NCG030055_June DMR_20231026

(((��� // / Pace Analytical Services,LLC
ace® N ���� Asheville,
Riverside 04
Asheville,NC 28804
[phone]
July 06, 2023
Ms. Mary Bowen
Meritor
160 Ash St.
Forest City, NC 28043
RE: Project: STORMWATER
Pace Project No.: 92674434
Dear Ms. Bowen:
Enclosed are the analytical results for sample(s)received by the laboratory on June 26,2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
•Pace Analytical Services-Asheville
•Pace Analytical Services-Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Jonathan W Biddix
[e-mail]
[phone]
Project Manager
Enclosures
cc: Mr.Bill Adams, Meritor
Mr.Brian Stepp,Meritor
Mitchell Swanger,Meritor-Forest City
44,00w,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 1 of 31

Pace Analytical Services,LLC
ace"
2225 Riverside Dr.
a■V_ Asheville,NC 28804
[phone]
SAMPLE ANALYTE COUNT
Project: STORMWATER
Pace Project No.: 92674434
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92674434001 STORMWATER OUTFALL#1 FIRE PON EPA 1664B MMH 1 PASI-C
EPA 200.7 Rev 4.4 1994 D13131 7 PASI-A
EPA 625.1 PKS 58 PASI-C
EPA 624.1 SAS 34 PASI-C
SM 2540D-2015 RVS 1 PASI-A
EPA 9040C SMS 1 PASI-A
EPA 420.4 Rev 1.0 1993 ARJ 1 PASI-A
SM 4500-CN-E-2016 EGC 1 PASI-A
SM 5220D-2011 MA132 1 PASI-A
92674434002 STORMWATER OUTFALL#2 NORTH DI EPA 1664B MMH 1 PASI-C
EPA 625.1 PKS 58 PASI-C
EPA 624.1 SAS 34 PASI-C
SM 2540D-2015 RVS 1 PASI-A
EPA 420.4 Rev 1.0 1993 ARJ 1 PASI-A
PASI-A=Pace Analytical Services-Asheville
PASI-C=Pace Analytical Services-Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 3 of 31

Pace Analytical Services,LLC
2225 Riverside Dr.
aeeo Asheville,NC 28804
[phone]
ANALYTICAL RESULTS
Project: STORMWATER
Pace Project No.: 92674434
Sample: STORMWATER OUTFALL Lab ID: 92674434001 Collected: 06/21/23 08:30 Received: 06/26/23 10:50 Matrix: Water
#1 FIRE PON
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE Analytical Method:EPA 625.1 Preparation Method:EPA 625.1
Pace Analytical Services-Charlotte
Fluorene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 22:50 86-73-7
Hexachloro-1,3-butadiene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 22:50 87-68-3
Hexachlorobenzena ND ug/L 4.2 1 06/28/23 08:51 06/29/23 22:50 118-74-1
Hexachlorocyclopentadiene ND ug/L 8.3 1 06/28/23 08:51 06/29/23 22:50 77-47-4
Hexachloroethane ND ug/L 4.2 1 06/28/23 08:51 06/29/23 22:50 67-72-1
Indeno(1,2,3-ed)pyrene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 22:50 193-39-5
Isophorone ND ug/L 8.3 1 06/28/23 08:51 06/29/23 22:50 78-59-1
Naphthalene ND ug/L 4.2 1 06!28!23 08:51 06/29/23 22:50 91-20-3
Nitrobenzene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 22:50 98-95-3
2-Nitrophenol ND ug/L 4.2 1 06/28/23 08:51 06/29/23 22:50 88-75-5
4-Nitrophenol ND ug/L 8.3 1 06/28/23 08:51 06/29/23 22:50 100-02-7
N-Nitrosodimethylamine ND ug/L 4.2 1 06/28/23 08:51 06/29/23 22:50 62-75-9
N-Nitroso-di-n-propylamine ND ug/L 4.2 1 06/28/23 08:51 06/29/23 22:50 621-64-7
N-Nitrosodiphenylamine ND ug/L 8.3 1 06/28/23 08:51 06/29/23 22:50 86-30-6
2,2'-Oxybis(1-chloropropane) ND ug/L 4.2 1 06/28/23 08:51 06/29/23 22:50 108-60-1
Pentachlorophenol ND ug/L 8.3 1 06/28/23 08:51 06/29/23 22:50 87-86-5
Phenanthrene ND ug/L 4.2 1 06!28/%3 03:51 06/29/23 22:50 85-01-8
Phenol ND ug/L 4.2 1 06/28/23 08:51 06/29/23 22:50 108-95-2
Pyrene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 22:50 129-00-0 L1
1,2,4-Trichlorobenzene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 22:50 120-82-1
2,4,6-Trichlorophenol ND ug/L 8.3 1 06/28/23 08:51 06/29/23 22:50 88-06-2
Surrogates
Nitrobenzene-d5(S) 102 % 10-120 1 06/28/23 08:51 06/29/23 22:50 4165-60-0
2-Fluorobiphenyl(S) 116 % 15-120 1 06/28/23 08:51 06/29/23 22:50 321-60-8
Terphenyl-d14(S) 138 % 11-131 1 06/28/23 08:51 06/29/23 22:50 1718-51-0 S3
Phenol-d6(S) 66 % 10-120 1 06/28/23 08:51 06/29/23 22:50 13127-88-3
2-Fluorophenol(S) 88 % 10-120 1 06/28/23 08:51 06/29/23 22:50 367-12-4
2,4,6-Tribromophenol(S) 127 % 10-137 1 06/28/23 08:51 06/29/23 22:50 118-79-6
624 Volatile Organics Analytical Method:EPA 624.1
Pace Analytical Services-Charlotte
Benzene ND ug/L 1.0 1 06/27/2319:48 71-43-2
Bromodichloromethane ND ug/L 2.0 1 06/27/2319:48 75-27-4
Bromoform ND ug/L 2.0 1 06/27/2319:48 75-25-2
Bromomethane ND ug/L 2.0 1 06/27/2319:48 74-83-9
Carbon tetrachloride ND ug/L 2.0 1 06/27/23 19:48 56-23-5
Chlorobenzene ND ug/L 2.0 1 06/27/2319:48 108-90-7
Chloroethane ND ug/L 2.0 1 06/27/2319:48 75-00-3
Chloroform ND ug/L 2.0 1 06/27/2319:48 67-66-3
Chloromethane ND ug/L 2.0 1 06/27/2319:48 74-87-3
Dibromochloromethane ND ug/L 2.0 1 06/27/2319:48 124-48-1 L1
1,2-Dichlorobenzene ND ug/L 2.0 1 06/27/2319:48 95-50-1
1,3-Dichlorobenzene ND ug/L 2.0 1 06/27/2319:48 541-73-1
1,4-Dichlorobenzene ND ug/L 2.0 1 06/27/2319:48 106-46-7
1,1-Dichloroethane ND ug/L 2.0 1 06/27/2319:48 75-34-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/06/2023 01:03 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 31

Pace Analytical Services,LLC
2225 Riverside Dr.
ace Asheville,NC 28804
[phone]
ANALYTICAL RESULTS
Project: STORMWATER
Pace Project No.: 92674434
Sample: STORMWATER OUTFALL Lab ID: 92674434002 Collected: 06/21/23 08:30 Received: 06/26/23 10:50 Matrix: Water
#2 NORTH DI
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
1664 SGT-HEM,TPH Analytical Method:EPA 1664B
Pace Analytical Services-Charlotte
Total Petroleum Hydrocarbons ND mg/L 4.8 1 07/05/23 12:49
625 RVE Analytical Method:EPA 625.1 Preparation Method:EPA 625.1
Pace Analytical Services-Charlotte
Acenaphthene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 83-32-9
Acenaphthylene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 208-96-8
Anthracene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21 59 120-12-7
Benzo(a)anthracene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 56-55-3
Benzo(a)pyrene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 50-32-8
Benzo(b)fluoranthene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 205-99-2
Benzo(g,h,i)perylene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 191-24-2
Benzo(k)fluoranthene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 207-08-9
4-Bromophenylphenyl ether ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 101-55-3
Butylbenzylphthalate ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 85-68-7
4-Chloro-3-methylphenol ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 59-50-7
bis(2-Chloroethoxy)methane ND ug/L 8.3 1 06/28/23 08:51 06/29/23 21:59 111-91-1
bis(2-Chloroethyl)ether ND ug/L 4.2 1 06/28/23 08:51 0E129/23 21-59 111-44-4
2-Chloronaphthalene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 91-58-7
2-Chlorophenol ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 95-57-8
4-Chlorophenylphenyl ether ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 7005-72-3
Chrysene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 218-01-9
Dibenz(a,h)anthracene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 53-70-3
3,3'-Dichlorobenzidine ND ug/L 8.3 1 06/28/23 08:51 06/29/23 21:59 91-94-1 IL
2,4-Dichlorophenol ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 120-83-2
Diethylphtha late ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 84-66-2 L1
2,4-Dimethylphenol ND ug/L 8.3 1 06/28/23 08:51 06/29/23 21:59 105-67-9 L1
Dim ethylphthalate ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 131-11-3 L1
Di-n-butylphthalate ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 84-74-2 L1
4,6-Dinitro-2-m ethyl phenol ND ug/L 8.3 1 06/28/23 08:51 06,129/23 21:59 534-52-1
2,4-Dinitrophenol ND ug/L 41.7 1 06/28/23 08:51 06/29/23 21:59 51-28-5
2,4-Dinitrotoluene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 121-14-2
2,6-Dinitrotoluene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 606-20-2
Di-n-octylphthalate ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 117-84-0
bis(2-Ethylhexyl)phthalate ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 117-81-7
Fluoranthene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 206-44-0
Fluorene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 86-73-7
Hexachloro-1,3-butadiene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 87-68-3
Hexachlorobenzene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21.59 118-74-1
Hexachlorocyclopentadiene ND ug/L 8.3 1 06/28/23 08:51 06/29/23 21:59 77-47-4
Hexachloroethane ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 67-72-1
Indeno(1,2,3-cd)pyrene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 193-39-5
Isophorone ND ug/L 8.3 1 06/28/23 08:51 06/29/23 21:59 78-59-1
Naphthalene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 91-20-3
Nitrobenzene ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 98-95-3
2-Nitrophenol ND ug/L 4.2 1 06/28/23 08:51 06/29/23 21:59 88-75-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/06/2023 01:03 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 31

Pace Analytical Services,LLC
2225 Riverside Dr.
?ace" Asheville,NC 28804
[phone]
ANALYTICAL RESULTS
Project: STORMWATER
Pace Project No.: 92674434
Sample: STORMWATER OUTFALL Lab ID: 92674434002 Collected: 06/21/23 08:30 Received: 06/26/23 10:50 Matrix: Water
#2 NORTH DI
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Quaff
624 Volatile Organics Analytical Method:EPA 624.1
Pace Analytical Services-Charlotte
Tetrachloroethene ND ug/L 2.0 1 06/27/23 20:06 127-18-4
Toluene ND ug/L 1.0 1 06/27/23 20:06 108-88-3
1,1,1-Trichloroethane ND ug/L 2.0 1 06/27/23 20:06 71-55-6
1,1,2-Trichloroethane ND ug/L 2.0 1 06/27/23 20:06 79-00-5
Trichloroethene ND ug/L 2.0 1 06/27/23 20:06 79-01-6
Trichlorofluoromethane ND ug/L 2.0 1 06/27/23 20:06 75-69-4 L1
Vinyl chloride ND ug/L 2.0 1 06/27/23 20:06 75-01-4
Surrogates
4-Bromofluorobenzene(S) 98 % 70-130 1 06/27/23 20:06 460-00-4
Toluene-d8(S) 101 % 70-130 1 06/27/23 20:06 2037-26-5
1,2-Dichloroethane-d4(S) 110 % 70-130 1 06/27/23 20:06 17060-07-0
2540D Total Suspended Solids Analytical Method:SM 254OD-2015
Pace Analytical Services-Asheville
Total Suspended Solids 4.6 mg!L 2.5 1 06/26/23 16:33
420.4 Phenolics,Total Analytical Method:EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services-Asheville
Phenolics,Total Recoverable ND mg/L 0.020 1 07/01/23 09:48 07/01/23 12:55 64743-03-9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/06/2023 01:03 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 31

Pace Analytical Services,LLC
2225 Riverside Dr.
aceo Asheville,NC 28804
[phone]
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92674434
QC Batch: 783588 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92674434001
METHOD BLANK: 4063929 Matrix: Water
Associated Lab Samples: 92674434001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Cadmium ug/L ND 1.0 06/30/23 00:22
Chromium ug/L ND 5.0 06/30/23 00:22
Copper ug/L ND 5.0 06/30/23 00:22
Lead ug/L ND 5.0 06/30/23 00:22
Nickel ug/L ND 5.0 06/30/23 00:22
Silver ug/L ND 5.0 06/30/23 00:22
Zinc ug/L ND 10.0 06/30/23 00:22
LABORATORY CONTROL SAMPLE: 4063930
Spike LCS LCS %Rec
Parameter Units Cone. Result %Rec Limits Qualifiers
Cadrniun,. ug/L 500 441 88 85-115
Chromium ug/L 500 448 90 85-115
Copper ug/L 500 445 89 85-115
Lead ug/L 500 446 89 85-115
Nickel ug/L 500 442 88 85-115
Silver ug/L 250 221 88 85-115
Zinc ug/L 500 442 88 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4063931 4063932
MS MSD
92674314001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD Qual
Cadmium ug/L ND 500 500 511 502 102 100 70-130 2
Chromium ug/L 2910 500 500 3430 3410 104 99 70-130 1
Copper ug/L 4.8J 500 500 517 507 103 100 70-130 2
Lead ug/L ND 500 500 504 498 101 100 70-130 1
Nickel ug/L 5.0 500 500 513 505 102 100 70-130 2
Silver ug/L ND 250 250 255 251 102 100 70-130 2
Zinc ug/L 18.6 500 500 530 521 102 101 70-130 2
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4063933 4063934
MS MSD
92674566002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD Qua]
Cadmium ug/L ND 500 500 500 487 100 97 70-130 3
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/06/2023 01:03 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 31

Pace Analytical Services,LLC
2225 Riverside Dr.
ace" Asheville,NC 28804
[phone]
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92674434
QC Batch: 783254 Analysis Method: EPA 624.1
QC Batch Method: EPA 624A Analysis Description: 624 MSV
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92674434001,92674434002
METHOD BLANK: 4062224 Matrix: Water
Associated Lab Samples: 92674434001,92674434002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1-Trichloroethane ug/L ND 2.0 06/27/23 11:00
1,1,2,2-Tetrachloroethane ug/L ND 2.0 06/27/23 11:00
1,1,2-Trichloroethane ug/L ND 2.0 06/27/23 11:00
1,1-Dichiometharle ug/L ND 2.0 06/27,2311:00
1,1-Dichloroethene ug/L ND 2.0 06/27i2311:00
1,2-Dichlorobenzene ug/L ND 2.0 06/27/23 11:00
1,2-Dichloroethane ug/L ND 2.0 06/27/23 11:00
1,2-Dichloropropane ug/L ND 2.0 06/27/23 11:00
1,3-Dichlorobenzene ug/L ND 2.0 06/27/23 11:00
1,4-Dichlorobenzene ug/L ND 2.0 06/27/23 11:00
Benzene ug/L ND 1.0 06/27/23 11:00
Bromodichloromethane ug/L ND 2.0 06/27/23 11:00
Bromoform ug/L ND 2.0 06/27/23 11:00
Bromomethane ug/L ND 2.0 06/2712311.00
Carbon tetrachloride ug/L ND 2.0 06/27/23 11:00
Chlorobenzene ug/L ND 2.0 06/27/23 11:00
Chloroethane ug/L ND 2.0 06/27/23 11:00
Chloroform ug/L ND 2.0 06/27/23 11:00
Chloromethane ug/L ND 2.0 06/27/23 11:00
cis-1,2-Dichloroethene ug/L ND 2.0 06/27/23 11:00
cis-1,3-Dichloropropene ug/L ND 2.0 06/27/23 11:00
Dibromochloromethane ug/L ND 2.0 06/27/23 11:00
Ethylbenzene ug/L ND 1.0 06/27/23 11:00
Methylene Chloride ug/L ND 2.0 06/27/23 11:00
Tetrachloroethene ug/L ND 2.0 06/27/23 11:00
Toluene ug/L ND 1.0 06/27/23 11:00
trans-1,2-Dichloroethene ug/L ND 2.0 06/27/23 11:00
trans-1,3-Dichloropropene ug/L ND 2.0 06/27/23 11:00
Trichloroethene ug/L ND 2.0 06/27/23 11:00
Trichlorofluoromethane ug/L ND 2.0 06/27/23 11:00
Vinyl chloride ug/L ND 2.0 06/27/23 11:00
1,2-Dichloroethane-d4(S) % 105 70-130 06/27/23 11:00
4-Bromofluorobenzene(S) % 97 70-130 06/27/23 11:00
Toluene-d8(S) % 102 70-130 06/27/23 11:00
LABORATORY CONTROL SAMPLE: 4062225
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,1,1-Trichloroethane ug/L 20 23.3 116 70-130
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/06/2023 01:03 PM without the written consent of Pace Analytical Services,LLC. Page 13 of 31

Pace Analytical Services,LLC
2225 Riverside Dr.
aceo Asheville,NC 28804
[phone]
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92674434
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4062226 4062227
MS MSD
92674289001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
1,2-Dichloropropane ug/L ND 20 20 23.5 24.7 117 123 70-156 5
1,3-Dichlorobenzene ug/L ND 20 20 23.1 23.9 116 120 70-143 4
1,4-Dichlorobenzene ug/L ND 20 20 22.4 23.9 112 120 70-142 7
Benzene ug/L ND 20 20 23.2 23.8 116 119 70-142 3
Bromodichloromethane ug/L 2.7 20 20 25.2 26.5 113 119 70-139 5
Bromoform ug/L ND 20 20 20.4 22.9 102 115 64-140 12
Bromomethane ug/L ND 20 20 13.7 17.4 69 87 28-192 24
Carbon tetrachloride ug/L ND 20 20 24.3 26.4 121 132 70-140 8
Chlorobenzene ug/L ND 20 20 23.4 24.8 117 124 70-141 6
Chloroethane ug/L ND 20 20 23.4 24.2 117 121 58-191 3
Chloroform ug/L 12.5 20 20 35.9 37.5 117 125 70-138 4
Chloromethane ug/L ND 20 20 20.7 22.5 103 112 43-162 8
cis-1,2-Dichloroethene ug/L ND 20 20 22.1 23.8 111 119 70-143 7
cis-1,3-Dichloropropene ug/L ND 20 20 21.9 23.5 109 117 68-151 7
Dibromochloromethane ug/L ND 20 20 23.0 25.7 114 127 70-144 11
Ethylbenzene ug/L ND 20 20 23.9 25.7 119 128 70-143 7
Methylene Chloride ug/L ND 20 20 21.5 23.4 108 117 70-144 8
Tetrachloroethene ug/L ND 20 20 24.3 25.2 122 126 70-143 3
Toluene ugrl, ND 20 20 21.7 22.7 108 1?,i 69-144 5
trans-1,2-Dichloroethene ug/I_ ND 20 20 22.5 24.5 113 122 70-151 8
trans-1,3-Dichloropropene ug/L ND 20 20 21.0 22.8 105 114 70-139 8
Trichloroethene ug/L ND 20 20 22.6 24.2 113 121 70-142 7
Trichlorofluoromethane ug/L ND 20 20 23.3 24.9 116 125 62-146 7
Vinyl chloride ug/L ND 20 20 20.8 21.6 104 108 61-162 4
1,2-Dichloroethane-d4(S) % 103 103 70-130
4-Bromofluorobenzene(S) % 97 97 70-130
Toluene-d8(S) % 100 98 70-130
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:07/06/2023 01:03 PM without the written consent of Pace Analytical Services,LLC. Page 15 of 31

Pace Analytical Services,LLC
2225 Riverside Dr.
aced Asheville,NC 28804
[phone]
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92674434
METHOD BLANK: 4062166 Matrix: Water
Associated Lab Samples: 92674434001,92674434002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Hexachloroethane ug/L ND 5.0 06/28/23 11:30
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 06/28/23 11:30
Isophorone ug/L ND 10.0 06/28/23 11:30
N-Nitroso-di-n-propylamine ug/L ND 5.0 06/28/23 11:30
N-Nitrosodimethylamine ;ig/L ND 5.0 06/28/23 11:30
N-Nitrosodiphenylamine ug/L ND 10.0 06/28/23 11:30
Naphthalene ug/L ND 5.0 06/28/23 11:30
Nitrobenzene ug/L ND 5.0 06/28/23 11:30
Pentachlorophenol ug.'L ND 10.0 06/28/23 11:30
Phenanthrene ug/L ND 5.0 06/28/23 11:30
Phenol ug/L ND 5.0 06/28/23 11:30
Pyrene ug/L ND 5.0 06/28/23 11:30
2,4,6-Tribromophenol(S) % 107 10-137 06/28/23 11:30
2-Fluorobiphenyl(S) % 74 15-120 06/28/23 11:30
2-Fluorophenol(S) % 65 10-120 06/28/23 11:30
Nitrobenzene-d5(S) % 87 10-120 06/28/23 11:30
Phenol-d6(S) % 50 10-120 06/28/23 11:30
Terphenyl-d14(S) % 103 11-131 06/28/23 11:30
LABORATORY CONTROL SAMPLE: 4062167
Spike LCS LCS %Rec
Parameter Units Cone. Result %Rec Limits Qualifiers
1,2,4-Trichlorobenzene ug/L 50 48.9 98 44-142
2,2'-Oxybis(1-chloropropane) ug/L 50 57.0 114 36-166
2,4,6-Trichlorophenol ug/L 50 60.8 122 37-144
2,4-Dichlorophenol ug/L 50 59.3 119 1-191
2,4-Dimethylphenol ug/L 50 96.9 194 32-119 L1
2,4-Dinitrophenol ug/L 250 326 131 1-181
2,4-Dinitrotoluene ug/L 50 62.0 124 39-139
2,6-Dinitrotoluene ug/L 50 65.1 130 50-158
2-Chloronaphthalene ug/L 50 54.5 109 60-118
2-Chlorophenol ug/L 50 49.1 98 23-134
2-Nitrophenol ug/L 50 57.2 114 29-182
3,3'-Dichlorobenzidine ug/L 100 131 131 1-262
4,6-Dinitro-2-methylphenol ug/L 100 126 126 1-181
4-Bromophenylphenyl ether ug/L 50 60.9 122 53-127
4-Chloro-3-methylphenol ug/L i 00 118 118 22-147
4-Chlorophenylphenyl ether ug/L 50 59.4 119 25-158
4-Nitrophenol ug/L 250 183 73 1-132
Acenaphthene ug/L 50 58.1 116 47-145
Acenaphthylene ug/L 50 57.3 115 33-145
Anthracene ug/L 50 53.7 107 1-166
Benzo(a)anthracene ug/L 50 62.6 125 33-143
Benzo(a)pyrene ug/L 50 58.3 117 17-163
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/06/2023 01:03 PM without the written consent of Pace Analytical Services,LLC. Page 17 of 31

Pace Analytical Services,LLC
2225 Riverside Dr.
aced Asheville,NC 28804
[phone]
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92674434
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4063369 4063370
MS MSD
92674162001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
2,4-Dimethylphenol ug/L ND 100 100 163 149 163 149 32-119 9 MO
2,4-Dinitrophenol ug/L ND 500 500 673 640 135 128 1-181 5
2,4-Dinitrotoluene ug/L ND 100 100 107 101 107 101 39-139 6
2,6-Dinitrotoluene ug/L ND 100 100 107 103 107 103 50-158 4
2-Chioronaphthalene ug/L ND 100 100 88.5 86.0 89 86 60-118 3
2-Chiorophenol ug/L ND 100 100 92.3 83.6 92 84 23-134 10
2-Nitrophenol ug/L ND 100 100 106 98.1 106 98 29-182 7
3,3'-Dichlorobenzidine ug/L ND 200 200 173 179 86 90 1-262 4
4,6-Dinitro-2-methylphenol ug/L ND 200 200 240 236 120 118 1-181 2
4-Bromophenylphenyl ether ug/L ND 100 100 102 96.3 102 96 53-127 5
4-Chloro-3-methylphenol ug/L ND 200 200 213 188 107 94 22-147 13
4-Chlorophenylphenyl ether ug/L ND 100 100 100 94.5 100 95 25-158 6
4-Nitrophenol ug/L NU 500 500 373 353 75 71 1-132 6
Acenaphthene ug/L ND 100 100 94.6 89.8 95 90 47-145 5
Acenaphthylene ug/L ND 100 100 94.1 88.4 94 88 33-145 6
Anthracene ug/L ND 100 100 90.0 86.6 90 87 1-166 4
Benzo(a)anth race ne ug/L ND 100 100 107 100 107 100 33-143 7
Benzo(a)pyrene ug/L ND 100 100 102 96.0 102 96 17-163 6
BFrrzo(b)fuoranthene ug/L ND 100 1t0 111 107 111 107 24-159 4
Senzo(g,h,i)perylene ug/L ND 100 100 92.6 89.9 93 90 1-219 3
Benzo(k)fluoranthene ug/L ND 100 100 102 97.1 102 97 11-162 5
bis(2-Chloroethoxy)methane ug/L ND 100 100 92.8 83.3 93 83 33-184 11
bis(2-Chloroethyl)ether ug/L ND 100 100 95.1 84.0 95 84 12-158 12
bis(2-Ethylhexyl)phthalate ug/L ND 100 100 119 111 119 111 8-158 7
Butylbenzylphthalate ug/L ND 100 100 115 112 115 112 1-152 3
Chrysene ug/L ND 100 100 100 95.0 100 95 17-168 5
Di-n-butylphthalate ug/L ND 100 100 101 96.5 101 97 1-118 4
Di-n-octylphthalate ug/L ND 100 100 115 113 115 113 4-146 2
Dibenz(a,h)anthracene ug/L ND 100 100 96.7 91.3 97 91 1-227 6
Diethyiphthalate ug/L ND 100 100 102 95.1 102 95 1-114 7
Dimethylphthalate ug/L ND 100 100 98.4 93.9 98 94 1-112 5
Fiuoranthene ug/L ND 100 100 97.8 95A 98 95 26-137 3
Fluorene ug/L ND 100 100 99.7 94.4 100 94 59-121 5
Hexachloro-1,3-butadiene ug/L ND 100 100 66.5 69.3 66 69 24-116 4
Hexachlorobenzene ug/L ND 100 100 98.9 94.2 99 94 1-152 5
Hexachlorocyclopentadiene ug/L ND 100 100 84.1 80.6 84 81 25-150 4
Hexachloroethane ug/L ND 100 100 45.7 50.5 46 51 40-113 10
Indeno(1,2,3-cd)pyrene ug/L ND 100 100 97.5 93.4 97 93 1-171 4
Isophorone ug/L ND 100 100 97.6 88.1 98 88 21-196 10
N-Nitroso-di-n-propylamine ug/L ND 100 100 96.9 86.1 97 86 1-230 12
N-Nitrosodimethylamine ug/L ND 100 100 101 88.2 101 88 25-150 13
N-Nitrosodiphenylamine ug/L ND 100 100 97.3 92.1 97 92 25-150 5
Naphthalene ug/L ND 100 100 79.7 75.7 80 76 21-133 5
Nitrobenzene ug/L ND 100 100 91.8 83.4 92 83 35-180 10
Pentachlorophenol ug/L ND 200 200 219 209 109 105 14-176 5
Phenanthrene ug/L ND 100 100 95.4 91.5 95 91 54-120 4
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/06/2023 01:03 PM without the written consent of Pace Analytical Services,LLC. Page 19 of 31

Pace Analytical Services,LLC
2225 Riverside Dr.
ace Asheville,NC 28804
[phone]
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92674434
QC Batch: 783041 Analysis Method: SM 2540D-2015
QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92674434001,92674434002
METHOD BLANK: 4061424 Matrix: Water
Associated Lab Samples: 92674434001,92674434002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 06/26/23 16:32
LABORATORY CONTROL SAMPLE: 4061425
Spike LCS LCS %Rec
Parameter Units Cone. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 250 254 101 90-110
SAMPLE DUPLICATE: 4061768
92674121002 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 75.0 76.0 1
SAMPLE DUPLICATE: 4061769
92674397001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 220 220 0
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/06/2023 01:03 PM without the written consent of Pace Analytical Services,LLC. Page 21 of 31

Pace Analytical Services,LLC
2225 Riverside Dr.
aeeo Asheville,NC 28804
[phone]
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92674434
QC Batch: 784086 Analysis Method: EPA 420.4 Rev 1.0 1993
QC Batch Method: EPA 420.4 Rev 1.0 1993 Analysis Description: 420.4 Phenolics
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92674434001,92674434002
METHOD BLANK: 4066467 Matrix: Water
Associated Lab Samples: 92674434001,92674434002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phenolics,Total Recoverable mg/L v ND 0.020 07/01/23 12:16 '
LABORATORY CONTROL SAMPLE: 4066468
Spike LCS LCS %Rec
Parameter Units Cone. Result %Rec Limits Qualifiers
Phenolics,Total Recoverable mg/L 0.05 0.052 105 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4066469 4066470
MS MSD
92673461001 Spike Spike MS MSD MS MSD %Rec
Parameter Uits Result Cone. Cone. Result Result %Rec ? Re., Limits RPD Qual
Phenolics,Total Recoverable mg/L ND 0.05 0.05 0.090 0.046 180 92 90-110 65 M1,R1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4066471 4066472
MS MSD
92673461002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD Qual
Phenolics,Total Recoverable mg/L ND 0.05 0.05 0.051 0.050 103 100 90-110 3
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/06/2023 01:03 PM without the written consent of Pace Analytical Services,LLC. Page 23 of 31

Pace Analytical Services,LLC
2225 Riverside Dr.
ace© Asheville,NC 28804
[phone]
QUALITY CONTROL DATA
Project: STORMWATER
Pace Project No.: 92674434
QC Batch: 784106 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92674434001
METHOD BLANK: 4066548 Matrix: Water
Associated Lab Samples: 92674434001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mg/L ND 25.0 06/30/23 16:38
LABORATORY CONTROL SAMPLE: 4066549
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 756 101 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4066550 4066551
MS MSD
92674093001 Spike Spike MS MSD MS MSD %Rec
Parameter Units i?r uit :,o,?C. Conc. Result Result %Rec %Rec Limits RP:? Qual
Chemical Oxygen Demand mg/L 99.4 100 100 189 182 90 83 90-110 4 M1,R1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4066552 4066553
MS MSD
92674414004 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 32.7 100 100 145 136 113 104 90-110 7 M1,R1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/06/2023 01:03 PM without the written consent of Pace Analytical Services,LLC. Page 25 of 31

Pace Analytical Services,LLC
2225 Riverside Dr.
ace© Asheville,NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: STORMWATER
Pace Project No.: 92674434
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92674434001 STORMWATER OUTFALL#1 FIRE EPA 1664B 784869
PON
92674434002 STORMWATER OUTFALL#2 EPA 1664E 784869
NORTH DI
92674434001 STORMWATER OUTFALL#1 FIRE EPA 200.7 Rev 4.4 1994 783588 EPA 200.7 Rev 4.4 1994 783657
PON
92674434001 STORMWATER OUTFALL#1 FIRE EPA 625.1 783242 EPA 625.1 783480
PON
92674434002 STORMWATER OUTFALL#2 EPA 625.1 783242 EPA 625.1 783480
NORTH DI
92674434001 STORMWATER OUTFALL#1 FIRE EPA 624 1 783254
PON
92674434002 STORMWATER OUTFALL#2 -EPA 624.1 783254
NORTH DI
92674434001 STORMWATER OUTFALL#1 FIRE SM 2540D-2015 783041
PON
92674434002 STORMWATER OUTFALL#2 SM 2540D-2015 783041
NORTH DI
92674434001 STORMWATER OUTFALL#1 FIRE EPA 9040C 783947
PON
92674434001 STORMWATER OUTFALL#1 FIRE EPA 420.4 Rev 1.0 1993 784086 EPA 420.4 Rev 1.0 1993 784329
PON
92674434002 STORMWATER OUTFALL#2 EPA 420.4 Rev 1.0 1993 784086 EPA 420.4 Rev 1.0 1993 784329
NORTH DI
92674434001 STORMWATER OUTFALL#1 FIRE SM 4500-CN-E-2016 783185 SM 4500-CN-E-2016 783322
PON
92674434001 STORMWATER OUTFALL#1 FIRE SM 5220D-2011 784106 SM 5220D-2011 784219
PON
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/06/2023 01:03 PM without the written consent of Pace Analytical Services,LLC. Page 27 of 31

� DC#_TENo;:ENV-FRM-HUN1-0083 v02_Sample Condlttan Upon Rsaeipt.
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Note: Whenevert here it a disceepanty affecting North Carolina core p fiance samples;a copy of this formwiii besent to th'e North Ca-rolina D ENR Certi fication Office(I.e:
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Page 29 of 31

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Page 31 of-31