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HomeMy WebLinkAboutWQ0004972_Monitoring - 07-2023_20230830 (3)Monitoring Report Submittal Permit Number#* Name of Facility:* Month:* July Report Information Type * GW-59 WQ0004972 Forest Lake RV WWTP Confirmation Email Address: * Name of Submitter: * Signature: Date of submittal: Initial Review Year:* 2023 Upload Document* 2023_July_GW Monitoring_WQ0004972 9.6MB complete.pdf PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). agrenier@greenerehssolutions.com Amanda Grenier ol�"a 8/30/2023 This will be filled in automatically Reviewer: Wanda.Gerald Is the project number correct?* WQ0004972 Is the monitoring report accepted?* Yes No Regional Office* Winston-Salem Reviewer: _anonymous Review Date: 9/8/2023 DocuSign Envelope ID: 90A1EB8F-DB1E-4E10-BA1E-CE057359BA3E SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 FACILITY INFORMATION Please Print Cleady or Type PERMIT Number: Expiration Date: 10/31/2027 Facility Name: Forest Lake RV WWTP Non -Discharge WQ0004972 UIC Permit Name (if different): NPDES Other Facility Address: 192 Thousand Trails Dr. TYPE OF PERMITTED OPERATION BEING MONITORED Advance °"" NC 27006 County Davie ❑ Lagoon ❑ Remediation: Infiltration Gallery IN Spray Field ❑ Remediation: Contact Person: Amanda Grenier Telephone#: 919-356-6509 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Forest Lake RV Spray Irrigation Field No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): 1 Date sample collected: 7/11/2023 FIELD ANALYSES: WAS Well Depth: 72 ft. Well Diameter: 2 in. pH 00400: 5.8 units Temp. 000lo: 16.7 oC DRY at Depth to Water Level 82546: 69.2 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. oo094: 70.7 µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft, a Odor 00085: None sampling,check Volume of water pumped/bailed before sampling: 4.5 gallons Appearance Clear here:® Samples for metals were collected unfiltered: ❑ YES N NO and field acidified: ❑ YES © NO LABORATORY INFORMATION Date sample analyzed: 7/12/2025 Laboratory Name: Pace Analytical Certification No. 12 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01o51 ug/L Coliform: MF Fecal 31616 23 /100mL Nitrate (NO3) as N 00620 <0.04 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.18 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 mg/L Al - Aluminum oil o5 mg/L pH (Lab) 00403 6.3 units Ba - Barium 01007 ug/L TOC 00680 6.9 mg/L Ca - Calcium oo916 mg/L Chloride 00940 1.9 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia oo610 0.11 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, NHaas N; Ammonia Nitrogen, Total) Mn -Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # ror Memealatlon systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% George Gudgeon, Sr. Vice President Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.06-07-2018 DocuSign Envelope ID: 90A1EB8F-DB1E-4E10-BA1E-CE057359BA3E SUBMIT FORM ON YFl I CHIN PAPER MIl Y GROUNDWATER QUALITY MONITORING: DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES COMPLIANCE REPORT FORM • • • • INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 10/31/2027 Facility Name: Forest Lake RV WWTP e Non -Discharge WQ0004972 UIC Permit Name (if different): NPDES Other Facility Address: 192 Thousand Trails Dr. TYPE OF PERMITTED OPERATION BEING MONITORED Advance NC 27006 County Davie ❑ Lagoon ❑ Remediation: Infiltration Gallery K Spray Field ❑ Remediation: Contact Person: Amanda Grenier Telephone#: 919-356-6509 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Forest Lake RV Spray Irrigation Field No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): 2 Date sample collected: 7/11/2023 FIELD ANALYSES: WAS Well Depth: 46 ft. Well Diameter: 2 in. pH 00400: 5.5 units Temp. 000lo: 16.3 oC DRY at Depth to Water Level 82546: 38.3 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 00094: 51.6 µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling,check Volume of water pumped/bailed before sampling: 3.75 gallons Appearance Clear here: Samples for metals were collected unfiltered: ❑ YES © NO and field acidified: ❑ YES N NO ❑ LABORATORY INFORMATION Date sample analyzed: 7/12/2023 Laboratory Name: Pace Analytical Certification No. 12 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N o0615 mg/L Pb - Lead olo51 uglL Coliform: MF Fecal 31616 86 /100mL Nitrate (NO3) as N 00620 0.45 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.18 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 70300 mg/L Al -Aluminum oil o5 mg/L pH (Lab) 004o3 5.8 units Ba - Barium 01007 ug/L TOC 00680 9.5 mg/L Ca - Calcium 00916 mg/L Chloride 0094o 3.4 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 <0.10 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen, N%as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 9 ug/L ,method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # �iJr ncmncuauvn ayslerns vniy tAi cn LaD Keports/: innuent I otal vU(;s: mg/L Effluent Total VOCs: mg/L VOC Removal% by: George Gudgeon, Sr. Vice President Permittee (or Authorized Agent) Name and Title - Please print or type Agent) 8/30/2023 GW-59 Rev.06-07-2018 DocuSign Envelope ID: 90A1EB8F-DB1E-4E10-BA1E-CE057359BA3E SUBMIT FORM ON YFI I OW PAPER OK11 Y GROUNDWATER QUALITY MONITORING: DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES COMPLIANCE REPORT FORM • • • • INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, INC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 10/31/2027 Facility Name: Forest Lake RV WWTP Non -Discharge WQ0004972 UIC Permit Name (if different): NPDES Other Facility Address: 192 Thousand Trails Dr, TYPE OF PERMITTED OPERATION BEING MONITORED Advance " NC 27006 County Davie ❑ Lagoon g ❑Remediation: Infiltration Gallery Spray Field ❑ Remediation: Contact Person: Amanda Grenier Telephone#: 919-356-6509 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Forest Lake RV Spray Irrigation Field No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): 3 Date sample collected: 7/11/2023 FIELD ANALYSES: WAS Well Depth: 20.4 ft. Well Diameter: 2 in, pH 00400: 4.5 units Temp. 000lo: 17.4 oC DRY at Depth to Water Level 82546: 9.3 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. oo094: 207 µMhos time of MeasuringPoint is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 000s5: None sampling, check Volume of water pumped/bailed before sampling: 5 gallons Appearance Clear here:❑ Samples for metals were collected unfiltered: ❑ YES ® NO and field acidified: ❑ YES ❑■ NO LABORATORY INFORMATION Date sample analyzed: 7/12/2023 Laboratory Name: Pace Analytical Certification No. 12 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 6 /100mL Nitrate (NO3) as N 00620 13.6 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.05 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids;Total 70300 mg/L Al -Aluminum o11o5 mg/L pH (Lab) 00403 4.9 units Ba - Barium 01007 ug/L TOC oo68o 1.1 mg/L Ca - Calcium 00916 mg/L Chloride 0094o 26 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 000lo <0.10 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 P mg/L Ni - Nickel 01067 ug/L method # . wi ..curcurauvrt 5yowitis Only jAUacn Lao meports): inrluent I otal vucs: mg/L Effluent Total VOCs: mg/L VOC Removal% George Gudgeon, Sr. Vice President Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 06-07-2018 DocuSign Envelope ID: 90A1EBSF-DB1E-4E10-BA1E-CE057359BA3E SUBMIT FORM ON YFI I ntint pnaFR nnu v NDWATER QUALITY MONITORING: LIANCE REPORT FORM I-AGILI I Y INFOKMATION r-iease t-nnr ueany or type Facility Name: Forest Lake RV WWTP Permit Name (if different): Facility Address: 192 Thousand Trails Dr. Advance NC 27006 County Davie act Person: Amanda Grenier Telephone#: 919-356-6509 Location/Site Name: Forest Lake RV Spray Irrigation Field No. of wells to be sampled: 4 DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 PERMIT Number: Expiration Date: 10/31/2027 Non -Discharge WQ0004972 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ME Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: °LL ID NUMBER (from Permit): 4 Date sample collected: 7/24/2023 ?II Depth: 39 ft. Well Diameter: 2 in. pth to Water Level 82546: 9.7 ft. below measuring point Screened Interval: ft. to ft. asuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. lume of water pumped/bailed before sampling: 5 gallons mples for metals were collected unfiltered: ❑ YES It NO and field acidified: ❑ YES ® NO Date sample analyzed: 7/25/2023 Laboratory Name: Pace Analytical PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD oo335 mg/L Nitrite (NO2) as N 00615 mg/L Coliform: MF Fecal 31616 1 /100mL Nitrate (NO3) as N 00620 4.2 mg/L Coliform: MF Total 31504 /100mL (Note: Use MPN method for highly turbid samples) Ived Solids:Total 70300 mg/L pH (Lab) 00403 units TOC 0068o 2.5 mg/L Chloride 0094o 7.4 mg/L Arsenic 01002 ug/L Grease and Oils 00552 mg/L Phenol 32730 ug/L Sulfate 00945 mg/L fic Conductance 00095 µMhos Total Ammonia 00610 <0.10 mg/L (Ammonia Nitrogen; N%as N; Ammonia Nitrogen, Total) TKN as N 00625 mg/L Phosphorus: Total as P 00665 0.14 mg/L Orthophosphate 70507 mg/L Al -Aluminum o11o5 mg/L Ba - Barium 01007 ug/L Ca - Calcium 00916 mg/L Cd - Cadmium 01027 ug/L Chromium: Total 01034 ug/L Cu - Copper 01042 mg/L Fe - Iron 01045 ug/L Hg - Mercury 71900 ug/L K- Potassium 00937 mg/L Mg - Magnesium 00927 mg/L Mn - Manganese o1o55 ug/L Ni - Nickel 01067 ug/L If FIELD ANALYSES: I WAS pH 00400: 8.4 units Temp. 000lo: 16.3 °C DRY at Spec. Cond. 00094: 87.9 µMhos time of Odor 00085: None sampling, check Appearance Clear here: El Certification No. 12 Pb - Lead 01051 ug/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 method # method # method # method # —• •- ..., ,..W,.,,., WY-1 a v.ny J�LWUu a.au FXVFIURSI: 1t111U6Ri 1 otat vut.s: mg/L Ltrluent Total VOCs: mg/L VOC Removal% George Gudgeon, Sr. Vice President Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev.06-07-2018 DocuSign Envelope ID: 90AI EB8F-DB1 E-4E1 0-BA1 E-CE057359BA3E UW-3JA L.V1VJrE1A1Nt-t, KhjrVRT FORM Permit # WQ0004972 (Submit one each monitoring period with GYV-59 forms.) 1 Enter date monitoring results were due. (7/31 /23 ) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? X 2 Was any required information missing on the GAT 59 report forms? YES NO IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. X 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Office for guidance. X 4 Are any monitored constituents equal to or above the established standards? YES NO if the answer to question 4 is NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: MW #1 - pH was 5.8, lab pH was 6.3. MW #2 - pH was 5.5 consistent with background MW #3 - pH was 4.5, Nitrate was 13.6 mg/I. X 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is NO", skip to section 8_ If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). X 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE if the answer is "NO", monitoring wells maybe improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO" contact the Reaional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation fines, and/or penalties. g The person completing this portion (GIN--59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. 1 hereby acknow%tl�e #�ai�ie above tnfo�C[rtafrcta �tvas eual�iat�cl and tk�e {nformatcol0 subbmitted to axis ` repor#{Gomplranee �epcet�G1AT-591�) [s true and �omplete�tQ the best,of y iCrrowfedge Signed by: 8/30/2023 Z L-AA Iti, Signature o ftt"ti MAQ#iorized Agent) Date GW-59A 12/8/2003 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 August 08, 2023 Amanda D. Grenier Greener EHS Solutions 21 Selby Ct. Holly Springs, NC 27540 RE: Project: Forest Lake MW- July Pace Project No.: 92679133 Dear Amanda Grenier: Enclosed are the analytical results for sample(s) received by the laboratory on July 25, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 16 ace Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: Forest Lake MW- July Pace Project No.: 92679133 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification M 37712 North Carolina Wastewater Certification #: 40 CERTIFICATIONS South Carolina Certification M 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification M E87627 Kentucky UST Certification M 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification M 460221 South Carolina Laboratory ID: 99030 South Carolina Certification M 99030001 Virginia/VELAP Certification M 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 16 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Forest Lake MW- July Pace Project No.: 92679133 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92679133001 Monitoring Well #4 EPA 350.1 Rev 2.0 1993 ARJ 1 PASI-A EPA 353.2 Rev 2.0 1993 MFO 1 PASI-A EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A SM 4500-CI-E-2011 Zip 1 PASI-A SM 531OB-2014 MJP 1 PASI-A 92679133002 Monitoring Well #4 Fecal SM 9222D-2015 KDF 1 PASI-C PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 16 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Forest Lake MW- July Pace Project No.: 92679133 Sample: Monitoring Well #4 Lab ID: 92679133001 Collected: 07/24/23 14:30 Received: 07/25/23 16:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia ND mg/L 0.10 1 08/03/23 12:36 7664-41-7 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Nitrate 4.2 mg/L 0.040 1 07/25/23 23:55 14797-55-8 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 0.14 mg/L 0.050 1 08/04/2316:29 08/07/2314:39 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 7.4 mg/L 1.0 1 08/01/2315:31 16887-00-6 5310B TOC Analytical Method: SM 531OB-2014 Pace Analytical Services -Asheville Total Organic Carbon 2.5 mg/L 1.0 1 08/02/23 00:24 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/08/2023 02:12 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 16 ANALYTICAL RESULTS Project: Forest Lake MW- July Pace Project No.: 92679133 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: Monitoring Well #4 Fecal Lab ID: 92679133002 Collected: 07/25/23 11:30 Received: 07/25/23 16:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte Fecal Coliforms 1.0 CFU/100 mL 1.0 1 07/25/23 17:11 07/26/23 16:30 Date: 08/08/2023 02:12 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 16 QUALITY CONTROL DATA Project: Forest Lake MW- July Pace Project No.: 92679133 QC Batch: 789181 Analysis Method: SM 9222D-2015 QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF) - CHT Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92679133002 METHOD BLANK: 4090584 Matrix: Water Associated Lab Samples: 92679133002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 07/26/23 16:30 SAMPLE DUPLICATE: 4090585 Parameter Fecal Coliforms 92679133002 Dup Units Result Result RPD Qualifiers CFU/100 mL 1.0 ND Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/08/2023 02:12 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 16 QUALITY CONTROL DATA Project: Forest Lake MW- July Pace Project No.: 92679133 QC Batch: 791089 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92679133001 METHOD BLANK: 4099668 Associated Lab Samples: 92679133001 Parameter Units Nitrogen, Ammonia mg/L LABORATORY CONTROL SAMPLE: 4099669 Parameter Units Nitrogen, Ammonia mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.10 08/03/23 12:09 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 5 5.1 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4099670 4099671 MS MSD 92680284001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 5.1 5.1 101 101 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4099672 4099673 MS MSD 92680284002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 5.2 5.2 102 102 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/08/2023 02:12 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 16 QUALITY CONTROL DATA Project: Forest Lake MW- July Pace Project No.: 92679133 QC Batch: 789214 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92679133001 METHOD BLANK: 4090710 Associated Lab Samples: 92679133001 Parameter Units Nitrogen, Nitrate mg/L LABORATORY CONTROL SAMPLE: 4090711 Parameter Units Nitrogen, Nitrate mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.040 07/25/23 23:53 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 1.5 1.6 107 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4090712 4090713 MS MSD 92679133001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L 4.2 1.5 1.5 5.8 5.8 109 106 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/08/2023 02:12 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 16 QUALITY CONTROL DATA Project: Forest Lake MW- July Pace Project No.: 92679133 QC Batch: 791302 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92679133001 METHOD BLANK: 4100941 Associated Lab Samples: 92679133001 Parameter Units Phosphorus mg/L LABORATORY CONTROL SAMPLE: 4100942 Parameter Units Phosphorus mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.050 08/07/23 14:38 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 2.5 2.6 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4100943 4100944 MS MSD 92680207001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L ND 2.5 2.5 2.6 2.6 105 106 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4100945 4100946 MS MSD 92680207002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L ND 2.5 2.5 2.6 2.6 106 105 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/08/2023 02:12 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 16 QUALITY CONTROL DATA Project: Forest Lake MW- July Pace Project No.: 92679133 QC Batch: 790385 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92679133001 METHOD BLANK: 4096280 Associated Lab Samples: 92679133001 Parameter Units Chloride mg/L LABORATORY CONTROL SAMPLE: 4096281 Parameter Units Chloride mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 08/01 /23 13:32 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 20 19.6 98 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4096282 4096283 MS MSD 92679133001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 7.4 10 10 17.4 17.2 100 98 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/08/2023 02:12 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 16 QUALITY CONTROL DATA Project: Forest Lake MW- July Pace Project No.: 92679133 QC Batch: 790647 Analysis Method: SM 531 OB-2014 QC Batch Method: SM 531 OB-2014 Analysis Description: 5310E TOC Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92679133001 METHOD BLANK: 4097589 Associated Lab Samples: 92679133001 Parameter Units Total Organic Carbon mg/L LABORATORY CONTROL SAMPLE: 4097590 Parameter Units Total Organic Carbon mg/L Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 08/01 /23 16:30 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 25 24.7 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4097591 4097592 MS MSD 92678043024 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L ND 25 25 24.2 24.1 95 95 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4097593 4097594 MS MSD 92678043025 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L ND 25 25 23.9 24.0 95 95 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/08/2023 02:12 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 16 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: Forest Lake MW- July Pace Project No.: 92679133 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/08/2023 02:12 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 16 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Forest Lake MW- July Pace Project No.: 92679133 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92679133002 Monitoring Well #4 Fecal SM 9222D-2015 789181 SM 9222D-2015 789182 92679133001 Monitoring Well #4 EPA 350.1 Rev 2.0 1993 791089 92679133001 Monitoring Well #4 EPA 353.2 Rev 2.0 1993 789214 92679133001 Monitoring Well #4 EPA 365.1 Rev 2.0 1993 791302 EPA 365.1 Rev 2.0 1993 791807 92679133001 Monitoring Well #4 SM 4500-CI-E-2011 790385 92679133001 Monitoring Well #4 SM 5310E-2014 790647 Date: 08/08/2023 02:12 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 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U �� > m m -I m E P. i D N- V7 `�\ O ZJ m m L 9 Z IT r SAMPLE TEMP AT COLLECTION m A OF CONTAINERS 1 J . m o n a v 0 y b � .� n Q� 'o m �V Unpresenred m � � a r H2504 a HNO3 m m cD i HCl w m Q m S Z! { _ NaOH Na25203 y � ? 1 Methanol ® c Other Analyses Test YIN o rAi i a� Fecal Colilorm MF, M-FC 0 m m a o u Ammonia/ T. Phos N ' C O � a oD I C \ Nitrate 93t G m Y M m TEMP in C - rn z ° m n M Residual Chlorine (YIN) z c a' 2 Received on (YIN) �n nz o < vsto y Sealed o O Cooler o (Y!N q - Inlact (YIN) t � � a Page 16 of 16 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 July 26, 2023 Amanda D. Grenier Greener EHS Solutions 21 Selby Ct. Holly Springs, NC 27540 RE: Project: FOREST LAKE-MW'S JULY Pace Project No.: 92676922 Dear Amanda Grenier: Enclosed are the analytical results for sample(s) received by the laboratory on July 12, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 22 ace Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FOREST LAKE-MW'S JULY Pace Project No.: 92676922 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification M 37712 North Carolina Wastewater Certification #: 40 CERTIFICATIONS South Carolina Certification M 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification M E87627 Kentucky UST Certification M 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification M 460221 South Carolina Laboratory ID: 99030 South Carolina Certification M 99030001 Virginia/VELAP Certification M 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 22 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: FOREST LAKE-MW'S JULY 92676922 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92676922001 MW#1 EPA 9040C YEG 1 PASI-A EPA 350.1 Rev 2.0 1993 EGC 1 PASI-A EPA 353.2 Rev 2.0 1993 MFO 1 PASI-A EPA 365.1 Rev 2.0 1993 MDW 1 PASI-A SM 4500-CI-E-2011 Zip 1 PASI-A SM 531OB-2014 MJP 1 PASI-A 92676922002 MW#2 EPA 9040C YEG 1 PASI-A EPA 350.1 Rev 2.0 1993 EGC 1 PASI-A EPA 353.2 Rev 2.0 1993 MFO 1 PASI-A EPA 365.1 Rev 2.0 1993 MDW 1 PASI-A SM 4500-CI-E-2011 Zip 1 PASI-A SM 531OB-2014 MJP 1 PASI-A 92676922003 MW#3 EPA 9040C YEG 1 PASI-A EPA 350.1 Rev 2.0 1993 EGC 1 PASI-A EPA 353.2 Rev 2.0 1993 MFO 1 PASI-A EPA 365.1 Rev 2.0 1993 MDW 1 PASI-A SM 4500-CI-E-2011 Zip 1 PASI-A SM 531OB-2014 MJP 1 PASI-A 92676922004 MW #1 SM 9222D-2015 KDF 1 PASI-C 92676922005 MW #2 SM 9222D-2015 KDF 1 PASI-C 92676922006 MW #3 SM 9222D-2015 KDF 1 PASI-C PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 22 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: FOREST LAKE-MW'S JULY Pace Project No.: 92676922 Sample: MW#1 Lab ID: 92676922001 Collected: 07/11/23 12:45 Received: 07/12/23 14:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 9040 pH Analytical Method: EPA 9040C Pace Analytical Services -Asheville pH at 25 Degrees C 6.3 Std. Units 0.10 1 07/18/23 12:22 H3 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 0.11 mg/L 0.10 1 07/25/23 16:50 7664-41-7 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Nitrate ND mg/L 0.040 1 07/13/23 00:19 14797-55-8 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 0.18 mg/L 0.050 1 07/24/23 18:34 07/24/23 22:05 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 1.9 mg/L 1.0 1 07/18/2315:50 16887-00-6 531013 TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon 6.9 mg/L 1.0 1 07/17/23 18:03 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/26/2023 12:07 AM without the written consent of Pace Analytical Services, LLC. Page 4 of 22 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: FOREST LAKE-MW'S JULY Pace Project No.: 92676922 Sample: MW#2 Lab ID: 92676922002 Collected: 07/11/23 13:32 Received: 07/12/23 14:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 9040 pH Analytical Method: EPA 9040C Pace Analytical Services -Asheville pH at 25 Degrees C 5.8 Std. Units 0.10 1 07/18/23 12:26 H3 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia ND mg/L 0.10 1 07/25/23 16:51 7664-41-7 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Nitrate 0.45 mg/L 0.040 1 07/13/23 00:20 14797-55-8 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 0.18 mg/L 0.050 1 07/24/23 18:34 07/24/23 22:05 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 3.4 mg/L 1.0 1 07/18/2315:51 16887-00-6 531013 TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon 9.5 mg/L 1.0 1 07/17/23 19:09 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/26/2023 12:07 AM without the written consent of Pace Analytical Services, LLC. Page 5 of 22 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: FOREST LAKE-MW'S JULY Pace Project No.: 92676922 Sample: MW#3 Lab ID: 92676922003 Collected: 07/11/23 15:47 Received: 07/12/23 14:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 9040 pH Analytical Method: EPA 9040C Pace Analytical Services -Asheville pH at 25 Degrees C 4.9 Std. Units 0.10 1 07/18/23 12:30 H3 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia ND mg/L 0.10 1 07/25/23 16:52 7664-41-7 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Nitrate 13.6 mg/L 0.20 5 07/13/23 00:32 14797-55-8 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus ND mg/L 0.050 1 07/24/23 18:34 07/24/23 22:07 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 26.0 mg/L 1.0 1 07/18/2315:52 16887-00-6 531013 TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon 1.1 mg/L 1.0 1 07/17/23 19:35 7440-44-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/26/2023 12:07 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 22 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: FOREST LAKE-MW'S JULY Pace Project No.: 92676922 Sample: MW #1 Lab ID: 92676922004 Collected: 07/12/23 09:45 Received: 07/12/23 14:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte Fecal Coliforms 23.0 CFU/100 mL 1.0 1 07/12/23 15:09 07/13/23 13:35 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/26/2023 12:07 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 22 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: FOREST LAKE-MW'S JULY Pace Project No.: 92676922 Sample: MW #2 Lab ID: 92676922005 Collected: 07/12/23 09:49 Received: 07/12/23 14:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte Fecal Coliforms 86.0 CFU/100 mL 1.0 1 07/12/23 15:09 07/13/23 13:35 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/26/2023 12:07 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 22 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: FOREST LAKE-MW'S JULY Pace Project No.: 92676922 Sample: MW #3 Lab ID: 92676922006 Collected: 07/12/23 09:59 Received: 07/12/23 14:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte Fecal Coliforms 6.0 CFU/100 mL 1.0 1 07/12/23 15:09 07/13/23 13:35 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/26/2023 12:07 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 22 QUALITY CONTROL DATA Project: FOREST LAKE-MW'S JULY Pace Project No.: 92676922 QC Batch: 786340 Analysis Method: SM 9222D-2015 QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF) - CHT Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92676922004, 92676922005, 92676922006 METHOD BLANK: 4076941 Matrix: Water Associated Lab Samples: 92676922004, 92676922005, 92676922006 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 07/13/23 13:35 SAMPLE DUPLICATE: 4076942 Parameter Fecal Coliforms 92676922006 Dup Units Result Result RPD Qualifiers CFU/100 mL 6.0 ND Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/26/2023 12:07 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 22 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE-MW'S JULY Pace Project No.: 92676922 QC Batch: 787442 Analysis Method: EPA 9040C QC Batch Method: EPA 9040C Analysis Description: 9040 pH Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92676922001, 92676922002, 92676922003 SAMPLE DUPLICATE: 4082193 92676714001 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 6.8 6.8 0 H3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/26/2023 12:07 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 22 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE-MW'S JULY Pace Project No.: 92676922 QC Batch: 788581 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92676922001, 92676922002, 92676922003 METHOD BLANK: 4087722 Matrix: Water Associated Lab Samples: 92676922001, 92676922002, 92676922003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 07/25/23 15:57 LABORATORY CONTROL SAMPLE: 4087723 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 5.1 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4087724 4087725 MS MSD 92677689005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L <0.10 5 5 5.2 5.1 103 103 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4087726 4087727 MS MSD 92677689006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L <0.10 5 5 4.9 4.9 98 98 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/26/2023 12:07 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 22 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE-MW'S JULY Pace Project No.: 92676922 QC Batch: 786421 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92676922001, 92676922002, 92676922003 METHOD BLANK: 4077400 Matrix: Water Associated Lab Samples: 92676922001, 92676922002, 92676922003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L ND 0.040 07/13/23 00:07 LABORATORY CONTROL SAMPLE: 4077401 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 1.5 1.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4077402 4077403 MS MSD 92676765001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L ND 1.5 1.5 1.5 1.5 101 102 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4077404 4077405 MS MSD 92677039001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L ND 1.5 1.5 1.5 1.6 102 103 90-110 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/26/2023 12:07 AM without the written consent of Pace Analytical Services, LLC. Page 13 of 22 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE-MW'S JULY Pace Project No.: 92676922 QC Batch: 788796 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92676922001, 92676922002, 92676922003 METHOD BLANK: 4088548 Matrix: Water Associated Lab Samples: 92676922001, 92676922002, 92676922003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 07/24/23 22:00 LABORATORY CONTROL SAMPLE: 4088549 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4088550 4088551 MS MSD 92676938001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 19.9 2.5 2.5 22.7 21.9 114 80 90-110 4 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4088552 4088553 MS MSD 92676938002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 4.1 2.5 2.5 6.7 6.5 104 97 90-110 3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/26/2023 12:07 AM without the written consent of Pace Analytical Services, LLC. Page 14 of 22 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE-MW'S JULY Pace Project No.: 92676922 QC Batch: 787298 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92676922001, 92676922002, 92676922003 METHOD BLANK: 4081493 Matrix: Water Associated Lab Samples: 92676922001, 92676922002, 92676922003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg/L ND 1.0 07/18/2315:23 LABORATORY CONTROL SAMPLE: 4081494 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride mg/L 20 20.6 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4081495 4081496 MS MSD 92677137001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 144 10 10 160 152 160 75 90-110 5 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4081497 4081498 MS MSD 92677215001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 26.3 10 10 34.5 34.8 82 84 90-110 1 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/26/2023 12:07 AM without the written consent of Pace Analytical Services, LLC. Page 15 of 22 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE-MW'S JULY Pace Project No.: 92676922 QC Batch: 787206 Analysis Method: SM 531 OB-2014 QC Batch Method: SM 531 OB-2014 Analysis Description: 5310E TOC Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92676922001, 92676922002, 92676922003 METHOD BLANK: 4080912 Matrix: Water Associated Lab Samples: 92676922001, 92676922002, 92676922003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 07/17/23 13:29 LABORATORY CONTROL SAMPLE: 4080913 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 25 24.8 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4080914 4080915 MS MSD 92677541001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L 9.1 25 25 33.1 32.6 96 94 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4080916 4080917 MS MSD 92677541004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L 8.0 25 25 31.9 32.1 95 96 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/26/2023 12:07 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 22 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: FOREST LAKE-MW'S JULY Pace Project No.: 92676922 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. ANALYTE QUALIFIERS H3 Sample was received or analysis requested beyond the recognized method holding time. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 07/26/2023 12:07 AM without the written consent of Pace Analytical Services, LLC. Page 17 of 22 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: FOREST LAKE-MW'S JULY 92676922 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92676922004 MW #1 SM 9222D-2015 786340 SM 9222D-2015 786341 92676922005 MW #2 SM 9222D-2015 786340 SM 9222D-2015 786341 92676922006 MW #3 SM 9222D-2015 786340 SM 9222D-2015 786341 92676922001 MW#1 EPA 9040C 787442 92676922002 MW#2 EPA 9040C 787442 92676922003 MW#3 EPA 9040C 787442 92676922001 MW#1 EPA 350.1 Rev 2.0 1993 788581 92676922002 MW#2 EPA 350.1 Rev 2.0 1993 788581 92676922003 MW#3 EPA 350.1 Rev 2.0 1993 788581 92676922001 MW#1 EPA 353.2 Rev 2.0 1993 786421 92676922002 MW#2 EPA 353.2 Rev 2.0 1993 786421 92676922003 MW#3 EPA 353.2 Rev 2.0 1993 786421 92676922001 MW#1 EPA 365.1 Rev 2.0 1993 788796 EPA 365.1 Rev 2.0 1993 788880 92676922002 MW#2 EPA 365.1 Rev 2.0 1993 788796 EPA 365.1 Rev 2.0 1993 788880 92676922003 MW#3 EPA 365.1 Rev 2.0 1993 788796 EPA 365.1 Rev 2.0 1993 788880 92676922001 MW#1 SM 4500-CI-E-2011 787298 92676922002 MW#2 SM 4500-CI-E-2011 787298 92676922003 MW#3 SM 4500-CI-E-2011 787298 92676922001 MW#1 SM 531OB-2014 787206 92676922002 MW#2 SM 531OB-2014 787206 92676922003 MW#3 SM 531OB-2014 787206 Date: 07/26/2023 12:07 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 18 of 22 I'Pace I _ ....r._ �........�....r„ , ..`..�.N Effective Date: 11/14/2022 Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersviiie ❑- Raleigh❑ Mechanicsville❑ Atlantan Kernersville❑ Upon : Client Name: Project ft: W�# 92676922 Courier: [-]Fed Ex [-]UPS ❑USPS ❑Client II I III I II II I I II I I I I III ❑ Commercial 'QPace ❑Other: 92676922 Custody Seal Present? ❑Yes -❑No Seals Intact? ❑Yes —❑No Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None ❑ Other Thermometer: IRGun ID: Type of Ice: ---OWet []Blue Correction Factor: Cooler Temp: ` Add/Subtract (°C) Cooler Temp Corrected USDA Regulated Soil (,A, water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maosl? MYes f-1Nn Date/Initials Person Examining Contents: \ ti) Biological Tissue Frozen? ❑Yes ❑No ❑N/A ❑None Temp should be above freezing to 6°C ❑Samples out of temp criteria. Samples on ice, cooling process has begun Did samples originate from a Foreign source (internationally, Lj.Cz, UIVu Comments/Discrepancy: Chain of Custody Present? --Dyes []No ❑N/A 1. Samples Arrived within Hold Time? Oyes []No []N/A 2. Short Hold Time Analysis (<72 hr.)? -QYes ❑No []N/A 3. Rush Turn Around Time Requested? ❑Yes []No DN/A 4. Sufficient Volume? .DYes ❑No ❑N/A S. Correct Containers Used? -Pace Containers Used? ]Yes ❑Yes ❑No ❑No ❑N/A ❑N/A 6. Containers Intact? []Yes ❑No ❑N/A 7. Dissolved analysis: Samples Field Filtered? []Yes [:]No ❑N/A 8. Sample Labels Match COC? -Includes Date/Time/ID/Analysis Matrix: Headspace in VOA Vials (>S-6mm)? []Yes ❑Yes ❑No ❑No ❑N/A .❑N/A 9. 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes [-]Yes []No ❑No ❑N/A ❑N/A 11. COMMENTS/SAMPLE DISCREPANCY -77 CLIENT NOTIFICATION/RESOLUTION lot ID of split containers: Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time: Date: Date: Field Data Re— /g7uired? LYes LINo l), ),):;z_� Qualtrax ID: 69614 Page 1 of 2 Page 19 of 22 Iav VVIII./III VII V VII I\CL.CI L ace - Effective Date: 11/14/202.2 "Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples. Exceptions: VOA, Coliform, TOC, oil and Grease, DRO/8015 (water) DOC, Mig "Bottom half of box is to list number of bottles ""Check all unpreserved Nitrates for chlorine WO#:92676922 r 1 vac« n PM: MWB Due Date: 07/26/23 CLIENT: 92-Greener Z a 2!i- Z �oJ Z o�J a Q Z 'av W v N = ry v = O Z 03 W N A a a v i1 C D l- Q Z M of d _ N < Z 0J ` v O. N v S y Q Z Q Z Q z L Z V Z .. x 0 1 14 M o'i -0 v a 'p v M u d a 7 u A a9 c u N Q. c a N = •J M = v Q Z N o fO 2 v jE a c D = n v _ y AJ O In _ c ry = V = Z 2 _ = O "AW N i a ? 0 n. = a�i a n. e i CL > v y 'a ry Z m CJ %n N Z n > o d a a e rp aJ E 14 .••I aJ E in N p a. Ji E o N M rl ;, = rl E In a J E O N J E i H E J, ,r-11 o v E Q w = ,-1 E Q ;, = rl ¢ E o N Q0! E " ,••1 ¢ J E O N QN E J E I O J E O Q J E > J E O > J E O !L J E O 0. N VI J E N VI E ✓1 o- a J E In 17 Q EO> J E O c V i E O W E ¢ E O u _ O co m a m 7 en m a m VI a m Z a. a m N C a m m Q a to u'. 3 N C7 Q = rt 6 ¢ O M t7 ¢ N rt iD Q V1 M U ¢ V 01 0 o i M 0 (n 7 01, � > M a V1 d sc `'t � > N N N N 'A N CL "I m O ¢ N t7 � Q M o 2 3 4 1 I J — — — — s 1 I 6 44 — I 7 N\ I 8 10 N \ 11 \N \ 1z pH Adjustment Log for Preserved Samples Sample 10 Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot # Note: Whpnpvpr thprp Ic a rif--n—, off—f- e1,.,,6 r.._I:-- --'--_-- _ -- - - - - •- .• -ter+ . 11 Out of hold, incorrect preservative, out of temp, incorrect containers. vc,ern UJ Inc Ivorul laronna UtNR CertiliWllon 011ice (i,C. Qualtrax ID: 69614 Page 2 of 2 Page 20 of 22 ITEM # ran m. ; a 3 a M N - O N O O n z o D n • O EZ V 3 O ^ 1G O N fD 7 n G L D u, m o fD u m u i cn 4 Q � ,n o \ o N I N m _ o v d x o ~ m 3 "-_o£:o_Tp.cq 1 a` 8 h o R n R 0 n n C 0 o m O N O➢� O � < 0 0 p 9� .O O a # s z j N 0 3 0 O r d � O 3 v MATRIX CODE (see valid codes to left) D) xt m SAMPLE TYPE (G=GRAB C=COrdP) _ T � o o > Lv m u (J m DLn o ' ti G) ;d r ra m O z D c Z i m n o z o r 0 _ y A m 3 o M m ` v a 1 �` L.n: a m IT 0 0 in o D z O m z O -�� J3 `v cn t .�, m r m r m z D m SAMPLE TEMP AT COLLECTION A '3 C m -1 EnD J N OF CONTAINERS d v a a l m o -o m p N u, i o or'. Fio Unpreserved iC i 0 0 o ? ' 0 �- H2SO4 = o n m Z a HNO3CD " m N HCI D ? N l �- LEI NaOH m l 0i c v Na2S203 r< D in m 3 - m 0 Methanol in CD Other Q Analyses Test Y/N n v TOC JD y �\ ` Chloride/ pH m = c o Fecal Coli(orm MF M c Ammonia! T. Phos a CL 3 r NitrateEL G y J E N n w ^ m m A a � m TEMP in C A � Residual Chlorine (YIN) y N �. m c ry Received on Ice z o 0 (YIN) m o C G r C� J `• '�J D uslo y Sealed Cooler T YIN i N Samples Intact (Y1N) �-i m � < CD C o CD a N 3 C p n CD = n 3 � pq, n. n C DI CD Page 21 of 22 ce Analyircal Sample Receiving Date: ,i ` I Evaluated by: Client: e 1-4 Non -Conformance Form (NCF) Affix Workorder/Login Label Here or List Pace Workorder Number or MTJL Log -in Number Here 1. If Chain -of -Custody (COC) is not received: contact client and if necessary, fill out a COC and indicate that it was filled out by lab personnel. Note issues on this NCF. 2. If COC is incomplete. check anolicable issues below and add details where annronriate: Collection date/time missing or Analyses or analytes: missing or V Samples listed on COC do not match samples incorrect clarification needed received (missing, additional, etc. Sample IDs on COC do not match sample labels Required trip blanks were not received Required signatures are missing Comments/Details/Other Issues not listed above: TO c vt6'-,, ��,(-:'e-�� 3. Samr)le intearitv issues: check aoolicable issues below and add details where annronriate: Samples: Condition needs to be brought to Samples: Past holding time lab ersonnel's attention details below Preservation: Improper Temperature: not within acceptance criteria (typically Samples: Not field filtered Containers: Broken or compromised 0-6C Samples: Insufficient volume received Containers: Incorrect Temperature: Samples arrived frozen Samples: Cooler damaged or Custody Seals: Missing or compromised on compromised samples, trip blanks or coolers Vials received with improper heads ace Samples: contain chlorine or sulfides Packing Material: Insufficient/Improper Other: Comments/Details: 4. If SamDles not oreserved Dronerly and Samnle Receiving adiusts nH_ add details halnw- Sam le ID: Date/Time: Amount/ty a pros added: Preserved by: Initial and Final H: Lot # of pres added: Sample ID: Date/Time: Amount/type res added: Preserved by: Initial and Final H: Lot # of pres added: Sample ID: Date/Time: Amount/type pres added: Preserved by: Initial and Final H: Lot # of pres added: 5. Client Contact: If client is contacted for any issue listed above, fill in details below: Client: I Contacted per: I PM Initials: I Date/Time: Client Comments/Instructions: F-ALL-C-01 1 -rev.00, 05Ju12018 Page 22 of 22