Loading...
The URL can be used to link to this page
Your browser does not support the video tag.
Home
My WebLink
About
WQ0002857_Monitoring - 07-2023_20230831
Monitoring Report Submittal ..................................................... Permit Number#* WQ0002857 Name of Facility:* Piedmont Custom Meats WWTF Month: * July Year: * 2023 Report Information Type* Upload Document* NDMR, NDAR-1, NDAR-2, NDMLR Piedmont Custom —July 2023.pdf 2.21MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address: * Jessica. Mize@pacelabs.com Name of Submitter: * Jessica Mize Signature: /& C6A jot Date of submittal: 8/31/2023 This will be filled in automatically Initial Review Reviewer: Wanda.Gerald Is the project number correct?* W00002857 Is the monitoring report accepted?* Yes NO Regional Office* Winston-Salem Reviewer: _anonymous Review Date: 9/15/2023 Page 1 of 3 NON -DISCHARGE WASTEWATER MONITORING REPORT PERMIT NUMBER: W00002857 MONTH: July YEAR: 2023 FACILITY NAME: Piedmont Custom Meats WWTF COUNTY: Caswell Flow Monitoring Point: Effluent: Influent: Parameter Monitoring Point: Effluent: El Influent: Surface Water S SW Code/Name: Was There Effluent Flow for this Month Generated At This Facility: Yes: 13 No: Lj D A T �. Operator Arrival Time 2400 Clock Operator Time on Site ORC on Site? 50050 00400 50060 D0310 00610 D0530 31616 70300 00620 00625 00940 00600 00665 Daily Rate (Flow) into Treatment S)slem pH Residual Chlorine BOD-5 20`C NH-3-N TSS Fecal Colifarm (Geo-metric Mean•) DS NO-3-N TAN Chloride Total Nitrogen Total Phosphorus HRS YIN GALLONS UNITS mgtL MG/L MG/L MG/L 11001VIL MGlL MG/L MGlL MG/L MG/L MG/L 1112 z 1,112 3, 0800 0.25 Y 1112 6.4 <0.01 4 1,112 5 1112 6 1,112 a 997 v u : 997 10 997 12 1054 0.25 B 997 6.3 <0.01 i t^ 14 997 ,5 140f' 16 1,401 ,z 1401 to 1,401 19 1347 -" 0.25' -- B 1401 6.3 <0.01 20 1,401 zt 1 401 22 1,188 23 1188 24 1,188 25 0830 0.50 Y 1188 6,5 ` <0.01 62.1 19.5 48.5 2,420 800 1.7 36.6 165 38.4- x6 1,188 27.. 1,188 2a 1,188 29 999 30 999 31 999 Average 1,158 <0.01 62.1 19.5 48.5 2420 800 1.7 36.6 165 38.4 4.9 Daily Maximum 1,401 6.50 <0.01 62.1 19.5 48.5 2420 800 1.7 36.6 165 38.4 4.9 Daily Minimum 997 6.30 <0.01 62.1 19.5 48.5 2420 800 1.7 36.6 165 38.4 4.9 Monthly Limits ( Avg) 5000 Composite © / Grab (G) Operator in Responsible Charge (ORC): Glenn Price Grade: SI Phone: 336-996-2841 Check Box if ORC Has Changed: F-1 ORC Certification Number: 987931/20771 Certified Laboratories (1): Pace Analytical Services (2): . Person(s) Collecting Samples: Glenn Price Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X _ e DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CIIA Division of Water Quality By this signature, 1 certify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: Compliant (Y,N) 1. Does all monitoring data and sampling frequencies meet permit requirements? If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permit Date Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 9683 Keres Chapel Road Gibsonville. NC (Permittee Address) 01002 Arsenic 01022 Boron 00310 BOD5 01027 Cadmium 00916 Calcium 00940 Chloride 50060 Chlorine, Total Residual 01034 Chromium 00340 COD Baron Neal McDuffie (Name of Signing Official -Please print or type) Field Services Director (Pace Analytical Services) PARAMETER CODES 31504 Coliform, Total 00094 Conductivity 01042 Copper 00300 Dissolved Oxygen 31616 Fecal Coliform 01051 Lead 00927 Magnesium 71900 Mercury 00610 NH3 as N 01067 Nickel (Position or Title) 336-582-8247 (Phone Number) 00600 Nitrogen, Total 00630 NO2 & NO3 00620 NO3 00556 Oil & Grease WQ09 PAN (Plant Available) 00400 pH 32730 Phenols 00665 Phosphorus, Total 00937 Potassium 00545 Settleable Matter 03/31 /21 (Permit Exp. Date) 00929 Sodium 00931 SAR 00745 Sulfide 00515 TDS 00010 Temperature 00625 TKN 00680 TOC 00530 TSS/TSR 076 Turbidity Fo092 Zinc Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facility's permit for reporting data. • If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b) (2) (D). Page 2 of 3 NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMIT NUMBER: NVQ0002857 MONTH: July YEAR: 2023 FACILITY NAME: Piedmont Custom heats WWTF COUNTY: Caswell Formulas: Daily Leading (inches) = (Volume Applied (gallons) x 0.1336 (cubic feet/gallon) x 12 (inches/foot)) / (Area Sprayed (acres) x 43,560 (square feettacre) or = (Volume Applied (gallons) / (Area Sprayed (acres) x 27.152 (gallons/acre-inch). Maximum Hourly Loading (inches) = Daily Loading (inches) / (Time irrigated (minutes) / 60 (minutes/hour)] Monthly Loading (inches) =Sum of Daily Loading (inches) 12 Month Floating Total (inches) = Sum of this month's Monthly Loading (inches) and previous 11 month's Monthly Loadings (inches) Average Weekly Loading (inches) = (Monthly Loading (inches/month) / Number of days in the month (days/month )I x 7 (daystweek) 'r. Irrigation Occur At This Facility ■ •. • • Occur No: U •. • •Field:Irrigation Yes Noll ® 1 II weamer s.oues: t-near, ri -parry eouay, Li-erouay, K-rain. Nn-snow, ar-sun Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336-996-2841 ORC Certification Number: 987931/20771 Check Box if ORC Has Changed Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit \ c DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By this signature, 1 certify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) 1. The did the limit(s) in the Compliant (Y,N) application rate(s) not exceed specified permit. 2. Adequate measures were taken to prevent wastewater runoff from the site(s). T 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. 4. All buffer zones as specified in the permit were maintained during each application. 5. The freeboard in the treatment and/or storage lagoon(s) was not less than the limit(s) specified in the permit. If the facility is non-comnliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Ln;d Z $r&Y -13 (Signature of Permite Date Baron Neal McDuffie (Authorized Aeent (Permittee-Please print or type) 9683 Keres Chapel Road Gibsonville. NC (Permittee Address) Baron Neal McDuffie (Name of Signing Official -Please print or type) Field Services Director (Pace Analytical Services) (Position or Title) 336-582-8247 (Phone Number) 03/31 /21 (Permit Exp. Date) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b) (2) (D). DENR Form NDAR-1 (5/2003) Page 3 of 3 NON -DISCHARGE APPLICATION REPORT SPRAT' IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMIT NUMBER: NVQ0002857 MONTH: .lulu YEAR: 2023 FACILITY NAME: Piedmont Custom Meats %N'%YTF COUNTY: CasN�ell Formulas: Daily Loading (inches) = [Volume Applied (gallons) x 0.1336 (cubic feet/gallon) x 12 (inches/foot)) / [Area Sprayed (acres) x 43,560 (square feetfacre) or = [Volume Applied (gallons) / (Area Sprayed (acres) x 27.152 (gallons/acre-inch). Maximum Hourly Loading (inches) = Daily Loading (inches) / [Time irrigated (minutes) / 60 (minutes/hour)) Monthly Loading (inches) =Sum of Daily Loading (inches) 12 Month Floating Total (inches) = Sum of this month's Monthly Loading (inches) and previous 11 month's Monthly Loadings (inches) Average Weekly Loading (inches) = [Monthly Loading (inches/month) / Number of days in the month (days/month )) x 7 (days/week) Did Irrigation Occur At This Facility Yes■ Did Irrigation Occu�his Field 'Did Irrigation■ No NON MENEEME ®®®®®®®®®®® -weather Codes: C-clear. I'C-partly cloudy, CI-claudl, R-rain, Sn-snow, Sl-sleet Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336-996-2841 ORC Certification Numhei-: 987931/20771 Check Box if ORC Has Changed: Mail ORIGINAL, and Two COPIP:S to: ATTN: Non -Discharge Compliance Unit S DENR (SIGNATURE OF OPE-RA7.OR IN RESPONS , : CIIARGE) Division of Water Quality By this signature, 1 certify that this report is accurate and 1617 Mail Service Center complete to the hest of my knowledge. ItU.EIGII,NC 27699-1617 DENR Form NDAR-1 (5/2003) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) 1. The application rate(s) did not exceed the limit(s) specified in the permit. 1 2. Adequate measures were taken to prevent wastewater runoff from the site(s). 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. 4. All buffer zones as specified in the permit were maintained during each application. S. The freeboard in the treatment and/or storage lagoon(s) was not less than the limit(s) specified in the permit. If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." -3_-2-3 (Signature of Permiee)* V Date Baron Neal McDuffie (Authorized Agent) (Permittee-Please print or type) 9683 Kerr's Chapel Road Gibsonville. NC (Permittee Address) Baron Neal McDuffie (Name of Signing Official -Please print or type) Field Services Director ( Pace Analytical Services) (Position or Title) 336-582-8247 (Phone Number) 03/31 /21 (Permit Exp. Date) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b) (2) (D). DENR Form NDAR-1 (5/2003) Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 August 03, 2023 Larry Moore Piedmont Custom Meats 430 NC Highway 49 South Asheboro, NC 27205 RE: Project: Piedmont Custom Meats Pace Project No.: 92678923 Dear Larry Moore: Enclosed are the analytical results for sample(s) received by the laboratory on July 25, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Eden If you have any questions concerning this report, please feel free to contact me. Sincerely, Ca Stephanie Knott stephanie.knott@pacelabs.com 704-977-0981 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 27 �ca; Project: Piedmont Custom Meats Pace Project No.: 92678923 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification* E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification * 37738 CERTIFICATIONS South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 Virginia/VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Page 2 of 27 (A"'�ace' SAMPLE ANALYTE COUNT Project: Piedmont Custom Meats Pace Project No.: 92678923 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92678923001 MW-1 SM 254OC-2015 LRB 1 PASI-E EPA 350.1 Rev 2.01993 SRS 1 PASI-E EPA 353.2 Rev 2.01993 SRS 1 PASI-E SM 9222D-2015 DAW 1 PASI-E EPA 120.1-1982 SMS 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 2 PASI-A SM 5310E-2014 MJP 1 PASI-A 92678923002 MW-4 SM 254OC-2015 VLG 1 PASI-E EPA 350.1 Rev 2.01993 SRS 1 PASI-E EPA 353.2 Rev 2.01993 SRS 1 PASI-E SM 9222D-2015 DAW 1 PASI-E EPA 120.1-1982 SMS 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 2 PASI-A SM 531OB-2014 MJP 1 PASI-A 92678923003 MW-5 SM 254OC-2015 LRB 1 PASI-E EPA 350.1 Rev 2.01993 SRS 1 PASI-E EPA 353.2 Rev 2.01993 SRS 1 PASI-E SM 9222D-2015 DAW 1 PASI-E EPA 120.1-1982 SMS 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 2 PASI-A SM 531OB-2014 MJP 1 PASI-A 92678923004 Effluent SM 254OC-2015 DAW 1 PASI-E SM 254OD-2015 RZB 1 PASI-E EPA 353.2 Rev 2.01993 SRS 2 PASI-E SM 5210E-2016 SRS 1 PASI-E Colilert-18 LRB 1 PASI-E TKN+NO3+NO2 Calculation MDW 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A EPA 350.1 Rev 2.0 1993 ARJ 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 365.1 Rev 2.01993 Zip 1 PASI-A PASI-A= Pace Analytical Services -Asheville PASI-E = Pace Analytical Services - Eden REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 3 of 27 �ce� ANALYTICAL RESULTS Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Project: Piedmont Custom Meats Pace Project No.: 92678923 Sample: MW-1 Lab ID: 92678923001 Collected: 07/25/23 09:53 Received: 07/25/23 10:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden Total Dissolved Solids 374 mg/L 50.0 1 07/28/23 15:03 350.1 Ammonia EDN Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Ammonia ND mg/L 0.10 1 07/27/23 15:22 7664-41-7 353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 21.4 mg/L 0.20 5 07/26/23 09:54 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Eden Fecal Coliforms ND CFU/100 mL 1.0 1 07/25/23 16:08 07/26/23 14:54 120.1 Specific Conductance Analytical Method: EPA 120.1-1982 Pace Analytical Services - Asheville Specific Conductance 496 umhos/cm 10.0 1 08/01/2311:42 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville Chloride 54.3 mg/L 1.0 1 07/28/23 00:33 16887-00-6 Sulfate 4.0 mg/L 1.0 1 07/28/23 00:33 14808-79-8 5310B TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services - Asheville Total Organic Carbon ND mg/L 1.0 1 07/31/23 02:31 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2023 12:58 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 27 ce� ANALYTICAL RESULTS Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Project: Piedmont Custom Meats Pace Project No.: 92678923 Sample: MW-4 Lab ID: 92678923002 Collected: 07/25/23 09:12 Received: 07/25/23 10:35 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden Total Dissolved Solids 590 mg/L 250 1 07/31/23 11:56 360.1 Ammonia EDN Analytical Method: EPA 350.1 Rev 2.01993 Pace Analytical Services - Eden Nitrogen, Ammonia 3.8 mg/L 0.10 1 07/27/23 14:34 7664A1-7 353.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate ND mg/L 0.040 1 07/26/23 09:38 14797-55-8 MBIO 9222D Focal Coliform EDN Analytical Method: SM 9222D-2015 Preparation Method: SM 922213-2015 Pace Analytical Services - Eden Fecal Coliforms 10.0 CFU/100 mL 1.0 1 07/25/23 15:43 07/26/23 14:54 120.1 Specific Conductance Analytical Method: EPA 120.1-1982 Pace Analytical Services - Asheville Specific Conductance 1000 umhos/cm 10.0 1 08/01/23 11:44 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 238 mg/L 5.0 5 07/2812314:20 16887-00-6 Sulfate 1.6 mg/L 1.0 1 07/28/23 01:50 14808-79-8 5310B TOC Analytical Method: SM 531OB-2014 Pace Analytical Services -Asheville Total Organic Carbon 7.2 mg/L 1.0 1 07/31/23 02:47 744044-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2023 12:58 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 27 (A"'09ace"' ANALYTICAL RESULTS Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Project: Piedmont Custom Meats Pace Project No.: 92678923 Sample: MW-5 Lab ID: 92678923003 Collected: 07/25/23 09:31 Received: 07/25/23 10:35 Matrix: Water Parameters 2640C Total Dissolved Solids Total Dissolved Solids 350.1 Ammonia EDN Nitrogen, Ammonia 353.2 NO2IN03 unpres EDN Nitrogen, Nitrate MBIO 9222D Fecal Coliform EDN Fecal Coliforms 120.1 Specific Conductance Specific Conductance 300.0 IC Anions 28 Days Chloride Sulfate 5310E TOC Total Organic Carbon Date: 08/03/2023 12:58 PM Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden 174 mg/L 25.0 1 0712812315:03 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Eden ND mg/L 0.10 1 07/27/2314:33 7664-41-7 Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden 0.17 mg/L 0.040 1 07/26/23 09:39 14797-55-8 Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Eden ND CFU/100 mL 1.0 1 07/25/23 15:43 07/26/23 14:54 Analytical Method: EPA 120.1-1982 Pace Analytical Services - Asheville 286 umhos/cm 10.0 1 08101/2311:46 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 58.3 mg/L 1.0 1 07/28/23 02:06 16887-00-6 ND mg/L 1.0 1 07/28/23 02:06 14808-79-8 Analytical Method: SM 531OB-2014 Pace Analytical Services -Asheville ND mg1L 1.0 1 07/31/23 03:04 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 27 �ce� ANALYTICAL RESULTS Project: Piedmont Custom Meats Pace Project No.: 92678923 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: Effluent Lab ID: 92678923004 Collected: 07/25/23 09:59 Received: 07/25123 10:35 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden Total Dissolved Solids 800 mg/L 125 1 07/28/23 12:39 2540D Total Suspended Solids Analytical Method: SM 254OD-2015 Pace Analytical Services - Eden Total Suspended Solids 48.5 mg/L 10.6 1 07/26/23 08:51 353.2 N021NO3 unpres EDN Analytical Method: EPA353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, NO2 plus NO3 1.8 mg/L 0.040 1 07/26123 09:53 Nitrogen, Nitrate 1.7 mg/L 0.040 1 07/26/23 09:53 14797-55-8 5210B BOD, 5 day EDN Analytical Method: SM 521 OB-2016 Preparation Method: SM 521 OB-2016 Pace Analytical Services - Eden BOD, 5 day 62.1 mg/L 2.0 1 07/26/23 10:23 07/31/23 11:02 Colilert-18 Fecal Colifonn EDN Analytical Method: Colilert-18 Preparation Method: Colilert-18 Pace Analytical Services - Eden Fecal Coliforms 2420 MPN/100ml- 1.0 1 07/25/23 15:07 07/26/23 09:15 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services - Asheville Total Nitrogen 38.4 mg/L 0.040 1 08/01/23 14:22 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville Chloride 165 mg/L 4.0 4 07/28/2314:35 16887-00-6 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 19.5 mg/L 0.50 5 08/02/23 13:00 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Kjeldahl, Total 36.6 mg/L 2.5 5 07/31/23 17:40 08/01/23 06:24 7727-37-9 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services - Asheville Phosphorus 4.9 mg/L 0.050 1 08/02/2312:57 08/03/2311:08 7723-14-0 Date: 08/03/2023 12:58 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. R6 El Page 7 of 27 (-"Pa c e ° QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92678923 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 789929 Analysis Method: SM 254OC-2015 QC Batch Method: SM 254OC-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92678923001, 92678923003 METHOD BLANK: 4093983 Matrix: Water Associated Lab Samples: 92678923001, 92678923003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L ND 25.0 07/28/23 15:02 LABORATORY CONTROL SAMPLE: 4093984 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg/L 250 230 92 90-110 SAMPLE DUPLICATE: 4093985 92678923001 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 374 392 5 SAMPLE DUPLICATE: 4093986 92679212002 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 244 235 4 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/0312023 12:58 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 27 �ce, QUALITY CONTROL DATA Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Project: Piedmont Custom Meats Pace Project No.: 92678923 QC Batch: 789936 Analysis Method: SM 254OC-2015 QC Batch Method: SM 254OC-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92678923004 METHOD BLANK: 4094000 Matrix: Water Associated Lab Samples: 92678923004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L ND 25.0 07/28/23 12:38 LABORATORY CONTROL SAMPLE: 4094001 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids mg/L 250 268 107 90-110 SAMPLE DUPLICATE: 4094002 92679382001 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 202 208 3 SAMPLE DUPLICATE: 4094003 92678923004 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 800 745 7 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2023 12:58 PM without the written consent of Pace Analytical Services, I.I.C. Page 9 of 27 ace" Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92678923 QC Balch: 789939 Analysis Method: SM 254OC-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92678923002 METHOD BLANK: 4094016 Associated Lab Samples: 92678923002 Parameter Units Total Dissolved Solids mg/L LABORATORY CONTROL SAMPLE: 4094017 Parameter Units Total Dissolved Solids mg/L SAMPLE DUPLICATE: 4094018 Parameter Total Dissolved Solids SAMPLE DUPLICATE: 4094019 Parameter Total Dissolved Solids Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 07/31/2311:54 Spike LCS LCS % Rec Cone. Result % Rec Limits Qualifiers 250 268 107 90-110 Units 92679382002 Result Dup Result mg/L 223 217 Units 92679181003 Result Dup Result mg/L 128 138 RPD Qualifiers 3 RPD Qualifiers 8 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2023 12:58 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 27 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92678923 QC Batch: 789252 Analysis Method: SM 254OD-2015 QC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92678923004 METHOD BLANK: 4090780 Associated Lab Samples: 92678923004 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 4090781 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 4090782 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 4090783 Parameter Units Total Suspended Solids mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 07/26/23 09:26 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 234 94 90-110 92679038001 Dup Result Result 3610 3400 92678923004 Dup Result Result 48.5 50.0 RPD Qualifiers 6 RPD Qualifiers 3 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 08/03/2023 12:58 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 27 (-�Faca, QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92678923 QC Batch: 789673 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia, EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92678923002, 92678923003 METHOD BLANK: 4092870 Matrix: Water Associated Lab Samples: 92678923002, 92678923003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 07/27/23 14:08 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 4092871 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 4.8 95 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4092872 MS 92678388003 Spike Parameter Units Result Cone. Nitrogen, Ammonia mg/L ND 5 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4092874 MS 92678388001 Spike Parameter Units Result Cone. Nitrogen, Ammonia mg/L ND 5 4092873 MSD Spike MS MSD MS MSD % Rec Cone. Result Result % Rec % Rec Limits RPD 5 5.1 5.1 101 102 90-110 0 4092875 MSD Spike MS MSD MS MSD % Rec Cone. Result Result % Rec % Rec Limits RPD 5 5.0 5.0 100 100 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08103/2023 12:58 PM without the written consent of Pace Analytical Services, LLC. Qual Qual Page 12 of 27 (-�Faca' QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92678923 QC Batch: 789674 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia, EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92678923001 METHOD BLANK: 4092888 Associated Lab Samples: 92678923001 Parameter Units Nitrogen, Ammonia mg/L LABORATORY CONTROL SAMPLE: 4092889 Parameter Units Nitrogen, Ammonia mg/L Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.10 07/2712314:57 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 5 4.7 94 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4092890 4092891 MS MSD 92678921001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc, Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 5.0 5.0 100 100 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4092892 4092893 MS MSD 92678990001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 5.2 5.1 101 101 90-110 1 Results presented on this page are In the units Indicated by the "UnIW column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 08/03/2023 12:58 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 27 (-�Pace-' QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92678923 QC Batch: 789262 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92678923001, 92678923002, 92678923003, 92678923004 METHOD BLANK: 4090799 Matrix: Water Associated Lab Samples: 92678923001, 92678923002, 92678923003, 92678923004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L ND 0.040 07/26/23 09:23 Nitrogen, NO2 plus NO3 mg1L ND 0.040 07/26/23 09:23 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 4090800 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg1L 1.5 1.5 99 90-110 Nitrogen, NO2 plus NO3 mg1L 2.5 2.4 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4090801 4090802 MS MSD 92678990003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L 0.95 1.5 1.5 2.4 2.4 97 95 90-110 1 Nitrogen, NO2 plus NO3 mg/L 0.95 2.5 2.5 3.4 3.4 98 97 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4090803 4090804 MS MSD 92678990002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L 0.90 1.5 1.5 2.4 2.4 100 101 90-110 1 Nitrogen, NO2 plus NO3 mg/L 0.90 2.5 2.5 3.4 3.4 1C0 100 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08103/2023 12:58 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 27 �ce Project: Piedmont Custom Meats Pace Project No.: 92678923 QC Batch: 789266 QC Batch Method: SM 521 OB-2016 Associated Lab Samples: 92678923004 METHOD BLANK: 4090810 Associated Lab Samples: 92678923004 Parameter Units BOD, 5 day mg/L QUALITY CONTROL DATA Analysis Method: SM 521OB-2016 Analysis Description: 5210B BOD, 5 day Final EDN Laboratory: Pace Analytical Services - Eden Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 07/31/23 09:32 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 4090811 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg/L 198 172 87 84.6-115 SAMPLE DUPLICATE: 4090813 92679050002 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 3.8 3.2 17 Results presented on this page are In the units Indicated by the "Units" column except where an ahemate unit Is presented to the rlght of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 08/03/2023 12:58 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 27 QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92678923 QC Batch: 789413 Analysis Method: SM 9222D-2015 QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF)-EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92678923001, 92678923002, 92678923003 METHOD BLANK: 4091591 Matrix: Water Associated Lab Samples: 92678923001, 92678923002, 92678923003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 07/26/23 14:54 METHOD BLANK: 4091593 Matrix: Water Associated Lab Samples: 92678923001, 92678923002, 92678923003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 07/26/23 14:54 METHOD BLANK: 4091594 Matrix: Water Associated Lab Samples: 92678923001, 92678923002, 92678923003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 07/26/23 14:54 METHOD BLANK: 4091595 Matrix: Water Associated Lab Samples: 92678923001, 92678923002, 92678923003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 07/26/23 14:54 SAMPLE DUPLICATE: 4091592 Parameter Fecal Coliforms 92678923003 Dup Units Result Result RPD Qualifiers CFU/100 mL ND ND Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2023 12:58 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 27 (�Vace" QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92678923 QC Batch: 789141 Analysis Method: Colilert-18 QC Batch Method: Colilert-18 Analysis Description: Colilert-18 Fecal Coliform EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92678923004 SAMPLE DUPLICATE: 4090345 Parameter Units Fecal Coliforms MPN/100mL 92679050001 Dup Result Result RPD Qualifiers ND ND Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2023 12:58 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 27 ( A` 9a ce, QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92678923 QC Batch: 790537 Analysis Method: EPA 120.1-1982 QC Batch Method: EPA 120.1-1982 Analysis Description: 120.1 Specific Conductance Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92678923001, 92678923002, 92678923003 METHOD BLANK: 4096986 Matrix: Water Associated Lab Samples: 92678923001, 92678923002, 92678923003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Specific Conductance umhos/em ND 10.0 08/01/23 11:32 Pace Analytical Services, LLC 1377 South Park Drive Kemersviiie, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 4096987 Spike LCS, LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Specific Conductance umhos/cm 1410 1420 100 90-110 SAMPLE DUPLICATE: 4096988 92679531003 Dup Parameter Units Result Result RPD Qualifiers Specific Conductance umhos/cm 259 259 0 SAMPLE DUPLICATE: 4096989 92678887001 Dup Parameter Units Result Result RPD Qualifiers Specific Conductance umhos/cm 35.8 35.7 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2023 12:58 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 27 �cee" QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92678923 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 789597 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92678923001, 92678923002, 92678923003, 92678923004 METHOD BLANK: 4092491 Matrix: Water Associated Lab Samples: 92678923001, 92678923002, 92678923003, 92678923004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg/L ND 1.0 07/27/23 23:46 Sulfate mg1L ND 1.0 07/27/23 23:46 LABORATORY CONTROL SAMPLE: 4092492 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg1L 50 49.8 100 90-110 Sulfate mg1L 50 49.9 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4092493 4092494 MS MSD 92678923001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg1L 54.3 50 50 100 102 92 96 90-110 2 Sulfate mg1L 4.0 50 50 50.1 56.9 104 106 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4092495 4092496 MS MSD 92679196002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg1L 2.2 50 50 54.3 55.3 104 106 90-110 2 Sulfate mg1L 1700 50 50 1740 1730 90 71 90-110 1 M1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2023 12:58 PM without the written consent of Pace Analytical Services, I.I.C. Page 19 of 27 ace Project: Piedmont Custom Meats Pace Project No.: 92678923 QC Batch: 790804 QC Batch Method: EPA 350.1 Rev 2.0 1993 Associated Lab Samples: 92678923004 METHOD BLANK: 4098241 Associated Lab Samples: 92678923004 Parameter Units Nitrogen, Ammonia mg/L QUALITY CONTROL DATA Analysis Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services -Asheville Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.10 08/02/2312:25 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 4098242 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 5.1 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4098243 4098244 MS MSD 92679453002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 80.7 5 5 86.6 88.8 118 163 90-110 3 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4098245 4098246 MS MSD 92679466001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 6.2 5 5 11.3 11.3 101 101 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2023 12:58 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 27 (-�Pace� QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92678923 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 790344 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92678923004 METHOD BLANK: 4096071 Matrix: Water Associated Lab Samples: 92678923004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mglL ND 0.50 08/01/23 04:46 LABORATORY CONTROL SAMPLE: 4096072 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 9.2 92 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4096073 4096074 MS MSD 92679331001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mglL 1.6 10 10 11.8 11.5 102 99 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4096075 4096076 MS MSD 92679331002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg1L 1.4 10 10 11.8 11.6 104 102 90-110 2 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2023 12:58 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 27 ace, Project: Piedmont Custom Meats Pace Project No.: 92678923 QC Batch: 790684 QC Batch Method: EPA 365.1 Rev 2.0 1993 Associated Lab Samples: 92678923004 METHOD BLANK: 4097785 Associated Lab Samples: 92678923004 Parameter Units Phosphorus mg/L QUALITY CONTROL DATA Analysis Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.050 08/03/2311:00 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 4097786 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.7 108 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4097787 4097788 MS MSD 92678645001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 5.5 2.5 2.5 9.5 9.1 160 142 90-110 5 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4097789 4097790 MS MSD 92679090001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 1.2 2.5 2.5 4.0 3.8 110 104 90-110 4 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 08/03/2023 12:58 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 27 �ce" QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92678923 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 790241 Analysis Method: SM 531 OB-2014 QC Batch Method: SM 531 OB-2014 Analysis Description: 5310E TOC Laboratory: Pace Analytical Services - Asheville Associated Lab Samples: 92678923001, 92678923002, 92678923003 METHOD BLANK: 4095657 Matrix: Water Associated Lab Samples: 92678923001, 92678923002, 92678923003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 07/30/23 15:50 LABORATORY CONTROL SAMPLE: 4095658 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 25 24.2 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4095659 4095660 MS MSD 92677753037 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L 0.50J 25 25 23.3 23.4 91 91 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4095661 4095662 MS MSD 92677753038 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L 1.1 25 25 24.9 24.8 95 95 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/0312023 12:58 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 27 (-�Pace, QUALIFIERS Project: Piedmont Custom Meats Pace Project No.: 92678923 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analyles. TNI - The NELAC Institute. ANALYTE QUALIFIERS El Reported value should be considered a minimum estimate since it is the maximum reportable number for this method based on the sample volume used. The true value is likely greater than the value reported. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R6 The RPD between valid sample dilutions exceeded 30%. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/03/2023 12:58 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 27 �ce' QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Piedmont Custom Meats Pace Project No.: 92678923 Lab ID 92678923001 92678923002 92678923003 92678923004 92678923004 92678923001 92678923002 92678923003 92678923001 92678923002 92678923003 92678923004 92678923004 92678923001 92678923002 92678923003 92678923004 92678923001 92678923002 92678923003 92678923004 92678923001 92678923002 92678923003 92678923004 92678923004 92678923004 92678923004 92678923001 92678923002 92678923003 Sample ID MW-1 MW-4 MW-5 Effluent Effluent MW-1 MW-4 MW-5 MW-1 MW-4 MW-5 Effluent Effluent MW-1 MW-4 MW-5 Effluent MW-1 MW-4 MW-5 Effluent MW-1 MW-4 MW-5 Effluent Effluent Effluent Effluent MW-1 MW-4 MW-5 Date: 08/03/2023 12:58 PM QC Batch Method SM 254OC-2015 SM 254OC-2015 SM 254OC-2015 SM 2540C-2015 SM 25400-2015 EPA 350.1 Rev 2.0 1993 EPA 350.1 Rev 2.0 1993 EPA 350.1 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993 SM 521OB-2016 SM 9222D-2015 SM 922213-2015 SM 922213-2015 Colilert-18 EPA 120.1-1982 EPA 120.1-1982 EPA 120.1-1982 TKN+NO3+NO2 Calculation EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 350.1 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 EPA 365.1 Rev 2.0 1993 SM 531OB-2014 SM 531OB-2014 SM 531OB-2014 QC Batch 789929 789939 789929 789936 789252 789674 789673 789673 789262 789262 789262 789262 789266 789413 789413 789413 789141 790537 790537 790537 790653 789597 789597 789597 789597 790804 790344 790684 790241 790241 790241 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Analytical Method SM 521OB-2016 SM 9222D-2015 SM 922213-2015 SM 9222D-2015 Colilert-18 Analytical Batch 789687 789414 789414 789414 789142 EPA 351.2 Rev 2.0 1993 790473 EPA 365.1 Rev 2.0 1993 790949 Page 25 of 27 :;o ON ed (sy0uew�o;uoO"IN ia4]0 dS1 HOaW 10H VN N A :poMaoatl 1 uelq dNi :S1Uaww0� Ain )o Q. � :dwoLPalaauoOIJafoo0 uaprtoOaaed Oo— ;—=:so13ei •Jjco !wa41 I JOPM Do Z :]d!aoay uodn dwal L 1ala03 2 p a 4"A :tHIl w+atu VN N A :paManH jugl8 dwal :o}ul amlendwal aldweS qe1 I V/N N :eaaawmao / # old-8 qs'I :xaxo ssa awl :adTaas 07e4=lt P-n ' N A =osaad oPTJTnS V :edTaa9 Hd }i N A otgeldoo-aw lid SL&MS : `' b/ :adTaIIB ID VH & )L auaaaxd auTIOM TI-PT801 �, its/ —TS 6-TPLaH UT satd as 0 N x aiTos Poaetn62x Vdsn yg oigeadaoot! aoedaptaA - VOA tlN N e*I uo PoATaoog'oaTdwv9 tlH Stipp owntoA 2uaTOT3ino yN N setalos wm=c] - tlN N aovaal eataao8'. �l R auasaad aanaOUSTS =caneTTOO YN H auaaaad axsMvu.6T9 Apoasn0 a*veal/2uasoaa sites dPoasna :asT"ootm 4d3oovu oTdueS T21 ,aw!Lia]eo� u1»V a!gel S E a V lZ/li/A :� :aw!l/aleo (amleu8!S):AuedwoO/Agpa . ay !L to:) wa!o Sdn x3a3i VN N a -(upb OOS>) pauaans (s)aldwes wa4apetl ;W paAMUJ saldul_N :#8u1pej1ge1 v .-pall IePKeW 8u!lped :(Sm04 Z4>)1N3s3Hd SOIOH LHOSS auoN Ala ant8 7aM :pa5n ail to ad61 Z 6 ,a (ajn] !$) :AuedwoOfhq pa4slnbu fol! rn a {am]eu8!s}:huedwoO/Aq pags!nbugag 6uuo1!uo jN jalempunolE) , :spjezeH aiq+ssod / suog!puaO leoadS / slhewaa iawolsnO Z Q1 Z < O 0 awl area awil ' aleO S O S O C] o Cl SJD IO qw0 , xuleyv OI aldwes,awoun� (ye1S al!sodwoO Z p is Z n ti o sea pu3 a] soduloO Jo) PalaalloO / dwaO 2 (LO) �a410'(n) jode/�'(S) Aesseo!g '(SL) anss1'(HV) MV'(dM) ad!M'(10) Polls} p!los/I!05 "(d) lan(>oJd O (MM) ja3_al_M'(M9) ja]eM punolg'(MO)1aleM 8uj4uuo :(molaq xoq zing!/j u! yasul) sapco xuleW . Z O C w (Alddtl saeie4o ai!Padx3) :PIaH ( ) v1 cn :s!sAleuV Ae0 S ( ) AeO d ( ) heO £ (1 Aga Z I 1 :aA!yaJV ( ) O ? ON( } saA I } Aea 1x2N I ) Ago awes () wnlay {) aleudadde se asods!0 E I o :(algea!Idde;!) pajall!i P! .4 :gsntl :!esods10 aldwe$ ro ON () sak I 1 o :ail uo ed A ale! awwl ,pai!nbaH alga punaewnl : amleu8!s) AS palaa!loO O CL :apoO uOpeool Ma :>i aloniO AS alln :# al SMd MO :#,aPjC aSeyoind -(1u!1d) ON[ ) saAt) Ue13 :8uo4d �8ul�ol!uoyi a9ue!ldwaO :# al A]!Ilsei/a]!s 13( ) LEI )Lw[ )Ld( ) / :paloa1103 allOZ awlL :A1lO/AlunoO :alel5 :lagwnN/aweN 13alcJd AwolsnO iaq* (0)'pa"i;swdun (n)'dSL (d) VU0104 wmuowwe (3) '41411ns wn!uowwe (8)'puergJo3Se (V)'auexa4 (6)'24e)!^so!41 wn!Pos (9)'al4ns:q wn!pos (L)'l-IZ41aw (9) 'atelo�e zu!1 (S)'apncapAy wn!pos (p!'ppe 3!414-'PAy (f) "p'3e:t-jins (Z)'Plm:;ypv (T) .sadA14Mle-vas M „ o n 8 MOLM d iaulewaj III 1111111111111111111 ' L9 VUB4 #0M ..,No m mn :ol sleaW wolsno }uowpald :01 uodaH :ssaippV splall luaAalai lie alaldwoO • SN3Wfia00IVD31 a s! Apo]snO-;o-u1e47 /j l f$Ujj9�2 juawn3oa lsonboU je,3gAjeuV AQo1sn:)-jo-Nlb'HD "� _ Document Name: Document Issued: November 15, 2021 2 Bottle identification Form j81Fj Page 1 of I Document No.: Issuing Authority: aceAnal,�flCci� 3 ` F-CAR-Cs-043-Rev.01 Pace Carolinas Quality Office "Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottles Project # a22 d v N v 01 Z Z G n' ~' 5 z0 H '� N d j < y V T' I 7. 4, �e I I a N 2 .Z. on' — z $ c 0 a c 0 o c v n C 7 0 N " 0 2 v a L M O Z A 0 M 5 w n_ 7 a n S v� n c aEE gy O S „� �. E J E d z Q ry A z d v C D Z ? S rNn o .N� Y a } M Y 2i a m YL+ A M w s z CL c ] a > c 4 p a n C 7 a J E a I J i E I a J c� E .`� a: m a E n E n E n E E v iu ;aE ¢ E d d E '� ON> M 0 E Q O 0 } E Q O E G' 10 w m w J E q' J E m J E ¢ J E 8 N E N E Q E v Vd in 6 f m 1 ID 0 m I m z M IL m H Q CL tb O W 17 3 ti li Q 2 M 4 7 M t7 Q v, .-1 Li Q M tri Q Q M t;� 4 t7 O 1= 01 } a O, t7 > 0. T t:� O 0 > sc V' e > r= N tL N N 6 N M rL m O Q t7 Vl > A ci G , 4 2 i l 8 I � , I , --- 12 ! \ pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added lot a i Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (Le Out of hold, incorrect preservative, out of temp, incorrect containers Page 27 of 27