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NCG510558_Application_20230929 (2)
ROY COOPER Governor ELIZABETH S. BISER Secretary RICHARD E. ROGERS, JR. Director Nathan Pinsker, Agent applicant for Aecom 5438 Wade Park Blvd Ste 200 Raleigh, NC 27607 Subject: Permit Application Application No. NCG510558 Speedway # 7997 Union County Dear Permittee: NORTH CAROLINA Environmental Quality October 02, 2023 The Water Quality Permitting Section acknowledges receipt of your application for a new NPDES WW permit, including supporting documentation and your check number 14592858 in the amount of $100.00 as payment of the application fee. These items were received in our offices on September 29, 2023. Your application will be assigned to a permit writer within the Section's NPDES WW permitting branch. The permit writer will contact you if additional information is required to complete evaluation of your application. Your timely and direct response to any such request will help to expedite the review process. Please note that acceptance of the application does not guarantee a NPDES permit will be issued for the proposed activity. A permit will only be issued following a complete review of the application, concluding the proposed discharge is allowable per applicable statutes and rules. Information regarding the status of your renewal application can be found online using the Department of Environmental Quality's Environmental Application Tracker at: https://dgq. nc.gov/permits-Mulations/permit-guidance/environmental-application-tracker If you have any additional questions about the permit, please contact the primary reviewer of the application using the links available within the Application Tracker. ec: WQPS Laserfiche File w/application Sincerely, 3-�L- Cynthia Demery Administrative Assistant Water Quality Permitting Section North Carolina Department of Environmental Quality I Division of Water Resources Mooresville Regional Office 1 610 East Center Avenue, Suite 301 1 Mooresville. North Carolina 28115 704.663.1699 General Discharge Permit NCG510000 /�_COM Imagined. /�� Delivered. September 27, 2023 Mr. Andrew Pitner North Carolina Department of Environmental Quality Water Quality Permitting Section 1617 Mail Service Center Raleigh, North Carolina 27699-1617 AECOM 5438 Wade Park Boulevard, Suite 200 Raleigh, INC 27607 USA T: 919.461.1100 F: 919.464.1415 aecom.com AECOM Project No. 60708764 RECENED Subject: General Discharge Permit NCG510000 SEP 2� 2023 Speedway Store No. 7997 6325 West Marshville Boulevard, NPpEs Marshville, North Carolina N'OEQIpWRI Dear Mr. Pitner, AECOM Technical Services of North Carolina, Inc. (AECOM), on behalf of Speedway, LLC (Speedway), is submitting this Application for Coverage Under General Permit NCG510000 for the Speedway Store No. 7997 (Site), located at 6325 West Marshville Boulevard, Marshville, North Carolina. The Site is operated by Speedway as a petroleum retail facility and convenience store. Speedway is proposing underground storage tank (UST) system replacement activities at the Site. Historically, groundwater depth has ranged from approximately 7 to 10 feet below ground surface (bgs) near the UST basin. Therefore, dewatering from the tank basin is anticipated. AECOM expects to discharge treated groundwater for approximately two weeks at an estimated flow of 20 to 170 gallons per minute (gpm) depending on the recharge rate of groundwater in the excavation. 170 gpm assumes worst case scenario and use of two pumps but will most likely be one pump working intermittently. AECOM proposes to pump groundwater to a 21,000-gallon frac tank and then treat it via 2,000-pound carbon vessels prior to discharge. Breakthrough calculations assume worst case scenario for flow and level of impacts. The treated groundwater would be discharged via aboveground piping to the Buck Branch (class C surface water) located approximately 235 feet west of the Site. AECOM sampled monitoring well MW-19, located downgradient of the tank field, on June 30, 2023 and analyzed for volatile organic compounds (VOCs) via standard Method (SM) 6200B, lead and total hardness via EPA Method 602013, total suspended solids (TSS) via SM2540D-2015, pH via SM4500-H+B- 2011, and total recoverable phenolics via EPA 420.4 Rev 1.0 1993. Carbon breakthrough was calculated using the current laboratory analytical data. If there are any questions or concerns regarding this report, please contact Nathan Pinsker at (919) 461-1559. Yours sincerely, Nathan Pinsker Project Manager Nathan. Pinsker L) aecom.com Marie Treiber Regional Senior Project Manager Marie.Treiber@ aecom.com w -COM Imagined. Delivered. Figure 1 Site Location Map Figure 2 Site Plan Figure 3 Groundwater Treatment System Process Flow Diagram Table 1 Alternatives Analysis Attachments: A — Application for Coverage Under General Permit NCG510000 B — Carbon Breakthrough Calculation C — Analytical Lab Report General Discharge Permit NCG510000 Figures AECOM 1 or EL OESSFR 13205 (1 O u LX { r x 15505�1 j\• / MarshvitCe c City Cem DR 'OUsr, GRO�, r . 05 `j NyE.CHU� D �� COLLEGEST y p,� y� /• 55 j. y h 550 2 TRAYW/CK RD rn 3 ' W UNION ST r W UNION ST 35[L F tirA!/y Sr 74 _ MAR SHVILLE BLVD T ►AARSHVILL+ SWID �! Marshville T4 j Mai hville SITE LOCATION sso rIRD RD 11•*��S \ M ^ r�5� \ �� o V i HAS NASTY RD� LOP: SO OLD NWV 7A ,450� SCALE IN FEET: A 2,000 0 2,000 f`' NOTE: ALL MAP FEATURES ARE APPROXIMATE / IN SCALE AND LOCATION. Speedway LLC. p y SITE LOCATION MAP FIGURE 1 s Speedway Store #7997 6325 West Marshville Boulevard Source: Topo USGS 7.5 Minute Topographic Map Quadrangle: Buffalo SE, NY /��0� Marshville, NC Copyright: 2019 National Geographic Society DATE: MAY 2023 DRAWN BY: I. DUMITRU REVIEWED By. N. PINSKER PROJECT NO.: 60708764 0 0-- v - SAN -~ —SAN---SAN17 - -�ANSAN- Bost Street S; � Concrete / Flume Frac Tanks, Sediment Filters &-,a Carbon Vessels Storage Area M W-17 - - - MW-8 - / Discharge Point MW-7 -- Gr Tr ---- Speedway Stre #797 i 4 X STREAM #2 $ MW-13� Kerosene i II �� Pump MWA D / MW-6 'Tank Field =___` #4 MW-4 --- --- / MW-19 _ _ #6_ _ - > . Canopy & � MW-3 f Vent Pipes - Dispenser Islands i i#21 l# i l_I - MW-14 MW-12,` �MW_2 MW-5R ---_-_ — r � � 1 *0 STREAM #1 MW-9 r- y Concrete LEGEND Approximate Site Property Boundary 1 — — Approximate Property Boundary ® Approximate Building Footprint 037® Product Dispenser Underground Storage Tank #1 2,000-Gal. PLUS Gasoline #2 3,000-Gal. PLUS Gasoline #3 15,000-Gal. RUL Gasoline #4 15,000-Gal. PUL Gasoline #5 10,000-Gal. Kerosene #6 10,000-Gal. Diesel Overhead Electric Utility Pole / Power Pole m Light Post / Traffic Light JG F Buried Electric Line co 1 --G- Natural Gas Line h --w-- Water Line m � Fire Hydrant E Water Meter ca [� Water Valve V --SAN-- Sanitary Sewer Os Sanitary Sewer Manhole cT Grease Trap --5.-- Storm Sewer / Catch Basin / Stormwater Inlet Monitoring Well X Surface Water Sample Location MWA 1 R Pedestal 1 r IMWAS , Highway 74 (West Marshville Boulevard) -0- MW-16 SCALE IN FEET: Speedway LLC. Speedway Store #7997 I 40 0 40 6325 West Marshville Boulevard NOTE: ALL MAP FEATURES AREAPPROXIMATE Marshville, NC IN SCALE AND LOCATION. DATE: MAY 2023 1 DRgwN ar I. DUMITRU SITE PLAN REVIEWED BY N. PINSKER I PROJECTNO.: 60708764 FIGURE 2 A.-EIMM SETTLING TANK INFLUENT O�•'F638io��C�ii': = SEAL 0GINE \ GRAVITY FEED 2 SUBMERSIBLE PUMPS (90 GPM each) UNDER WEIR -GENERATOR Speedway LLC. Speedway Store #7997 6325 West Marshville Boulevard Marshville, NC DATEMAY 2023 DRAWN BT: I. DUMITRU 90 GPM 2000 HPV MEDIA VESSEL 2,000 LBS ACTIVATED CARBON 90 GPM -) SEDIMENT BAG TO CUSTOMERS DISCHARGE POINT (90-180 GPM) GROUND WATER TREATMENT FIGURE 3 SYSTEM PROCESS FLOW DIAGRAM A--MM REVIEWED BV: N. PINSKER I PROJEC-NO 60708764 General Discharge Permit NCG510000 1 1 Tables AECOM Table 1 Alternatives Analysis Speedway No. 7997 Marshville, North Carolina Dewatering Options Description Feasible? Estimated Cost Dewatering to stormwater Groundwater will be pumped to settling tanks, filtered through carbon, sediment filtration bags, and then Yes $70,000 drain discharge to Buck Branch (class C surface water). Wet set Contractor does not drain tank pit. Use divers to Yes $250,000 assist with tank installation. Infiltration gallery Install injections wells onsite to discharge treated No $200,000 water to. Max flow is 5 m. Using trucks to transport groundwater 24/7. Cost of Trucking trucking is $110/hour and disposal fee is No $1 Million $0.50/gallon. Trucks will not be able to keep up with recharcie rates. Page 1 of 1 General Discharge Permit NCG510000 LI Attachment A —Application for Coverage Under General Permit NCG510000 I AECOM F PJ Division of Water Resources National Pollutant Discharge Elimination System (NPDES) NCDENR Application for Coverage Under General Permit NCG510000 Authorization to Construct groundwater remediation projects designed to treat petroleum -contaminated groundwater. NOTICE OF INTENT [Required by 15A NCAC 02H .0127(d)l; [term definition see 15A NCAC 02H .0103(19)] FOR AGENCY USE ONLY Date Received Year Month Day (23 1 09 A9 Certificate of Coverage N I C I G 1 5 I IQ 6 S Check # Amount Assigned To: (Please print or type) 1) Mailing address of owner/operator (address to which all permit correspondence will be mailed): Company Name AECOM RECEIVED Company Contact Street Address City Telephone # Cell/Mobile # Nathan Pinsker 5438 Wade Park Boulevard, Suite 200 Raleigh State NC ZIP 919-461-1559 Fax SEP 2 9 2023 27607 - NCDEQ/DWR/NPDES 804-339-8763 Email nathan.pinsker@aecom.com 2) Location of facility producing discharge: Facility Name Speedway Store No. 7997 Facility Contact Nathan Pinsker Street Address 6325 West Marshville Boulevard City Marshville State NC ZIP 28103 - 1176 County Union Telephone 919-461-1559 Fax 3) Physical location information: Please provide a narrative description of how to get to the facility (use street names, state road numbers, and distance and direction from a roadway intersection). The Saeedwav Store No. 7997 (Site) is located at 6325 West Marshville Blvd. Marshville. NC and can be accessed from Andrew Jackson Highwav and Chambers Street. The Site is aanroximately 130 feet north of US-74 W (Andrew Jackson Highway). (A copy of a county map or USGS quad sheet with facility clearly located on the map is required to be submitted with this application.) Page 1 of 5 Revised 911113 NCG510000 New Application 4) This NPDES permit application applies to which of the following: ® New [term definition see 15A NCAC 02H .0103(16)1 or Proposed Does the facility have an approved CAP? ❑ Yes —Date approved: Click here to enter a date. ® No — Please contact the Regional Office Groundwater Section to determine the status of CAP approval and/or authorization to proceed if immediate remediation is recommended. Regional Office contact person: Site Ranking (A - E): I-150-D GW incident #: 27657 ❑ Modification Please describe the modification: ❑ Renewal Please specify existing permit number and original issue date: Click here to enter a date. 5) Does this facility have any other NPDES permits [tenor definition see 15A NCAC 02H .010305)1? ❑ Yes - List the permit numbers for all current NPDES permits for this facility: ® No 6) Description of discharge: [Required by 15A NCAC 02H .0105(c)(1)] a) Is the discharge directly to the receiving water? ❑ Yes ® No - If no, submit a site map with the pathway to the potential receiving waters clearly marked. b) Number of discharge points (ditches, pipes, etc. that convey wastewater from the property): 1 c) Volume of discharge per each discharge point (in GPD): 0-240,000 7) Discharge frequency: [Required by 15A NCAC 02H .0105(c)(1)l a) The discharge is: ® Continuous ❑ Intermittent - Describe when the discharge will occur: Intermittently for up to two weeks b) What is the source(s) of contamination (i.e. gasoline, diesel, solvents, etc.)?: Gasoline and diesel General permits may be obtained for gasoline and/or heavy fuel contamination. An individual permit application must be submitted for sites contaminated with other constituents such as solvents and pesticides. c) Is free product present? ❑ Yes - Product storage tank and an oil/water separator are required. Free product is defined as any measurable accumulation of 1/8" or more in a well or floating on surface water. ® No Page 2 of 5 Revised 911113 NCG510000 New Application 8) Treatment system components: [Required by 15A NCAC 02H .0105(c)(3)] Please note: Final design specifications for the actual system that will be installed must be included in this section. Do not submit this application if only bid specifications are known. Check all of the following that apply: ❑ Oil/Water Separator ❑ Air Stripper ® Carbon Adsorption ® Filters ❑ Other: a) If an Oil/Water separator is present, please provide the following information: i) Rated flow capacity of the unit (in GPM): NA ii) Volume of unit (gal): NA iii) Detention time (min): NA iv) Free product disposal method: NA b) If an air stripper is present, please provide the following information: i) Rated flow capacity of the unit (in GPM): NA ii) Air provided for stripping (in CFM): NA iii) Air to Water ratio: NA iv) Number of trays (if applicable): NA (Removal efficiencies for all chemicals of concern should be included in this submittal. Efficiencies should be expressed as a percentage, i.e. 98% or 0.98) c) If carbon adsorption is present, please provide the following information: i) Rated flow capacity of the unit(s) (in GPM): 90 ii) Number of carbon units and arrangement if number exceeds one (i.e., in parallel or in series): 2 parallel iii) Pounds of carbon in each unit: 2,000 iv) Specify carbon breakthrough time: 16 days per vessel (The method used to calculate breakthrough time must included in the submittal.) d) If filters are used, please provide the following information: 91 i) Rated flow capacity of each unit(s) (in GPM): >300 ii) Arrangement of particulate filters within the system: ® Parallel ❑ Series e) Solids disposal method: Landfill f) If other components to be included, please specify: 9) Receiving waters: [Required by 15A NCAC 02H .0105(c)(1)] a) What is the name of the body or bodies of water (creek, stream, river, lake, etc.) that the facility wastewater discharges into? If the wastewater discharge is to a separate storm sewer system (4S), name the operator of the 4S (e.g. City of Raleigh). Buck Branch Tributary b) Stream Classification (i.e. WS-IV, C, SA, etc): C 10) Alternatives to direct discharge: [Evaluation required by G.S. § 143-215.1(b)(5)(a) and 15A NCAC 02H .0105(c)(2)] Address the feasibility of implementing each of the following non -discharge alternatives: a) Connection to a Municipal or Regional Sewer Collection System b) Subsurface disposal (including nitrification field, infiltration gallery, injection wells, etc.) c) Spray irrigation Page 3 of 5 Revised 911113 NCG510000 New Application The alternatives to discharge analysis should include boring logs and/or other information indicating that a subsurface system is neither feasible nor practical as well as written confirmation indicating that connection to a POTW is not an option. It should also include a present value of costs analysis as outlined in the Division's "Engineering Alternatives _ Analysis (EAA) Guidance Document". Additional Application Requirements: For new or proposed discharges, the following information must be included in triplicate with this application or it will be returned as incomplete; per 15A NCAC 02H .0105(c). a) 7.5 minute series USGS topographic map (or a photocopied portion thereof) with discharge location clearly indicated. b) A site map clearly tracing the pathway of the discharged water from the site to its discharge point, if the discharge is not directly to a stream. c) If the discharge will cross or empty into any easements, right-of-ways, or other public/private property, i.e. DOT, utilities, ditches, etc., before entering the permitted discharge stream, proof that approval was received from the appropriate landowners and/or agencies must be provided prior to issuance of the permit. d) If this application is being submitted by a consulting engineer (or engineering firm), include documentation from the applicant showing that the engineer (or firm) submitting the application has been designated an authorized representative of the applicant; per 15A NCAC 02H .0138(b)(1). e) Final plans for the treatment system (if application is for a new or modified permit). The plans must be signed and sealed by a North Carolina registered Professional Engineer and stamped -"Final Design -Not released for construction;" per 15A NCAC 02H .0139. f) Final specifications for all major treatment components (if application is for a new or modified permit). The specifications must be signed and sealed by a North Carolina registered Professional Engineer and shall include a narrative description of the treatment system to be constructed, per 15A NCAC 02H .0139. g) Site map identifying the location of the monitoring wells, the recovery wells, and the treatment system unit. h) Analytical monitoring data which sufficiently characterizes the type and concentration of contaminants on site. This includes a listing of any chemicals found with the maximum observed concentrations reported. The data provided must be no older than one year prior to the date of this application. At a minimum, the following parameters must be reported: Benzene, Toluene, Ethylbenzene, Xylene, Lead, Phenol, MTBE, and 1,2-Dichlorethane. j Page 4 of 5 Revised 911113 NCG510000 New Application CERTIFICATION I certify that I am familiar with the information contained in this application and that to the best of my knowledge and belief such information is true, complete, and accurate. Printed Name of Person Signing: Nathan Pinsker as limited field agent for Speedway, LLC Title: Project Manager (Please review 15A NCAC 02H .0106 a for authorized signing officials) Ins a r, � k k bry'R�nake , Na hart W-USBVLI, am Nathan aN-Na�A.0.5-OC'00' a2aClick here to enter a date. Data: a3.1keraa�a.0a @ (Signature of Applicant) (Date Signed) 10/2/2023 North Carolina General Statute $ 143-215.6B provides that: Any person who knowingly makes any false statement representation, or certification in any application, record, report, plan, or other document filed or required to be maintained under this Article or a rule implementing this Article; or who knowingly makes a false statement of a material fact in a rulemaking proceeding or contested case under this Article; or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device or method required to be operated or maintained under this Article or rules of the Commission implementing this Article, shall be guilty of a Class 2 misdemeanor which may include a fine not to exceed ten thousand dollars ($10,000). 18 U.S.C. Section 1001 provides a punishment by a fine or imprisonment not more than 5 years, or both, for a similar offense. • This application must be accompanied by a check or money order for $100.00 [per G.S. 5 143-215.3(a)(lb)1 made payable to: NCDENR Mail this application and one copy of the entire package (with check) to: NC DENR / DWR / Water Quality Permitting Section 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attn: Charles Weaver Final Checklist This application will be returned as incomplete, as allowed by 15A NCAC 02H .0107(b), unless all of the following items have been included: ❑ Complete application with all supporting documents (plus one copy of entire package) ❑ Check or money order for $100.00, payable to NCDENR ❑ 3 copies of county map or USGS quad sheet with location of facility clearly marked on map ❑ 3 sets of plans and specifications signed and sealed by a North Carolina P.E. (if new or modified permit) ❑ Thorough responses to items I -I I on this application ❑ Alternatives analysis including present value of costs for all alternatives Note: The submission of this document does not guarantee the issuance of an NPDES aermit Page 5 of 5 Revised 911113 General Discharge Permit NCG510000 AC0MImagined. Delivered. September 27, 2023 Mr. Andrew Pitner North Carolina Department of Environmental Quality Water Quality Permitting Section 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Subject: General Discharge Permit NCG510000 Speedway Store No. 7997 6325 West Marshville Boulevard, Marshville, North Carolina Dear Mr. Pitner, AECOM 5438 Wade Park Boulevard, Suite 200 Raleigh, NC 27607 USA T: 919.461.1100 F:919.464.1415 aecom.com AECOM Project No. 60708764 RECEIVED SEP 2 9 2023 NCDEQ/DWR/NPDES AECOM Technical Services of North Carolina, Inc. (AECOM), on behalf of Speedway, LLC (Speedway), is submitting this Application for Coverage Under General Permit NCG510000 for the Speedway Store No. 7997 (Site), located at 6325 West Marshville Boulevard, Marshville, North Carolina. The Site is operated by Speedway as a petroleum retail facility and convenience store. Speedway is proposing underground storage tank (UST) system replacement activities at the Site. Historically, groundwater depth has ranged from approximately 7 to 10 feet below ground surface (bgs) near the UST basin. Therefore, dewatedng from the tank basin is anticipated. AECOM expects to discharge treated groundwater for approximately two weeks at an estimated flow of 20 to 170 gallons per minute (gpm) depending on the recharge rate of groundwater in the excavation. 170 gpm assumes worst case scenario and use of two pumps but will most likely be one pump working intermittently. AECOM proposes to pump groundwater to a 21,000-gallon frac tank and then treat it via 2,000-pound carbon vessels prior to discharge. Breakthrough calculations assume worst case scenario for flow and level of impacts. The treated groundwater would be discharged via aboveground piping to the Buck Branch (class C surface water) located approximately 235 feet west of the Site. AECOM sampled monitoring well MW-19, located downgradient of the tank field, on June 30, 2023 and analyzed for volatile organic compounds (VOCs) via standard Method (SM) 6200B, lead and total hardness via EPA Method 6020B, total suspended solids (TSS) via SM2540D-2015, pH via SM4500-H+B- 2011, and total recoverable phenolics via EPA 420.4 Rev 1.0 1993. Carbon breakthrough was calculated using the current laboratory analytical data. If there are any questions or concerns regarding this report, please contact Nathan Pinsker at (919) 461-1559. Yours sincerely, Nathan Pinsker Project Manager Nathan.Pinsker@aecom.com I Marie Treiber Regional Senior Project Manager Marie.Treiber@ aecom,com NCG510000 New Application 1 CERTIFICATION I certify that I am familiar with the information contained in this application and that to the best of my knowledge and belief such information is true, complete, and accurate. Printed Name of Person Signing: Title: (Please review 15A NCAC 02H .0106(e) for authorized signing officials) (Signature of Applicant) North Carolina General Statute § 143-215.613 provides that: Click here to enter a date. (Date Signed) Any person who knowingly makes any false statement representation, or certification in any application, record, report, plan, or other document filed or required to be maintained under this Article or a rule implementing this Article; or who knowingly makes a false statement of a material fact in a rulemaking proceeding or contested case under this Article; or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device or method required to be operated or maintained under this Article or rules of the Commission implementing this Article, shall be guilty of a Class 2 misdemeanor which may include a fine not to exceed ten thousand dollars ($10,000). 18 U.S.C. Section 1001 provides a punishment by a fine or imprisonment not more than 5 years, or both, for a similar offense. I ..... This application must be accompanied by a check or money order for $100.00 [per G.S. § 143-215.3(a)(1b)1 made payable to: NCDENR Mail this application and one copy of the entire package (with check) to: NC DENR / DWR / Water Quality Permitting Section 1617 Mail Service Center Raleigh, North Carolina 27699-1617 Attn: Charles Weaver Final Checklist This application will be returned as incomplete, as allowed by 15A NCAC 02H .0107(b), unless all of the following items have been included: ❑ Complete application with all supporting documents (plus one copy of entire package) ❑ Check or money order for $100.00, payable to NCDENR ❑ 3 copies of county map or USGS quad sheet with location of facility clearly marked on map ❑ 3 sets of plans and specifications signed and sealed by a North Carolina P.E. (if new or modified permit) ❑ Thorough responses to items 1-11 on this application ❑ Alternatives analysis including present value of costs for all alternatives Note: The submission of this document does not guarantee the issuance of an NPDES permit. Page 5 of 5 Revised 911113 General Discharge Permit NCG510000 Attachment B — Carbon Breakthrough Calculations AECOM Iace DC# Title: ENV-FRM-HUN1-0083 v02_Sample Condition Upon Receipt Effective Date: 11/14/2022 `Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, llHg "Bottom half of box is to list number of bottles "'Check all unpreserved Nitrates for chlorine Project WO#:92675415 PM: BV Due Date: 07/12/23 CLIENT: 82-7-Eleven w u a ar : V 4 a A U n � m y z a Z ? v a a ° iu _ r ` z D t Z a o u z L d _ a N z m 2 d w C m C d C 7 d n C J a O = MO Z S u z N 2 O z V A L d d C GJ n V S d ii 7 MW a 2 e O ry I MW u = 2 N z ? V = O N N Z d C Y O M = n l� Y A 6 a. A G. GI n z d q W a yEi a J o o �E _q n " a ,n a o ry o vEi N a 'o E a C M aE E a C E a d E < J o -0 a J E O > o a J E OQ o > o O > o Y a E O d a N ' M ° ✓ J ,^ N ° n o N 0 a o 'A C E a V vt o N E a of 7C L _ 7 0. m a cc 7 a m a cc ~ N o cc Z 0. © ~ N 6 Cis cc u do3 t7 a S t7 a O l9 a Vf e) a 0 U a O 0 o S 0 o H Q > 7 V > > t7 o 7 a sc Y > ~ f a 0 N H a. 0 P'1 a m O l7 a :7 l7 �^ > O) o \N 3 � 4 5 6 � r - 9 I 10 \ 11 \ \ \ 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added lot # v d Note whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DENR Certification Office (i C. fD Dut of hold, incorrect preservative, out of temp, incorrect containers. rn 0 " Clualtrax ID. 69614 Page 2 of 2 DC#_Title: ENV-FRM-HUN1-0083 v02_5ample Condition Upon Receipt Pffartiva Data: 11/14/2022 Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood Huntersville Z Raleigh[:] Mechanicsville❑ Atlanta❑ Kernersville❑ Sample Condition Upon Receipt"'e�".` Project It: WO# ' 92675415 Courier: []Fed Ex ❑UPS ❑USPS [ClientTill III II I l I II III ❑ Commercial [—]Pace Other: 92676 Custody Seal Present? ❑Yes to11" Seals Intact? []Yes eNNo �`_ �ILI, Packing Material: ❑Bubble Wrap 2 Bubble Bags []None ❑ Other Thermome ` IR Gun ID: J,� Type of Ice: wet ❑Blue Correction Factor: Cooler Temp: v ' Add/Subtract ('C)) Cooler Temp Corrected (*, ! L l USDA Regulated Sail ( 0 N/A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC Date/Initials Person Examining Contents: Biological Tissue F zen? [—] Yes []NoN/A ❑Yone Temp should be above freezing to VC ❑Samples out of temp criteria. Samples on ice, cooling process has begun Did samples originate from a foreign source (internationally, [check maps)? UYes UNo including Hawaii and Puerto Rico)? LJYes LJNo Comments/Discrepancy: Chain of Custody Present? Y s [:]No ❑N/A 1. Samples Arrived within Hold Time? Yes ❑No ❑N/A 2 Short Hold Time Analysis (02 hr.)? []Yes N ❑N/A I Rush Turn Around Time Requested? ❑Yes No ❑N/A 4. Sufficient volume? e JYes []NO ❑N/A 5. Correct Containers Used? -Pace Containers Used? E Yes Yp ❑No ❑No ❑N/A ❑N/A 6. Containers Intact? Yes [:)NO ❑N/ 7. Dissolved analysis: Samples Field Filtered? ❑Yes []No N/A R. Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: Yes ,11 ❑No []N/A 9. Headspace in VOA Vials (>5-6mm)? [:)Yes ❑No I�/A 10, Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes [:]Yes ❑No ❑No nNJA �n 11. COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review v Project Manager SRF Review: m rn 0 � Qualtrax ID 69614 Lot ID of split containers: Date/Time. Field Data Required? LJYes UNo Date: Date: Page 1 of 2 (-"69ace' QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Speedway 7997 Marshville Pace Project No.: 92675415 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92675415001 MW-19 EPA1664B 784869 92675415001 MW-19 EPA 3010A 784526 EPA 6020B 784585 92675415001 MW-19 EPA 8260D 784848 92675415001 MW-19 SM 2540D-2015 784842 92675415001 MW-19 SM 4500-H+B-2011 784518 92675415001 MW-19 EPA 420.4 Rev 1.0 1993 784903 EPA 420.4 Rev 1.0 1993 785113 Date: 07/07/2023 10:44 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 14 of 17 �ce QUALIFIERS Project: Speedway 7997 Marshville Pace Project No.: 92675415 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL- Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SWB46 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as 'Total' may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/07/2023 10:44 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 17 ace QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Speedway 7997 Marshville Pace Project No.: 92675415 QC Batch: 784903 Analysis Method: EPA 420.4 Rev 1.0 1993 QC Batch Method: EPA 420.4 Rev 1.0 1993 Analysis Description: 420.4 Phenolics Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92675415001 METHOD BLANK: 4070095 Matrix: Water Associated Lab Samples: 92675415001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Phenolics, Total Recoverable mg/L ND 0.020 0.0076 07/06/2313:51 LABORATORY CONTROL SAMPLE: 4070096 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phenolics, Total Recoverable mg/L 0.05 0.050 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4070097 4070098 MS MSD 35809399001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Phenolics, Total mg/L 0.0076U 0.05 0.05 0.046 0.043 84 79 90-110 6 10 M1 Recoverable MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4070099 4070100 MS MSD 35809399002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conic. Result Result % Rec % Rec Limits RPD RPD Qual Phenolics, Total mg/L 0.0097J 0.05 0.05 0.041 0.043 62 66 90-110 5 10 M1 Recoverable Results presented on this page are in the units indicated by the 'Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/07/2023 10:44 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 17 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Speedway 7997 Marshville Pace Project No.: 92675415 QC Batch: 784518 Analysis Method: SM 4500-H+B-2011 QC Batch Method: SM 4500-H+B-2011 Analysis Description: 4500H+B pH Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92675415001 SAMPLE DUPLICATE: 4068891 92674063001 Dup Max Parameter Units Result Result RPD RPD Qualifiers pH at 25 Degrees C Std. Units 6.2 6.1 0 10 H3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/07/2023 10:44 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 17 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 0 QUALITY CONTROL DATA Project: Speedway 7997 Marshville Pace Project No.: 92675415 QC Batch: 784842 Analysis Method: SM 2540D-2015 QC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92675415001 METHOD BLANK: 4069742 Matrix: Water Associated Lab Samples: 92675415001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 2.5 07/05/23 14:13 LABORATORY CONTROL SAMPLE: 4069743 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 250 100 90-110 SAMPLE DUPLICATE: 4069744 92675555001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Suspended Solids mg/L 258 272 6 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/07/2023 10:44 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 17 QUALITY CONTROL DATA Project: Speedway 7997 Marshville Pace Project No.: 92675415 QC Batch: 784848 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92675415001 METHOD BLANK: 4069779 Matrix: Water Associated Lab Samples: 92675415001 Blank Reporting Parameter Units Result Limit MDL Analyzed 1,2-Dichloroethane ug/L ND 1.0 0.32 07/06/23 00:11 1,2-Dichloroethane-d4 (S) % 109 70-130 07/06/23 00:11 4-Bromofluorobenzene (S) % 89 70-130 07/06/23 00:11 Toluene-d8 (S) % 103 70-130 07/06/23 00:11 LABORATORY CONTROL SAMPLE: 4069780 Parameter Units 1,2-Dichloroethane ug/L 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28076 (704)875-9092 Qualifiers Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 20 23.1 115 70-130 113 70-130 96 70-130 93 70-130 MATRIX SPIKE SAMPLE: 4069781 92675453004 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,2-Dichloroethane ug/L ND 20 23.3 117 69-143 1,2-Dichloroethane-d4 (S) % 111 70-130 4-Bromofluorobenzene (S) % 103 70-130 Toluene-d8 (S) % 101 70-130 SAMPLE DUPLICATE: 4069782 92675453005 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloroethane-d4 (S) % 108 114 4-Bromofluorobenzene (S) % 98 95 Toluene-d8 (S) % 103 104 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/07/2023 10:44 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 17 Project: Speedway 7997 Marshville Pace Project No.: 92675415 QC Batch: 784526 QC Batch Method: EPA 3010A Associated Lab Samples: 92675415001 METHOD BLANK: 4068920 Associated Lab Samples: 92675415001 Parameter Units Hardness, Total(SM 2340B) ug/L Lead ug/L QUALITY CONTROL DATA Analysis Method: EPA 6020B Analysis Description: 6020 MET Laboratory: Pace Analytical Services - Asheville Matrix: Water Blank Reporting Result Limit MDL Analyzed ND 541 541 07/04/23 01:37 ND 1.0 0.077 07/04/23 01:37 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, INC 28078 (704)875-9092 Qualifiers LABORATORY CONTROL SAMPLE: 4068921 Spike LCS LCS % Rec Parameter Units Conc. Result °o Rec Limits Qualifiers Hardness, Total(SM 2340B) u9/L 16500 Lead ug/L 50 49.2 98 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4068922 4068923 MS MSD 92674864021 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Hardness, Total(SM 2340B) ug/L 41100 56400 56200 0 20 Lead ug/L ND 50 50 49.7 49.7 99 99 75-125 0 20 Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/07/2023 10:44 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 17 (-"P'ace OUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Speedway 7997 Marshville Pace Project No.: 92675415 QC Batch: 784869 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 SGT-HEM, TPH Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92675415001 METHOD BLANK: 4069909 Matrix: Water Associated Lab Samples: 92675415001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Petroleum Hydrocarbons mg/L ND 5.0 5.0 07/05/23 12:49 LABORATORY CONTROL SAMPLE: 4069910 Spike 1-CS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L 20 22.6 113 64-132 MATRIX SPIKE SAMPLE: 4069911 92674107003 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Total Petroleum Hydrocarbons mg/L ND 20 20.2 86 64-132 SAMPLE DUPLICATE: 4069912 92674107004 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Petroleum Hydrocarbons mg/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/07/2023 10:44 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 17 (-'09a c e ANALYTICAL RESULTS Project: Speedway 7997 Marshville Pace Project No.: 92675415 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-19 Parameters Lab ID: 92675415001 Collected: Report Results Units Limit 06/30/23 11:00 Received: 06/30/23 13:25 Matrix: Water MDL DF Prepared Analyzed CAS No. Qual 1664 SGT-HEM, TPH Analytical Method: EPA 1664B Pace Analytical Services - Charlotte Total Petroleum Hydrocarbons ND mg/L 4.8 4.8 1 07/05/23 12:49 6020 MET ICPMS Analytical Method: EPA 6020B Preparation Method: EPA 3010A Pace Analytical Services - Asheville Lead 14.2 ug/L 1.0 0.077 1 07/03/23 15:41 07/04/23 04:08 7439-92-1 Hardness, Total(SM 234013) 83300 ug/L 1620 1620 3 07/03/23 15:41 07/05/23 13:45 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2-Dichloroethane ND ug/L 1.0 0.32 1 07/06/23 04:55 107-06-2 Surrogates 4-Bromofluorobenzene (S) 97 % 70-130 1 07/06/23 04:55 460-00-4 1,2-Dichloroethane-d4(S) 108 % 70-130 1 07/06/23 04:55 17060-07-0 Toluene-d8 (S) 102 % 70-130 1 07/06/23 04:55 2037-26-5 2540D Total Suspended Solids Analytical Method: SM 2540D-2015 Pace Analytical Services - Asheville Total Suspended Solids 705 mg/L 25.0 25.0 1 07/05/23 14:13 4500H+ pH, Electrometric Analytical Method: SM 4500-H+6-2011 Pace Analytical Services - Asheville pH at 25 Degrees C 6.6 Std. Units 0.10 0.10 1 07/03/23 1 B:13 H3 420.4 Phenolics, Total Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993 Pace Analytical Services - Asheville Phenolics, Total Recoverable 0.0078J mg/L 0.020 0.0076 1 07/06/23 10:38 07/06/23 14:06 64743-03-9 Date: 07/07/2023 10:44 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 17 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 I-11111MMUZY4161a1I:3 Iffowelli Project: Pace Project No.: Speedway 7997 Marshville 92675415 Lab Sample ID Client Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers 92675415001 MW-19 EPA 6020B Lead 14.2 ug/L 1.0 07/04/23 04:08 EPA 6020B Hardness, Total(SM 23406) 83300 ug/L 1620 07/05/23 13:45 SM 2540D-2015 Total Suspended Solids 705 mg/L 25.0 07/05/23 14:13 SM 4500-H+B-2011 pH at 25 Degrees C 6.6 Std. Units 0.10 07/03/23 18:13 H3 EPA 420.4 Rev 1.0 1993 Phenolics, Total Recoverable 0.0078J mg/L 0.020 07/06/23 14:06 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 17 ace SAMPLE ANALYTE COUNT Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Speedway 7997 Marshville Pace Project No.: 92675415 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92675415001 MW-19 EPA 1664E MMH 1 PASI-C EPA 6020B CRW, KRL 2 PASI-A EPA 8260D SAS 4 PASI-C SM 2540D-2015 JMH1 1 PASI-A SM 4500-H+B-2011 MDW 1 PASI-A EPA 420.4 Rev 1.0 1993 ARJ 1 PASI-A PASI-A = Pace Analytical Services - Asheville PAS I-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 17 Project: Speedway 7997 Marshville Pace Project No.: 92675415 Lab ID Sample ID 92675415001 MW-19 SAMPLE SUMMARY Matrix Date Collected Date Received Water 06/30/2311:00 06/30/2313:25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 17 Project: Speedway 7997 Marshville Pace Project No.: 92675415 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 CERTIFICATIONS South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 17 11*1p ace July 07, 2023 Nathan Pinsker AECOM 5438 Wade Park Blvd Suite 200 Raleigh, NC 27607 RE: Project: Speedway 7997 Marshville Pace Project No.: 92675415 Dear Nathan Pinsker: Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Enclosed are the analytical results for sample(s) received by the laboratory on June 30, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, t��. U Bonnie Vang bonnie.vang@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 17 General Discharge Permit NCG510000 Attachment C - Analytical Lab Report AECOM Project No. 60708764 Page 2 of 2 Client 7-Eleven Date 17-Aug-23 /1 _/�O� Imagine it. Site Speedway Store No.7997 Prepared by Angie Sastogue Ardila /r+��` Delivered. Subject Carbon Breakthrough Calculation Approved by Brett G. Schaefer, PE Calculate vessel change -out frequency based on use of 2,000-lb carbon beds (contractor -supplied units) Diameter (D) 48 in Geotech GAC-L-2000 4ft Height (H) 88 in Geotech GALL-2000 7.33 ft z nD Cross-section area (CSA) 1809.56 in' CSA = 12.57 ft2 Volume 92.15 ft3 V = CSA x H 689.31 gal Carbon density (rl) 30 Ib/113 Typical - https://www.calgoncarbon.com/app/uploads/SGL8x30.pdf Carbon per vessel (Wt) 75% packed height Geotech GAC-L-2000 2074 Ibs Wt = V x 71 x packed height Surface Loading Rate 7.16 gpm/ftz Surface loading rate = influent flow rate / CSA Single Vessel EBCT 8 min EBCT = V / influent flow rate L fe per vessel 16.0 da Life per vessel = Wt / total carbon consumption from Table 1. 7997-Marshville, INC CarbAdsorb Calc.xlsx Project No. 60708764 Page 1 of 2 Client 7-Eleven, Inc Date 17-Aug-23 /tr �O� Imagine it Site Speedway Store No.7997 Prepared by Angie Sastogue Ardila A Delivered. Subject Carbon Breakthrough Calculation Approved by Brett G. Schaefer, PE OBJECTIVE Determine the time it will take for breakthrough to occur in granular activated carbon (GAC) vessels used for treating groundwater with concentrations of dissolved petroleum hydrocarbons. GIVEN/ REFERENCES NPDES General Permit NCG510000 United States Army Corps of Engineers (USACE) Adsorption Design Guide (DG 1110-1-2), March 1, 2001 CALCULATIONS Using the following design basis, calculate the carbon consumption rate (lb/day) and the time for breakthrough to occur. Inout data: Basis: Two GAC vessels in parallel. Calculation applies to each vessel. Contractor -supplied process flow diagram Influent flow rate (per vessel) = 90 gallons per minute (gpm) Contractor -supplied process flow diagram On -Line Factor = 100 % Continuous operation during dewatering activities Surface loading rate = 2-10 gpm/ ft2 Recommended Empty Bed Contact Time (EBCT) _ >7 minutes Recommended: Inlet concentrations = see C-in, Table 1 below. Maximum concentrations from groundwater monitoring data. See Table 1- Component Name to see what well exhibits the highest COC concentration. Outlet concentrations = see C-out, Table 1 below. Effluent limitations (average monthly) from NCAC 2L Standards Adsorptive capacity = see carbon adsorptive capacity in Table 1 below. Calculated Calculate mass of solute adsorbed per mass of adsorbent using Fruendlich Isotherm Equation (from USACE DG 1110-1-2, p. 2-5): where x 1 x = amount of solute adsorbed (µg, mg, or g) - = KC* m = mass of adsorbent (mg or g) m C = conc. of solute remaining in solution after adsorption is complete (at equilibrium) (mg/L) K, n = constants that must be determined for each solute, carbon type, and temperature. Table 1: Carbon Adsorptive Capacity Component Name K 1/n Reference' C-in (mg/L) x/m-in C-out (mg/L) x/m-out Benzene (MW-1) 16.6 0.40 1 1.04 16.86 0.051 5.05 Toluene (MW-1) 100 0.45 2 0.0182 16.48 0.011 13.14 Ethylbenzene (MW-2) 175 0.53 2 0.14 61.73 0.097 50.82 Total Xylenes (MW-2) 174 0.47 2 0.0371 37.00 0.670 144.15 Methyl Tert-Butyl Ether (MW-7) 16.6 0.40 3 0.0808 6.07 1.500 19.52 Total Lead (MW-19) 16.6 0.40 3 0.0142 3.03 0.003 1.63 1,2 Dichloroethane (MW-1) 3.6 0.83 2 0.0011 0.01 0.037 0.23 Naphthalene (MW-1) 132.0 0.42 2 0.719 114.92 0.012 20.60 Total Recoverable Phenolics MW-19 16.6 0.40 3 0.000 0.15 0.300 10.26 'References for K and n constants are as follows: 1 = USACE DG 1110-1-2, Table 2-1 for Filtrasorb® 400. Assumes that the carbon used in this application has similar adsorptive capacity. 2 = USACE DG 1110-1-2, Table 2-2 3 = Isotherm constants not available in USACE DG 1110-1-2, Tables 2-1 and 2-2. Taken as the most abundant BTEX compound present in groundwater (benzene). Table 2: Carbon Consumption Rates Component Name Average Component Carbon Adsorptive Carbon Carbon Carbon Flowrate Concentration (pg/L) Capacity (mg/g GAC) Usage Consumption Consumption (gpm) Inlet Outlet` Inlet Outlet (lb/hr) (lb/mo) (lb/day) TOTAL 21,000 Benzene 90 1040 51 16.86 5.05 4.539 17,648.7 108.94 Toluene 90 18.2 11 16.48 13.14 0.022 85.3 0.53 Ethylbenzene 90 140 97 61.73 50.82 0.034 134.0 0.83 Total Xylenes 90 37.1 670 37.00 144.15 Methyl Tert-Butyl Ether 90 80.8 1500 6.07 19.52 Total Lead 90 14.2 3 3.03 1.63 0.223 868.6 5.36 1,2 Dichloroethane 90 1.1 37 0.01 0.23 Naphthalene 90 719 12 114.92 20.60 0.579 2,252.4 13.90 Total Recoverable Phenolics 90 0.0078 300 0.15 10.26 Total 129.56 7997-Marshville, NC CarbAdsorb Calc.xlsx CHAIN -OF -CUSTODY / Analytical Request Document ce The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. C!ihminlnn a aamnln via thie chain of ruetndv rnnslihdns arknnwlwdnment and arrenlanco of tho Para Terms and Cnnditinns found at httos:I/info.i)acelabs.com/hubfs/oas-standard-terms.odf. Section A Section 8 Section C Required Client Information: Required Project Information: Invoice Information: Page: 1 Of t Company: 7-Eleven AECOM Report To: Nathan Pinsker Attention: Address: 5438 Wade Park Blvd Copy To: Company Name: Suite 200. Raleigh. NC 27607 Address: Regul&IM Ag*ncV Email: nalhen.pinsker@aecom.com Purchase Order WPace Quote: Phone: (804)339-8763 Fax Project Name: 7997 Marshville, NC Pace Project Manager: laylor.connon@pacelabs.com. Stets, I Location Requested Due Date: Project 11: Pace Profile 0: ask PM NC R u•st•d Ana b Fllter•d o a 2 tlAmiX CODE e9f COLLECTED Z O Preservatives } Dr,-N DIV VI WT p <3 m U W.". 1V\V < W Z P —c! P SAMPLE ID o"'SaA SL K �_ -"ART END ° � � c One Character per box. W, tIVP o $ ~ (A-Z. 0-9 1. -) otro or O m 8 cD Sample Ids must be unique T„n,. Ts a o a = N m ME 'c E m o' ~ y D DATE TIME O O S Z S 2 2 O H n O Zf cc 1 Moo - i`l 'A X �K x C ) X -J, 2 3 4 5 6 7 8 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY I AFFILIATKW DATE BY I AFFILIATION DATE TIME SAMPLE COND,� FnMACCEPTED �r.. v�Al SAMPLER NAME AND SIGNATURE O a L PRINT Name o1 SAMPLER: 02 on�ritiY�� w _ $ E SIGNATURE of SAMPLER: DATE Signed: m > ' y A C `- Page 17 of 17 �ce Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 CERTIFICATIONS South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 64 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 July 11, 2023 Brett Schaefer AECOM 6000 Fairview Rd Suite 200 Charlotte, NC 28210 RE: Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Dear Brett Schaefer: Enclosed are the analytical results for sample(s) received by the laboratory on June 30, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, ; nn _try' -,�)GLAA� Bonnie Vang bonnie.vang@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 64 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: SPEEDWAY 7997 MARSHVILLE 92675483 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92675483001 MW-1 SM 6200B GAW 69 PASI-C 92675483002 MW-1 D SM 62006 GAW 69 PASI-C 92675483003 MW-2 SM 6200B GAW 69 PASI-C 92675483004 MW-3 SM 6200B SAS 69 PASI-C 92675483005 MW-4 SM 6200B GAW 69 PASI-C 92675483006 MW-5R SM 6200B GAW 69 PASI-C 92675483007 MW-6 SM 6200B GAW 69 PASI-C 92675483008 MW-7 SM 6200B GAW 69 PASI-C 92675483009 MW-8 SM 6200B GAW 69 PASI-C 92675483010 MW-9 SM 6200B GAW 69 PASI-C 92675483011 MW-14 SM 6200B GAW 69 PASI-C 92675483012 MW-19 SM 6200B GAW 69 PASI-C 92675483013 MW-16 SM 6200B GAW 69 PASI-C 92675483014 MW-18 SM 6200B GAW 69 PASI-C 92675483015 MW-10 SM 6200B GAW 69 PASI-C 92675483016 MW-11R SM 6200B GAW 69 PASI-C 92675483017 TRIP BLANK SM 6200B LMB 69 PASI-C PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 64 SAMPLE SUMMARY Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Lab ID Sample ID Matrix Date Collected 92675483001 MW-1 Water 06/29/2310:45 92675483002 MW-1 D Water 06/29/23 14:00 92675483003 MW-2 Water 06/29/2312:45 92675483004 MW-3 Water 06/29/2315:30 92675483005 MW-4 Water 06/29/2313:00 92675483006 MW-5R Water 06/29/2314:15 92675483007 MW-6 Water 06/29/2312:30 92675483008 MW-7 Water 06/29/2310:30 92675483009 MW-8 Water 06/29/2313:15 92675483010 MW-9 Water 06/29/2311:45 92675483011 MW-14 Water 06/29/2311:15 92675483012 MW-19 Water 06/29/2311:20 92675483013 MW-16 Water 06/29/2312:00 92675483014 MW-18 Water 06/29/2311:35 92675483015 MW-10 Water 06/30/2310:00 92675483016 MW-11 R Water 06/30/23 10:30 92675483017 TRIP BLANK Water 06/30/23 00:00 Date Received 06/30/23 13:25 O6/30/23 13:25 06/30/23 13:25 06/30/23 13:25 06/30/23 13:25 06/30/23 13:25 O6/30/23 13:25 O6/30/23 13:25 O6/30/23 13:25 O6/30/23 13:25 O6/30/23 13:25 O6/30/23 13:25 06/30/23 13:25 06/30/23 13:25 O6/30/23 13:25 O6/30/23 13:25 06/30/23 13:25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 64 SUMMARY OF DETECTION Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Lab Sample ID Method Client Sample ID Parameters 92675483006 MW-5R SM 6200B tert-Amyl Alcohol SM 6200B tert-Butyl Alcohol SM 6200B Chloroform SM 6200B Diisopropyl ether SM 6200B Methyl-tert-butyl ether 92675483007 MW-6 SM 6200B Benzene SM 6200B tert-Butyl Alcohol SM 6200B Chloroform SM 6200B Diisopropyl ether SM 6200B Methyl-tert-butyl ether 92675483008 MW-7 SM 6200B Benzene SM 6200B tert-Butyl Alcohol SM 6200B Chloroform SM 6200B Diisopropyl ether SM 6200B Methyl-tert-butyl ether 92675483009 MW-8 SM 6200B Chloroform SM 6200B Methyl-tert-butyl ether 92675483010 MW-9 SM 6200B Chloroform 92675483011 MW-14 SM 6200B tert-Amyl Alcohol SM 6200B tert-Amylmethyl ether SM 6200B Benzene SM 6200B tert-Butyl Alcohol SM 6200B Chloroform SM 6200B Diisopropyl ether SM 6200B Ethylbenzene SM 6200B Isopropylbenzene (Cumene) SM 6200B Methyl-tert-butyl ether SM 6200B Naphthalene SM 6200B n-Propylbenzene SM 6200B Toluene SM 6200B 1,2,4-Trimethyl benzene SM 6200B m&p-Xylene 92675483012 MW-19 SM 6200B tert-Amyl Alcohol SM 6200B tert-Amylmethyl ether SM 6200B Benzene SM 6200B tert-Butyl Alcohol SM 6200B Chloroform SM 6200B Chloromethane Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Result Units Report Limit Analyzed 202 ug/L 100 07/06/2318:08 36.7J ug/L 50.0 07/06/2318:08 0.30J ug/L 0.50 07/06/2318:08 C9 1.4 ug/L 0.50 07/06/2318:08 4.0 ug/L 0.50 07/06/2318:08 3.7 ug/L 1.2 07/06/23 22:40 3050 ug/L 125 07/06/23 22:40 0.39J ug/L 1.2 07/06/23 22:40 C9 15.1 ug/L 1.2 07/06/23 22:40 20.1 ug/L 1.2 07/06/23 22:40 2.2 ug/L 2.0 07/06/23 22:58 4170 ug/L 200 07/06/23 22:58 1.1J ug/L 2.0 07/06/23 22:58 C9 13.3 ug/L 2.0 07/06/23 22:58 80.8 ug/L 2.0 07/06/23 22:58 0.26J ug/L 0.50 07/06/2318:26 C9 0.57 ug/L 0.50 07/06/2318:26 0.21 J ug/L 0.50 07/06/23 18:45 C9 506 ug/L 100 07/06/2319:03 1.5J ug/L 10.0 07/06/2319:03 9.7 ug/L 0.50 07/06/2319:03 128 ug/L 50.0 07/06/2319:03 0.32J ug/L 0.50 07/06/2319:03 C9 10.2 ug/L 0.50 07/06/2319:03 7.1 ug/L 0.50 07/06/2319:03 1.0 ug/L 0.50 07/06/2319:03 17.2 ug/L 0.50 07/06/2319:03 5.8 ug/L 2.0 07/06/2319:03 2.6 ug/L 0.50 07/06/2319:03 0.31J ug/L 0.50 07/06/2319:03 1.3 ug/L 0.50 07/06/2319:03 1.5 ug/L 1.0 07/06/2319:03 196 ug/L 100 07/06/23 22:04 4.OJ ug/L 10.0 07/06/23 22:04 45.0 ug/L 0.50 07/06/23 22:04 1310 ug/L 50.0 07/06/23 22:04 0.22J ug/L 0.50 07/06/23 22:04 C9 0.52J ug/L 1.0 07/06/23 22:04 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Qualifiers Page 6 of 64 (-"'09ace' SUMMARY OF DETECTION Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: SPEEDWAY 7997 MARSHVILLE 92675483 Lab Sample ID Client Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers 92675483001 MW-1 SM 6200B tert-Amyl Alcohol 715J ug/L 1000 07/06/23 23:52 SM 6200B Benzene 1040 ug/L 5.0 07/06/23 23:52 SM 6200B tert-Butyl Alcohol 1180 ug/L 500 07/06/23 23:52 SM 6200B sec-Butylbenzene 16.2 ug/L 5.0 07/06/23 23:52 SM 6200B Chloroform 2.4J ug/L 5.0 07/06/23 23:52 C9 SM 6200B Diisopropyl ether 28.0 ug/L 5.0 07/06/23 23:52 SM 6200B Ethylbenzene 20.2 ug/L 5.0 07/06/23 23:52 SM 6200B Isopropylbenzene (Cumene) 134 ug/L 5.0 07/06/23 23:52 SM 6200B Methyl-tert-butyl ether 51.8 ug/L 5.0 07/06/23 23:52 SM 6200B Naphthalene 719 ug/L 20.0 07/06/23 23:52 SM 6200B n-Propylbenzene 363 ug/L 5.0 07/06/23 23:52 SM 6200B Toluene 18.2 ug/L 5.0 07/06/23 23:52 SM 6200B m&p-Xylene 33.1 ug/L 10.0 07/06/23 23:52 SM 6200B o-Xylene 4.1J ug/L 5.0 07/06/23 23:52 92675483002 MW-1D SM 6200B tert-Butyl Alcohol 202 ug/L 50.0 07/06/23 22:22 SM 6200B Diisopropyl ether 3.6 ug/L 0.50 07/06/23 22:22 SM 6200B Methyl-tert-butyl ether 79.8 ug/L 0.50 07/06/23 22:22 92675483003 MW-2 SM 6200B tert-Amyl Alcohol 292J ug/L 400 07/06/23 23:16 SM 6200B tert-Amylmethyl ether 14.7J ug/L 40.0 07/06/23 23:16 SM 6200B Benzene 467 ug/L 2.0 07/06/23 23:16 SM 6200B tert-Butyl Alcohol 457 ug/L 200 07/06/23 23:16 SM 6200B sec -Butyl benzene 14.0 ug/L 2.0 07/06/23 23:16 SM 6200B Chloroform 1.3J ug/L 2.0 07/06/23 23:16 C9 SM 6200B Diisopropyl ether 93.7 ug/L 2.0 07/06/23 23:16 SM 6200B Ethylbenzene 140 ug/L 2.0 07/06/23 23:16 SM 6200B Isop ropylbenzene (Cumene) 145 ug/L 2.0 07/06/23 23:16 SM 6200B Methyl-tert-butyl ether 43.0 ug/L 2.0 07/06/23 23:16 SM 6200B Naphthalene 435 ug/L 8.0 07/06/23 23:16 SM 6200B n-Propylbenzene 364 ug/L 2.0 07/06/23 23:16 SM 6200B Toluene 6.5 ug/L 2.0 07/06/23 23:16 SM 6200I3 m&p-Xylene 32.0 ug/L 4.0 07/06/23 23:16 SM 6200B o-Xylene 5.1 ug/L 2.0 07/06/23 23:16 92675483004 MW-3 SM 6200B Chloroform 0.23J ug/L 0.50 07/06/23 15:12 SM 6200B Diisopropyl ether 3.4 ug/L 0.50 07/06/23 15:12 SM 620013 Methyl-tert-butyl ether 18.7 ug/L 0.50 07/06/23 15:12 92675483005 MW-4 SM 620013 Chlorobenzene 2.9 ug/L 0.50 07/06/23 17:50 SM 620013 Chloroform 0.28J ug/L 0.50 07/06/23 17:50 C9 SM 62003 Diisopropyl ether 3.4 ug/L 0.50 07/06/23 17:50 SM 62003 Methyl-tert-butyl ether 16.2 ug/L 0.50 07/06/23 17:50 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 64 (--"Pace- ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Sample: MW-1 Lab ID: 92675483001 Collected: 06/29/23 10:45 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte tert-Amyl Alcohol 715J ug/L 1000 74.4 10 07/06/23 23:52 75-85-4 tert-Amylmethyl ether ND ug/L 100 1.2 10 07/06/23 23:52 994-05-8 Benzene 1040 ug/L 5.0 0.79 10 07/06/23 23:52 71-43-2 Bromobenzene ND ug/L 5.0 1.4 10 07/06/23 23:52 108-86-1 Bromochloromethane ND ug/L 5.0 0.94 10 07/06/23 23:52 74-97-5 Bromodichloromethane ND ug/L 5.0 1.7 10 07/06/23 23:52 75-27-4 Bromoform ND ug/L 5.0 2.0 10 07/06/23 23:52 75-25-2 Bromomethane ND ug/L 50.0 2.2 10 07/06/23 23:52 74-83-9 tert-Butyl Alcohol 1180 ug/L 500 40.9 10 07/06/23 23:52 75-65-0 n-Butylbenzene ND ug/L 5.0 0.66 10 07/06/23 23:52 104-51-8 sec-Butylbenzene 16.2 ug/L 5.0 0.85 10 07/06/23 23:52 135-98-8 tert-Butyl benzene ND ug/L 5.0 0.86 10 07/06/23 23:52 98-06-6 tert-Butyl Formate ND ug/L 500 3.0 10 07/06/23 23:52 762-75-4 Carbon tetrachloride ND ug/L 5.0 1.7 10 07/06/23 23:52 56-23-5 Chlorobenzene ND ug/L 5.0 0.85 10 07/06/23 23:52 108-90-7 Chloroethane ND ug/L 10.0 1.7 10 07/06/23 23:52 75-00-3 Chloroform 2.4J ug/L 5.0 0.69 10 07/06/23 23:52 67-66-3 Chloromethane ND ug/L 10.0 1.8 10 07/06/23 23:52 74-87-3 2-Chlorotoluene ND ug/L 5.0 1.3 10 07/06/23 23:52 95-49-8 4-Chlorotoluene ND ug/L 5.0 0.96 10 07/06/23 23:52 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 10.0 1.8 10 07/06/23 23:52 96-12-8 Dibromochloromethane ND ug/L 5.0 1.5 10 07/06/23 23:52 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 5.0 1.5 10 07/06/23 23:52 106-93-4 Dibromomethane ND ug/L 5.0 1.9 10 07/06/23 23:52 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 0.94 10 07/06/23 23:52 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 0.98 10 07/06/23 23:52 541-73-1 1,4-Dichlorobenzene ND ug/L 5.0 0.90 10 07/06/23 23:52 106-46-7 Dichlorodifluoromethane ND ug/L 5.0 1.2 10 07/06/23 23:52 75-71-8 1,1-Dichloroethane ND ug/L 5.0 0.56 10 07/06/23 23:52 75-34-3 1,2-Dichloroethane ND ug/L 5.0 1.1 10 07/06/23 23:52 107-06-2 1,1-Dichloroethene ND ug/L 5.0 0.79 10 07/06/23 23:52 75-35-4 cis-1,2-Dichloroethene ND ug/L 5.0 1.1 10 07/06/23 23:52 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 1.0 10 07/06/23 23:52 156-60-5 1,2-Dichloropropane ND ug/L 5.0 1.4 10 07/06/23 23:52 78-87-5 1,3-Dichloropropane ND ug/L 5.0 0.85 10 07/06/23 23:52 142-28-9 2,2-Dichloropropane ND ug/L 5.0 1.2 10 07/06/23 23:52 594-20-7 1,1-Dichloropropene ND ug/L 5.0 0.66 10 07/06/23 23:52 563-58-6 cis-1,3-Dichloropropene ND ug/L 5.0 0.90 10 07/06/23 23:52 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 5.0 1.3 10 07/06/23 23:52 10061-02-6 Diisopropyl ether 28.0 ug/L 5.0 0.72 10 07/06/23 23:52 108-20-3 Ethanol ND ug/L 2000 50.5 10 07/06/23 23:52 64-17-5 Ethylbenzene 20.2 ug/L 5.0 0.81 10 07/06/23 23:52 100-41-4 Ethyl-tert-butyl ether ND ug/L 100 1.1 10 07/06/23 23:52 637-92-3 Hexachloro-1,3-butadiene ND ug/L 20.0 3.5 10 07/06/23 23:52 87-68-3 Isopropylbenzene (Cumene) 134 ug/L 5.0 1.1 10 07/06/23 23:52 98-82-8 REPORT OF LABORATORY ANALYSIS C9 L1 This report shall not be reproduced, except in full, Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 64 ace SUMMARY OF DETECTION Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Pace Project No.: SPEEDWAY 7997 MARSHVILLE 92675483 Lab Sample ID Client Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers 92675483012 MW-19 SM 6200B Diisopropyl ether 67.4 ug/L 0.50 07/06/23 22:04 SM 6200B Ethylbenzene 1.0 ug/L 0.50 07/06/23 22:04 SM 6200B Ethyl-tert-butyl ether 1.3J ug/L 10.0 07/06/23 22:04 SM 6200B Isopropylbenzene (Cumene) 2.0 ug/L 0.50 07/06/23 22:04 SM 6200B Methyl-tert-butyl ether 38.9 ug/L 0.50 07/06/23 22:04 SM 6200B Naphthalene 3.6 ug/L 2.0 07/06/23 22:04 SM 6200B n-Propylbenzene 3.5 ug/L 0.50 07/06/23 22:04 SM 6200B Toluene 0.77 ug/L 0.50 07/06/23 22:04 SM 6200B m&p-Xylene 5.5 ug/L 1.0 07/06/23 22:04 SM 6200B o-Xylene 0.68 ug/L 0.50 07/06/23 22:04 92675483013 MW-16 SM 6200B Chloroform 0.34J ug/L 0.50 07/06/23 19:21 C9 SM 6200B Naphthalene 0.42J ug/L 2.0 07/06/23 19:21 92675483014 MW-18 SM 6200B Chloroform 0.31J ug/L 0.50 07/06/23 19:39 C9 92675483015 MW-10 SM 6200B Chloroform 0.29J ug/L 0.50 07/06/23 19:57 C9 SM 6200B Diisopropyl ether 0.13J ug/L 0.50 07/06/23 19:57 92675483016 MW-11R SM 6200B Benzene 1.5 ug/L 0.50 07/06/23 20:15 SM 6200B Chloroform 0.31J ug/L 0.50 07/06/23 20:15 C9 SM 6200B Diisopropyl ether 0.27J ug/L 0.50 07/06/23 20:15 SM 6200B Ethylbenzene 1.6 ug/L 0.50 07/06/23 20:15 SM 6200B Methyl-tert-butyl ether 0.95 ug/L 0.50 07/06/23 20:15 SM 6200B n-Propylbenzene 0.44J ug/L 0.50 07/06/23 20:15 SM 6200B 1,2,4-Trimethylbenzene 1.4 ug/L 0.50 07/06/23 20:15 SM 6200B 1,3,5-Trimethylbenzene 0.39J ug/L 0.50 07/06/23 20:15 SM 6200B m&p-Xylene 2.2 ug/L 1.0 07/06/23 20:15 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 64 (-"Face' ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Sample: MW-1D Lab ID: 92675483002 Collected: 06/29/23 14:00 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte tert-Amyl Alcohol ND ug/L 100 7.4 1 07/06/23 22:22 75-85-4 tert-Amylmethyl ether ND ug/L 10.0 0.12 1 07/06/23 22:22 994-05-8 Benzene ND ug/L 0.50 0.079 1 07/06/23 22:22 71-43-2 Bromobenzene ND ug/L 0.50 0.14 1 07/06/23 22:22 108-86-1 Bromochloromethane ND ug/L 0.50 0.094 1 07/06/23 22:22 74-97-5 Bromodichloromethane ND ug/L 0.50 0.17 1 07/06/23 22:22 75-27-4 Bromoform ND ug/L 0.50 0.20 1 07/06/23 22:22 75-25-2 Bromomethane ND ug/L 5.0 0.22 1 07/06/23 22:22 74-83-9 tert-Butyl Alcohol 202 ug/L 50.0 4.1 1 07/06/23 22:22 75-65-0 n-Butylbenzene ND ug/L 0.50 0.066 1 07/06/23 22:22 104-51-8 sec -Butyl benzene ND ug/L 0.50 0.085 1 07/06/23 22:22 135-98-8 tert- Butyl benzene ND ug/L 0.50 0.086 1 07/06/23 22:22 98-06-6 tert-Butyl Formate ND ug/L 50.0 0.30 1 07/06/23 22:22 762-75-4 Carbon tetrachloride ND ug/L 0.50 0.17 1 07/06/23 22:22 56-23-5 Chlorobenzene ND ug/L 0.50 0.085 1 07/06/23 22:22 108-90-7 Chloroethane ND ug/L 1.0 0.17 1 07/06/23 22:22 75-00-3 Chloroform ND ug/L 0.50 0.069 1 07/06/23 22:22 67-66-3 Chloromethane ND ug/L 1.0 0.18 1 07/06/23 22:22 74-87-3 2-Chlorotoluene ND ug/L 0.50 0.13 1 07/06/23 22:22 95-49-8 4-Chlorotoluene ND ug/L 0.50 0.096 1 07/06/23 22:22 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1.0 0.18 1 07/06/23 22:22 96-12-8 Dibromochloromethane ND ug/L 0.50 0.15 1 07/06/23 22:22 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 0.50 0.15 1 07/06/23 22:22 106-93-4 Dibromomethane ND ug/L 0.50 0.19 1 07/06/23 22:22 74-95-3 1,2-Dichlorobenzene ND ug/L 0.50 0.094 1 07/06/23 22:22 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 0.098 1 07/06/23 22:22 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 0.090 1 07/06/23 22:22 106-46-7 Dichlorodifluoromethane ND ug/L 0.50 0.12 1 07/06/23 22:22 75-71-8 L1 1,1-Dichloroethane ND ug/L 0.50 0.056 1 07/06/23 22:22 75-34-3 1,2-Dichloroethane ND ug/L 0.50 0.11 1 07/06/23 22:22 107-06-2 1,1-Dichloroethene ND ug/L 0.50 0.079 1 07/06/23 22:22 75-35-4 cis-1,2-Dichloroethene ND ug/L 0.50 0.11 1 07/06/23 22:22 156-59-2 trans-1,2-Dichloroethene ND ug/L 0.50 0.10 1 07/06/23 22:22 156-60-5 1,2-Dichloropropane ND ug/L 0.50 0.14 1 07/06/23 22:22 78-87-5 1,3-Dichloropropane ND ug/L 0.50 0.085 1 07/06/23 22:22 142-28-9 2,2-Dichloropropane ND ug/L 0.50 0.12 1 07/06/23 22:22 594-20-7 1,1-Dichloropropene ND ug/L 0.50 0.066 1 07/06/23 22:22 563-58-6 cis-1,3-Dichloropropene ND ug/L 0.50 0.090 1 07/06/23 22:22 10061-01-5 trans-1,3-Dichloropropene ND ug/L 0.50 0.13 1 07/06/23 22:22 10061-02-6 Diisopropyl ether 3.6 ug/L 0.50 0,072 1 07/06/23 22:22 108-20-3 Ethanol ND ug/L 200 5.0 1 07/06/23 22:22 64-17-5 Ethylbenzene ND ug/L 0.50 0.081 1 07/06/23 22:22 100-41-4 Ethyl-tert-butyl ether ND ug/L 10.0 0.11 1 07/06/23 22:22 637-92-3 Hexachloro-1,3-butadiene ND ug/L 2.0 0.35 1 07/06/23 22:22 87-68-3 Isopropylbenzene (Cumene) ND ug/L 0.50 0.11 1 07/06/23 22:22 98-82-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 64 'P ace ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-1 Lab ID: 92675483001 Collected: 06/29/23 10:45 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte Methylene Chloride ND ug/L 20.0 18.9 10 07/06/23 23:52 75-09-2 Methyl-tert-butyl ether 51.8 ug/L 5.0 0.53 10 07/06/23 23:52 1634-04-4 Naphthalene 719 ug/L 20.0 1.0 10 07/06/23 23:52 91-20-3 n-Propylbenzene 363 ug/L 5.0 1.0 10 07/06/23 23:52 103-65-1 Styrene ND ug/L 5.0 1.4 10 07/06/23 23:52 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 0.91 10 07/06/23 23:52 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 5.0 0.74 10 07/06/23 23:52 79-34-5 Tetrachloroethene ND ug/L 5.0 0.86 10 07/06/23 23:52 127-18-4 Toluene 18.2 ug/L 5.0 0.90 10 07/06/23 23:52 108-88-3 1,2,3-Trichlorobenzene ND ug/L 20.0 1.2 10 07/06/23 23:52 87-61-6 1,2,4-Trichlorobenzene ND ug/L 20.0 1.6 10 07/06/23 23:52 120-82-1 1,1,1-Trichloroethane ND ug/L 5.0 1.1 10 07/06/23 23:52 71-55-6 1,1,2-Trichloroethane ND ug/L 5.0 0.96 10 07/06/23 23:52 79-00-5 Trichloroethene ND ug/L 5.0 1.7 10 07/06/23 23:52 79-01-6 Trichlorofluoromethane ND ug/L 10.0 1.4 10 07/06/23 23:52 75-69-4 1,2,3-Trichloropropane ND ug/L 5.0 1.7 10 07/06/23 23:52 96-18-4 1,2,4-Trimethylbenzene ND ug/L 5.0 0.31 10 07/06/23 23:52 95-63-6 1,3,5-Trimethylbenzene ND ug/L 5.0 0.71 10 07/06/23 23:52 108-67-8 Vinyl chloride ND ug/L 10.0 1.5 10 07/06/23 23:52 75-01-4 m&p-Xylene 33.1 ug/L 10.0 0.94 10 07/06/23 23:52 179601-23-1 o-Xylene 4.1J ug/L 5.0 1.4 10 07/06/23 23:52 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 94 % 70-130 10 07/06/23 23:52 17060-07-0 4-Bromofluorobenzene (S) 98 % 70-130 10 07/06/23 23:52 460-00-4 Toluene-d8 (S) 101 % 70-130 10 07/06/23 23:52 2037-26-5 Date: 07/11/2023 01:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 64 ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-2 Lab ID: 92675483003 Collected: 06/29/23 12:45 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200E MSV tert-Amyl Alcohol tert-Amylmethyl ether Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane tert-Butyl Alcohol n-Butylbenzene sec-Butylbenzene tert- Butyl benzene tert-Butyl Formate Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1, 1 -Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether Ethanol Ethylbenzene Ethyl-tert-butyl ether Hexachloro-1, 3-butadiene Isopropylbenzene (Cumene) Date: 07/11/2023 01:23 PM Analytical Method: SM 6200B Pace Analytical Services - Charlotte 292J ug/L 400 29.8 4 07/06/23 23:16 75-85-4 14.7J ug/L 40.0 0.50 4 07/06/23 23:16 994-05-8 467 ug/L 2.0 0.31 4 07/06/23 23:16 71-43-2 ND ug/L 2.0 0.54 4 07/06/23 23:16 108-86-1 ND ug/L 2.0 0.38 4 07/06/23 23:16 74-97-5 ND ug/L 2.0 0.68 4 07/06/23 23:16 75-27-4 ND ug/L 2.0 0.79 4 07/06/23 23:16 75-25-2 ND ug/L 20.0 0.89 4 07/06/23 23:16 74-83-9 457 ug/L 200 16.4 4 07/06/23 23:16 75-65-0 ND ug/L 2.0 0.27 4 07/06/23 23:16 104-51-8 14.0 ug/L 2.0 0.34 4 07/06/23 23:16 135-98-8 ND ug/L 2.0 0.34 4 07/06/23 23:16 98-06-6 ND ug/L 200 1.2 4 07/06/23 23:16 762-75-4 ND ug/L 2.0 0.68 4 07/06/23 23:16 56-23-5 ND ug/L 2.0 0.34 4 07/06/23 23:16 108-90-7 ND ug/L 4.0 0.69 4 07/06/23 23:16 75-00-3 1.3J ug/L 2.0 0.28 4 07/06/23 23:16 67-66-3 ND ug/L 4.0 0.70 4 07/06/23 23:16 74-87-3 ND ug/L 2.0 0.52 4 07/06/23 23:16 95-49-8 ND ug/L 2.0 0.38 4 07/06/23 23:16 106-43-4 ND ug/L 4.0 0.72 4 07/06/23 23:16 96-12-8 ND ug/L 2.0 0.59 4 07/06/23 23:16 124-48-1 ND ug/L 2.0 0.59 4 07/06/23 23:16 106-93-4 ND ug/L 2.0 0.75 4 07/06/23 23:16 74-95-3 ND ug/L 2.0 0.38 4 07/06/23 23:16 95-50-1 ND ug/L 2.0 0.39 4 07/06/23 23:16 541-73-1 ND ug/L 2.0 0.36 4 07/06/23 23:16 106-46-7 ND ug/L 2.0 0.49 4 07/06/23 23:16 75-71-8 ND ug/L 2.0 0.22 4 07/06/23 23:16 75-34-3 ND ug/L 2.0 0.42 4 07/06/23 23:16 107-06-2 ND ug/L 2.0 0.31 4 07/06/23 23:16 75-35-4 ND ug/L 2.0 0.44 4 07/06/23 23:16 156-59-2 ND ug/L 2.0 0.40 4 07/06/23 23:16 156-60-5 ND ug/L 2.0 0.54 4 07/06/23 23:16 78-87-5 ND ug/L 2.0 0.34 4 07/06/23 23:16 142-28-9 ND ug/L 2.0 0.49 4 07/06/23 23:16 594-20-7 ND ug/L 2.0 0.26 4 07/06/23 23:16 563-58-6 ND ug/L 2.0 0.36 4 07/06/23 23:16 10061-01-5 ND ug/L 2.0 0.53 4 07/06/23 23:16 10061-02-6 93.7 ug/L 2.0 0.29 4 07/06/23 23:16 108-20-3 ND ug/L 800 20.2 4 07/06/23 23:16 64-17-5 140 ug/L 2.0 0.32 4 07/06/23 23:16 100-41-4 ND ug/L 40.0 0.45 4 07/06/23 23:16 637-92-3 ND ug/L B.0 1.4 4 07/06/23 23:16 87-68-3 145 ug/L 2.0 0.42 4 07/06/23 23:16 98-82-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services, LLC. C9 L1 Page 12 of 64 ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-1 D Lab ID: 92675483002 Collected: 06/29/23 14:00 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte Methylene Chloride ND ug/L 2.0 1.9 1 07/06/23 22:22 75-09-2 Methyl -tent -butyl ether 79.8 ug/L 0.50 0.053 1 07/06/23 22:22 1634-04-4 Naphthalene ND ug/L 2.0 0.10 1 07/06/23 22:22 91-20-3 n-Propylbenzene ND ug/L 0.50 0.10 1 07/06/23 22:22 103-65-1 Styrene ND ug/L 0.50 0.14 1 07/06/23 22:22 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 0.091 1 07/06/23 22:22 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 0.074 1 07/06/23 22:22 79-34-5 Tetrachloroethene ND ug/L 0.50 0.086 1 07/06/23 22:22 127-18-4 Toluene ND ug/L 0.50 0.090 1 07/06/23 22:22 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 0.12 1 07/06/23 22:22 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 0.16 1 07/06/23 22:22 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 0.11 1 07/06/23 22:22 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 0.096 1 07/06/23 22:22 79-00-5 Trichloroethene ND ug/L 0.50 0.17 1 07/06/23 22:22 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.14 1 07/06/23 22:22 75-69-4 1,2,3-Trichloropropane ND ug/L 0.50 0.17 1 07/06/23 22:22 96-18-4 1,2,4-Trimethylbenzene ND ug/L 0.50 0.031 1 07/06/23 22:22 95-63-6 1,3,5-Trimethylbenzene ND ug/L 0.50 0.071 1 07/06/23 22:22 108-67-8 Vinyl chloride ND ug/L 1.0 0.15 1 07/06/23 22:22 75-01-4 m&p-Xylene ND ug/L 1.0 0.094 1 07/06/23 22:22 179601-23-1 o-Xylene ND ug/L 0.50 0.14 1 07/06/23 22:22 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 94 % 70-130 1 07/06/23 22:22 17060-07-0 4-Bromofluorobenzene (S) 98 % 70-130 1 07/06/23 22:22 460-00-4 Toluene-d8 (S) 100 % 70-130 1 07/06/23 22:22 2037-26-5 Date: 07/11/2023 01:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. without the written consent of Pace Analytical Services, LLC. Page 11 of 64 (-"' Fa ce ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-3 Lab ID: 92675483004 Collected: 06/29/23 15:30 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV tert-Amyl Alcohol tert-Amylmethyl ether Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane tert-Butyl Alcohol n-Butylbenzene sec- Butyl benzene tert-Butylbenzene tert-Butyl Formate Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether Ethanol Ethylbenzene Ethyl-tert-butyl ether Hexachloro-1,3-butadiene Isopropylbenzene (Cumene) Analytical Method: SM 6200B Pace Analytical Services - Charlotte ND ug/L 100 7.4 1 07/06/2315:12 75-85-4 ND ug/L 10.0 0.12 1 07/06/2315:12 994-05-8 ND ug/L 0.50 0.079 1 07/06/2315:12 71-43-2 ND ug/L 0.50 0.14 1 07/06/2315:12 108-86-1 ND ug/L 0.50 0.094 1 07/06/2315:12 74-97-5 ND ug/L 0.50 0.17 1 07/06/2315:12 75-27-4 ND ug/L 0.50 0.20 1 07/06/2315:12 75-25-2 ND ug/L 5.0 0.22 1 07/06/2315:12 74-83-9 ND ug/L 50.0 4.1 1 07/06/2315:12 75-65-0 ND ug/L 0.50 0.066 1 07/06/2315:12 104-51-8 ND ug/L 0.50 0.085 1 07/06/2315:12 135-98-8 ND ug/L 0.50 0.086 1 07/06/2315:12 98-06-6 ND ug/L 50.0 0.30 1 07/06/2315:12 762-75-4 ND ug/L 0.50 0.17 1 07/06/2315:12 56-23-5 ND ug/L 0.50 0.085 1 07/06/2315:12 108-90-7 ND ug/L 1.0 0.17 1 07/06/2315:12 75-00-3 0.23J ug/L 0.50 0.069 1 07/06/2315:12 67-66-3 ND ug/L 1.0 0.18 1 07/06/2315:12 74-87-3 ND ug/L 0.50 0.13 1 07/06/2315:12 95-49-8 ND ug/L 0.50 0.096 1 07/06/2315:12 106-43-4 ND ug/L 1.0 0.18 1 07/06/2315:12 96-12-8 ND ug/L 0.50 0.15 1 07/06/2315:12 124-48-1 ND ug/L 0.50 0.15 1 07/06/2315:12 106-93-4 ND ug/L 0.50 0.19 1 07/06/2315:12 74-95-3 ND ug/L 0.50 0.094 1 07/06/2315:12 95-50-1 ND ug/L 0.50 0.098 1 07/06/2315:12 541-73-1 ND ug/L 0.50 0.090 1 07/06/2315:12 106-46-7 ND ug/L 0.50 0.12 1 07/06/2315:12 75-71-8 ND ug/L 0.50 0.056 1 07/06/2315:12 75-34-3 ND ug/L 0.50 0.11 1 07/06/2315:12 107-06-2 ND ug/L 0.50 0.079 1 07/06/2315:12 75-35-4 ND ug/L 0.50 0.11 1 07/06/2315:12 156-59-2 ND ug/L 0.50 0.10 1 07/06/2315:12 156-60-5 ND ug/L 0.50 0.14 1 07/06/2315:12 78-87-5 ND ug/L 0.50 0.085 1 07/06/2315:12 142-28-9 ND ug/L 0.50 0.12 1 07/06/2315:12 594-20-7 ND ug/L 0.50 0.066 1 07/06/2315:12 563-58-6 ND ug/L 0.50 0.090 1 07/06/2315:12 10061-01-5 ND ug/L 0.50 0.13 1 07/06/2315:12 10061-02-6 3.4 ug/L 0.50 0.072 1 07/06/2315:12 108-20-3 ND ug/L 200 5.0 1 07/06/2315:12 64-17-5 ND ug/L 0.50 0.081 1 07/06/2315:12 100-41-4 ND ug/L 10.0 0.11 1 07/06/2315:12 637-92-3 ND ug/L 2.0 0.35 1 07/06/2315:12 87-68-3 ND ug/L 0.50 0.11 1 07/06/2315:12 98-82-8 REPORT OF LABORATORY ANALYSIS M1,R1 R1 M1 M M1 This report shall not be reproduced, except in full, Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 64 �ce ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-2 Lab ID: 92675483003 Collected: 06/29/23 12:45 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte Methylene Chloride ND ug/L 8.0 7.6 4 07/06/23 23:16 75-09-2 Methyl-tert-butyl ether 43.0 ug/L 2.0 0.21 4 07/06/23 23:16 1634-04-4 Naphthalene 435 ug/L 8.0 0.40 4 07/06/23 23:16 91-20-3 n-Propylbenzene 364 ug/L 2.0 0.42 4 07/06/23 23:16 103-65-1 Styrene ND ug/L 2.0 0.55 4 07/06/23 23:16 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 2.0 0.36 4 07/06/23 23:16 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 2.0 0.30 4 07/06/23 23:16 79-34-5 Tetrachloroethene ND ug/L 2.0 0.34 4 07/06/23 23:16 127-18-4 Toluene 6.5 ug/L 2.0 0.36 4 07/06/23 23:16 108-88-3 1,2,3-Trichlorobenzene ND ug/L 8.0 0.48 4 07/06/23 23:16 87-61-6 1,2,4-Trichlorobenzene ND ug/L 8.0 0.62 4 07/06/23 23:16 120-82-1 1,1,1-Trichloroethane ND ug/L 2.0 0.43 4 07/06/23 23:16 71-55-6 1,1,2-Trichloroethane ND ug/L 2.0 0.38 4 07/06/23 23:16 79-00-5 Trichloroethene ND ug/L 2.0 0.68 4 07/06/23 23:16 79-01-6 Trichlorofluoromethane ND ug/L 4.0 0.58 4 07/06/23 23:16 75-69-4 1,2,3-Trichloropropane ND ug/L 2.0 0.69 4 07/06/23 23:16 96-18-4 1,2,4-Trimethylbenzene ND ug/L 2.0 0.12 4 07/06/23 23:16 95-63-6 1,3,5-Trimethyl benzene ND ug/L 2.0 0.29 4 07/06/23 23:16 108-67-8 Vinyl chloride ND ug/L 4.0 0.60 4 07/06/23 23:16 75-01-4 m&p-Xylene 32.0 ug/L 4.0 0.37 4 07/06/23 23:16 179601-23-1 o-Xylene 5.1 ug/L 2.0 0.58 4 07/06/23 23:16 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 97 % 70-130 4 07/06/23 23:16 17060-07-0 4-Bromofluorobenzene (S) 98 % 70-130 4 07/06/23 23:16 460-00-4 Toluene-d8 (S) 102 % 70-130 4 07/06/23 23:16 2037-26-5 Date: 07/11/2023 01:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 13 of 64 ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-4 Lab ID: 92675483005 Collected: 06/29/23 13:00 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV tert-Amyl Alcohol tert-Amylmethyl ether Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane tert-Butyl Alcohol n-Butylbenzene sec-Butylbenzene tert- Butyl benzene tert-Butyl Formate Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether Ethanol Ethylbenzene Ethyl-tert-butyl ether Hexachloro-1,3-butadiene Isopropylbenzene (Cumene) Analytical Method: SM 6200B Pace Analytical Services - Charlotte ND ug/L 100 7.4 1 07/06/2317:50 75-85-4 ND ug/L 10.0 0.12 1 07/06/2317:50 994-05-8 ND ug/L 0.50 0.079 1 07/06/2317:50 71-43-2 ND ug/L 0.50 0.14 1 07/06/2317:50 108-86-1 ND ug/L 0.50 0.094 1 07/06/2317:50 74-97-5 ND ug/L 0.50 0.17 1 07/06/2317:50 75-27-4 ND ug/L 0.50 0.20 1 07/06/2317:50 75-25-2 ND ug/L 5.0 0.22 1 07/06/2317:50 74-83-9 ND ug/L 50.0 4.1 1 07/06/2317:50 75-65-0 ND ug/L 0.50 0.066 1 07/06/2317:50 104-51-8 ND ug/L 0.50 0.085 1 07/06/2317:50 135-98-8 ND ug/L 0.50 0.086 1 07/06/2317:50 98-06-6 ND ug/L 50.0 0.30 1 07/06/2317:50 762-75-4 ND ug/L 0.50 0.17 1 07/06/2317:50 56-23-5 2.9 ug/L 0.50 0.085 1 07/06/2317:50 108-90-7 ND ug/L 1.0 0.17 1 07/06/2317:50 75-00-3 0.28J ug/L 0.50 0.069 1 07/06/2317:50 67-66-3 ND ug/L 1.0 0.18 1 07/06/2317:50 74-87-3 ND ug/L 0.50 0.13 1 07/06/2317:50 95-49-8 ND ug/L 0.50 0.096 1 07/06/2317:50 106-43-4 ND ug/L 1.0 0.18 1 07/06/2317:50 96-12-8 ND ug/L 0.50 0.15 1 07/06/2317:50 124-48-1 ND ug/L 0.50 0.15 1 07/06/2317:50 106-93-4 ND ug/L 0.50 0.19 1 07/06/2317:50 74-95-3 ND ug/L 0.50 0.094 1 07/06/2317:50 95-50-1 ND ug/L 0.50 0.098 1 07/06/2317:50 541-73-1 ND ug/L 0.50 0.090 1 07/06/2317:50 106-46-7 ND ug/L 0.50 0.12 1 07/06/2317:50 75-71-8 ND ug/L 0.50 0.056 1 07/06/2317:50 75-34-3 ND ug/L 0.50 0.11 1 07/06/2317:50 107-06-2 ND ug/L 0.50 0.079 1 07/06/2317:50 75-35-4 ND ug/L 0.50 0.11 1 07/06/2317:50 156-59-2 ND ug/L 0.50 0.10 1 07/06/2317:50 156-60-5 ND ug/L 0.50 0.14 1 07/06/2317:50 78-87-5 ND ug/L 0.50 0.085 1 07/06/2317:50 142-28-9 ND ug/L 0.50 0.12 1 07/06/2317:50 594-20-7 ND ug/L 0.50 0.066 1 07/06/2317:50 563-58-6 ND ug/L 0.50 0.090 1 07/06/2317:50 10061-01-5 ND ug/L 0.50 0.13 1 07/06/2317:50 10061-02-6 3.4 ug/L 0.50 0.072 1 07/06/2317:50 108-20-3 ND ug/L 200 5.0 1 07/06/2317:50 64-17-5 ND ug/L 0.50 0.081 1 07/06/2317:50 100-41-4 ND ug/L 10.0 0.11 1 07/06/2317:50 637-92-3 ND ug/L 2.0 0.35 1 07/06/2317:50 87-68-3 ND ug/L 0.50 0.11 1 07/06/2317:50 98-82-8 REPORT OF LABORATORY ANALYSIS C9 L1 This report shall not be reproduced, except in full, Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 64 ( ace ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-3 Lab ID: 92675483004 Collected: 06/29/23 15:30 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte Methylene Chloride ND ug/L 2.0 1.9 1 07/06/23 15:12 75-09-2 Methyl-tert-butyl ether 18.7 ug/L 0.50 0.053 1 07/06/23 15:12 1634-04-4 Naphthalene ND ug/L 2.0 0.10 1 07/06/23 15:12 91-20-3 n-Propylbenzene ND ug/L 0.50 0.10 1 07/06/23 15:12 103-65-1 Styrene ND ug/L 0.50 0.14 1 07/06/23 15:12 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 0.091 1 07/06/23 15:12 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 0.074 1 07/06/23 15:12 79-34-5 Tetrachloroethene ND ug/L 0.50 0.086 1 07/06/23 15:12 127-18-4 Toluene ND ug/L 0.50 0.090 1 07/06/23 15:12 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 0.12 1 07/06/23 15:12 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 0.16 1 07/06/23 15:12 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 0.11 1 07/06/23 15:12 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 0.096 1 07/06/23 15:12 79-00-5 Trichloroethene ND ug/L 0.50 0.17 1 07/06/23 15:12 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.14 1 07/06/23 15:12 75-69-4 M1 1,2,3-Trichloropropane ND ug/L 0.50 0.17 1 07/06/23 15:12 96-18-4 1,2,4-Trimethylbenzene ND ug/L 0.50 0.031 1 07/06/23 15:12 95-63-6 1,3,5-Trimethylbenzene ND ug/L 0.50 0.071 1 07/06/23 15:12 108-67-8 Vinyl chloride ND ug/L 1.0 0.15 1 07/06/23 15:12 75-01-4 m&p-Xylene ND ug/L 1.0 0.094 1 07/06/23 15:12 179601-23-1 o-Xylene ND ug/L 0.50 0.14 1 07/06/23 15:12 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 104 %, 70-130 1 07/06/23 15:12 17060-07-0 4-Bromofluorobenzene (S) 97 % 70-130 1 07/06/23 15:12 460-00-4 Toluene -dB (S) 99 % 70-130 1 07/06/23 15:12 2037-26-5 Date: 07/11/2023 01:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 64 CHAIN -OF -CUSTODY ! Analytical Request Document Face The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. -0-1.. 1000ct. d- nrkoo..endompnt nod ootn...,n of th. oe.-e Tnrma nod (`nrdffinrc fn!md at hNnsd/info.nacplahs.comlhubfs/nas-standard-terms_odf. Section A Section B Section C Required Client Information: Required Project Inforrnation: Invoice Information: Pe e : 1 Of 1 Company: 7-Eleven AECOM Report To: Nathan Pinsker Attention: Address: 5438 Wade Park Blvd Copy To: Company Name: Suite 200. Raleigh, NC 27607 Address: Regulatory e Email: nathan.pinsker@aeeom.eom Purchase Order #: Pace Quote: Phone: (804)339-8763 JFax Project Name: 7997 Marshville, NC Pace Project Manager: le or.cannon pacelabs.com, Stab I Location Requested Due Date: Project #: Pace Profile 0: ask PM NC Requested Ana b Filtered o a MATRIX CODE s i $ COLLECTED o Preservatives � c_'N 1Ys!n DIV V.— WT 8 U - U W.-WH> WIV m yy !p SAMPLE ID S.,,Wd st k �_ -,TART END t- E a OL One Character per box. w'as WP w w n i s m n o `o (A-Z' 0-9 1' rnti oT O w '- $t m tII !. u ~ Sample Ids must be unique T— Ts x wJ w O c UO W S O 6 O Vl U O N 5 Q vl a m m o w D DATE TIME O N _ _Z U = N z W = ! a a' 1 L)lJ - Ih � Z v b X !` X C ) �O/ X, i� 2 3 4 5 6 7 8 9 10 11 12 ADDIrIOKAL COMMENTS RELINQUISHED BY 1 AFFILIATION DATE TIME ACCEPTED BY 1 AFFILIATION DATE TIME SAMPLE CONDITIONS tUL 125� Al .le- SAMPLER NAME AND SIGNATURE U a is n PRINT Name of SAMPLER: V p� !7Dnn tn.h�tl w > ' i c SIGNATURE of SAMPLER: ', DATE Signed: N (n - Page 17 of 17 '6 ('9ace- ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-5R Lab ID: 92675483006 Collected: 06/29/23 14:15 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200E MSV tert-Amyl Alcohol tert-Amylmethyl ether Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane tert-Butyl Alcohol n-Butylbenzene sec-Butylbenzene tert-Butylbenzene tert-Butyl Formate Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans- 1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether Ethanol Ethylbenzene Ethyl-tert-butyl ether Hexachloro-1,3-butadiene Isopropylbenzene (Cumene) Analytical Method: SM 6200B Pace Analytical Services - Charlotte 202 ug/L 100 7.4 1 07/06/2318:08 75-85-4 ND ug/L 10.0 0.12 1 07/06/2318:08 994-05-8 ND ug/L 0.50 0.079 1 07/06/2318:08 71-43-2 ND ug/L 0.50 0.14 1 07/06/2318:08 108-86-1 ND ug/L 0.50 0.094 1 07/06/2318:08 74-97-5 ND ug/L 0.50 0.17 1 07/06/2318:08 75-27-4 ND ug/L 0.50 0.20 1 07/06/2318:08 75-25-2 ND ug/L 5.0 0.22 1 07/06/2318:08 74-83-9 36.7J ug/L 50.0 4.1 1 07/06/2318:08 75-65-0 ND ug/L 0.50 0.066 1 07/06/2318:08 104-51-8 ND ug/L 0.50 0.085 1 07/06/2318:08 135-98-8 ND ug/L 0.50 0.086 1 07/06/2318:08 98-06-6 ND ug/L 50.0 0.30 1 07/06/2318:08 762-75-4 ND ug/L 0.50 0.17 1 07/06/2318:08 56-23-5 ND ug/L 0.50 0.085 1 07/06/2318:08 108-90-7 ND ug/L 1.0 0.17 1 07/06/2318:08 75-00-3 0.30J ug/L 0.50 0.069 1 07/06/2318:08 67-66-3 ND ug/L 1.0 0.18 1 07/06/2318:08 74-87-3 ND ug/L 0.50 0.13 1 07/06/2318:08 95-49-8 ND ug/L 0.50 0.096 1 07/06/2318:08 106-43-4 ND ug/L 1.0 0.18 1 07/06/2318:08 96-12-8 ND ug/L 0.50 0.15 1 07/06/2318:08 124-48-1 ND ug/L 0.50 0.15 1 07/06/2318:08 106-93-4 ND ug/L 0.50 0.19 1 07/06/2318:08 74-95-3 ND ug/L 0.50 0.094 1 07/06/2318:08 95-50-1 ND ug/L 0.50 0.098 1 07/06/2318:08 541-73-1 ND ug/L 0.50 0.090 1 07/06/2318:08 106-46-7 ND ug/L 0.50 0.12 1 07/06/2318:08 75-71-8 ND ug/L 0.50 0.056 1 07/06/2318:08 75-34-3 ND ug/L 0.50 0.11 1 07/06/2318:08 107-06-2 ND ug/L 0.50 0.079 1 07/06/2318:08 75-35-4 ND ug/L 0.50 0.11 1 07/06/2318:08 156-59-2 ND ug/L 0.50 0.10 1 07/06/2318:08 156-60-5 ND ug/L 0.50 0.14 1 07/06/2318:08 78-87-5 ND ug/L 0.50 0.085 1 07/06/2318:08 142-28-9 ND ug/L 0.50 0.12 1 07/06/2318:08 594-20-7 ND ug/L 0.50 0.066 1 07/06/2318:08 563-58-6 ND ug/L 0.50 0.090 1 07/06/2318:08 10061-01-5 ND ug/L 0.50 0.13 1 07/06/2318:08 10061-02-6 1.4 ug/L 0.50 0.072 1 07/06/2318:08 108-20-3 ND ug/L 200 5.0 1 07/06/2318:08 64-17-5 ND ug/L 0.50 0.081 1 07/06/2318:08 100-41-4 ND ug/L 10.0 0.11 1 07/06/2318:08 637-92-3 ND ug/L 2.0 0.35 1 07/06/2318:08 87-68-3 ND ug/L 0.50 0.11 1 07/06/2318:08 98-82-8 REPORT OF LABORATORY ANALYSIS C9 L1 This report shall not be reproduced, except in full, Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 64 (-""Face" ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-4 Lab ID: 92675483005 Collected: 06/29/23 13:00 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte Methylene Chloride ND ug/L 2.0 1.9 1 07/06/23 17:50 75-09-2 Methyl-tert-butyl ether 16.2 ug/L 0.50 0.053 1 07/06/23 17:50 1634-04-4 Naphthalene ND ug/L 2.0 0.10 1 07/06/23 17:50 91-20-3 n-Propylbenzene ND ug/L 0.50 0.10 1 07/06/23 17:50 103-65-1 Styrene ND ug/L 0.50 0.14 1 07/06/23 17:50 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 0.091 1 07/06/23 17:50 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 0.074 1 07/06/23 17:50 79-34-5 Tetrachloroethene ND ug/L 0.50 0.086 1 07/06/23 17:50 127-18-4 Toluene ND ug/L 0.50 0.090 1 07/06/23 17:50 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 0.12 1 07/06/23 17:50 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 0.16 1 07/06/23 17:50 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 0.11 1 07/06/23 17:50 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 0.096 1 07/06/23 17:50 79-00-5 Trichloroethene ND ug/L 0.50 0.17 1 07/06/23 17:50 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.14 1 07/06/23 17:50 75-69-4 1,2,3-Trichloropropane ND ug/L 0.50 0.17 1 07/06/23 17:50 96-18-4 1,2,4-Trimethylbenzene ND ug/L 0.50 0.031 1 07/06/23 17:50 95-63-6 1,3,5-Trimethylbenzene ND ug/L 0.50 0.071 1 07/06/23 17:50 108-67-8 Vinyl chloride ND ug/L 1.0 0.15 1 07/06/23 17:50 75-01-4 m&p-Xylene ND ug/L 1.0 0.094 1 07/06/23 17:50 179601-23-1 o-Xylene ND ug/L 0.50 0.14 1 07/06/23 17:50 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 96 % 70-130 1 07/06/23 17:50 17060-07-0 4-Bromofluorobenzene (S) 96 % 70-130 1 07/06/23 17:50 460-00-4 Toluene -dB (S) 102 % 70-130 1 07/06/23 17:50 2037-26-5 Date: 07/11/2023 01:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 17 of 64 II (-"69ace' ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-5R Lab ID: 92675483006 Collected: 06/29/23 14:15 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte Methylene Chloride ND ug/L 2.0 1.9 1 07/06/23 18:08 75-09-2 Methyl-tert-butyl ether 4.0 ug/L 0.50 0.053 1 07/06/23 18:08 1634-04-4 Naphthalene ND ug/L 2.0 0.10 1 07/06/23 18:08 91-20-3 n-Propylbenzene ND ug/L 0.50 0.10 1 07/06/23 18:08 103-65-1 Styrene ND ug/L 0.50 0.14 1 07/06/23 18:08 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 0.091 1 07/06/23 18:08 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 0.074 1 07/06/23 18:08 79-34-5 Tetrachloroethene ND ug/L 0.50 0.086 1 07/06/23 18:08 127-18-4 Toluene ND ug/L 0.50 0.090 1 07/06/23 18:08 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 0.12 1 07/06/23 18:08 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 0.16 1 07/06/23 18:08 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 0.11 1 07/06/23 18:08 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 0.096 1 07/06/23 18:08 79-00-5 Trichloroethene ND ug/L 0.50 0.17 1 07/06/23 18:08 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.14 1 07/06/23 18:08 75-69-4 1,2,3-Trichloropropane ND ug/L 0.50 0.17 1 07/06/23 18:08 96-18-4 1,2,4-Trimethyl benzene ND ug/L 0.50 0.031 1 07/06/23 18:08 95-63-6 1,3,5-Trimethylbenzene ND ug/L 0.50 0.071 1 07/06/23 18:08 108-67-8 Vinyl chloride ND ug/L 1.0 0.15 1 07/06/23 18:08 75-01-4 m&p-Xylene ND ug/L 1.0 0.094 1 07/06/23 18:08 179601-23-1 o-Xylene ND ug/L 0.50 0.14 1 07/06/23 18:08 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 96 % 70-130 1 07/06/23 18:08 17060-07-0 4-Bromofluorobenzene (S) 97 % 70-130 1 07/06/23 18:08 460-00-4 Toluene-d8 (S) 99 % 70-130 1 07/06/23 18:08 2037-26-5 Date: 07/11/2023 01:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 19 of 64 ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-6 Lab ID: 92675483007 Collected: 06/29/23 12:30 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV tert-Amyl Alcohol tert-Amylmethyl ether Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane tert-Butyl Alcohol n-Butylbenzene sec-Butylbenzene tert- Butyl benzene tert-Butyl Formate Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1, 2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether Ethanol Ethylbenzene Ethyl-tert-butyl ether Hexachloro-1,3-butadiene Isopropylbenzene (Cumene) Date: 07/11/2023 01:23 PM Analytical Method: SM 6200B Pace Analytical Services - Charlotte ND ug/L 250 18.6 2.5 07/06/23 22:40 75-85-4 ND ug/L 25.0 0.31 2.5 07/06/23 22:40 994-05-8 3.7 ug/L 1.2 0.20 2.5 07/06/23 22:40 71-43-2 ND ug/L 1.2 0.34 2.5 07/06/23 22:40 108-86-1 ND ug/L 1.2 0.24 2.5 07/06/23 22:40 74-97-5 ND ug/L 1.2 0.42 2.5 07/06/23 22:40 75-27-4 ND ug/L 1.2 0.49 2.5 07/06/23 22:40 75-25-2 ND ug/L 12.5 0.56 2.5 07/06/23 22:40 74-83-9 3050 ug/L 125 10.2 2.5 07/06/23 22:40 75-65-0 ND ug/L 1.2 0.17 2.5 07/06/23 22:40 104-51-8 ND ug/L 1.2 0.21 2.5 07/06/23 22:40 135-98-8 ND ug/L 1.2 0.21 2.5 07/06/23 22:40 98-06-6 ND ug/L 125 0.75 2.5 07/06/23 22:40 762-75-4 ND ug/L 1.2 0.42 2.5 07/06/23 22:40 56-23-5 ND ug/L 1.2 0.21 2.5 07/06/23 22:40 108-90-7 ND ug/L 2.5 0.43 2.5 07/06/23 22:40 75-00-3 0.39J ug/L 1.2 0.17 2.5 07/06/23 22:40 67-66-3 ND ug/L 2.5 0.44 2.5 07/06/23 22:40 74-87-3 ND ug/L 1.2 0.32 2.5 07/06/23 22:40 95-49-8 ND ug/L 1.2 0.24 2.5 07/06/23 22:40 106-43-4 ND ug/L 2.5 0.45 2.5 07/06/23 22:40 96-12-8 ND ug/L 1.2 0.37 2.5 07/06/23 22:40 124-48-1 ND ug/L 1.2 0.37 2.5 07/06/23 22:40 106-93-4 ND ug/L 1.2 0.47 2.5 07/06/23 22:40 74-95-3 ND ug/L 1.2 0.24 2.5 07/06/23 22:40 95-50-1 ND ug/L 1.2 0.24 2.5 07/06/23 22:40 541-73-1 ND ug/L 1.2 0.22 2.5 07/06/23 22:40 106-46-7 ND ug/L 1.2 0.31 2.5 07/06/23 22:40 75-71-8 ND ug/L 1.2 0.14 2.5 07/06/23 22:40 75-34-3 ND ug/L 1.2 0.26 2.5 07/06/23 22:40 107-06-2 ND ug/L 1.2 0.20 2.5 07/06/23 22:40 75-35-4 ND ug/L 1.2 0.28 2.5 07/06/23 22:40 156-59-2 ND ug/L 1.2 0.25 2.5 07/06/23 22:40 156-60-5 ND ug/L 1.2 0.34 2.5 07/06/23 22:40 78-87-5 ND ug/L 1.2 0.21 2.5 07/06/23 22:40 142-28-9 ND ug/L 1.2 0.30 2.5 07/06/23 22:40 594-20-7 ND ug/L 1.2 0.16 2.5 07/06/23 22:40 563-58-6 ND ug/L 1.2 0.22 2.5 07/06/23 22:40 10061-01-5 ND ug/L 1.2 0.33 2.5 07/06/23 22:40 10061-02-6 15.1 ug/L 1.2 0.18 2.5 07/06/23 22:40 108-20-3 ND ug/L 500 12.6 2.5 07/06/23 22:40 64-17-5 ND ug/L 1.2 0.20 2.5 07/06/23 22:40 100-41-4 ND ug/L 25.0 0.28 2.5 07/06/23 22:40 637-92-3 ND ug/L 5.0 0.88 2.5 07/06/23 22:40 87-68-3 ND ug/L 1.2 0.26 2.5 07/06/23 22:40 98-82-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. C9 L1 Page 20 of 64 11 �ce" ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Sample: MW-7 Lab ID: 92675483008 Collected: 06/29/23 10:30 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte tert-Amyl Alcohol ND ug/L 400 29.8 4 07/06/23 22:58 75-85-4 tert-Amylmethyl ether ND ug/L 40.0 0.50 4 07/06/23 22:58 994-05-8 Benzene 2.2 ug/L 2.0 0.31 4 07/06/23 22:58 71-43-2 Bromobenzene ND ug/L 2.0 0.54 4 07/06/23 22:58 1 OB-86-1 Bromochloromethane ND ug/L 2.0 0.38 4 07/06/23 22:58 74-97-5 Bromodichloromethane ND ug/L 2.0 0.68 4 07/06/23 22:58 75-27-4 Bromoform ND ug/L 2.0 0.79 4 07/06/23 22:58 75-25-2 Bromomethane ND ug/L 20.0 0.89 4 07/06/23 22:58 74-83-9 tert-Butyl Alcohol 4170 ug/L 200 16.4 4 07/06/23 22:58 75-65-0 n-Butylbenzene ND ug/L 2.0 0.27 4 07/06/23 22:58 104-51-8 sec-Butylbenzene ND ug/L 2.0 0.34 4 07/06/23 22:58 135-98-8 tert-Butylbenzene ND ug/L 2.0 0.34 4 07/06/23 22:58 98-06-6 tert-Butyl Formate ND ug/L 200 1.2 4 07/06/23 22:58 762-75-4 Carbon tetrachloride ND ug/L 2.0 0.68 4 07/06/23 22:58 56-23-5 Chlorobenzene ND ug/L 2.0 0.34 4 07/06/23 22:58 108-90-7 Chloroethane ND ug/L 4.0 0.69 4 07/06/23 22:58 75-00-3 Chloroform 1.1i ug/L 2.0 0.28 4 07/06/23 22:58 67-66-3 Chloromethane ND ug/L 4.0 0.70 4 07/06/23 22:58 74-87-3 2-Chlorotoluene ND ug/L 2.0 0.52 4 07/06/23 22:58 95-49-8 4-Chlorotoluene ND ug/L 2.0 0.38 4 07/06/23 22:58 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 4.0 0.72 4 07/06/23 22:58 96-12-8 Dibromochloromethane ND ug/L 2.0 0.59 4 07/06/23 22:58 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 2.0 0.59 4 07/06/23 22:58 106-93-4 Dibromomethane ND ug/L 2.0 0.75 4 07/06/23 22:58 74-95-3 1,2-Dichlorobenzene ND ug/L 2.0 0.38 4 07/06/23 22:58 95-50-1 1,3-Dichlorobenzene ND ug/L 2.0 0.39 4 07/06/23 22:58 541-73-1 1,4-Dichlorobenzene ND ug/L 2.0 0.36 4 07/06/23 22:58 106-46-7 Dichlorodifluoromethane ND ug/L 2.0 0.49 4 07/06/23 22:58 75-71-8 1, 1 -Dichloroethane ND ug/L 2.0 0.22 4 07/06/23 22:58 75-34-3 1,2-Dichloroethane ND ug/L 2.0 0.42 4 07/06/23 22:58 107-06-2 1,1-Dichloroethene ND ug/L 2.0 0.31 4 07/06/23 22:58 75-35-4 cis- 1,2-Dichloroethene ND ug/L 2.0 0.44 4 07/06/23 22:58 156-59-2 trans-1,2-Dichloroethene ND ug/L 2.0 0.40 4 07/06/23 22:58 156-60-5 1,2-Dichloropropane ND ug/L 2.0 0.54 4 07/06/23 22:58 78-87-5 1,3-Dichloropropane ND ug/L 2.0 0.34 4 07/06/23 22:58 142-28-9 2,2-Dichloropropane ND ug/L 2.0 0.49 4 07/06/23 22:58 594-20-7 1,1-Dichloropropene ND ug/L 2.0 0.26 4 07/06/23 22:58 563-58-6 cis-1,3-Dichloropropene ND ug/L 2.0 0.36 4 07/06/23 22:58 10061-01-5 trans-1,3-Dichloropropene ND ug/L 2.0 0.53 4 07/06/23 22:58 10061-02-6 Diisopropyl ether 13.3 ug/L 2.0 0.29 4 07/06/23 22:58 108-20-3 Ethanol ND ug/L 800 20.2 4 07/06/23 22:58 64-17-5 Ethylbenzene ND ug/L 2.0 0.32 4 07/06/23 22:58 100-41-4 Ethyl-tert-butyl ether ND ug/L 40.0 0.45 4 07/06/23 22:58 637-92-3 Hexachloro-1,3-butadiene ND ug/L 8.0 1.4 4 07/06/23 22:58 87-68-3 Isopropylbenzene (Cumene) ND ug/L 2.0 0.42 4 07/06/23 22:58 98-82-8 REPORT OF LABORATORY ANALYSIS C9 L1 This report shall not be reproduced, except in full, Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 64 Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Sample: MW-6 Parameters 6200B MSV Methylene Chloride Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrach loroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethyl benzene 1,3, 5-Trimethylbenzene Vinyl chloride m&p-Xylene o-Xylene Surrogates 1,2-Dichloroethane-d4 (S) 4-8romofluorobenzene (S) Toluene-d8 (S) Date: 07/11/2023 01:23 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Lab ID: 92675483007 Collected: 06/29/23 12:30 Received: 06/30/23 13:25 Matrix: Water Report Results Units Limit MDL DF Prepared Analyzed CAS No. Analytical Method: SM 6200B Pace Analytical Services - Charlotte ND ug/L 5.0 4.7 2.5 07/06/23 22:40 75-09-2 20.1 ug/L 1.2 0.13 2.5 07/06/23 22:40 1634-04-4 ND ug/L 5.0 0.25 2.5 07/06/23 22:40 91-20-3 ND ug/L 1.2 0.26 2.5 07/06/23 22:40 103-65-1 ND ug/L 1.2 0.34 2.5 07/06/23 22:40 100-42-5 ND ug/L 1.2 0.23 2.5 07/06/23 22:40 630-20-6 ND ug/L 1.2 0.18 2.5 07/06/23 22:40 79-34-5 ND ug/L 1.2 0.21 2.5 07/06/23 22:40 127-18-4 ND ug/L 1.2 0.22 2.5 07/06/23 22:40 108-88-3 ND ug/L 5.0 0.30 2.5 07/06/23 22:40 87-61-6 ND ug/L 5.0 0.39 2.5 07/06/23 22:40 120-82-1 ND ug/L 1.2 0.27 2.5 07/06/23 22:40 71-55-6 ND ug/L 1.2 0.24 2.5 07/06/23 22:40 79-00-5 ND ug/L 1.2 0.43 2.5 07/06/23 22:40 79-01-6 ND ug/L 2.5 0.36 2.5 07/06/23 22:40 75-69-4 ND ug/L 1.2 0.43 2.5 07/06/23 22:40 96-18-4 ND ug/L 1.2 0.077 2.5 07/06/23 22:40 95-63-6 ND ug/L 1.2 0.18 2.5 07/06/23 22:40 108-67-8 ND ug/L 2.5 0.37 2.5 07/06/23 22:40 75-01-4 ND ug/L 2.5 0.23 2.5 07/06/23 22:40 179601-23-1 ND ug/L 1.2 0.36 2.5 07/06/23 22:40 95-47-6 95 % 70-130 2.5 07/06/23 22:40 17060-07-0 98 % 70-130 2.5 07/06/23 22:40 460-00-4 101 % 70-130 2.5 07/06/23 22:40 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Qual Page 21 of 64 (-'� Fa ce ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-8 Lab ID: 92675483009 Collected: 06/29/23 13:15 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV tert-Amyl Alcohol tert-Amylmethyl ether Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane tert-Butyl Alcohol n-Butylbenzene sec-Butylbenzene tert-Butyl benzene tert-Butyl Formate Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether Ethanol Ethylbenzene Ethyl-tert-butyl ether Hexachloro-1,3-butadiene Isopropylbenzene (Cumene) Analytical Method: SM 6200B Pace Analytical Services - Charlotte ND ug/L 100 7.4 1 07/06/2318:26 75-85-4 ND ug/L 10.0 0.12 1 07/06/2318:26 994-05-8 ND ug/L 0.50 0.079 1 07/06/2318:26 71-43-2 ND ug/L 0.50 0.14 1 07/06/2318:26 108-86-1 ND ug/L 0.50 0.094 1 07/06/23 18:26 74-97-5 ND ug/L 0.50 0.17 1 07/06/2318:26 75-27-4 ND ug/L 0.50 0.20 1 07/06/2318:26 75-25-2 ND ug/L 5.0 0.22 1 07/06/2318:26 74-83-9 ND ug/L 50.0 4.1 1 07/06/2318:26 75-65-0 ND ug/L 0.50 0.066 1 07/06/2318:26 104-51-8 ND ug/L 0.50 0.085 1 07/06/2318:26 135-98-8 ND ug/L 0.50 0.086 1 07/06/2318:26 98-06-6 ND ug/L 50.0 0.30 1 07/06/2318:26 762-75-4 ND ug/L 0.50 0.17 1 07/06/2318:26 56-23-5 ND ug/L 0.50 0.085 1 07/06/2318:26 108-90-7 ND ug/L 1.0 0.17 1 07/06/2318:26 75-00-3 0.26J ug/L 0.50 0.069 1 07/06/2318:26 67-66-3 ND ug/L 1.0 0.18 1 07/06/2318:26 74-87-3 ND ug/L 0.50 0.13 1 07/06/2318:26 95-49-8 ND ug/L 0.50 0.096 1 07/06/2318:26 106-43-4 ND ug/L 1.0 0.18 1 07/06/2318:26 96-12-8 ND ug/L 0.50 0.15 1 07/06/2318:26 124-48-1 ND ug/L 0.50 0.15 1 07/06/2318:26 106-93-4 ND ug/L 0.50 0.19 1 07/06/2318:26 74-95-3 ND ug/L 0.50 0.094 1 07/06/2318:26 95-50-1 ND ug/L 0.50 0.098 1 07/06/2318:26 541-73-1 ND ug/L 0.50 0.090 1 07/06/2318:26 106-46-7 ND ug/L 0.50 0.12 1 07/06/2318:26 75-71-8 ND ug/L 0.50 0.056 1 07/06/2318:26 75-34-3 ND ug/L 0.50 0.11 1 07/06/2318:26 107-06-2 ND ug/L 0.50 0.079 1 07/06/2318:26 75-35-4 ND ug/L 0.50 0.11 1 07/06/2318:26 156-59-2 ND ug/L 0.50 0.10 1 07/06/2318:26 156-60-5 ND ug/L 0.50 0.14 1 07/06/2318:26 78-87-5 ND ug/L 0.50 0.085 1 07/06/2318:26 142-28-9 ND ug/L 0.50 0.12 1 07/06/2318:26 594-20-7 ND ug/L 0.50 0.066 1 07/06/2318:26 563-58-6 ND ug/L 0.50 0.090 1 07/06/2318:26 10061-01-5 ND ug/L 0.50 0.13 1 07/06/2318:26 10061-02-6 ND ug/L 0.50 0.072 1 07/06/2318:26 108-20-3 ND ug/L 200 5.0 1 07/06/2318:26 64-17-5 ND ug/L 0.50 0.081 1 07/06/2318:26 100-41-4 ND ug/L 10.0 0.11 1 07/06/2318:26 637-92-3 ND ug/L 2.0 0.35 1 07/06/2318:26 87-68-3 ND ug/L 0.50 0.11 1 07/06/2318:26 98-82-8 REPORT OF LABORATORY ANALYSIS C9 L1 This report shall not be reproduced, except in full, Date: 07/11 /2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 64 1 7 J A I ace r,1.Y-11tw4flof A 40*111111W Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-7 Lab ID: 92675483008 Collected: 06/29/23 10:30 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200E MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte Methylene Chloride ND ug/L 8.0 7.6 4 07/06/23 22:58 75-09-2 Methyl-tert-butyl ether 80.8 ug/L 2.0 0.21 4 07/06/23 22:58 1634-04-4 Naphthalene ND ug/L 8.0 0.40 4 07/06/23 22:58 91-20-3 n-Propylbenzene ND ug/L 2.0 0.42 4 07/06/23 22:58 103-65-1 Styrene ND ug/L 2.0 0.55 4 07/06/23 22:58 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 2.0 0.36 4 07/06/23 22:58 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 2.0 0.30 4 07/06/23 22:58 79-34-5 Tetrachloroethene ND ug/L 2.0 0.34 4 07/06/23 22:58 127-18-4 Toluene ND ug/L 2.0 0.36 4 07/06/23 22:58 108-88-3 1,2,3-Trichlorobenzene ND ug/L 8.0 0.48 4 07/06/23 22:58 87-61-6 1,2,4-Trichlorobenzene ND ug/L 8.0 0.62 4 07/06/23 22:58 120-82-1 1,1,1-Trichloroethane ND ug/L 2.0 0.43 4 07/06/23 22:58 71-55-6 1,1,2-Trichloroethane ND ug/L 2.0 0.38 4 07/06/23 22:58 79-00-5 Trichloroethene ND ug/L 2.0 0.68 4 07/06/23 22:58 79-01-6 Trichlorofluoromethane ND ug/L 4.0 0.58 4 07/06/23 22:58 75-69-4 1,2,3-Trichloropropane ND ug/L 2.0 0.69 4 07/06/23 22:58 96-18-4 1,2,4-Trimethylbenzene ND ug/L 2.0 0.12 4 07/06/23 22:58 95-63-6 1,3,5-Trimethylbenzene ND ug/L 2.0 0.29 4 07/06/23 22:58 108-67-8 Vinyl chloride ND ug/L 4.0 0.60 4 07/06/23 22:58 75-01-4 m&p-Xylene ND ug/L 4.0 0.37 4 07/06/23 22:58 179601-23-1 o-Xylene ND ug/L 2.0 0.58 4 07/06/23 22:58 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 99 % 70-130 4 07/06/23 22:58 17060-07-0 4-Bromofluorobenzene (S) 100 % 70-130 4 07/06/23 22:58 460-00-4 Toluene -dB (S) 102 % 70-130 4 07/06/23 22:58 2037-26-5 Date: 07/11/2023 01:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, without the written consent of Pace Analytical Services, LLC. Page 23 of 64 (-'�Face ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-9 Lab ID: 92675483010 Collected: 06/29/23 11:45 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte tert-Amyl Alcohol ND ug/L 100 7.4 1 07/06/23 18:45 75-85-4 tert-Amylmethyl ether ND ug/L 10.0 0.12 1 07/06/23 18:45 994-05-8 Benzene ND ug/L 0.50 0.079 1 07/06/23 18:45 71-43-2 Bromobenzene ND ug/L 0.50 0.14 1 07/06/23 18:45 108-86-1 Bromochloromethane ND ug/L 0.50 0.094 1 07/06/23 18:45 74-97-5 Bromodichloromethane ND ug/L 0.50 0.17 1 07/06/23 18:45 75-27-4 Bromoform ND ug/L 0.50 0.20 1 07/06/23 18:45 75-25-2 Bromomethane ND ug/L 5.0 0.22 1 07/06/23 18:45 74-83-9 tert-Butyl Alcohol ND ug/L 50.0 4.1 1 07/06/23 18:45 75-65-0 n-Butylbenzene ND ug/L 0.50 0.066 1 07/06/23 18:45 104-51-8 sec- Butylbenzene ND ug/L 0.50 0.085 1 07/06/23 18:45 135-98-8 tert- Butyl benzene ND ug/L 0.50 0.086 1 07/06/23 18:45 98-06-6 tert-Butyl Formate ND ug/L 50.0 0.30 1 07/06/23 18:45 762-75-4 Carbon tetrachloride ND ug/L 0.50 0.17 1 07/06/23 18:45 56-23-5 Chlorobenzene ND ug/L 0.50 0.085 1 07/06/23 18:45 108-90-7 Chloroethane ND ug/L 1.0 0.17 1 07/06/23 18:45 75-00-3 Chloroform 0.21J ug/L 0.50 0.069 1 07/06/23 18:45 67-66-3 Chloromethane ND ug/L 1.0 0.18 1 07/06/23 18:45 74-87-3 2-Chlorotoluene ND ug/L 0.50 0.13 1 07/06/23 18:45 95-49-8 4-Chlorotoluene ND ug/L 0.50 0.096 1 07/06/23 18:45 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1.0 0.18 1 07/06/23 18:45 96-12-8 Dibromochloromethane ND ug/L 0.50 0.15 1 07/06/23 18:45 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 0.50 0.15 1 07/06/23 18:45 106-93-4 Dibromomethane ND ug/L 0.50 0.19 1 07/06/23 18:45 74-95-3 1,2-Dichlorobenzene ND ug/L 0.50 0.094 1 07/06/23 18:45 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 0.098 1 07/06/23 18:45 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 0.090 1 07/06/23 18:45 106-46-7 Dichlorodifluoromethane ND ug/L 0.50 0.12 1 07/06/23 18:45 75-71-8 1,1-Dichloroethane ND ug/L 0.50 0.056 1 07/06/23 18:45 75-34-3 1,2-Dichloroethane ND ug/L 0.50 0.11 1 07/06/23 18:45 107-06-2 1,1-Dichloroethene ND ug/L 0.50 0.079 1 07/06/23 18:45 75-35-4 cis- 1,2-Dichloroethene ND ug/L 0.50 0.11 1 07/06/23 18:45 156-59-2 trans-1,2-Dichloroethene ND ug/L 0.50 0.10 1 07/06/23 18:45 156-60-5 1,2-Dichloropropane ND ug/L 0.50 0.14 1 07/06/23 18:45 78-87-5 1,3-Dichloropropane ND ug/L 0.50 0.085 1 07/06/23 18:45 142-28-9 2,2-Dichloropropane ND ug/L 0.50 0.12 1 07/06/23 18:45 594-20-7 1,1-Dichloropropene ND ug/L 0.50 0.066 1 07/06/23 18:45 563-58-6 cis-1,3-Dichloropropene ND ug/L 0.50 0.090 1 07/06/23 18:45 10061-01-5 trans- 1,3-Dichloropropene ND ug/L 0.50 0.13 1 07/06/23 18:45 10061-02-6 Diisopropyl ether ND ug/L 0.50 0.072 1 07/06/23 18:45 108-20-3 Ethanol ND ug/L 200 5.0 1 07/06/23 18:45 64-17-5 Ethylbenzene ND ug/L 0.50 0.081 1 07/06/23 18:45 100-41-4 Ethyl-tert-butyl ether ND ug/L 10.0 0.11 1 07/06/23 18:45 637-92-3 Hexachloro-1,3-butadiene ND ug/L 2.0 0.35 1 07/06/23 18:45 87-68-3 Isopropylbenzene (Cumene) ND ug/L 0.50 0.11 1 07/06/23 18:45 98-82-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/11 /2023 01:23 PM without the written consent of Pace Analytical Services, LLC. i C9 L1 Page 26 of 64 ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-8 Lab ID: 92675483009 Collected: 06/29/23 13:15 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200E MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte Methylene Chloride ND ug/L 2.0 1.9 1 07/06/23 18:26 75-09-2 Methyl-tert-butyl ether 0.57 ug/L 0.50 0.053 1 07/06/23 18:26 1634-04-4 Naphthalene ND ug/L 2.0 0.10 1 07/06/23 18:26 91-20-3 n-Propylbenzene ND ug/L 0.50 0.10 1 07/06/23 18:26 103-65-1 Styrene ND ug/L 0.50 0.14 1 07/06/23 18:26 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 0.091 1 07/06/23 18:26 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 0.074 1 07/06/23 18:26 79-34-5 Tetrachloroethene ND ug/L 0.50 0.086 1 07/06/23 18:26 127-18-4 Toluene ND ug/L 0.50 0.090 1 07/06/23 18:26 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 0.12 1 07/06/23 18:26 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 0.16 1 07/06/23 18:26 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 0.11 1 07/06/23 18:26 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 0.096 1 07/06/23 18:26 79-00-5 Trichloroethene ND ug/L 0.50 0.17 1 07/06/23 18:26 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.14 1 07/06/23 18:26 75-69-4 1,2,3-Trichloropropane ND ug/L 0.50 0.17 1 07/06/23 18:26 96-18-4 1,2,4-Trimethyl benzene ND ug/L 0.50 0.031 1 07/06/23 18:26 95-63-6 1,3,5-Trimethylbenzene ND ug/L 0.50 0.071 1 07/06/23 18:26 108-67-8 Vinyl chloride ND ug/L 1.0 0.15 1 07/06/23 18:26 75-01-4 m&p-Xylene ND ug/L 1.0 0.094 1 07/06/23 18:26 179601-23-1 o-Xylene ND ug/L 0.50 0.14 1 07/06/23 18:26 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 97 % 70-130 1 07/06/23 18:26 17060-07-0 4-Bromofluorobenzene (S) 96 °% 70-130 1 07/06/23 18:26 460-00-4 Toluene-d8 (S) 100 % 70-130 1 07/06/23 18:26 2037-26-5 Date: 07/11/2023 01:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 25 of 64 (-"' "Face ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Sample: MW-14 Lab ID: 92675483011 Collected: 06/29/23 11:15 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte tert-Amyl Alcohol 506 ug/L 100 7.4 1 07/06/23 19:03 75-85-4 tert-Amylmethyl ether 1.5J ug/L 10.0 0.12 1 07/06/23 19:03 994-05-8 Benzene 9.7 ug/L 0.50 0.079 1 07/06/23 19:03 71-43-2 Bromobenzene ND ug/L 0.50 0.14 1 07/06/23 19:03 108-86-1 Bromochloromethane ND ug/L 0.50 0.094 1 07/06/23 19:03 74-97-5 Bromodichloromethane ND ug/L 0.50 0.17 1 07/06/23 19:03 75-27-4 Bromoform ND ug/L 0.50 0.20 1 07/06/23 19:03 75-25-2 Bromomethane ND ug/L 5.0 0.22 1 07/06/23 19:03 74-83-9 tert-Butyl Alcohol 128 ug/L 50.0 4.1 1 07/06/23 19:03 75-65-0 n-Butylbenzene ND ug/L 0.50 0.066 1 07/06/23 19:03 104-51-8 sec-Butylbenzene ND ug/L 0.50 0.085 1 07/06/23 19:03 135-98-8 tert- Butyl benzene ND ug/L 0.50 0.086 1 07/06/23 19:03 98-06-6 tert-Butyl Formate ND ug/L 50.0 0.30 1 07/06/23 19:03 762-75-4 Carbon tetrachloride ND ug/L 0.50 0.17 1 07/06/23 19:03 56-23-5 Chlorobenzene ND ug/L 0.50 0.085 1 07/06/23 19:03 108-90-7 Chloroethane ND ug/L 1.0 0.17 1 07/06/23 19:03 75-00-3 Chloroform 0.32J ug/L 0.50 0.069 1 07/06/23 19:03 67-66-3 Chloromethane ND ug/L 1.0 0.18 1 07/06/23 19:03 74-87-3 2-Chlorotoluene ND ug/L 0.50 0.13 1 07/06/23 19:03 95-49-8 4-Chlorotoluene ND ug/L 0.50 0.096 1 07/06/23 19:03 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1.0 0.18 1 07/06/23 19:03 96-12-8 Dibromochloromethane ND ug/L 0.50 0.15 1 07/06/23 19:03 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 0.50 0.15 1 07/06/23 19:03 106-93-4 Dibromomethane ND ug/L 0.50 0.19 1 07/06/23 19:03 74-95-3 1,2-Dichlorobenzene ND ug/L 0.50 0.094 1 07/06/23 19:03 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 0.098 1 07/06/23 19:03 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 0.090 1 07/06/23 19:03 106-46-7 Dichlorodifluoromethane ND ug/L 0.50 0.12 1 07/06/23 19:03 75-71-8 1,1-Dichloroethane ND ug/L 0.50 0.056 1 07/06/23 19:03 75-34-3 1,2-Dichloroethane ND ug/L 0.50 0.11 1 07/06/23 19:03 107-06-2 1,1-Dichloroethene ND ug/L 0.50 0.079 1 07/06/23 19:03 75-35-4 cis-1,2-Dichloroethene ND ug/L 0.50 0.11 1 07/06/23 19:03 156-59-2 trans-1,2-Dichloroethene ND ug/L 0.50 0.10 1 07/06/23 19:03 156-60-5 1,2-Dichloropropane ND ug/L 0.50 0.14 1 07/06/23 19:03 78-87-5 1,3-Dichloropropane ND ug/L 0.50 0.085 1 07/06/23 19:03 142-28-9 2,2-Dichloropropane ND ug/L 0.50 0.12 1 07/06/23 19:03 594-20-7 1,1-Dichloropropene ND ug/L 0.50 0.066 1 07/06/23 19:03 563-58-6 cis-1,3-Dichloropropene ND ug/L 0.50 0.090 1 07/06/23 19:03 10061-01-5 trans-1,3-Dichloropropene ND ug/L 0.50 0.13 1 07/06/23 19:03 10061-02-6 Diisopropyl ether 10.2 ug/L 0.50 0.072 1 07/06/23 19:03 108-20-3 Ethanol ND ug/L 200 5.0 1 07/06/23 19:03 64-17-5 Ethylbenzene 7.1 ug/L 0.50 0.081 1 07/06/23 19:03 100-41-4 Ethyl-tert-butyl ether ND ug/L 10.0 0.11 1 07/06/23 19:03 637-92-3 Hexachloro-1,3-butadiene ND ug/L 2.0 0.35 1 07/06/23 19:03 87-68-3 Isopropylbenzene (Cumene) 1.0 ug/L 0.50 0.11 1 07/06/23 19:03 98-82-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. C9 L1 Page 28 of 64 A ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-9 Lab ID: 92675483010 Collected: 06/29/23 11:45 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte Methylene Chloride ND ug/L 2.0 1.9 1 07/06/23 18:45 75-09-2 Methyl-tert-butyl ether ND ug/L 0.50 0.053 1 07/06/23 18:45 1634-04-4 Naphthalene ND ug/L 2.0 0.10 1 07/06/23 18:45 91-20-3 n-Propylbenzene ND ug/L 0.50 0.10 1 07/06/23 18:45 103-65-1 Styrene ND ug/L 0.50 0.14 1 07/06/23 18:45 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 0.091 1 07/06/23 18:45 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 0.074 1 07/06/23 18:45 79-34-5 Tetrachloroethene ND ug/L 0.50 0.086 1 07/06/23 18:45 127-18-4 Toluene ND ug/L 0.50 0,090 1 07/06/23 18:45 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 0.12 1 07/06/23 18:45 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 0.16 1 07/06/23 18:45 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 0.11 1 07/06/23 18:45 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 0.096 1 07/06/23 18:45 79-00-5 Trichloroethene ND ug/L 0.50 0.17 1 07/06/23 18:45 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.14 1 07/06/23 18:45 75-69-4 1,2,3-Trichloropropane ND ug/L 0.50 0.17 1 07/06/23 18:45 96-18-4 1,2,4-Trimethylbenzene ND ug/L 0.50 0.031 1 07/06/23 18:45 95-63-6 1,3,5-Trimethyl benzene ND ug/L 0.50 0.071 1 07/06/23 18:45 108-67-8 Vinyl chloride ND ug/L 1.0 0.15 1 07/06/23 18:45 75-01-4 m&p-Xylene ND ug/L 1.0 0.094 1 07/06/23 18:45 179601-23-1 o-Xylene ND ug/L 0.50 0.14 1 07/06/23 18:45 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 96 % 70-130 1 07/06/23 18:45 17060-07-0 4-Bromofluorobenzene (S) 97 % 70-130 1 07/06/23 18:45 460-00-4 Toluene-d8 (S) 101 % 70-130 1 07/06/23 18:45 2037-26-5 Date: 07/11/2023 01:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 27 of 64 (--'69a ce ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-19 Lab ID: 92675483012 Collected: 06/29/23 11:20 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV tert-Amyl Alcohol tert-Amylmethyl ether Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane tert-Butyl Alcohol n-Butylbenzene sec- Butylbenzene tert-Butylbenzene tert-Butyl Formate Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1, 1 -Dichloropropene cis-1,3-Dichloropropene trans-1, 3-Dichloropropene Diisopropyl ether Ethanol Ethylbenzene Ethyl-tert-butyl ether Hexachloro-1,3-butadiene Isopropylbenzene (Cumene) Date: 07/11/2023 01:23 PM Analytical Method: SM 6200B Pace Analytical Services - Charlotte 196 ug/L 100 7.4 1 07/06/23 22:04 75-85-4 4.OJ ug/L 10.0 0.12 1 07/06/23 22:04 994-05-8 45.0 ug/L 0.50 0.079 1 07/06/23 22:04 71-43-2 ND ug/L 0.50 0.14 1 07/06/23 22:04 108-86-1 ND ug/L 0.50 0.094 1 07/06/23 22:04 74-97-5 ND ug/L 0.50 0.17 1 07/06/23 22:04 75-27-4 ND ug/L 0.50 0.20 1 07/06/23 22:04 75-25-2 ND ug/L 5.0 0.22 1 07/06/23 22:04 74-83-9 1310 ug/L 50.0 4.1 1 07/06/23 22:04 75-65-0 ND ug/L 0.50 0.066 1 07/06/23 22:04 104-51-8 ND ug/L 0.50 0.085 1 07/06/23 22:04 135-98-8 ND ug/L 0.50 0.086 1 07/06/23 22:04 98-06-6 ND ug/L 50.0 0.30 1 07/06/23 22:04 762-75-4 ND ug/L 0.50 0.17 1 07/06/23 22:04 56-23-5 ND ug/L 0.50 0.085 1 07/06/23 22:04 108-90-7 ND ug/L 1.0 0.17 1 07/06/23 22:04 75-00-3 0.22J ug/L 0.50 0.069 1 07/06/23 22:04 67-66-3 0.52J ug/L 1.0 0.18 1 07/06/23 22:04 74-87-3 ND ug/L 0.50 0.13 1 07/06/23 22:04 95-49-8 ND ug/L 0.50 0.096 1 07/06/23 22:04 106-43-4 ND ug/L 1.0 0.18 1 07/06/23 22:04 96-12-8 ND ug/L 0.50 0.15 1 07/06/23 22:04 124-48-1 ND ug/L 0.50 0.15 1 07/06/23 22:04 106-93-4 ND ug/L 0.50 0.19 1 07/06/23 22:04 74-95-3 ND ug/L 0.50 0.094 1 07/06/23 22:04 95-50-1 ND ug/L 0.50 0.098 1 07/06/23 22:04 541-73-1 ND ug/L 0.50 0.090 1 07/06/23 22:04 106-46-7 ND ug/L 0.50 0.12 1 07/06/23 22:04 75-71-8 ND ug/L 0.50 0.056 1 07/06/23 22:04 75-34-3 ND ug/L 0.50 0.11 1 07/06/23 22:04 107-06-2 ND ug/L 0.50 0.079 1 07/06/23 22:04 75-35-4 ND ug/L 0.50 0.11 1 07/06/23 22:04 156-59-2 ND ug/L 0.50 0.10 1 07/06/23 22:04 156-60-5 ND ug/L 0.50 0.14 1 07/06/23 22:04 78-87-5 ND ug/L 0.50 0.085 1 07/06/23 22:04 142-28-9 ND ug/L 0.50 0.12 1 07/06/23 22:04 594-20-7 ND ug/L 0.50 0.066 1 07/06/23 22:04 563-58-6 ND ug/L 0.50 0.090 1 07/06/23 22:04 10061-01-5 ND ug/L 0.50 0.13 1 07/06/23 22:04 10061-02-6 67.4 ug/L 0.50 0.072 1 07/06/23 22:04 108-20-3 ND ug/L 200 5.0 1 07/06/23 22:04 64-17-5 1.0 ug/L 0.50 0.081 1 07/06/23 22:04 100-41-4 1.3J ug/L 10.0 0.11 1 07/06/23 22:04 637-92-3 ND ug/L 2.0 0.35 1 07/06/23 22:04 87-68-3 2.0 ug/L 0.50 0.11 1 07/06/23 22:04 98-82-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, without the written consent of Pace Analytical Services, LLC. C9 L1 Page 30 of 64 _ti I ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-14 Lab ID: 92675483011 Collected: 06/29/23 11:15 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte Methylene Chloride ND ug/L 2.0 1.9 1 07/06/23 19:03 75-09-2 Methyl-tert-butyl ether 17.2 ug/L 0.50 0.053 1 07/06/23 19:03 1634-04-4 Naphthalene 5.8 ug/L 2.0 0.10 1 07/06/23 19:03 91-20-3 n-Propylbenzene 2.6 ug/L 0.50 0,10 1 07/06/23 19:03 103-65-1 Styrene ND ug/L 0.50 0.14 1 07/06/23 19:03 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 0.091 1 07/06/23 19:03 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 0.074 1 07/06/23 19:03 79-34-5 Tetrachloroethene ND ug/L 0.50 0.086 1 07/06/23 19:03 127-18-4 Toluene 0.31J ug/L 0.50 0.090 1 07/06/23 19:03 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 0.12 1 07/06/23 19:03 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 0.16 1 07/06/23 19:03 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 0.11 1 07/06/23 19:03 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 0.096 1 07/06/23 19:03 79-00-5 Trichloroethene ND ug/L 0.50 0.17 1 07/06/23 19:03 79-01-6 Trichloroll uoromethane ND ug/L 1.0 0.14 1 07/06/23 19:03 75-69-4 1,2,3-Trichloropropane ND ug/L 0.50 0.17 1 07/06/23 19:03 96-18-4 1,2,4-Trimethylbenzene 1.3 ug/L 0.50 0.031 1 07/06/23 19:03 95-63-6 1,3,5-Trimethylbenzene ND ug/L 0.50 0.071 1 07/06/23 19:03 10B-67-8 Vinyl chloride ND ug/L 1.0 0.15 1 07/06/23 19:03 75-01-4 m&p-Xylene 1.5 ug/L 1.0 0.094 1 07/06/23 19:03 179601-23-1 o-Xylene ND ug/L 0.50 0.14 1 07/06/23 19:03 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 98 % 70-130 1 07/06/23 19:03 17060-07-0 4-Bromofluorobenzene (S) 97 % 70-130 1 07/06/23 19:03 460-00-4 Toluene-d8 (S) 99 %, 70-130 1 07/06/23 19:03 2037-26-5 Date: 07/11/2023 01:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 29 of 64 r' �ce ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-16 Lab ID: 92675483013 Collected: 06/29/23 12:00 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200E MSV tert-Amyl Alcohol tert-Amylmethyl ether Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane tert-Butyl Alcohol n-Butylbenzene sec-Butylbenzene tert-Butyl benzene tert-Butyl Formate Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether Ethanol Ethylbenzene Ethyl-tert-butyl ether Hexachloro-1,3-butadiene Isopropylbenzene (Cumene) Date: 07/11/2023 01:23 PM Analytical Method: SM 6200B Pace Analytical Services - Charlotte ND ug/L 100 7.4 1 07/06/2319:21 75-85-4 ND ug/L 10.0 0.12 1 07/06/2319:21 994-05-8 ND ug/L 0.50 0.079 1 07/06/2319:21 71-43-2 ND ug/L 0.50 0.14 1 07/06/2319:21 108-86-1 ND ug/L 0.50 0.094 1 07/06/2319:21 74-97-5 ND ug/L 0.50 0.17 1 07/06/2319:21 75-27-4 ND ug/L 0.50 0.20 1 07/06/2319:21 75-25-2 ND ug/L 5.0 0.22 1 07/06/2319:21 74-83-9 ND ug/L 50.0 4.1 1 07/06/2319:21 75-65-0 ND ug/L 0.50 0.066 1 07/06/2319:21 104-51-8 ND ug/L 0.50 0.085 1 07/06/2319:21 135-98-8 ND ug/L 0.50 0.086 1 07/06/2319:21 98-06-6 ND ug/L 50.0 0.30 1 07/06/2319:21 762-75-4 ND ug/L 0.50 0.17 1 07/06/2319:21 56-23-5 ND ug/L 0.50 0.085 1 07/06/2319:21 108-90-7 ND ug/L 1.0 0.17 1 07/06/2319:21 75-00-3 0.34J ug/L 0.50 0.069 1 07/06/2319:21 67-66-3 ND ug/L 1.0 0.18 1 07/06/2319:21 74-87-3 ND ug/L 0.50 0.13 1 07/06/2319:21 95-49-8 ND ug/L 0.50 0.096 1 07/06/2319:21 106-43-4 ND ug/L 1.0 0.18 1 07/06/2319:21 96-12-8 ND ug/L 0.50 0.15 1 07/06/2319:21 124-48-1 ND ug/L 0.50 0.15 1 07/06/2319:21 106-93-4 ND ug/L 0.50 0.19 1 07/06/2319:21 74-95-3 ND ug/L 0.50 0.094 1 07/06/2319:21 95-50-1 ND ug/L 0.50 0.096 1 07/06/2319:21 541-73-1 ND ug/L 0.50 0.090 1 07/06/2319:21 106-46-7 ND ug/L 0.50 0.12 1 07/06/2319:21 75-71-8 ND ug/L 0.50 0.056 1 07/06/2319:21 75-34-3 ND ug/L 0.50 0.11 1 07/06/2319:21 107-06-2 ND ug/L 0.50 0.079 1 07/06/2319:21 75-35-4 ND ug/L 0.50 0.11 1 07/06/2319:21 156-59-2 ND ug/L 0.50 0.10 1 07/06/2319:21 156-60-5 ND ug/L 0.50 0.14 1 07/06/2319:21 78-87-5 ND ug/L 0.50 0.085 1 07/06/2319:21 142-28-9 ND ug/L 0.50 0.12 1 07/06/2319:21 594-20-7 ND ug/L 0.50 0.066 1 07/06/2319:21 563-58-6 ND ug/L 0.50 0.090 1 07/06/2319:21 10061-01-5 ND ug/L 0.50 0.13 1 07/06/2319:21 10061-02-6 ND ug/L 0.50 0.072 1 07/06/2319:21 108-20-3 ND ug/L 200 5.0 1 07/06/2319:21 64-17-5 ND ug/L 0.50 0.081 1 07/06/2319:21 100-41-4 ND ug/L 10.0 0.11 1 07/06/2319:21 637-92-3 ND ug/L 2.0 0.35 1 07/06/2319:21 87-68-3 ND ug/L 0.50 0.11 1 07/06/2319:21 98-82-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. C9 L1 Page 32 of 64 1 1 I [1 (-'09ace ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-19 Lab ID: 92675483012 Collected: 06/29/23 11:20 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte Methylene Chloride ND ug/L 2.0 1.9 1 07/06/23 22:04 75-09-2 Methyl-tert-butyl ether 38.9 ug/L 0.50 0.053 1 07/06/23 22:04 1634-04-4 Naphthalene 3.6 ug/L 2.0 0.10 1 07/06/23 22:04 91-20-3 n-Propylbenzene 3.5 ug/L 0.50 0.10 1 07/06/23 22:04 103-65-1 Styrene ND ug/L 0.50 0.14 1 07/06/23 22:04 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 0.091 1 07/06/23 22:04 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 0.074 1 07/06/23 22:04 79-34-5 Tetrachloroethene ND ug/L 0.50 0.086 1 07/06/23 22:04 127-18-4 Toluene 0.77 ug/L 0.50 0.090 1 07/06/23 22:04 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 0.12 1 07/06/23 22:04 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 0.16 1 07/06/23 22:04 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 0.11 1 07/06/23 22:04 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 0.096 1 07/06/23 22:04 79-00-5 Trichloroethene ND ug/L 0.50 0.17 1 07/06/23 22:04 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.14 1 07/06/23 22:04 75-69-4 1,2,3-Trichloropropane ND ug/L 0.50 0.17 1 07/06/23 22:04 96-18-4 1,2,4-Trimethylbenzene ND ug/L 0.50 0.031 1 07/06/23 22:04 95-63-6 1,3,5-Trimethyl benzene ND ug/L 0.50 0.071 1 07/06/23 22:04 108-67-8 Vinyl chloride ND ug/L 1.0 0.15 1 07/06/23 22:04 75-01-4 m&p-Xylene 5.5 ug/L 1.0 0.094 1 07/06/23 22:04 179601-23-1 o-Xylene 0.68 ug/L 0.50 0.14 1 07/06/23 22:04 95-47-6 Surrogates 1,2-Dichloroethane-d4(S) 97 % 70-130 1 07/06/23 22:04 17060-07-0 4-Bromofluorobenzene (S) 99 % 70-130 1 07/06/23 22:04 460-00-4 Toluene-d8 (S) 99 % 70-130 1 07/06/23 22:04 2037-26-5 Date: 07/11/2023 01:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 31 of 64 �ce ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-18 Lab ID: 92675483014 Collected: 06/29/23 11:35 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV tert-Amyl Alcohol tert-Amylmethyl ether Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane tert-Butyl Alcohol n-Butylbenzene sec-Butylbenzene tert-Butylbenzene tert-Butyl Formate Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether Ethanol Ethylbenzene Ethyl-tert-butyl ether Hexachloro-1,3-butadiene Isopropylbenzene (Cumene) Analytical Method: SM 6200B Pace Analytical Services - Charlotte ND ug/L 100 7.4 1 07/06/2319:39 75-85-4 ND ug/L 10.0 0.12 1 07/06/2319:39 994-05-8 ND ug/L 0.50 0.079 1 07/06/2319:39 71-43-2 ND ug/L 0.50 0.14 1 07/06/2319:39 108-86-1 ND ug/L 0.50 0.094 1 07/06/2319:39 74-97-5 ND ug/L 0.50 0.17 1 07/06/2319:39 75-27-4 ND ug/L 0.50 0.20 1 07/06/2319:39 75-25-2 ND ug/L 5.0 0.22 1 07/06/2319:39 74-83-9 ND ug/L 50.0 4.1 1 07/06/2319:39 75-65-0 ND ug/L 0.50 0.066 1 07/06/2319:39 104-51-8 ND ug/L 0.50 0.085 1 07/06/2319:39 135-98-8 ND ug/L 0.50 0.086 1 07/06/2319:39 98-06-6 ND ug/L 50.0 0.30 1 07/06/2319:39 762-75-4 ND ug/L 0.50 0.17 1 07/06/2319:39 56-23-5 ND ug/L 0.50 0.085 1 07/06/2319:39 10B-90-7 ND ug/L 1.0 0.17 1 07/06/2319:39 75-00-3 0.31 J ug/L 0.50 0.069 1 07/06/23 19:39 67-66-3 ND ug/L 1.0 0.18 1 07/06/2319:39 74-87-3 ND ug/L 0.50 0.13 1 07/06/2319:39 95-49-8 ND ug/L 0.50 0.096 1 07/06/2319:39 106-43-4 ND ug/L 1.0 0.18 1 07/06/2319:39 96-12-8 ND ug/L 0.50 0.15 1 07/06/2319:39 124-48-1 ND ug/L 0.50 0.15 1 07/06/2319:39 106-93-4 ND ug/L 0.50 0.19 1 07/06/2319:39 74-95-3 ND ug/L 0.50 0.094 1 07/06/2319:39 95-50-1 ND ug/L 0.50 0.098 1 07/06/2319:39 541-73-1 ND ug/L 0.50 0.090 1 07/06/2319:39 106-46-7 ND ug/L 0.50 0.12 1 07/06/2319:39 75-71-8 ND ug/L 0.50 0.056 1 07/06/2319:39 75-34-3 ND ug/L 0.50 0.11 1 07/06/2319:39 107-06-2 ND ug/L 0.50 0.079 1 07/06/2319:39 75-35-4 ND ug/L 0.50 0.11 1 07/06/2319:39 156-59-2 ND ug/L 0.50 0.10 1 07/06/2319:39 156-60-5 ND ug/L 0.50 0.14 1 07/06/2319:39 78-87-5 ND ug/L 0.50 0.085 1 07/06/2319:39 142-28-9 ND ug/L 0.50 0.12 1 07/06/2319:39 594-20-7 ND ug/L 0.50 0.066 1 07/06/2319:39 563-58-6 ND ug/L 0.50 0.090 1 07/06/2319:39 10061-01-5 ND ug/L 0.50 0.13 1 07/06/2319:39 10061-02-6 ND ug/L 0.50 0.072 1 07/06/2319:39 108-20-3 ND ug/L 200 5.0 1 07/06/2319:39 64-17-5 ND ug/L 0.50 0.081 1 07/06/2319:39 100-41-4 ND ug/L 10.0 0.11 1 07/06/2319:39 637-92-3 ND ug/L 2.0 0.35 1 07/06/2319:39 87-68-3 ND ug/L 0.50 0.11 1 07/06/2319:39 98-82-8 REPORT OF LABORATORY ANALYSIS C9 L1 This report shall not be reproduced, except in full, Date: 07/11 /2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 64 E 1 1 (--'$Pace ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-16 Lab ID: 92675483013 Collected: 06/29/23 12:00 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte Methylene Chloride ND ug/L 2.0 1.9 1 07/06/23 19:21 75-09-2 Methyl-tert-butyl ether ND ug/L 0.50 0.053 1 07/06/23 19:21 1634-04-4 Naphthalene 0.42J ug/L 2.0 0.10 1 07/06/23 19:21 91-20-3 n-Propylbenzene ND ug/L 0.50 0.10 1 07/06/23 19:21 103-65-1 Styrene ND ug/L 0.50 0.14 1 07/06/23 19:21 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 0.091 1 07/06/23 19:21 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 0.074 1 07/06/23 19:21 79-34-5 Tetrachloroethene ND ug/L 0.50 0.086 1 07/06/23 19:21 127-18-4 Toluene ND ug/L 0.50 0.090 1 07/06/23 19:21 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 0.12 1 07/06/23 19:21 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 0.16 1 07/06/23 19:21 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 0.11 1 07/06/23 19:21 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 0.096 1 07/06/23 19:21 79-00-5 Trichloroethene ND ug/L 0.50 0.17 1 07/06/23 19:21 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.14 1 07/06/23 19:21 75-69-4 1,2,3-Trichloropropane ND ug/L 0.50 0.17 1 07/06/23 19:21 96-18-4 1,2,4-Trimethyl benzene ND ug/L 0.50 0.031 1 07/06/23 19:21 95-63-6 1,3,5-Trimethyl benzene ND ug/L 0.50 0.071 1 07/06/23 19:21 108-67-8 Vinyl chloride ND ug/L 1.0 0.15 1 07/06/23 19:21 75-01-4 m&p-Xylene ND ug/L 1.0 0.094 1 07/06/23 19:21 179601-23-1 o-Xylene ND ug/L 0.50 0.14 1 07/06/23 19:21 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 97 % 70-130 1 07/06/23 19:21 17060-07-0 4-Bromofluorobenzene (S) 97 % 70-130 1 07/06/23 19:21 460-00-4 Toluene-d8 (S) 103 % 70-130 1 07/06/23 19:21 2037-26-5 Date: 07/11/2023 01:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 33 of 64 (--'*Pa ce ANALYTICAL RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Sample: MW-10 Lab ID: 92675483015 Collected: 06/30/23 10:00 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte tert-Amyl Alcohol ND ug/L 100 7.4 1 07/06/23 19:57 75-85-4 tert-Amylmethyl ether ND ug/L 10.0 0.12 1 07/06/23 19:57 994-05-8 Benzene ND ug/L 0.50 0.079 1 07/06/23 19:57 71-43-2 Bromobenzene ND ug/L 0.50 0.14 1 07/06/23 19:57 108-86-1 Bromochloromethane ND ug/L 0.50 0.094 1 07/06/23 19:57 74-97-5 Bromodichloromethane ND ug/L 0.50 0.17 1 07/06/23 19:57 75-27-4 Bromoform ND ug/L 0.50 0.20 1 07/06/23 19:57 75-25-2 Bromomethane ND ug/L 5.0 0.22 1 07/06/23 19:57 74-83-9 tert-Butyl Alcohol ND ug/L 50.0 4.1 1 07/06/23 19:57 75-65-0 n-Butylbenzene ND ug/L 0.50 0.066 1 07/06/23 19:57 104-51-8 sec- Butyl benzene ND ug/L 0.50 0.085 1 07/06/23 19:57 135-98-8 tert-Butylbenzene ND ug/L 0.50 0.086 1 07/06/23 19:57 98-06-6 tert-Butyl Formate ND ug/L 50.0 0.30 1 07/06/23 19:57 762-75-4 Carbon tetrachloride ND ug/L 0.50 0.17 1 07/06/23 19:57 56-23-5 Chlorobenzene ND ug/L 0.50 0.085 1 07/06/23 19:57 108-90-7 Chloroethane ND ug/L 1.0 0.17 1 07/06/23 19:57 75-00-3 Chloroform 0.29J ug/L 0.50 0.069 1 07/06/23 19:57 67-66-3 C9 Chloromethane ND ug/L 1.0 0.18 1 07/06/23 19:57 74-87-3 2-Chlorotoluene ND ug/L 0.50 0.13 1 07/06/23 19:57 95-49-8 4-Chlorotoluene ND ug/L 0.50 0.096 1 07/06/23 19:57 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1.0 0.18 1 07/06/23 19:57 96-12-8 Dibromochloromethane ND ug/L 0.50 0.15 1 07/06/23 19:57 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 0.50 0.15 1 07/06/23 19:57 106-93-4 Dibromomethane ND ug/L 0.50 0.19 1 07/06/23 19:57 74-95-3 1,2-Dichlorobenzene ND ug/L 0.50 0.094 1 07/06/23 19:57 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 0.098 1 07/06/23 19:57 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 0.090 1 07/06/23 19:57 106-46-7 Dichlorodifluoromethane ND ug/L 0.50 0.12 1 07/06/23 19:57 75-71-8 L1 .` 1,1-Dichloroethane ND ug/L 0.50 0.056 1 07/06/23 19:57 75-34-3 1,2-Dichloroethane ND ug/L 0.50 0.11 1 07/06/23 19:57 107-06-2 1,1-Dichloroethene ND ug/L 0.50 0.079 1 07/06/23 19:57 75-35-4 cis-1,2-Dichloroethene ND ug/L 0.50 0.11 1 07/06/23 19:57 156-59-2 trans- 1,2-Dichloroethene ND ug/L 0.50 0.10 1 07/06/23 19:57 156-60-5 1,2-Dichloropropane ND ug/L 0.50 0.14 1 07/06/23 19:57 78-87-5 1,3-Dichloropropane ND ug/L 0.50 0.085 1 07/06/23 19:57 142-28-9 2,2-Dichloropropane ND ug/L 0.50 0.12 1 07/06/23 19:57 594-20-7 1,1-Dichloropropene ND ug/L 0.50 0.066 1 07/06/23 19:57 563-58-6 cis-1,3-Dichloropropene ND ug/L 0.50 0.090 1 07/06/23 19:57 10061-01-5 trans-1,3-Dichloropropene ND ug/L 0.50 0.13 1 07/06/23 19:57 10061-02-6 Diisopropyl ether 0.13J ug/L 0.50 0.072 1 07/06/23 19:57 108-20-3 Ethanol ND ug/L 200 5.0 1 07/06/23 19:57 64-17-5 Ethylbenzene ND ug/L 0.50 0.081 1 07/06/23 19:57 100-41-4 Ethyl-tert-butyl ether ND ug/L 10.0 0.11 1 07/06/23 19:57 637-92-3 Hexachloro-1,3-butadiene ND ug/L 2.0 0.35 1 07/06/23 19:57 87-68-3 Isopropylbenzene (Cumene) ND ug/L 0.50 0.11 1 07/06/23 19:57 98-82-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 64 1 1 r_ [1 ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-18 Lab ID: 92675483014 Collected: 06/29/23 11:35 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte Methylene Chloride ND ug/L 2.0 1.9 1 07/06/23 19:39 75-09-2 Methyl-tert-butyl ether ND ug/L 0.50 0.053 1 07/06/23 19:39 1634-04-4 Naphthalene ND ug/L 2.0 0.10 1 07/06/23 19:39 91-20-3 n-Propylbenzene ND ug/L 0.50 0.10 1 07/06/23 19:39 103-65-1 Styrene ND ug/L 0.50 0.14 1 07/06/23 19:39 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 0.091 1 07/06/23 19:39 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 0.074 1 07/06/23 19:39 79-34-5 Tetrachloroethene ND ug/L 0.50 0.086 1 07/06/23 19:39 127-18-4 Toluene ND ug/L 0.50 0.090 1 07/06/23 19:39 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 0.12 1 07/06/23 19:39 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 0.16 1 07/06/23 19:39 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 0.11 1 07/06/23 19:39 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 0.096 1 07/06/23 19:39 79-00-5 Trichloroethene ND ug/L 0.50 0.17 1 07/06/23 19:39 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.14 1 07/06/23 19:39 75-69-4 1,2,3-Trichloropropane ND ug/L 0.50 0.17 1 07/06/23 19:39 96-18-4 1,2,4-Trimethylbenzene ND ug/L 0.50 0.031 1 07/06/23 19:39 95-63-6 1,3,5-Trimethyl benzene ND ug/L 0.50 0.071 1 07/06/23 19:39 108-67-8 Vinyl chloride ND ug/L 1.0 0.15 1 07/06/23 19:39 75-01-4 m&p-Xylene ND ug/L 1.0 0.094 1 07/06/23 19:39 179601-23-1 o-Xylene ND ug/L 0.50 0.14 1 07/06/23 19:39 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 97 % 70-130 1 07/06/23 19:39 17060-07-0 4-Bromofluorobenzene (S) 98 % 70-130 1 07/06/23 19:39 460-00-4 Toluene-d8 (S) 103 % 70-130 1 07/06/23 19:39 2037-26-5 Date: 07/11/2023 01:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 35 of 64 ace" ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-11R Lab ID: 92675483016 Collected: 06/30/23 10:30 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV tert-Amyl Alcohol tert-Amylmethyl ether Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane tert-Butyl Alcohol n-Butylbenzene sec-Butylbenzene tert-Butylbenzene tert-Butyl Formate Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropane 1,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis-1, 3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether Ethanol Ethylbenzene Ethyl-tert-butyl ether Hexachloro-1,3-butadiene Isopropylbenzene (Cumene) Analytical Method: SM 62006 Pace Analytical Services - Charlotte ND ug/L 100 7.4 1 07/06/23 20:15 75-85-4 ND ug/L 10.0 0.12 1 07/06/23 20:15 994-05-8 1.5 ug/L 0.50 0.079 1 07/06/23 20:15 71-43-2 ND ug/L 0.50 0.14 1 07/06/23 20:15 108-86-1 ND ug/L 0.50 0.094 1 07/06/23 20:15 74-97-5 ND ug/L 0.50 0.17 1 07/06/23 20:15 75-27-4 ND ug/L 0.50 0.20 1 07/06/23 20:15 75-25-2 ND ug/L 5.0 0.22 1 07/06/23 20:15 74-83-9 ND ug/L 50.0 4.1 1 07/06/23 20:15 75-65-0 ND ug/L 0.50 0.066 1 07/06/23 20:15 104-51-8 ND ug/L 0.50 0.085 1 07/06/23 20:15 135-98-8 ND ug/L 0.50 0.086 1 07/06/23 20:15 98-06-6 ND ug/L 50.0 0.30 1 07/06/23 20:15 762-75-4 ND ug/L 0.50 0.17 1 07/06/23 20:15 56-23-5 ND ug/L 0.50 0.085 1 07/06/23 20:15 108-90-7 ND ug/L 1.0 0.17 1 07/06/23 20:15 75-00-3 0.31J ug/L 0.50 0.069 1 07/06/23 20:15 67-66-3 ND ug/L 1.0 0.18 1 07/06/23 20:15 74-87-3 ND ug/L 0.50 0.13 1 07/06/23 20:15 95-49-8 ND ug/L 0.50 0.096 1 07/06/23 20:15 106-43-4 ND ug/L 1.0 0.18 1 07/06/23 20:15 96-12-8 ND ug/L 0.50 0.15 1 07/06/23 20:15 124-48-1 ND ug/L 0.50 0.15 1 07/06/23 20:15 106-93-4 ND ug/L 0.50 0.19 1 07/06/23 20:15 74-95-3 ND ug/L 0.50 0.094 1 07/06/23 20:15 95-50-1 ND ug/L 0.50 0.098 1 07/06/23 20:15 541-73-1 ND ug/L 0.50 0.090 1 07/06/23 20:15 106-46-7 ND ug/L 0.50 0.12 1 07/06/23 20:15 75-71-8 ND ug/L 0.50 0.056 1 07/06/23 20:15 75-34-3 ND ug/L 0.50 0.11 1 07/06/23 20:15 107-06-2 ND ug/L 0.50 0.079 1 07/06/23 20:15 75-35-4 ND ug/L 0.50 0.11 1 07/06/23 20:15 156-59-2 ND ug/L 0.50 0.10 1 07/06/23 20:15 156-60-5 ND ug/L 0.50 0.14 1 07/06/23 20:15 78-87-5 ND ug/L 0.50 0.085 1 07/06/23 20:15 142-28-9 ND ug/L 0.50 0.12 1 07/06/23 20:15 594-20-7 ND ug/L 0.50 0.066 1 07/06/23 20:15 563-58-6 ND ug/L 0.50 0.090 1 07/06/23 20:15 10061-01-5 ND ug/L 0.50 0.13 1 07/06/23 20:15 10061-02-6 0.27J ug/L 0.50 0.072 1 07/06/23 20:15 108-20-3 ND ug/L 200 5.0 1 07/06/23 20:15 64-17-5 1.6 ug/L 0.50 0.081 1 07/06/23 20:15 100-41-4 ND ug/L 10.0 0.11 1 07/06/23 20:15 637-92-3 ND ug/L 2.0 0.35 1 07/06/23 20:15 87-68-3 ND ug/L 0.50 0.11 1 07/06/23 20:15 98-82-8 REPORT OF LABORATORY ANALYSIS C9 L1 This report shall not be reproduced, except in full, Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 64 (-'09aca ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-10 Lab ID: 92675483015 Collected: 06/30/23 10:00 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte Methylene Chloride ND ug/L 2.0 1.9 1 07/06/23 19:57 75-09-2 Methyl-tert-butyl ether ND ug/L 0.50 0.053 1 07/06/23 19:57 1634-04-4 Naphthalene ND ug/L 2.0 0.10 1 07/06/23 19:57 91-20-3 n-Propylbenzene ND ug/L 0.50 0.10 1 07/06/23 19:57 103-65-1 Styrene ND ug/L 0.50 0.14 1 07/06/23 19:57 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 0.091 1 07/06/23 19:57 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 0.074 1 07/06/23 19:57 79-34-5 Tetrachloroethene ND ug/L 0.50 0.086 1 07/06/23 19:57 127-18-4 Toluene ND ug/L 0.50 0.090 1 07/06/23 19:57 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 0.12 1 07/06/23 19:57 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 0.16 1 07/06/23 19:57 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 0.11 1 07/06/23 19:57 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 0.096 1 07/06/23 19:57 79-00-5 Trichloroethene ND ug/L 0.50 0.17 1 07/06/23 19:57 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.14 1 07/06/23 19:57 75-69-4 1,2,3-Trichloropropane ND ug/L 0.50 0.17 1 07/06/23 19:57 96-18-4 1,2,4-Trimethyl benzene ND ug/L 0.50 0.031 1 07/06/23 19:57 95-63-6 1,3,5-Trimethyl benzene ND ug/L 0.50 0.071 1 07/06/23 19:57 108-67-8 Vinyl chloride ND ug/L 1.0 0.15 1 07/06/23 19:57 75-01-4 m&p-Xylene ND ug/L 1.0 0.094 1 07/06/23 19:57 179601-23-1 o-Xylene ND ug/L 0.50 0.14 1 07/06/23 19:57 95-47-6 Surrogates 1,2-Dichloroethane-d4 (S) 97 % 70-130 1 07/06/23 19:57 17060-07-0 4-Bromofluorobenzene (S) 98 % 70-130 1 07/06/23 19:57 460-00-4 Toluene-d8 (S) 102 % 70-130 1 07/06/23 19:57 2037-26-5 Date: 07/11/2023 01:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 37 of 64 Pace Analytical Services, LLC 9800 Kinoey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Sample: TRIP BLANK Lab ID: 92675483017 Collected: 06/30/23 00:00 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte tert-Amyl Alcohol ND ug/L 100 7.4 1 07/05/23 13:52 75-85-4 tert-Amylmethyl ether ND ug/L 10.0 0.12 1 07/05/23 13:52 994-05-8 Benzene ND ug/L 0.50 0.079 1 07/05/23 13:52 71-43-2 Bromobenzene ND ug/L 0.50 0.14 1 07/05/23 13:52 108-86-1 Bromochloromethane ND ug/L 0.50 0.094 1 07/05/23 13:52 74-97-5 Bromodichloromethane ND ug/L 0.50 0.17 1 07/05/23 13:52 75-27-4 Bromoform ND ug/L 0.50 0.20 1 07/05/23 13:52 75-25-2 Bromomethane ND ug/L 5.0 0.22 1 07/05/23 13:52 74-83-9 tert-Butyl Alcohol ND ug/L 50.0 4.1 1 07/05/23 13:52 75-65-0 n-Butylbenzene ND ug/L 0.50 0.066 1 07/05/23 13:52 104-51-8 sec-Butylbenzene ND ug/L 0.50 0.085 1 07/05/23 13:52 135-98-8 tert-Butylbenzene ND ug/L 0.50 0.086 1 07/05/23 13:52 98-06-6 tert-Butyl Formate ND ug/L 50.0 0.30 1 07/05/23 13:52 762-75-4 Carbon tetrachloride ND ug/L 0.50 0.17 1 07/05/23 13:52 56-23-5 Chlorobenzene ND ug/L 0.50 0.085 1 07/05/23 13:52 108-90-7 Chloroethane ND ug/L 1.0 0.17 1 07/05/23 13:52 75-00-3 Chloroform ND ug/L 0.50 0.069 1 07/05/23 13:52 67-66-3 Chloromethane ND ug/L 1.0 0.18 1 07/05/23 13:52 74-87-3 2-Chlorotoluene ND ug/L 0.50 0.13 1 07/05/23 13:52 95-49-8 4-Chlorotoluene ND ug/L 0.50 0.096 1 07/05/23 13:52 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1.0 0.18 1 07/05/23 13:52 96-12-8 Dibromochloromethane ND ug/L 0.50 0.15 1 07/05/23 13:52 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 0.50 0.15 1 07/05/23 13:52 106-93-4 Dibromomethane ND ug/L 0.50 0.19 1 07/05/23 13:52 74-95-3 1,2-Dichlorobenzene ND ug/L 0.50 0.094 1 07/05/23 13:52 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 0.098 1 07/05/23 13:52 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 0.090 1 07/05/23 13:52 106-46-7 Dichlorodifluoromethane ND ug/L 0.50 0.12 1 07/05/23 13:52 75-71-8 1,1-Dichloroethane ND ug/L 0.50 0.056 1 07/05/23 13:52 75-34-3 1,2-Dichloroethane ND ug/L 0.50 0.11 1 07/05/23 13:52 107-06-2 1,1-Dichloroethene ND ug/L 0.50 0.079 1 07/05/23 13:52 75-35-4 cis-1,2-Dichloroethene ND ug/L 0.50 0.11 1 07/05/23 13:52 156-59-2 trans-1,2-Dichloroethene ND ug/L 0.50 0.10 1 07/05/23 13:52 156-60-5 1,2-Dichloropropane ND ug/L 0.50 0.14 1 07/05/23 13:52 78-87-5 1,3-Dichloropropane ND ug/L 0.50 0.085 1 07/05/23 13:52 142-28-9 2,2-Dichloropropane ND ug/L 0.50 0.12 1 07/05/23 13:52 594-20-7 1,1-Dichloropropene ND ug/L 0.50 0.066 1 07/05/23 13:52 563-58-6 cis-1,3-Dichloropropene ND ug/L 0.50 0.090 1 07/05/23 13:52 10061-01-5 trans-1,3-Dichloropropene ND ug/L 0.50 0.13 1 07/05/23 13:52 10061-02-6 Diisopropyl ether ND ug/L 0.50 0.072 1 07/05/23 13:52 108-20-3 Ethanol ND ug/L 200 5.0 1 07/05/23 13:52 64-17-5 Ethylbenzene ND ug/L 0.50 0.081 1 07/05/23 13:52 100-41-4 Ethyl-tert-butyl ether ND ug/L 10.0 0.11 1 07/05/23 13:52 637-92-3 Hexachloro-1,3-butadiene ND ug/L 2.0 0.35 1 07/05/23 13:52 87-68-3 Isopropylbenzene (Cumene) ND ug/L 0.50 0.11 1 07/05/23 13:52 98-82-8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 64 1 I �1 ANALYTICAL RESULTS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: MW-11 R Lab ID: 92675483016 Collected: 06/30/23 10:30 Received: 06/30/23 13:25 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6200E MSV Analytical Method: SM 6200B Pace Analytical Services - Charlotte Methylene Chloride ND ug/L 2.0 1.9 1 07/06/23 20:15 75-09-2 Methyl-tert-butyl ether 0.95 ug/L 0.50 0.053 1 07/06/23 20:15 1634-04-4 Naphthalene ND ug/L 2.0 0.10 1 07/06/23 20:15 91-20-3 n-Propylbenzene 0.44J ug/L 0.50 0.10 1 07/06/23 20:15 103-65-1 Styrene ND ug/L 0.50 0.14 1 07/06/23 20:15 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 0.091 1 07/06/23 20:15 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 0.074 1 07/06/23 20:15 79-34-5 Tetrachloroethene ND ug/L 0.50 0.086 1 07/06/23 20:15 127-18-4 Toluene ND ug/L 0.50 0.090 1 07/06/23 20:15 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 0.12 1 07/06/23 20:15 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 0.16 1 07/06/23 20:15 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 0.11 1 07/06/23 20:15 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 0.096 1 07/06/23 20:15 79-00-5 Trichloroethene ND ug/L 0.50 0.17 1 07/06/23 20:15 79-01-6 Trichlorofluoromethane ND ug/L 1.0 0.14 1 07/06/23 20:15 75-69-4 1,2,3-Trichloropropane ND ug/L 0.50 0.17 1 07/06/23 20:15 96-18-4 1,2,4-Trimethylbenzene 1.4 ug/L 0.50 0.031 1 07/06/23 20:15 95-63-6 1,3,5-Trimethylbenzene 0.39J ug/L 0.50 0.071 1 07/06/23 20:15 108-67-8 Vinyl chloride ND ug/L 1.0 0.15 1 07/06/23 20:15 75-01-4 m&p-Xylene 2.2 ug/L 1.0 0.094 1 07/06/23 20:15 179601-23-1 o-Xylene ND ug/L 0.50 0.14 1 07/06/23 20:15 95-47-6 Surrogates 1,2-Dichloroethane-d4(S) 97 % 70-130 1 07/06/23 20:15 17060-07-0 4-Bromofluorobenzene (S) 98 % 70-130 1 07/06/23 20:15 460-00-4 Toluene-d8 (S) 102 %, 70-130 1 07/06/23 20:15 2037-26-5 Date: 07/11/2023 01:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 39 of 64 (-� Fa Ce, QUALITY CONTROL DATA Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 QC Batch: 784771 Analysis Method: SM 6200B QC Batch Method: SM 6200B Analysis Description: 6200B MSV Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92675483017 METHOD BLANK: 4069433 Associated Lab Samples: 92675483017 Parameter Units Matrix: Water Blank Reporting Result Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 0.50 0.091 07/05/23 11:11 1,1,1-Trichloroethane ug/L ND 0.50 0.11 07/05/23 11:11 1,1,2,2-Tetrachloroethane ug/L ND 0.50 0.074 07/05/23 11:11 1,1,2-Trichloroethane ug/L ND 0.50 0.096 07/05/23 11:11 1,1-Dichloroethane ug/L ND 0.50 0.056 07/05/23 11:11 1,1-Dichloroethene ug/L ND 0.50 0.079 07/05/23 11:11 1,1-Dichloropropene ug/L ND 0.50 0.066 07/05/23 11:11 1,2,3-Trichlorobenzene ug/L ND 2.0 0.12 07/05/23 11:11 1,2,3-Trichooropropane ug/L ND 0.50 0.17 07/05/23 11:11 1,2,4-Trichlorobenzene ug/L ND 2.0 0.16 07/05/23 11:11 1,2,4-Trimethylbenzene ug/L ND 0.50 0.031 07/05/23 11:11 1,2-Dibromo-3-chloropropane ug/L ND 1.0 0.18 07/05/23 11:11 1,2-Dibromoethane (EDB) ug/L ND 0.50 0.15 07/05/23 11:11 1,2-Dichlorobenzene ug/L ND 0.50 0.094 07/05/23 11:11 1,2-Dichloroethane ug/L ND 0.50 0.11 07/05/23 11:11 1,2-Dichloropropane ug/L ND 0.50 0.14 07/05/23 11:11 1,3,5-Trimethyl benzene ug/L ND 0.50 0.071 07/05/23 11:11 1,3-Dichlorobenzene ug/L ND 0.50 0.098 07/05/23 11:11 1,3-Dichloropropane ug/L ND 0.50 0.085 07/05/23 11:11 1,4-Dichlorobenzene ug/L ND 0.50 0.090 07/05/23 11:11 2,2-Dichloropropane ug/L ND 0.50 0.12 07/05/23 11:11 2-Chlorotoluene ug/L ND 0.50 0.13 07/05/23 11:11 4-Chlorotoluene ug/L ND 0.50 0.096 07/05/23 11:11 Benzene ug/L ND 0.50 0.079 07/05/23 11:11 Bromobenzene ug/L ND 0.50 0.14 07/05/23 11:11 Bromochloromethane ug/L ND 0.50 0.094 07/05/23 11:11 Bromodichloromethane ug/L ND 0.50 0.17 07/05/23 11:11 Bromoform ug/L ND 0.50 0.20 07/05/23 11:11 Bromomethane ug/L ND 5.0 0.22 07/05/23 11:11 Carbon tetrachloride ug/L ND 0.50 0.17 07/05/23 11:11 Chlorobenzene ug/L ND 0.50 0.085 07/05/23 11:11 Chloroethane ug/L ND 1.0 0.17 07/05/23 11:11 Chloroform ug/L ND 0.50 0.069 07/05/23 11:11 Chloromethane ug/L ND 1.0 0.18 07/05/23 11:11 cis-1,2-Dichloroethene ug/L ND 0.50 0.11 07/05/23 11:11 cis-1,3-Dichloropropene ug/L ND 0.50 0.090 07/05/23 11:11 Dibromochloromethane ug/L ND 0.50 0.15 07/05/23 11:11 Dibromomethane ug/L ND 0.50 0.19 07/05/23 11:11 Dichlorodifluoromethane ug/L ND 0.50 0.12 07/05/23 11:11 Diisopropyl ether ug/L ND 0.50 0.072 07/05/23 11:11 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 64 I (/A'o ?a ce Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Sample: TRIP BLANK Parameters 6200B MSV Methylene Chloride Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1, 2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethyl benzene 1,3,5-Trimethyl benzene Vinyl chloride m&p-Xylene o-Xylene Surrogates 1,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Date: 07/11/2023 01:23 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Lab ID: 92675483017 Collected: 06/30/23 00:00 Received: 06/30/23 13:25 Matrix: Water Report Results Units Limit MDL DF Prepared Analyzed CAS No. Analytical Method: SM 6200B Pace Analytical Services - Charlotte ND ug/L 2.0 1.9 1 07/05/2313:52 75-09-2 ND ug/L 0.50 0.053 1 07/05/2313:52 1634-04-4 ND ug/L 2.0 0.10 1 07/05/2313:52 91-20-3 ND ug/L 0.50 0.10 1 07/05/2313:52 103-65-1 ND ug/L 0.50 0.14 1 07/05/2313:52 100-42-5 ND ug/L 0.50 0.091 1 07/05/2313:52 630-20-6 ND ug/L 0.50 0.074 1 07/05/2313:52 79-34-5 ND ug/L 0.50 0.086 1 07/05/2313:52 127-18-4 ND ug/L 0.50 0.090 1 07/05/2313:52 108-88-3 ND ug/L 2.0 0.12 1 07/05/2313:52 87-61-6 ND ug/L 2.0 0.16 1 07/05/2313:52 120-82-1 ND ug/L 0.50 0.11 1 07/05/2313:52 71-55-6 ND ug/L 0.50 0.096 1 07/05/2313:52 79-00-5 ND ug/L 0.50 0.17 1 07/05/2313:52 79-01-6 ND ug/L 1.0 0.14 1 07/05/2313:52 75-69-4 ND ug/L 0.50 0.17 1 07/05/2313:52 96-18-4 ND ug/L 0.50 0.031 1 07/05/2313:52 95-63-6 ND ug/L 0.50 0.071 1 07/05/2313:52 108-67-8 ND ug/L 1.0 0.15 1 07/05/2313:52 75-01-4 ND ug/L 1.0 0.094 1 07/05/2313:52 179601-23-1 ND ug/L 0.50 0.14 1 07/05/2313:52 95-47-6 85 % 70-130 1 07/05/2313:52 17060-07-0 98 % 70-130 1 07/05/2313:52 460-00-4 96 % 70-130 1 07/05/2313:52 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Qual Page 41 of 64 ace, QUALITY CONTROL DATA Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 LABORATORY CONTROL SAMPLE: Parameter 4069434 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,2-Dibromo-3-chloropropane ug/L 20 17.2 86 60-140 1,2-Dibromoethane (EDB) ug/L 20 19.6 98 60-140 1,2-Dichlorobenzene ug/L 20 20.5 103 60-140 1,2-Dichloroethane ug/L 20 16.7 84 60-140 1,2-Dichloropropane ug/L 20 20.1 100 60-140 1,3,5-Trimethyl benzene ug/L 20 19.5 97 60-140 1,3-Dichlorobenzene ug/L 20 20.2 101 60-140 1,3-Dichloropropane ug/L 20 18.8 94 60-140 1,4-Dichlorobenzene ug/L 20 20.2 101 60-140 2,2-Dichloropropane ug/L 20 17.2 86 60-140 2-Chlorotoluene ug/L 20 19.2 96 60-140 4-Chlorotoluene ug/L 20 18.5 93 60-140 Benzene ug/L 20 19.0 95 60-140 Bromobenzene ug/L 20 19.7 99 60-140 Bromochloromethane ug/L 20 18.3 92 60-140 Bromodichloromethane ug/L 20 17.7 89 60-140 Bromoform ug/L 20 20.1 100 60-140 Bromomethane ug/L 20 12.5 62 60-140 Carbon tetrachloride ug/L 20 19.5 97 60-140 Chlorobenzene ug/L 20 20.0 100 60-140 Chloroethane ug/L 20 17.2 86 60-140 Chloroform ug/L 20 17.2 86 60-140 Chloromethane ug/L 20 20.4 102 60-140 cis-1,2-Dichloroethene ug/L 20 17.8 89 60-140 cis-1,3-Dichloropropene ug/L 20 18.8 94 60-140 Dibromochloromethane ug/L 20 18.6 93 60-140 Dibromomethane ug/L 20 20.8 104 60-140 Dichlorod ifluoromethane ug/L 20 24.9 124 60-140 Diisopropyl ether ug/L 20 16.7 83 60-140 Ethanol ug/L 800 591 74 60-140 Ethyl-tert-butyl ether ug/L 40 34.2 86 60-140 Ethylbenzene ug/L 20 19.1 96 60-140 Hexachloro-1,3-butadiene ug/L 20 22.4 112 60-140 Isopropyl benzene (Cumene) ug/L 20 20.4 102 60-140 m&p-Xylene ug/L 40 38.2 96 60-140 Methyl-tert-butyl ether ug/L 20 17.4 87 60-140 Methylene Chloride ug/L 20 16.4 82 60-140 n-Butylbenzene ug/L 20 18.1 91 60-140 n-Propylbenzene ug/L 20 18.3 91 60-140 Naphthalene ug/L 20 18.4 92 60-140 o-Xylene ug/L 20 19.5 97 60-140 sec-Butylbenzene ug/L 20 18.8 94 60-140 Styrene ug/L 20 19.8 99 60-140 tert-Amyl Alcohol ug/L 400 358 89 60-140 tert-Amylmethyl ether ug/L 40 37.6 94 60-140 tert-Butyl Alcohol ug/L 200 160 80 60-140 tert-Butyl Formate ug/L 160 140 88 60-140 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers kin Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 64 �ca Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 METHOD BLANK: 4069433 Associated Lab Samples: 92675483017 Parameter Units Ethanol ug/L Ethyl-tert-butyl ether ug/L Ethylbenzene ug/L Hexachloro-1,3-butadiene ug/L Isopropylbenzene (Cumene) ug/L m&p-Xylene ug/L Methyl-tert-butyl ether ug/L Methylene Chloride ug/L n-Butylbenzene ug/L n-Propylbenzene ug/L Naphthalene ug/L o-Xylene ug/L sec-Butylbenzene ug/L Styrene ug/L tert-Amyl Alcohol ug/L tert-Amylmethyl ether ug/L tert-Butyl Alcohol ug/L tert-Butyl Formate ug/L tert-Butylbenzene ug/L Tetrachloroethene ug/L Toluene ug/L trans- 1,2-Dichloroethene ug/L trans- 1,3-Dichloropropene ug/L Trichloroethene ug/L Trichlorofluoromethane ug/L Vinyl chloride ug/L 1,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) % Toluene-d8 (S) LABORATORY CONTROL SAMPLE: 4069434 QUALITY CONTROL DATA Matrix: Water Blank Result Reporting Limit MDL Analyzed ND 200 5.0 07/05/2311:11 ND 10.0 0.11 07/05/2311:11 ND 0.50 0.081 07/05/2311:11 ND 2.0 0.35 07/05/2311:11 ND 0.50 0.11 07/05/2311:11 ND 1.0 0.094 07/05/2311:11 ND 0.50 0.053 07/05/2311:11 ND 2.0 1.9 07/05/2311:11 ND 0.50 0.066 07/05/2311:11 ND 0.50 0.10 07/05/2311:11 ND 2.0 0.10 07/05/2311:11 ND 0.50 0.14 07/05/2311:11 ND 0.50 0.085 07/05/2311:11 ND 0.50 0.14 07/05/2311:11 ND 100 7.4 07/05/2311:11 ND 10.0 0.12 07/05/2311:11 ND 50.0 4.1 07/05/2311:11 ND 50.0 0,30 07/05/2311:11 ND 0.50 0.086 07/05/2311:11 ND 0.50 0.086 07/05/2311:11 ND 0.50 0.090 07/05/2311:11 ND 0.50 0.10 07/05/2311:11 ND 0.50 0.13 07/05/2311:11 ND 0.50 0.17 07/05/2311:11 ND 1.0 0.14 07/05/2311:11 ND 1.0 0.15 07/05/2311:11 84 70-130 07/05/2311:11 97 70-130 07/05/2311:11 96 70-130 07/05/2311:11 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 20 20.3 101 60-140 1,1,1-Trichloroethane ug/L 20 17.5 87 60-140 1,1,2,2-Tetrachloroethane ug/L 20 18.4 92 60-140 1,1,2-Trichloroethane ug/L 20 20.1 100 60-140 1,1-Dichloroethane ug/L 20 17.9 90 60-140 1,1-Dichloroethene ug/L 20 18.2 91 60-140 1,1-Dichloropropene ug/L 20 19.2 96 60-140 1,2,3-Trichlorobenzene ug/L 20 21.3 107 60-140 1,2,3-Trichloropropane ug/L 20 18.1 91 60-140 1,2,4-Trichlorobenzene ug/L 20 20.6 103 60-140 1,2,4-Trimethylbenzene ug/L 20 18.6 93 60-140 -.P. Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/11 /2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 64 (-"*ga ce Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4069435 MS Parameter Bromomethane Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropene Dibromochloromethane Dibromomethane Dichlorodifluoromethane Diisopropyl ether Ethanol Ethyl-tert-butyl ether Ethylbenzene Hexachloro-1,3-butadiene Isopropylbenzene (Cumene) m&p-Xylene Methyl-tert-butyl ether Methylene Chloride n-Butylbenzene n-Propylbenzene Naphthalene o-Xylene sec- Butylbenzene Styrene tert-Amyl Alcohol tert-Amylmethyl ether tert-Butyl Alcohol tert-Butyl Formate tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride 1,2-Dichloroethene-d4 (S) 4-13romofluorobenzene (S) Toluene-d8 (S) Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L 92675427006 Spike Result Conc. MSD Spike Conc. ND 20 20 ND 20 20 ND 20 20 ND 20 20 ND 20 20 ND 20 20 ND 20 20 ND 20 20 ND 20 20 ND 20 20 ND 20 20 ND 20 20 ND 800 800 ND 40 40 ND 20 20 ND 20 20 ND 20 20 4069436 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 10.7 12.4 54 62 60-140 15 30 M1 22.8 22.2 114 111 60-140 3 30 22.5 22.7 113 114 60-140 1 30 20.2 19.4 101 97 60-140 4 30 20.7 19.9 103 100 60-140 4 30 23.6 22.9 118 115 60-140 3 30 21.8 21.1 109 105 60-140 4 30 21.3 20.9 106 104 60-140 2 30 21.4 21.0 107 105 60-140 2 30 22.9 22.3 115 111 60-140 3 30 28.6 27.6 143 138 60-140 4 30 M1 20.2 19.9 101 100 60-140 1 30 784 730 98 91 60-140 7 30 41.1 39.8 103 100 60-140 3 30 22.0 21.8 110 109 60-140 1 30 25.1 25.0 126 125 60-140 1 30 23.6 23.8 118 119 60-140 1 30 ug/L ND 40 40 44.5 43.9 111 110 60-140 ug/L ND 20 20 20.3 19.8 101 99 60-140 ug/L ND 20 20 19.9 19.2 99 96 60-140 ug/L ND 20 20 21.5 21.8 107 109 60-140 ug/L ND 20 20 21.6 21.7 108 108 60-140 ug/L ND 20 20 21.1 21.9 106 109 60-140 ug/L ND 20 20 22.6 22.3 113 112 60-140 ug/L ND 20 20 22.2 22.4 111 112 60-140 ug/L ND 20 20 22.3 22.4 112 112 60-140 ug/L ND 400 400 423 415 106 104 60-140 ug/L ND 40 40 43.3 42.5 10B 106 60-140 ug/L ND 200 200 248 243 124 122 60-140 ug/L ND 160 160 6.BJ 8.4J 4 5 60-140 ug/L ND 20 20 18.3 18.4 91 92 60-140 ug/L ND 20 20 23.6 24.0 118 120 60-140 ug/L ND 20 20 20.8 20.2 104 101 60-140 ug/L ND 20 20 23.0 22.5 115 113 60-140 ug/L ND 20 20 20.6 20.1 103 100 60-140 ug/L ND 20 20 24.0 23.5 120 118 60-140 ug/L ND 20 20 20.6 20.0 103 100 60-140 ug/L ND 20 20 20.2 19.7 101 98 60-140 % 85 85 70-130 % 96 96 70-130 % 95 95 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS 1 30 2 30 4 30 1 30 0 30 4 30 1 30 1 30 0 30 2 30 2 30 2 30 30 M1 1 30 2 30 3 30 2 30 2 30 2 30 3 30 3 30 This report shall not be reproduced, except in full. Date: 07/11 /2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 64 _I& Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 LABORATORY CONTROL SAMPLE: 4069434 Spike 1-CS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers tert-Butylbenzene ug/L 20 15.4 77 60-140 Tetrachloroethene ug/L 20 21.2 106 60-140 Toluene ug/L 20 17.9 89 60-140 trans-1,2-Dichloroethene ug/L 20 18.6 93 60-140 trans- 1,3-Dichloropropene ug/L 20 18.6 93 60-140 Trichloroethene ug/L 20 21.0 105 60-140 Trichlorofluoromethane ug/L 20 17.4 87 60-140 Vinyl chloride ug/L 20 16.5 82 60-140 1,2-Dichloroethane-d4 (S) % 85 70-130 4-Bromofluorobenzene (S) % 95 70-130 Toluene-d8 (S) °% 95 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4069435 4069436 MS MSD 92675427006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 22.7 22.8 113 114 60-140 0 30 1,1,1-Trichloroethane ug/L ND 20 20 21.6 20.9 108 105 60-140 3 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 21.5 21.2 107 106 60-140 1 30 1,1,2-Trichloroethane ug/L ND 20 20 22.4 21.8 112 109 60-140 2 30 1,1-Dichloroethane ug/L ND 20 20 22.1 21.5 111 108 60-140 3 30 1,1-Dichloroethene ug/L ND 20 20 23.0 22.3 115 112 60-140 3 30 1,1-Dichloropropene ug/L ND 20 20 23.5 23.0 117 115 60-140 2 30 1,2,3-Trichlorobenzene ug/L ND 20 20 24.1 24.3 121 122 60-140 1 30 1,2,3-Trichloropropane ug/L ND 20 20 20.9 20.4 105 102 60-140 3 30 1,2,4-Trichlorobenzene ug/L ND 20 20 23.4 23.6 117 118 60-140 1 30 1,2,4-Trimethylbenzene ug/L ND 20 20 22.1 22.0 110 110 60-140 0 30 1,2-Dibromo-3- ug/L ND 20 20 19.8 20.4 99 102 60-140 3 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 22.0 21.7 110 109 60-140 1 30 1,2-Dichlorobenzene ug/L ND 20 20 23.2 23.4 116 117 60-140 1 30 1,2-Dichloroethane ug/L ND 20 20 19.9 19.4 99 97 60-140 2 30 1,2-Dichloropropane ug/L ND 20 20 23.6 22.8 118 114 60-140 3 30 1,3,5-Trimethylbenzene ug/L ND 20 20 22.9 23.1 114 115 60-140 1 30 1,3-Dichlorobenzene ug/L ND 20 20 22.9 22.7 115 114 60-140 1 30 1,3-Dichloropropane ug/L ND 20 20 22.4 21.6 112 108 60-140 4 30 1,4-Dichlorobenzene ug/L ND 20 20 22.7 22.6 114 113 60-140 1 30 2,2-Dichloropropane ug/L ND 20 20 20.0 19.7 100 99 60-140 1 30 2-Chlorotoluene ug/L ND 20 20 22.3 22.6 112 113 60-140 1 30 4-Chlorotoluene ug/L ND 20 20 21.5 22.0 108 110 60-140 2 30 Benzene ug/L ND 20 20 22.7 22.0 114 110 60-140 3 30 Bromobenzene ug/L ND 20 20 22.4 22.4 112 112 60-140 0 30 Bromochloromethane ug/L ND 20 20 21.2 20.7 106 104 60-140 3 30 Bromodichloromethane ug/L ND 20 20 20.3 19.8 101 99 60-140 2 30 Bromoform ug/L ND 20 20 21.7 21.7 108 108 60-140 0 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 64 (-) '9'a ce Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 METHOD BLANK: 4070955 Associated Lab Samples: 92675483004 Parameter Units Ethanol ug/L Ethyl-tert-butyl ether ug/L Ethylbenzene ug/L Hexachloro-1,3-butadiene ug/L Isopropylbenzene (Cumene) ug/L m&p-Xylene ug/L Methyl-tert-butyl ether ug/L Methylene Chloride ug/L n-Butylbenzene ug/L n-Propylbenzene ug/L Naphthalene ug/L o-Xylene ug/L sec-Butylbenzene ug/L Styrene ug/L tert-Amyl Alcohol ug/L tert-Amylmethyl ether ug/L tert-Butyl Alcohol ug/L tert-Butyl Formate ug/L tert-Butylbenzene ug/L Tetrachloroethene ug/L Toluene ug/L trans-1,2-Dichloroethene ug/L trans-1,3-Dichloropropene ug/L Trichloroethene ug/L Trichlorofluoromethane ug/L Vinyl chloride ug/L 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene -dB (S) % QUALITY CONTROL DATA Matrix: Water Blank Result Reporting Limit MDL Analyzed ND 200 5.0 07/06/2314:19 ND 10.0 0.11 07/06/2314:19 ND 0.50 0.081 07/06/2314:19 ND 2.0 0.35 07/06/2314:19 ND 0.50 0.11 07/06/2314:19 ND 1.0 0.094 07/06/2314:19 ND 0.50 0.053 07/06/2314:19 ND 2.0 1.9 07/06/2314:19 ND 0.50 0.066 07/06/2314:19 ND 0.50 0.10 07/06/2314:19 ND 2.0 0.10 07/06/2314:19 ND 0.50 0.14 07/06/2314:19 ND 0.50 0.085 07/06/2314:19 ND 0.50 0.14 07/06/2314:19 ND 100 7.4 07/06/2314:19 ND 10.0 0.12 07/06/2314:19 ND 50.0 4.1 07/06/2314:19 ND 50.0 0.30 07/06/2314:19 ND 0.50 0.086 07/06/2314:19 ND 0.50 0.086 07/06/2314:19 ND 0.50 0.090 07/06/2314:19 ND 0.50 0.10 07/06/2314:19 ND 0.50 0.13 07/06/2314:19 ND 0.50 0.17 07/06/2314:19 ND 1.0 0.14 07/06/2314:19 ND 1.0 0.15 07/06/2314:19 104 70-130 07/06/2314:19 99 70-130 07/06/2314:19 98 70-130 07/06/2314:19 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers LABORATORY CONTROL SAMPLE: 4070956 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 20 24.5 122 60-140 1,1,1-Trichloroethane ug/L 20 23.0 115 60-140 1,1,2,2-Tetrachloroethane ug/L 20 24.1 120 60-140 1,1,2-Trichloroethane ug/L 20 24.3 121 60-140 1,1-Dichloroethane ug/L 20 23.5 118 60-140 1,1-Dichloroethene ug/L 20 23.6 118 60-140 1,1-Dichloropropene ug/L 20 25.1 125 60-140 1,2,3-Trichlorobe nzene ug/L 20 25.2 126 60-140 1,2,3-Trichloropropane ug/L 20 22.6 113 60-140 1,2,4-Trichlorobenzene ug/L 20 23.5 117 60-140 1,2,4-Trimethylbenzene ug/L 20 24.8 124 60-140 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 64 (-�Face- QUALITY CONTROL DATA Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 QC Batch: 785108 Analysis Method: SM 6200B QC Batch Method: SM 6200B Analysis Description: 6200B MSV Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92675483004 METHOD BLANK: 4070955 Associated Lab Samples: 92675483004 Parameter Units Matrix: Water Blank Reporting Result Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 0.50 0.091 07/06/23 14:19 1,1,1-Trichloroethane ug/L ND 0.50 0.11 07/06/23 14:19 1,1,2,2-Tetrachloroethane ug/L ND 0.50 0.074 07/06/23 14:19 1,1,2-Trichloroethane ug/L ND 0.50 0.096 07/06/23 14:19 1,1-Dichloroethane ug/L ND 0.50 0.056 07/06/23 14:19 1,1-Dichloroethene ug/L ND 0.50 0.079 07/06/23 14:19 1,1-Dichloropropene ug/L ND 0.50 0.066 07/06/23 14:19 1,2,3-Trichlorobenzene ug/L ND 2.0 0.12 07/06/23 14:19 1,2,3-Trichloropropane ug/L ND 0.50 0.17 07/06/23 14:19 1,2,4-Trichlorobenzene ug/L ND 2.0 0.16 07/06/23 14:19 1,2,4-Trimethyl benzene ug/L ND 0.50 0.031 07/06/23 14:19 1,2-Dibromo-3-chloropropane ug/L ND 1.0 0.18 07/06/23 14:19 1,2-Dibromoethane (EDB) ug/L ND 0.50 0.15 07/06/23 14:19 1,2-Dichlorobenzene ug/L ND 0.50 0.094 07/06/23 14:19 1,2-Dichloroethane ug/L ND 0.50 0.11 07/06/23 14:19 1,2-Dichloropropane ug/L ND 0.50 0.14 07/06/23 14:19 1,3,5-Trimethylbenzene ug/L ND 0.50 0.071 07/06/23 14:19 1,3-Dichlorobenzene ug/L ND 0.50 0.098 07/06/23 14:19 1,3-Dichloropropane ug/L ND 0.50 0.085 07/06/23 14:19 1,4-Dichlorobenzene ug/L ND 0.50 0.090 07/06/23 14:19 2,2-Dichloropropane ug/L ND 0.50 0.12 07/06/23 14:19 2-Chlorotoluene ug/L ND 0.50 0.13 07/06/23 14:19 4-Chlorotoluene ug/L ND 0.50 0.096 07/06/23 14:19 Benzene ug/L ND 0.50 0.079 07/06/23 14:19 Bromobenzene ug/L ND 0.50 0.14 07/06/23 14:19 Bromochloromethane ug/L ND 0.50 0.094 07/06/23 14:19 Bromodichloromethane ug/L ND 0.50 0.17 07/06/23 14:19 Bromoform ug/L ND 0.50 0.20 07/06/23 14:19 Bromomethane ug/L ND 5.0 0.22 07/06/23 14:19 Carbon tetrachloride ug/L ND 0.50 0.17 07/06/23 14:19 Chlorobenzene ug/L ND 0.50 0.085 07/06/23 14:19 Chloroethane ug/L ND 1.0 0.17 07/06/23 14:19 Chloroform ug/L ND 0.50 0.069 07/06/23 14:19 Chloromethane ug/L ND 1.0 0.18 07/06/23 14:19 cis-1,2-Dichloroethene ug/L ND 0.50 0.11 07/06/23 14:19 cis-1,3-Dichloropropene ug/L ND 0.50 0.090 07/06/23 14:19 Dibromochloromethane ug/L ND 0.50 0.15 07/06/23 14:19 Dibromomethane ug/L ND 0.50 0.19 07/06/23 14:19 Dichlorodifluoromethane ug/L ND 0.50 0.12 07/06/23 14:19 Diisopropyl ether ug/L ND 0.50 0.072 07/06/23 14:19 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 64 'F ace QUALITY CONTROL DATA Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 4070956 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers tert-Butylbenzene ug/L 20 19.3 96 60-140 Tetrachloroethene ug/L 20 22.9 115 60-140 Toluene ug/L 20 22.5 112 60-140 trans-1,2-Dichloroethene ug/L 20 24.1 120 60-140 trans- 1,3-Dichloroprope ne ug/L 20 24.7 124 60-140 Trichloroethene ug/L 20 23.6 118 60-140 Trichlorofluoromethane ug/L 20 20.7 104 60-140 Vinyl chloride ug/L 20 20.4 102 60-140 1,2-Dichloroethane-d4 (S) % 100 70-130 4-Bromofluorobenzene (S) % 100 70-130 Toluene-d8 (S) % 99 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4070957 MS 92675483004 Spike Parameter Units Result Conc. MSD Spike Conc. 4070958 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 19.6 24.7 98 123 60-140 23 30 1,1,1-Trichloroethane ug/L ND 20 20 18.3 23.8 92 119 60-140 26 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 17.8 23.1 89 115 60-140 26 30 1,1,2-Trichloroethane ug/L ND 20 20 17.6 22.2 88 111 60-140 23 30 1,1-Dichloroethane ug/L ND 20 20 19.8 25.3 99 127 60-140 24 30 1,1-Dichloroethene ug/L ND 20 20 22.8 28.7 114 144 60-140 23 30 M1 1,1-Dichloropropene ug/L ND 20 20 19.9 25.6 100 128 60-140 25 30 1,2,3-Trichlorobenzene ug/L ND 20 20 21.1 24.7 106 124 60-140 16 30 1,2,3-Trichloropropane ug/L ND 20 20 18.8 22.2 94 111 60-140 16 30 1,2,4-Trichlorobenzene ug/L ND 20 20 21.6 25.0 108 125 60-140 15 30 1,2,4-Trimethyl benzene ug/L ND 20 20 21.7 24.5 109 122 60-140 12 30 1,2-Dibromo-3- ug/L ND 20 20 16.9 21.4 85 107 60-140 23 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 19.5 24.6 97 123 60-140 23 30 1,2-Dichlorobenzene ug/L ND 20 20 21.5 24.8 108 124 60-140 14 30 1,2-Dichloroethane ug/L ND 20 20 19.7 25.6 99 128 60-140 26 30 1,2-Dichloropropane ug/L ND 20 20 21.0 26.5 105 132 60-140 23 30 1,3,5-Trimethylbenzene ug/L ND 20 20 21.8 24.6 109 123 60-140 12 30 1,3-Dichlorobenzene ug/L ND 20 20 21.9 25.3 109 127 60-140 15 30 1,3-Dichloropropane ug/L ND 20 20 19.6 24.8 98 124 60-140 24 30 1,4-Dichlorobenzene ug/L ND 20 20 22.2 25.0 111 125 60-140 12 30 2,2-Dichloropropane ug/L ND 20 20 20.7 27.0 104 135 60-140 26 30 2-Chlorotoluene ug/L ND 20 20 20.7 24.2 104 121 60-140 15 30 4-Chlorotoluene ug/L ND 20 20 20.9 24.3 105 121 60-140 15 30 Benzene ug/L ND 20 20 21.6 27.0 108 135 60-140 22 30 Bromobenzene ug/L ND 20 20 19.9 23.3 99 117 60-140 16 30 Bromochloromethane ug/L ND 20 20 19.3 24.3 97 122 60-140 23 30 Bromodichloromethane ug/L ND 20 20 20.4 25.8 102 129 60-140 23 30 Bromoform ug/L ND 20 20 16.6 21.1 83 106 60-140 24 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 64 �ce QUALITY CONTROL DATA Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 LABORATORY CONTROL SAMPLE: Parameter 4070956 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,2-Dibromo-3-chloropropane ug/L 20 22.3 111 60-140 1,2-Dibromoethane (EDB) ug/L 20 24.5 122 60-140 1,2-Dichlorobenzene ug/L 20 24.4 122 60-140 1,2-Dichloroethane ug/L 20 24.3 121 60-140 1,2-Dichloropropane ug/L 20 23.9 119 60-140 1,3,5-Trimethylbenzene ug/L 20 24.5 123 60-140 1,3-Dichlorobenzene ug/L 20 24.0 120 60-140 1,3-Dichloropropane ug/L 20 23.8 119 60-140 1,4-Dichlorobenzene ug/L 20 23.1 115 60-140 2,2-Dichloropropane ug/L 20 23.2 116 60-140 2-Chlorotoluene ug/L 20 23.2 116 60-140 4-Chlorotoluene ug/L 20 23.7 118 60-140 Benzene ug/L 20 23.0 115 60-140 Bromobenzene ug/L 20 22.9 115 60-140 Bromochloromethane ug/L 20 23.8 119 60-140 Bromodichloromethane ug/L 20 22.5 113 60-140 Bromoform ug/L 20 21.1 105 60-140 Bromomethane ug/L 20 21.7 109 60-140 Carbon tetrachloride ug/L 20 22.8 114 60-140 Chlorobenzene ug/L 20 23.3 116 60-140 Chloroethane ug/L 20 23.1 116 60-140 Chloroform ug/L 20 23.1 115 60-140 Chloromethane ug/L 20 23.2 116 60-140 cis-1,2-Dichloroethene ug/L 20 23.8 119 60-140 cis-1,3-Dichloropropene ug/L 20 23.8 119 60-140 Dibromochloromethane ug/L 20 23.2 116 60-140 Dibromomethane ug/L 20 22.6 113 60-140 Dichlorodifluoromethane ug/L 20 23.4 117 60-140 Diisopropyl ether ug/L 20 24.0 120 60-140 Ethanol ug/L 800 947 118 60-140 Ethyl-tert-butyl ether ug/L 40 46.4 116 60-140 Ethylbenzene ug/L 20 23.1 116 60-140 Hexachloro-1,3-butadiene ug/L 20 25.4 127 60-140 Isopropylbenzene (Cumene) ug/L 20 24.3 121 60-140 m&p-Xylene ug/L 40 46.9 117 60-140 Methyl-tert-butyl ether ug/L 20 23.4 117 60-140 Methylene Chloride ug/L 20 21.2 106 60-140 n-Butylbenzene ug/L 20 24.6 123 60-140 n-Propylbenzene ug/L 20 22.9 114 60-140 Naphthalene ug/L 20 27.2 136 60-140 o-Xylene ug/L 20 23.7 118 60-140 sec- Butyl benzene ug/L 20 23.7 119 60-140 Styrene ug/L 20 25.5 128 60-140 tert-Amyl Alcohol ug/L 400 437 109 60-140 tert-Amylmethyl ether ug/L 40 47.4 119 60-140 tert-Butyl Alcohol ug/L 200 227 114 60-140 tert-Butyl Formate ug/L 160 193 121 60-140 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/11 /2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 49 of 64 QUALITY CONTROL DATA Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QC Batch: 785157 Analysis Method: SM 6200B QC Batch Method: SM 6200B Analysis Description: 6200E MSV Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92675483001, 92675483002, 92675483003, 92675483005, 92675483006, 92675483007, 92675483008, 92675483009, 92675483010, 926754B3011, 92675483012, 92675483013, 92675483014, 92675483015, 92675483016 METHOD BLANK: 4071281 Matrix: Water Associated Lab Samples: 92675483001, 92675483002, 92675483003, 92675483005, 92675483006, 92675483007, 92675483008, 92675483009, 92675483010, 92675483011, 92675483012, 92675483013, 92675483014, 92675483015, 92675483016 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 0.50 0.091 07/06/23 14:49 1,1,1-Trichloroethane ug/L ND 0.50 0.11 07/06/23 14:49 1,1,2,2-Tetrachloroethane ug/L ND 0.50 0.074 07/06/23 14:49 1,1,2-Trichloroethane ug/L ND 0.50 0.096 07/06/23 14:49 1,1-Dichloroethane ug/L ND 0.50 0.056 07/06/23 14:49 1,1-Dichloroethene ug/L ND 0.50 0.079 07/06/23 14:49 1,1-Dichloropropene ug/L ND 0.50 0.066 07/06/23 14:49 1,2,3-Trichlorobe nzene ug/L ND 2.0 0.12 07/06/23 14:49 1,2,3-Trichloropropane ug/L ND 0.50 0.17 07/06/23 14:49 1,2,4-Trichlorobenzene ug/L ND 2.0 0.16 07/06/23 14:49 1,2,4-Trimethylbenzene ug/L ND 0.50 0.031 07/06/23 14:49 1,2-Dibromo-3-chloropropane ug/L ND 1.0 0.18 07/06/23 14:49 1,2-Dibromoethane (EDB) ug/L ND 0.50 0.15 07/06/23 14:49 1,2-Dichlorobenzene ug/L ND 0.50 0.094 07/06/23 14:49 1,2-Dichloroethane ug/L ND 0.50 0.11 07/06/23 14:49 1,2-Dichloropropane ug/L ND 0.50 0.14 07/06/23 14:49 1,3,5-Trimethylbenzene ug/L ND 0.50 0.071 07/06/23 14:49 1,3-Dichlorobenzene ug/L ND 0.50 0.098 07/06/23 14:49 1,3-Dichloropropane ug/L ND 0.50 0.085 07/06/23 14:49 1,4-Dichlorobenzene ug/L ND 0.50 0.090 07/06/23 14:49 2,2-Dichloropropane ug/L ND 0.50 0.12 07/06/23 14:49 2-Chlorotoluene ug/L ND 0.50 0.13 07/06/23 14:49 4-Chlorotoluene ug/L ND 0.50 0.096 07/06/23 14:49 Benzene ug/L ND 0.50 0.079 07/06/23 14:49 Bromobenzene ug/L ND 0.50 0.14 07/06/23 14:49 Bromochloromethane ug/L ND 0.50 0.094 07/06/23 14:49 Bromodichloromethane ug/L ND 0.50 0.17 07/06/23 14:49 Bromoform ug/L ND 0.50 0.20 07/06/23 14:49 Bromomethane ug/L ND 5.0 0.22 07/06/23 14:49 Carbon tetrachloride ug/L ND 0.50 0.17 07/06/23 14:49 Chlorobenzene ug/L ND 0.50 0.085 07/06/23 14:49 Chloroethane ug/L ND 1.0 0.17 07/06/23 14:49 Chloroform ug/L ND 0.50 0.069 07/06/23 14:49 Chloromethane ug/L ND 1.0 0.18 07/06/23 14:49 cis-1,2-Dichloroethene ug/L ND 0.50 0.11 07/06/23 14:49 cis-1,3-Dichloropropene ug/L ND 0.50 0.090 07/06/23 14:49 Dibromochloromethane ug/L ND 0.50 0.15 07/06/23 14:49 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 64 ace QUALITY CONTROL DATA Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4070957 MS 92675483004 Spike Parameter Units Result Conc. MSD Spike Conc. 4070958 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual Bromomethane ug/L ND 20 20 10.7 17.8 54 89 60-140 50 30 M1,R1 Carbon tetrachloride ug/L ND 20 20 22.1 27.7 111 138 60-140 22 30 Chlorobenzene ug/L ND 20 20 21.4 27.3 107 136 60-140 24 30 Chloroethane ug/L ND 20 20 22.5 29.1 113 146 60-140 26 30 M1 Chloroform ug/L 0.23J 20 20 15.9 21.2 78 105 60-140 29 30 Chloromethane ug/L ND 20 20 21.0 27.8 105 139 60-140 28 30 cis-1,2-Dichloroethene ug/L ND 20 20 19.1 24.8 95 124 60-140 26 30 cis-1,3-Dichloropropene ug/L ND 20 20 20.1 25.1 100 126 60-140 22 30 Dibromochloromethane ug/L ND 20 20 18.5 23.6 93 118 60-140 24 30 Dibromomethane ug/L ND 20 20 19.3 24.1 96 121 60-140 22 30 Dichlorodifluoromethane ug/L ND 20 20 29.5 37.6 148 188 60-140 24 30 M1 Diisopropyl ether ug/L 3.4 20 20 20.6 26.4 86 115 60-140 25 30 Ethanol ug/L ND 800 800 723 951 90 119 60-140 27 30 Ethyl-tert-butyl ether ug/L ND 40 40 35.6 45.7 89 114 60-140 25 30 Ethylbenzene ug/L ND 20 20 19.9 24.8 99 124 60-140 22 30 Hexachloro-1,3-butadiene ug/L ND 20 20 23.7 26.2 118 131 60-140 10 30 Isopropylbenzene ug/L ND 20 20 20.9 25.7 105 128 60-140 20 30 (Cumene) m&p-Xylene ug/L ND 40 40 39.5 48.9 99 122 60-140 21 30 Methyl-tert-butyl ether ug/L 18.7 20 20 31.4 41.7 63 115 60-140 28 30 Methylene Chloride ug/L ND 20 20 19.8 25.6 99 128 60-140 25 30 n-Butylbenzene ug/L ND 20 20 23.2 25.9 116 130 60-140 11 30 n-Propylbenzene ug/L ND 20 20 21.7 25.0 109 125 60-140 14 30 Naphthalene ug/L ND 20 20 19.6 24.4 98 122 60-140 22 30 o-Xylene ug/L ND 20 20 19.5 24.3 97 121 60-140 22 30 sec-Butylbenzene ug/L ND 20 20 22.3 25.1 111 126 60-140 12 30 Styrene ug/L ND 20 20 18.9 23.6 94 118 60-140 22 30 tert-Amyl Alcohol ug/L ND 400 400 361 475 90 119 60-140 27 30 tert-Amylmethyl ether ug/L ND 40 40 38.6 48.9 96 122 60-140 24 30 tert-Butyl Alcohol ug/L ND 200 200 161 238 81 119 60-140 38 30 R1 tert-Butyl Formate ug/L ND 160 160 138 168 86 105 60-140 20 30 tert-Butylbenzene ug/L ND 20 20 18.0 20.3 90 102 60-140 12 30 Tetrachloroethene ug/L ND 20 20 21.6 26.6 108 133 60-140 21 30 Toluene ug/L ND 20 20 19.2 23.8 96 119 60-140 22 30 trans-1,2-Dichloroethene ug/L ND 20 20 20.9 27.2 104 136 60-140 26 30 trans-1,3-Dichloropropene ug/L ND 20 20 19.5 24.7 97 124 60-140 24 30 Trichloroethene ug/L ND 20 20 22.1 27.5 111 137 60-140 22 30 Trichlorofluoromethane ug/L ND 20 20 21.5 28.4 107 142 60-140 28 30 M1 Vinyl chloride ug/L ND 20 20 18.7 23.9 93 119 60-140 24 30 1,2-Dichloroethane-d4 (S) % 95 97 70-130 4-Bromofluorobenzene (S) % 98 101 70-130 Toluene-d8 (S) % 101 98 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full, Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 64 Pace Analytical Services, LLC ace ^ 9800 Kincey Ave. Suite 100 i/ / -/..� Huntersville, NC 28078 (�( (� V (704)875-9092 QUALITY CONTROL DATA Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 LABORATORY CONTROL SAMPLE: 4071282 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1-Dichloropropene ug/L 20 21.8 109 60-140 1,2,3-Trichlorobenzene ug/L 20 22.4 112 60-140 1,2,3-Trichloropropane ug/L 20 22.4 112 60-140 1,2,4-Trichlorobenzene ug/L 20 22.4 112 60-140 1,2,4-Trimethylbenzene ug/L 20 21.8 109 60-140 1,2-Dibromo-3-chloropropane ug/L 20 20.0 100 60-140 1,2-Dibromoethane (EDB) ug/L 20 23.1 115 60-140 1,2-Dichlorobenzene ug/L 20 22.7 114 60-140 1,2-Dichloroethane ug/L 20 22.5 112 60-140 1,2-Dichloropropane ug/L 20 23.1 115 60-140 1,3,5-Trimethylbenzene ug/L 20 21.9 109 60-140 1,3-Dichlorobenzene ug/L 20 22.7 113 60-140 1,3-Dichloropropane ug/L 20 22.4 112 60-140 1,4-Dichlorobenzene ug/L 20 22.8 114 60-140 2,2-Dichloropropane ug/L 20 22.2 111 60-140 2-Chlorotoluene ug/L 20 21.7 108 60-140 4-Chlorotoluene ug/L 20 21.5 108 60-140 Benzene ug/L 20 23.8 119 60-140 Bromobenzene ug/L 20 21.6 108 60-140 Bromochloromethane ug/L 20 21.8 109 60-140 Bromodichloromethane ug/L 20 22.9 115 60-140 Bromoform ug/L 20 19.7 99 60-140 Bromomethane ug/L 20 19.1 95 60-140 Carbon tetrachloride ug/L 20 24.3 122 60-140 Chlorobenzene ug/L 20 22.3 112 60-140 Chloroethane ug/L 20 24.4 122 60-140 Chloroform ug/L 20 19.1 95 60-140 Chloromethane ug/L 20 25.0 125 60-140 cis-1,2-Dichloroethene ug/L 20 21.4 107 60-140 cis-1,3-Dichloropropene ug/L 20 22.7 113 60-140 Dibromochloromethane ug/L 20 21.3 106 60-140 Dibromomethane ug/L 20 21.6 108 60-140 Dichlorodifluoromethane ug/L 20 31.0 155 60-140 L1 Diisopropyl ether ug/L 20 20.5 103 60-140 Ethanol ug/L 800 816 102 60-140 Ethyl-tert-butyl ether ug/L 40 41.1 103 60-140 Ethylbenzene ug/L 20 21.8 109 60-140 Hexachloro-1,3-butadiene ug/L 20 23.3 116 60-140 Isopropylbenzene (Cumene) ug/L 20 22.3 111 60-140 m&p-Xylene ug/L 40 43.5 109 60-140 Methyl-tert-butyl ether ug/L 20 20.4 102 60-140 Methylene Chloride ug/L 20 23.3 116 60-140 n-Butylbenzene ug/L 20 22.4 112 60-140 n-Propylbenzene ug/L 20 21.6 108 60-140 Naphthalene ug/L 20 22.7 113 60-140 o-Xylene ug/L 20 21.7 108 60-140 sec- Butyl benzene ug/L 20 22.0 110 60-140 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 54 of 64 (-"09ace QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 METHOD BLANK: 4071281 Matrix: Water Associated Lab Samples: 92675483001, 92675483002, 92675483003, 92675483005, 92675483006, 92675483007, 92675483008, 92675483009, 92675483010, 92675483011, 92675483012, 92675483013, 92675483014, 92675483015, 92675483016 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Dibromomethane ug/L ND 0.50 0.19 07/06/23 14:49 Dichlorodifluoromethane ug/L ND 0.50 0.12 07/06/23 14:49 Diisopropyl ether ug/L ND 0.50 0.072 07/06/23 14:49 Ethanol ug/L ND 200 5.0 07/06/23 14:49 Ethyl-tert-butyl ether ug/L ND 10.0 0.11 07/06/23 14:49 Ethylbenzene ug/L ND 0.50 0.081 07/06/23 14:49 Hexachloro-1,3-butadiene ug/L ND 2.0 0.35 07/06/23 14:49 Isopropylbenzene (Cumene) ug/L ND 0.50 0.11 07/06/23 14:49 m&p-Xylene ug/L ND 1.0 0.094 07/06/23 14:49 Methyl-tert-butyl ether ug/L ND 0.50 0.053 07/06/23 14:49 Methylene Chloride ug/L ND 2.0 1.9 07/06/23 14:49 n-Butylbenzene ug/L ND 0.50 0.066 07/06/23 14:49 n-Propylbenzene ug/L ND 0.50 0.10 07/06/23 14:49 Naphthalene ug/L ND 2.0 0.10 07/06/23 14:49 o-Xylene ug/L ND 0.50 0.14 07/06/23 14:49 sec- Butyl benzene ug/L ND 0.50 0.085 07/06/23 14:49 Styrene ug/L ND 0.50 0.14 07/06/23 14:49 tert-Amyl Alcohol ug/L ND 100 7.4 07/06/23 14:49 tert-Amylmethyl ether ug/L ND 10.0 0.12 07/06/23 14:49 tert-Butyl Alcohol ug/L ND 50.0 4.1 07/06/23 14:49 tert-Butyl Formate ug/L ND 50.0 0.30 07/06/23 14:49 tert-Butylbenzene ug/L ND 0.50 0.086 07/06/23 14:49 Tetrachloroethene ug/L ND 0.50 0.086 07/06/23 14:49 Toluene ug/L ND 0.50 0.090 07/06/23 14:49 trans- 1, 2-Dichloroethene ug/L ND 0.50 0.10 07/06/23 14:49 trans-1,3-Dichloropropene ug/L ND 0.50 0.13 07/06/23 14:49 Trichloroethene ug/L ND 0.50 0.17 07/06/23 14:49 Trichlorofluoromethane ug/L ND 1.0 0.14 07/06/23 14:49 Vinyl chloride ug/L ND 1.0 0.15 07/06/23 14:49 1,2-Dichloroethane-d4 (S) % 92 70-130 07/06/23 14:49 4-Bromofluorobenzene (S) % 97 70-130 07/06/23 14:49 Toluene-d8 (S) % 103 70-130 07/06/23 14:49 LABORATORY CONTROL SAMPLE: 4071282 Spike LCS 1-CS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 20 22.6 113 60-140 1,1,1-Trichloroethane ug/L 20 20.2 101 60-140 1,1,2,2-Tetrachloroethane ug/L 20 21.3 107 60-140 1,1,2-Trichloroethane ug/L 20 20.7 103 60-140 1,1-Dichloroethane ug/L 20 22.0 110 60-140 1,1-Dichloroethene ug/L 20 24.7 124 60-140 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 07/11 /2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 53 of 64 (-"'Face- Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 LABORATORY CONTROL SAMPLE: 4071282 Parameter Styrene tert-Amyl Alcohol tert-Amylmethyl ether tert-Butyl Alcohol tert-Butyl Formate tert-Butylbenzene Tetrachloroethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene Trichlorofluoromethane Vinyl chloride 1,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) QUALITY CONTROL DATA Units Spike Conc. LCS Result LCS % Rec % Rec Limits ug/L 20 22.1 110 60-140 ug/L 400 419 105 60-140 ug/L 40 44.8 112 60-140 ug/L 200 192 96 60-140 ug/L 160 168 105 60-140 ug/L 20 17.9 89 60-140 ug/L 20 23.1 116 60-140 ug/L 20 21.3 107 60-140 ug/L 20 22.8 114 60-140 ug/L 20 22.0 110 60-140 ug/L 20 24.1 120 60-140 ug/L 20 23.1 116 60-140 ug/L 20 20.5 103 60-140 % 93 70-130 % 99 70-130 % 98 70-130 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4071283 4071284 MS MSD 92675822002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 19.0 22.3 95 112 60-140 16 30 1,1,1-Trichloroethane ug/L ND 20 20 18.1 21.3 91 107 60-140 16 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 17.9 20.8 90 104 60-140 15 30 1,1,2-Trichloroethane ug/L ND 20 20 16.4 19.5 82 98 60-140 17 30 1,1-Dichloroethane ug/L ND 20 20 19.6 23.5 98 118 60-140 18 30 1,1-Dichloroethene ug/L ND 20 20 21.6 26.3 108 131 60-140 19 30 1,1-Dichloropropene ug/L ND 20 20 18.4 22.8 92 114 60-140 21 30 1,2,3-Trichlorobenzene ug/L ND 20 20 18.9 21.8 94 109 60-140 14 30 1,2,3-Trichloropropane ug/L ND 20 20 18.5 20.3 92 102 60-140 9 30 1,2,4-Trichlorobenzene ug/L ND 20 20 18.7 21.6 93 108 60-140 15 30 1,2,4-Trimethyl benzene ug/L ND 20 20 18.5 21.8 93 109 60-140 16 30 1,2-Dlbromo-3- ug/L ND 20 20 15.9 18.4 80 92 60-140 15 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 18.6 21.7 93 109 60-140 15 30 1,2-Dichlorobenzene ug/L ND 20 20 18.8 22.2 94 111 60-140 17 30 1,2-Dichloroethane ug/L ND 20 20 19.4 23.1 97 116 60-140 18 30 1,2-Dichloropropane ug/L ND 20 20 19.0 22.9 95 115 60-140 18 30 1,3,5-Trimethylbenzene ug/L ND 20 20 18.7 22.0 93 110 60-140 16 30 1,3-Dichlorobenzene ug/L ND 20 20 18.9 22.1 94 110 60-140 16 30 1,3-Dichloropropane ug/L ND 20 20 18.4 22.1 92 110 60-140 18 30 1,4-Dichlorobenzene ug/L ND 20 20 18.5 21.9 93 110 60-140 17 30 2,2-Dichloropropane ug/L ND 20 20 19.6 23.9 98 119 60-140 20 30 2-Chlorotoluene ug/L ND 20 20 18.4 21.5 92 108 60-140 16 30 4-Chlorotoluene ug/L ND 20 20 18.3 21.4 91 107 60-140 16 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 55 of 64 (--"Face QUALITY CONTROL DATA Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4071283 4071284 MS MSD 92675822002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Benzene ug/L ND 20 20 19.2 23.6 96 118 60-140 21 30 Bromobenzene ug/L ND 20 20 18.0 21.1 90 106 60-140 16 30 Bromochloromethane ug/L ND 20 20 19.0 22.6 95 113 60-140 18 30 Bromodichloromethane ug/L ND 20 20 18.7 22.7 93 114 60-140 19 30 Bromoform ug/L ND 20 20 15.6 17.8 78 89 60-140 13 30 Bromomethane ug/L ND 20 20 16.1 19.5 80 98 60-140 19 30 Carbon tetrachloride ug/L ND 20 20 20.3 24.7 102 123 60-140 19 30 Chlorobenzene ug/L ND 20 20 18.9 22.3 94 111 60-140 17 30 Chloroethane ug/L ND 20 20 22.2 27.0 111 135 60-140 19 30 Chloroform ug/L 0.36J 20 20 16.9 19.3 83 95 60-140 13 30 Chloromethane ug/L ND 20 20 19.0 24.2 95 121 60-140 24 30 cis-1,2-Dichloroethene ug/L ND 20 20 18.9 22.4 94 112 60-140 17 30 cis-1,3-Dichloropropene ug/L ND 20 20 18.0 21.6 90 108 60-140 18 30 Dibromochloromethane ug/L ND 20 20 17.2 20.3 86 102 60-140 17 30 Dibromomethane ug/L ND 20 20 18.0 21.5 90 108 60-140 18 30 Dichlorodifluoromethane ug/L ND 20 20 24.1 30.2 121 151 60-140 22 30 M0 Diisopropyl ether ug/L ND 20 20 17.1 21.0 85 105 60-140 21 30 Ethanol ug/L ND 800 800 700 818 87 102 60-140 16 30 Ethyl-tert-butyl ether ug/L ND 40 40 34.0 40.7 85 102 60-140 18 30 Ethylbenzene ug/L ND 20 20 19.1 22.3 95 111 60-140 15 30 Hexachloro-1,3-butadiene ug/L ND 20 20 19.8 23.6 99 118 60-140 17 30 Isopropylbenzene ug/L ND 20 20 19.4 22.7 97 114 60-140 16 30 (Cumene) m&p-Xylene ug/L ND 40 40 37.4 44.4 94 111 60-140 17 30 Methyl-tert-butyl ether ug/L ND 20 20 16.6 20.1 83 101 60-140 20 30 Methylene Chloride ug/L ND 20 20 19.8 23.5 99 117 60-140 17 30 n-Butylbenzene ug/L ND 20 20 19.4 22.8 97 114 60-140 16 30 n-Propylbenzene ug/L ND 20 20 18.5 21.8 93 109 60-140 16 30 Naphthalene ug/L ND 20 20 18.6 21.5 93 107 60-140 14 30 o-Xylene ug/L ND 20 20 18.6 21.9 93 109 60-140 17 30 sec-Butylbenzene ug/L ND 20 20 19.1 22.3 96 111 60-140 15 30 Styrene ug/L ND 20 20 18.0 21.2 90 106 60-140 16 30 tert-Amyl Alcohol ug/L ND 400 400 342 391 86 98 60-140 13 30 tert-Amylmethyl ether ug/L ND 40 40 35.6 42.3 89 106 60-140 17 30 tert-Butyl Alcohol ug/L ND 200 200 216 269 108 135 60-140 22 30 tert-Butyl Formate ug/L ND 160 160 28.6J 22.1J 18 14 60-140 30 M1 tert-Butylbenzene ug/L ND 20 20 15.7 18.4 78 92 60-140 16 30 Tetrachloroethene ug/L ND 20 20 19.7 23.7 98 119 60-140 19 30 Toluene ug/L ND 20 20 18.4 21.8 92 109 60-140 17 30 trans-1,2-Dichloroethene ug/L ND 20 20 20.2 24.4 101 122 60-140 19 30 trans-1,3-Dichloropropene ug/L ND 20 20 17.6 21.3 88 106 60-140 19 30 Trichloroethene ug/L ND 20 20 19.5 24.2 97 121 60-140 22 30 Trichlorofluoromethane ug/L ND 20 20 20.6 25.1 103 126 60-140 20 30 Vinyl chloride ug/L ND 20 20 17.5 21.1 87 106 60-140 19 30 1,2-Dichloroethane-d4 (S) % 104 108 70-130 4-Bromofluorobenzene (S) % 96 95 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/11 /2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 56 of 64 QUALITY CONTROL DATA Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4071283 4071284 MS MSD 92675822002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result °% Rec % Rec Limits RPD RPD Qual Toluene-d8 (S) % 101 102 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/11/2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 57 of 64 (-)Pace QUALIFIERS Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as 'Total' may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS C9 Common Laboratory Contaminant. L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. MO Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R1 RPD value was outside control limits. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/11 /2023 01:23 PM without the written consent of Pace Analytical Services, LLC. Page 58 of 64 �ce QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: SPEEDWAY 7997 MARSHVILLE Pace Project No.: 92675483 Lab ID Sample ID QC Batch Method QC Batch 92675483001 MW-1 SM 6200B 785157 92675483002 MW-1 D SM 6200E 785157 92675483003 MW-2 SM 6200B 785157 92675483004 MW-3 SM 6200B 785108 92675483005 MW-4 SM 6200B 785157 92675483006 MW-5R SM 6200B 785157 92675483007 MW-6 SM 6200E 785157 92675483008 MW-7 SM 6200B 785157 92675483009 MW-8 SM 6200B 785157 92675483010 MW-9 SM 6200B 785157 92675483011 MW-14 SM 6200B 785157 92675483012 MW-19 SM 6200B 785157 92675483013 MW-16 SM 6200B 785157 92675483014 MW-18 SM 6200B 785157 92675483015 MW-10 SM 6200E 785157 92675483016 MW-11R SM 6200B 785157 92675483017 TRIP BLANK SM 6200B 784771 Date: 07/11/2023 01:23 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Analytical Method Analytical Batch Page 59 of 64 DC#_Title: ENV-FRM-HUN1-0083 v02 - Sample Condition Upon Receipt Pace,,,W—UtIA Effective Date: 11/14/2022 Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑ SampleClient Name: • • WO## • 92675483 � � Project tt: Courier: ❑Fed Ex ❑UPS ❑USPS Client II I II' I II III I' I I II I III ❑ Commercial ❑Pace ❑Other: 92679483 Custody Seal Present? ❑Yes No Seals Intact? []Yes ON, Packing Material: []Bubble Wrap Bubble Bags ❑None ❑ Other Thermomete � IR Gun 1D: 1`2 ,y� U Type of ice: 01let ❑Blue Correction Factor: Cooler Temp: `' Add/Subtract (•C) Cooler Temp Corrected (•C): USDA Regulated Soil ( water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check mans)? MYes MNo Date/Initials Person Examining Contents: 0.11VA Biological Tissue ozen? / ❑Yes ❑No N/A []None Temp should be above freezing to VC ❑Samples out of temp criteria. Samples on ice, cooling process has begun Did samples originate from a foreign source (internationally, inriMino Hn—ii and P—rin Rirn17 11V— Mtdn Comments/Discrepancy: Chain of Custody Present? Yes ON. ❑N/A 1. Samples Arrived within Hold Time? es ❑No []N/A 2. Short Hold Time Analysis (<72 hr.)? ❑Yes No []N/A 3. Rush Turn Around Time Requested? ❑Yes ZNo ❑N/A 4. Sufficient Volume? a es [:]No ❑N/A 5. Correct Containers Used? -Pace Containers Used? Y a ❑No ❑No ❑N/A []N/A 6. Containers Intact? Yes ❑No ❑N/ 7. Dissolved analysis: Samples Field Filtered? []Ye ❑No 2 N/A 8. Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: es ❑No []N/A 9. Headspace in VOA Vials (>5-6mm)? [:]YK No ❑N/A 10. Trip Blank Present? Trip Blank Custody Seals Present? Oes ❑Yes CJ No ❑N/A []N/A 11. IPLE DISCREPANCY 1 u.� 1 � N•.C.Gr Lot ID of split containers. CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Date: Date: Field Data Required? ❑Yes "No Qualtrax ID: 69614 Page 1 of 2 Page 60 of 64 C w xx rn t7 0) A T N cn (D N O i CO m 0 A 3 m 0 z 9 A ii O ro ro 3 ' M v 0 0 'm b G ro 2 O 3 n m �^ D a o b O. (A v 3 ro 3 d r c O b C OQ. 1 m n fD N (D 3 r{D „ M t1 a v `c' A LA Iv n 3 N 0 fD i n 3 c b 0, a a � ro CL Z b ro 0 a N p %D 00 v m u o w n> • Item# zxzzzzzzzxxV BP4U-125 ml. Plastic Unpreserved (N/A) (Cl-) BP3U.2SO ml. Plastic Unpreserved (N/A) BP2U-500 mL Plastic Unpreserved (N/A) BP1U-1 liter Plastic Unpreserved (N/A) OP45-125 ml. Plastic H2SO4 (pH < 2) (Cl-) BP3N-250 ml. plastic HNO3 (pH < 2) BP4Z-125 mL Plastic ZN Acetate & NaOH (>9) BP46-125 mL Plastic NaOH (pH> 12) (Cl-) WGFU-Wide-mouthed Glass jar Unpreserved AGIU-1 liter Amber Unpreserved (N/A) (Cl-) zzzzzzz AG1H-1 liter Amber HCI (pH < 2) AG3U-250 mL Amber Unpreserved (N/A) (Cl-) AG15-1 liter Amber H2SO4 (pH < 2) AG3S-250 mL Amber H2504 (pH < 2) DG94-40 mL Amber NH4Cl (N/A)(CI-) S S- S ,� S S ,� .-Z DG9H.40 ml. VOA HCI (N/A) VG9T-40 mL VOA Na2S203 (N/A) VG9U-40 mL VOA Unpreserved (N/A) DG9V-40 ml. VOA H3PO4 (N/A) KP71.1-50 ml. Plastic Unpreserved (N/A) V/GK (3 vials per kit)-VPH/Gas kit (N/A) SPST-125 mL Sterile Plastic (N/A - lab) SP2T-250 mL Sterile Plastic (N/A- lab) 8P311-250 mL Plastic (NH2)2SO4 (9.3-9.7) AGOU-100 mL Amber Unpreserved (N/A) (Cl-) VSGU-20 mL Scintillation vials (N/A) DG91J-40 mL Amber Unpreserved vials (N/A) + f r1 + W m S n o 9 s m n 0 �c 3 < S o3i I� 01 D OJ � rt 'O -0ir y Cr o S m Mx N ui O M -Ow EL G ^ b cr z — n0 x :Y .�► b tv Cr !' n 0.(Np S— A G 0 Cr 0 °; a 0 o 0 ro rp � it 3 n E Cu OM ° 3 0 or u� 0 r1 3 r � c w fD M CL o+ CL M �- 2. r+ rt U m Z CO f0 N 1 N is w CL O Y w 0 M w O v N N W 1 N M OD W e n .[. O M' m rn N O_ O) A r v N a w N ItemN BP41.1•125 mL Plastic Unpreserved (N/A) (CI-) SP311.250 ml. Plastic Unpreserved (N/A) BP21.1-500 ml Plastic Unpreserved (N/A) BP11.1-1 liter Plastic Unpreserved IN/A) j/ BP45-125 ml Plastic H2SO4 (pH < 21 (CI-) / BP3N-250 ml plastic HNO3 (pH < 2) BP4Z-125 mL Plastic ZN Acetate & NaOH (>9) BP46.125 mL Plastic NaOH (pH > 12) (CI-) WGFU-Wide-mouthed Glass jar Unpreserved AGIU-1 liter Amber Unpreserved (N/A) (Cl.) / AG1H-1 liter Amber HCI (pH < 21 A63U-250 ml Amber Unpreserved (N/A) (CI-) AG1S-1 Inter Amber H2SO4 (pH < 2) AG3S-250 mL Amber H2SO4 (pH < 2) OG94-40 mL Amber NH4Cl (N/A)(CI-) _ DG9H-40 ml VOA HCl (N/A) VG9T-40 mL VOA Na2S203 (N/A) VG9U.40 ml. VOA Unpreserved (N/A) OG9V-40 mL VOA H3PO4 (N/A) KP71.1-50 ml Plastic Unpreserved (N/A) V/GK (3 vials per kit)-VPH/Gas kit (N/A) SPST-125 ml Sterile Plastic (N/A — tab) SP2T-250 mL Sterile Plastic (N/A — lab) 71 BP3R-250 mL Plastic (NH2)2SO4 (9.3-9.7) AGOU-100 mL Amber Unpreserved (N/A) (Cl-) VSGU-20 mL Scintillation vials (N/A) 1 I I DG9U-40 mL Amber Unpreserved vials (N/A) ♦ . F f n ♦ ID O M 'r 3 < a a � is C T M C o M x 3 u { N - M 0 d C C! C w x C G1 S C d a el 0 S — p { OR O C `0 .�. 11 M z T ry � � 1A £ O a 3 2 9 OI ON n N rn � r0- a C a el T Ci CD CHAIN -OF -CUSTODY I Analytical Request Document /'�a7 Ce The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. r___ ...A r....A: i— f--A el h--Irmfn nern1,h< lf auwnnuny a >a nPie ..a 1 -- ,....,, ,.r ,................ ............. n ,..., ...... ..., r ..,... ,,....... ___ . _...._ _.._ -_.._ _ _ Section A Section B Section C Required Client Information: Required Project Information: Invoice Information: Page: 1 Of 1 Company. Speedwa AECOM Report To: Schaefer, Brell Attention: Address: 6000 Fai-ew Road Copy To: Company Name: Suite 2D0, Charlotte. NC 28210 Address: Regulatory Agency Email: brett schaeferaecom.com Purchase Order #: Pace Quote: PO# 1100654135 Phone: NONE JFax Project Name: Speedway 7997 MamhNlle Pace Project Manager: bonnie.Yan pacelabs.com, Stall I Location Requested Due Date Proiecl #: Pace Profile /: 16669 NC R twalad Ana Ia FDtarad YM I.aralx Coot: - COLLECTED = Preservatives >' m DA""... °v1 Wets w'T " f3 at o U Y/Sits WNM IYY1 Aoaucl P - at a� C SAMPLE ID o^'swA „ _ -rwr END a II- = a One Character per box. W- WPAA w a i _ -c° at (A-Z, 0-91. -) an. 01 Sample Ids must be unique Tn,,,. Ts 0 K g w '�' t u m 'rL%i m OH a $ W a n u O ~ 2 Ll D DATE TIME * _ 2 _ _ o ¢ I12A i 3 /wT ✓ `t 2 il'�f X D�7� 3 h1w z 4 Im w . X CCU 5 m uI �U(r' 6 w ti itir> 7 w (J 6 Mw 9 10 M UV 11 ln1 I'' ills l ot2 12 rv1whIWO ADDITIONAL COMMENTS RELMOUIBNED BY I AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS Remed,elxm Pm)ect(IDS i—ce Lab Upload) 1 I�'i� ►f- T It- 7 �. 11 ALL 5A1niLGi — �160 h1T8� IPE'r�A3 ; 5 oxYs, E7,j,aNOL � s� SAMPLER NAME AND SIGNATURE c 0 c a ° r y$m m PRINT Nam of SAMPLER: t'140G 12 >�ISLQfAD SIGNATURE of SAMPLER: DATE SlBned: r rc w > ? B $ c� c U to rp m O m A CHAIN -OF -CUSTODY / Analytical Request Document Ce The Chain -of -Custody is a LEGAL DOCUMENT All relevant fields must be completed accurately. lhtc ch:!;n .r C„ernsnd—Pnlanr.P of the Para Terms and Cnndilions found at htfos:/Iinfo.nacelabs.com/hubfs/Das-standard-terms. odf. Section A Section 6 Section C Required Client Information: Required Project Informatlon: Invoice Information: Page ; 1 0( 1 Company Speed"AECOM Report To. Schaefer, Breit Altenhon. Address'. 6000 Fa.— Road Copy To Company Name Suite 200. Charlotte, NC 28210 Address: L Regulatory Agency Finail Drell. schaefer@aecom.com Purchase Order n Pace Quote. POd 1100654135 Pnone. NONE Fax Project Name: Speedy 7997 Marshville Pace Project Manager. bon— van @pacelabs corn. State I Location Requested Due Date. Project It. Pace Profile 0: 16669 1 NC Requested Ana sfa Filtered YIN 1.1,1140, CODE O U COLLECTED Z Preservatives a) prnlry l•:ais OW WT S U 0 W1111 Waw WW W= W Pratl„cl P SAMPLE ID S.'WC SL 3 5MT END One Character per box. N. '!P _ i u U (A-Z, 0-9 I, -) 01- or o w i Z i' o Sample Ids must be unique T,.r,,. s w o vU O c ,P w a s n u o = o L t, H I A TIME Z'? _ = z i O K Itl 2 3 fyl IN l u �a Z•� Cc / 4 7 5 6 7 6 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED eY / AFFILIATION DATE TIME ACCEPTED BY f AFFILIATION DATE TIME SAMPLE CONDITIONS Rcrn Mrnlion Protect (IDS Invoke - Lab Upbad) i"A / 1 \ QC(-` `, 1 ` �." SAMPLER NAME AND SIGNATURE U o PRINT Name of SAMPLER: c w = 2_ SIGNATURE of SAMPLER: / DATE Signed: //t (, OGEL Pp 205 Z. �5 A 11 Marshvii(e .� c\ City Cem( FOR DR ti NX 205 s 0 yu O C (r COLLEGE ST O� �g0 t lj, y y 550 2 b Z a TRAYWIC`RO rn � 1 '^. E uNjON sT r Masso550 rshville SITE LOCATION � 1`t 9 S � �0 11.tC� B'1 � t HASTY RO . \_ Nam• ... ,,� \) g � NASTY RD OLD NWY 74 s \ e y m 550 o SCALE IN FEET: 2,000 0 2,000 j f t`\ ��) NOTE: ALL MAP FEATURES ARE APPROXIMATE Jl \ I �� IN SCALE AND LOCATION. s Speedway LLC. SITE LOCATION MAP FIGURE 1 2 Speedway Store #7997 Source: Topo USGS 7.5 Minute Topographic Map 6325 West Marshville Boulevard Quadrangle: Buffalo SE, NY Marshville, NC Copyright: 2019 National Geographic Society aCOM SI DATE: MAY 2023 DRAWN BY: I. DUMITRU REVIEWED BY: N. PINSKER I PROJECT NO.: 60708764 ©-SAN- SAN-=- � STREAM #3 -SAN -SAN---SAN- SAN----SAN---SANBOSAr$trB9t SAN---SAN -AN --- yAN- Frac Tanks, Sediment Filters & Carbon Vessels Storage Area MW-17 —o-- - / Discharge Point MW-7 STREAM #2 MW-13-0- I MW-15 I MW-6 I Tank Field .- I II / MW-19 / Vent Pipes I MW-12 1� I11 I i� --ST i i Imo/ 0 STREAM #1 i MW-1 D -o-1 #3 c: #4 / G 1#21l#� LMW-2 MW-5R M i i MW -CAN -SAN---SAN- Sgry 7 : z .SqN lb Concrete Flume ,SPN� L - J Grease Speedwa � I Trap Y Store #7997 JKerosene Pump I J 1 MW-4 Canopy & MW-3 Dispenser Islands - ® 0C�7o MW-14 W-11 R MW-10\ -18 Highway 74 (West Marshville Boulevard) Concrete Pedestal LEGEND —••— Approximate Site Property Boundary — — Approximate Property Boundary ® Approximate Building Footprint 1�0® Product Dispenser k- i Underground Storage Tank #1 2,000-Gal. PLUS Gasoline #2 3,000-Gal. PLUS Gasoline #3 15,000-Gal. RUL Gasoline #4 15,000-Gal. PUL Gasoline #5 10,000-Gal. Kerosene #6 10,000-Gal. Diesel --OH/E-- Overhead Electric Co-) Utility Pole / Power Pole Light Post / Traffic Light --UG/E-- Buried Electric Line --G-- Natural Gas Line -- — Water Line Fire Hydrant Water Meter X Water Valve --SAN-- Sanitary Sewer 0 Sanitary Sewer Manhole cr Grease Trap --ST-- Storm Sewer O Catch Basin / Stormwater Inlet Monitoring Well 0 Surface Water Sample Location SETTLING TANK > INFLUENT GRAVITY FEED .�O•.•oFE �oti,ti9. •.�� SEAL — G i SGNP\���. 2 SUBMERSIBLE PUMPS (90 GPM each) UNDER WEIR 90 GPM 2000 HPV MEDIA VESSEL 2,000 LBS ACTIVATED CARBON 90 GPM -) SEDIMENT BAG 0 y n S D X G) m TO CUSTOMERS DISCHARGE POINT (90-180 GPM)