WQ0000889_Lab Data_19960921

PCs
Phos atev AURORA DIVISION
P.O. BOX 48, AURORA, NC 27806
August 21,1996
Ms. Betty Wilcox
Groundwater Section
Division of Environmental Management
North Carolina DEHNR
P. O. Box 29535
Raleigh, North Carolina 27626-0578
Re: Triennial Groundwater Monitoring
Results for PCS Phosphate's Domestic
Wastewater Treatment Plant
Permit No. WQ0000889
Dear Ms. Wilcox;
SEP 9895
ENV 'WANAGEMENT
�A
FA.
YE776VILLE REG. OFFICE c
� r
N
N �
CO
r
Attached are three (3) sets of groundwater analyses and an additional TOC analysis
for the the four (4) monitoring wells (WWMW #1, WWMW #2, WWMW #3 and
WWMW #4) for the PCS Phosphate - Aurora Division, Domestic Wastewater
Treatment Plant. These analyses are submitted to satisfy Specific Condition No. 2 of
Section IV, Groundwater Requirements, of the above referenced permit. Please note
that WWMW-1 (the up gradient well) & WWMW-2 (a down gradient well) initially
sampled high for TOC, 13.4mg/l & 10.5 mg/l respectively. As a precautionary
measure, both wells were resampled and sent out for TOC analysis per Specific
Condition No. 4 of Section IV, even though the WWMW-1 is considered to be the
background well. The additional sampling shows normal, 'low', TOC values for
both wells.
Please do not hesitate to contact me at [phone], should you require any
additional information pertaining to this matter.
Sincerely,
Leon M. Montg r3' o en ry
Environmental Affairs
Attachments
PC: W. Hardison (WaRO-DEM)
S. R. Phillips / 00-19-000 (w/o attch)
M. L. Asby / J. A. Hardy (w/o attch)
T. L. Baker / T. W. Davis [O&03-170-01-04 (w/attch)]
12-01-004-19 (w/attch)
12-01-009-05-000 (w/attch)

b DIVISION OF1ENVIRONM�ENTYALIMYU. � MENT y k
�.c::.# max+
GROUNDWp►TER`QUALITI( MONITORING° P;®. BOxi29535 '`r �<
ry
:c'a?`
COMPLIANCE REPORT£FORM i ,a RALEIGH C 27626 Os35 V sx
-�
"{919) 733 3221
Facility Name: PCS PHOSPHATE CO., INC. AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA. NC 27806
PERMIT NO.: WQ0000889
Non -Discharge Waste Water Treatment Plant
_Lagoon -Septic Tank(DrainField
X_SprnyField _SubsurfawLow-Pressure
Land Anal of Sludee
Well Location:
Waste Water Treatment Plant
Rotary Distributor x_other
Well LD. Number:
WWMW-1
Well Dept 21.50 Well Depth:
Well Diameter
2"
Sample (Screened) Interval
16.00
FT to
21.00 FT
Depth to Water Level
9.12
ft. below meas. pt.(before sampling) or
11.66
(MSL)
Measuring Point is
2.50 feet above land surface or
20.78 ft. (MSL)
Milliliters of water pumped before sampling
2100
Field Analysis: pH
7.2
Specific Conductance
925
uMhos Temp
23.3 oC Odor
NONE
Date Sample Collected
07/02/96
Date Lab Sample Analyzed 7/02-07/22
1994
Appearance: CLEAR
Laboratory Name
PCS Phosphate
Certification No. 330 AND 78
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES
X
NO
COD
N/A
mg/1
NO2 as N
N/A
mg/I
Ni - Nickel
N/A
mg/1
Coliform: MF Fecal
N/A
/100m1
NO3 as N
0.285
mg/I
Pb - Lead
N/A
mg/I
Coliform: MF Total
<1.0
/100ml
Phosphorus: Total as P
NIA
mg/I
Zn - Zinc
N/A
mg/1
Dissolved Solids: Total
804
mg/I
Al - Aluminum
N/A
mg/1
Pesticides/Herbicides (Specify)
pH (when analyzed)
7.3
units
Ba - Barium
N/A
mg/I
ug/I
TOC *
13.4
mg/I
Ca - Calcium
N/A
mg/I
ug/I
Chloride
3.3
mg/I
Cd - Cadmium
N/A
mg/I
ug/l
Arsenic
N/A
mg/I
Chromium: Total
N/A
mg/I
Other VOC
N/A
mg/I
Grease and Oils
N/A
mg/1
Cu - Copper
N/A
mg/I
Other MIBK
N/A
ug/I
Hardness: Total
N/A
mg/1
Fe - Iron
N/A
mg/I
Other Ag - Silver
N/A
mg/l
Phenol
N/A
mg/I
Hg - Mercury
N/A
mg/1
Other Se - Selenium
N/A
mg/I
Sulfate
N/A
mg/1
K - Potassium
N/A
mg/I
ug/I
Specific Conductance
N/A
uMohs
Mg - Magnesium
N/A
mg/I
ug/I
Total Ammonia(NH4 +NH3)
0.325
mg/I
Mn - Manganese
N/A
mg/1
Note: Values should reflect total concentrations
TKN as N N/A mg/I
Na - Sodium N/A mg/I
Note: Micro -Purge System used for sampling. * TOC resample 5.1 mg/l
I CERTIFY I
T REPORT IS TRUE AND ACCURATE
r�
SIGNATURE PERM TEE (OR AUTHORIZED AGENT)
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
�a
DATE

(. (.;I. LECTION AND ANALYSIS OF GROUNDWATER SAMPLES
1 ��lr�.r I;:: slurulcl It[ a(tah'zr.cl a:; ;;c�Urr a possiblu allar colleciium SAMPLES WHICH ARE HOT ANALYSED WITHIN THE HOLD11IG 11KIE SPECI-
FIED FOR THE METHOD USED (SEE 04. BELOW) MUST BE DISCARDED A14D NEW SAMPLES COLLECTED.
t:Ir�i ::liral� ;i;;;: I;:;ct �:!..urclrucl Molhod 3030C for sample pit,paration (rnr.rcury excluded). PQ-NOT FILTEH-METALS SAMPLE,9-I11 M1E.HEI.1► !!!
rr r ;r;rl s:3nrl-les nnrsl br: e:��llr�rled for motals, then field acidified with 5 ml concentrated nitric acid per liter of sample, and should be subnrilled Io I!11-
I,tt•:ilhirr 2.1 hc:rrr:-.
`,anrltlo prepar'rtion in Ille is holatory (extraction and filtration) must be cornplcled within 72 hours of collection.
Allf'.l. 'ISES ARE TO BE hIADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GIK1.IIIDWATEn, NOT THOSE THAT ARE A PABI OE 5-EDRAENT A SOCKED ►L� WELL C NS RUCTION Og aAMMNG PRDCEbU IES.
CHECK WITH YOUR LABORATORY 014 PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
As 1•-;r I ille 15. Hoilll Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
Ill( I;IIlowinrl publicalions, or by other methods approved beforehand by the Director, Division of Environmental
P.l,Irr trlerum It:
(a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental, Protection Agency publication rturrtber
EPA 600I4-79-020, as revised March 1983;
(c) Test Methods for Evaluating Solid Wastes: Physical/Cltentical Methods, 3rd Edition, 1986, U.S. Environmental Prbtec:liorr Agency
publication number SW-846;
(d) :Test Procedures for the Analysis of Polluanls Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in [lie well should be pumped or bailed prior to collecting a sample for analysis. 11 the well is pumped/bailed dry before-3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recornmendalions by the manufacturer.
9. Samples must be liltered through a 0.45 micron tiller immediately after collection when a dissolved analysis is required. (See 44. above)
10.The sarTtple container should be labeled at the lime of collection with the facility name, well identification number and dale and lime collected.
I I ."Authorized agent" is any corporate officer or public ollicial authorized by the company, corporation, or governmental body to sign official documents.

%WiMX j .Y'_.' ..7 k. •, .q..r.G.${,3>iaz.s J
DIVISION OF ENVIRONMENTAL M7A'NAGEMENT
-
.GROUNDWATER QUALITY MONITORING'. Pao Box29535
hill
COMPLIANCE REPORT FORM r�RAIEIGHNc27626 os35
...*
(919) 733=3221A
Facility Name: PCS PHOSPHATE CO., INC. AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: WQ0000889
Non -Discharge Waste Water Treatment Plant
_lagoon _Septic Tank/Drain Field
X Spray Field _Subsurface Low -Pressure
Land Appl of Sludge
Well Location:
Waste Water Treatment Plant
Rotary Distributor x_Other
Well I.D. Number:
WWMW-2
Well Dept 21.50 Ft.
Well Diameter
2"
Sample (Screened) Interval
16.00 FT to
21.00 FT
Depth to Water Level
10.84
ft. below meas. pt.(before sampling) or
10.00
(MSL)
Measuring Point is
2.50 feet above land surface or
20.84 ft. (MSL)
Milliliters of water pumped before sampling
2100
Field Analysis: pH
7.3
Specific Conductance
1656 uMhos Temp
25.2 oC Odor
NONE
Date Sample Collected
07/02/96
Date Lab Sample Analyzed 7/02-07/22
1994
Appearance: CLEAR
Laboratory Name
PCS Phosphate
Certification No. 330 AND 78
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES
X
NO
COD
N/A
mg/I
NO2 as N
N/A
mg/I
Ni - Nickel
N/A
mg/1
Coliform: MF Fecal
N/A
/100ml
NO3 as N
32.104
mg/I
Pb - Lead
N/A
mg/1
Coliform: MF Total
<1.0
/100m1
Phosphorus: Total as P
N/A
mg/I
Zn - Zinc
N/A
mg/l =
Dissolved Solids: Total
1088
mg/I
Al - Aluminum
N/A
mg/l
Pesticides/Herbicides (Specify)
pH (when analyzed)
7.4
units
Ba - Barium
N/A
mg/l
ug/l
TOC *
10.5
mg/l
Ca -Calcium
N/A
mg/1
u9/1-�
Chloride
263.3
mg/l
Cd - Cadmium
N/A
mg/I
ug/l .,
Arsenic
N/A
mg/I
Chromium: Total
N/A
mg/l
Other VOC
N/A
in
Grease and Oils
N/A
mg/I
Cu - Copper
N/A
mg/l
Other MIBK
N/A
u
Hardness: Total
N/A
mg/I
Fe - Iron
N/A
mg/I
Other Ag - Silver
N/A
mg/I
Phenol
N/A
mg/I
Hg - Mercury
N/A
mg/I
Other Se - Selenium
N/A
mg/l
Sulfate
N/A
mg/l
K - Potassium
N/A
mg/I
ug/l
Specific Conductance
N/A
uMohs
Mg - Magnesium
N/A
mg/I
ug/l
Total Ammonia(NH4 + NH3)
<0.10
mg/l
Mn - Manganese
N/A
mg/1
Note: Values should reflect total concentrations
TKN as N N/A mg/l
Na - Sodium N/A mg/l
Note: Micro -Purge system used for sampling. * TOC resample 5.5 mg/l
I CERTIFY TI- IS REPORT IS TRUE AND ACCURATE
SIGNATURE OF PE ITTEE (OR AUTHORIZED AGENT)
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
DATE

QQ1. LECTION AI4D ANALYSIS OF GROUNDWATER SAMPLES
��►i� ! I��; shcnrlcl I)� anal�z(:cl a:; ; cu�r� tr ; p�ssiblc: t.�llrr rollcrliurt. SAMPLES WHICH ARE IIOT ANALYSED WITHIN THE HOLDIIIG 1IME SPECI-
FIED FOR THE METHOD USED (SEE 44. BELOW) MUST BE DISCARDED AND NEW SAMPLES COLLECTED.
::'uurh•;i;;;: I; ;e �:!..ui:lrrr(1 f.l(;lhod 3030C for sample preparation (mercury excluder!). QQ-NDT FILTEH METALS SAh1Pl,E�_IiJ.1�lE_1=1E1.1) !!!
s:3nrf,lrrs nnrsl b!: cc-,llncled for metals, then field acidified with 5 rnl concentrated nitric acid per liter of sample, and should be submilled I�: !I��
lah •.1thirr 2.1
`;;un1)le plepar,rliorr in the hholatory (extinction and fillralion) must be completed within 72 hours of collection.
AlIPA ISES ARE TO BE MADE OF THE MOBILE C014STITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
GIU111IUWATER, NOT THOSE MAT ARE A PABI OE $EDI UIENT A S CIM.ED ILIILTF[j WELL CONS RLCS�QN Og AMP�(�G PR�CEpU�iES.
,CIIECK WITH YOUR LABORATORY 014 PROPERPROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
As 1•1!r I isle 15. Hoillr Carolina Adniinisir@live Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
Ihr fAlowing puhlicalions, or by other methods approved beforehand by the Director, Division of Environmental
t.1,i�•ulcmcnL•
(a) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17111 Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency. publication number
EPA-60014.79-020, as revised March 1983;
(c:) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986. U.S. Environrnenlal Protection Agency
publication number SW-846;
(d) -Test Procedures for the Analysis of Polluants.Under the Clean Water Act, Federal Register Vol. 49, No. 209. 40 CFR Part 136,
October 26, 1984;
5. MQas6ro and record the depth of water in the well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. II the well is pumped/bailed dry before 3 well
volrrrnes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination for pH. Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples rnust be filtered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See 44. above)
10.The sample container should be labeled at the time of 'colleclion with the facility name, well identification number and dale and time collected.
I I ."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official documents.

Facility Name: PCS PHOSPHATE CO., INC. AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA, NC 27806
PERMIT NO.: WQ0000889
Non -Discharge Waste Water Treatment Plant
_Lagoon _Septic Tw&Drain Feld
_X Spray Feld _Subsurface Low -Pressure
Land Aunt of Sludee
Well Location:
Waste Water Treatment Plant
Rotary Distributor
xOther
Well I.D. Number:
W WMW-3
Well Dept 21.50 Ft.
Well Diameter
2"
Sample (Screened) Interval
16.00 FT to
21.00 FT
Depth to Water Level
11.66
ft. below meas. pt.(before sampling) or
8.49
(MSL)
Measuring Point is
2.50 feet above land surface or
20.15 ft. (MSL)
Milliliters of watere pumped before sampling
2100
Field Analysis: pH
7.3
Specific Conductance
882 uMhos Temp
23.3 oC Odor
NONE
Date Sample Collected
07/02/96
Date Lab Sample Analyzed 7/2-7/22
1994
Appearance: CLEAR
LaboratoryName
PCS Phosphate
Certification No. 330 AND 78
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED YES
X
NO
COD
N/A
mg/1
NO2 as N
N/A
1119/1
Ni - Nickel
N/A
mg/l
Coliform: MF Fecal
N/A
/100m1
NO3 as N
0.001
1119/1
Pb - Lead
N/A
mg/l
Coliform: MF Total
<I.0
/1 OOmI
Phosphorus: Total as P
N/A
mg/1
Zn - Zinc
N/A
mg/1
Dissolved Solids: Total
756
mg/1
Al - Aluminum
N/A
mg/1
Pesticides/Herbicides (Specify)
C7
PH (when analyzed)
7.3
units
Ba - Barium
N/A
m9/1
ug/1
TOC
6.3
mg/1
Ca - Calcium
N/A
mg/l
ug/l
Chloride
6.1
mg/l
Cd - Cadmium
N/A
mg/1
ug/1
Arsenic
N/A
mg/l
Chromium: Total
N/A
mg/1
Other VOC
N/A
mg/1
Grease and Oils
N/A
mg/1
Cu - Copper
N/A
1119/1
Other MIBK
N/A
ug/l _
Hardness: Total
N/A
mg/l
Fe - Iron
N/A
1119/1
Other Ag - Silver
N/A
mg/1
Phenol
N/A
mg/1
Hg - Mercury
N/A
mg/l
Other Se - Selenium
N/A
mg/1
Sulfate
N/A
mg/1
K-Potassium
N/A
m9/1
ug/l
Specific Conductance
N/A
uMohs
Mg - Magnesium
N/A
m9/1
ug/l
Total Ammonia(NH4 + NH3)
<0.10
mg/1
Mn - Manganese
N/A
1119/1
Note: Values should reflect total concentrations
TKN as N N/A mg/1
Na - Sodium N/A mg/1
Note: Micro -Purge system used for sampling.
I CERTIFY THAT TH48,IIZEPORT IS TRUE AND ACCURATE
SIGNATURE OF PERMITTESE (OR AUTHORIZED AGENT)
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
DATE

Q(.A. LECTION AND ANALYSIS OF GROUNDWATER SAMPLES
1 �;r�� l I� ;: sl►oulcl fig anal`'<<.c1 8;);;cjort .1 ; possible altar colleclion. SAMPLES WHICH ARE HOT ANALYSED WITHIN THE HOLDIIIG 11ME SPECI-
FIED FOR THE METHOD USED (SEE 44. BELOW) MUST BE DISCARDED A14D NEW SAMPLES COLLECTED.
2. N1r•I•::' IInI •spa: I;;;c� :!..lrrcl:rr;l I.lothod 3030C for sample preparation (rrtcrcury excluded). QQ-NDT FILTER METALS SAh1Pl ES_IjJ 1HE.!=1ELl) !!!
h ' :i:rl s:3nrf,lr�s mist br: cc,llecled for metals, then field acidified with 5 rrll concentrated nitric acid per liter of sample, and should be subnIill()'cl to Ill—
lah -Jthili 2.1 h,,nw-.
`;anrlrle plep'llatiori ill flu; iaboullory (extinction and filtration) trust be completed within 72 hours of collection.
3 All"A 'ISES ARE TO BE MADE OF THE MOBILE C014STITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE
Gfl: I.111DWATER, NOT THOSE THAT ARE A PABI OF S_EDIjrAENT A SOCIATED WjTH WELL CONS TlUCTION Og SAMPLING PRQ.CEpl.1RES.
CHECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. As I•.!I I ille 15. Hol1lr Carolina Administrative Code. Subchapler 2L, analytical procedures shall be in accordance with the methods described in one of
Ih; following publications, or by olher methods approved beforehand by the Director, Division of Environmental
rdolI'll gnu rrt:
(a) Standard Methods lot the Examination of Water and Wastewater, 161h Edition, 1985 and 17th Edition, 1989, published )oinlly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication rlurrrber
EPA-600/4--79-020. as revised March 1983;
(c:) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Prolec:tion Agr:ru;y
publication number SW-846;
(d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209, 40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth of water in [lie well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis. If the well is pumped/balled dry before 3 well
volumes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Determination for pH, Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is
collected.
8. Field equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples must be filtered through a 0.45 micron lilter, immediately after collection when a dissolved analysis is required. (See #4. above)
10.The sample container should be labeled at the time of collection with the facility name, well identification number and dale and time collected.
11."Authorized agent" is any corporate officer or public official authorized by the company, corporation, or governmental body to sign official docurTlerlis.

Facility Name: PCS PHOSPHATE CO., INC. AURORA DIVISION County: BEAUFORT
Address P.O. BOX 48 AURORA. NC 27806
PERMIT NO.: WQ0000889
Non -Discharge Waste Water Treatment Plant
_Lagoon _Septic TankMrain Field
X SprayFeld _Subsurface Low -Pressure
Land Annl of Slud¢e
Well Location:
Waste Water Treatment Plant
RotaryDishibutor
x other
Well I.D. Number:
W WMW-4
Well Dept 21.50
Ft.
Well Diameter
2"
Sample (Screened) Interval
16.00 FT to
21.00 FT
Depth to Water Level
14.13 ft. below meas. pt.(before sampling) or
6.68 (MSL)
Measuring Point is
2.50
feet above land surface or
20.81 ft. (MSL)
Milliliters of water pumped before sampling
2100
Field Analysis: pH
7.1
Specific Conductance
1207
uMhos Temp
25.0 oC Odor
NONE
Date Sample Collected
07/02/96
Date Lab Sample Analyzed
7/02-07/22
1994
Appearance: CLEAR
Laboratory Name
PCS Phosphate
Certification No.
330 AND 78
SAMPLES FOR METALS WERE COLLECTED UNFILTERED AND FIELD ACIDIFIED
YES X
NO
COD
N/A
mg/1
NO2 as N
N/A
mg/1
Ni - Nickel
N/A
mg/1
Coliform: MF Fecal
N/A
/100ml
NO3 as N
0.3095
mgQ
Pb - Lead
N/A
mg/l
Coliform: MF Total
<1.0
/100m1
Phosphorus: Total as P
N/A
mg/1
Zn - Zinc
N/A
mg/1
Dissolved Solids: Total
826
mg/1
Al - Aluminum
N/A
1119/1
Pesticides/Herbicides (Specify)
pH (when analyzed)
7.4
units
Ba - Barium
N/A
m9/1
ug/1
TOC
8.05
mg/l
Ca - Calcium
N/A
m9/1
ug/1
Chloride
146.2
mg/1
Cd - Cadmium
N/A
m9/1
ug/l
Arsenic
N/A
mg/1
Chromium: Total
N/A
1119/1
Other VOC
N/A
m9/1 t r
'7
Grease and Oils
N/A
mg/1
Cu - Copper
N/A
mg/l
Other MIBK
N/A
ug/1 t
Hardness: Total
N/A
my/1
Fe - Iron
N/A
1119/1
Other Ag - Silver
N/A
mg/1
Phenol
N/A
mg/1
Hg - Mercury
N/A
m9/1
Other Se - Selenium
N/A
mg/l '
Sulfate
N/A
mg/1
K - Potassium
N/A
mg/1
ug/1 i J
Specific Conductance
N/A
uMohs
Mg - Magnesium
N/A
mg/1
ug/1 J
Total Ammonia(NH4 + NH3)
0.34
mg/1
Mn - Manganese
N/A
1119/1
Note: Values should reflect total concentrations
TKN as N N/A mg/l
Na - Sodium N/A mg/1 d
Note: Micro -Purge system used for sampling.
I CERTIFY THAT TI�I5k4_:PORT IS TRUE AND ACCURATE
SIGNATURE OF PERMITTED (OR AUTHORIZED AGENT)
Note: Values should reflect dissolved and
colloidal concentrations. (see #3 on back)
%)-'�4 )'O'l
DATE
rz

G("I. LECTION AND ANALySIS OF GROUNDWATER SAMPLES
1 ��rr� l I�r:: SI Ir)IlI(I b(i analvz(2(1 a:s : cu0n cm possiblu caller collection. SAMPLES WHICH ARE tIOT ANALYSED WITHIN THE HOLDIIIG TIME SPECI-
FIED FOR THE METHOD USED (SEE 04. BELOW) MUST BE DISCARDED AN:D NEW SAMPLES COLLECTED.
I.lothod 3030C for sample preparation (rnr..rcury excluded). t1QNDT FILTER METALS SAh1Pl,E� IjJ.1�iE-.I=1E1.1► !!!
s:3i111.11 rs must b!: cl.'Ilecled for metals, then lield acidified wilh.5 rnl concentrated nitric acid per liter of sample, and should be submilled lu Ill •
Int, --thin 2.1 1wm!-.
`;an1ple preparation in the f,It)Oratory (extiaclion and filtration) must be completed within 72 hours of collection.
3 AIIP 1. 'tSES ARE TO BE bIADE OF THE MOBILE CONSTITUENTS (DISSOLVED AS WELL AS COLLOIDAL) IN THE.
GIIL'IIIJUWATEfI, NOT THOSE THAT ARE A PLEL OF MOWER! A SOCIA�ED_Wfljj WELL C NS SUCTION OgAMPLlNG PROCEDURES.
CIIECK WITH YOUR LABORATORY ON PROPER PROCEDURES FOR SAMPLE COLLECTION AND PRESERVATION.
4. A!: I•-!r I isle 15. Hof Ili Carolina Administrative Code. Subchapter 2L, analytical procedures shall be in accordance with the methods described in one of
tlrr IAlowinrl publications, or by other methods approved beforehand by the Director, Division of Environmental
ra,�n•„ lernent: •
(ca) Standard Methods for the Examination of Water and Wastewater, 16th Edition, 1985 and 17th Edition, 1989, published jointly by
American Public Health Association, American Water Works Association and Water Pollution Control Federation;
(b) Methods for Chemical Analysis of Water and Waste, 1979, U.S. Environmental Protection Agency publication number
EPA-600,4.79-020. as revised March 1983;
(c;) Test Methods for Evaluating Solid Wastes: Physical/Chemical Methods, 3rd Edition, 1986, U.S. Environmental Protection Agency
publication number SW-846;
(d) Test Procedures for the Analysis of Polluants Under the Clean Water Act, Federal Register Vol. 49, No. 209.40 CFR Part 136,
October 26, 1984;
5. Measure and record the depth of water in the well prior to pumping or bailing any water from the well.
6. At least 3 volumes of water in the well should be pumped or bailed prior to collecting a sample for analysis.11 the well is pumped/bailed dry before 3 well
volrrrnes are removed, samples can be collected as soon as the well recovers to the point where enough water is available to collect your sample.
7. Delermination for pH. Specific Conductance, temperature, odor and appearance must be made in the field on unfiltered samples when the sample is
collected.
8. Fiold equipment must be calibrated in accordance with recommendations by the manufacturer.
9. Samples must be liltered through a 0.45 micron filter immediately after collection when a dissolved analysis is required. (See #4. above)
10.The sample container should be labeled at the tirrre of collection with the facility name, well identification number and dale and time collected.
I I ."Authorized agent" is any corporate officer or public ollicial authorized by the company, corporation, or governmental body to sign official documents.

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PCS PHOSPHATE CO.*-.INC. PCS G HO.SPHATE CO., INC.
MR. MIKE ASBY
P.O. BOX 48
AURORA, NC 2780E DATE COLLECTED.. 07/25/ G
REVIEWED Y.
601/602 SERIES: _
PURGABLE HALOCARBOI S; DOM. DOM. # TPZIP
PURGABLE AROMATICS WELL 01 WELL02 ' BLANK-'
BROMODICHLOROMETHANE,mg/l {0.0005 {0.0005 {0.0005. -.
BROMOFORM.wiq/1 {0.0005 <0`0005' {0.0005
BROMOMETHANE, mg/l {0.00.05' � <0..0005 0.0005.',
CARBONTETRACHLORIDE9m0/1 {0.0005... {0.0005 {0-.0005
`CHLOROBENZENE,mg/1" - <0.0005.-{0.0005 <0..0005
CHLOROETHANE, mg/1. {0.=0005 <0. 0005 t0. 0005
=CHLOROETHYLVINYL, mg/l, <0.0005 (0.0005 . W. 0005
CHOLOROF.ORM, mg/1 {0.0005 .{0.0005 (0'.0005
CHLOROMETHANE, mg/l (0.0005 . .'<0.0005- (& 0005:
D.LBROMOCHLOROMETHAM, mg/l - {0.0005 - (0.0005 {0..0005
1,2-DICHLOROBENZENE,mg/1 -{0.0005 {0.0005 {0e0005
113-DICHLOROBENZENE",mg/l <0.0005 -{0.0005 <0.0005
i,4-DICI-lLOROBEHZENE,mg/1 {0.0005 {0.0005 <0..0005
DICHLORODTELUOROIIETHANE,mg/l. <0.0005 {0.0005 {0.0005
11.1-DICHLORGETHANE,.mg/1 <0.0005 <0.0005_- _{0.0005-
1, 2-DICHLOROETHANE alg/l - (0.0005. {0.0005' <0.0005-
1,1-DICHLOROETHEHE, my/l {0. 0005 {O.-0005 <0.0005
trans-1,2"DICHLOROETHENE,mg/l .{0.0005 <00000 (0.0005
1, 2-DICHLOROPROPANE, wg/1'. <0. 0005. <0'. 0005 {00 0005
Cis-1, 3-D'o GHLOROPROPENE, rilg/l. ' {0. 0005 (0. 0005. (0.0005 "
trans-1, 3-D.ICHLOROPROPENE, mg/I <0.0005,... {0._0005-_. <0. 0005 "
'METHYLENE -CHLORIDE, nr'g/l. (0.0005 {0. 0005 ' <0.0005 ;
JETRACHLOROiETHAHL�nig/l' t0.0005 <0.0005 {0.0005
TETRACHLORO' ETHENE, mg/1 <0. 0005 <0. 0005 _ {0.0005
-I 1" 1,1. TRIGLOROE THANE., mg/1 - <0. 0005: ; . <0.:0005. (0.0005
191,2-TRICHLOROETHAI,IE,'nig/l <0.0005 <0.0005 {0.0005
TRICHLOROETHENE, mg/l ' ' <0.0005 - <0.0005 --<0.0005.
Tr` ICHLOROFLUOROMETHAIIE, mgil {0. 0005 ± "{0.0005 : {0.0005'
VINYL CHLORIDE,mg/l {0.000 <0.0005' {0.0005
BENZENE, mg/1 <0.-0005 <0.0005 {0.0005
CHLOROBENZENE;mg/l {0.0005 {0.0005 (P.0005
1,27DICHLORODENZENE,rng/l <0.0005 {0.0005 ;{0..0005
1, 3-DICHLOROBEHZENE-4 nig/1 <0.0005 {0.0005 (0.0005
1,4-DICHLORO,BENZENE,mg/1 0-0033 0.0036 0.'0008
ETHYLBE0ZE1%jE,'rng/1 ',-{0a0005':: <0.0005 {0.0005
TOLUENE,mg/l. <0.0005 {0.0005- {0..0005..'
Laboratory Analyses - Environmental Consultants
Form # 0069