenzene
SW 646 Method 8260D/5030B
<0.5 pg/L
11/22/2022
2,2-Dichloropropane
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
2-Chlorotoluene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Benzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Bromochloromethane
SW 846 Method 82GOD/5030B
<0.5 pg/L
11/22/2022
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Bromoform
SW 846 Method 82600/50308
<0.5 pg/L
11 /2212022
Bromomethane
SW 846 Method 826OD150308
<0.5 pg/L
11/22/2022
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Chlorobenzene
SW 646 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Chloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
Chloroform
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
cis-1,2-Dichloroethene
SW 846 Method 626OD/50308
<0.5 pg/L
11/22/2022
cis-1, 3-Dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Dibromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Dibromomethane
SW 846 Method 8260DY5030B
<0.5 pg/L
11/22/2022
Dichlorodifluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Ethylbenzene
SW 846 Method 8280D/5030B
<0.5 pg/L
11/22/2022
Hexachlorobutadiene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Isopropylbenzene
SW 846 Method 82BOD/50308
<0.5 pg/L
11/22/2022
- M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
11/22/2022
Methylene chloride
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
n-Butylbenzene
SW 646 Method 8260D/50308
<0.5 pg/L
11/22/2022
Report # 2022-23081
Page 14 of 32-w.

ro"'7— ---7"q1
';M
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392.4,424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway; Jacksonville, NC 28540 + 910.347.5843 Lab/Fax
[e-mail]
Albemarle Utility
Date of Report: Dec 06, 2022
862 Holiday Island Road
Customer PO #:
Hertford NC
27944
Customer ID: 09110024
Attention:
Report #: 2022-23081
Project ID: Monitoring Wells
n-Propylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
ortho-Xylene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
p-Isopropyltoluene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
sec-Butylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Styrene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
tert-Butylbenzene
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
Tetrachloroethene
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
Toluene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Trans-1,2-Dichloroethene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Trans-1,3-dichloropropene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Trichloroethene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Trichlorofluoromethane
SW 846 Method 8260D/6030B
<0.5 pg/L
11 /22/2022
Vinyl chloride
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2, Rev.2.0, 1993 0.03 mg/L 11/18/2022
Nitrate+Nitrite-Nitrogen EPA 353,2, Rev. 2.0, 1993 0.03 mg/L 11/22/2022
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/05/2022
Report #: 2022-23081 Page 16 of 32

SUBMIT FORM ON _OW PAPER ONLY
ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
Facility Name: Albemarle Utility Company
Permit Name (if different):
Facility Address: 862 Holiday Island Rd
Hertford NC
27944
or
County Perquimans
IContact Person: Danny Shelton Perry ORC Telephone#: [phone]
Well Location/Site Name: West Of Spray Field No. of wells to be sampled: 10
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
:RMIT Number: Expiration Date: 05-25-2025
,n-Discharge WQ0001817 UIC
'DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑■ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW -
6
Date sample collected: 11/17/2022
FIELD ANALYSES:
WAS
Well Depth: 12 ft.
Well Diameter: 2 in.
pH 00400: 6.0 units Temp. 00010: 17.5 °C
DRY at
Depth to Water Level 82546: 10.0 ft. below measuring point Screened Interval: -2 ft. to
-12 ft.
Spec. Cord. 000sa: µMhos
time ofsampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: none
check
Volume of water pumped/bailed before sampling:
4.0
gallons
Appearance Tan
here:
❑
Samples for metals were collected unfiltered: El YES
0 NO and field acidified: El YES ® NO
LABORATORY INFORMATION
Date sample analyzed: 11 /17/2022
Laboratory Name: Environmental Chemists,
Inc
Certification No. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.08
mg/L
Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <2 colonies
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 560
mg/L
Al - Aluminum oil o5
mg/L
pH (Lab) 00403 6.0
units
Ba - Barium 01007
ug/L
TOC 00680 3.9
mg/L
Ca - Calcium 00916
mg/L
Chloride oos4o 151
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese olo55
ug/L
, method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Shayne Lamb - Corporate Secretary
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.06-07-2018
Siqnature of Permittee

1
.',
ANALYTICAL & CONSULTING CHEMISTS
Albemarle Utility
862 Holiday Island Road
Hertford NC
Attention:
Lab ID Sample ID:
22-56762 Site: MW-6
Test
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab m 910.392.4424 Pax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highwav, Jacksonville, NC 28540 • 910.347.5843 Lab/:tax
info(i)envirorlrnentalchenlists.com
Date of Report: Dec 06, 2022
Customer PO #:
27944 Customer ID: 09110024
Report #: 2022-23081
Project ID: Monitoring Wells
Color
Depth to water, ft.
Ammonia Nitrogen
Gallons bailed before sampling
Odor
Total Dissolved Solids (TDS)
Temperature
pH
Total Organic Carbon (TOC)
Chloride
1, 1, 1,2-Tetrachloroethane
1, 1, 1 -Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1, 1 -Dichloroethane
1,1-Dichloroethene
1, 1 -Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
t ,2-Dichloropropane
Collect Date/Time Matrix
11/17/2022 9:40 AM Water
Method
Color
Depth to Water, Ft
EPA 350.1, Rev. 2 0, 1993
Gallons Bailed before sampling
Qualitative
SM 2540 C-2015
SM 2550 B-2010
SM 4500 H B-2011
SM 5310 B-2014
SM4500 Cl E-2011
SW 846 Method 8260D150308
SW 846 Method 826013/503013
SW 846 Method 8260D/5030B
SW 846 Method 826OD15030B
SW 846 Method 826OD15030B
SW 846 Method 8260D/5030B
SW 846 Method 826OD150308
SW 846 Method 8260D/50308
SW 846 Method 82600/5030B
SW 846 Method 8260D15030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/50308
SW 846 Method 8260D/50308
SW 846 Method 8260D/50308
SW 846 Method 8260D/50308
SW 846 Method 8260D/5030B
Results
Sampled by
Jay Baker
Date Analyzed
Tan
11/17/2022
10.0 feet
11/17/2022
< 0.2 mg/L
12/01 /2022
4.0 gallons
11/17/2022
None
11/17/2022
560 mg/L
11/19/2022
17.5 C
11/17/2022
6.0 units
11/17/2022
3.9 mg/L
11/29/2022
151 mg/L
11/21/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
/ <0.5 pg/L
11/22/2022
<0.5pg/L
11/22/2022
<0. 5 pg/L
11 /22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0, 5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
<0.5 pg/L
11/22/2022
Report # 2022-23081 Page 16 of 32

F777
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab w 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 » 252.473.5702 Lab/ Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
infow environmentalchemists.com
Albemarle Utility
Date of Report: Dec 06, 2022
862 Holiday Island Road
Customer PO #:
Hertford NC
27944
Customer ID: 09110024
Attention:
Report #: 2022-23081
Project ID: Monitoring Wells
1,3,5-Trimethylbenzene
SW 846 Method 8260W50308
<0.5 pg/L
11/22/2022
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,4-Dichlorobenzene
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Bromodichloromethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Bromoform
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Bromomethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Carbon tetrachloride
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Chloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Chloromethane
SW 846 Method 826OD150308
<0.5 pg/L
11/22/2022
cis- 1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
cis-1,3-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Dibromochloromethane
SW 846 Method 8260D/6030B
<0.5 pg/L
11/22/2022
Dibromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Dichlorodifluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Ethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1 sopropyl benzene
SW 846 Method 8260D150308
<0.5 pg/L
11/22/2022
M+P Xylene
SW 846 Method 8260DI50308
<1.0 pg/L
11/22/2022
Methylene chloride
SW 846 Method 826013/503013
<0.5 pg/L
11/22/2022
Naphthalene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11 /2212022
Report #:: 2022-23081
Page 17 of 32

Environmental Chemists,
Inc.
•
6602 Windmill "lay,
Wilmington, NC.. 28405 • 910.392.0223 Lab o 910.392.4424 =� x
41,
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington
Highway, Jacksonville, NC 28540 + 910.347.5843
Lab Fax
ANALYTICAL & CONSULTING CHEMISTS
infoCo,,envirorrmerrtalchemists.com
Albemarle Utility
Date of Report: Dec 06, 2022
862 Holiday Island Road
Customer PO #:
Hertford NC 27944
Customer ID: 09110024
Attention:
Report #: 2022-23081
Project ID: Monitoring Wells
n-Propylbenzene
SW 846 Method 8260015030E
<0.5 pg/L
11/22/2022
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
p-isopropyitoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
sec-B utyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Styrene
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
tert-B utyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Tetrachloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Toluene
SW 845 Method 5260D/5030B
<0.5 ug/L
11/22/2022
Trans-1 ,2-Dichicroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Trans-1,3-dichloropropene
SW 846 Method 8260D/5030B
<0,5 pg/L
11/22/2022
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Vinyl chloride
SW 846 Method 8260D/5030B
<0, 5 pg/L
11/22/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2, Rev. 2 0. 1993 0.08mg/L 11/18/2022
Nitrate+Nitrite-Nitrogen EPA353.2, Rev, 20, 1993 0.03 mg/L 11/22/2022
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/05/2022
9
Report #. 2022-23081 Pav Is of ;a;;:

SUBMIT FORM ON _ OW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name: Albemarle Utility Company
Permit Name (if different):
Facility Address: 862 h
Hertford
Please Print Clearly or Type
Island Rd
NC 27944 County Perquimans
Contact Person: Danny Shelton Perry ORC
Well Location/Site Name: West of Baffle lagoon
Telephone#: [phone]
No. of wells to be sampled: 10
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
:RMIT Number: Expiration Date: 05-31-2025
�n-Discharge WQ0001817 UIC
'DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
0 Lagoon ❑ Remediation: Infiltration Gallery
0 Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): MW - 7 Date sample collected: 11/17/2022
Well Depth: 16.9 ft. Well Diameter: 2 in.
Depth to Water Level 82546: 4.1 ft. below measuring point Screened Interval: 11.9 ft. to 16.9 ft.
Measuring Point is 2•5 ft. above land surface Relative M.P. Elevation: ft.
Volume of water pumped/bailed before sampling: 5.0 gallons
Samples for metals were collected unfiltered: ❑ YES 0 NO and field acidified: ❑ YES N NO
FIELD ANALYSES:
pH 00400: 5.7 units Temp. 000lo: 1 7.5 °C
Spec. Cond. 00094: µMhos
Odor 00085: none
Appearance Red/Brown
If WELL
WAS
DRY at
time of
sampling,
check
here: El
LABORATORY INFORMATION
Date sample analyzed: 11 /17/2022
Laboratory Name: Environmental Chemists, Inc
Certification No. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L
Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 colonies
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 221
mg/L
Al - Aluminum ollo5
mg/L
pH (Lab) 00403 5.7
units
Ba - Barium 01007
ug/L
TOC 00680 16.0
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 33
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
ipecific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 0.5
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
, method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Shayne Lamb - Corporate Secretary
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.06-07-2018

enviro•
gin+
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6002 Windmill Way, Wilmington, NC 28405 « 910.392.0223 Lab 910.392.4424 fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910,347.5843 Lab/Fax
info,a environmentalchemists.com
Albemarle Utility Date of Report: Dec 06, 2022
862 Holiday Island Road Customer PO #:
Hertford NC 27944 Customer ID: 09110024
Attention: Report #: 2022-23081
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by.,..
22-56763 Site: MW-7 11/17/2022 11:05 AM Water Jay Baker
Test Method Results Date Analyzed
Color
Color
Red/Brown
11/17/2022
Depth to water, ft.
Depth to water, Ft.
4.1 feet
11/17/2022
Ammonia Nitrogen
EPA 350.1, Rev. 2.0,1993
0.5 mg/L
12/01/2022
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
11/17/2022
Odor
Qualitative
None
11/17/2022
Total Dissolved Solids (TDS)
SM 2540 C-2015
221 mg/L
11 /19/2022
Temperature
SM 2550 B-2010
17.5 C
11/17/2022
pH
SM 4500 H B-2011
5.7 units
11/17/2022
Total Organic Carbon (TOC)
SM 5310 8-2014
16.0 mg/L
11 /29/2022
Chloride
SM4500 Cl E-2011
33 mg/L
11121 /2022
1, 1, 1,2-Tetrachloroethane
SW 846 Method 826013/50308
<0.5 pg/L
11/22/2022
1, 1, 1 -Trichloroethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
1,1,2,2-Tetrach loroethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
1,1,2-Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,1-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,1-Dichloroethene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
1,1-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,2,3-Trichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
11/22/2022
1,2, 3-Trichloropropane
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
1,2,4-Trichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
1,2,4-Trimethylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
11/22/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 82600/50308
<0.5 pg/L
11/22/2022
^ 1,2-Dibromoethane
SW 846 Method 8280D/5030B
<0.5 pg/L
11/22/2022
1,2-Dichlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
1,2-Dichloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
1,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Report #:: 2022-23081 Page 19 of 32

-envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4.124 Fax
710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info@envi ronnientaicllemists.com
Albemarle Utility
862 Holiday Island Road
Hertford NC
Attention:
27944
Date of Report: Dec 06, 2022
Customer PO #:
Customer ID: 09110024
Report #: 2022-23081
Project ID: Monitoring Wells
1,3,5-Trimethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
1,3-Dichlorobenzene
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11 /22/2022
1,4-Dichlorobenzene
SW 848 Method 826OD/5030B
<0.5 pg/L
11/22/2022
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
2-Chlorotoluene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
4-Chlorotoluene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Benzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Bromobenzene
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Bromodichloromethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Bromoform
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Bromomethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Carbon tetrachloride
SW 846 Method 8260D/6030B
<0.5 pg/L
11/22/2022
Chlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/2212022
Chloroethane
SW 846 Method 8260015030E
<0.5 pg/L
11/22/2022
Chloroform
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Chloromethane
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
cis-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
cis-1,3-Dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Dibromochloromethane
SW 846 Method 8260D/50308
<0.5 pg/L
11 /22/2022
Dibromomethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Dichlorodifluoromethane
SW 846 Method 8260D150308
<0.5 pg/L
11/22/2022
Ethylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Hexachlorobutadiene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Isopropylbenzene
SW 846 Method 826OD/50306
<0.5 pg/L
11/22/2022
M+P Xylene
SW 846 Method 826OD15030B
<1.0 pg/L
11/22/2022
Methylene chloride
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
!Naphthalene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
n-Butylbenzene
SW 846 Method 8280D/503013
<0.5 pg/L
11/22/2022
Report #:: 2022-23081
Page 20 of 32mm� T

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab a 910.39 '.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.58431,ab/Fax
info cr environmentalchemists.coni
Albemarle Utility
Date of Report: Dec 06, 2022
862 Holiday Island Road
Customer PO #:
Hertford NC
27944
Customer ID: 09110024
Attention:
Report #: 2022-23081
Project ID: Monitoring Wells
n-Propylbenzene
SW 846 Method 8260D/5D30B
<0.5 pg/L
11/22/2022
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
sec -Butyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Styrene
SW 846 Method 6260D/5030B
<0.5 pg/L
11/22/2022
tert-Butyl benzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Tetrachloroethene
SW 846 Method 8260DIS0308
<0.5 pg/L
11/22/2022
Toluene
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
Trans-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Trans-1 ,3-dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Vinyl chloride
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2, Rev. 2 0, 1993 < 0.02 mg/L 11/18/2022
Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2 0, 1993 < 0.02 mg/L 11/22/2022
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/05/2022
Report # . 2022-23081 Page 21 ca" 32

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 05-31-2025
Facility Name: Albemarle Utility Company
Non -Discharge WQ0001817 UIC
NPDES Other
Permit Name (if different):
Facility Address: 862 Holiday Island Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑■ Lagoon ❑ Remediation: Infiltration Gallery
Hertford NC 27944 County Perquimans
❑■ Spray Field ❑ Remediation:
Contact Person: Danny Shelton Perry ORC
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: East of Spray Field
No. of wells to be sampled: 10
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW - 8
Date sample collected: 11/27/2022
FIELD ANALYSES:
WAS
Well Depth: 15 ft.
Well Diameter: 2 in.
pH 00400: 5.5 units Temp. 000lo: 1 7.8 °C
DRY at
Depth to Water Level 82546: 8.3 ft. below measuring point Screened Interval: 5 ft. to
15 ft. Spec. Cond. 00094: µMhos
of
timesampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: Sulur
check
Volume of water pumped/bailed before sampling:
5.0
gallons
Appearance Tan/Brown
here:❑
Samples for metals were collected unfiltered: El
NNO and field acidified: ❑YES ■❑ NO
LABORATORY INFORMATION
Date sample analyzed:11/17/2022
Laboratory Name: Environmental Chemists, Inc Certification No. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.04
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <2 colonies
/100mL
Nitrate (NO3) as N 00620 0.47
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 341
mg/L
Al - Aluminum oilo5
mg/L
pH (Lab) 00403 5.5
units
Ba - Barium 01007
ug/L
TOC 00680 5.0
mg/L
Ca - Calcium 00916
mg/L
Chloride oo94o 90
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total olo34
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate oo945
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 0.3
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese olo55
ug/L , method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.06-07-2018

r- 7-111--l...,...IlplllllllllllN k Environmental Chemists, Inc.
--envirochem1 6602 Windmill Way, Wilmington, NC 28405 • 910.392,0223 l..,ab 1 910,392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ® 252.473.5702 Lab/Fax
w 255-A Wilmington Highway, Jacksonville, NC 28540 • 91.0.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infofo environmentalchemists.com
Albemarle Utility Date of Report: Dec 06, 2022
862 Holiday Island Road Customer PO #:
Hertford NC 27944 Customer ID: 09110024
Attention: Report #: 2022-23081
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-56764 Site: MW-8 11/17/2022 10:45 AM Water Jay Baker
Test Method Results Date Analyzed
Color
Color
Tan/Brown
11/17/2022
Depth to water, ft.
Depth to Water, Ft
8.3 feet
11/17/2022
Ammonia Nitrogen
EPA 350.1, Rev. 2.0, 1993
0.3 mg/L
12/01/2022
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
11/17/2022
Odor
Qualitative
Sulfur
11/17/2022
Total Dissolved Solids (TDS)
SM 2540 C-2015
341 mg/L
11 /19/2022
Temperature
SM 2550 B-2010
17.8 C
11/17/2022
pH
SM 4500 H B-2011
5.5 units
11/17/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
5.0 mg/L
11 /29/2022
Chloride
SM4500 Cl E-2011
90 mg/L
11 /21/2022
1,1;1,2-Tetrachloroethane
SW 846 Method 826oD/5030B
<0.5 pg/L
11/22/2022
1, 1, 1 -Trichloroethane
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
1,1,2,2-Tetrachloroethane
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
1,1,2-Trichloroethane
SW B46 Method 8260D/50308
<0.5 pg/L
11/22/2022
1,1-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,1-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
1,1-Dichloropropene
SW 846 Method 8280D/5030B
<0.5 pg/L
11/22/2022
1,2,3-Trichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
1,2,3-Trichloropropane
SW 846 Method 8260Dt5O3OB
<0.5 pg/L
11/22/2022
1,2,4-Trichlorobenzene
SW 846 Method 8260D/5030B
<0,5 pg/L
11/22/2022
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,2-Dibromoethane
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
1,2-Dichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
1, 2-Dichloroethane
SW 846 Method 826oD/5030B
<0.5 pg/L
11/22/2022
1,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Report #:: 2022-23081 Page 22 of 32

Environmental Chemists, Inc.
envirochemm6602 Windmill Way, Wilmington, NC 28405 - 9:10.392.0223 Lab - 910.392.4424 Pax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
M 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info(a;environrnentalchemists.com
Albemarle Utility Date of Report: Dec 06, 2022
862 Holiday Island Road Customer PO #:
Hertford NC 27944 Customer ID: 09110024
Attention: Report #: 2022-23081
Project ID: Monitoring Wells
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
1112.2/2022
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
2-Chlorotoluene
SW 646 Method 8260D/5030B
<0.5 pg/L
11/22/2022
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Benzene
SW 846 Method 8260D150308
<0.5 pg/L
11/22/2022
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Bromochloromethane
SW 846 Method 826013/50306
<0.5 pg/L
11/22/2022
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Bromomethane
SW 846 Method 826=50308
<0.5 pg/L
11/22/2022
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Chloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Chloroform
SW 846 Method 8260015030E
<0.5 pg/L
11/22/2022
Chloromethane
SW 848 Method 8260D/5030B
<0.5 pg/L
11/22/2022.
cis- 1,2-Dichloroethene
SW 846 Method 826013/50308
<0.5 pg/L
11/22/2022
cis-1, 3-Dish loropropene
SW 846 Method 8260D/6030B
<0.5 pg/L
11/22/2022
Dibromochloromethane
SW 846 Method 8260DI50306
<0.5 pg/L
11/22/2022
Dibromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Dichlorodifluoromethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Ethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
lsopropylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
M+P Xylene
SW 846 Method 8260D/50308
<1.0 pg/L
11/22/2022
Methylene chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Naphthalene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Report # 2022-2308+
- - _ -
-
Page 23 of 32 ._.

Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab A 910.392.4424 F ii x
710 Bowsertown Road, Manteo, NC 27954 ^ 252.473.5702 Lab/Fax
M 255-A Wilmington Highwav, Jacksonville, NC 28540 m 910.347.5843 Lab'/Fax
ANALYTICAL & CONSULTING CHEMISTS
info(ucnvironmcntalctrenlists.corn
Albemarle Utility
Date of Report: Dec 06, 2022
862 Holiday Island Road
Customer PO #:
Hertford NC
27944
Customer ID: 09110024
Attention:
Report #: 2022-23081
Project ID: Monitoring Wells
n-Propylbenzene
SW 846 Method 82600/50308
<0.5 pg/L
11/22/2022
ortho-Xylene
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
sec- Butyl benzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Styrene
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
tert-Butylbenzene
SW 846 Method 826OD150308
<0.5 pg/L
11/22/2022
Tetrachloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Toluene
SW 846 Method 82600/50306
<0.5 pg/L
11/22/2022
Trans- 1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Trans- 1,3-dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Trichloroethene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 0.04 mg/L 11/18/2022
Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 0.51 mg/L 11/22/2022
Nitrate Nitrogen Subtraction Method 0.47 mg/L 12/05/2022
Report # 2022-23061 � Pmio 2A of 32

SUBMIT FORM ON OW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Please Print Clearly or Type
Facility Name: Albemarle Utility Company
Permit Name (if different):
Facility Address: 862 Holiday Island Rd
Hertford NC 27944 County Perquimans
Contact Person: Danny Shelton Perry ORC
Well Location/Site Name: West of Spray Field
Telephone#: [phone]
No. of wells to be sampled: 10
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
RMIT Number: Expiration Date: 05-31-2025
n-Discharge WQ0001817 UIC
'DES Other
PE OF PERMITTED OPERATION BEING MONITORED
❑■ Lagoon ❑ Remediation: Infiltration Gallery
N Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW - 9
Date sample collected: 11/17/2022
FIELD ANALYSES:
WAS
Well Depth: 15 ft.
Well Diameter: 2 in.
pH 00400: 6.1 units Temp. oo010: 17.6 °C
DRY at
Depth to Water Level 82546: 9.4 ft. below measuring point Screened Interval: 4 ft. to 14 ft. Spec. Cond. 000sa: µMhos
time ofsampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: Sulfur
check
Volume of water pumped/bailed before sampling: 5.0
gallons
Appearance Clear
here:
❑
Samples for metals were collected unfiltered: El YES
0 NO and field acidified: El YES N NO
Date sample analyzed:11/17/2022 Laboratory Name: Environmental Chemists, Inc
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
Coliform: MF Fecal 31616
<1 colonies
/100mL
Nitrate (NO3) as N 00620 0.04
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
issolved Solids:Total 70300
68.0
mg/L
Al - Aluminum 01105
pH (Lab) 00403
6.1
units
Ba - Barium 01007
TOC 00680
0.9
mg/L
Ca - Calcium 00916
Chloride oosao
7
mg/L
Cd - Cadmium 01027
Arsenic 01002
ug/L
Chromium: Total 01034
Grease and Oils 00552
mg/L
Cu - Copper 01042
Phenol 32730
ug/L
Fe - Iron 01045
Sulfate 00945
mg/L
Hg - Mercury 71900
pecific Conductance 00095
µMhos
K - Potassium 00937
Total Ammonia 00610
<0•2
mg/L
Mg - Magnesium 00927
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
TKN as N 00625
mg/L
Ni - Nickel 01067
mg/L
mg/L
mg/L
mg/L
mg/L
ug/L
mg/L
ug/L
ug/L
mg/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
Pb - Lead 01051
Zn - Zinc 01092
Certification No. 94
ug/L
mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes (1) ❑ No (0)
VOC 7873 method #
method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.06-07-2018

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC. 28405 • 910.392.0223 Lab . 9L0.392.4424 Fx,,
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
M 255-A Wilmington Highway, Jacksonville, NC 28540 « 910.347.5843 Lab/Fax
ANALYTICAL $ CONSULTING CHEMISTS inf'o(q-�environmen talchemists.corn
Albemarle Utility Date of Report: Dec 06, 2022
862 Holiday Island Road Customer PO #:
Hertford NC 27944 Customer ID: 09110024
Attention: Report #: 2022-23081
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-56765 Site: MW-9 11/17/2022 10:15 AM Water Jay Baker
Test Method Results Date Analyzed
Color
Color
Clear
11/17/2022
Depth to water, ft.
Depth to water, Ft.
9.4 feet
11/17/2022
Ammonia Nitrogen
EPA 350.1, Rev. 2.0, 1993
< 0.2 mg/L
12/01/2022
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
11/17/2022
Odor
Qualitative
Sulfur
11/17/2022
Total Dissolved Solids (TDS)
SM 2540 C-2015
68.0 mg/L
11/19/2022
Temperature
SM 2550 B-2010
17.6 C
11/17/2022
pH
SM 4500 H B-2011
6.1 units
11/17/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
0.9 mg/L
11/29/2022
Chloride
SM4500 Cl E-2011
7 mg/L
11 /2112022
1, 1, 1,2-Tetrachloroethane
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/22/2022
1, 1, 1 -Trichloroethane
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/22/2022
1,1,2,2-Tetrach loroethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
1,1,2-Trichloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
1,1-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,1-Dich loroethene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
1,1-Dichloropropene
SW 846 Method B260D/5030B
<0.5 pg/L
11/22/2022
1,2,3-Trichlorobenzene
SW 846 Method 82BOD15030B
<0.5 pg/L
11/22/2022
1, 2, 3-Trich loropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1, 2,4-Trichlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
1,2,4-Trimethylbenzene
SW 848 Method 826OD/5030B
<0.5 pg/L
11/22/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,2-Dibromoethane
SW 846 Method 8260D150308
<0.5 pg/L
11/22/2022
1,2-Dichlorobenzene
SW 846 Method 8260D/503013
<0.5 pg/L
11/22/2022
,1,2-Dichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
11/22/2022
1,2-Dichloropropane
SW 846 Method 8260D16030B
<0.5 pg/L
11/22/2022
'deport # 2022-23061 Page 25 of 32

Environmental Chemists,
Inc.
t
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ° 910.392.r�-#24
Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 I-ab/Fax
w
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 I,ab/l ax
ANALYTICAL & CONSULTING CHEMISTS
info@)environmentalchemists.com
Albemarle Utility
Date of Report: Dec 06, 2022
862 Holiday Island Road
Customer PO #:
Hertford NC 27944
Customer ID: 09110024
Attention:
Report #: 2022-23081
Project ID: Monitoring Wells
1,3,5-Trimethylbenzene
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
1,3-Dichlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
1,3-Dichloropropane
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
1,4-Dichlorobenzene
SW 846 Method 8260D/6030B
<0.5 pg/L
11/22/2022
2,2-Dichloropropane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
2-Chlorotoluene
SW 846 Method 826OD150308
<0.5 pg/L
11/22/2022
4-Chlorotoluene
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
Benzene
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
Bromobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Bromodichloromethane
SW 846 Method 826OD/50306
<0.5 pg/L
11/22/2022
Bromoform
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Bromomethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Chlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
Chloroethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Chloromethane
SW 846 Method 826013/50308
<0.5 pg/L
11/22/2022
cis- 1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
CIS-1,3-Dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Dibromochloromethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Dibromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Dichlorodifluoromethane
SW 845 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Bthylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1 sopropyl benzene
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
11/22/2022
Methylene chloride
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
n-Butylbenzene
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
Report #:: 2022,23081
Page 26 of 32

Environmental Chemists, �����-�������]�������� ��J��N������m^s,Inc.
b6n2w8odmiUwa�w{lmiogmn NC28^V5 ^ vl0,3eZ�0223Lnh ~ 910.392.4424Fux
7loeov,serto,vnRoad, x4an/eo'w[zr954 ^ 252.4735702Lxb/rax
z55'AWilmington Highway, Jacksonville, N[2854o ^ 910]47s843Lob/pax
ANALYTICAL aCONSULTING CHEMISTS
ink`@nnvi,nnmo`u\ch,mim,^.Com
Albemarle Utility
Date mVReport: Dec U8.2O22
882Holiday Island Road
Customer PO#:
Hertford NC 27944
Customer ID: 09110024
Attention:
Repork#: 2022'23081
Project ID: Monitoring Wells
n-pnopy|benrano
aw«4eMethod ^x«nom»n»a «0.5pg/L
11/22/2022
ortho'Xy|ena
aw»^aMethod a:«»mn»»uo <0.5pg/L
11/22/2022
p'|oopnopy|bn|ueno
uw«*aMethod uz««omu»oa «O.Spg/L
11/22/2022
aao'8uty|benzene
oww»Method «««»om»»ue <0.6pQ/L
11/22/2022
Styrene
aw«*«Method nu««oo»»»o <0.5pg/L
11/22/2022
had-Buh/|benzene
aw»*nMethod nus»ua»ooa <0.5ug/L
11/22/2022
Tatnsch|onuathene
o«««*«Method ou»«om«»»a <0.5pg/L
11/22/2022
Toluene
o««»4»Method au««om»»«a <0.5pg/L
11/22/2022
Trans'1.2-Dich|onoethene
awwmMethod 826»om030o <8.5pg/L
11/22/2022
Trans- 1.3-dich|onmpnopena
owwoMethod »xe»om«»»a ^0.5pg/L
11/22/2022
T,ich|onoethene
a»»o4«Method »ue«»m»»»B <0.5pg/L
11/22/2022
Trioh|wnoOuoromathonm
uwo*«Method nus«oso»«a <O.5ug/L
11/22/2022
Vinyl chloride
owa4nMethod ee«000»u»a <0.5pg/L
11/22/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA »��Rev. 2.u1»m <O. 02nng/L 11/18/2022
Nitrab*+Nitrde'Nitnogen EPA ma,2,Rev. 2,u1*m 0.04mg/L 11/22/022
Nitrate Nitrogen Subtraction Method 0.04mg/L 12/05/2022
4

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, INC 27699-1617
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 05-31-2025
Facility Name: Albemarle Utility Company
Non -Discharge WQ0001817 UIC
Permit Name (if different):
NPDES Other
Facility Address: 862 Holiday Island Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑■ Lagoon ❑ Remediation: Infiltration Gallery
Hertford N.C. 27944 County Perquimans
❑■ Spray Field ❑ Remediation:
Contact Person: Danny Shelton Perry ORC
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: South of Spray Field
No. of wells to be sampled: 10
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-10
Date sample collected: 11/17/2022
FIELD ANALYSES:
WAS
Well Depth: 15 ft.
Well Diameter: 2 in.
pH o0400: 5.5 units Temp. 000lo: 17.5 °C
DRY at
Depth to Water Level 82546: 11.5 ft. below measuring point Screened Interval: 5 ft. to
14
ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: Sulfur
check
Volume of water pumped/bailed before sampling:
5.0
gallons
Appearance Tan
here:❑
Samples for metals were collected unfiltered: ❑ YES
❑■ NO and field acidified: ❑ YES ® NO
LABORATORY INFORMATION
Date sample analyzed:11/17/2022
Laboratory Name: Environmental Chemists„ Inc Certification No. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 < 0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 colonies
/100mL
Nitrate (NO3) as N 00620 0.55
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
11OOmL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 310
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 5.5
units
Ba - Barium 01007
ug/L
TOC 00680 1.5
mg/L
Ca - Calcium 00916
mg/L
Chloride o0940 910
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron o1045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total)
Mn - Manganese o1055
ug/L
, method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Shayne Lamb Corporate Secretary
Permittee (or Authorized Aqent) Name and Title - Please print or type
(Date)
GW-59 Rev.06-07-2018

Environmental Chemists, Inc.
�r ochel
' 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 930.392.4424 Fax
710 Bowsertown Road, Manteo, NC: 27954 - 252.473.5702 Lab/lax
M 255-A Wilmington Highway, Jacksonville, NC 28540 ! 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info a environmentalchemists.com
Albemarle Utility Date of Report: Dec 06, 2022
862 Holiday Island Road Customer PO #:
Hertford NC 27944 Customer ID: 09110024
Attention: Report #: 2022-23081
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-56766 Site: MW-10 11/17/2022 10:30 AM Water Jay Baker
Test Method Results Date Analyzed
Color
color
Tan
11/17/2022
Depth to water, ft.
Depth to water, Ft.
11.5 feet
11/17/2022
Ammonia Nitrogen
EPA 350.1. Rev. 2.0, 1993
< 0.2 mg/L
12/01/2022
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
11/17/2022
Odor
Qualitative
Sulfur
11/17/2022
Total Dissolved Solids (TDS)
SM 2540 c-2015
310 mg/L
11/19/2022
Temperature
SM 2550 B-2010
17.5 C
11/17/2022
pH
SM 4500 H B•2011
5.5 units
11/17/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
1.5 mg/L
11/29/2022
Chloride
SM4500 cl E-2011
110 mg/L
11 /21 /2022
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0,5 pg/L
11/22/2022
1, 1, 1-Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11 /2212022
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/50308
<0.5pg/L
11/22/2022
1,1,2-Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,1-Dichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
1,1-Dichloroethene
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/22/2022
1,1-Dichloropropene
SW 846 Method 826aD/5030B
<0.5 pg/L
11/22/2022
1,2,3-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,2,3-Trichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,2,4-Trichlorobenzene
SW 848 Method 8260D/50308
<0.5 pg/L
11/22/2022
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260DI5030B
<0.5 pg/L
11/22/2022
1,2-Dibromoethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
1,2-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
1,2-Dichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
1,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Report # 2022-23081 Page 28 of 32

envirochem
SM
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 9 910.392.0223 Lab - 910.392.4424 ?.a'
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fa.x
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info;a environmentalchemists.com
Albemarle Utility Date of Report: Dec 06, 2022
862 Holiday Island Road Customer PO #:
Hertford NC 27944 Customer ID: 09110024
Attention: Report #: 2022-23081
Project ID: Monitoring Wells
1,3,5-Trimethylbenzene
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
1,3-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
1,3-Dichloropropane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
1,4-Dichlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
2,2-Dichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
2-Chlorotoluene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
4-Chlorotoluene
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
Benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Bromobenzene
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Bromodichloromethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Bromoform
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
Bromomethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Carbon tetrachloride
SW 846 Method 826013/50308
<0.5 pg/L
11/22/2022
Chlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Chloroethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Chloroform
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Chloromethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
cis- 1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11 /2212022
cis- 1,3-Dichloropropene
SW 846 Method 825OD/50306
<0.5 pg/L
11/22/2022
Dibromochloromethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11 /22/2022
Dibromomethane
SW 846 Method 826013/503013
<0.5 pg/L
11/22/2022
Dichlorodifluoromethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Ethylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Isopropylbenzene
SW 846 Method 826OD/50308
<0.5 pg/L
11/22/2022
M+P Xylene
SW 846 Method 8260D15030B
<1.0 pg/L
11/22/2022
Methylene chloride
SW 846 Method 826013/50306
<0.5 pg/L
11/22/2022
Naphthalene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
n-Butylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/22/2022
Report # 2022-23081
Page 29 of 32 ,

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 9"10.392.4424 Fax
710 F3owsertown Road, Manteo, NC 27954 « 252.473,5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(t?environmentalchemists.ci)m
Albemarle Utility
Date of Report: Dec 06, 2022
862 Holiday Island Road
Customer PO #:
Hertford NC 27944
Customer ID: 09110024
Attention:
Report #: 2022-23081
Project ID: Monitoring Wells
n-Propylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
11/22/2022
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
p-isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11 /22/2022
sec-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Styrene
SW 846 Method 8260D/50306
<0.5 pg/L
11/22/2022
tert-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
11/22/2022
Tetrachloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Toluene
SW 846 Method 8260D/50308
<0.5 pg/L
11/22/2022
Trans- l ,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
11/22/2022
Trans-1,3-dichloropropene
SW 846 Method 82600/5030B
<0.5 pg/L
11/22/2022
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/22/2022
Vinyl chloride
SW 846 Method 8260D/50306
<0.5 pg/L
11/22/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 3532, Rev. 20, 1993
< 0.02 mg/L
11/18/2022
Nitrate+Nitrite-Nitrogen
EPA353.2, Rev. 20, 1993
0.55mg/L
11/22/2022
Nitrate Nitrogen
Subtraction Method
0.55 mg/L
12/05/2022
Lab ID Sample ID: M-3817
Collect Date/Time Matrix Sampled by
22-56769 Site: MW-1
11/17/2022
11:20 AM Water Jay Baker
Test
Method
Results Date
Analyzed
Fecal Coliform
SM9222 D-2015MF
<2 Colonies/100ml-
11/17/2022
Lab ID Sample ID: M-3818
Collect Date/Time Matrix Sampled +byLL -
22-56772 Site: MW-2
11/17/2022
11:35 AM Water Jay Baker
Test
Method
Results Date
Analyzed
Fecal Coliform
SM 9222 D-2015 MF
<2 Colonies/100mL 11/17/2022
Report # 2022-23081 Page 30 of 32

GW-59A COMPLIANCE REPORT FORM Permit # 000
(Submit one each monitoring period with GW-59 forms.)
I
Enter date monitoring results were due. (I 7 -3i- ��. Will this monitoring report (GW-59 and GW-59A)
YES
NO
be submitted after the established due date?
2
Was any required information missing on the GW-59 report forms?
YES
9NO
IF the answer to question 1 or 2 is "YES', list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO ,
identification plate, area overgrown, etc.)? ff the answer is "Yes ", contact the Regional Office for guidance.
OrN
4
Are any monitored constituents equal to or above the established standards?
ES
NO
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below:
f ! 1 w Q!!S�
�c`�= 'l� 1190� (� S b�
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YE
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly
located; contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
groundwater quality problem?
YES
NO
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation,
fines, and/or penalties.
8
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current G W-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report (Compliance Report G�59A)ieand complete to the best of my knowledge.
6M151q;3
Signature of Permi ee (or Authorized Agent) Date
GW-59A 12/8/2003

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