The URL can be used to link to this page

Home My WebLink AboutWQ0002052_Monitoring - 04-2023_20230508NC DEQ Division of Water Quality Information Processing Unit 1617 Mail Service Center Raleigh , N.C. 27699-1617 Dear Ground Water Specialist: May 5th, 2023 �,�v 0 8 2023 Re: Permit No. WQ0002052 Milliken & Co. Golden Valley Plant Attached are two copies of form GW-59 to include analysis data from the ground water monitoring wells. Also attached, form GW-59A. The pH field analysis for the monitor wells was performed by a certified operator from WaterTech Laboratories Inc. All required parameters are included. If you have any questions concerning this data or if there is anything else needed, please contact me at ( 828 ) 247-4313. Si cerely , Greg Marana Engineering Services Leader Milliken & Company Golden Valley Plant o = N O N w GW-59A COMPLIANCE REPORT FORM Permit # (Submit one each monitoring period with GW-59 forms.) 1 Enter date monitoring results were due. ( S- 1 - ) Will this monitoring report (GW-59 and GW-59A) YES be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES O IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? /f the answer is "Yes ",contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) repotted, and sample collection date for each occurrence (for the last two years). Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the Dermittee to a Notice of Violation, fines, and/or penalties. g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge. Signatur of Wermittee (or Authorized Agent) Date GW-59A 12/8/2003 SIIRMIT FORM ON YELLOW PAPER ONLY DEPARIWff&OF NMENTAL QUALITY - DIV. OF ESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 7/31/2028 Facility Name: Milliken and Company -Golden Valley Plant Non -Discharge W00002052 UIC Permit Name (if different): NPDES Other Facility Address: 2080 NC Hwy. 226 TYPE OF PERMITTED OPERATION BEING MONITORED Bostic (Street) NC 28018 County Rutherford ❑Lagoon El Remediation: Infiltration Gallery Icfty> (Sta'a) V,P) ❑■ Spray Field ❑ Remediation: Contact Person: Greg Marana Telephone#: 828-247-4300 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Monitor Well #6 (Upgradient) No. of wells to be sampled: 3 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): N76Y6 Date sample collected: 4/4/2023 FIELD ANALYSES: WAS Well Depth: 40 ft. Well Diameter: 2 in. pH 00400: 6.5 units Temp. 000lo: °C DRY at Depth to Water Level 82546: 37.5 ft. below measuring point Screened Interval: 29.5 ft. to 40 ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 2 ft. above land surface Relative M.P. Elevation: 1174.8 ft. Odor 00085: check Volume of water pumped/bailed before sampling: 1.22 gallons Appearance here:❑ Samples for metals were collected unfiltered: ❑ YES NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed: 4/18/2023 Laboratory Name: Water Tech and Meritech Certification No. 50 and 165 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 0.35 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method M ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # 8260D Total Ammonia 00610 <1.0 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.06-07-2018 RI IRMIT FORM ON YPI I OW PAPER ONLY MF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 7/31/2028 Facility Name: Milliken and Company -Golden Valley Plant Non -Discharge WQ0002052 UIC Permit Name (if different): NPDES Other Facility Address: 2080 NC Hwy. 226 TYPE OF PERMITTED OPERATION BEING MONITORED Bostic '" ") NC 28018 County Rutherford ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (State) (zip) K Spray Field ❑ Remediation: Contact Person: Greg Marana Telephone#: 828-247-4300 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Monitor Well #7 (Downgradient) No. of wells to be sampled: 3 ❑ Water Source Heat Pump ❑ Other: from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): N76Y7 Date sample collected: 4/4/2023 FIELD ANALYSES: WAS Well Depth: 30 ft. Well Diameter: 2 in. pH 0040o: 6.6 units Temp. 000lo: °C DRY at time ofsampling, Depth to Water Level 82546: 4.33 ft. below measuring point Screened Interval: 19 ft. to 29 ft. Spec. Cond. 00094: µMhos Measuring Point is 2 ft. above land surface Relative M.P. Elevation: 1106.2 ft. Odor 00085: check Volume of water pumped/bailed before sampling: 12.55 gallons Appearance here:❑ Samples for metals were collected unfiltered: ❑ YES NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed: 4/18/2023 Laboratory Name: Water Tech and Meritech Certification No. 50 and 165 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 0.33 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # 8260D Total Ammonia 00610 <1.0 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, N113as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOGS: mg/L vut, Kenr io GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAILS ERVICE CENTER, RALEIGH, INC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date //31/2028 Facility Name: Milliken and Company -Golden Valley Plant Non -Discharge W00002052 UIC Permit Name (if different): NPDES Other Facility Address: 2080 NC Hwy. 226 TYPE OF PERMITTED OPERATION BEING MONITORED Bostic (Street) NC 28018 CountyRutherford El Lagoon El Remediation: Infiltration Gallery (City) (Slate) (Zip) ❑■ Spray Field El Remediation: Contact Person: Greg Marana Telephone#: 828-247-4300 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Monitor Well #8 (Downgradient) No. of wells to be sampled: 3 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): N76Y8 Date sample collected: 4/4/2023 FIELD ANALYSES: WAS Well Depth: 30 ft. Well Diameter: 2 in. pH 0040o: 6.6 units Temp. 000lo: °C DRY at Depth to Water Level 82546: 8.167 ft. below measuring point Screened Interval: 19.5 ft. to 30 ft. Spec. Cond. 000sa: µMhos time ofsampling, Measuring Point is 2 ft. above land surface Relative M.P. Elevation: 1073.5 ft. Odor 00085: check Volume of water pumped/bailed before sampling: 10.68 gallons Appearance here:❑ Samples for metals were collected unfiltered: ❑ YES ❑■ NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed: 4/18/2023 Laboratory Name: Water Tech and Meritech Certification No. 50 and 165 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01o51 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 0.60 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 mg/L All -Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑■ Yes (1) ❑ No (0) pecific Conductance 00095 FtMhos K - Potassium 00937 mg/L VOC 7873 method # 8260D Total Ammonia 00610 <1.0 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NH3 as N. Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% 1dRTER rffcm LRRR,hm POST OFFICE BOX 1056 - #!5 PINEW000 PLAZA DR, GRANITE FALLS, NORTH CAROLINA 28630 (828)396-4444 SAMPLE: Milliken -Golden Valley Well#6 COLLECTION DATE., 4/4/2023 PERMIT #: COLLECTION TIME., 10:18 ADDRESS: Milliken & Co. RECEIVED DATE 4/4/2023 RL 2, Highway 226 RECEIVED TIME: 12:45 Bostic, NC 28018 REPORTED: 4/27/2023 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST . NO3 as N 0.35 mg#L 4/18/23 jsg VOC's meritech NH3 <1.0 mglL 4/6123 jrg LOG ID: 2304-023 REPORTED BY: NC CERTIFIED LAB # 50 fo0o" Tony Gragg, Lab Supervisor mimmrrCH L11911ac. POST OFFICE BOX 1056 ^ #5 PINEWOOD PLAZA DR. GRANITE FALLS, NORTH CAROLINA 28630 (828) 396-4444 SAMPLE., Milliken -Golden Valley Well#7 COLLECTION DATE: 4/4/2023 PERMIT #: COLLECTION TIME: 10:35 ADDRESS: Milliken & Co. RECEIVED DATE: 4/4/2023 Rt. 2, Highway 226 RECEIVED TIME: 12:45 Bostic, NC 28018 REPORTED: 4/27/2023 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST NO3 as N 0.33 mg;L 4118123 jsg VOC's meritech NH3 <1.0 mg!L 4/6123 irg LOG ID: 2304-024 REPORTED BY: NC CERTIFIED LAB # 50 fp� * Tony Gragg, Lab Supervisor morrarnirccm LR, ivs-mc. POST OFFICE BOX 1056 • #5 PINEWOOD PLA7.A DR. GRANITE FAILS, NORTH CAROLINA 28630 (828) 3964444 SAMPLE: Milliken -Golden Valley Well#8 COLLECTION DATE: 4/4/2023 PERMIT A COLLECTION TIME: 10:52 ADDRESS: Milliken & Co. RECEIVED DATE: 4/4/2023 Rt. 2, Highway 226 RECEIVED TIME. 12:46 Bostic, NC 28018 REPORTED: 4/27/2023 ANALYSIS ANALYSIS RESULTS UNITS DATE ANALYST NO3 as N 0.60 mg/L 4/18/23 isg VOC's medtech NH3 <1.0 mg/L 4/6/23 Jrg i LOG ID: 2304-025 REPORTED BY: NC CERTIFIED LAB # 50 Tony Gragg, Lab Supervisor Water Tech Labs Method SM 20 Ed 4500-H-2011 Wastewater pH BENCHSHEET Analysis Date Time Sam le ID Collection Date Time Results SU's Analyst 3 101 S Buffer 4.00 Buffer 10.00 ***** ***** jQ,QQ 01 q Buffer 7.00 QC ***** ***** ***** Slope Efficiency ***** ***** I Oar JAZ1l`►Or, 4 - -a3 10 t . s' 1039 11 i 11 3S 10ss 11 fi osa .� v ►� IOSa �'. �f� 00 �•0� BUFFERS: 4.00 LOT # 8208112 EXP AUG 2024 7.00 LOT # 8210229 EXP OCT 2024 10.00 LOT # 8206193 EXP JUN 2024 * NON REPORTABLE FOR NPDES COMPLIANCE MONITORING EXCEEDS HOLD TIME DUPLICATE/S f 0.1 SU'S Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Cathy Gragg Report Date: 4/19/2023 Client: Water Tech Labs, Inc 5 Pinewood Plaza Drive Granite Falls, NC 28630 Date Sample Rcvd: 4/5/2023 Meritech Work Order # 04052364 Sample: Milliken-MW #6 Grab 4/4/23 Ezra eters Bit Analysis Da#e Reporting Limit Method EPA 8260 Attached 4/13/23 - EPA 8260 Meritech Work Order # 04052365 Sample: Milliken-MW #7 Grab, 4/4/23 Parameters Resul Analysis Date R&po�ing Limit Method EPA 8260 Attached 4/13/23 - EPA 8260 Meritech Work Order # 040S2366 Sampler Milliken-MW #8 Grab 4/4/23 Parameters Result Analysis Date Reporting Limit Method EPA 8260 Attached 4/13/23 - EPA 8260 I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 MERITECH, INC. Environmental Laboratories . �r Laboratory Certificatlon #165 or Iff Client: Water Tech Labs, Inc. Meritech ID#: 04052364 Project: 8260D Analysis: 04/13/23 Client Sample ID: Milliken-MW # 6 Analyst: VWV Sample Collection: 04/04/23 Dilution Factor: 1 Report Date: 04/ 17/23 SW-846-8260D VOLATILE ORGANICS - Water Acetone < 5.00 ug/L cis-1,3-Dichloropropene < 0.500 ug/L Benzene < 0.500 ug/L trans-1,3-Dichloropropene < 0.500 ug/L Bromobenzene < 0.500 ug/L Ethanol < 50.0 ug/L Bromodichloromethane < 0.500 ug/L Ethyl benzene < 0.500 ug/L Bromochloromethane < 0.500 ug/L Hexachlorobutadiene < 0.500 ug/L Bromoform < 0.500 ug/L 2-Hexanone < 1.00 ug/L Bromomethane < 0.500 ug/L Isopropylbenzene < 0.500 ug/L 2-Butanone (MEIC) < 5.00 ug/L p-lsopropyltoluone < 0.500 ug/L n-Butylbenzene < 0.500 ug/L Methylene chloride < 0.500 ug/L, sec-Butylbenzene < 0.500 ug/L Methly Isobutyl Ketone (MIBK) < 0.500 ug/L tert-Butylbenzene < 0.500 ug/L Naphthalene < 0.500 ug/L Carbon Tetrachloride < 0.500 ug/L n-Propylbenzene < 0.500 ug/L Chlorobenzene < 0.500 ug/L Styrene < 0.500 ug/L Chl.oroethane < 0.500 ug/L 1,1,1,2-Tetrachloroetliane < 0.500 ug/L Chloroform < 0.500 ug/L 1,1,2,2-Tetrachloroethane < 0.500 ug/L Chloromethane <0.500 ug/L Tetrachloroethene(PCE) <0.500 ug/L 2-Chlorotoluene < 0.500 ug/L Toluene < 0.500 ug/L 4-Chlorotoluene < 0.500 ug/L 1, 1, 1 -Trichloroethane < 0.500 ug/L Dibromoehlorornethane <0:500 ug/L 1,1,2-Trichloroethane <0.500 ug/L 1,2-Dibromo-3-chlorop►-opane <0.500ug/L rrioliloroethene (TCE) <0.500 ug/L 1,2-Dibromoethane (EDB) < 0.500 ug/L 1,2,3-TrJohlorobenzene < 0.500 ug/L Dibroniomethane <0.500 ug/L 1,2,4-Trichlorobenzene <0.500 ug/L Dichlorodifluoromethane < 0.500 ug/L 1,2,3-Triehloropropane < 0.500 ug/L l,l-Dichloroethane < 0.500 ug/L Trichlorofluoromethane < 0.500 ug/L 1,2-Dichloroethane <0.500 ug/L 1,2,4-Trimethylbenzene < 0.500 ug/L 1,4-Dichlorobenzene <0.500 ug/L 1,3,5-Trimethylbenzene <0.500 ug/L 1,2-Dichlorobenzene <0.500 ug/L Vinyl acetate <.1.00 ug/L 1,3-Dichlorobenzene <0.500 ug/L Vinyl chloride <0.500 ug/L 1,1-Dichloroethene <0.500 ug/L rn/p-Xylenes < 1.00 ug/L cis-1,2-Dichloroethene < 0.500 ug/L o-Xylene < 0.500 ug/L trans-1,2-Dichloroethene <0.500 ug/L 1,2-Dichloropropane <0.500 ug/L Additional Compounds 1,3-Dichloropropane < 0.500 ug/L Methyl-tert-butyl ether (MTBE) < 0.500 ug/L 2,2-Dichloropropane < 0.500 ug(L Isopropyl ether (IPE) < 0.500 ug/L 1,1-Dichloropropene <0,500 ug/L 1,2-Dichloropropene <0.500 ug/L I hereby certify that I have reviewed and approve these data. Laboratory R et ative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * info@meritechlabs,com MERITECH, INC. Environmental Laboratories -d Laboratory Certification #166 Client: Water Tech Labs, Inc. Meritech ID#: 04052365 Project: 8260D Analysis: 04/13/23 Client Sample ID: Milliken MW # 7 Analyst: VWV Sample Collection: 04/04/23 Dilution Factor: 1 Report Date: 04/l7/23 SW-846-8260D VOLATILE ORGANICS -Water Acetone <5.00 ug/L cis-1,3-Dichloropropene <0.500 ug(L Benzene < 0,500 ug/L trans-1,3-Dichloropropene < 0.500 ug/L Bromobenzene < 0.500 ug/L Ethanol < 50.0 ug/L Bxoinodichloromethane < 0.500 ug/L Ethyl benzene < 0.500 4g/L Bromochloromethane < 0.500 ug/L Hexachlorobutadiene < 0.500 ug/L Bromoform < 0.500 u /I, 2-Hexanone < 1.00 ug/L Bromomethane < 0.500 ug/L lsopropylbenzene < 0.500 ug/L 2-Butanone (MEK) < 5.00 ug/L p-Isopropyltoluene < 0.500 iig/i., n-Butylbenzene < 0.500 tig/L Methylene chloride < 0.500 ug/L sec-Butylbenzene < 0.500 ug/L Methly isobutyl Ketone (MIRK) < 0.500 ug/L tert-B utyl benzene < 0.500 ug/L Naphthalene < 0.500 ug/L Carbon Tetrachloride < 0.500 ug/L n-Propylbenzene < 0.500 ug/L Chlorobenzene < 0.500 ug/L Styrene < 0.500 ug/L Chloroethane < 0.500 ug/L 1,1,1,2-Tetrachloroethane < 0.500 ug/L Chloroform < 0.500 ug/L 1,1,2,2-Tetrachloroethane < 0.500 ug/L Chloromethane < 0.500 ug/L Tetrachloroethene (PCE) < 0,500 ug/L 2-Chlorotoluene < 0.500 ug/L Toluene < 0.500 ug/L 4-Chlorotottiene <0.500 ug/L 1,1,.1-Trichioroethane <0.500 ug/L Dibromochloromethane <0.500 ug/L 1,1,2-Trichloroethane <0.500 ug/L 1,2-Dibromo-3-chloropropane < 0.500 ug/L Teichloroethene (TCE) <0.500 ug/L 1,2-Dibromoethane(EDB) <0,500 ug/L 1,2,3-Trichlorobenzene <0.500 ug/L Dibromomethane < 0.500 ug/L 1,2,4-Trichlorobenzene < 0.500 ug/L Dichlorodifluoromethane < 0.500 ug/L 1,2,3-Trichloropropane < 0.500 ug/L 1, 1 -Dichloroethane <0.500 ug/L Trichlorofluo.romethane <0.500 ug/L 1,2-Dichloroethene < 0.500 ug/L 1,2,4-Trimethylbenzene < 0.500 ug/L 1,4-Dichlorobenzene <0.500 ug/L 1,3,5-Trimethylbenzene <0.500 ug/L 1,2-Dichlorobenzene < 0.500 ug/L Vinyl acetate < 1.00 ugf.L 1,3-Dichlorobenzene < 0.500 ug/L Vinyl chloride < 0.500 ug/L 1, 1 -Dichloroethene < 0.500 ug/L m/p-Xylenes < 1.00 ug/L cis-1,2-Dichloroethene < 0.500 ug/L o-Xylene < 0.500 ug/L trans-1,2-Dichloroethene < 0.500 ug/L 1,2-Dichloropropane < 0.500 ug/L Additional Compounds 1,3-Dichloropropane < 0.500 ug/L Methyl-tert-butyl ether (MTBE) < 0.500 ug/L 2,2-Dichloropropane < 0.500 ug/L Isopropyl ether (1PE) < 0.500 ug/L l,l-Dlcliloropropene <0.500 ug/L 1,2-Dichloropropene <0.500 ug/L I hereby certify that I have reviewed and approve these data. Laboratory R se tive 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * info@meritechiabs.com MERITECH, INC. Environmental Laboratories Laboratory Certiflcation #165 Client: Water Tech Labs, Inc. Meritech ID#: 04052366 Project, 8260D Analysis: 04/13/23 Client Sample ID: Milliken-MW # 8 Analyst: VWV Sample Collection: 04/04/23 Dilution Factor: 1 Repot-t Date: 04117/23 S'W-846-8260D 'VOLATILE ORGANICS -Water Acetone < 5.00 ug/L cis-1,3-Dichloropropene < 0.500 tig/L Benzene <0.500 ug/L trans-1,3-Dichloropropene <0.500 tig/L Bromobenzene < 0.500 ug/L Ethanol < 50.0 ug/L Bromodi.chlorofnethane < 0.500 ug/L Ethyl benzene < 0.500 ug/L Bromochloromethane <O.S00 ug/L Hexachlorobutadiene <0.500 ug/L Bromoform <0.500 ug/L 2-Hexanone < 1.00 ug/L Bromomethane < 0.500 ug/L isopropylbenzene < 0.500 ug/L 2-'Butanone(MEK) <5.00 ug/L p4sopropyltoluene <0.500 ug/L n-Butylbenzene < 0.500 ug/L Methylene chloride < 0.500 ug/L sec-Butyibenzene <0.500 ug/L Methly Isobutyl Ketone (M1BK) <0.500 ug/L text-Butylbenzene < 0.500 ug/L Naphthalene c 0.500 tig/L Carbon Tetrachloride < 0.500 ug/L n-Propylbenzene < 0.500 ug/L, Chlorobenzene < 0.500 ug/L Styrene < 0.500 ug/L Chloroethane <0.500 ug/L 1,1,1,2-Tetrachloroethane <0.500 ug/L Chloroform <0.500 ug/L 1,1,2,2-Tetrachloroethane <0.500 ug/L Chloromethane < 0.500 ug/L Tetrachloroethene (PCE) < 0.500 ug/L 2-Ch lorotolvene < 0.500 ug/L Toluene < 0.500 ug/L 4-Chlorotoluene < 0.500 ug/L. 1,1,1-Trichloroethane < 0.500 ug/L Dibromochloromethane <0.500 ug/L 1,1,2-Tricltloroethane <0.500 ug/L 1,2-Dibrorno-3-chloropropane < 0.500 ug/L Trichloroethene (TCE) < 0.500 ug/L 1,20bromoethane (EDB) <0.500 ug/L 1,2,3-Trichlorobenzene <0.500 ug/L Dibromomethane 1< 0.500 ug/L 1,2,4-Tri.chlorobenzene < 0.500 ug1L Dichlorodifluoromethane < 0.500 ug/L 1,2,3-Trichloropropane < 0.500 ug/L 1,1-Dichloroethane < 0.500 ug/L 'rrichlorofluorosnethane < 0.500 ug/L 1,2-Dichloroethane < 0.500 ug/L 1,2,4-Trimethylbenzene < 0.500 ug/L 1.,4-Dichlorobenzene <0.500 ug/L 1,3,5-Trimethylbenzene <0.500 ug/L 1,2-Dichlorobenzene < 0.500 ug/L Vinyl acetate < 1.00 ug/L 1,3-Dichlorobenzene <0.500 ug/L Vinyl chloride <0.500 ug/L I,1-Dichloroethene < 0.500 ug/L nilp-Xylenes < 1.00 ug/L cis-1,2-Diichloroethene <0.500 ug/L o-Xylene < 0,500 ugh trans-1,2-Dichloroethene <0.500 ug/L 1,2-Dichloropropane <0.500 ug/L Additional Compounds 1,3-Dichloropropane < 0.500 ug/L Methyl-tert-butyl ether (MME) < 0.500 ug/L 2,2-Dichloropropane < 0.500 ug/L, isopropyl ether (IPE) < 0.500 ug/L I,1-Dichloropropene <0.500 ug/L 1,2-Dichloropropene < 0,500 ug/L I hereby certify that 1 have reviewed and approve these data. Laboratory Repr 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * info@meritechlabs.com 1