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Home My WebLink AboutWQ0001817_Monitoring - 03-2023_20231027Monitoring Report Submittal Permit Number#* Name of Facility:* Month: * March Report Information Type * Revised - GW-59 Confirmation Email Address: Name of Submitter: * Signature: Date of submittal: Initial Review WQ0001817 Albemarle Utility Company Year:* 2023 Upload Document* March 2023 revised.pdf 15.06MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). danny.perry@albemarleplantation.com Danny S Perry O�,ls04w Reviewer: Wanda.Gerald 10/27/2023 This will be filled in automatically Is the project number correct?* WQ0001817 Is the monitoring report accepted?* Yes No Regional Office* Washington Reviewer: _anonymous Review Date: 10/30/2023 JUDivii i r umm VIV .uvv Y/1YGK UNLI GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Albemarle Utility Comapany Permit Name (if different): Facility Address: 862 Holiday Island RD Hertford N.0 or 27944 County Pergimans IContact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 Well Location/Site Name: North of Holding Lagoon No. of wells to be sampled: 10 WELL ID NUMBER (from Permit): MW -1 Date sample collected: 3/23/2023 Well Depth: 20 ft. Well Diameter: 2 in. Depth to Water Level 82546:15.0 ft. below measuring point Screened Interval: -5 ft. Measuring Point is 3 ft. above land surface Relative M.P. Elevation: Volume of water pumped/bailed before sampling: 5.0 gallons to -20 ft. ft. Samples for metals were collected unfiltered: ❑ YES E NO and field acidified: ❑ YES 0 NO DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 :RMIT Number: Expiration Date: 05-31-2025 ,n-Discharge WQ0001817 UIC 'DES Other 'PE OF PERMITTED OPERATION BEING MONITORED N Lagoon ❑ Remediation: Infiltration Gallery 0 Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date sample analyzed:3/23/2023 Laboratory Name: Environmental Chemists, Inc PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.07 Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 0.03 Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 )issolved Solids:Total 70300 239 mg/L All - Aluminum o1105 pH (Lab) 00403 6.2 units Ba - Barium 01007 TOC 00680 5.3 mg/L Ca - Calcium 00916 Chloride 00940 12 mg/L Cd - Cadmium 01027 Arsenic 01002 ug/L Chromium: Total 01034 Grease and Oils 00552 mg/L Cu - Copper 01042 Phenol 32730 ug/L Fe - Iron 01045 Sulfate oo945 mg/L Hg - Mercury 71900 Specific Conductance 00095 µMhos K - Potassium 00937 Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 TKN as N 00625 mg/L Ni - Nickel 01067 mg/L mg/L mg/L mg/L mg/L ug/L mg/L ug/L ug/L mg/L ug/L ug/L mg/L mg/L ug/L ug/L FIELD ANALYSES: pH 00400: 6.2 units Spec. Cond. 00094: Odor 00085: None Appearance Tan Pb - Lead 01051 Zn - Zinc 01092 If WELL Temp. 000lo: 16.7 °C DRY at uMhos time of Certification No. 94 ug/L mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 method # method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Lamb Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 01 envirochem ANALYTICAL S CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 ' 910-392.0223 Lab R 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 2-52.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax intb@a environmentalchemistscom Albemarle Utility Date of Report: Apr 05, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27W Customer ID: 09110024 Attention: Report #: 2023-05799 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14596 Site: MW-1 3/23/2023 10:00 AM Water Jay Baker Test Method Results Date Analyzed Color Color Tan 03/23/2023 Depth to water, ft. Depth to water, Ft. 15.0 feet 03/23/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/23/2023 Odor Qualitative None 03/23/2023 Total Dissolved Solids (TDS) SM 2540 c-2015 239 mg/L 03/24/2023 Temperature SM 2550 B-2010 16.7 C 03/23/2023 pH SM 4500 H B-2011 6.2 units 03/23/2023 Total Organic Carbon (TOC) SM 5310 B-2014 5.3 mg/L 03/24/2023 Fecal Coliform SM 9222 c-2015 W <1 Colonies/100ml- 03/23/2023 Chloride SM4500 Ci E-2011 12 mg/L 03/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev 2 0, 1993 0,07 mg/L 03/23/2023 Nitrate+Nitrite-Nitrogen EPA 3532,Rev 2.0.1993 0.10mg/L 03/27/2023 Nitrate Nitrogen Subtraction Method 0.03 mg/L 04/04/2023 Report #. 2023-05799 Page 1 of 10 SUBMIT FORM OI LOW PAPER ONLY (GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Please Print Clearly or Type Facility Name: Albemarle Utility Company Permit Name (if different): Facility Address: 862 Holiday Island Rd Hertford NC 27944 County Perquimans IContact Person: Danny Shelton Perry ORC Well Location/Site Name: East of Baffle Lagoon WELL ID NUMBER (from Permit): MW-2 Well Depth: 12 ft. Depth to Water Level 82546: 4.5 ft. below measuring point Measuring Point is 3 ft. above land surface Volume of water pumped/bailed before sampling: 5.0 Samples for metals were collected unfiltered: ❑ YES L■ Telephone#: 252-426-1007 No. of wells to be sampled: 10 Date sample collected: 3/23/2023 Well Diameter: 2 in. Screened Interval: -2 ft. Relative M.P. Elevation: gallons to -12 ft. ft. NO and field acidified: ❑ YES ® NO DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 :RMIT Number: Expiration Date: 05-31-2025 in -Discharge WQ0001817 UIC 'DES Other 'PE OF PERMITTED OPERATION BEING MONITORED X Lagoon ❑ Remediation: Infiltration Gallery N Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: pH 00400: 5.3 units Spec. Cond. 00094: Odor =85: none Appearance Tan Temp. 000lo: 15.5 oC uMhos Date sample analyzed:3/23/2023 Laboratory Name: Environment Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.10 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 0.05 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 251 mg/L Al - Aluminum of lo5 mg/L pH (Lab) 00403 5.3 units Ba - Barium 01007 ug/L TOC 00680 31.2 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 14 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 < 0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese oio55 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%, Shayne Lamb Corporate Secretary Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.06-07-2018 If WELL DRY at time of sampling, check here:❑ :enviroehem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 r 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 A 910.347.5843 Lab/Fax info(2!envi ronmen t alchemi sts.com Albemarle Utility Date of Report: Apr 05, 2023 862 Holiday Island Road Customer PO #: Hertford NC 279" Customer ID: 09110024 Attention: Report M 2023-05799 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14597 Site: MW-2 3/23/2023 10:10 AM Water Jay Baker Test Method Results Date Analyzed Color Color Tan 03/23/2023 Depth to water, ft. Depth to water, Ft. 4.5 feet 03/23/2023 Ammonia Nitrogen EPA 350.1, Rev 2.0, 1993 < 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Baled before sampling 5.0 gallons 03/23/2023 Odor Qualitative None 03/23/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 251 mg/L 03/24/2023 Temperature SM 2550 B-2010 15.5 C 03/23/2023 pH SM 4500 H B-2011 5.3 units 03/23/2023 Total Organic Carbon (TOC) SM 5310 B-2014 31.2 mg/L 03/30/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/23/2023 Chloride SM450o Cl E-2011 14 mg/L 03/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0. 1993 0.10 mg/L 03/23/2023 Nitrate+Nitrite-Nitrogen EPA 3532, Rev, 2.0, 1993 0.15 mg/L 03/27/2023 Nitrate Nitrogen subtract on Method 0.05 mg/L 04/04/2023 Report M. 2023-05799 Page 2 of 10 SUBMIT FORM Ol` LOW PAPER ONLY • . DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, INC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-31-2025 Facility Name: Albemarle Utility Company Non -Discharge WQ0001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ElRotary Distributor ElLand Application of Sludge Well Location/Site Name: South East of Spray field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 3 Date sample collected: 3/23/2023 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 5.8 units Temp. 000lo: 15.4 °C DRY at Depth to Water Level 82546: 7.0 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec. Cond. 00094: µMhos time of 3 sampling,check Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor 00085: none Volume of water pumped/bailed before sampling: 1 gallons Appearance Tan/Grey here:❑ Samples for metals were collected unfiltered: ❑ YES ® NO and field acidified: ❑ YES E NO LABORATORY INFORMATION Date sample analyzed:3/23/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.05 mg/L Pb - Lead oio51 ug/L Coliform: MF Fecal 31616 4 colonies /100mL Nitrate (NO3) as N 00620 0.68 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 951 mg/L Al - Aluminum of lo5 mg/L pH (Lab) 00403 5.8 units Ba - Barium 01007 ug/L TOC 00680 22.3 mg/L Ca - Calcium 00916 mg/L Chloride oo94o < 5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 000m µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH. as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Byrum - Corporate Secretary Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) GW-59 Rev.06-07-2018 7envirochl-e7m� ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax info@environmentalchemists.com Albemarle Utility Date of Report: Apr 05, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-05799 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14598 Site: MW-3 3/23/2023 10:20 AM Water Jay Baker Test Method Results Date Analyzed Color Color Tan/Grey 03/23/2023 Depth to water, ft. Depth to Water, Ft. 7.0 feet 03/23/2023 Ammonia Nitrogen EPA 350,1, Rev. 2.0, 1993 < 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Bailed before sampling 1(Dry) gallons 03/23/2023 Odor Qualitative None 03/23/2023 Total Dissolved Solids (TDS) SM 2540 c-2015 951 mg/L 03/24/2023 Temperature SM 2550 B-2010 15.4 C 03/23/2023 pH SM 4500 H B-2011 5.8 units 03/23/2023 Total Organic Carbon (TOC) SM 5310 0-2014 22.3 mg/L 03/30/2023 Fecal Coliform SM 9222 0.2015 MF 4 Colonies/100ml- 03/23/2023 Chloride SM4500 Cl E-2011 < 5 mg/L 03/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2, Rev 20, 1993 0.05 mg/L 03/23/2023 Nitrate+ Nitrite-N itrogen EPA 353.2, Rev 2 0, 1993 0.73 mg/L 03/27/2023 Nitrate Nitrogen Subtraction Method 0.68 mg/L 04/04/2023 Report # 2023-05799 Page 3 of 10 SUBMIT FORM ON _ DW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FArII ITV IIJPnDMATInrd Please Print Clearfv or Facility Name: Albemarle Utility Company Permit Name (if different): Facility Address: 862 Holiday Island Rd Hertford NC 27944 County Perquimans act Person: Danny Shelton Perry ORC Location/Site Name: South West of Spray field Telephone#: 252-426-1007 No. of wells to be sampled: 10 DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 PERMIT Number: Expiration Date: 05-31-2025 Non -Discharge WQ0001817 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: WELL ID NUMBER (from Permit): MW - 4 Date sample collected: 3/23/2023 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH oo400: 5.9 units Temp. 000lo: 1 5.4 °C DRY at Depth to Water Level 82546:7.0 ft. below measuring point Screened Interval: -2 ft. to -12 ft. Spec. Cond. 00094: µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: none sampling, check Volume of water pumped/bailed before sampling: 4.0 gallons Appearance Tan/Grey here: m Sales for metals were collected unfiltered: El M NO and field acidified: El N NO LABORATORY INFORMATION Date sample analyzed:3/23/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.07 Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 <0.02 Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 issolved Solids:Total 70300 174 mg/L Al - Aluminum o1105 pH (Lab) 00403 5.9 units Ba - Barium 01007 TOC 00680 20.8 mg/L Ca - Calcium 00916 Chloride 00940 < 5 mg/L Cd - Cadmium 01027 Arsenic 01002 ug/L Chromium: Total 01034 Grease and Oils 00552 mg/L Cu - Copper 01042 Phenol 32730 ug/L Fe - Iron 01045 Sulfate 00945 mg/L Hg - Mercury 71900 pecific Conductance 00095 µMhos K - Potassium 00937 Total Ammonia 00610 0.2 mg/L Mg - Magnesium 00927 (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 TKN as N 00625 mg/L Ni - Nickel 01067 mg/L mg/L mg/L mg/L mg/L ug/L mg/L ug/L ug/L mg/L ug/L ug/L mg/L mg/L ug/L ug/L Pb - Lead 01051 Zn - Zinc 01092 ug/L mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 method # method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Lamb - Corporate Secretary Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.06-07-2018 of PermittV (or Authorized Agent) 4-3 ro"P7 —'1_7 Environmental Chemists, Inc. envirolchem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab , 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 ° 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/ Fax ANALYTICAL & CONSULTING CHEMISTS info(u)environmentalchemistscom Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Date of Report: Apr 05, 2023 Customer PO #: Customer ID: 09110024 Report #: 2023-05799 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14599 Site: MW-4 3/23/2023 10:30 AM Water Jay Baker Test Method Results Date Analyzed Color Color Tan/Grey 03/23/2023 Depth to water, ft. Depth to water, Ft. 7.0 feet 03/23/2023 Ammonia Nitrogen EPA 350.1, Rev 2.0. 1993 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Bailed before sampling 4.0 gallons 03/23/2023 Odor Qualitative None 03/23/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 174 mg/L 03/24/2023 Temperature SM 2550 B-2010 15.4 C 03/23/2023 pH SM 4500 K B-2011 5.9 units 03/23/2023 Total Organic Carbon (TOC) SM 5310 B-2014 20.8 mg/L 03/30/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/23/2023 Chloride SM4500 Cl E-2011 < 5 mg/L 03/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353 2, Rev. 2 0. 1993 0.07 mg/L 03/23/2023 Nitrate+ N itrite-N itrogen EPA 353 2 Rev. 2 0, 1993 0.07 mg/L 03/27/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/04/2023 Report 9 2023-05799 Page 4 of 10 SUBMIT FORM Of LOW PAPER ONLY ROUNDWATER QUALITY MONITORING: OMPLIANCE REPORT FORM Please Print Clearly or Type Icility Name: Albemarle Utility Company =it Name (if different): icility Address: 862 Holiday Island Rd Hertford NC 27944 County Perquimans act Person: Danny Shelton Perry ORC Location/Site Name: South West of Sprayfield Telephone#: 252-426-1007 No. of wells to be sampled: 10 DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 PERMIT Number: Expiration Date: 05-31-2025 Non -Discharge WQ0001817 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑E Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: If WELL WELL ID NUMBER (from Permit): MW - 5 Date sample collected: 3/23/2023 Well Depth: 15 ft. Well Diameter: 2 in. Depth to Water Level 82546: 9.1 ft. below measuring point Screened Interval: 12 ft. to 2 ft. Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 5.0 gallons Samples for metals were collected unfiltered: ❑ YES 0 NO and field acidified: ❑ YES ® NO FIELD ANALYSES: pH 00000: 6.0 units Temp. 000lo: 15.4 °C Spec. Cond. 000sa: µMhos Odor 000s5: None Appearance Grey/ Tan WAS DRY at time ofsampling, check here:❑ LABORATORY INFORMATION Date sample analyzed:3/23/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.03 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 3.71 mg/L All - Aluminum 01105 mg/L pH (Lab) 00403 6.0 units Ba - Barium 01007 ug/L TOC 00680 5.2 mg/L Ca - Calcium 00916 mg/L Chloride 00940 81 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0•2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn -Manganese 01055 ug/L ,method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Lamb - Corporate Secretary Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 envirochem ANALYTICAL 8 CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392,4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax infort?• environ mentalchemists.com Albemarle Utility Date of Report: Apr 05, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-05799 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14600 Site: MW-5 3/23/2023 10:40 AM Water Jay Baker Test Method Results Date Analyzed Color Color Grey/Tan 03/23/2023 Depth to water, ft. Depth to Water. Ft. 9.1 feet 03/23/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0,1993 < 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Balled before sampting 5.0 gallons 03/23/2023 Odor Qualitative None 03/23/2023 Total Dissolved Solids (TDS) SM 2540 c-2015 371 mg/L 03/24/2023 Temperature SM 2550 8-2010 15.4 C 03/23/2023 pH SM4500 H B-2011 6.0 units 03/23/2023 Total Organic Carbon (TOC) SM 5310 B-2014 5.2 mg/L 03/30/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/23/2023 Chloride SM4500CIE•2011 81 mg/L 03/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 Rev 2 0 1993 0.03 mg/L 03/23/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev 2 0 1993 0.04 mg/L 03/27/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/04/2023 Report C 2023-05799 Page 5 of 10 SUBMIT FORM ON OW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 05-25-2025 Facility Name: Albemarle Utility Company Non -Discharge W00001817 UIC NPDES Other Permit Name (if different): Facility Address: 862 Holiday Island Rd TYPE OF PERMITTED OPERATION BEING MONITORED Hertford NC 27944 County Perquimans ❑■ Lagoon ❑ Remediation: Infiltration Gallery N Spray Field ❑ Remediation: Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: West Of Spray Field No. of wells to be sampled: 10 ❑ Water Source Heat Pump ❑ Other: from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 6 Date sample collected: 3/23/2023 FIELD ANALYSES: WAS Well Depth: 12 ft. Well Diameter: 2 in. pH 00400: 5.9 units Temp. 000lo: 15.7 °C DRY at Depth to Water Level 82546: 8.7 ft. below measuring point Screened Interval: -2 fL to -12 ft. Spec. Cond. 00094: µMhos time ofsampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: none check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Grey here: El Samples for metals were collected unfiltered: ❑ YES M NO and field acidified: ❑ YES M NO LABORATORY INFORMATION Date sample analyzed:3/23/2023 Laboratory Name: Environmental Chemists, Inc Certification No. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.08 mg/L Pb - Lead o1051 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 715 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 5.9 units Ba - Barium 01007 ug/L TOC 00680 6.0 mg/L Ca - Calcium 00916 mg/L Chloride 00940 213 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.06-07-2018 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info@environmentalchemists.com Albemarle Utility Date of Report: Apr 05, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-05799 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14601 Site: MW-6 3/23/2023 10:50 AM Water Jay Baker Test Method Results Date Analyzed Color Color Grey 03/23/2023 Depth to water, ft. Depth to Water. Ft. 8.7 feet 03/23/2023 Ammonia Nitrogen EPA 350.1, Rev. 2.0, 1993 < 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Balled before sampling 5.0 gallons 03/23/2023 Odor Qualitative None 03/23/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 715 mg/L 03/24/2023 Temperature SM 2550 B-2010 15.7 C 03/23/2023 pH SM4500 H B-2011 5.9 units 03/23/2023 Total Organic Carbon (TOC) SM 5310 B-2014 6.0 mg/L 03/30/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/23/2023 Chloride SM4500 Cl E-2011 213 mg/L 03/24/2023 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2, Rev 2.0, 1993 0.08 mg/L 03/23/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev 20, 1993 0.06 mg/L 03/27/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/04/2023 Report #:: 2023-05799 Page 6 of 10 SUBMIT FORM Of LOW PAPER ONLY UNDWATER QUALITY MONITORING: PLIANCE REPORT FORM Please Print Clearly or Type Facility Name: Albemarle Utility Company Permit Name (if different): Facility Address: 862 Holiday Island Rd Hertford NC 27944 County Perquimans Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 Well Location/Site Name: West of Baffle lagoon No. of wells to be sampled: 10 WELL ID NUMBER (from Permit): MW - 7 Well Depth: 16.9 ft. Depth to Water Level 82546: 4.0 ft. below measuring point Measuring Point is 2•5 ft. above land surface Volume of water pumped/bailed before sampling: 5.0 Samples for metals were collected unfiltered: ❑ YES 0 Date sample collected: 3/23/2023 Well Diameter: 2 in. Screened Interval: 11.9 ft. Relative M.P. Elevation: gallons to 16.9 ft. ft. NO and field acidified: ❑ YES ® NO DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 :RMIT Number: Expiration Date: 05-31-2025 ,n-Discharge WQ0001817 UIC 'DES Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date sample analyzed:3/23/2023 Laboratory Name: Environmental Chemists, Inc PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.05 Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 <0.02 Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 )issolved Solids:Total 70300 301 mg/L Al - Aluminum o1105 pH (Lab) 00403 6.4 units Ba - Barium 01007 TOC 00680 19.3 mg/L Ca - Calcium 00916 Chloride 00940 40 mg/L Cd - Cadmium 01027 Arsenic 01002 ug/L Chromium: Total 01034 Grease and Oils 00552 mg/L Cu - Copper 01042 Phenol 32730 ug/L Fe - Iron 01045 Sulfate 00945 mg/L Hg - Mercury 71900 >pecific Conductance 00095 µMhos K - Potassium 00937 Total Ammonia 00610 < 0.2 mg/L Mg - Magnesium 00927 (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 TKN as N 00625 mg/L Ni - Nickel 01067 mg/L mg/L mg/L mg/L mg/L ug/L mg/L ug/L ug/L mg/L ug/L ug/L mg/L mg/L ug/L ug/L FIELD ANALYSES: pH 00400: 6.4 unitE Spec. Cond. 00094: Odor 00085: Appearance Pb - Lead o1o51 Zn - Zinc 01092 If WELL Temp. 000lo: 14.0 °C DRY at µMhos time of none RedfTan Certification No. 94 ug/L mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 method # method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% X GW-59 Rev.06-07-2018 envirochem I, ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab , 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 4 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 ° 910.347.5843 Lab/Fax info@environmentalchemists.com Albemarle Utility Date of Report: Apr 05, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-05799 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14602 Site: MW-7 3/23/2023 9:50 AM Water Jay Baker Test Method Results Date Analyzed Color Color Red/Tan 03/23/2023 Depth to water, ft. Depth to water, Ft. 4.0 feet 03/23/2023 Ammonia Nitrogen EPA 3501, Rev. 2.0, 1093 < 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/23/2023 Odor oualitative None 03/2312023 Total Dissolved Solids (TDS) sea 2540 C-2015 301 mg/L 03/24/2023 Temperature SM 2550 B-2010 14.0 C 03/23/2023 pH SM 45GO H 8-2011 6.4 units 03123/2023 Total Organic Carbon (TOC) SM 5310 B-2014 19.3 mg/L 03/30/2023 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 03/23/2023 Chloride SM4500 Cl E-2011 40 mg/L 03/24/2023 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 3532. Rev. 2.0. 1993 0.05 mg/L 03/23/2023 Nitrate+Nitrite-Nitrogen EPA 353.2. Rev 2.0, 1903 < 0.02 mg/L 03/27/2023 Nitrate Nitrogen Subtraction Method <0.02 mg/L 04/04/2023 Report # 2023-05799 Page 7 of 10 SUBMIT FORM ON v -' LOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Albemarle Utility Company Permit Name (if different): Facility Address: 862 F Hertford Print or Type Island Rd NC 27944 County Perquimans act Person: Danny Shelton Perry ORC Location/Site Name: East of Spray Field Telephone#: 252-426-1007 No. of wells to be sampled: 10 DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER , IURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 PERMIT Number: Expiration Date: 05-31-2025 Non -Discharge WQ0001817 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑■ Lagoon ❑ Remediation: Infiltration Gallery ❑■ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 8 Date sample collected: 3/23/2023 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 5.8 units Temp. 000lo: 15.5 °C DRY at Depth to Water Level 82546: 5.0 ft. below measuring point Screened Interval: 5 ft. to 15 ft. Spec. Cond. 00094: µ time ofMhos sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: none check Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan here:❑ Samples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified: ❑ YES ■❑ NO )ate sample analyzed:3/23/2023 Laboratory Name: Environmental Chemists, Inc 'ARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.03 mg/L Coliform: MF Fecal 31616 3 colonies /100mL Nitrate (NO3) as N 00620 0.09 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L issolved Solids:Total 70300 405 mg/L Al - Aluminum o11o5 mg/L pH (Lab) 00403 5.8 units Ba - Barium 01007 ug/L TOC 00680 6.8 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 141 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total wom ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L Phenol 32730 ug/L Fe - Iron 01045 ug/L Sulfate 00945 mg/L Hg - Mercury 71900 ug/L pecific Conductance 00095 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 < 0.2 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; N113as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L TKN as N 00625 mg/L Ni - Nickel 01067 ug/L Certification No. 94 Pb - Lead 01051 ug/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 method # method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Shayne Lamb - Corporate Secetary Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 Signature of :envirochem ANALYTICAL 8 CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 i 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax inib,acnvi ron mentalchem ists.com Albemarle Utility Date of Report: Apr 05, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-05799 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14603 Site: MW-8 3/23/2023 11:05 AM Water Jay Baker Test Method Results Date Analyzed Color Color Clear/Tan 03/23/2023 Depth to water, ft. Depth to water. Ft. 5.0 feet 03/23/2023 Ammonia Nitrogen EPA 330.1. Rev. 2.0,1993 < 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 03/23/2023 Odor Qualitative None 03/23/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 405 mg/L 03/24/2023 Temperature SM 2550 B-2010 15.5 C 03/23/2023 pH SM 4500 H 8-2011 5.8 units 03/23/2023 Total Organic Carbon (TOC) SM 5310 8.2014 6.8 mg/L 03/24/2023 Fecal Coliform SM 9222 D-2015 MF 3 Coloniesl100m L 03/23/2023 Chloride SM4500 CI E-2011 141 mg/L 03/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 0.03 mg/L 03/23/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev, 2.0, 1993 0.12 mg/L 03/27/2023 Nitrate Nitrogen Subtraction Method 0.09 mg/L 04/04/2023 Report 0: 2023-05799 Page 8 of 10 SUBMIT FORM Of LOW PAPER ONLY Mail origi�nal ROUNDWATER QUALITY MONITORING: and 1 copy to: OMPLIANCE REPORT FORM Facility Name: Albemarle Utility Company Permit Name (if different): Facility Address: 862 Holiday Island Rd Hertford NC Please Print Clearly or Type 27944 County Perquimans Contact Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 Well Location/Site Name: West of Spray Field No. of wells to be sampled: 10 DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 ERMIT Number: Expiration Date: 05-31-2025 on -Discharge WQ0001817 UIC PDES Other YPE OF PERMITTED OPERATION BEING MONITORED N Lagoon ❑ Remediation: Infiltration Gallery K Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW - 9 Date sample collected: 3/23/2023 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH 00400: 6.3 units Temp. 000lo: 1 5.0 °C DRY at Depth to Water Level 82546: 6.4 ft. below measuring point Screened Interval: 4 ft. to 14 ft. Spec. Cond. 00094: µMhos time of sampling,check Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: none Volume of water pumped/bailed before sampling: 5.0 gallons Appearance Clear/Tan here: El Samples for metals were collected unfiltered: ❑ YES M NO and field acidified: ❑ YES ® NO Date sample analyzed:3/23/2023 Laboratory Name: Environmental Chemists, Inc PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.02 Coliform: MF Fecal 31616 8 colonies /100mL Nitrate (NO3) as N 00620 0.03 Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 (Note: Use WIN method for highly turbid samples) Orthophosphate 70507 issolved Solids:Total 70300 85.0 mg/L All - Aluminum 01105 pH (Lab) 00403 6.3 units Ba - Barium 01007 TOC 00680 4.1 mg/L Ca - Calcium 00916 Chloride 00940 5 mg/L Cd - Cadmium 01027 Arsenic 01002 ug/L Chromium: Total 01034 Grease and Oils 00552 mg/L Cu - Copper 01042 Phenol 32730 ug/L Fe - Iron 01045 Sulfate 00945 mg/L Hg - Mercury 71900 Specific Conductance 00095 µMhos K - Potassium 00937 Total Ammonia 00610 '0.2 mg/L Mg - Magnesium 00927 (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 TKN as N 00625 mg/L Ni - Nickel 01067 mg/L mg/L mg/L mg/L mg/L ug/L mg/L ug/L ug/L mg/L ug/L ug/L mg/L mg/L ug/L ug/L Pb - Lead 01051 Zn - Zinc 01092 Certification No. 94 ug/L mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 method # method # method # method # For R—em—ea—iaTion Systems Only . .. otal 1• •/L EAluent Total VOCs:• • I certify that. to the best of my knowledge and belief. the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DW R-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisorment for kno� ing violations. Shayne • - Corporate Secretary ittee (or Authorized Aqent) Name and Title - Please print or type Siqn—ature of (- •. - GW-59 Rev. 1. 1 1 F0,07- 49 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Apr 05, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-05799 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14604 Site: MW-9 3/23/2023 11:35 AM Water Jay Baker Test Method Results Date Analyzed Color Color Clearlran 03/23/2023 Depth to water, ft. Depth to Water. Ft. 6.4 feet 03/23/2023 Ammonia Nitrogen EPA 350.1, Rev, 2.0, 1993 < 0.2 mg/L 03/27/2023 Gallons bailed before sampling Gallons Sailed before sampling 5.0 gallons 03/23/2023 Odor Qualitative None 03/23/2023 Total Dissolved Solids (TDS) SM 2540 C-2015 85.0 mg/L 03/24/2023 Temperature SM 2550 B-2010 15.0 C 03/23/2023 pM SM 4500 H 8-2011 6.3 units 03/23/2023 Total Organic Carbon (TOC) SM 5310 B-2014 4.1 mg/L 03/24/2023 Fecal Coliform SM 9222 D-2015 MF 8 Colonies/100mL 03/23/2023 Chloride SM4500 Cl E-2o11 5 mg/L 03/24/2023 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2, Rev. 2.0, 1993 0.02 mg/L 03/23/2023 Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 0.05 mg/L 03/27/2023 Nitrate Nitrogen subtraction Method 0.03 mg/L 04/04/2023 Report aye 2023.06799 Page 9 of 10 SUBMIT FORM ON Vim' LOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Facility Name: Albemarle Utility Compal Permit Name (if different): Facility Address: 862 Holiday Island Rd Hertford N.0 27944 County Perquimans ict Person: Danny Shelton Perry ORC Telephone#: 252-426-1007 Location/Site Name: South of Spray Field No. of wells to be sampled: 10 DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER. )URCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 PERMIT Number: Expiration Date: 05-31-2025 Non -Discharge WQ0001817 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ■❑ Lagoon ❑ Remediation: Infiltration Gallery ■❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-10 Date sample collected: 3/23/2023 FIELD ANALYSES: WAS Well Depth: 15 ft. Well Diameter: 2 in. pH oo400: 6.0 units Temp. 000lo: 16.3 °C DRY at Depth to Water Level 82546: 9.0 ft. below measuring point Screened Interval: 5 ft. to 14 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: 5•0 gallons Appearance Tan here: El Samples for metals were collected unfiltered: ❑ YES 0 NO and field acidified: ❑ YES ❑■ NO )ate sample analyzed:3/23/2023 Laboratory Name: Environmental Chemists„ Inc Certification No. 94 'ARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 0.02 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 colonies /100mL Nitrate (NO3) as N 00620 0.16 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 415 mg/L All - Aluminum 01105 mg/L pH (Lab) 00403 6.0 units Ba - Barium 01007 ug/L TOC 00680 1.5 mg/L Ca - Calcium 00916 mg/L Chloride 00940 152 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.2 mg/L Mg - Magnesium 00927 _ mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Permittee (or Authorized Aqent) Name and Title - Please print or type GW-59 Rev.06-07-2018 Siqnature of envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347,5843 Lab/Fax infoi'a:enviro nmentalchemists.com Albemarle Utility Date of Report: Apr 05, 2023 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Report #: 2023-05799 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 23-14605 Site: MW-10 3/23/2023 11:20 AM Water Jay Baker Test Method Results Date Analyzed Color Color Depth to water, ft. Depth to water, Ft. Ammonia Nitrogen EPA 350.1, Rev 2.0, 1993 Gallons bailed before sampling Gallons Baled before sampling Odor Qualitative Total Dissolved Solids (TDS) SM 2540 C-2015 Temperature SM 2550 B-2010 pH SM 4500 H B-2011 Total Organic Carbon (TOC) SM 5310 B-2014 Fecal Coliform SM 9222 0-2015 MF Chloride SM4500 CI E-2011 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA353.2, Rev 2.0. 1993 Nitrate+Nitrite-Nitrogen EPA353.2, Rev. 2.0, 1993 Nitrate Nitrogen Subtracton Method Comment: t X' Reviewed by: Tan 03/23/2023 9.0 feet 03/23/2023 < 0.2 mg/L 03/27/2023 5.0 gallons 03/23/2023 None 03/23/2023 415 mg/L 03/24/2023 16.3 C 03/23/2023 6.0 units 03/23/2023 1.5 mg/L 03/24/2023 <1 Colonies/100ml- 03/23/2023 152 mg/L 03/24/2023 0.02 mg/L 03/23/2023 0.18 mg/L 03/27/2023 0.16 mg/L 04/04/2023 Report #:: 2023-05799 Page 10 of 10 GW-59A COMPLIANCE REPORT FORM Permit # w Q om! 3 (Submit one each monitoring period with GW-59 forms.) 1 Enter date monitoring results were due. ( -30 .Z31 Will this monitoring report (GW-59 and GW-59A) be submitted after the established due date? ;YE7SNO 2 Was any required information missing on the GW-59 report forms? IF the answer to question 1 or 2 is "YES'; list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YE NO identification plate, area overgrown, etc.)? ff the answer is "Yes ", contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is "NO'; skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: Z-.o w PN t4li� k TO 5 --) p -3 —C�S 1 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YE NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO'; skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection for each occurrence (for the last two years). date Are the monitoring wells listed in section 5 located at or beyond the review boundary? YE NO If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. g The person completing this portion (GIN--59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Reportt/GW-59A) is true and complete to the best of my knowledge. Oignai�ure of ermittee (or Authorized Agent) tDate GW-59A 12/8/2003 ze' P14 Vt . , Z s e ��` _& 7 V -6r V 7/ 5— ;- - 5-co 3 _3 7 AA in i IKJ d- DO-1 21" O.S 44- 3 - ?()7 . 6 - 4? S)cf y d�I/�Da� Lv;.OPH 5. -3 57, & ci lL 5" s— ec )VO p 19 . All