NC0003417_Renewal (Application)_20230928

dai a SCATS
ROY COOPER t -
Governor
ELIZABETH S.BISER ""o°"
Secretary " f3
RICHARD E.ROGERS,JR. NORTH CAROLINA
Director Environmental Quality
September 28, 2023
Duke Energy Progress, LLC
Attn: Jeffery Hines, GM-II
1199 Black Jack Church Road
Goldsboro, NC 27530
Subject: Permit Renewal
Application No. NC0003417
Lee Steam Electric Plant
Wayne County
Dear Applicant:
The Water Quality Permitting Section acknowledges the September 28, 2023 receipt of your permit renewal application
and supporting documentation. Your application will be assigned to a permit writer within the Section's NPDES WW
permitting branch. Per G.S. 150B-3 your current permit does not expire until permit decision on the application is made.
Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit. The
permit writer will contact you if additional information is required to complete your permit renewal. Please respond in a
timely manner to requests for additional information necessary to allow a complete review of the application and renewal
of the permit.
Information regarding the status of your renewal application can be found online using the Department of Environmental
Quality's Environmental Application Tracker at:
https://deq.nc.gov/permits-regulations/permit-guidance/environmental-application-tracker
If you have any additional questions about the permit, please contact the primary reviewer of the application using the
links available within the Application Tracker.
Sincerely,
Wren Thedford
Administrative Assistant
Water Quality Permitting Section
ec: WQPS Laserfiche File w/application
D_E Q ' North
Washington Caroline Regiona DepalrtmentOffice of1 943 EnviroWashnmental ington QualitySquare I Division of Water Resources North Mall Washington Carolina 27889
ai44." l sww� /"/ 252.946.6481

/ra DUKE H.F.Lee Energy Complex
ENERGY* Duke Energy Progress
1199 Black Jack Church Road
PROGRESS Goldsboro, NC 27530
September 14, 2023
Mr. Doug Dowden RECEIVED
Supervisor—NC NPDES Industrial Permitting
NC Division of Water Resources
1617 Mail Service Center SEP 28 2023
Raleigh, NC 27699-1617
Subject: Duke Energy Progress, LLC
H. F. Lee Energy Complex
NPDES Permit NC0003417—Permit Renewal Application NCDEQ/DWR/NPDES
Wayne County
Dear Mr. Dowden:
Duke Energy Progress, LLC (Duke) requests the subject permit be renewed and reissued. The above referenced
permit expires on March 31, 2024. As mandated by North Carolina Administrative Code 15A NCAC 2H .0105(e),this
permit renewal application is being submitted at least 180 days prior to expiration of the current permit.
Please find enclosed the renewal application package(one original and two copies):
• EPA Form 1
• Site Maps
• EPA Form 2C for outfalls 001,002, and 005b
• Narrative—Supplemental Information
• Process Flow Diagram
• Potential Discharges Not Covered By Analysis
• Fish Tissue
• Water Quality Instream Monitoring
With reissuance, Duke requests the following modifications:
1. Supplemental to Permit Cover Sheet
a. Outfall 001-Remove reference to Ash Pond Decant, Phase I
b. Outfall 002 and 002A—Cooling Pond — Remove reference to coal pile runoff. The coal pile has
been remediated and flow to the cooling pond has ceased
2. Condition A (1.) Phase 1 Ash Pond Decant (Outfall 001) — Dewatering of the basin began on 7/16/2019.
Duke requests removal of this Condition.
3. Condition A(2.)Phase II Ash Pond Dewatering and Groundwater Remediation(Outfall 001)
a. Change the monitoring frequency for Nitrite/Nitrate from weekly to monthly based upon sampling
results during permit term and to align with sampling frequency in Condition A(7) and A(8) Ash
Pond Dewatering—Outfalls 005a and 005b.
b. Change monitoring frequency for arsenic, mercury, selenium, copper, zinc, and Total Hardness
from weekly to monthly based upon sample results during the last permit term.
c. Removal of testing requirements for chromium, lead, and cadmium based upon sampling results
during the last permit term.

d. Removal of testing requirement for total dissolved solids to align with sampling frequency in
Condition A(7)and A(8)Ash Pond Dewatering—Outfalls 005a and 005b.
e. Change the monitoring frequency for Chronic Toxicity from monthly to quarterly to align with
reissued other Duke Energy permits and based on demonstrated compliance during the last
permit term.
f. Change frequency for Chronic Toxicity from monthly to quarterly in Note#6.
g. The active ash basin is in the dewatering/excavation phase. The liquid level within the basin has
been lowered and maintained for excavation. Duke request removal of Note a.
h. Removal of Note d - based upon the data from last permit term and the nonstandard permit
language.
i. Removal of Note e — This requirement is included in Condition A (3) Phase Ill - Groundwater
Extraction.
4. Condition A(3)—Phase III—Groundwater Extraction(Outfall 001)
a. Change the monitoring frequency for Chronic Toxicity from month►y to quarterly to align with
reissued other Duke Energy permits.
b. Removal of Note b - based upon sample results at Outfall 001 during last permit term and the
nonstandard permit language.
5. Condition A(4)—Cooling Pond (Outfall 002)
a. Remove reference to coal pile runoff. The coal pile has been remediated and flow to the cooling
pond has ceased. Duke requests the Daily Maximum Limit for TSS be increased from 50 mg/I to
100 mg/I based upon removal of coal pile runoff for both outfalls 002 and 002A.
b. Analysis for the 126 Priority Pollutants is conducted with the required 2C sampling with permit
renewal. Duke requests removal of Note#7.
6. Condition A (6) — Coal Ash Beneficiation (Outfall 004) — This outfall has not been constructed. Duke
requests that this outfall remain in permit
7. Condition A(7)—Inactive Ash Pond Dewatering(Outfall 005a)
a. Change the monitoring frequency for Chronic Toxicity from monthly to quarterly to align with
reissued other Duke Energy permits.
b. Change frequency for Chronic Toxicity from monthly to quarterly in Note#6.
c. The active ash basin is in the dewatering/excavation phase. The liquid level within the basin has
been lowered and maintained for excavation. Duke request removal of Note a.
d. Removal of Notes c and d - based upon the data from last permit term and nonstandard permit
language.
8. Condition(8)-Inactive Ash Pond Dewatering(Outfall 005b)
a. Change monitoring frequency for Total Hardness from weekly to monthly based upon sample
results during the last permit term.
b. Removal of testing requirements for antimony and thallium based upon sampling results during
the last permit term.
c. Change the monitoring frequency for Chronic Toxicity from monthly to quarterly to align with
reissued other Duke Energy permits and based on demonstrated compliance during the last
permit term.
d. Change frequency for Chronic Toxicity from monthly to quarterly in Note#6.
e. The active ash basin is in the dewatering/excavation phase. The liquid level within the basin has
been lowered and maintained for excavation. Duke request removal of Note a.
f. Removal of Notes c,d,and e-based upon the data from last permit term and nonstandard permit
language.
9. Condition A (14) Chronic Toxicity Limit (Monthly— Outfall 001, Outfall 005a and Outfall 005b) — Duke
requests the change of monitoring frequency for Chronic Toxicity from monthly to quarterly to align with

reissued other Duke Energy permits and based on demonstrated compliance during the previous permit
term.
10. Condition A(22)—Clean Water Act Section 316(B)—The 316(B)Study was submitted to DWR on 7/14/2022.
Duke requests removal of this Condition.
11. Condition A(25) —Ash Pond Closure—The Ash Basin Closure Plans have been submitted to DWR. Duke
requests removal of this Condition.
12. Condition A(26)—Instream Monitoring
a. Duke requests that instream monitoring be revised from monthly to quarterly based on review of
the data from permit term demonstrated the lack of impact from ash basin dewatering as
documented in the provided upstream and downstream data.
b. Duke requests removal of testing requirements for bromide, and dissolved cadmium based upon
data from the last permit term.
c. Duke request removal of the requirement for instream monitoring to be submitted with permit
renewal application based upon this data is reported with DMRs.
d. The DMR location for reporting of downstream data has been changed from downstream of Outfall
003 to Outfall 002. The change was made to allow for removal of outfall 003 from BIMS system.
The physical sampling location has not changed. Duke requests that the downstream sampling
location be designated as"downstream of outfall 002—at Stevens Mill Road bridge".
13. Condition 27—Fish Tissue Monitoring Near Ash Basin Discharge(Outfall 001)
a. Based upon data from this permit term,Duke requests that monitoring frequency be changed from
annually to once per permit term completed during years 1 to 4 of the permit's effective term.
Should you have any questions or need additional information please feel free to contact Joyce Dishmon at 336-623-
0238 or via email at [e-mail].
"l certify under penalty of law that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and
evaluate the information submitted. Based on my inquiry of gathering the information,submitted is, to the
best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fine and imprisonment for knowing
violations."
Sin erel ,
Je ery . Ines
eneral Manager II
H. F. Lee Energy Complex
Enclosure: Permit Renewal Application
Cc: David May,Washington Regional Office-NC DEQ DWR
Mike Graham,EHS Site Professional—via email
Joyce Dishmon, EHS Permitting&Compliance—via email
1

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
OMB No.2040-0004
NCD000830661 NC0003417 H.F.Lee Energy Complex
U.S.Environmental Protection Agency
Form Application for NPDES Permit to Discharge Wastewater
NPDES - EPA GENERAL INFORMATION
SECTION 1.ACTIVITIES REQUIRING AN NPDES PERMIT(40 CFR 122.21(f)and(f)(1))
1.1 Applicants Not Required to Submit Form 1
1.1.1 Is the facility a new or existing publicly owned Is the facility a new or existing treatment works
1.1.2 treatin domestic sewage?
treatment works? g
If yes,STOP.Do NOT complete D No If yes, STOP.Do NOT No
Form 1.Complete Form 2A. complete Form 1.Complete
Form 2S.
1.2 Applicants Required to Submit Form 1
1.2.1 Is the facility a concentrated animal feeding 1.2.2 Is the facility an existing manufacturing,
operation or a concentrated aquatic animal commercial,mining,or silvicultural facility that is
o_ production facility? currently discharging process wastewater?
oEl Yes 4 Complete Form 1 El No ✓0 Yes 4 Complete Form ❑ No
z and Form 2B. 1 and Form 2C.
1.2.3 Is the facility a new manufacturing,commercial, 1.2.4 Is the facility a new or existing manufacturing,
mining,or silvicultural facility that has not yet commercial,mining,or silvicultural facility that
commenced to discharge? discharges only nonprocess wastewater?
Yes 4 Complete Form 1 ❑ No Yes 4 Complete Form El No
ce and Form 2D. 1 and Form 2E.
1.2.5 Is the facility a new or existing facility whose
y discharge is composed entirely of stormwater
a associated with industrial activity or whose
discharge is composed of both stormwater and
non-stormwater?
Yes Complete Form 1 ✓0 No
and Form 2F
unless exempted by
40 CFR
122.26(b)(14)(x)or
b 15 .
SECTION 2.NAME,MAILING ADDRESS,AND LOCATION(40 CFR 122.21(f)(2))
2.1 Facility Name
H.F.Lee Energy Complex
2.2 EPA Identification Number
0 NCD000830661
2.3 Facility Contact
y Name(first and last) Title Phone number
v Jeffery Hines GM-II Regulated Station [phone]
Email address
[e-mail]
2.4 Facility Mailing Address
£ Street or P.O.box
1199 Black Jack Church Road
City or town State ZIP code
Goldsboro NC 27530
EPA Form 3510-1(revised 3-19) Page 1

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCD000830661 NC0003417 H.F.Lee Energy Complex OMB No.2040-0004
y 7, 2.5 Facility Location
ly Street,route number,or other specific identifier
0 1199 Black Jack Church Road
07
c County name County code(if known)
Ta M v Wayne
E —r City or town State
o
ZIP code
Goldsboro NC 27530
SECTION 3.SIC AND NAICS CODES(40 CFR 122.21(f)(3))
3.1 SIC Code(s) Description(optional)
4911 Electric Services
in
d
6
O
U
N
U
3.2 NAICS Code(s) Description(optional)
221112 Fossil Fuel Power Generation
U
SECTION 4.OPERATOR INFORMATION(40 CFR 122.21(f)(4))
4.1 Name of Operator
Duke Energy Progress,LLC
4.2 Is the name you listed in Item 4.1 also the owner?
✓❑ Yes ❑ No
4.3 Operator Status
❑ Other (specify)
is ❑ Public—federal 0 Public—state public
o ✓❑ Private 0 Other(specify)
4.4 Phone Number of Operator
[phone]
4.5 Operator Address
Street or P.O.Box
E d 1199 Black Jack Church Road
c City or town State ZIP code
0 o Goldsboro NC 27530
A v
Q Email address of operator
[e-mail]
SECTION 5.INDIAN LAND(40 CFR 122.21(f)(5))
c 5.1 Is the facility located on Indian Land?
c -J ❑Yes ❑✓ No
EPA Form 3510-1(revised 3-19) Page 2

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCD000830661 NC0003417 H.F.Lee Energy Complex OMB No.2040-0004
SECTION 6.EXISTING ENVIRONMENTAL PERMITS(40 CFR 122.21(f)(6))
6,1 Existing Environmental Permits(check all that apply and print or type the corresponding permit number for each)
Tcs
d m NPDES(discharges to surface m RCRA(hazardous wastes) 0 UIC(underground injection of
water) fluids)
o w NC0003417 See Attached
.5 E
w a ❑✓ PSD(air emissions) ElNonattainment program(CM) 0 NESHAPs(CM)
01812T50 Title V Air Permit
x ❑ Ocean dumping(MPRSA) 0 Dredge or fill(CWA Section 404) ❑Other(specify)
uI SAW-2010-00973 See Attached List
SECTION 7.MAP(40 CFR 122.21(f)(7))
7.1 Have you attached a topographic map containing all required information to this application?(See instructions for
0 specific requirements.)
✓❑Yes ❑No 0 CAFO—Not Applicable(See requirements in Form 2B.)
SECTION 8.NATURE OF BUSINESS(40 CFR 122.21(f)(8))
8.1 Describe the nature of your business.
The H.F.Lee Energy Complex is an electric generating facility consisting of five simple cycle combustion
turbines and three combined cycle combustion turbines
N
C
y
7
m
w
O
G1
i6
SECTION 9.COOLING WATER
INTAKE STRUCTURES(40 CFR 122.21(f)(9))
9.1 Does your facility use cooling water?
L d ✓❑ Yes ❑ No 4 SKIP to Item 10.1.
CO . 9.2 Identify the source of cooling water.(Note that facilities that use a cooling water intake structure as described at
g 40 CFR 125,Subparts I and J may have additional application requirements at 40 CFR 122.21(r).Consult with your
NPDES permitting authority to determine what specific information needs to be submitted and when.)
O
R U c H.F.Lee Energy Complex's source of cooling water is treated water from a closed system. Water from the Neuse
River is used as make-up water as needed. In accordance with the provisions of NPDES Permit NC0003417,Part I
A.(22.),the required Clean Water Act§316(b)information for the H.F.Lee Energy Complex was submitted 7/14/22.
SECTION 10.VARIANCE REQUESTS(40 CFR 122.21(f)(10))
10.1 Do you intend to request or renew one or more of the variances authorized at 40 CFR 122.21(m)?(Check all that
apply.Consult with your NPDES permitting authority to determine what information needs to be submitted and
when.)
c ❑ Fundamentally different factors(CWA ❑ Water quality related effluent limitations(CWA Section
Section 301(n)) 302(b)(2))
❑ Non-conventional pollutants(CWA ❑ Thermal discharges(CWA Section 316(a))
Section 301(c)and(g))
❑ Not applicable
EPA Form 3510-1(revised 3-19) Page 3

Duke Energy Progress, LLC
H.F. Lee Energy Complex
Existing Environmental Permits
Issuing Agency Type of Permit ID Number
Division of Water Quality NPDES Wastewater NC0003417
NPDES Stormwater NCG200529
Division of Water Quality Ash Reuse Program Permit WQ0000020
USCoAE CWA Section 404 SAW-2010-00973
Division of Land Quality Dam Safety Permit to Impound
WAYNE-009 H
WAYNE-022 H
WAYNE-031 H
WAYNE-032 H
WAYNE-033 H
Division of Air Quality Title V Air Permit 01812T50
RCRA Handler ID
Gas Turbine NCD0991302624
Coal Station NCD000830661

d
EPA Identification Number NPDES Permit Number Facility Name FormOMB Nve d0 0 03/05/199
NCD000830661 NC0003417 H.F.Lee Energy Complex
SECTION 11.CHECKLIST AND CERTIFICATION STATEMENT(40 CFR 122.22(a)and(d))
11.1 In Column 1 below,mark the sections of Form 1 that you have completed and are submitting with your application.
For each section,specify in Column 2 any attachments that you are enclosing to alert the permitting authority.Note
that not all applicants are required to provide attachments.
Column 1 Column 2
✓❑ Section 1:Activities Requiring an NPDES Permit 0 wl attachments
✓❑ Section 2: Name,Mailing Address,and Location 0 w/attachments
❑✓ Section 3: SIC Codes ❑ wl attachments
✓❑ Section 4:Operator Information ❑ wl attachments
❑✓ Section 5:Indian Land ❑ w/attachments
❑✓ Section 6: Existing Environmental Permits ✓❑ wl attachments
wl topographic ❑ wl additional attachments
0 Section 7: Map ❑ map
0
❑✓ Section 8:Nature of Business 0 wl attachments
.47
4.3
❑✓ Section 9: Cooling Water Intake Structures ❑ wl attachments
❑ Section 10:Variance Requests ❑ w/attachments
y ✓❑ Section 11:Checklist and Certification Statement ❑ w/attachments
Y
CD 11.2 Certification Statement
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted.Based on my inquiry of the person or persons who manage the system,or those persons
directly responsible for gathering the information, the information submitted is,to the best of my knowledge and
belief, true, accurate,and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fine and imprisonment for knowing violations.
Name(print or type first and last name) Official title
Jeffery Hines GM-II Regulated Station
Sig Date signed
/q/ 3
EPA Form 3510.1(revised 3-19) Page 4

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Figure 1
Legend
il ,ir.,DUKE
NPDES Permit No. NC0003417
9 ENERGY„ -••- Property Boundary
Site Location Map
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Outfall 78°4'6.49"W 35'22'45.182"N
Figure 2
s Legend Outfall 002: 78°5'5.83"W 35°22'52.019"N N
.- Outfall 78°3'S0.836"W 35°22'14.001"N NPDES Permit No.NC0003417
. U.. ••♦ _••_Property Boundary
• �., „4 Outfall 004: 78°6'9.407"W 35°22'18.845"NA NPDES Outfall Locations
�' �'•� r� NPDES Outfall Location Outfall 005a: 78°6'7.482"W 35°22'40.573"N H.F.Lee EnergyComplex
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p 4• .._ Outfall 005b: 78°6'11.69"W 35°22'21.968"N 0 700 1.400 Goldsboro,North Carolina
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EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCD000830661 NC0003417 H.F.Lee Energy Complex OMB No.2040-0004
Form U.S.Environmental Protection Agency
2C EPA Application for NPDES Permit to Discharge Wastewater
NPDES EXISTING MANUFACTURING,COMMERCIAL,MINING,AND SILVICULTURE OPERATIONS
SECTION 1.OUTFALL LOCATION(40 CFR 122.21(g)(1))
1.1 Provide information on each of the facility's outfalls in the table below.
o Numbelr Receiving Water Name Latitude Longitude
U
J
001 Neuse River 35° 22' 45.3* 78° 4' 6.46"
fts
3 002 Neuse River 35° 22' 51.74" 78° 5' 5.93"
0
002A Neuse River 35° 22' 1.74" 78° 4' 59.59
SECTION 2.LINE DRAWING(40 CFR 122.21(g)(2))
p, 2.1 Have you attached a line drawing to this application that shows the water flow through your facility with a water
c .3 balance?(See instructions for drawing requirements.See Exhibit 2C-1 at end of instructions for example.)
J �
❑✓ Yes ❑ No
SECTION 3.AVERAGE FLOWS AND TREATMENT(40 CFR 122.21(g)(3))
3.1 For each outfall identified under Item 1.1, provide average flow and treatment information.Add additional sheets if
necessary.
**Outfall Number** 001
Operations Contributing to Flow
Operation Average Flow
Dewatering and Excavation of Ash Basin 0.264 mgd
c
The ash pond no longer receives wastewater discharges mgd
is
L
Discharge consists of Stormwater Runoff,Groundwater, mgd
fO and Ash Pore Water mgd
o Treatment Units
Description Code from Final Disposal of Solid or
(include size,flow rate through each treatment unit, Table 2C-1 Liquid Wastes Other Than
retention time,etc.) by Discharge
pH adjustment,flocculation 1-G,1-U,2-K 4-A
bioreactor(as needed) 3-C 4-A
EPA Form 3510-2C(Revised 3-19) Page 1

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCD000830661 NC0003417 H.F.Lee Energy Complex
OMB No.2040-0004
Form U.S.Environmental Protection Agency
2C 8 EPA Application for NPDES Permit to Discharge Wastewater
NPDES EXISTING MANUFACTURING,COMMERCIAL,MINING,AND SILVICULTURE OPERATIONS
SECTION 1.OUTFALL LOCATION(40 CFR 122.21(g)(1))
1.1 Provide information on each of the facility's outfalls in the table below.
o Numbelr Receiving Water Name Latitude Longitude
O 005a Neuse River 35° 22' 40.40° 78° 6' 7.64°
005b Neuse River 35° 22' 21.94° 78° 6' 11,61
O
SECTION 2.LINE DRAWING(40 CFR 122.21(g)(2))
a, 2.1 Have you attached a line drawing to this application that shows the water flow through your facility with a water
a) .0 balance?(See instructions for drawing requirements.See Exhibit 2C-1 at end of instructions for example.)
o ❑✓ Yes ❑ No
SECTION 3.AVERAGE FLOWS AND TREATMENT(40 CFR 122.21(g)(3))
3.1 For each outfall identified under Item 1.1,provide average flow and treatment information.Add additional sheets if
necessary.
**Outfall Number** 005b
Operations Contributing to Flow
Operation Average Flow
Dewatering&Excavation of Ash 0.45 mgd
The ash pond no longer receives wastewater discharges mgd
Discharge consists of Stormwater Runoff,Groundwater mgd
j h and Ash Pore water mgd
o Treatment Units
rr
Description Code from Final Disposal of Solid or
(include size,flow rate through each treatment unit, Table 2C•1 Liquid Wastes Other Than
retention time,etc.) by Discharge
pH adjustment,flocculation 1-G,1-U,2-K 4-A
EPA Form 3510-2C(Revised 3-19) Page 1

EPA Identification Number NPDES Permit Number I Facility Name Form Approved 03/05/19
NCD000830661 NC0003417 H.F.Lee Energy Complex OMB No.2040-0004
3.1 **Outfall Number** 002/002A
cont. Operations Contributing to Flow
Operation Average Flow
Emergency Overflow-Cooling Pond NA mgd
g Y
mgd
mgd
mgd
Treatment Units
Description Code from Final Disposal of Solid or
(include size,flow rate through each treatment unit, Table 2C-1 Liquid Wastes Other Than
retention time,etc.) by Discharge
condenser cooling water,reverse osmosis reject 1-F 4-A
=
wastewater,low volume wastewater,containment
0
U
drain wastewater
d
E
Ca
**Outfall Number** 005a
y Operations Contributing to Flow
0 Operation Average Flow
U-
rn Dewatering&Excavation of Ash NA mgd
to
m
The ash pond no longer receives wastewater discharges mgd
Discharge consists of Stormwater Runoff,Groundwater mgd
and Ash Pore water-outfall has not been constructed mgd
Treatment Units
Description Code from Final Disposal of Solid or
(include size,flow rate through each treatment unit, Table 2C.1 Liquid Wastes Other Than
retention time,etc.) by Discharge
pH adjustment,flocculation 1-G,1-U,2-K 4-A
3.2 Are you applying for an NPDES permit to operate a privately owned treatment works?
E ✓ 4.
�, L ❑ Yes ❑ No-� SKIP to Section
3.3 Have you attached a list that identifies each user of the treatment works?
❑ Yes ❑ No
EPA Form 3510-2C(Revised 3-19) Page 2

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
OMB No.2040-0004
NCD000830661 NC0003417 H.F.Lee Energy Complex
SECTION 4.INTERMITTENT FLOWS(40 CFR 122.21(g)(4))
4.1 Except for storm runoff,leaks,or spills,are any discharges described in Sections 1 and 3 intermittent or seasonal?
❑ Yes ✓❑ No 4 SKIP to Section 5.
4.2 Provide information on intermittent or seasonal flows for each applicable outfall.Attach additional pages,if necessary.
Outfall Operation Frecuency Flow Rate
Number (list) Average Average Long-Term Maximum Duration
DayslWeek Months/Year Average Daily
1 days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
SECTION 5.PRODUCTION(40 CFR 122.21(g)(5))
5.1 Do any effluent limitation guidelines(ELGs)promulgated by EPA under Section 304 of the CWA apply to your facility?
✓❑ Yes ❑ No 4 SKIP to Section 6.
5.2 Provide the following information on applicable ELGs.
ELG Category ELG Subcategory Regulatory Citation
0
3 Steam Electric Steam Electric Power Industry 40 CFR 423
0
d
5.3 Are any of the applicable ELGs expressed in terms of production(or other measure of operation)?
❑ Yes 0 No-4 SKIP to Section 6.
0
•;g 5.4 Provide an actual measure of daily production expressed in terms and units of applicable ELGs.
2.1 Outfall Operation,Product,or Material Quanti Da Unit of
ry pery Measure
-a Number
0
c.�
0
L
EPA Form 3510-2C(Revised 3-19) Page 3

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
OMB No.2040-0004
NCD000830661 NC0003417 H.F.Lee Energy Complex
SECTION 6.IMPROVEMENTS(40 CFR 122.21(g)(6))
6.1 Are you presently required by any federal,state,or local authority to meet an implementation schedule for constructing,
upgrading,or operating wastewater treatment equipment or practices or any other environmental programs that could
affect the discharges described in this application?
0 Yes 0 No 4 SKIP to Item 6.3.
6.2 Briefly identify each applicable project in the table below.
Affected Final Compliance Dates
Brief Identification and Description of Outfalls Source(s)of
Project (list outfall Discharge Required Projected
Q number)
E
d
V
rn
a
6.3 Have you attached sheets describing any additional water pollution control programs(or other environmental projects
that may affect your discharges)that you now have underway or planned?(optional item)
❑ Yes 0 No 0 Not applicable
SECTION 7.EFFLUENT AND INTAKE CHARACTERISTICS(40 CFR 122.21(g)(7))
See the instructions to determine the pollutants and parameters you are required to monitor and,in turn,the tables you must
complete.Not all applicants need to complete each table.
Table A.Conventional and Non-Conventional Pollutants
7.1 Are you requesting a waiver from your NPDES permitting authority for one or more of the Table A pollutants for any of
your outfalls?
❑ Yes ❑ No 4 SKIP to Item 7.3.
7.2 If yes,indicate the applicable outfalls below.Attach waiver request and other required information to the application.
Outfall Number Outfall Number Outfall Number
7.3 Have you completed monitoring for all Table A pollutants at each of your outfalls for which a waiver has not been
requested and attached the results to this application package?
❑ No;a waiver has been requested from my NPDES
0 Yes permitting authority for all pollutants at all outfalls.
UTable B.Toxic Metals,Cyanide,Total Phenols,and Organic Toxic Pollutants
7.4 Do any of the facility's processes that contribute wastewater fall into one or more of the primary industry categories
listed in Exhibit 2C-3?(See end of instructions for exhibit.)
0 Yes 0 No 4 SKIP to Item 7.8.
7.5 Have you checked"Testing Required"for all toxic metals,cyanide,and total phenols in Section 1 of Table B?
0 Yes 0 No
7.6 List the applicable primary industry categories and check the boxes indicating the required GC/MS fraction(s)identified
in Exhibit 2C-3.
PrimaryRequired GC/MS Fraction(s)
Industry Category
(Check applicable boxes.)
Electric Power Plants 0 Volatile 0 Acid 0 Base/Neutral 0 Pesticide
❑Volatile 0 Acid 0 Base/Neutral 0 Pesticide
Cl Volatile 0 Acid ❑Base/Neutral 0 Pesticide
EPA Form 3510-2C(Revised 3-19) Page 4

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCD000830661 NC0003417 H.F.Lee Energy Complex OMB No.2040-0004
7.7 Have you checked"Testing Required"for all required pollutants in Sections 2 through 5 of Table B for each of the
GC/MS fractions checked in Item 7.6?
0 Yes ❑ No
7.8 Have you checked"Believed Present"or"Believed Absent"for all pollutants listed in Sections 1 through 5 of Table B
where testing is not required?
✓❑ Yes ❑ No
7.9 Have you provided(1)quantitative data for those Section 1,Table B,pollutants for which you have indicated testing is
required or(2)quantitative data or other required information for those Section 1,Table B,pollutants that you have
indicated are"Believed Present"in your discharge?
Yes ❑ No
7.10 Does the applicant qualify for a small business exemption under the criteria specified in the instructions?
❑ Yes 4 Note that you qualify at the top of Table B, Q No
-p then SKIP to Item 7.12.
c 7.11 Have you provided(1)quantitative data for those Sections 2 through 5,Table B,pollutants for which you have
c determined testing is required or(2)quantitative data or an explanation for those Sections 2 through 5,Table B,
y pollutants you have indicated are"Believed Present"in your discharge?
✓❑ Yes ❑ No
c•
; Table C.Certain Conventional and Non-Conventional Pollutants
7.12 Have you indicated whether pollutants are"Believed Present"or"Believed Absent"for all pollutants listed on Table C
s for all outfalls?
Y ❑ Yes
❑ No
7.13 Have you completed Table C by providing(1)quantitative data for those pollutants that are limited either directly or
c indirectly in an ELG and/or(2)quantitative data or an explanation for those pollutants for which you have indicated
co "Believed Present"?
ElYes ❑ No
w Table D.Certain Hazardous Substances and Asbestos
7.14 Have you indicated whether pollutants are"Believed Present"or"Believed Absent"for all pollutants listed in Table D for
all outfalls?
El Yes ❑ No
7.15 Have you completed Table D by(1)describing the reasons the applicable pollutants are expected to be discharged
and(2)by providing quantitative data,if available?
❑� Yes ❑ No
Table E.2,3,7,8-Tetrachlorodibenzo-p-Dioxin(2,3,7,8-TCDD)
7.16 Does the facility use or manufacture one or more of the 2,3,7,8-TCDD congeners listed in the instructions,or do you
know or have reason to believe that TCDD is or may be present in the effluent?
❑ Yes 4 Complete Table E. ElNo SKIP to Section 8.
7.17 Have you completed Table E by reporting qualitative data for TCDD?
❑ Yes ❑ No
SECTION 8.USED OR MANUFACTURED TOXICS(40 CFR 122.21(g)(9))
8.1 Is any pollutant listed in Table B a substance or a component of a substance used or manufactured at your facility as
an intermediate or final product or byproduct?
❑ Yes ❑✓ No SKIP to Section 9.
y 8.2 List the pollutants below.
c
1. 4. 7.
2. 5. 8.
co
3. 6. 9.
EPA Form 3510-2C(Revised 3.19) Page 5

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
OMB No.2040-0004
NCD000830661 NC0003417 H.F.Lee Energy Complex
SECTION 9.BIOLOGICAL TOXICITY TESTS(40 CFR 122.21(g)(11))
9.1 Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made
within the last three years on(1)any of your discharges or(2)on a receiving water in relation to your discharge?
p Yes 0 No 4 SKIP to Section 10.
11)
9.2 Identify the tests and their purposes below.
Submitted to NPDES
Test(s) Purpose of Test(s) Date Submitted
Permitting Authority?
0
Chronic Toxicity(outfall NPDES Permit ✓❑ Yes ❑ No 07/17/2023
001) Requirement-
0
Chronic Toxicity(outfall NPDES Permit ✓❑ Yes ❑ No 05/26/2023
005b) Requirement
NPDES Permit ❑ Yes ❑ No
Re.uirement
SECTION 10.CONTRACT ANALYSES(40 CFR 122.21(g)(12))
10.1 Were any of the analyses reported in Section 7 performed by a contract laboratory or consulting firm?
❑✓ Yes ❑ No 4 SKIP to Section 11.
10.2 Provide information for each contract laboratory or consulting firm below.
Laboratory Number 1 Laboratory Number 2 Laboratory Number 3
Name of laboratory/firm Pace Analytical Services,LLC Duke Energy Analytical Pace Analytical Services,
Certification#40 Laboratory LLC
Certification#248 Certification#329
Laboratory address 2225 Riverside Court 13339 Hagers Ferry Road 106 Vantage Point Drive
Asheville,NC 28804 Huntersville,NC 28078-7929 West Columbia,SC 29172
v
0 Phone number
U
[phone] [phone] [phone]
Pollutant(s)analyzed Instream Testing- 2C Analysis- 2C Analysis-BOD,COD,
Total-As,Cr,Se,Hg Oil/Grease,As,Cd,Cr,Cu,Pb, Ammonia,TKN,TP,Fecal
Dissolved-Cd,Pb,Zn,Cu,Zn, Se,Zn,TSS,Bromide,Fluoride, Coliform,Color,Cyanide,
Total Hardness,Total Sulfate,Al,Ba,B,Fe,Mg,Mn, MBAS,PCB,Sulfide,Sulfite,
Dissolved Solids,Bromide Sn,Ti,Sb,Be,Co,Mo,Ni,Ag,TI, Semi-Volatiles,Volatiles,
TOC Hg,NO2NO3;Total Phenols
SECTION 11.ADDITIONAL INFORMATION(40 CFR 122.21(g)(13))
11.1 Has the NPDES permitting authority requested additional information?
0 Yes ✓❑ No 4 SKIP to Section 12.
0
E11.2 List the information requested and attach it to this application.
1. 4.
0
2. 5.
3. 6.
EPA Form 3510-2C(Revised 3-19) Page 6

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NCD000830661 NC0003417 H.F.Lee Energy Complex OMB No.2040-0004
SECTION 9.BIOLOGICAL TOXICITY TESTS(40 CFR 122.21(g)(11))
9.1 Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made
within the last three years on(1)any of your discharges or(2)on a receiving water in relation to your discharge?
❑✓ Yes ❑ No 4 SKIP to Section 10.
1-4
thetests and their our poses below.
9.2 Identify p
Test(s) Purpose of Test(s) Submitted to NPDES Date Submitted
Permitting Authority?
0
F-
Tri Chronic Toxicity(outfall NPDES Permit ✓❑ Yes ❑ No 07/17/2023
001) Requirement-
0
Chronic Toxicity(outfall NPDES Permit ✓❑ Yes ❑ No 05/26/2023
005b) Requirement
NPDES Permit ❑ Yes ❑ No
Re.uirement
SECTION 10.CONTRACT ANALYSES(40 CFR 122.21(g)(12))
10.1 Were any of the analyses reported in Section 7 performed by a contract laboratory or consulting firm?
❑✓ Yes ❑ No 4 SKIP to Section 11.
10.2 Provide information for each contract laboratory or consulting firm below.
Laboratory Number 1 Laboratory Number 2 Laboratory Number 3
Name of laboratory/firm ETT Environmental,Inc. Duke Energy Analytical Pace Analytical Services,
NC#22 Laboratory LLC
Certification#248 Certification#329
N
Laboratory address 4 Craftsman Court, 13339 Hagers Ferry Road 106 Vantage Point Drive
rti
Greer,SC 29650 Huntersville,NC 28078-7929 West Columbia,SC 29172
U
Phone number
[phone] (980)87S-5245 [phone]
Pollutant(s)analyzed Outfalls 001/005b- NPDES Compliance Analysis- NPDES Compliance Analysis
Chronic Toxicity 001/005b -001/005b
Oil/Grease,Ca,Mg,Total Hg,NO2/NO3,Nitrogen,
Hardness,As,Cd,Cr,Cu,Pb,Se, TP,TKN.TP
Sb,TI,Zn,TSS,TDS,Turbidity
SECTION 11.ADDITIONAL INFORMATION(40 CFR 122.21(g)(13))
11.1 Has the NPDES permitting authority requested additional information?
❑ Yes ✓0 No 4 SKIP to Section 12.
0
E 11.2 List the information requested and attach it to this application.
1, 4.
2. 5.
3. 6.
EPA Form 3510-2C(Revised 3-19) Page 6

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
OMB No.2040-0004
NCD000830661 NC0003417 H.F.Lee Energy Complex
SECTION 12.CHECKLIST AND CERTIFICATION STATEMENT(40 CFR 122.22(a)and(d))
12.1 In Column 1 below, mark the sections of Form 2C that you have completed and are submitting with your application.
For each section,specify in Column 2 any attachments that you are enclosing to alert the permitting authority.Note
all sections or provide attachments.
that not all applicants are required to complete
PP
Column 1 Column 2
✓❑ Section 1:Outfall Location ✓❑ wl attachments
O Section 2:Line Drawing 0 wl line drawing 0 w/additional attachments
w/list of each user of
Q Section 3:Average Flows and 0 w/attachments ❑ privately owned treatment
Treatment works
❑ Section 4:Intermittent Flows ❑ w/attachments
0 Section 5:Production 0 w/attachments
w/optional additional
sheets describing any
❑ Section 6:Improvements 0 w/attachments 0 additional pollution control
plans
0 w/request for a waiver and ❑ wl explanation for identical
supporting information outfalls
0
/small business exemption
E request El w/other attachments
iii ❑ Section 7:Effluent and Intake 0 w/Table A ✓❑ w/Table B
Characteristics
R ✓❑ wl Table C
✓ wl Table D
w/analytical results as an
0 0 w/Table E ❑ attachment
c ❑ Section 8:Used or Manufactured ❑ w/attachments
-• Toxics
❑ Section 9:Biological Toxicity ❑ w/attachments
d
s Tests
U
0 Section 10:Contract Analyses 0 w/attachments
❑ Section 11:Additional Information ❑ w/attachments
❑ Section 12:Checklist and El Section attachments
Certification Statement
12.2 Certification Statement
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who manage the system,or those persons directly
responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the
possibility of fine and imprisonment for knowing violations.
Name(print or type first and last name) Official title
Jeffrey Hines GM II-Regulated Station
Sign a ?/_... Date signed
' /z,
EPA Form 3510-2C(Revised 3-19) Page 7

TABLE A. CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(iii))1 OUTFALL 001
Effluent Intake(optional)
Pollutant Maximum Maximum Long-Term Long Term
Waiver Daily Monthly Average Daily Number of Average
Analyses
Number of
Requested Units Discharge Discharge Discharge y Value Analyses
(if applicable) (specify) (required) (if available) (if available)
❑ Check here if you have applied to your NPDES permitting authority for a waiver for all of the pollutants listed on this table for the noted outfall.
Biochemical oxygen demand El
mg/L <2.0 1 2.0
1 (BODS)
Mass lb/Day <4.89 1
Concentration mg/L <20 1 <20 1
2. Chemical oxygen demand(COD)
Mass lb/Day <48.9 1
Enter INTAKE flow below
Concentration mg/L 3.1 1 3.1 1 if you want to calculate
3. Total organic carbon(TOC)
lb/Day
Mass lb/Day 7.58 1
Concentration mg/L <2.5 1 <2.5 1 0.293
4. Total suspended solids(TSS) ii
Mass lb/Day <6.11 1
Concentration mg/L <0.10 1 <0.10 1
5. Ammonia(as N) 71
Mass lb/Day <0.24 1
6. Flow ❑ Rate MGD 0.293 1
Temperature(winter) ❑ C °C
7.
Temperature(summer) ❑ °C C 29.4 1
pH(minimum) ❑ Standard Units s.u. 8.6 1
8.
pH(maximum) ❑ Standard Units s.u. 8.6 1

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 001
Presence or Absence Intake
Effluent(check one) (optional)
Pollutant/Parameter Units Long-Term
(and CAS Number,if Testing (specify) Maximum Maximum Average Long- Number
available) Required Believed Believed Daily Monthly Daily Number of Term of
Present Absent Analyses Average Analyses
Discharge Discharge Discharge Value y
(required) (if available) (if available)
Check here if you qualify as a small business per the instructions to Form 2C and,therefore,do not need to submit quantitative data for any of the organic toxic pollutants in Sections 2
through 5 of this table. Note,however,that you must still indicate in the appropriate column of this table if you believe any of the pollutants listed are present in your discharge.
Section 1.Toxic Metals,Cyanide,and Total Phenols
Concentration ug/L 2.40 1 2.40 1
1.1 Antimony,total(7440-36-0) E E ❑ Mass lb/Day 0.00587 1
Concentration ug/L 5.12 1 5.12 1
1.2 Arsenic,total(7440-38-2) 2 0
Mass lb/Day 0.0125 1
Concentration ug/L <1 1 <1 1
1.3 Beryllium,total(7440-41-7) E ❑
Mass lb/Day <0.00245 1
Concentration ug/L <0.1 1 <0.1 1
1.4 Cadmium,total(7440-43-9) E 0
Mass lb/Day <0.000245 1
Concentration ug/L <1 1 <1 1
1.5 Chromium,total (7440-47-3) 0 0
Mass lb/Day <0.00245 1
Concentration ug/L <2 1 <2 1
1.6 Copper,total(7440-50-8) 0 ❑
Mass lb/Day <0.00489 1
Concentration ug/L <1 1 <1 1
1.7 Lead,total(7439-92-1) E 0 0
Mass lb/Day <0.00245 1
Concentration ng/L <0.500 1 <0.500 1
1.8 Mercury,total(7439-97-6) 0 ❑ 0
Mass lb/Day <0.00000122 1
Concentration ug/L 2.20 1 2.20 1
1.9 Nickel,total(7440-02-0) 0 E ❑ Mass lb/Day 0.00538 1
Concentration ug/L 29.9 1 29.9 1
1.10 Selenium,total(7782-49-2) 2 E
Mass lb/Day 0.0731 1
Concentration ug/L <1 1 <1 1
1.11 Silver,total(7440-22-4) E D
Mass lb/Day <0.00245 1

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 001
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant/Parameter Units Long-Term
Testing _
(and CAS Number,if available) (specify) Maximum Maximum Average Long Number
Required Believed Believed Number of Term
Present Absent Daily Monthly Daily Analyses Average of
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
Concentration ug/L 0.349 1 0.349 1
1.12 Thallium,total(7440-28-0) 0 0 0
-
Mass lb/Day 0.000853 1
Concentration mg/L <0.005 1 <0.005 1
1.13 Zinc,total(7440-66-6) 0 0 0
Mass lb/Day <0.0122 1
Concentration mg/L <0.010 1 <0.010 1
1.14 Cyanide,total(57-12-5) 0 0 0
Mass lb/Day <0.0245 1
Concentration ug/L <1.6 1 <1.6 1
1.15 Phenols,total 0 0 0
Mass lb/Day <0.00391 1
Section 2.Organic Toxic Pollutants(GC/MS Fraction-Volatile Compounds)
2.1 Acrolein(107-02-8) Concentration ug/L <5.0 1 <5.0 1
Mass lb/Day <0.0122 1
2.2 Acrylonitrile(107-13-1) Concentration ug/L <5.0 1 <5.0 1
0 0 Mass lb/Day <0.0122 1
Concentration ug/L <1.0 1 <1.0 1
2.3 Benzene(71-43-2) 0 0 0
Mass lb/Day <0.00245 1
•
Concentration ug/L <1.0 1 <1.0 1
2.4 Bromoform(75-25-2) 0 0 0
Mass lb/Day <0.00245 1
Concentration ug/L <1.0 1 <1.0 1
2.5 Carbon tetrachloride(56-23-5) 0 0 0
Mass lb/Day <0.00245 1
Concentration ug/L <1.0 1 <1.0 1
2.6 Chlorobenzene(108-90-7) 0 0 0
Mass lb/Day <0.00245 1
Chlorodibromomethane Concentration ug/L <1.0 1 <1.0 1
2.7 (124-48-1) 0 0 0
Mass lb/Day <0.00245 1
Concentration ug/L <2.0 1 <2.0 1
2.8 Chloroethane(75-00-3) 0 0 0
Mass lb/Day <0.00489 1

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 001
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant/Parameter Units Long-Term
Testing Long
-
(and CAS Number,if available) (specify) Maximum Maximum Average Number
Required Believed Believed Number of Term
Present Absent Daily Monthly Daily of
Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
2-chloroethylvinyl ether Concentration ug/L <5.0 1 <5.0 1
2.9 (110-75-8) 0 ❑ ❑ Mass lb/Day <0.0122 1
Concentration ug/L <1.0 1 <1.0 1
2.10 Chloroform(67-66-3) 2 ❑ El Mass lb/Day <0.00245 1
Dichlorobromomethane Concentration ug/L <1.0 1 <1.0 1
2.11 (75 27-4) 0 ❑ E
Mass lb/Day <0.00245 1
Concentration ug/L <1.0 1 <1.0 1
2.12 1,1-dichloroethane(75-34-3) E ❑
Mass lb/Day <0.00245 1
Concentration ug/L <1.0 1 <1.0 1
2.13 1,2-dichloroethane(107-06-2) E ❑ E
Mass lb/Day <0.00245 1
2.14 1,1-dichloroethylene(75-35-4) Concentration ug/L <1.0 1 <1.0 1
❑ Mass lb/Day <0.00245 1
Concentration ug/L <1.0 1 <1.0 1
2.15 1,2-dichloropropane(78-87-5) E ❑
Mass lb/Day <0.00245 1
1,3-dichloropropylene Concentration ug/L <1.0 1 <1.0 1
2.16 El ❑ E
(542-75-6) Mass lb/Day <0.00245 1
Concentration ug/L <1.0 1 <1.0 1
2.17 Ethylbenzene(100-41-4) E ❑ EMass lb/Day <0.00245 1
Concentration ug/L <2.0 1 <2.0 1
2.18 Methyl bromide(74-83-9) E ❑ 0 Mass lb/Day <0.00489 1
Concentration ug/L <2.0 1 <2.0 1
2.19 Methyl chloride(74-87-3)
❑ ❑ ❑ Mass lb/Day <0.00489 1
Concentration ug/L <1.0 1 <1.0 1
2.20 Methylene chloride(75-09-2) E ❑ 0
Mass lb/Day <0.00245 1
1,1,2,2-tetrachloroethane Concentration ug/L <1.0 1 <1.0 1
2.21 (79-34-5) 0 ❑ Mass lb/Day <0.00245 1

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 001
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant/Parameter Units Long-Term
Testing Long
(and CAS Number,if (specify) Maximum Maximum Average Number
available) Required Believed Believed Number of Term
Daily Monthly Daily of
Present Absent Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
Tetrachloroethylene Concentration ug/L <1.0 1 <1.0 1
2.22 (127-18-4) Mass lb/Day <0.00245 1
Concentration ug/L <1.0 1 <1.0 1
2.23 Toluene(108-88-3) E 0 0
Mass lb/Day <0.00245 1
1,2-trans-dichloroethylene Concentration ug/L <1.0 1 <1.0 1
2.24 (156-60-5) Mass lb/Day <0.00245 1
1,1,1-trichloroethane Concentration ug/L <1.0 1 <1.0 1
2.25 (71-55-6) Mass lb/Day <0.00245 1
1,1,2-trichloroethane Concentration ug/L <1.0 1 <1.0 1
2.26 (79-00-5) Mass lb/Day <0.00245 1
Concentration ug/L <1.0 1 <1.0 1
2.27 Trichloroethylene(79-01-6) 0 0 E
Mass lb/Day <0.00245 1
Concentration ug/L <1.0 1 <1.0 1
2.28 Vinyl chloride(75-01-4) E 0 E
Mass lb/Day <0.00245 1
Section 3.Organic Toxic Pollutants(GC/MS Fraction-Acid Components)
Concentration ug/L <1.6 1 <1.6 1
3.1 2-chlorophenol(95-57-8) 0 ❑ E
Mass lb/Day <0.00391 1
2,4-dichlorophenol Concentration ug/L <1.6 1 <1.6 1
3.2 (120-83-2) Mass lb/Day <0.00391 1
2,4-dimethylphenol Concentration ug/L <1.6 1 <1.6 1
3.3 (105-67-9) 0 0
Mass lb/Day <0.00391 1
3.4 4,6-dinitro-o-cresol Concentration ug/L <8.0 1 <8.0 1
(534-52-1) Mass lb/Day <0.0196 1
Concentration ug/L <8.0 1 <8.0 1
3.5 2,4-dinitrophenol(51-28-5) 0 ❑
Mass lb/Day <0.0196 1

TABLE B.TOXIC METALS, CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 001
Presence or Absence Intake
Effluent
(check one) (optional)
Pollutant/Parameter Units Long-Term
Testing Long
(and CAS Number, if (specify) Maximum Maximum Average Number
available) Required Believed Believed Number of Term
Daily Monthly Daily of
Present Absent Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
2-nitrophenol Concentration ug/L <3.2 1 <3.2 1
3.6
(88-75-5) F_I I J E] Mass lb/Day <0.00782 1
4-nitrophenol Concentration ug/L <8.0 1 <8.0 1
3.7 (100-02-7) H Mass lb/Day <0.0196 1
3.8 p-chloro-m-cresol Concentration ug/L <1.6 1 <1.6 1
(59-50-7) ❑ Mass lb/Day <0.00391 1
Pentachlorophenol Concentration ug/L <8.0 1 <8.0 1
3.9 (87-86-5) ' Mass lb/Day <0.0196 1
Phenol Concentration mg/L <0.0050 1 <0.0050 1
3.10
(108-95-2) - ❑ Mass lb/Day <0.0122 1
2,4,6-trichlorophenol Concentration ug/L <1.6 1 <1.6 1
3.11 1:: 1-7 f�l
(88-05-2) Mass lb/Day <0.00391 1
Section 4.Organic Toxic Pollutants(GC/MS Fraction-Base/Neutral Compounds)
Acenaphthene Concentration ug/L <1.6 1 <1.6 1
4.1 2 ❑ ❑�
(83-32-9) Mass lb/Day <0.00391 1
Acenaphthylene Concentration ug/L <1.6 1 <1.6 1
4.2 (208-96-8) 0 ❑ 0 Mass lb/Day <0.00391 1
Concentration ug/L <1.6 1 <1.6 1
4.3 Anthracene(120-12-7) 2 ❑
Mass lb/Day <0.00391 1
Concentration ug/L <8.0 1 <8.0 1
4.4 Benzidine(92-87-5) 2 ❑ 0 Mass lb/Day <0.0196 1
Benzo(a)anthracene Concentration ug/L <1.6 1 <1.6 1
4.5 2 ❑ 0
(56-55-3) Mass lb/Day <0.00391 1
Benzo(a)pyrene Concentration ug/L <1.6 1 <1.6 1
4.6 (50-32-8) H ❑ H Mass lb/Day <0.00391 1

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFIZ 122.21(g)(7)(v))1 OUTFALL 001
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant/Parameter Units Long-Term
Testing
(and CAS Number,if available) (specify) Maximum Maximum Average Long- Number
Required Believed Believed Number of Term
Present Absent Daily Monthly Daily Analyses Average of
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
3,4-benzofluoranthene Concentration ug/L <1.6 1 <1.6 1
4.7
(205-99-2) Mass lb/Day <0.00391 1
Concentration ug/L <1.6 1 <1.6 1
4.8 Benzo(ghi)perylene(191-24-2)
❑ ❑ Mass lb/Day <0.00391 1
4.9 Benzo(k)fluoranthene(207-08- Concentration ug/L <1.6 1 <1.6 1
9) Mass lb/Day <0.00391 1
4.10 Bis(2-chloroethoxy)methane Concentration ug/L <1.6 1 <1.6 1
(111-91-1) 0 Mass lb/Day <0.00391 1
4.11 Bis(2-chloroethyl)ether(111-44- Concentration ug/L <1.6 1 <1.6 1
4) Mass lb/Day <0.00391 1
4.12 Bis(2-chloroisopropyl)ether(102 Concentration ug/L <1.6 1 <1.6 1
80-1) Mass lb/Day <0.00391 1
4.13 Bis(2-ethylhexyl)phthalate(117- Concentration ug/L <8.0 1 <8.0 1
81-7) Mass lb/Day <0.0196 1
4.14 4-bromophenyl phenyl ether(101. Concentration ug/L <1.6 1 <1.6 1
55-3) 2 E Mass lb/Day <0.00391 1
Concentration ug/L <1.6 1 <1.6 1
4.15 Butyl benzyl phthalate(85-68-7) 0
Mass lb/Day <0.00391 1
Concentration ug/L <1.6 1 <1.6 1
4.16 2-chloronaphthalene(91-58-7) E 0
Mass lb/Day <0.00391 1
4.17 4-chlorophenyl phenyl ether Concentration ug/L <1.6 1 <1.6 1
(7005-72-3) LI ❑ Mass lb/Day <0.00391 1
4.18 Chrysene(218 01-9) Concentration ug/L <1.6 1 <1.6 1
� E Mass lb/Day <0.00391 1
4.19 Dibenzo(a,h)anthracene(53-70- Concentration ug/L <1.6 1 <1.6 1
3) LI ❑ 0 Mass lb/Day <0.00391 1

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 001
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Units Long-Term
Testing Lon
(and CAS Number,if (specify) Maximum Maximum Average g Number
available) Required Believed Believed Number of Term
Daily Monthly Daily of
Present Absent Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
1,2-dichlorobenzene Concentration ug/L <1.0 1 <1.0 1
4.20 E � 2 -
(95-50-1) Mass lb/Day <0.00245 1
1,3-dichlorobenzene Concentration ug/L <1.0 1 <1.0 1
4.21 (541-73-1) E ❑ E
Mass lb/Day <0.00245 1
1,4-dichlorobenzene Concentration ug/L <1.0 1 <1.0 1
4.22 (106-46-7) Mass lb/Day <0.00245 1
3,3-dichlorobenzidine Concentration ug/L <8.0 1 <8.0 1
4.23 ❑ ❑ ❑
(91-94-1)
Mass lb/Day <0.0196 1
Diethyl phthalate Concentration ug/L <1.6 1 <1.6 1
❑ ❑ ❑
4.24 (84 66 2)
Mass lb/Day <0.00391 1
Dimethyl phthalate Concentration ug/L <1.6 1 <1.6 1
4.25 (131-11-3) 0 Mass lb/Day <0.00391 1
Di-n-butyl phthalate Concentration ug/L <1.6 1 <1.6 1
4.26 0 ❑ E
(84-74-2) Mass lb/Day <0.00391 1
2,4-dinitrotoluene Concentration ug/L <3.2 1 <3.2 1
4.27 ❑ ❑ ❑
(121-14-2) Mass lb/Day <0.00782 1
2,6-dinitrotoluene Concentration ug/L <3.2 1 <3.2 1
4.28 ❑ ❑ ❑
(606 20 2)
Mass lb/Day <0.00782 1
Di-n-octyl phthalate Concentration ug/L <1.6 1 <1.6 1
❑ ❑ ❑
4.29 (117 84 0)
Mass lb/Day <0.00391 1
1,2-Diphenylhydrazine Concentration ug/L <1.6 1 <1.6 1
4.30 (as azobenzene)(122-66-7) 0 Mass lb/Day <0.00391 1
Fluoranthene Concentration ug/L <1.6 1 <1.6 1
4.31 2 ❑ 0
(206-44-0) Mass lb/Day <0.00391 1
Fluorene Concentration ug/L <1.6 1 <1.6 1
4.32 (86 73 7) E � E
Mass lb/Day <0.00391 1

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 001
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Units Long-Term
Testing Long
(and CAS Number, if (specify) Maximum Maximum Average Number
available) Required Believed Believed Number of Term
Daily Monthly Daily of
Present Absent Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
Hexachlorobenzene Concentration ug/L <1.6 1 <1.6 1
4.33 E ❑ E
(118-74-1) Mass lb/Day <0.00391 1
Hexachlorobutadiene Concentration ug/L <1.6 1 <1.6 1
❑ ❑ ❑
4.34 (87 68 3)
Mass lb/Day <0.00391 1
1
Hexachlorocyclopentadiene Concentration ug/L <8.0 1 <8.0 1
4.35 (77-47-4) Mass lb/Day <0.0196 1
Hexachloroethane Concentration ug/L <1.6 1 <1.6 1
4.36 (67 72 1) 0 Mass lb/Day <0.00391 1
Indeno(1,2,3-cd)pyrene Concentration ug/L <1.6 1 <1.6 1
4.37 (193395) 0 ❑ E
Mass lb/Day <0.00391 1
Isophorone Concentration ug/L <1.6 1 <1.6 1
4.38 (78 59 1) 2 ❑ 2
Mass lb/Day <0.00391 1
Naphthalene Concentration ug/L <1.6 1 <1.6 1
4.39 E ❑ E
(91-20-3) Mass lb/Day <0.00391 1
Nitrobenzene Concentration ug/L <1.6 1 <1.6 1
4.40 1=1 ❑ 2
(98-95-3) Mass lb/Day <0.00391 1
N-nitrosodimethylamine Concentration ug/L <1.6 1 <1.6 1
4.41 (62 75 9) Mass lb/Day <0.00391 1
N-nitrosodi-n-propylamine Concentration ug/L <1.6 1 <1.6 1
4.42 (621-64-7) 0 � 2
Mass lb/Day <0.00391 1
N-nitrosodiphenylamine Concentration ug/L <1.6 1 <1.6 1
4.43 (86-30-6) 0 ❑ 2
Mass lb/Day <0.00391 1
Phenanthrene Concentration ug/L <1.6 1 <1.6 1
4.44 (85 01 8) 2 ❑ 2
Mass lb/Day <0.00391 1
Pyrene Concentration ug/L <1.6 1 <1.6 1
4.45 (129-00-0) Mass lb/Day <0.00391 11

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uogealueouoo 100-,b'17 L 9
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9 5
uo!lanueouo3 euepaolq
ssew El J (8-98-61E) 9.9
uouu.quaouoO OH8-4
ssew (6-68-89) .9
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uolleJluaouo3 OH8-°
ssew (Z-00-60E)
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TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 001
Presence or Absence Intake
Effluent
(check one) (optional)
Pollutant/Parameter Units Long-Term
Testing
(and CAS Number, if (specify) Maximum Maximum Average Long- Number
available) Required Believed Believed Number of Term
Daily Monthly Daily of
Present Absent Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
(3-endosulfan _ Concentration
5.12 Li 1
(115-29-7) Mass
5.13 Endosulfan sulfate Concentration
ji
(1031-07-8) L . Mass
Endrin Concentration
5.14 (72-20-8) L-I E HI Mass
Endrin aldehyde Concentration
5.15 (7421-93-4) I-' L� HI Mass
Heptachlor Concentration
5.16 (76-44-8) H, - HI Mass
Heptachlor epoxide Concentration
5.17 ❑ LJ 2
(1024-57-3) Mass
PCB-1242 Concentration ug/L <0.40 1 <0.40 1
5.18 (53469-21-9) LJ - Mass lb/Day <0.000978 1
PCB-1254 Concentration ug/L <0.40 1 <0.40 1
5.19 11097 69 1 - -_
( ) �� Mass lb/Day <0.000978 1
PCB-1221 Concentration ug/L <0.40 1 <0.40 1
5.20 HI [II H
(1 1 1 04-28-2) Mass lb/Day <0.000978 1
PCB-1232 Concentration ug/L <0.40 1 <0.40 1
5.21 '_
(1 1 1 41-1 6-5) ' , 70 Mass lb/Day <0.000978 1
PCB-1248 Concentration ug/L <0.40 1 <0.40 1
5.22 �L L_L H
(12672-29-6) Mass lb/Day <0.000978 1
PCB-1260 Concentration ug/L <0.40 1 <0.40 1
5.23 (11096-82-5) Mass lb/Day <0.000978 1
PCB-1016 Concentration ug/L <0.40 1 <0.40 1
5.24 (12674-11-2) =L Mass lb/Day <0.000978 1

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 001
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant/Parameter Units Long-Term
Testing
(and CAS Number, if (specify) Maximum Maximum Average Long- Number
available) Required Believed Believed Number of Term
Daily MonthlyDailyof
Present Absent Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
Toxaphene Concentration
5.25 (8001-35-2) ❑
Mass

Presence or AbsenceII Intake
Effluent o tional
(check one) (optional)
Pollutant/Parameter Units Long-Term
(and CAS Number, if available) (specify) Maximum Maximum Average Long- Number
Believed Believed Number of Term
Present Absent Daily Monthly Daily of
Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
❑ Check here if you believe all pollutants on Table C to be present in your discharge from the noted outfall. You need not complete the"Presence or Absence"column of Table C for each pollutant.
❑ Check here if you believe all pollutants on Table C to be absent in your discharge from the noted outfall. You need not complete the"Presence or Absence"column of Table C for each pollutant.
Bromide Concentration mg/L 0.11 1 0.11 1
1. (24959-67-9) ❑ 0 Mass lb/Day 0.269 1
Chlorine,total Concentration mg/L <0.028 1 <0.028 1
2. residual Ell 0 Mass lb/Day <0.0685 1
Concentration color units 5.0 1 5.0 1
3. Color 0
Mass lb/Day 1
Concentration MPN/100mL 66.3 1 66.3 1
4. Fecal Coliform 0 0
Mass lb/Day 1
Fluoride Concentration mg/L 0.34 1 0.34 1
5' (16984-48-8) ❑ 0 Mass lb/Day 0.831 1
Concentration mg/L 0.022 1 0.022 1
6. Nitrate-nitrite 0
Mass lb/Day 0.0538 1
Nitrogen,total Concentration mg/L 0.282 1 0.282 1
7' organic(as N) 0 ❑ Mass lb/Day 0.689 1
Concentration mg/L <5 1 <5 1
8. Oil and Grease 0 0
Mass lb/Day <12.2 1
Phosphorus(as P), Concentration mg/L <0.050 1 <0.050 1
9' total(7723-14-0) ❑ 0 Mass lb/Day <0.122 1
Sulfate(as SO4) Concentration mg/L 83 1 83 1
10. (14808-79-8) 0 ❑ Mass lb/Day 203 1
Concentration mg/L <1.0 1 <1.0 1
11. Sulfide(as S) 0 0
Mass lb/Day <2.45 1

TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 001
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Units Long-Term
(and CAS Number, if (specify) Maximum Maximum Average Long- Number
available) Believed Believed Daily Monthly Daily Number of Term of
Present Absent Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
Sulfite(as SO3) Concentration mg/L 2.0 1 2.0 1
12' (14265 45 3) 0 ❑
Mass lb/Day 4.89 1
13. Surfactants Concentration mg/L <0.1 1 <0.1 1
E Mass lb/Day <0.0245 1
14 Aluminum,total Concentration mg/L 0.328 1 0.328 1
(7429-90-5) 0 Mass lb/Day 0.802 1
15 Barium,total Concentration mg/L 0.104 1 0.104 1
(7440-39-3) Mass lb/Day 0.254 1
Boron,total Concentration mg/L 1.05 1
16. ❑ ❑
(7440-42-8) Mass lb/Day 2.57 1
Cobalt,total Concentration ug/L <1 1 <1 1
17. (7440-48-4) Mass lb/Day <0.00245 1
Iron,total Concentration mg/L 0.047 1 0.047 1
18. (7439-89-6) Mass lb/Day 0.115 1
Magnesium,total Concentration mg/L 7.69 1 7.69 1
19. (7439-95-4) Mass lb/Day 18.8 1
20 Molybdenum,total Concentration ug/L 52.3 1 52.3 1
(7439-98-7) 0 Mass lb/Day 0.128 1
Manganese,total Concentration mg/L 0.056 1 0.056 1
21. (7439-96-5) 0 Mass lb/Day 0.137 1
22 Tin,total Concentration mg/L <0.01 1 <0.01 1
(7440 31 5) 0 EMass lb/Day <0.0245 1
Titanium,total Concentration mg/L <0.005 1 <0.005 1
23. (7440-32-6) Mass lb/Day <0.0122 1

TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(v))' OUTFALL 001
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant/Parameter Units Long-Term
(and CAS Number, if (specify) Maximum Maximum Average Long- Number
available) Believed Believed Daily Monthly Daily Number of Term of
Present Absent Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
24. Radioactivity
Concentration
Alpha,total
Mass
Concentration
Beta,total
Mass
Concentration
Radium,total `_
Mass
Concentration
Radium 226,total
Mass

TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(g)(7)(v))1 OUTFALL 001
Presence or Absence
(check one) Available Quantitative Data
Pollutant Reason Pollutant Believed Present in Discharge
Believed Believed (specify units)
Present Absent
1. Asbestos ❑ E
2. Acetaldehyde ❑ I
3. Allyl alcohol ❑ El
4. Allyl chloride ❑ E
5. Amyl acetate ❑ El
6. Aniline ❑ E
7. Benzonitrile ❑ E
8. Benzyl chloride ❑ E
9. Butyl acetate ❑ E
10. Butylamine ❑ 0
11. Captan ❑ E
12. Carbaryl ❑ El
13. Carbofuran ❑ CI
14. Carbon disulfide ❑ 0
15. Chlorpyrifos ❑ El
16. Coumaphos ❑ CI
17. Cresol ❑ El
18. Crotonaldehyde ❑ El
19. Cyclohexane ❑ El

TABLE D. CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(g)(7)(v))1 OUTFALL 001
Presence or Absence
(check one) Available Quantitative Data
Pollutant Reason Pollutant Believed Present in Discharge
Believed Believed (specify units)
Present Absent
20. 2,4-D (2,4-dichlorophenoxyacetic acid) ❑ ❑
21- Diazinon ❑ 0
22. Dicamba El ❑
23. Dichlobenil El El
24. Dichlone ❑ ❑
25. 2,2-dichloropropionic acid ❑ El
26. Dichlorvos ❑ El
27. Diethyl amine ❑ El
28 Dimethyl amine ❑ El
29. Dintrobenzene ❑ El
30- Diquat ❑ El
31. Disulfoton ❑ El
32. Diuron ❑ El
33. Epichlorohydrin ❑ 0
34. Ethion ❑ El
35. Ethylene diamine ❑ CI
36. Ethylene dibromide ❑ El
37. Formaldehyde ❑ El
38. Furfural El El

TABLE D. CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS 440 CFR 122.21(g)(7)(v))1 OUTFALL 001
Presence or Absence
(check one) Available Quantitative Data
Pollutant Reason Pollutant Believed Present in Discharge
Believed Believed (specify units)
Present Absent
39. Guthion ❑
40. Isoprene ❑ 0
41. Isopropanolamine ❑
42. Kelthane ❑
43- Kepone ❑ 0
44. Malathion ❑
45. Mercaptodimethur ❑ ❑
46. Methoxychlor ❑
47- Methyl mercaptan ❑
48. Methyl methacrylate ❑ 2
49. Methyl parathion ❑ 0
50. Mevinphos ❑ 2
51. Mexacarbate ❑ 0
52. Mo 0 n ethY I amine ❑ RI
53. Monomethyl amine ❑ RI
54. Naled ❑ RI
55. Naphthenic acid ❑ RI
56. Nitrotoluene ❑ RI
57 Parathion ❑ RI

TABLE D. CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(g)(7)(v))1 OUTFALL 001
Presence or Absence
(check one) Available Quantitative Data
Pollutant Reason Pollutant Believed Present in Discharge
Believed Believed (specify units)
Present Absent
58. Phenolsulfonate
59. Phosgene
60. Propargite 2
61. Propylene oxide
62. Pyrethrins ❑�
63. Quinoline
64. Resorcinol 0
65. Strontium ❑
66. Strychnine ❑ 0
67. Styrene
68. 2,4,5-T(2,4,5-
trichlorophenoxyacetic acid)
69. TDE(tetrachlorodiphenyl ethane)
70 2,4,5-TP[2-(2,4,5-trichlorophenoxy)
propanoic acid]
71. Trichlorofon ❑ 0
72. Triethanolamine ❑ L
73. Triethylamine ❑ LI
74. Trimethylamine 0
75. Uranium ❑ 0
76. Vanadium ❑ LI

TABLE D. CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS (40 CFR 122.21(g)(7)(v))1 OUTFALL 001
Presence or Absence
(check one) Available Quantitative Data
Pollutant Reason Pollutant Believed Present in Discharge
Believed Believed (specify units)
Present Absent
77. Vinyl acetate
78. Xylene
79. Xylenol
80. Zirconium
' Sampling shall be conducted according to sufficiently sensitive test procedures (i.e., methods) approved under 40 CFR 136 for the analysis of pollutants or pollutant
parameters or required under 40 CFR chapter I, subchapter N or O. See instructions and 40 CFR 122.21(e)(3).

TABLE E.2,3,7,8 TETRACHLORODIBENZO P DIOXIN(2,3,7,8 TCDD)(40 CFR 122.21(g)(7)(viii)) OUTFALL 001
TCDD Presence or Absence
Pollutant Congeners (check one) Results of Screening Procedure
Used or Believed Believed
Manufactured Present Absent
2,3,7,8-TCDD1 ❑ LI
Sampling shall be conducted according to sufficiently sensitive test procedures (i.e., methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under
40 CFR chapter I,subchapter N or O. See instructions and 40 CFR 122.21(e)(3).

,
TABLE A. CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(iii))1 OUTFALL 002
Effluent Intake(optional)
Pollutant Maximum Maximum Long-Term Long Term
Waiver Daily Monthly Average Daily Number of Average Number of
Requested Units Discharge Discharge Discharge Analyses Value Analyses
(if applicable) (specify) (required) (if available) (if available)
0 Check here if you have applied to your NPDES permitting authority for a waiver for all of the pollutants listed on this table for the noted outfall.
Biochemical oxygen demand Concentration mg/L 2.6 1 2.6 1
1. 0
(RODS)
Mass lb/Day
Concentration mg/L 34 1 34 1
2. Chemical oxygen demand(COD) ❑
Mass lb/Day
Enter INTAKE flow below
Concentration mg/L 3.1 1 3.1 1 if you want to calculate
3. Total organic carbon(TOC) ❑ lb/Day
Mass lb/Day
Concentration mg/L <2.5 1 <2.5 1 Intake Flow Here
4. Total suspended solids(TSS) ❑
Mass lb/Day
Concentration mg/L 0.12 1 0.12 1
5. Ammonia(as N) ❑
Mass lb/Day
6. Flow ❑ Rate Enter Flow
Here
Temperature(winter) ❑ °C °C
7.
Temperature(summer) 0 °C °C 31.8 1
pH(minimum) 0 Standard Units s.u. 7.8 1
8.
pH(maximum) 0 Standard Units s.u. 7.8 1

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))' OUTFALL 002
Presence or Absence Intake
Effluent
(check one) (optional)
Pollutant/Parameter Units Long-Term
(and CAS Number,if Testing (specify) Maximum Maximum Average Long- Number
available) Required Believed Believed Number of Term
Daily Monthly Daily of
Present Absent Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
111
Check here if you qualify as a small business per the instructions to Form 2C and,therefore,do not need to submit quantitative data for any of the organic toxic pollutants in Sections 2
through 5 of this table.Note,however,that you must still indicate in the appropriate column of this table if you believe any of the pollutants listed are present in your discharge.
Section 1.Toxic Metals,Cyanide,and Total Phenols
Concentration ug/L 2.4 1 2.4 1
1.1 Antimony,total(7440-36-0) ❑ 0 ❑ Mass lb/Day
Concentration ug/L 5.12 1 5.12 1
1.2 Arsenic,total(7440-38-2) 0 2 ❑ Mass lb/Day
Concentration ug/L <1 1 <1 1
1.3 Beryllium,total(7440-41-7) 2 ❑ E Mass lb/Day
Concentration ug/L <0.1 1 <0.1 1
1.4 Cadmium,total(7440-43-9) 2 ❑ 2 Mass lb/Day
Concentration ug/L <1 1 <1 1
1.5 Chromium,total(7440-47-3) 0 ❑ E Mass lb/Day
Concentration ug/L <2 1 <2 1
1.6 Copper,total(7440-50-8) 2 ❑ 0 Mass lb/Day
Concentration ug/L <1 1 <1 1
1.7 Lead,total(7439-92-1) 2 ❑ 0 Mass lb/Day
Concentration ng/L 1.79 1 1.79 1
1.8 Mercury,total(7439-97-6) 2 2 ❑ Mass lb/Day
Concentration ug/L 2.2 1 2.2 1
1.9 Nickel,total(7440-02-0) 0 2 ❑ Mass lb/Day
Concentration ug/L 29.9 1 29.9 1
1.10 Selenium,total(7782-49-2) Q 2 ❑
Mass lb/Day
Concentration ug/L <1 1 <1 1
1.11 Silver,total(7440-22-4) 2 ❑
Mass Ib/Day

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))' OUTFALL 002
Presence or Absence Intake
Effluent(check one) (optional)
Pollutant/Parameter Units Long-Term
(and CAS Number,if available) Testing (specify) Maximum Maximum Average Long- Number
Required Believed Believed Number of Term
Present Absent Daily Monthly Daily of
Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
Concentration ug/L 0.349 1 0.349 1
1.12 Thallium,total(7440-28-0) 0 ❑ C
Mass lb/Day
Concentration mg/L <0.005 1 <0.005 1
1.13 Zinc,total(7440-66-6) E ❑ 2 Mass lb/Day
Concentration mg/L <0.010 1 <0.010 1
1.14 Cyanide,total(57-12-5) Q ❑ 0 Mass lb/Day
Concentration ug/L <8.0 1 <8.0 1
1.15 Phenols,total 0 ❑ El Mass lb/Day
Section 2.Organic Toxic Pollutants(GC/MS Fraction-Volatile Compounds)
Concentration ug/L <5.0 1 <5.0 1
2.1 Acrolein(107-02-8) Ti. El0 -
Mass lb/Day
Concentration ug/L <5.0 1 <5.0 1
2.2 Acrylonitrile(107-13-1) ❑ ❑ 0
Mass lb/Day
Concentration ug/L <1.0 1 <1.0 1
2.3 Benzene(71-43-2) ❑ ❑ ❑
Mass lb/Day
Concentration ug/L <1.0 1 <1.0 1
2.4 Bromoform(75-25-2) 7 ❑
Mass lb/Day
Concentration ug/L <1.0 1 <1.0 1
2.5 Carbon tetrachloride(56-23-5) 0 ❑ 2 Mass lb/Day
Concentration ug/L <1.0 1 <1.0 1
2.6 Chlorobenzene(108-90-7) 0 ❑ E Mass lb/Day
Chlorodibromomethane Concentration ug/L <1.0 1 <1.0 1
2.7 (124-48-1) ❑ Mass lb/Day
Concentration ug/L <2.0 1 <2.0 1
2.8 Chloroethane(75-00-3) 0 ❑
Mass lb/Day

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 002
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Units Long-Term
(and CAS Number,if available) Testing (specify) Maximum Maximum Average Long- Number
Required Believed Believed Number of Term
Present Absent Daily Monthly Daily of
Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
2-chloroethylvinyl ether Concentration ug/L <5.0 1 <5.0 1
2.9 (110-75-8) 0 El 0 Mass lb/Day
Concentration ug/L <1.0 1 <1.0 1
2.10 Chloroform(67-66-3) 0 ❑
Mass lb/Day
Dichlorobromomethane Concentration ug/L <1.0 1 <1.0 1
2.11 (75-27-4) Mass lb/Day
Concentration ug/L <1.0 1 <1.0 1
2.12 1,1-dichloroethane(75-34-3) 0 0
Mass lb/Day
Concentration ug/L <1.0 1 <1.0 1
2.13 1,2-dichloroethane(107-06-2) 0 0
Mass lb/Day
Concentration ug/L <1.0 1 <1.0 1
2.14 1,1-dichloroethylene(75-35-4) 2 ❑ 0
Mass lb/Day
Concentration ug/L <1.0 1 <1.0 1
2.15 1,2-dichloropropane(78-87-5) 0 ❑ 0
Mass lb/Day
1,3-dichloropropylene Concentration ug/L <1.0 1 <1.0 1
2.16 (542-75 6) El 0 El
Mass lb/Day
Concentration ug/L <1.0 1 <1.0 1
2.17 Ethylbenzene(100-41-4) 0 0 0
Mass lb/Day
Concentration ug/L <2.0 1 <2.0 1
2.18 Methyl bromide(74-83-9) 0 ❑ 0
Mass lb/Day
Concentration ug/L <2.0 1 <2.0 1
2.19 Methyl chloride(74-87-3) 0 0 0
Mass lb/Day
Concentration ug/L <1.0 1 <1.0 1
2.20 Methylene chloride(75-09-2) 0 0 0
Mass lb/Day
1,1,2,2-tetrachloroethane Concentration ug/L <1.0 1 <1.0 1
2.21 (79345) 0 ❑ El
Mass lb/Day

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))' OUTFALL 002
Presence or Absence Intake
Effluent
(check one) (optional)
Pollutant/Parameter Units Long-Term
Testing Lon
(and CAS Number,if (specify) Maximum Maximum Average g Number
available) Required Believed Believed Number of Term
Daily Monthly Daily of
Present Absent Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
Tetrachloroethylene Concentration ug/L <1.0 1 <1.0 1
2.22 (127-18-4) 0 ❑ 0
Mass lb/Day
Concentration ug/L <1.0 1 <1.0 1
2.23 Toluene(108-88-3) 0 ❑ 0 Mass lb/Day
1,2-trans-dichloroethylene Concentration ug/L <1.0 1 <1.0 1
2.24 El(156-60-5) ❑ Mass lb/Day
1,1,1-trichloroethane Concentration ug/L <1.0 1 <1.0 1
2.25 El(71-55-6) ❑ Mass lb/Day
1,1,2-trichloroethane Concentration ug/L <1.0 1 <1.0 1
2.26 0 ❑ 0
(79-00-5) Mass lb/Day
Concentration ug/L <1.0 1 <1.0 1
2.27 Trichloroethylene(79-01-6) 0 ❑ 0
Mass lb/Day
Concentration ug/L <1.0 1 <1.0 1
2.28 Vinyl chloride(75-01-4) 0 ❑ 0
Mass lb/Day
Section 3.Organic Toxic Pollutants(GC/MS Fraction-Acid Components)
Concentration ug/L <8.0 1 <8.0 1
3.1 2-chlorophenol(95-57-8) 0 ❑ 0 Mass lb/Day
2,4-dichlorophenol Concentration ug/L <8.0 1 <8.0 1
3.2 (120-83-2) CI ❑ 0
Mass lb/Day
2,4-dimethylphenol Concentration ug/L <8.0 1 <8.0 1
3.3 (105-67-9) CI 0 Mass lb/Day
4,6-dinitro-o-cresol Concentration ug/L <40 1 <40 1
3.4 (534-52-1) ❑ ❑ 0 Mass lb/Day
Concentration ug/L <40 1 <40 1
3.5 2,4-dinitrophenol(51-28-5) 0 ❑ 0
Mass lb/Day

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 002
Presence or Absence Intake
Effluent
(check one) (optional)
Pollutant/Parameter Units Long-Term
(and CAS Number, if Testing (specify) Maximum Maximum Average Long- Number
available) Required Believed Believed Number of Term
Daily Monthly Daily of
Present Absent Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
2-nitrophenol Concentration ug/L <16 1 <16 1
3.6 0 El0 '
(88-75-5) Mass lb/Day
4-nitrophenol Concentration ug/L <40 1 <40 1
3.7 (100-02-7) 0 ❑ 0
Mass lb/Day
p-chloro-m-cresol Concentration ug/L <8.0 1 <8.0 1
3.8 (59-50-7) ❑ ❑ 0 Mass lb/Day
Pentachlorophenol Concentration ug/L <40 1 <40 1
3.9 (87-86-5) �' ❑ 0 Mass lb/Day
`Phenol Concentration mg/L <0.0050 1 <0.0050 1
3.10
(108-95-2) ❑ ❑ 0 Mass lb/Day
2,4,6-trichlorophenol Concentration ug/L <8.0 1 <8.0 1
3.11 (88-05-2) u ❑ 0 Mass lb/Day
Section 4.Organic Toxic Pollutants(GC/MS Fraction-Base/Neutral Compounds)
Acenaphthene Concentration ug/L <8.0 1 <8.0 1
4.1 (83-32-9) C — 0 Mass lb/Day
Acenaphthylene Concentration ug/L <8.0 1 <8.0 1
4'2 (208-96-8) ❑ 0 Mass lb/Day
Concentration ug/L <8.0 1 <8.0 1
4.3 Anthracene(120-12-7) 2 ❑ 0 Mass lb/Day
Concentration ug/L <40 1 <40 1
4.4 Benzidine(92-87-5) 0 ❑ 0
Mass lb/Day
Benzo(a)anthracene Concentration ug/L <8.0 1 <8.0 1
4.5 0 ❑ 0
(56 55 3) Mass lb/Day
Benzo(a)pyrene Concentration ug/L <8.0 1 <8.0 1
4.6 (50328) 0 ❑ ❑�
Mass lb/Day

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 002
Presence or Absence Intake
Effluent(check one) (optional)
P )
Pollutant/Parameter Units Long-Term
(and CAS Number,if available) Testing (specify) Maximum Maximum Average Long- Number
Required Believed Believed Number of Term
Present Absent Daily Monthly Daily y g of
Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
3,4-benzofluoranthene Concentration ug/L <8.0 1 <8.0 1
4.7 (205-99-2) ❑ Mass lb/Day
Concentration ug/L <8.0 1 <8.0 1
4.8 Benzo(ghi)perylene(191-24-2) 0 ❑
Mass lb/Day
Benzo(k)fluoranthene(207-08- Concentration ug/L <8.0 1 <8.0 1
4.9 9) ❑ Mass lb/Day
Bis(2-chloroethoxy)methane Concentration ug/L <8.0 1 <8.0 1
4.10 (111 91 1) ❑ Mass lb/Day
Bis(2-chloroethyl)ether(111-44- Concentration ug/L <8.0 1 <8.0 1
4.11 4) ❑ Mass lb/Day
Bis(2-chloroisopropyl)ether(102 Concentration ug/L <8.0 1 <8.0 1
4.12 80-1) ❑ Mass lb/Day
Bis(2-ethylhexyl)phthalate(117- Concentration ug/L <40 1 <40 1
4.13 81-7) ❑ Mass lb/Day
4-bromophenyl phenyl ether(101. Concentration ug/L <8.0 1 <8.0 1
4.14 El
55-3) 0 ❑ Mass lb/Day
Concentration ug/L <8.0 1 <8.0 1
4.15 Butyl benzyl phthalate(85-68-7) 2 ❑ E Mass lb/Day
Concentration ug/L <8.0 1 <8.0 1
4.16 2-chloronaphthalene(91-58-7) 2 ❑ 0
Mass lb/Day
4-chlorophenyl phenyl ether Concentration ug/L <8.0 1 <8.0 1
4.17 (7005-72-3) ❑ Mass lb/Day
Concentration ug/L <8.0 1 <8.0 1
4.18 Chrysene(218-01-9) E ❑
Mass lb/Day
Dibenzo(a,h)anthracene(53-70- Concentration ug/L <8.0 1 <8.0 1
4.19
3) 2 0 2 Mass lb/Day

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 002
Presence or Absence Intake
Effluent(check one) (optional)
Pollutant/Parameter Units Long-Term
(and CAS Number,if Testing (specify) Maximum Maximum Average Long- Number
available) Required Believed Believed Daily Monthly Daily Number of Term of
Present Absent Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
1,2-dichlorobenzene Concentration ug/L <1.0 1 <1.0 1
4.20 (95-50-1) ❑ Mass lb/Day
1,3-dichlorobenzene Concentration ug/L <1.0 1 <1.0 1
4.21 (541-73-1) 0 ❑ Mass lb/Day
1,4-dichlorobenzene Concentration ug/L <1.0 1 <1.0 1
4.22 0 ❑ Mass lb/Day
(106-46-7)
3,3-dichlorobenzidine Concentration ug/L <40 1 <40 1
4.23 (91-94-1) ❑ Mass lb/Day
Diethyl phthalate Concentration ug/L <8.0 1 <8.0 1
4.24 (84-66-2) ❑ Mass lb/Day _
Dimethyl phthalate Concentration ug/L <8.0 1 <8.0 1
4.25 0 ❑ Mass lb/Day
(131-11 3)
Di-n-butyl phthalate Concentration ug/L <8.0 1 <8.0 1
4.26 (84 74 2) ❑ Mass lb/Day
2,4-dinitrotoluene Concentration ug/L <16 1 <16 1
4.27 ❑ Mass lb/Day
(121 14 2)
2,6-dinitrotoluene Concentration ug/L <16 1 <16 1
4.28 (606-20-2) 0 Mass lb/Day
Di-n-octyl phthalate Concentration ug/L <8.0 1 <8.0 1
4.29 (117 84 0) ❑ Mass lb/Day
1,2-Diphenylhydrazine Concentration ug/L <8.0 1 <8.0 1
4.30 (as azobenzene) (122-66-7) E ❑ Mass lb/Day
Fluoranthene Concentration ug/L <8.0 1 <8.0 1
4.31 (206-44-0) ElMass lb/Day
Fluorene Concentration ug/L <8.0 1 <8.0 1
4.32 (86 73 7) ❑ Mass lb/Day

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 002
Presence or Absence Intake
Effluent(check one) (optional)
Pollutant/Parameter Units Long-Term
(and CAS Number, if Testing (specify) Maximum Maximum Average Long- Number
available) Required Believed Believed Daily Monthly Daily Number of Term of
Present Absent Analyses Average Analyses
Discharge Discharge Discharge Value Y
(required) (if available) (if available)
Hexachlorobenzene Concentration ug/L <8.0 1 <8.0 1
4.33 (118 74 1) E ❑ 0
Mass lb/Day
4.34 Hexachlorobutadiene J Concentration ug/L <8.0 1 <8.0 1
❑
(87-68-3) Mass lb/Day
Hexachlorocyclopentadiene Concentration ug/L <40 1 <40 1
4.35 (77 47 4) ❑ ❑ Mass lb/Day
Hexachloroethane Concentration ug/L <8.0 1 <8.0 1
4.36 (67 72 1) 0 ❑ Mass lb/Day
Indeno(1,2,3-cd)pyrene Concentration ug/L <8.0 1 <8.0 1
4.37 (193-39-5) 0 ❑ Mass lb/Day
Isophorone Concentration ug/L <8.0 1 <8.0 1
4.38 (78-59-1) ❑ Mass lb/Day
Naphthalene Concentration ug/L <8.0 1 <8.0 1
4.39 (91-20-3) 2 ❑ 0
Mass lb/Day
Nitrobenzene Concentration ug/L <8.0 1 <8.0 1
4.40 (98-95-3) ❑ Mass lb/Day
N-nitrosodimethylamine Concentration ug/L <8.0 1 <8.0 1
4.41 (62 75 9) ❑ Mass lb/Day
N-nitrosodi-n-propylamine Concentration ug/L <8.0 1 <8.0 1
4.42 L ❑ L1
(621-64-7) Mass lb/Day
N-nitrosodiphenylamine Concentration ug/L <8.0 1 <8.0 1
4.43 (86-30-6) ❑ Mass lb/Day
Phenanthrene Concentration ug/L <8.0 1 <8.0 1
4.44 (85-01-8) ❑ Mass lb/Day
Pyrene Concentration ug/L <8.0 1 <8.0 1
4.45 (129-00-0) ❑ Mass lb/Day

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR.122.21(g)(7)(v))' OUTFALL 002
Presence or Absence Intake
Effluent(check one) (optional)
Pollutant/Parameter Units Long-Term
Testing Long-
(and CAS Number, if Required (specify) Maximum Maximum Average Number
9 Believed Believed g Number of Term
available) Present Absent Daily Monthly Daily Analyses Average of
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
1,2,4-trichlorobenzene Concentration ug/L <8.0 1 <8.0 1
4.46 (120 82 1) ❑ 0 Mass Ib/Day
Section 4.Organic Toxic Pollutants(GC/MS Fraction-Base/Neutral Compounds)
' Aldrin Concentration
5.1 (309-00-2) ❑ ❑ ❑ Mass
a-BHC Concentration
5.2 (319-84-6) ❑ ❑ Mass
R-BHC Concentration
5.3 (319-85-7) ❑ ❑ ❑ Mass
y-BHC Concentration
5.4 (58 89 9) ❑ ❑ Mass
O-BHC Concentration
5.5 (319-86-8) ❑ ❑ Mass
Chlordane Concentration
5.6 (57 74 9) ❑ ❑ Mass
4,4'-DDT Concentration
5.7 (50-29-3) ❑ ❑ Mass
4,4'-DDE Concentration
5.8 (72-55-9) El ❑ ❑ Mass
4,4'-DDD Concentration
5.9 (72-54-8) ❑ ❑ 0 Mass
Dieldrin Concentration
5.10 ❑ ❑ ❑
(60-57-1) Mass
a-endosulfan Concentration
5.11 ❑ ❑ ❑
(115-29-7) Mass

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 002
Presence or Absence Intake
Effluent
(check one) (optional)
Pollutant/Parameter Units Long-Term
(and CAS Number, if Testing (specify) Maximum Maximum Average Long- Number
available) Required Believed Believed Number of Term
Daily Monthly Daily of
Present Absent Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
(3-endosulfan Concentration
5.12 (115297) ❑ ❑ E
Mass
Endosulfan sulfate Concentration
5.13 (1031 07 8) ❑ 0
Mass
Endrin Concentration
5.14 ❑ 2
(72-20-8) Mass
Endrin aldehyde Concentration
5.15 (7421 93 4) ❑ 2
Mass
Heptachlor Concentration
5.16 (76-44-8) ❑ 0 E
Mass
Heptachlor epoxide Concentration
5.17 (1024-57-3) Ell ❑ 0
Mass
PCB-1242 Concentration ug/L <0.40 1 <0.40 1
5.18 (53469-21-9) Mass lb/Day
PCB-1254 Concentration ug/L <0.40 1 <0.40 1
5.19 (11097-69-1) Mass lb/Day
PCB-1221 Concentration ug/L <0.40 1 <0.40 1
5.20 (11104282) 2 ❑ 0
Mass lb/Day
PCB-1232 Concentration ug/L <0.40 1 <0.40 1
5.21 (11141-16-5) 0 ❑ LI
Mass lb/Day
PCB-1248 Concentration ug/L <0.40 1 <0.40 1
5.22 (12672-29-6) Mass lb/Day
PCB-1260 Concentration ug/L <0.40 1 <0.40 1
5.23 (11096-82-5) Mass lb/Day
PCB-1016 Concentration ug/L <0.40 1 <0.40 1
5.24 (12674-11-2) 0 LI
Mass lb/Day

TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 002
Presence or Absence Intake
Effluent
(check one) (optional)
Pollutant/Parameter Units Long-Term
-
(and CAS Number, if Testing (specify) Maximum Maximum Average Long Number
available) Required Believed Believed Number of Term
Daily Monthly Daily of
Present Absent Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
Toxaphene Concentration
5.25 (8001 35 2) ❑ � 2
Mass

Presence or Absence Intake
Effluent o tional
(check one) (optional)
Pollutant/Parameter Units Long-Term
(and CAS Number, if available) (specify) Maximum Maximum Average Long- Number
Believed Believed Daily Monthly Daily Number of Term of
Present Absent Analyses Average
Discharge Discharge Discharge Value Analyses
(required) (if available) (if available)
❑ Check here if you believe all pollutants on Table C to be present in your discharge from the noted outfall. You need not complete the"Presence or Absence"column of Table C for each pollutant.
❑ Check here if you believe all pollutants on Table C to be absent in your discharge from the noted outfall. You need not complete the"Presence or Absence"column of Table C for each pollutant.
Bromide Concentration mg/L 0.11 1 0.11 1
1. 24959 67 9 2 ❑
( ) Mass lb/Day
Chlorine,total Concentration ug/L <10 1 <10 1
2. ❑ ❑
residual Mass lb/Day
HUIVI I
Concentration alp <25 1 <25 1
3. Color ❑
Mass lb/Day
Concentration MPN/100mL 101.7 1 101.7 1
4. Fecal Coliform 0 ❑
Mass lb/Day
Fluoride Concentration mg/L 0.34 1 0.34 1
5. (16984-48-8) ❑ 0 Mass lb/Day
Concentration mg/L 0.20 1 0.20 1
6. Nitrate-nitrite 0 ❑
Mass lb/Day
Nitrogen,total Concentration mg/L 1.3 1 1.3 1
7. organic(as N) 0 ❑ Mass lb/Day
Concentration mg/L <5 1 <5 1
8. Oil and Grease ❑ 0
Mass lb/Day
9 Phosphorus(as P), Concentration mg/L 0.054 1 0.054 1
total (7723-14-0) ❑ ❑ Mass lb/Day
Sulfate(as SO4) Concentration mg/L 83 1 83 1
10. (14808-79-8) 0 ❑ Mass lb/Day
Concentration mg/L <1.0 1 <1.0 1
11. Sulfide(as S) 0 0 Mass lb/Day

TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 002
Presence or Absence Intake
Effluent
(check one) (optional)
Pollutant/Parameter Units Long-Term
Long-
(and CAS Number, if (specify) Maximum Maximum Average Number
available) Believed Believed Daily Monthly Daily Number of Term of
Present Absent Analyses Average
Discharge Discharge Discharge Analyses
Value
(required) (if available) (if available)
Sulfite (as S03) Concentration mg/L <2.0 1 <2.0 1
12. (14265-45-3) 0 Mass lb/Day
Concentration mg/L <0.1 1 <0.1 1
13. Surfactants ❑ 0
Mass lb/Day
Aluminum,total Concentration mg/L 0.328 1 0.328 1
14. (7429-90-5) Mass lb/Day
Barium,total Concentration mg/L 0.104 1 0.104 1
15. (7440-39-3) 0 Mass lb/Day
Boron,total Concentration mg/L 1.05 1 1.05 1
16. (7440-42-8) Mass lb/Day
Cobalt,total Concentration ug/L <1 1 <1 1
17. (7440-48-4) Mass lb/Day
Iron,total Concentration mg/L 0.047 1 0.047 1
18. (7439-89-6) Mass lb/Day
Magnesium,total Concentration mg/L 7.69 1 7.69 1
19' (7439-95-4) 2 0 Mass lb/Day
Molybdenum,total Concentration ug/L 52.3 1 52.3 1
20. (7439-98-7) Mass lb/Day
Manganese,total Concentration mg/L 0.056 1 0.056 1
21. (7439-96-5) 0 Mass lb/Day
Tin,total Concentration mg/L <0.01 1 <0.01 1
22. (7440-31-5) Mass lb/Day
Titanium,total Concentration mg/L 0.005 1 0.005 1
23. (7440-32-6) 0 Mass lb/Day

TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(v))1 OUTFALL 002
Presence or Absence Intake
Effluent
(check one) (optional)
Pollutant/Parameter Units Long-Term
(and CAS Number, if (specify) Maximum Maximum Average Long- Number
Number of Term
available) Believed Believed Daily Monthly Daily of
Present Absent Analyses Average Analyses
Discharge Discharge Discharge Value y
(required) (if available) (if available)
24. Radioactivity
Concentration
Alpha,total ❑
Mass
Concentration
Beta, total ❑
Mass
Concentration
Radium,total ❑
Mass
Concentration
Radium 226,total El 2 Mass

TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(g)(7)(v))1 OUTFALL 002
Presence or Absence
(check one) Available Quantitative Data
Pollutant Reason Pollutant Believed Present in Discharge
Believed Believed (specify units)
Present Absent
1- Asbestos ❑ E
2. Acetaldehyde ❑ ❑
3. Allyl alcohol ❑ ❑
4. Allyl chloride ❑ L
5- Amyl acetate ❑ [
6. Aniline ❑ L
7. Benzonitrile ❑ LI
8. Benzyl chloride ❑ 0
9. Butyl acetate ❑ LI
10. Butylamine ❑ LI
11. Captan ❑ 0
12- Carbaryl ❑ 2
13. Carbofuran ❑ LI
14. Carbon disulfide ❑ 0
15- Chlorpyrifos ❑ LI
16. Coumaphos ❑ 0
17_ Cresol ❑ LI
18. Crotonaldehyde ❑ LI
19. Cyclohexane ❑ E

TABLE D. CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(g)(7)(v))1 OUTFALL 002
Presence or Absence
(check one) Available Quantitative Data
Pollutant Reason Pollutant Believed Present in Discharge
Believed Believed (specify units)
Present Absent
20. 2,4-D (2,4-dichlorophenoxyacetic acid) ❑ ❑
21. Diazinon ❑
22. Dicamba ❑
23. Dichlobenil ❑
24. Dichlone ❑ 0
25. 2,2-dichloropropionic acid ❑
26. Dichlorvos ❑ ❑
27. Diethyl amine ❑ ❑
28 Dimethyl amine ❑
29. Dintrobenzene ❑ L7
30. Diquat ❑
31. Disulfoton ❑ 0
32. Diuron ❑
33. Epichlorohydrin ❑ 0
34. Ethion ❑
35. Ethylene diamine ❑ 0
36. Ethylene dibromide ❑
37. Formaldehyde ❑
38. Furfural ❑ ❑

TABLE D. CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS$40 CFR 122.21(g)(7)(v))' OUTFALL 002
Presence or Absence
(check one) Available Quantitative Data
Pollutant Reason Pollutant Believed Present in Discharge
Believed Believed (specify units)
Present Absent
39- Guthion ❑
40. Isoprene ❑
41. Isopropanolamine ❑
42. Kelthane ❑
43- Kepone ❑ 0
44- Malathion ❑
45- Mercaptodimethur ❑ 0
46. Methoxychlor ❑ 0
47. Methyl mercaptan ❑ 0
48. Methyl methacrylate ❑ 21
49. Methyl parathion ❑ 0
50. Mevinphos ❑ 0
51. Mexacarbate ❑ 0
52. Monoethyl amine ❑ 21
53. Monomethyl amine ❑ ❑
54. Naled ❑ 21
55. Naphthenic acid ❑ 21
56. Nitrotoluene ❑ 0
57 Parathion ❑ 21

TABLE D. CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(g)(7)(v))1 OUTFALL 002
Presence or Absence
(check one) Available Quantitative Data
Pollutant Reason Pollutant Believed Present in Discharge
Believed Believed (specify units)
Present Absent
58. Phenolsulfonate ❑
59. Phosgene ❑ ❑Q
60. Propargite ❑ ❑�
61. Propylene oxide ❑
62. Pyrethrins ❑ ❑�
63. Quinoline ❑ ❑✓
64. Resorcinol ❑
65. Strontium ❑ ❑�
66. Strychnine ❑
67. Styrene ❑ ❑�
68. 2,4,5-T(2,4,5- ❑ ❑
trichlorophenoxyacetic acid)
69. TDE (tetrachlorodiphenyl ethane) ❑ ❑
70 2,4,5-TP[2-(2,4,5-trichlorophenoxy) ❑ ❑
propanoic acid]
71. Trichlorofon ❑
72. Triethanolamine ❑ ❑�
73. Triethylamine ❑ 0
74. Trimethylamine ❑ ❑✓
75. Uranium ❑ ❑✓
76. Vanadium ❑ ❑✓

TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(g)(7)(v))1 OUTFALL 002
Presence or Absence
(check one) Available Quantitative Data
Pollutant Reason Pollutant Believed Present in Discharge
Believed Believed (specify units)
Present Absent
77. Vinyl acetate ❑ ❑✓
78. Xylene ❑ 2
79. Xylenol ❑ ❑�
80. Zirconium ❑ 2
' Sampling shall be conducted according to sufficiently sensitive test procedures (i.e., methods) approved under 40 CFR 136 for the analysis of pollutants or pollutant
parameters or required under 40 CFR chapter I, subchapter N or O. See instructions and 40 CFR 122.21(e)(3).

TABLE E.2,3,7,8 TETRACHLORODIBENZO P DIOXIN(2,3,7,8 TCDD)(40 CFR 122.21(g)(7)(viii)) OUTFALL 002
TCDD Presence or Absence
Pollutant Congeners (check one)
Used or Results of Screening Procedure
Believed Believed
Manufactured Present Absent
2,3,7,8-TCDD ❑ ❑ E
'Sampling shall be conducted according to sufficiently sensitive test procedures(i.e., methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or required under
40 CFR chapter I,subchapter N or O. See instructions and 40 CFR 122.21(e)(3).

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex 005b OMB No.2040-0004
TABLE A.CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(iii))1
Effluent Intake
Waiver (Optional)
Pollutant Requested Units Maximum Maximum Long-Term
(if applicable) (specify) Daily Monthly Average Daily Number of Long-Term Number of
Discharge Discharge Discharge Analyses Average Value Analyses
(required) (if available) (if available)
❑ Check here if you have applied to your NPDES permitting authority for a waiver for all of the pollutants listed on this table for the noted outfall.
Biochemical oxygen demand Concentration mg/L <2.0 1 <2.0 1
1. El(BOD5) Mass lbs/day <2.2 1
Chemical oxygen demand Concentration mg/L <20 1 <20 1
2. (COD) ❑ Mass lbs/day <21.5 1
Concentration mg/L 2.7 1 2.7 1
3. Total organic carbon(TOC) ❑
Mass lbs/day 2.9 1
Concentration mg/L 11 1 11 1
4. Total suspended solids(TSS) ❑
Mass lbs/day 11.8 1
Concentration mg-N/L <0.10 1 <0.10 1
5. Ammonia(as N) 0
Mass lbs/day <0.108 1
6. Flow ❑ Rate MGD 0.129 1
Temperature(winter) 0 °C °C
7.
Temperature(summer) ❑ °C °C 31.9 1
pH(minimum) ❑ Standard units s.u. 7.7 1
I 8
pH(maximum) ❑ Standard units s.u. 7.7 1
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 9

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex 005b OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Daily of Term of
Discharge Discharge Discharge Analyses Average Analyses
(required) (if available) Value
(if available)
Check here if you qualify as a small business per the instructions to Form 2C and,therefore,do not need to submit quantitative data for any of the organic toxic pollutants in Sections
2 through 5 of this table.Note,however,that you must still indicate in the appropriate column of this table if you believe any of the pollutants listed are present in your discharge.
Section 1.Toxic Metals,Cyanide,and Total Phenols
1.1 Antimony,total � Concentration ug/L <1.0 1 <1.0 1
(7440-36-0) ✓ Mass Ibs/day <0.00108 1
1.2 Arsenic,total O 0 Concentration ug/L 5.45 1 5.45 1
0(7440-38-2) Mass lbs/day 0.00587 1
Beryllium,total0 Concentration ug/L <1.0 1 <1.0 1
1.3 0 0
(7440-41-7) Mass lbs/day <0.00108 1
1.4 Cadmium,total 0 Concentration ug/L <0.1 1 <0.1 1
0 0
(7440-43-9) Mass lbs/day <0.000108 1
1.5 Chromium,total 0 Concentration ug/L <1.0 1 <1.0 1
(7440-47-3) Mass lbs/day <0.00108 1
1.6 Copper,total 0 Concentration ug/L <2.0 1 <2.0 1
El El
(7440-50-8) Mass lbs/day <0.00215 1
1.7 Lead,total 0 Concentration ug/L <1.0 1 <1.0 1
El El
(7439-92-1) Mass lbs/day <0.00108 1
1.8 Mercury,total 00 Concentration ng/L 0.952 1 0.952 1
(7439-97-6) ✓ Mass lbs/day 0.00000102 1
1 9 Nickel,total 0 Concentration ug/L 1.88 1 1.88 1
El l
(7440-02-0) ✓ Mass lbs/day 0.00202 1
Selenium,total0 Concentration ug/L 7.82 1 7.82 1
1.10 (7782-49-2) Mass lbs/day 0.00842 1
1.11 Silver,total 0 Concentration ug/L <1.0 1 <1.0 1
0 0
(7440-22-4) Mass lbs/day <0.00108 1
EPA Form 3510-2C(Revised 3-19) Page 11

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex 005b OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long-
Number
Present Absent Daily Monthly Daily of Term of
Discharge Discharge Discharg(if Analyses AverageValue Analyses
(required) (if available) available)e
Thallium,total Concentration ug/L 0.848 1 0.848 1
1.12 El 0
(7440-28-0) Mass lbs/day 0.000913 1
1.13 Zinc,total ❑ 0
❑ Concentration mg/L 0.021 1 0.021 1
(7440-66-6) Mass lbs/day 0.0226 1
1.14 Cyanide,total ❑ ❑ ❑ Concentration mg/L <0.006 1 <0.006 1
(57-12-5) Mass lbs/day <0.0064 1
Concentration ug/L 3.0 1 3.0 1
1.15 Phenols,total ❑✓ 0 0
Mass lbs/day 0.00323 1
Section 2.Organic Toxic Pollutants(GCIMS Fraction-Volatile Compounds)
2.1 Acrolein El ❑ 0
Concentration ug/L <5.0 1 <5.0 1
(107-02-8) Mass lbs/day <0.00538 1
2.2 Acrylonitrile El ❑ ❑ Concentration ug/L <5.0 1 <5.0 1
(107-13-1) Mass lbs/day <0.00538 1
2.3 Benzene El El Concentration ug/L <1.0 1 <1.0 1
(71-43-2) Mass lbs/day <0.00108 1
Bromoform 0 Concentration ug/L <1.0 1 <1.0 1
2.4 El(75-25-2) El lbs/day <0.00108 1
Carbon tetrachloride Concentration ug/L <1.0 1 <1.0 1
2.5 El(56-23-5) El Mass lbs/day <0.00108 1
2.6 Chlorobenzene CI ❑ 0 Concentration ug/L <1.0 1 <1.0 1
(108-90-7) Mass lbs/day <0.00108 1
2.7 Chlorodibromomethane El ❑ 0 Concentration ug/L <1.0 1 <1.0 1
(124-48-1) Mass lbs/day <0.00108 1
Chloroethane Concentration ug/L <2.0 1 <2.0 1
2.8 (75-00-3) ❑ 0 0 Mass lbs/day <0.00215 1
EPA Form 3510-2C(Revised 3-19) Page 12

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex 005b OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Daily of Term of
D(requiischa red)a D(if available)ischarge
Discharge Analyses AValuee Analyses
(if available)
2-chloroethylvinyl ether Concentration ug/L <5.0 1 <5.0 1
2.9 El El I:I
(110-75-8) Mass lbs/day <0.00538 1
Concentration ug/L <1.0 1 <1.0 1
2.10 Chloroform(67-66-3) ID ❑ ElMass lbs/day <0.00108 1
Dichlorobromomethane Concentration ug/L <1.0 1 <1.0 1
2.11 (75-27-4) Mass lbs/day <0.00108 1
1,1-dichloroethane Concentration ug/L <1.0 1 <1.0 1
2.12 El El El
(75-34-3) Mass lbs/dy <0.00108 1
2.13 1,2-dichloroethane Concentration ug/L <1.0 1 <1.0 1
El El
(107-06-2) ✓ Mass lbs/day <0.00108 1
2.14 1,1-dichloroethylene 0✓ Concentration ug/L <1.0 1 <1.0 1
(75-35-4) Mass lbs/day <0.00108 1
2.15 12-dichloropropane Concentration ug/L <1.0 1 <1.0 1
(78-87-5) Mass Lbs/day <0.00108 1
2.16 1,3-dichloropropylene Concentration ug/L <1.0 1 <1.0 1 El 0 El
(542-75-6) Mass lbs/day <0.00108 1
Ethylbenzene Concentration ug/L <1.0 1 <1.0 1
2.17 (100-41-4) Mass lbs/day <0.00108 1
2.18 Methyl bromide Concentration ug/L <2.0 1 <2.0 1
(74-83-9) ✓ Mass lbs/day <0.00215 1
2.19 Methyl chloride 0 Concentration ug/L <2.0 1 <2.0 1
(74-87-3) ✓ Mass lbs/day <0.00215 1
Methylene chloride Concentration ug/L <1.0 1 <1.0 1
2.20 (75-09-2) Mass lbs/day <0.00108 1
1,1,2,2-tetrachloroethane Concentration ug/L <1.0 1 <1.0 1
2.21 (79-34-5) 0 0 0 Mass lbs/day <0.00108 1
EPA Form 3510-2C(Revised 3-19) Page 13

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex 005b OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term Lon
(and CAS Number,if available) Required Believed Believed Maximum Maximum Long
-
(and (specify) Average Number Term Number
Daily Monthly
Present Absent Daily of of
Discharge Discharge Discharge Analyses Average Analyses
(required) (if available) Value
(if available)
Tetrachloroethylene Concentration ug/L <1.0 1 <1.0 1
2.22 (127-18-4) Mass lbs/day <0.00108 1
Toluene Concentration ug/L <1.0 1 <1.0 1
2.23 (108-88-3) Mass lbs/day <0.00108 1
2.24 1,2-trans-dichloroethylene Concentration ug/L <1.0 1 <1.0 1
(156-60-5) Mass lbs/day <0.00108 1
1,1,1-trichloroethane Concentration ug/L <1.0 1 <1.0 1
2.25 (71-55-6) Mass lbs/day <0.00108 1
2.26 1,1,2-trichloroethane Concentration ug/L <1.0 1 <1.0 1
El 0
(79-00-5) ✓ Mass lbs/day <0.00108 1
2.27 Trichloroethylene Concentration ug/L <1.0 1 <1.0 1
i2 El
(79-01-6) ✓ Mass lbs/day <0.00108 1
Vinyl chloride Concentration ug/L <1.0 1 <1.0 1
2.28 El El El
(75-01-4) Mass lbs/day <0.00108 1
Section 3.Organic Toxic Pollutants(GCIMS Fraction-Acid Compounds)
3.1 2-chlorophenol 0 Concentration ug/L <1.6 1 <1.6 1
(95-57-8) ✓ Mass lbs/day <0.00172 1
3.2 2,4-dichlorophenol Concentration ug/L <1.6 1 <1.6 1
(120-83-2) ✓ Mass lbs/day <0.00172 1
2,4-dimethylphenol Concentration ug/L <1.6 1 <1.6 1
3.3 (105-67-9) Mass lbs/day <0.00172 1
4,6-dinitro-o-cresol Concentration ug/L <8.0 1 <8.0 1
3.4 (534-52-1) Mass lbs/day <0.00861 1
2,4-dinitrophenol Concentration ug/L <8.0 1 <8.0 1
3.5 (51-28-5) Mass lbs/day <0.00861 1
EPA Form 3510-2C(Revised 3-19) Page 14

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex 005b OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Daily Monthly Term
Present Absent Daily of of
Discharge Discharge Discharge Analyses Average Analyses
(required) (if available) Value
(if available)
3.6 2-nitrophenol El 0
❑ Concentration ug/L <3.2 1 <3.2 1
(88-75-5) Mass lbs/day <0.00344 1
Concentration ug/L <8.0 1 <8.0 1
3.7 4-nitrophenol ❑ ❑ ❑ 9
(100-02-7) Mass lbs/day <0.00861 1
3.8 p-chloro-m-cresol ❑ 0 ❑ Concentration ug/L <1.6 1 <1.6 1
(59-50-7) Mass lbs/day <0.00172 1
Concentration ug/L <8.0 1 <8.0 1
3.9 Pentachlorophenol 0 ❑ ❑ 9 -
(87-86-5) Mass lbs/day <0.00861 <0.00861 1
Phenol Concentration ug/L 3.0 1 3.0 1
3.10 El 0 -
(108-95-2) Mass lbs/day 0.0032 1
3.11 2,4,6-trichlorophenol 0 ❑ ❑ Concentration ug/L <1.6 1 <1.6 1
(88-05-2) Mass lbs/day <0.00172 1
Section 4.Organic Toxic Pollutants(GC/MS Fraction-Base/Neutral Compounds)
4.1 Acenaphthene 0
❑ 0 Concentration ug/L <1.6 1 <1.6 1
(83-32-9) Mass lbs/day <0.00172 1
4.2 Acenaphthylene El 0
0 Concentration ug/L <1.6 1 <1.6 1
(208-96-8) Mass lbs/day <0.00172 1
4.3 Anthracene ❑ 0
0 Concentration ug/L <1.6 1 <1.6 1
(120-12-7) Mass lbs/day <0.00172 1
4.4 Benzidine 0
0
0 Concentration ug/L <8.0 1 <8.0 1
(92-87-5) Mass lbs/day <0.00861 1
Benzo(a)anthracene Concentration ug/L <1.6 1 <1.6 1
4.5 (56-55-3) ❑ 0 0 Mass lbs/day <0.00172 1
Benzo(a)pyrene Concentration ug/L <1.6 1 <1.6 1
4.6 El El El(50-32-8) Mass lbs/day <0.00172 1
EPA Form 3510-2C(Revised 3-19) Page 15

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex 005b OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Daily of Term of
Discharge Discharge Discharge Analyses Average Analyses
(required) (if available) Value
(if available)
4 7 3,4-benzofluoranthene ✓ 0Concentration ug/L <1.6 1 <1.6 1
(205-99-2) Mass lbs/day <0.00172 1
4 8 Benzo(ghi)perylene 0 0 Concentration ug/L <1.6 1 <1.6 1
El
(191-24-2) Mass lbs.day <0.00172 1
4.9 Benzo(k)fluoranthene El Concentration ug/L <1.6 1 <1.6 1
(207-08-9) Mass lbs/day <0.00172 1
Bis(2-chloroethoxy)methane 1:1Concentration ug/L <1.6 1 <1.6 1
4.10 El
(111-91-1) ✓ Mass lbs/day <0.00172 1
Bis(2-chloroethyl)ether 0 Concentration ug/L <1.6 1 <1.6 1
4.11 (111-44-4) Mass lbs/day <0.00172 1
4.12 Bis(2-chloroisopropyl)ether 0Concentration ug/L <1.6 1 <1.6 1
(102-80-1) Mass lbs/day <0.00172 1
4.13 Bis(2-ethylhexyl)phthalate � ❑ Concentration ug/L <8.0 1 <8.0 1
(117-81-7) Mass lbs/day <0.00861 1
4-bromophenyl phenyl ether 0 Concentration ug/L <1.6 1 <1.6 1
4.14 El D
(101-55-3) Mass lbs./ay <0.00172 1
4.15 Butyl benzyl phthalate 0Concentration ug/L <1.6 1 <1.6 1
(85-68-7) Mass lbs/day <0.00172 1
4.16 2-chloronaphthalene ✓ 0Concentration ug/L <1.6 1 <1.6 1
(91-58-7) Mass lbs/day <0.00172 1
4-chlorophenyl phenyl ether ✓ Concentration ug/L <1.6 1 <1.6 1
4.17 El 0
(7005-72-3) Mass lbs.day <0.00172 1
Chrysene 0 Concentration ug/L <1.6 1 <1.6 1
4.18 0 El
(218-01-9) Mass lbs/day <0.00172 1
Dibenzo(a,h)anthracene Concentration ug/L <1.6 1 <1.6 1
4.19 0 El El
(53-70-3) Mass lbs/day <0.00172 1
EPA Form 3510-2C(Revised 3-19) Page 16

EPA Identification Number NPDES Permit Number Facility Name Dutfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex 005b OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Daily Monthly Term
Present Absent Daily of of
Discharge Discharge Discharge Analyses Average Analyses
(required) (if available) Value
(if available)
4.20 1,2-dichlorobenzene 0 ✓� Concentration ug/L <1.0 1 <1.0 1
(95-50-1) Mass lbs.day <0.00108 1
1,3-dichlorobenzene Concentration ug/L <1.0 1 <1.0 1
4.21 El 0
(541-73-1) Mass lbs/day <0.00108 1
4.22 1,4-dichlorobenzene ❑ Concentration ug/L <1.0 1 <1.0 1
El El
(106-46-7) Mass lbs/day <0.00108 1
4.23 3,3-dichlorobenzidine � Concentration ug/L <8.0 1 <8.0 1
El El
(91-94-1) ✓ Mass lbs/day <0.00861 1
4.24 Diethyl phthalate © 0 Concentration ug/L <1.6 1 <1.6 1
(84-66-2) ✓ Mass lbs./ay <0.00172 1
4.25 Dimethyl phthalate 0Concentration ug/L <1.6 1 <1.6 1
El El
(131-11-3) Mass lbs./ay <0.00172 1
4.26 Di-n-butyl phthalate El � Concentration ug/L <1.6 1 <1.6 1
0
(84-74-2) ✓ Mass lbs/day <0.00172 1
4.27 2,4-dinitrotoluene 0Concentration ug/L <3.2 1 <3.2 1
El 0
(121-14-2) Mass lbs/day <0.00344 1
2,6-dinitrotoluene Concentration ug/L <3.2 1 <3.2 1
4.28 I:I El
(606-20-2) Mass lbs/day <0.00344 1
4.29 Di-n-octyl phthalate ✓� Concentration ug/L <1.6 1 <1.6 1
El
(117-84-0) ✓ Mass lbs/day <0.00172 1
4.30 1,2-Diphenylhydrazine ❑ Concentration ug/L <1.6 1 <1.6 1
l El
(as azobenzene)(122-66-7) ✓ Mass lbs/day <0.00172 1
4.31 Fluoranthene ❑ Concentration ug/L <1.6 1 <1.6 1
(206-44-0) ✓ Mass lbs/day <0.00172 1
4.32 Fluorene � Concentration ug/L <1.6 1 <1.6 1
El
(86-73-7) ✓ ✓ Mass lbs/day <0.00172 1
EPA Form 3510-2C(Revised 3-19) Page 17
L.

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex 005b OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Maximum I Maximum Long-Term Long-
(and CAS Number,if available) Required Believed Believed (specify) Daily Monthly Average Number Term Number
Present Absent Daily of of
Discharge Discharge Average
(required) (if available) Discharge Analyses Value Analyses
(if available)
Hexachlorobenzene Concentration ug/L <1.6 1 <1.6 1
4.33 (118-74-1) Mass lbs/day <0.00172 1
4.34 Hexachlorobutadiene Concentration ug/L <1.6 1 <1.6 1
El El
(87-68-3) ✓ Mass lbs/day <0.00172 1
4.35 Hexachlorocyclopentadiene 0 Concentration ug/L <8.0 1 <8.0 1
El
(77-47-4) ✓ Mass lbs/day <0.00861 1
4.36 Hexachloroethane Concentration ug/L <1.6 1 <1.6 1
0 El
(67-72-1) ✓ Mass lbs/day <0.00172 1
Indeno(1,2,3-cd)pyrene 0 El ✓ Concentration ug/L <1.6 1 <1.6 1
4.37 (193-39-5) Mass lbs/day <0.00172 1
4.38 Isophorone � 0Concentration ug/L <1.6 1 <1.6 1
(78-59-1) Mass lbs/day <0.00172 1
4.39 Naphthalene Concentration ug/L <1.6 1 <1.6 1
(91-20-3) ✓ Mass lbs/day <0.00172 1
4.40 Nitrobenzene 0 Concentration ug/L <1.6 1 <1.6 1
0 0
(98-95-3) Mass lbs/day <0.00172 1
N-nitrosodimethylamine 0 Concentration ug/L <1.6 1 <1.6 1
4.41 El 0
(62-75-9) Mass lbs/day <0.00172 1
4.42 N-nitrosodi-n-propylamine Concentration ug/L <1.6 1 <1.6 1
(621-64-7) Mass lbs.day <0.00172 _ 1
4.43 N-nitrosodiphenylamine 0
Concentration ug/L <1.6 1 <1.6 1
(86-30-6) Mass lbs/day <0.00172 1
4.44 Phenanthrene � Concentration ug/L <1.6 1 <1.6 1
El El
(85-01-8) ✓ Mass lbs.day <0.00172 1
Pyrene Concentration ug/L <1.6 1 <1.6 1
4.45 0 El El
(129-00-0) Mass lbs/day <0.00172 1
EPA Form 3510-2C(Revised 3-19) Page 18

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex 005b OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Daily of Term of
Discharge Discharge Discharge Analyses Average Analyses
(required) (if available) Value
(if available)
1,2,4-trichlorobenzene Concentration ug/L <1.6 1 <1.6 1
4.46 (120-82-1) El Mass lbs/day <0.00172 1
Section 5.Organic Toxic Pollutants(GCIMS Fraction—Pesticides)
El 0
5.1 Aldrin Concentration
(309-00-2) ✓ Mass
a-BHC Concentration
5.2 (319-84-6) Mass
3i-BHC Concentration
5.3 (319-85-7) Mass
y-BHC Concentration
5.4 (58-89-9) El ❑ Mass
6-BHC Concentration
5.5 (319-86-8) Mass
5.6 Chlordane ❑ Concentration
0 0
(57-74-9) Mass
5.7 4,4'-DDT Concentration
(50-29-3) ✓ Mass
4,4'-DDE ✓ Concentration
5.8 (72-55-9) Mass
5.9 4,4'-DDD 0 Concentration
El 0
(72-54-8) Mass
5.10 Dieldrin 0 Concentration
El 0
(60-57-1) Mass
a-endosulfan EI Concentration
5.11 El 0
(115-29-7) Mass
EPA Form 3510-2C(Revised 3-19) Page 19

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex 005b OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long Term Number
Present Absent Daily Monthly Daily of of
Discharge Discharge Discharge Analyses Average Analyses
(required) (if available) (if available) Value
5.12 13-endosulfan 0 Concentration
0 0
(115-29-7) Mass
5.13 Endosulfan sulfate 0 Concentration
El 0
(1031-07-8) Mass
5.14 Endrin Concentration
El 0 El
(72-20-8) Mass
5.15 Endrin aldehyde 0 Concentration
El 0
(7421-93-4) Mass
5.16 Heptachlor 0 0 0 Concentration
(76-44-8) Mass
Heptachlor epoxide ✓ Concentration
5.17 (1024-57-3) 0 El Mass
PCB-1242 Concentration ug/L <0.4 1 <0.4 1
5.18 (53469-21-9) 0 Mass lbs/day <0.00043 1
PCB-1254 0 Concentration ug/L <0.4 1 <0.4 1
5.19 (11097-69-1) 0 0
Mass lbs/day <0.00043 1
PCB-1221 Concentration ug/L <0.4 1 <0.4 1
5.20 (11104-28-2) 0 El
0 Mass lbs/day <0.00043 1
PCB-1232 Concentration ug/L <0.4 1 <0.4 1
5.21 (11141-16-5) 0 0 0 Mass lbs/day <0.00043 1
PCB-1248 Concentration ug/L <0.4 1 <0.4 1
5.22 (12672-29-6) 0 0 0 Mass lbs/day <0.00043 1
PCB-1260 Concentration ug/L <0.4 1 <0.4 1
5.23 (11096-82-5) 0 0 0
Mass lbs/day <0.00043 1
PCB-1016 0 Concentration ug/L <0.4 1 <0.4 1
5.24 (12674-11-2) 0 El
Mass lbs/day <0.00043 1
EPA Form 3510-2C(Revised 3-19) Page 20

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex 005b OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent (optional)
PollutantiParameter Testing Units Long-Term Long
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Number
Present Absent Daily Monthly Daily of Term of
Discharge Discharge Discharge Analyses' Average Analyses
(required) (if available) Value
(if available)
Toxaphene Concentration
5.25 (8001-35-2) 0 El El
Mass
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0. See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 21

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0000830661 NC0003417 HF Lee Energy Complex 001 OMB No.2040-0004
TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(vi))1
Presence or Absence Intake
(check one) Effluent (Optional)
Pollutant Units Maximum Long-Term
Believed Believed (specify) Maximum DailyLong-Term
Present Absent Discharge Monthly Average Daily Number of Average Number of
Discharge Discharge Analyses Analyses
(required) Value
(if available) (if available)
❑ Check here if you believe all pollutants on Table C to be present in your discharge from the noted outfall.You need not complete the"Presence or Absence"column of Table C for
each pollutant.
❑ Check here if you believe all pollutants on Table C to be absent in your discharge from the noted outfall.You need not complete the"Presence or Absence"column of Table C for
each pollutant.
Bromide 0 ❑✓ Concentration mg/L <0.2 1 <0.2 1
1' (24959-67-9) Mass lbs/day <0.215 1
2 Chlorine,total ❑ ❑ Concentration mg/L <0.028 1 <0.028 1
residual Mass lbs/day <0.0301 1
Concentration color units <10 1 <10 1
3. Color 0 ElMass lbs/day NA 1
Concentration MPN/100 67 1 67 1
4. Fecal coliform 0 ✓❑ Mass lbs/day NA 1
5 Fluoride 0 ❑ Concentration mg/L <0.2 1 <0.2 1
(16984-48-8) Mass lbs/day <0.215 1
Concentration mg-N/L <0.02 1 <0.02 1
6 Nitrate nitrite ❑ El
Mass lbs/day <0.0215 1
Nitrogen,total Concentration mg-N/L 0.24 1 0.24 1
7' organic(as N) ❑ Mass lbs/day 0.258 1
Concentration mg/L <5 1 <5 1
8. Oil and grease ❑ ✓❑
Mass mg/L <5.38 1
9 Phosphorus(as ❑ ❑ Concentration mg-P/L <0.050 1 <0.050 1
P),total(7723-14-0) Mass lbs/day <0.0538 1
10. Sulfate(as SO4) ❑✓ ❑ Concentration mg/L 86 1 86 1
(14808-79-8) Mass lbs/day 92.6 1
Concentration mg/L <1.0 1 <1.0 1
11. Sulfide(as S) 0 0Mass lbs/day <1.08 1
EPA Form 3510-2C(Revised 3-19) Page 23

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex 001 OMB No.2040-0004
TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(vi))l
Presence or Absence
(check one) Effluent Intake
(Optional)
Units
Pollutant Maximum Long-Term
Believed Believed (specify) Maximum Daily Long-Term
Present Absent Discharge Monthly Average Daily Number of Average Number of
Discharge Discharge Analyses Analyses
(required) Value
(if available) (if available)
12. Sulfite(as SO3) ❑ ✓❑ Concentration mg/L <2.0 1 <2.0 1
(14265-45-3) Mass lbs./ay <2.15 1
13. Surfactants Concentration mgMBAS/ <0.1 1 <0.1 1
Mass lbs/day <0.11 1
14, Aluminum,totalEl ❑ Concentration mg/L 8.37 1 8.37 1
(7429-90-5) Mass lbs/day 9.01 1
15. Barium,totalEl El Concentration mg/L 0.239 1 0.239 1
(7440-39-3) Mass lbs/day 0.257 1
0
18. Boron,total Concentration mg/L 0.252 1 0.252 1
(7440-42-8) El Mass lbs/day 0.271 1
17 Cobalt,total Concentration ug/L <1.0 1 <1.0 1
0 El
(7440-48-4) Mass lbs/day <0.00108 1
18 Iron,total Concentration mg/L 0.193 1 0.193 1
(7439-89-6) ✓ Mass lbs/day 0.208 1
19 Magnesium,total ❑✓ ❑ Concentration mg/L 2.53 1 2.53 1
(7439-95-0) Mass lbs/day 2.72 1
Molybdenum, Concentration ug/L 1.96 1 1.96 1
20. total 0 0(7439-98-7) Mass lbs/day 0.00211 1
21. Manganese,total ❑ El Concentration mg/L 0.41 1 0.41 1
(7439-96-5) Mass lbs/day 0.0441 1
22. Tin,total ❑ 0 Concentration mg/L <0.01 1 <0.01 1
(7440-31-5) Mass lbs/day <0.0108 1
23. Titanium,totalEl 0 Concentration mg/L 0.008 1 0.008 1
(7440-32-6) Mass lbs/day 0.00861 1
EPA Form 3510-2C(Revised 3-19) Page 24

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC000083O661 NC0003417 HF Lee Energy Complex 001 OMB No.2040-0004
TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(vi))1
Presence or Absence
(check one) Effluent Intake
(Optional)
Units
Pollutant Maximum Long-Term
Believed Believed (specify) Maximum Daily Long-Term
Present Absent Discharge Monthly Average Daily Number of Average Number of
Discharge Discharge Analyses Analyses
(required) Value
(if available) (if available)
24. Radioactivity
Concentration
Alpha,total ❑ ❑✓ Mass
Concentration
Beta,total 0 ❑✓ Mass
Concentration
Radium,total 0 ❑✓ Mass
Concentration
Radium 226,total ❑ 0 Mass
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 25

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex 001 OMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(g)(7)(vii))'
Presence or Absence
Pollutant (check one) Reason Pollutant Believed Present in Discharge Available Quantitative Data
Believed Believed (specify units)
Present Absent
1. Asbestos 0 ✓❑
2. Acetaldehyde 0 ✓❑
3. Ally!alcohol 0 ✓❑
4. Allyl chloride ❑ ✓❑
5. Amyl acetate 0 ✓❑
6. Aniline ❑ ✓❑
7. Benzonitrile ❑ ✓❑
8. Benzyl chloride ❑ ✓❑
9. Butyl acetate ❑ 0
10. Butylamine ❑ 0
11. Captan ❑ 0
12. Carbaryl 0 0
13. Carbofuran ❑ ✓❑
14. Carbon disulfide ❑ ✓❑
15. Chlorpyrifos 0 ✓❑
16. Coumaphos ❑ ✓❑
17. Cresol ❑ ✓❑
18. Crotonaldehyde ❑ ✓❑
19. Cyclohexane ❑ 0
EPA Form 3510-2C(Revised 3-19) Page 27

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex onOMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 12221(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Reason Pollutant Believed Present in Discharge Available Quantitative Data
Believed Believed (specify units)
Present Absent
20. 2,4-D(2,4-dichlorophenoxyacetic acid) ❑ ✓❑
21. Diazinon ❑ p
22. Dicamba ❑ ✓❑
23. Dichlobenil ❑ ✓❑
24. Dichlone ❑ ✓❑
25. 2,2-dichloropropionic acid 0 ❑✓
26. Dichlorvos 0 ✓❑
27. Diethyl amine ❑ El
28. Dimethyl amine ❑ 0
29. Dintrobenzene ❑ ❑✓
30. Diquat 0 ❑✓
31. Disulfoton 0 ✓❑
32. Diuron ❑ ✓❑
33. Epichlorohydrin 0 ✓❑
34. Ethion 0 ✓❑
35. Ethylene diamine ❑ ✓❑
36. Ethylene dibromide ❑ ✓❑
37. Formaldehyde ❑ ✓❑
38. Furfural 0 ✓❑
EPA Form 3510-2C(Revised 3-19) Page 28

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex 001 OMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 12221(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Reason Pollutant Believed Present in Discharge Available Quantitative Data
Believed Believed (specify units)
Present Absent
39. Guthion 0 ✓❑
40. Isoprene ❑ ✓❑
41. Isopropanolamine 0 ✓❑
42. Kelthane ❑ ✓❑
43. Kepone 0 ✓❑
44. Malathion 0 ✓❑
45. Mercaptodimethur 0 ✓❑
46. Methoxychlor ❑ ✓❑
47. Methyl mercaptan ❑ ✓❑
48. Methyl methacrylate 0 ❑✓
49. Methyl parathion 0 0
50. Mevinphos ❑ ✓❑
51. Mexacarbate 0 ✓❑
52. Monoethyl amine 0 0
53. Monomethyl amine 0 ✓❑
54. Naled 0 ✓❑
55. Naphthenic acid 0 ❑✓
56. Nitrotoluene 0 ✓❑
57. Parathion 0 ✓❑
EPA Form 3510-2C(Revised 3-19) Page 29

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex 001 OMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Reason Pollutant Believed Present in Discharge Available Quantitative Data
Believed Believed (specify units)
Present Absent
58. Phenolsulfonate 0 ✓❑
59. Phosgene ❑ ✓❑
60. Propargite ❑ ✓❑
61. Propylene oxide 0 ✓❑
62. Pyrethrins 0 ❑✓
63. Quinoline ❑ ✓❑
64. Resorcinol 0 0
65. Strontium ❑ ✓❑
66. Strychnine ❑ ✓❑
67. Styrene ❑ ❑✓
68. 2,4,5-T(2,4,5-trichlorophenoxyacetic ❑ ❑
acid)
69. TDE(tetrachlorodiphenyl ethane) 0 ✓❑
70. 2,4,5-TP[2-(2,4,5-trichlorophenoxy) ❑ ✓❑
propanoic acid]
71. Trichlorofon 0 ✓❑
72. Triethanolamine 0 ✓❑
73. Triethylamine 0 0
74. Trimethylamine 0 ❑✓
75. Uranium 0 ✓❑
76. Vanadium 0 ✓❑
EPA Form 3510-2C(Revised 3-19) Page 30

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex 001 OMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 12221(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Available Quantitative Data
Believed Believed Reason Pollutant Believed Present in Discharge (specify units)
Present Absent
77. Vinyl acetate ❑ p
78. Xylene 0 0
79. Xylenol ❑ 0
80. Zirconium 0 ✓❑
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 31

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCD000830661 NC0003417 HF Lee Energy Complex 001 OMB No.2040-0004
TABLE E.2,3,7,8 TETRACHLORODIBENZO P DIOXIN(2,3,7,8 TCDD)(40 CFR 122.21(g)(7)(viii))
TCDD Presence or
Congeners Absence
Pollutant (check one) Results of Screening Procedure
Used or
Manufactured Believed Believed
Present Absent
2,3,7,8-TCDD El ❑ ✓U
EPA Form 3510-2C(Revised 3-19) Page 33

H.F. Lee Combined Cycle Station
Supplemental Information - NC0003417
Introduction and Background
The H.F. Lee Energy Complex consists of 3 combined cycle combustion turbines brought online in 2012.
Also, located on the site is the Wayne County Combustion Turbine Plant/Site which consists of 5 simple
cycle combustion turbines,four of them brought online in 2000 and the fifth in 2009. Altogether,the five
Y g
simple cycle combustion turbines and the three combined cycle combustion turbines generate a total
electric capacity of over 1800 Megawatts. All units are capable of firing oil and natural gas.
Previously,the H.F. Lee Energy Complex had three coal-fired units and four oil-fueled combustion turbine
units. These were retired in September and October of 2012. The coal-fired generating units and the four
oil-fueled combustion turbines have been demolished and the coal pile has been removed. The Active
and Inactive Ash Basins are currently being dewatered to allow for ash excavated.
Outfall Descriptions
Outfall 001 —Active Ash Basin (Phase II Ash Pond Dewaterina and Groundwater Extraction)
No process wastewater flows are being sent to the active ash basin. The active ash basin is being
dewatered to accommodate the excavation and beneficiation of ash. Wastewater from the dewatering
process will contain stormwater,groundwater, and interstitial water.
A bioreactor has been installed for treatment to remove Selenium, as needed. Sludge removed from the
bioreactor will be shipped off-site for disposal at a facility permitted to accept this waste.
Outfa11001 —Active Ash Basin (Phase Ill-Groundwater Extraction)
After completing the decanting and dewatering of the ash basin, groundwater remediation may be
required. If treatment of the groundwater is required,the groundwater will be treated as a waste stream
to the ash ponds (for treatment through WTS), direct treatment through the WTS or direct treatment
through a dedicated groundwater treatment system.
Outfalls 002 and 002A—Cooling Pond
The facility uses an existing 545 acre closed-cycle cooling pond with baffled dikes to treat recirculating
condenser cooling and process water. Approximately 369 MG of condenser cooling water is recirculated
per day. Water is withdrawn from the Neuse River, as required, to make up evaporative, seepage and
discharge losses from the cooling pond. Discharges from the cooling pond is rare, usually only during an
extremely heavy rainfall or a hurricane. Up to12.7 MGD can be withdrawn from the Neuse River as make-
up water.
In addition to the recirculating condenser cooling, other wastewaters sent to the cooling pond include:
H.F. Lee Combined Cycle
During routine maintenance, the water treatment plant may be drained to the cooling pond to allow for
inspection of the clarifier. This activity typically occurs annually but may occur more frequently.
Additionally, should the filter press not be operational, clarifier solids may temporarily be directed to the

wastewater cooling pond for a short duration until the filter press can be repaired. This is expected to be
infrequent and will not be a routine operating mode.
Plant process wastewaters consisting of RO reject wastewater, excess evaporative cooling water, process
drains(low volume wastes), and waters from the oil water separator will be routed to the cooling pond.
The combined cycle plant utilizes water from the cooling pond as its source for fire protection water.
Infrequently, flushing and testing of the fire system may result in release of the fire water to the cooling
pond.
Cooling tower blowdown from the Heat Recovery Steam Generator (HRSG), wastewater from routine
cleaning, fuel oil/water condensate, false start materials, equipment drains containing potential oil, and
compressor wash water are directed to the cooling pond. Any of these waters with a potential for
containing oil are routed through the oil water separator.
Wayne County Combustion Turbine Wastewaters
Water from the cooling pond passes through a clarifier, dual media sand filters and then through a five-
micron cartridge pre-filter before entering either of two reverse osmosis (RO) units. The two RO units
may be operated in parallel or series depending on operational needs. The treated water is stored in a
tank until needed. Reject wastewater from the reverse osmosis process is sent to a sump where it will be
routed to the cooling pond.
Cooling tower blowdown from the Wet Surface Air Cooler(WSAC),wastewater from routine cleaning,fuel
oil/water condensate, false start materials, equipment drains containing potential oil, and compressor
wash water are directed to the cooling pond. Any of these waters with a potential for containing oil are
routed through the oil water separator.
Historically, the primary containments around the accessary module, liquid fuel, and atomizing air
modules empty into collection tanks. Once there is quantity of liquid collected in the tanks, the
wastewater is removed for off-site disposal. The wash water drain tank that collects water and detergent
used to clean the CT compressors is directed to cooling or disposed of offsite.
An oil water separator treats storm water from the containment areas around the facility's fuel oil storage
tanks,the fuel forwarding pumps,and the fuel oil unloading area. Water from the oil water separator will
be conveyed to the new collection sump and routed to cooling pond. Storm water collection containment
areas around transformers and substations are examined for presence of an oily substances; if oily
substances are not present in the water, the water is drained to the ground. If oil substances are present
nothing will be drained from the containments until that substance is removed.
In additions to the RO reject wastewater, excess evaporative cooling water, process drains (low volume
wastes), and waters from the oil water separator will be routed to the cooling pond.

Non-engineered seeps
There are 15 seeps (non-engineered) located around the cooling pond. Seeps identified are covered in
permit modification dated 12/1/2022.
Outfall 004—Beneficiation Facility
Ponded ash will be removed from the ash basins and placed in an enclosed load out area for use in the
beneficiation unit. The excavated ash is re-burned to remove the carbon to make the material suitable
for reuse as a product in cement. Wastewaters generated include truck wash water, wastewater from
dust suppression and stormwater that contacts ash. Wastewaters will be collected in a holding basin and
treated in an oil/water separator. Currently,the wastewater is being shipped offsite for disposal.
Outfall 005a—Inactive Ash Basins 1 and 2
The inactive ash basins are being dewatered to accommodate the excavation and beneficiation of ash.
Wastewater from the dewatering process will contain stormwater,groundwater, and interstitial water.
Outfall 005b—Inactive Ash Basin 3
The inactive ash basin is being dewatered to accommodate the excavation and beneficiation of ash.
Wastewater from the dewatering process will contain stormwater, groundwater, and interstitial water.
Outfalls 006, 007, 008, and 009—Inactive Basins Emergency Spillway
These outfalls were permitted to provide added safety of the basins as these spillways will allow flow from
flooding events and heavy precipitation to enter and/or exit the basin in a controlled and safe manner
reducing potential overtopping of the basin's dams. The wastewater within the basins consists of
stormwater,groundwater, and interstitial water. These outfalls have not been constructed.

1
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ENERGYE NPDES Permit No. NC0003417
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co Process Flow Diagram
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ERM www.erm,com Goldsboro, North Carolina

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New Lee Combined Cycle Site
Stream Estimated Average Comments
Flow
A 12.7 MGD Make-up water from Neuse River
B 12.7 MGD Make-up water to cooling pond
D 453 MGD Circulating water withdrawal from cooling pond
E 453 MGD Condenser cooling water return
F Lee Combined Cycle Plant Site wastewaters from
oil/water separator
I 11.3 MGD Cooling pond evaporation & seepage (estimated)
K 0.43 MGD Treated water to reverse osmosis system and plant
processes
M Rare Occurence Cooling pond discharge to Neuse River(Outfall
002/002A)
N 453 MGD Condenser cooling water supply
P Wayne County CT Site wastewater from sump lift station
N
Q 2,400 gal/event Collection and Drains Tank
ce Q new 2,400 gal/event New Wayne County CC Site wastewaters from oil/water
separator(for new Combined cycle)
R 0.048 MGD Wastewater from filter plant, recirculated back to
clarifier
LL U 0.48 MGD Raw water to filter plant (cycle make-up)
V 0.168 MGD New WCT CC plant process drains
E W 0.036 R.O. reject stream
X Flow from New Collection Sump 7to Cooling Pond
Z Z 0.005 MGD Wastewater from beneficiation plant
AA 1.8 MGD Est groundwater extraction well flow to treatment
system
BB 0.8 MGD Bulk/interstrial ash pond water to treatment system
CC 0.3 MGD Recirculated flow from treatment system to ash pond
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5 ERM www.erm.com Goldsboro, North Carolina

H. F. Lee Energy Complex
Duke Energy Progress, Inc. NPDES Permit Number NC0003417
Potential Discharges Not Covered By Analysis
Estimated
Quantity
(used per
Chemical year) Frequency Purpose
NALCO Stabrex ST-70 800 gal As required Wet Surface Air Cooler biocide
NALCO 3D Trasar 3DT 189 300 gal As required Wet Surface Air Cooler corrosion
control
NALCO BT 3000 150 lb As needed Boiler corrosion inhibitor
Ammonium Hydroxide (19%) 1,200 gal As required Boiler condensate pH control
NALCO Y302939.52
Sodium hypochlorite, 10-16% 34,000 gal As required Raw water biocide
Winter alum liquid 36,000 gal As required Raw water treatment
Caustic, 25% tech grade 21,000 gal Continuous Raw water pH control
Caustic, 50% tech grade 12,000 gal Continuous Ash pond pH control
Soda Ash 4,000 lb As required Ash pond pH control
Connect 6000 280 gal As required Wayne County Combustion
Turbine Site Turbine compressor
cleaning
NALCO PC-77 110 gal As required Wayne County Combustion
Turbine Site RO System
membrane low pH cleaner
NALCO PC 98 400 gal As required Wayne County Combustion
Turbine Site RO System
membrane high pH cleaner
NALCO PermaTreat PC-191 220 gal Continuous Wayne County Combustion
Turbine Site RO System
antiscalant
NALCO 7408 (sodium bisulfate) 880 gal As needed Various water stream
dechlorination
NALCO PC 11 variable As required Biocide for Reverse osmosis
system
ChemTreat P896L <55 gallons As required Reverse Osmosis Clarification
Miscellaneous laboratory solutions 2 gal As required Wayne County Combustion
and reagents Turbine Site RO water testing
Nalco 7465 < 1 gallon As required Foam Control
Nalco 7468 < 1 gallon As required Foam Control
A5-1 Dec 2022

H. F. Lee Energy Complex
Duke Energy Progress, Inc. NPDES Permit Number NC0003417
Sulfuric Acid
As required pH adjustment of ash basin
discharge
Acetic Acid As required pH adjustment of ash basin
discharge
Citric Acid As required pH adjustment of ash basin
discharge
Hydrochloric acid As required pH adjustment of ash basin
discharge
Alum As required pH adjustment of ash basin
discharge
COS As required pH adjustment of ash basin
discharge
Ferric chloride 7,500 gal As required Wastewater treatment additive
Ferric sulfate 7,500 gal As required Wastewater treatment additive
Ash Pond Water Wastewater Treatment System
Chlorine Dioxide < 500 As needed Biofouling control
gallons
Sulfuric Acid (98%) < 500 As needed Membrane cleaning
gallons
ChemTreat P860E Polymer <1000 Continuous Polymer
gallons
Ferric Chloride 30,000 Continuous Wastewater treatment additive
gallons
Sodium Hypochlorite 30,000 Continuous Wastewater treatment additive
gallons
Sodium Bisulfite 2,000 Continuous Wastewater treatment additive
gallons
ChemTreat RL9004 <1000 As needed Antiscalant
gallons
Sodium Hydroxide <10,000 Continuous Wastewater treatment additive
gallons
MobyFlox <1,000 As needed Wheel wash wastewater
gallons treatment additive
Eco Ultimate <500 As needed Fugitive emission suppression
gallons
Ultimer 7752 <250 As needed Wastewater treatment
gallons flocculant
A5-2 Dec 2022

H. F. Lee Energy Complex
2019-2022 FISH TISSUE MONITORING REPORT
` e a
NPDES Permit # NC0003417
July 2023
Prepared by:
DUKE ENERGY PROGRESS, LLC.
Environmental Field Support -Water Resources
New Hill, North Carolina
1

Table of Contents
Pane
1.0 introduction 1
2.0 Study Site Description and Sampling Locations 1
3.0 Target Species 3
4.0 Field Sampling Methods 3
5.0 Laboratory Processing and Analysis 3
6.0 Data Analysis and Reporting 3
7.0 References 4
List of Tables
Page
Table
1 Sample location, species, number collected, and size (length and weight) of fish collected for
trace element analysis from 2019 through 2022 4
2 Means and ranges of trace elements in fish muscle tissue collected from the two sampling
areas from 2019 through 2022 4
List of Figures
Page
Figure
1 Sampling areas for fish tissue trace elements monitoring on the Neuse River. 2

1.0 Introduction
Duke Energy owns and operates the gas fired H.F.Lee Combined Cycle Plant(H.F.Lee Plant)located
adjacent to the Neuse River in Wayne County,North Carolina. The coal fired H. F. Lee Steam Electric
Plant was retired in 2012 and demolition was completed in 2015. Currently, coal combustion residual
related operations onlyinclude removal and recycling of material from existing ash basins as a result of
P
Y g
former coal fired plant operations. The H. F. Lee Energy Complex National Pollutant Discharge
Elimination System(NPDES)Permit(No.NC0003417),effective April 1,2019,and expiring on March
31, 2024, includes a requirement in Section A.22 for annual monitoring of trace elements (arsenic,
selenium, and mercury) in fish muscle tissues near the ash pond discharge (Outfall 001) (Figure 1).
Monitoring results are required to be reported with the subsequent NPDES renewal application. In
addition, the permit requires a fish tissue monitoring plan to be submitted for approval. The plan was
submitted to the North Carolina Division of Environmental Quality, Division of Water Resources
(NCDEQ-DWR)in September 2019 and subsequently approved in October 2019.Fish collected for this
permit were processed and analyzed at Duke Energy's Harris Energy and Environmental Center
laboratory for trace elements in tissues according to the approved monitoring plan.
2.0 Study Site Description and Sampling Locations
Fish were collected from the Neuse River at locations UP and DI(Figure 1)for individual muscle tissue
trace elements analysis. Sampling location UP, is upstream of Outfall 001 and served as reference
location to monitor background trace element concentrations in fish muscle tissue. Sampling location
DI is in the immediate vicinity and downstream of Outfall 001 and was used to monitor near-field uptake
tissue. Location UP starts approximately and assimilation of trace elements in fish musclepp Y 12.5 river
kilometers (rkm)above Outfall 001 and extends approximately 4.8 rkm downstream.Location DI starts
approximately at Outfall 001 and extends downstream approximately 5.6 rkm.
1

o a sn,;h,, .Outfall 001
N P/aROaa OutfaII002
A, Ash Pond
T.
0
i rr, H.F.Lee
Combined.-.. DI Start '
Cycle Plant'
DI End
ct Neuse River c2
ri UP End0
4‘9Na,R�
al
UP Start
N H.F. Lee Combined Cycle Plant
ANPDES Permit#NC0003417
• 0.41001 : DI End • UP End -'''
• Outfail 002 2 DI Stem • UP Start .
r ,, �' stsa•N DUKE
0 0.5 1 Miles
I t ' ENERGY
0 0.5 1 Kilometers
Figure 1. Sampling areas for fish tissue trace elements monitoring on the Neuse River.
2

3.0 Target Species
The target fish species for tissue analysis at both sampling locations included catfish (Ictaluridae)
and sunfish (Lepomis spp.). The study plan stated that six individuals per species group would be
collected annually within each sampling location for a total of 24 fish per year. An attempt was
made to limit the smallest fish to 75% of the largest fish total length by species depending on
availability, keeping with the US Environmental Protection Agency (US EPA 2000)
recommendations for whole body fish tissue assessments.
4.0 Field Sampling Methods
Fish were collected following the Duke Energy ESFP-SW-0600-Trace Elements Procedure-Rev. 0.
Prior to 2020, collections followed procedure NR-0095-Trace Elements Field Procedure Rev. 1.
Only live fish that showed little or no signs of deterioration were retained for analysis. Retained
fish were identified to species,measured for total length(mm),weighed(g),tagged(Floy tags),and
bagged by species and site. Fish were placed on ice and frozen within 24 hours of collection.
5.0 Laboratory Processing and Arsenic, Selenium and Mercury Analysis
All individual fish samples were processed in Duke Energy's New Hill Trace Element Laboratory
according to procedure ESFP-SW-0601-Trace Elements Sample Preparation-Rev.0. Samples prior
to 2020 were processed using Duke Energy procedure NR-00107-Trace Element Monitoring
Laboratory Procedure-Rev. 4. The processed samples included lyophilized left axial muscle (and
included right axial muscle if insufficient left axial muscle was obtained). Samples were analyzed
for arsenic, selenium, and mercury by x-ray fluorometry. Quality control was achieved by use of
duplicates and standard reference materials. Remaining sample materials were archived and kept
for a minimum of two years.
6.0 Data Analysis and Reporting
Six fish,from the two species' groups,at two different locations were collected annually from 2019
to 2022. In total 96 fish (48 sunfish and 48 catfish) were collected and analyzed for trace elements
(Table 1).
3

Table 1. Sample location,species, number collected,and size (length and weight)of fish
collected for trace element analysis from 2019 through 2022.
Sample Species Number Length (mm) Weight (g)
location collected Mean Range Mean Range
UP Catfish 24 443 (229-587) 923 (120-2000)
Sunfish 24 176 (140-251) 116 (53-325)
DI Catfish 24 486 (273-665) 1550 (176-3825)
Sunfish 24 173 (136-214) 107 (43-196)
In addition to the length and weight of each fish, the dry-to-wet weight ratios are presented for
convenience to convert arsenic, selenium, and mercury wet weight concentrations back to dry
weight values (Appendix A). From 2019 through 2022 concentrations of arsenic and selenium for
all fish in both species' groups were below the USEPA wet weight screening values for recreational
fishermen (USEPA 2000) (Appendix A). Mercury concentrations were below the screening values
for recreational fishermen for all fish in both species' groups except for two catfish from the UP
sampling location (one in 2019 and one in 2021). For the same period the mean concentrations of
arsenic, mercury, and selenium for sunfish and catfish at both locations were below the screening
values for recreational fishermen (Table 2).
Table 2. Means and ranges of trace element concentrations in fish muscle tissue
collected from the two sampling locations from 2019 through 2022. All values
are wet weight (µg/g). The USEPA screening values are shown next to each
element.
Sample Arsenic (1.2) Mercury (0.4) Selenium (20.0)
Location Species Mean Range Mean Range Mean Range
UP Catfish 0.16 (0.13-0.24) 0.18 (0.10-0.45) 0.25 (0.19-0.33)
Sunfish 0.17 (0.13-0.21) 0.13 (0.06-0.33) 0.41 (0.20-0.61)
DI Catfish 0.14 (0.11-0.17) 0.20 (0.06-0.36) 0.23 (0.17-0.29)
Sunfish 0.16 (0.13-0.21) 0.11 (0.06-0.18) 0.43 (0.24-0.68)
7.0 References
U.S.EPA. 2000. Guidance for assessing chemical contaminant data for use in fish advisories.Vol.Fish
sampling and analysis. Third edition. EPA 823-B-00-007. United States Environmental Protection
Agency,Office of Water,Washington,DC.
4

APPENDICES
5

Appendix A. Arsenic, mercury,and selenium concentrations (wet weight*) in individual
fish axial muscle collected and analyzed from 2019-2022 for the H. F. Lee
Plant NPDES permit#NC0003417.
S ecies Length Weight Arsenic Mercury Selenium Dry to Wet
Species group Location Collection Date (mm) (g) (As) (Hg) (Se)µg/L Weight
µ� µ�
Redear Sunfish Sunfish UP 10/7/2019 156 58 0.18 0.13 0.45 0.2
Bluegill Sunfish UP 10/7/2019 194 171 0.21 0.19 0.39 0.2
Bluegill Sunfish UP 10/7/2019 187 125 0.18 0.18 0.42 0.2
Bluegill Sunfish UP 10/7/2019 201 146 0.15 0.33 0.24 0.19
Redear Sunfish Sunfish UP 10/7/2019 177 109 0.18 0.1 0.49 0.21
Redbreast Sunfish Sunfish UP 10/7/2019 191 143 0.2 0.19 0.37 0.2
Channel Catfish Catfish UP 10/7/2019 562 1700 0.24 0.42 0.2 0.19
Channel Catfish Catfish UP 10/7/2019 490 1075 0.14 0.24 0.19 0.19
Channel Catfish Catfish UP 10/7/2019 384 528 0.16 0.17 0.26 0.19
Channel Catfish Catfish UP 10/7/2019 467 906 0.17 0.13 0.29 0.2
Flathead Catfish Catfish UP 10/7/2019 418 730 0.13 0.12 0.23 0.18
Channel Catfish Catfish UP 10/7/2019 565 1675 0.14 0.19 0.26 0.19
Bluegill Sunfish DI 10/7/2019 159 77 0.17 0.13 0.53 0.2
Bluegill Sunfish DI 10/7/2019 147 50 0.15 0.1 0.41 0.18
Bluegill Sunfish DI 10/7/2019 159 72 0.13 0.09 0.38 0.18
Bluegill Sunfish DI 10/7/2019 136 43 0.16 0.13 0.43 0.18
Bluegill Sunfish DI 10/7/2019 163 69 0.16 0.1 0.39 0.19
Bluegill Sunfish DI 10/7/2019 155 58 0.14 0.1 0.51 0.18
Channel Catfish Catfish DI 10/7/2019 460 764 0.12 0.17 0.25 0.17
Channel Catfish Catfish DI 10/7/2019 531 1075 0.14 0.15 0.29 0.19
Channel Catfish Catfish DI 10/7/2019 500 1050 0.14 0.24 0.24 0.18
Channel Catfish Catfish DI 10/7/2019 488 1050 0.15 0.19 0.24 0.19
Channel Catfish Catfish DI 10/7/2019 370 424 0.14 0.2 0.22 0.18
Channel Catfish Catfish DI 10/7/2019 453 880 0.13 0.24 0.23 0.19
Bluegill Sunfish UP 4/29/2020 146 64 0.16 0.21 0.2 0.21
Redear Sunfish Sunfish UP 4/29/2020 176 100 0.18 0.13 0.44 0.2
Redear Sunfish Sunfish UP 4/29/2020 152 60 0.15 <0.06 0.3 0.2
Redear Sunfish Sunfish UP 4/29/2020 182 110 0.18 0.11 0.55 0.2
Redear Sunfish Sunfish UP 4/29/2020 157 62 0.16 <0.06 0.34 0.2
Bluegill Sunfish UP 4/29/2020 144 61 0.21 0.11 0.41 0.21
Channel Catfish Catfish UP 4/29/2020 449 740 0.19 0.13 0.25 0.21
Channel Catfish Catfish UP 4/29/2020 355 342 0.18 0.1 0.25 0.19
Channel Catfish Catfish UP 4/29/2020 372 442 0.17 0.11 0.25 0.19
Channel Catfish Catfish UP 4/29/2020 408 658 0.17 0.11 0.21 0.19
Channel Catfish Catfish UP 4/29/2020 422 630 0.13 0.17 0.22 0.18
Channel Catfish Catfish UP 4/29/2020 446 1050 0.16 0.12 0.23 0.21
Bluegill Sunfish DI 4/29/2020 214 196 0.21 0.14 0.49 0.2
Bluegill Sunfish DI 4/29/2020 185 138 0.15 0.12 0.44 0.2
Bluegill Sunfish DI 5/13/2020 181 119 0.16 0.13 0.37 0.2
Bluegill Sunfish DI 5/13/2020 166 92 0.14 0.09 0.37 0.2
Bluegill Sunfish DI 5/13/2020 155 73 0.16 0.08 0.4 0.2
Bluegill Sunfish DI 5/13/2020 156 78 0.16 0.12 0.42 0.2
Channel Catfish Catfish DI 4/29/2020 368 402 0.14 0.17 0.23 0.18
Channel Catfish Catfish DI 4/29/2020 420 588 0.13 0.13 0.24 0.19
Flathead Catfish Catfish DI 5/13/2020 387 605 0.13 0.11 0.24 0.18
Flathead Catfish Catfish DI 5/13/2020 365 440 0.13 0.08 0.24 0.18
Flathead Catfish Catfish DI 5/13/2020 310 222 0.13 <0.05 0.2 0.18
6

S ecies Length Weight Arsenic Mercury Selenium Dry to Wet
Species roa Location Collection Date (mm) (g) (As) (Hg) (Se)µgm Weight
group µg/L µg/L Ratio
Flathead Catfish Catfish DI 5/13/2020 273 176 0.13 0.06 0.23 0.18
Bluegill Sunfish UP 4/7/2021 174 120 0.18 0.12 0.61 0.22
Bluegill Sunfish UP 4/7/2021 150 70 0.16 0.06 0.56 0.21
Bluegill Sunfish UP 10/19/2021 190 170 0.21 0.15 0.38 0.21
Redear Sunfish Sunfish UP 10/19/2021 251 325 0.19 0.16 0.56 0.21
Redear Sunfish Sunfish UP 10/19/2021 223 204 0.18 0.1 0.42 0.2
Redear Sunfish Sunfish UP 10/19/2021 216 180 0.17 0.1 0.59 0.2
Flathead Catfish Catfish UP 4/7/2021 470 1100 0.14 0.32 0.29 0.2
Flathead Catfish Catfish UP 4/7/2021 528 1800 0.13 0.45 0.26 0.19
Flathead Catfish Catfish UP 4/7/2021 355 ** 0.14 0.2 0.3 0.19
Flathead Catfish Catfish UP 7/21/2021 587 2000 0.13 0.4 0.21 0.19
Flathead Catfish Catfish UP 7/21/2021 229 120 0.14 0.11 0.28 0.19
Flathead Catfish Catfish UP 10/19/2021 330 328 0.13 0.27 0.33 0.19
Bluegill Sunfish DI 4/7/2021 174 102 0.16 0.09 0.68 0.23
Redear Sunfish Sunfish DI 4/7/2021 210 160 0.16 0.13 0.53 0.2
Bluegill Sunfish DI 4/7/2021 162 78 0.17 0.09 0.52 0.22
Bluegill Sunfish DI 4/7/2021 168 98 0.14 0.06 0.41 0.18
Bluegill Sunfish DI 4/7/2021 170 89 0.18 0.1 0.47 0.2
Bluegill Sunfish DI 4/7/2021 174 100 0.16 0.18 0.43 0.21
Blue Catfish Catfish DI 10/7/2021 550 3675 0.15 0.24 0.26 0.2
Blue Catfish Catfish DI 10/7/2021 572 3725 0.15 0.26 0.21 0.2
Channel Catfish Catfish DI 10/7/2021 420 675 0.17 0.11 0.27 0.2
Blue Catfish Catfish DI 10/7/2021 590 3300 0.17 0.21 0.24 0.21
Blue Catfish Catfish DI 10/7/2021 597 3825 0.14 0.29 0.22 0.2
Blue Catfish Catfish DI 10/7/2021 585 3550 0.14 0.3 0.25 0.21
Bluegill Sunfish UP 6/7/2022 175 112 0.13 0.1 0.35 0.18
Bluegill Sunfish UP 6/7/2022 170 99 0.15 0.08 0.31 0.18
Bluegill Sunfish UP 6/7/2022 165 85 0.16 0.09 0.31 0.18
Bluegill Sunfish UP 6/7/2022 158 82 0.18 0.09 0.37 0.19
Bluegill Sunfish UP 6/7/2022 155 78 0.16 0.09 0.43 0.2
Bluegill Sunfish UP 6/7/2022 140 53 0.15 0.09 0.41 0.19
Channel Catfish Catfish UP 6/7/2022 450 784 0.22 0.13 0.24 0.2
Channel Catfish Catfish UP 6/7/2022 390 500 0.14 0.1 0.23 0.19
Channel Catfish Catfish UP 6/7/2022 492 978 0.18 0.1 0.25 0.2
Channel Catfish Catfish UP 6/7/2022 498 1050 0.17 0.11 0.26 0.22
Channel Catfish Catfish UP 6/7/2022 482 1050 0.16 0.11 0.26 0.2
Channel Catfish Catfish UP 6/7/2022 480 1050 0.16 0.12 0.27 0.21
Bluegill Sunfish DI 6/7/2022 182 136 0.15 0.11 0.4 0.19
Bluegill Sunfish DI 6/7/2022 198 160 0.17 0.12 0.24 0.2
Bluegill Sunfish DI 6/7/2022 195 180 0.15 0.09 0.4 0.19
Bluegill Sunfish DI 6/7/2022 193 148 0.19 0.09 0.44 0.2
Bluegill Sunfish DI 6/7/2022 193 155 0.18 0.11 0.31 0.17
Bluegill Sunfish DI 6/7/2022 168 95 0.14 0.14 0.34 0.17
Channel Catfish Catfish DI 6/7/2022 510 1100 0.15 0.1 0.23 0.19
Channel Catfish Catfish DI 6/7/2022 500 1000 0.16 0.13 0.27 0.2
Channel Catfish Catfish DI 6/7/2022 490 1125 0.11 0.32 0.21 0.17
Channel Catfish Catfish DI 6/7/2022 640 2250 0.14 0.35 0.17 0.18
Channel Catfish Catfish DI 6/7/2022 615 2400 0.14 0.3 0.2 0.19
Channel Catfish Catfish DI 6/7/2022 665 2900 0.15 0.36 0.22 0.2
*To convert to a dry weight,divide the fresh weight concentrations by the dry-to-wet weight ratio.
**No weight measured.This fish was excluded from the mean weight of catfish in Table 1.
7

Water Quality Instream Monitoring Data
Permit Renewal Application — NC0003417
September 2023

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Chemical Name Dissolved Zinc (ug/L) Hardness (mg/L) Tot
Location OUTFALL 002 Upstream OUTFALL 003 Downstream OUTFALL 002 Upstream OUTFALL 003 Downstream OUTFALL 002 Upstream al ArsenOUTFALL 003 Downstream _ OUTFALL 002 ic (ug/L) pstreamromiuOU(ug/L)
FALL 003 Downstream
Date
-
2019-07 < 5.0 < 5.0
2019-08 < 5.0 33.4 33.8 0.65 0.8
24.768
0..2
2019-09 < 5.0 8 25.6 0.62 0.69 68 0.1.3
2019-10 < 5.0 < 5.0 30.1 32.7 0.72 0.76 - 16 0.62
2019-11 < 5.0 < 5.0 40.2 40.8 0.48 0.71 - 0, .5 .5
< 5.0 33.1 32.3 < 0.50 < 0.50
2019-12 0.510.56 2020-01
0.84
1 < 5.0 < 5.0 24.2 24.9 0.38 0.38 0.60.62 0.57
2020-02 < 5.0 < 5.0 24.0 24.5 0.55 0.53 1.4
2020-03 < 5.0 < 5.0 23.3 23.1 0.44 0.44 1 1.2
2020-04 < 5.0 < 5.0 23.6 23.9 0.52 0.55 1.3 1.1
2020-05 .3 1.1
< 5.0 < 5.0 23.3 23.0 0.57 0.56 1.3 1.2
2020-06 < 5.0 < 5.0 30.0 28.0 0.47 0.51 0.18 0.88
2020-07 8 . < 5.0 27.2 25.6 0.58 0.66 1.1
2020-081
< .85. < 5.0 25.6 27.4 0.63 0.71 .3 1.3
2020-09 < 5.0 7.7 18.3 19.2 0.7 0.73 2.3 3.0
2020-10 < 5.0 < 5.0 12.0 13.9 0.73 0.82 1.4 1.7
2020-115. < 5.0 28.7 28.2 0.62 0.64 1.41 1.0
2020-12 <11.5 9.2 39.7 23.3 0.46 0.8 17 1.0
2021-01 < 5.0 11 24.9 25.8 0.39 0.42 1.1 0.88
2021-02 < 5.0 < 5.0 16.7 17.3 0.41 0.43 0.19
2021-03 < 5.10.0 < 5.0 18.3 19.3 0.43 0.44 1.0
< 10.0 1.6 1.4
< 10.0 < 10.0 19.7 20.8 < 1.0 < 1.0 1.0
2021-04 23.01.0
2021-05 < 10.0 < 10.0 22.4 < 1.0 < 1.0 1.3
33.2 33.1 < 1.0 11.
2021-06 < 10.0 < 10.0 < 1.0 < 1,0 < 1.0
2021-07
29.9 34.0 < 1.0
2021-08 1.0
< 10.0 < 10.0 27.4 26.3 < 1.0 <l10 < 1.0 < 1.0
2021-09 < 10.0 < 10.0 25.5 22.7 < 1.0 < 1.0 1< .0 1.1
37.2
2021-10 < 10.0 < 10.0 36.9< 10.0 < 1.0 < 1.0 < �0 1.1
2021-11 < 10.0 < 10.0 37.8 38.6 < 1.0 .1
_ < 1.0 _ < 1.0 < 1.0
2021-121 < 10.0 < 10.0 30.7 30.4 < 1.0 < 1.0 < 1.0 11.
39.0 < 1.0
1.0
2022-01 45.0 < 1.0
2022-02 < 10.0 < 10.0 18.3 20.1 < 1.0 < 1.0 < 1. <2.6
2022 03 < 10.0 < 10.0 _ 29.1 30.7 < 1.0 < 1.0 1.7
< 10.0 28.9 < 1.0 < 1.0
2022-04 < 10.0 < 10.0 28.4 < 1.0 < 1.0 < 1.0 < 1.0
2022-05 30.4 29.7 < 1.0 < 1.0< 10.0 < 10.0 11.3 11.36.6 < 1.0
2022-06 < 10.0 < 10.0 37.0 < 1.0 < 1.0
29.0 27.90
< .2
2022-07 < 10.0 < 10.0 < 1.0 < 1.0 1.6
2022-08 < 10.0 38.9 36.3 < 1.0 < 1.0 1.2 1.0
< 10.0 28.0 27.6 <1.1
2022-09 < 10.0 < 1.0 < 1.0 1.3
<
10.0 32.5 32.4 < 1.0 1.
2022-10 < 10.0 < 1.0 < 1.0 < 1.0
< 10.0 23.7
2022-11 < 10.0 < 10.0 24.7 < 1.0 < 1.0 1.0
33.1 33.0 < 1.0
2022-12 < 10.0 30.3 < 1.0 < 1.0 < 1.0 < 1.0
< 10.0 31.2
2023-01 < 10.0 < 10.0 < 1.0 < 1.0 < 1.0 < 1.0
2023-0228.1 27.6 < 1.0 < 1.0
< 10.0 < 10.0 25.4 - < 1.0 < 1.0
2023-03 < 10.0 26.0 < 1.0 < 1.0 < 1.0< 10.0 29.9 30.4 - < 1.0 _
2023-04 < 10.0 < 1.0 < 1.0 < 1.0 < 1.0
< 10.0 29.3 8 < 1.0 < 1.0 29.
2023-05 < 10.0 < 10.
< 1.0 < 1.0 _
0 23.0 24.6
2023-06 < 10.0 < 10.0 32.2 < 1.0 _ < 1.0 _ 1.4 1.3
32.1 < 1.0 < 1.0 < 1.0 1.0

Chemical Name Total Dissolved Solids (mg/L) Total Mercury (ng/L) Total Selenium (ug/L)
Location OUTFALL 002 Upstream OUTFALL 003 Downstream OUTFALL 002 Upstream OUTFALL 003 Downstream OUTFALL 002 Upstream OUTFALL 003 Downstream
Date
2019-07 110 130 3.96 3.29 < 0.50
2019-08 < 0.50
95.2 97.2 5.52 3.00 < 0.50 < 0.50
2019-09 112
120 2.89 2.82 < 0.50
2019-10 157 162 1.71 < 0.50
2019-11 � 127 126 Z.06 < 0.50 < 0.50
2.71 2.42 < 0.50 < 0.50
2019-12 82.4 81.2 4.20 4.63 < 0.50
2020-01 < 0.50
67.2 61.6 7.99 7.63 < 0.50 < 0.50
2020-02 82.4 87.6 5.68 5.59 < 0.50
2020-03 66.8 < 0.50
78.4 7.59 7.06 < 0.50 < 0.50
2020-04 86 82.8 7.32 7.18 < 0.50
2020-05 98 91.6 3.60 < 0.50
3.51 < 0.50 < 0.50
2020-06 85.6 80.8 4.22 5.04 < 0.50 < 0.50
2020-07 107 115 10.40 14.30 < 0.50 <
0.50
2020-08 82
86.4 20.20 14.90 < 0.50 < 0.50
2020-09 62 60.4 7.49 9.00 < 0.50 < 0.50
2020-10 67.6 72 4.77 3.88 < 0.50 < 0.50
2020-11 106 89.9 3.46 3.57 < 0.50 < 0.80
2020-12 74.8 74 5.01 8.59 < 0.50 < 0.50
2021-01 65.2 63.6 6.84 6.82 < 0.50 < 0.50
2021-02 59.6 61.2 4.88 4.72 < 0.50 < 0.50
2021-03 64.4 56.8 4.28 --
4.46 < 2.0 < 2.0
2021-04 72.4 70.4 4.74 4.18 < 2.0 < 2.0
2021-05 104 102 2.59 1.98 < 2.0
2021-06 112 112 < 2.0
4.97 4.45 < 2.0 < 2.0
2021-07 95 91 3.11 3.22 < 2.0
2021-08 76 79 < 2.0
3.78 4.10 < 2.0 < 2.0
2021-09 119 123 2.53 2.55 < 2.0 < 2.0
2021-10 147 136 1.76 2.19 < 2.0 < 2.0
2021-11 97 97 2.64 3.19 < 2.0 < 2.0
2021-12 150 152 1.02 1.24 < 2.0 < 2.0
2022-01 93 95 15.3 16,9 < 2.0
2022-02 106 < 2.0
103 1.91 1.87 < 2.0 < 2.0
2022-03 89 111
3.61 3.09 < 2.0 < 2.0
2022-04 98 88 3.89
3.54
2022-05 113 108 2.07 2.23 < 2.0 < 2.0
< 2.0 < 2
2022-06 .0
90 86 8.28 7.18
< 2.0 < 2.0
2022-07 143 138 3.87 2.07 < 2.0 < 2.0
2022-08 106 110 5.55 4.11 < 2.0 < 2.0
2022-09 142 147 2.94 2.23 < 2.0 < 2.0
2022-10 99 102 7.36 5.95 < 2.0 < 2.0
2022-11 138
2022 12 106 2.71 3.12 < 2.0 < 2.0
127
2.77 3.68 < 2.0 < 2.0
2023-01 91 99
2023-02 85 81
5.36 7.59 < 2.0 < 2.0
2023-03 101 99 7.23 6.52 < 2.0 < 2.0
4.15 3.62 < 2.0 < 2.0
2023-04 102 96
4.75 3.80 < 2.0 < 2.0
2023-05 69
2023 06 114 116 9.92 9.95 < 2.0 < 2.0
6.08 6.65 < 2.0 < 2.0