NC0044440_Lab Report_20150428

Pace Analytical Services,Inc.
/� 1 9800 Kincey Ave. Suite 100
/ ar,P,Anal i al Huntersville,NC 28078
www.pacelabs.com [phone]
ORIGINAL
April 17, 2015
Larry Wright
Cherryville WWTP
1165 Mountain St
Cherryville, NC 28021 RECEIVED/DENR/DWR
APR 2 8 .2015
RE: Project: CHERRYVILLE BIOASSAY Water Quality
Permitting Section
Pace Project No.: 92244163
Dear Larry Wright:
Enclosed are the analytical results for sample(s) received by the laboratory on April 07, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stacy Tarle
[e-mail]
Project Manager
Enclosures
cc: Paige Green,Cherryville(City of)
Patty Hall,Cherryville(City of)
REPORT OF LABORATORY ANALYSIS
` NI; This report shall not be reproduced,except in full,
1461ii 59-lam without the written consent of Pace Analytical Services,Inc.. Page 1 of 7

ORIGINAL
Effluent Aquatic Toxicity Report Form -Acute Pass/Fail//il� Date 4- Ito-lb
Facility NPDES#NC O Pipe#(.LL County Q6'�1:1[l
Laboratory,*erformin Test
f W t m Comments wOg4 (f)7
Sign-r of Opera • ../esponsibl°C arge
Signature of Labora • Supervisgi
MAIL O R I G I N A L TO. DivEnvironmental!of Wate QualSity Branch
N.C.DENR
1621 Mail Service Center
North Carolina Acute Pass/Fail Toxicity Test Raleigh, North Carolina 27699-1621
Collection Date: -4-�-15 Organism Tested
Collection Time: Q6 fl
Test Start Date: A-4R=I5 \cr1QT �S mPV),�
SampleType/Duration
Control 2:�.
Grab Com.. Duration pH
0 o Treatment `
Hardness(mg/I .4
Spec.Cond.(pmhos I(p25 0 Control E
Chlorine(mg/I D.O.
Treatment EU
Sample temp. at receip y 0,(C
Mortality Replicate Mean Mortality
Treatment 1 (Control) A BCD
Treatment 2 (Exposure) A BC D
Concentration nfo0% % �% ^% 'll/o
Tested V
(NOTE: If mean control mortality exceedsl0%,the test is considered invalid)
Calculate using
Arc-Sine Calculated Student's t _ PASS
Square Root
transformed Tabular Student's t FAIL
data (ONE TAILED)
If the absolute value of the calculated t is less than or equal
to the absolute value of the tabular t,check PASS.
If the absolute value of the calculated t is greater than the
absolute value of the tabular t,check FAIL.
If all vessels within each treatment have the same response
but the treatment two response is greater than the control,check FAIL.
DWQ form AT-2(8/91)

Pace Analytical
Data Sheet for Acute Pass/Fail Test- Fathead minnow Pimephales promelas
Client: Q k\ \ft4\ \LQ, NPDES #: NC 0_04-i446 Reviewed by:
Test Organism:Ti .cls ,,.Qlc S Organism Born(Date/Time) �5 /i C 'Age of Organism: • I Time Fed: /2#Replicates per Treatment: JJ'4 Total Organisms per Vessel: 10 Test Vessel Size:552-P` Volume/Vessel: Z -v`Z--
Dilution Water Batch: I�J`t Temperature: 2-4,1' Randomized: \/ Incubator: (.3 ef'')
Start Date: 4--Si J Time: E`ZG Analyst: V(
End Date: "4-0)-16 Time: 4 I./ Analyst:
# Organisms # Alive after 24hrs D.O. Temp. pH Conductivity
exposed (mg/L) (°C) (µS/cm)
Total Chlorine Total
Concentration A BCD AB CD Alive 0 24 0 24 0 24 0 24 (mg/L) Hardness
(m'
Control
1() 10 ` 10 lO I® IU 4.2o 6,36.25.5,24g g.)C 1.0 162,s d,ci8 : {
r
¢9C> f
1U \C) 1 \(,) 10 l® i0 to 4o Co, oIO*D 240i:)2-41114)T-7,113-40 359,D -4:
Comments:
100% Sample:
PH- .
conductivity(µS/cm) -7499

•
Document Name:
Date Revised:June 22,2012 ti
1, BloalaSay Chain of Custody 5
1(1 UthentNumber: Page 1 of r i
k Issuing Authority: 1.
- ., 1 Cs 007;r�3v 01 Pace Carolinas Quality Mee '
ww«u xRN io-Ya.iw 1
Bioassay Chain ofCustody worm 2
Facility Name: . , . C. V
Address: S..
oc..t "i' P.4:Sox:
. Cker.c V�I(P /�T lPhone#: 7 .x5
S1% -11 „
1% tin .;.( __'� 73
3S 3° c>1' ` ' (1t of Contact: 11efr VUrA7 }
Give-r.i'ivi tle% oto - _
County: Sfon ....NFAVS permit# Op'��t`f Q pipe: S. c> . I
l ;
•%Effluent DiiutiQn(()NC): Test Method; 2 Pi o uc; ;re
Plant Flow: �p
1.
9
3 :
Sample Collector: Print j . ; i
Signature _ •MEW' )
Sample Type; H ; i
Composite a: ;y`}fi .7 C .. w_:. i ;
Date Started `. .: • � is-i9. i;s�,•
:uc:: E • ;
• date Irnded '_ � "_+i/•r PM
Samples per.Hr: or R ; f
Grab Per flcl n ` , 22:&,,..:::L. t
Date: • s
Trine: AM or PM • • 1
Sample.Volume: I,4E. I
• ;�r�$Jorg • i
1••'-
Y —Method ofTrahs
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:
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: :, �. �'Ro lit a y Date Tuna' Regie
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• rComments:
a
' ' ..Ibi i ce " Adios', Inc. Use Only:
Pace Work order Number: 22 4 t(.3
Receiving Temperature:
-' Received By
. ! F.,
Pace Analytical Services,Inc.Address:6709•Conference fir:;Raleigh,NC 27607 Phone:[phone]
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vv'uniern rvaniC. "��u"1 "v
aceAnalytical" Sam•le Condition U.on Recei.t SCUR Pa 1 of 2
Document Number: Issuing Authority:
F-CHR-CS-003-rev.15 Pace Huntersville Quality Office
`
Client Name: '�`r\,l,rryvii Il qe. ;A)I)-) 1 1 P
Courier: ❑ Fed Ex ❑ UPC] USPS❑ Client❑ Commercial❑ Pace Other rg6iil•Ltc1t�
-r b4 1
Custody Seal on Cooler/Box Present: ❑ yes 0---no Seals intact: ❑ yes ❑ no ,.Z`r14 � ® '. '° '� .ia
i °.., :..e ' s.aV4.4,sem'
Packing Material: ❑ Bubble v[p ❑ Bubble Bags ❑ None ❑ Other
Thermometer Used: IR Gun T1401 Type of Ice: Wet Blue None Samples on ice,cooling process has begun
Temp Correction Factor T1401 No Correction ,
�j Biological Tissue is Frozen: Yes No NIA Date and Initials of person examining
Corrected Cooler Temp.: P C contents: .3‘ 4.- 4 -1.15 •
Temp should be above freezing to 6°C Comments: ,
Chain of Custody Present: DYes ❑No ON/A 1. i
Chain of Custody Filled Out: DYes ONo ON/A 2.
Chain of Custody Relinquished: .DYes ONo ON/A 3.
Sampler Name&Signature on COC: ,DYes ONo ON/A 4.
Samples Arrived within Hold Time: QOYes ONo ON/A 5.
Short Hold Time Analysis (<72hr): ❑Yes DNo ON/A 6.
Rush Turn Around Time Requested: ❑Yes ONo ON/A 7.
Sufficient Volume: pYes ❑No ON/A 8.
Correct Containers Used: Wes ONo ON/A 9.
-Pace Containers Used: pies ONo ON/A
Containers Intact: ❑Yes ONo ON/A 10.
Filtered volume received for Dissolved tests DYes ONo ,ON/A 11.
Sample Labels match COC: DYes ONo ON/A 12.
-Includes date/time/ID/Analysis Matrix: uti
i"
.-
All
All containers needing preservation have been checked.
DYes ❑No ,,[3N/A 13.
All containers needing preservation are found to be in ❑Yes ONo ON/A
compliance with EPA recommendation.
exceptions: VOA, coliform,TOC,O&G,WI-DRO(water) DYes ❑No _
Samples checked for dechlorination: DYes ❑No j:?N/A 14.
Headspace in VOA Vials(>6mm): ❑Yes ONo ,ON/A 15.
Trip Blank Present: ❑Yes ONo ON/A 16.
Trip Blank Custody Seals Present DYes ❑No ,(IN/A
Pace Trip Blank Lot#(if purchased):
Client Notification/Resolution: Field Data Required? Y / N
Person Contacted: Date/Time:
Comments/Resolution:
SCURF Review: Date: Place label here
SRF Review: Date: OR
Note: Whenever there is a discrepancy affecting North Carolina compliance
samples,a copy of this form will be sent to the North Carolina DEHNR Handwrite project number
Certification Office(i.e out of hold,incorrect preservative,out of temp, (if no label available)
incorrect,:ontairieis)