NC0003417_J15060347report_20150805

Lab
DUI E Analytical Laboratory APagel1aof84
ENERGY
Order Number:
Project Name:
Customer Name(s):
Customer Address:
Lab Contact:
Report Authorized By:
(Signature)
Program Comments:
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
J15060347
HF LEE PLANT - AB GW ASSESSMENT WATER
Tim Hunsucker, Judd Mahan, Kathy Webb, John Toepfer
1677 Old Smithfield Rd
Goldsboro NC 27530,
Mary Ann Ogle
Phone: [phone]
Mary Ann Ogle
j ` I ✓ 2015.06.25 10:43:50 Date:
-04'00'
Mary Ann Ogle
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
6/25/2015
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Collection
Sample ID Plant/Station Date and Time
Collected By
Sample Description
2015018388
HF LEE PLANT
10-Jun-15 11:05 AM
ILLEGIBLE
IABMW-1S
2015018389
HF LEE PLANT
10-Jun-15 10:30 AM
ILLEGIBLE
IABMW-1
2015018390
HF LEE PLANT
10-Jun-15 3:22 PM
ILLEGIBLE
AMW-13S
2015018391
HF LEE PLANT
10-Jun-15 4:00 PM
ILLEGIBLE
AMW-13BC
2015018392
HF LEE PLANT
10-Jun-15 10:25 AM
ILLEGIBLE
IABMW-3S
2015018393
HF LEE PLANT
10-Jun-15 1:05 PM
ILLEGIBLE
IABMW-2S
2015018394
HF LEE PLANT
10-Jun-15 4:53 PM
ILLEGIBLE
AMW-12S
2015018395
HF LEE PLANT
10-Jun-15 3:41 PM
ILLEGIBLE
AMW-12BC
2015018396
HF LEE PLANT
10-Jun-15 8:04 AM
ILLEGIBLE
Filter Blank
2015018397
HF LEE PLANT
10-Jun-15 8:04 AM
ILLEGIBLE
Equipment Blank
10 Total Samples
Analytical Lab
Page 2 of 84

Analytical Lab
Page 3 of 84
Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals 0 Yes ❑ No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes 0 No
All laboratory QA/QC requirements are acceptable. 0 Yes ❑ No
Report Sections Included:
E%-'] Job Summary Report
❑� Sample Identification
Technical Validation of Data Package
❑� Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
❑d Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
❑� Chain of Custody
❑� Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Mary Ann Ogle Date: 6/25/2015

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: IABMW-1 S
Collection Date: 10-Jun-15 11:05 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
M2 0.01
INORGANIC IONS BY IC
Chloride
13
mg/L
1
Sulfate
11
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.087
mg/L
0.005
Barium (Ba)
0.204
mg/L
0.005
Boron (B)
0.220
mg/L
0.05
Iron (Fe)
47.9
mg/L
0.01
Manganese (Mn)
5.11
mg/L
0.005
Strontium (Sr)
0.493
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
57.3
mg/L
0.01
Magnesium (Mg)
30.6
mg/L
0.05
Potassium (K)
1.41
mg/L
0.1
Sodium (Na)
18.4
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.100
mg/L
0.005
Barium (Ba)
0.215
mg/L
0.005
Boron (B)
0.226
mg/L
0.05
Iron (Fe)
49.1
mg/L
R1 0.01
Manganese (Mn)
5.34
mg/L
0.005
Strontium (Sr)
0.512
mg/L
0.005
Zinc (Zn)
0.005
mg/L
0.005
Sample #: 2015018388
Matrix: GW WW
Analytical Lab
Page 4 of 84
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
06/17/2015 12:07
LSTARLI
10
EPA 300.0
06/15/2015 11:52
BGN9034
10
EPA 300.0
06/15/2015 11:52
BGN9034
1
EPA 245.1
06/18/2015 11:23
ACPAYNE
1
EPA 245.1
06/16/2015 11:04
ACPAYNE
1
EPA 200.7
06/12/2015 13:09
MHALL3
1
EPA 200.7
06/12/2015 13:09
MHALL3
1
EPA 200.7
06/12/2015 13:09
MHALL3
1
EPA 200.7
06/12/2015 13:09
MHALL3
1
EPA 200.7
06/12/2015 13:09
MHALL3
1
EPA 200.7
06/12/2015 13:09
MHALL3
1
EPA 200.7
06/12/2015 13:09
MHALL3
1
EPA 200.7
06/17/2015 12:58
MHALL3
10
EPA 200.7
06/17/2015 12:58
MHALL3
1
EPA 200.7
06/17/2015 12:58
MHALL3
1
EPA 200.7
06/17/2015 12:58
MHALL3
1
EPA 200.7
06/13/2015 14:42
MHALL3
1
EPA 200.7
06/13/2015 14:42
MHALL3
1
EPA 200.7
06/13/2015 14:42
MHALL3
1
EPA 200.7
06/13/2015 14:42
MHALL3
1
EPA 200.7
06/13/2015 14:42
MHALL3
1
EPA 200.7
06/13/2015 14:42
MHALL3
1
EPA 200.7
06/13/2015 14:42
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: IABMW-1 S
Collection Date: 10-Jun-15 11:05 AM
Analyte
Result
Units Qualifiers
RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
1.82
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
27.7
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
4.46
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
1.91
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
27.2
ug/L
1
Copper (Cu)
28.9
ug/L
1
Lead (Pb)
1.42
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
4.38
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
RADIOLOGICAL - (Analysis Performed by GEL)
Vendor Parameter
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS 400 mg/L 25
Total Carbon
TOC 3.7 mg/L 0.1
Sample #: 2015018388
Matrix: GW WW
Analytical Lab
Page 5 of 84
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/22/2015 17:02
SLS2560
1
EPA 200.8
06/22/2015 17:02
SLS2560
1
EPA 200.8
06/22/2015 17:02
SLS2560
1
EPA 200.8
06/22/2015 17:02
SLS2560
1
EPA 200.8
06/22/2015 17:02
SLS2560
1
EPA 200.8
06/22/2015 17:02
SLS2560
1
EPA 200.8
06/22/2015 17:02
SLS2560
1
EPA 200.8
06/22/2015 17:02
SLS2560
1
EPA 200.8
06/22/2015 17:02
SLS2560
1
EPA 200.8
06/22/2015 17:02
SLS2560
1
EPA 200.8
06/22/2015 17:02
SLS2560
1
EPA 200.8
06/22/2015 17:02
SLS2560
1
EPA 200.8
06/22/2015 17:02
SLS2560
1
EPA 200.8
06/20/2015 21:55
JAHERMA
1
EPA 200.8
06/20/2015 21:55
JAHERMA
1
EPA 200.8
06/20/2015 21:55
JAHERMA
1
EPA 200.8
06/20/2015 21:55
JAHERMA
1
EPA 200.8
06/20/2015 21:55
JAHERMA
1
EPA 200.8
06/20/2015 21:55
JAHERMA
1
EPA 200.8
06/20/2015 21:55
JAHERMA
1
EPA 200.8
06/20/2015 21:55
JAHERMA
1
EPA 200.8
06/20/2015 21:55
JAHERMA
1
EPA 200.8
06/20/2015 21:55
JAHERMA
1
EPA 200.8
06/20/2015 21:55
JAHERMA
1
EPA 200.8
06/20/2015 21:55
JAHERMA
1
EPA 200.8
06/20/2015 21:55
JAHERMA
Vendor Method V_SHEALY
Vendor Method v GEL
Vendor Method V_ELE1
1 SM2540C 06/15/201510:03 AGIBBS5
1 SM5310C/EPA9060A 06/24/201514:12 GHUTCHI

Analytical Lab
Certificate of Laboratory Analysis Page 6 of 84
This report shall not be reproduced, except in full.
Order # J15060347
Site: IABMW-1S Sample #: 2015018388
Collection Date: 10-Jun-15 11:05 AM Matrix: GW WW
Analyte Result Units Qualifiers RDL DF Method Analysis Date/Time Analyst
TOTAL SUSPENDED SOLIDS
TSS 16 mg/L 5 1 SM2540D 06/12/2015 08:21 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: IABMW-1
Collection Date: 10-Jun-15 10:30 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.010
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
5.9
mg/L
0.1
Sulfate
64
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.013
mg/L
0.005
Barium (Ba)
0.599
mg/L
0.005
Boron (B)
1.15
mg/L
0.05
Iron (Fe)
6.40
mg/L
0.01
Manganese (Mn)
0.492
mg/L
0.005
Strontium (Sr)
5.10
mg/L
0.005
Zinc (Zn)
0.016
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
214
mg/L
0.1
Magnesium (Mg)
15.0
mg/L
0.005
Potassium (K)
17.7
mg/L
0.1
Sodium (Na)
39.5
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.018
mg/L
0.005
Barium (Ba)
0.622
mg/L
0.005
Boron (B)
1.21
mg/L
0.05
Iron (Fe)
6.60
mg/L
0.01
Manganese (Mn)
0.514
mg/L
0.005
Strontium (Sr)
5.28
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015018389
Matrix: GW WW
Analytical Lab
Page 7 of 84
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
06/17/2015 12:11
LSTARLI
1
EPA 300.0
06/15/2015 12:08
BGN9034
10
EPA 300.0
06/15/2015 12:08
BGN9034
1
EPA 245.1
06/18/2015 11:25
ACPAYNE
1
EPA 245.1
06/16/2015 11:07
ACPAYNE
1
EPA 200.7
06/12/2015 13:12
MHALL3
1
EPA 200.7
06/12/2015 13:12
MHALL3
1
EPA 200.7
06/12/2015 13:12
MHALL3
1
EPA 200.7
06/12/2015 13:12
MHALL3
1
EPA 200.7
06/12/2015 13:12
MHALL3
1
EPA 200.7
06/12/2015 13:12
MHALL3
1
EPA 200.7
06/12/2015 13:12
MHALL3
10
EPA 200.7
06/17/2015 13:02
MHALL3
1
EPA 200.7
06/17/2015 13:02
MHALL3
1
EPA 200.7
06/17/2015 13:02
MHALL3
1
EPA 200.7
06/17/2015 13:02
MHALL3
1
EPA 200.7
06/13/2015 14:54
MHALL3
1
EPA 200.7
06/13/2015 14:54
MHALL3
1
EPA 200.7
06/13/2015 14:54
MHALL3
1
EPA 200.7
06/13/2015 14:54
MHALL3
1
EPA 200.7
06/13/2015 14:54
MHALL3
1
EPA 200.7
06/13/2015 14:54
MHALL3
1
EPA 200.7
06/13/2015 14:54
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: IABMW-1
Collection Date: 10-Jun-15 10:30 AM
Analyte
Result
Units Qualifiers
RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
29.2
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
4.55
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
21.0
ug/L
1
Nickel (Ni)
4.74
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
1.09
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
30.1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
4.26
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
22.4
ug/L
1
Nickel (Ni)
4.44
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
1.25
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
RADIOLOGICAL - (Analysis Performed by GEL)
Vendor Parameter
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS 790 mg/L 25
Total Carbon
TOC 1.6 mg/L 0.1
Sample #: 2015018389
Matrix: GW WW
Analytical Lab
Page 8 of 84
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/22/2015 17:09
SLS2560
1
EPA 200.8
06/22/2015 17:09
SLS2560
1
EPA 200.8
06/22/2015 17:09
SLS2560
1
EPA 200.8
06/22/2015 17:09
SLS2560
1
EPA 200.8
06/22/2015 17:09
SLS2560
1
EPA 200.8
06/22/2015 17:09
SLS2560
1
EPA 200.8
06/22/2015 17:09
SLS2560
1
EPA 200.8
06/22/2015 17:09
SLS2560
1
EPA 200.8
06/22/2015 17:09
SLS2560
1
EPA 200.8
06/22/2015 17:09
SLS2560
1
EPA 200.8
06/22/2015 17:09
SLS2560
1
EPA 200.8
06/22/2015 17:09
SLS2560
1
EPA 200.8
06/22/2015 17:09
SLS2560
1
EPA 200.8
06/20/2015 22:02
JAHERMA
1
EPA 200.8
06/20/2015 22:02
JAHERMA
1
EPA 200.8
06/20/2015 22:02
JAHERMA
1
EPA 200.8
06/20/2015 22:02
JAHERMA
1
EPA 200.8
06/20/2015 22:02
JAHERMA
1
EPA 200.8
06/20/2015 22:02
JAHERMA
1
EPA 200.8
06/20/2015 22:02
JAHERMA
1
EPA 200.8
06/20/2015 22:02
JAHERMA
1
EPA 200.8
06/20/2015 22:02
JAHERMA
1
EPA 200.8
06/20/2015 22:02
JAHERMA
1
EPA 200.8
06/20/2015 22:02
JAHERMA
1
EPA 200.8
06/20/2015 22:02
JAHERMA
1
EPA 200.8
06/20/2015 22:02
JAHERMA
Vendor Method V_SHEALY
Vendor Method v GEL
Vendor Method V_ELE1
1 SM2540C 06/15/201510:03 AGIBBS5
1 SM5310C/EPA9060A 06/24/201514:12 GHUTCHI

Analytical Lab
Certificate of Laboratory Analysis Page 9 of 84
This report shall not be reproduced, except in full.
Order # J15060347
Site: IABMW-1 Sample #: 2015018389
Collection Date: 10-Jun-15 10:30 AM Matrix: GW WW
Analyte Result Units Qualifiers RDL DF Method Analysis Date/Time Analyst
TOTAL SUSPENDED SOLIDS
TSS 9.0 mg/L 5 1 SM2540D 06/12/2015 08:21 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: AMW-13S
Collection Date: 10-Jun-15 3:22 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.023
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
29
mg/L
1
Sulfate
16
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.005
mg/L
0.005
Barium (Ba)
0.090
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.044
mg/L
0.01
Manganese (Mn)
0.025
mg/L
0.005
Strontium (Sr)
0.064
mg/L
0.005
Zinc (Zn)
0.010
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
5.42
mg/L
0.01
Magnesium (Mg)
6.38
mg/L
0.005
Potassium (K)
0.197
mg/L
0.1
Sodium (Na)
20.3
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.012
mg/L
0.005
Barium (Ba)
0.096
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.066
mg/L
0.01
Manganese (Mn)
0.026
mg/L
0.005
Strontium (Sr)
0.066
mg/L
0.005
Zinc (Zn)
0.012
mg/L
0.005
Sample #: 2015018390
Matrix: GW WW
Analytical Lab
Page 10 of 84
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
06/17/2015 12:12
LSTARLI
10
EPA 300.0
06/15/2015 15:25
BGN9034
10
EPA 300.0
06/15/2015 15:25
BGN9034
1
EPA 245.1
06/18/2015 11:27
ACPAYNE
1
EPA 245.1
06/16/2015 11:09
ACPAYNE
1
EPA 200.7
06/12/2015 13:16
MHALL3
1
EPA 200.7
06/12/2015 13:16
MHALL3
1
EPA 200.7
06/12/2015 13:16
MHALL3
1
EPA 200.7
06/12/2015 13:16
MHALL3
1
EPA 200.7
06/12/2015 13:16
MHALL3
1
EPA 200.7
06/12/2015 13:16
MHALL3
1
EPA 200.7
06/12/2015 13:16
MHALL3
1
EPA 200.7
06/17/2015 13:10
MHALL3
1
EPA 200.7
06/17/2015 13:10
MHALL3
1
EPA 200.7
06/17/2015 13:10
MHALL3
1
EPA 200.7
06/17/2015 13:10
MHALL3
1
EPA 200.7
06/13/2015 14:58
MHALL3
1
EPA 200.7
06/13/2015 14:58
MHALL3
1
EPA 200.7
06/13/2015 14:58
MHALL3
1
EPA 200.7
06/13/2015 14:58
MHALL3
1
EPA 200.7
06/13/2015 14:58
MHALL3
1
EPA 200.7
06/13/2015 14:58
MHALL3
1
EPA 200.7
06/13/2015 14:58
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: AMW-13S
Collection Date: 10-Jun-15 3:22 PM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
1.31
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
7.15
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
4.81
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
7.28
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
140
mg/L
25
Total Carbon
TOC
1.6
mg/L
0.1
TOTAL SUSPENDED SOLIDS
TSS
< 5
mg/L
5
Sample #: 2015018390
Matrix: GW WW
Analytical Lab
Page 11 of 84
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/22/2015 17:16
SLS2560
1
EPA 200.8
06/22/2015 17:16
SLS2560
1
EPA 200.8
06/22/2015 17:16
SLS2560
1
EPA 200.8
06/22/2015 17:16
SLS2560
1
EPA 200.8
06/22/2015 17:16
SLS2560
1
EPA 200.8
06/22/2015 17:16
SLS2560
1
EPA 200.8
06/22/2015 17:16
SLS2560
1
EPA 200.8
06/22/2015 17:16
SLS2560
1
EPA 200.8
06/22/2015 17:16
SLS2560
1
EPA 200.8
06/22/2015 17:16
SLS2560
1
EPA 200.8
06/22/2015 17:16
SLS2560
1
EPA 200.8
06/22/2015 17:16
SLS2560
1
EPA 200.8
06/22/2015 17:16
SLS2560
1
EPA 200.8
06/20/2015 21:34
JAHERMA
1
EPA 200.8
06/20/2015 21:34
JAHERMA
1
EPA 200.8
06/20/2015 21:34
JAHERMA
1
EPA 200.8
06/20/2015 21:34
JAHERMA
1
EPA 200.8
06/20/2015 21:34
JAHERMA
1
EPA 200.8
06/20/2015 21:34
JAHERMA
1
EPA 200.8
06/20/2015 21:34
JAHERMA
1
EPA 200.8
06/20/2015 21:34
JAHERMA
1
EPA 200.8
06/20/2015 21:34
JAHERMA
1
EPA 200.8
06/20/2015 21:34
JAHERMA
1
EPA 200.8
06/20/2015 21:34
JAHERMA
1
EPA 200.8
06/20/2015 21:34
JAHERMA
1
EPA 200.8
06/20/2015 21:34
JAHERMA
Vendor Method V_SHEALY
Vendor Method V_ELE1
1 SM2540C 06/15/201510:03 AGIBBS5
1 SM5310C/EPA9060A 06/24/201514:12 GHUTCHI
1 SM2540D 06/12/2015 08:21 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: AMW-13BC
Collection Date: 10-Jun-15 4:00 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
16
mg/L
1
Sulfate
5.7
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.027
mg/L
0.005
Barium (Ba)
0.339
mg/L
0.005
Boron (B)
0.072
mg/L
0.05
Iron (Fe)
10.6
mg/L
0.01
Manganese (Mn)
0.097
mg/L
0.005
Strontium (Sr)
0.124
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
31.6
mg/L
0.01
Magnesium (Mg)
7.65
mg/L
0.005
Potassium (K)
1.59
mg/L
0.1
Sodium (Na)
15.8
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.075
mg/L
0.005
Barium (Ba)
0.342
mg/L
0.005
Boron (B)
0.073
mg/L
0.05
Iron (Fe)
10.8
mg/L
0.01
Manganese (Mn)
0.099
mg/L
0.005
Strontium (Sr)
0.125
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015018391
Matrix: GW WW
Analytical Lab
Page 12 of 84
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
06/17/2015 12:13
LSTARLI
10
EPA 300.0
06/15/2015 18:58
BGN9034
1
EPA 300.0
06/15/2015 18:58
BGN9034
1
EPA 245.1
06/18/2015 11:29
ACPAYNE
1
EPA 245.1
06/16/2015 11:11
ACPAYNE
1
EPA 200.7
06/12/2015 13:20
MHALL3
1
EPA 200.7
06/12/2015 13:20
MHALL3
1
EPA 200.7
06/12/2015 13:20
MHALL3
1
EPA 200.7
06/12/2015 13:20
MHALL3
1
EPA 200.7
06/12/2015 13:20
MHALL3
1
EPA 200.7
06/12/2015 13:20
MHALL3
1
EPA 200.7
06/12/2015 13:20
MHALL3
1
EPA 200.7
06/17/2015 13:14
MHALL3
1
EPA 200.7
06/17/2015 13:14
MHALL3
1
EPA 200.7
06/17/2015 13:14
MHALL3
1
EPA 200.7
06/17/2015 13:14
MHALL3
1
EPA 200.7
06/13/2015 15:01
MHALL3
1
EPA 200.7
06/13/2015 15:01
MHALL3
1
EPA 200.7
06/13/2015 15:01
MHALL3
1
EPA 200.7
06/13/2015 15:01
MHALL3
1
EPA 200.7
06/13/2015 15:01
MHALL3
1
EPA 200.7
06/13/2015 15:01
MHALL3
1
EPA 200.7
06/13/2015 15:01
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: AMW-13BC
Collection Date: 10-Jun-15 4:00 PM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
1.11
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
0.324
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
170
mg/L
25
Total Carbon
TOC
1.4
mg/L
0.1
TOTAL SUSPENDED SOLIDS
TSS
12
mg/L
5
Sample #: 2015018391
Matrix: GW WW
Analytical Lab
Page 13 of 84
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/22/2015 17:24
SLS2560
1
EPA 200.8
06/22/2015 17:24
SLS2560
1
EPA 200.8
06/22/2015 17:24
SLS2560
1
EPA 200.8
06/22/2015 17:24
SLS2560
1
EPA 200.8
06/22/2015 17:24
SLS2560
1
EPA 200.8
06/22/2015 17:24
SLS2560
1
EPA 200.8
06/22/2015 17:24
SLS2560
1
EPA 200.8
06/22/2015 17:24
SLS2560
1
EPA 200.8
06/22/2015 17:24
SLS2560
1
EPA 200.8
06/22/2015 17:24
SLS2560
1
EPA 200.8
06/22/2015 17:24
SLS2560
1
EPA 200.8
06/22/2015 17:24
SLS2560
1
EPA 200.8
06/22/2015 17:24
SLS2560
1
EPA 200.8
06/20/2015 22:09
JAHERMA
1
EPA 200.8
06/20/2015 22:09
JAHERMA
1
EPA 200.8
06/20/2015 22:09
JAHERMA
1
EPA 200.8
06/20/2015 22:09
JAHERMA
1
EPA 200.8
06/20/2015 22:09
JAHERMA
1
EPA 200.8
06/20/2015 22:09
JAHERMA
1
EPA 200.8
06/20/2015 22:09
JAHERMA
1
EPA 200.8
06/20/2015 22:09
JAHERMA
1
EPA 200.8
06/20/2015 22:09
JAHERMA
1
EPA 200.8
06/20/2015 22:09
JAHERMA
1
EPA 200.8
06/20/2015 22:09
JAHERMA
1
EPA 200.8
06/20/2015 22:09
JAHERMA
1
EPA 200.8
06/20/2015 22:09
JAHERMA
Vendor Method V_SHEALY
Vendor Method V_ELE1
1 SM2540C 06/15/201510:03 AGIBBS5
1 SM5310C/EPA9060A 06/24/201514:12 GHUTCHI
1 SM2540D 06/12/2015 09:12 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: IABMW-3S
Collection Date: 10-Jun-15 10:25 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
9.4
mg/L
0.1
Sulfate
42
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.100
mg/L
0.005
Barium (Ba)
0.204
mg/L
0.005
Boron (B)
0.622
mg/L
0.05
Iron (Fe)
57.1
mg/L
0.1
Manganese (Mn)
1.18
mg/L
0.005
Strontium (Sr)
0.489
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
26.4
mg/L
0.01
Magnesium (Mg)
10.6
mg/L
0.005
Potassium (K)
1.64
mg/L
0.1
Sodium (Na)
13.0
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.115
mg/L
0.005
Barium (Ba)
0.221
mg/L
0.005
Boron (B)
0.655
mg/L
0.05
Iron (Fe)
58.0
mg/L
0.1
Manganese (Mn)
1.21
mg/L
0.005
Strontium (Sr)
0.544
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015018392
Matrix: GW WW
Analytical Lab
Page 14 of 84
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
06/17/2015 12:14
LSTARLI
1
EPA 300.0
06/15/2015 19:15
BGN9034
10
EPA 300.0
06/15/2015 19:15
BGN9034
1
EPA 245.1
06/18/2015 11:32
ACPAYNE
1
EPA 245.1
06/16/2015 11:14
ACPAYNE
1
EPA 200.7
06/12/2015 13:24
MHALL3
1
EPA 200.7
06/12/2015 13:24
MHALL3
1
EPA 200.7
06/12/2015 13:24
MHALL3
10
EPA 200.7
06/12/2015 13:24
MHALL3
1
EPA 200.7
06/12/2015 13:24
MHALL3
1
EPA 200.7
06/12/2015 13:24
MHALL3
1
EPA 200.7
06/12/2015 13:24
MHALL3
1
EPA 200.7
06/17/2015 13:17
MHALL3
1
EPA 200.7
06/17/2015 13:17
MHALL3
1
EPA 200.7
06/17/2015 13:17
MHALL3
1
EPA 200.7
06/17/2015 13:17
MHALL3
1
EPA 200.7
06/13/2015 15:05
MHALL3
1
EPA 200.7
06/13/2015 15:05
MHALL3
1
EPA 200.7
06/13/2015 15:05
MHALL3
10
EPA 200.7
06/13/2015 15:05
MHALL3
1
EPA 200.7
06/13/2015 15:05
MHALL3
1
EPA 200.7
06/13/2015 15:05
MHALL3
1
EPA 200.7
06/13/2015 15:05
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: IABMW-3S
Collection Date: 10-Jun-15 10:25 AM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
3.44
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
1.28
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
1.12
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
0.624
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
4.29
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
1.21
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
1.13
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
0.743
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
230
mg/L
25
Total Carbon
TOC
4.5
mg/L
0.1
TOTAL SUSPENDED SOLIDS
TSS
34
mg/L
5
Sample #: 2015018392
Matrix: GW WW
Analytical Lab
Page 15 of 84
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/22/2015 17:31
SLS2560
1
EPA 200.8
06/22/2015 17:31
SLS2560
1
EPA 200.8
06/22/2015 17:31
SLS2560
1
EPA 200.8
06/22/2015 17:31
SLS2560
1
EPA 200.8
06/22/2015 17:31
SLS2560
1
EPA 200.8
06/22/2015 17:31
SLS2560
1
EPA 200.8
06/22/2015 17:31
SLS2560
1
EPA 200.8
06/22/2015 17:31
SLS2560
1
EPA 200.8
06/22/2015 17:31
SLS2560
1
EPA 200.8
06/22/2015 17:31
SLS2560
1
EPA 200.8
06/22/2015 17:31
SLS2560
1
EPA 200.8
06/22/2015 17:31
SLS2560
1
EPA 200.8
06/22/2015 17:31
SLS2560
1
EPA 200.8
06/20/2015 22:16
JAHERMA
1
EPA 200.8
06/20/2015 22:16
JAHERMA
1
EPA 200.8
06/20/2015 22:16
JAHERMA
1
EPA 200.8
06/20/2015 22:16
JAHERMA
1
EPA 200.8
06/20/2015 22:16
JAHERMA
1
EPA 200.8
06/20/2015 22:16
JAHERMA
1
EPA 200.8
06/20/2015 22:16
JAHERMA
1
EPA 200.8
06/20/2015 22:16
JAHERMA
1
EPA 200.8
06/20/2015 22:16
JAHERMA
1
EPA 200.8
06/20/2015 22:16
JAHERMA
1
EPA 200.8
06/20/2015 22:16
JAHERMA
1
EPA 200.8
06/20/2015 22:16
JAHERMA
1
EPA 200.8
06/20/2015 22:16
JAHERMA
Vendor Method V_SHEALY
Vendor Method V_ELE1
1 SM2540C 06/15/201510:03 AGIBBS5
1 SM5310C/EPA9060A 06/24/201514:12 GHUTCHI
1 SM2540D 06/12/2015 09:12 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: IABMW-2S
Collection Date: 10-Jun-15 1:05 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.042
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
17
mg/L
1
Sulfate
98
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.047
mg/L
0.005
Barium (Ba)
0.223
mg/L
0.005
Boron (B)
1.67
mg/L
0.05
Iron (Fe)
24.6
mg/L
0.01
Manganese (Mn)
4.62
mg/L
0.005
Strontium (Sr)
2.92
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
91.3
mg/L
0.01
Magnesium (Mg)
46.1
mg/L
0.005
Potassium (K)
1.11
mg/L
0.1
Sodium (Na)
17.6
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.057
mg/L
0.005
Barium (Ba)
0.231
mg/L
0.005
Boron (B)
1.72
mg/L
0.05
Iron (Fe)
25.3
mg/L
0.01
Manganese (Mn)
4.74
mg/L
0.005
Strontium (Sr)
3.00
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015018393
Matrix: GW WW
Analytical Lab
Page 16 of 84
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
06/17/2015 12:15
LSTARLI
10
EPA 300.0
06/15/2015 16:47
BGN9034
10
EPA 300.0
06/15/2015 16:47
BGN9034
1
EPA 245.1
06/18/2015 11:48
ACPAYNE
1
EPA 245.1
06/16/2015 11:16
ACPAYNE
1
EPA 200.7
06/12/2015 13:28
MHALL3
1
EPA 200.7
06/12/2015 13:28
MHALL3
1
EPA 200.7
06/12/2015 13:28
MHALL3
1
EPA 200.7
06/12/2015 13:28
MHALL3
1
EPA 200.7
06/12/2015 13:28
MHALL3
1
EPA 200.7
06/12/2015 13:28
MHALL3
1
EPA 200.7
06/12/2015 13:28
MHALL3
1
EPA 200.7
06/17/2015 13:49
MHALL3
1
EPA 200.7
06/17/2015 13:49
MHALL3
1
EPA 200.7
06/17/2015 13:49
MHALL3
1
EPA 200.7
06/17/2015 13:49
MHALL3
1
EPA 200.7
06/13/2015 15:09
MHALL3
1
EPA 200.7
06/13/2015 15:09
MHALL3
1
EPA 200.7
06/13/2015 15:09
MHALL3
1
EPA 200.7
06/13/2015 15:09
MHALL3
1
EPA 200.7
06/13/2015 15:09
MHALL3
1
EPA 200.7
06/13/2015 15:09
MHALL3
1
EPA 200.7
06/13/2015 15:09
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: IABMW-2S
Collection Date: 10-Jun-15 1:05 PM
Analyte
Result
Units Qualifiers
RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
6.09
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
50.9
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
2.20
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
6.75
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
50.6
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
2.27
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
0.368
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
570
mg/L
25
Total Carbon
TOC
3.1
mg/L
0.1
TOTAL SUSPENDED SOLIDS
TSS
23
mg/L
5
Sample #: 2015018393
Matrix: GW WW
Analytical Lab
Page 17 of 84
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/22/2015 18:29
SLS2560
1
EPA 200.8
06/22/2015 18:29
SLS2560
1
EPA 200.8
06/22/2015 18:29
SLS2560
1
EPA 200.8
06/22/2015 18:29
SLS2560
1
EPA 200.8
06/22/2015 18:29
SLS2560
1
EPA 200.8
06/22/2015 18:29
SLS2560
1
EPA 200.8
06/22/2015 18:29
SLS2560
1
EPA 200.8
06/22/2015 18:29
SLS2560
1
EPA 200.8
06/22/2015 18:29
SLS2560
1
EPA 200.8
06/22/2015 18:29
SLS2560
1
EPA 200.8
06/22/2015 18:29
SLS2560
1
EPA 200.8
06/22/2015 18:29
SLS2560
1
EPA 200.8
06/22/2015 18:29
SLS2560
1
EPA 200.8
06/20/2015 22:23
JAHERMA
1
EPA 200.8
06/20/2015 22:23
JAHERMA
1
EPA 200.8
06/20/2015 22:23
JAHERMA
1
EPA 200.8
06/20/2015 22:23
JAHERMA
1
EPA 200.8
06/20/2015 22:23
JAHERMA
1
EPA 200.8
06/20/2015 22:23
JAHERMA
1
EPA 200.8
06/20/2015 22:23
JAHERMA
1
EPA 200.8
06/20/2015 22:23
JAHERMA
1
EPA 200.8
06/20/2015 22:23
JAHERMA
1
EPA 200.8
06/20/2015 22:23
JAHERMA
1
EPA 200.8
06/20/2015 22:23
JAHERMA
1
EPA 200.8
06/20/2015 22:23
JAHERMA
1
EPA 200.8
06/20/2015 22:23
JAHERMA
Vendor Method V_SHEALY
Vendor Method V_ELE1
1 SM2540C 06/15/201510:03 AGIBBS5
1 SM5310C/EPA9060A 06/24/201514:12 GHUTCHI
1 SM2540D 06/12/2015 09:12 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: AMW-12S
Collection Date: 10-Jun-15 4:53 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
4.2
mg-N/L
0.05
INORGANIC IONS BY IC
Chloride
11
mg/L
1
Sulfate
4.9
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
1.10
mg/L
0.005
Barium (Ba)
0.146
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.010
mg/L
0.01
Manganese (Mn)
0.020
mg/L
0.005
Strontium (Sr)
0.026
mg/L
0.005
Zinc (Zn)
0.013
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
1.58
mg/L
0.01
Magnesium (Mg)
2.69
mg/L
0.005
Potassium (K)
2.47
mg/L
0.1
Sodium (Na)
4.25
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
1.10
mg/L
0.005
Barium (Ba)
0.152
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.060
mg/L
0.01
Manganese (Mn)
0.020
mg/L
0.005
Strontium (Sr)
0.026
mg/L
0.005
Zinc (Zn)
0.014
mg/L
0.005
Sample #: 2015018394
Matrix: GW WW
Analytical Lab
Page 18 of 84
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
5
EPA 353.2
06/17/2015 12:25
LSTARLI
10
EPA 300.0
06/15/2015 19:48
BGN9034
1
EPA 300.0
06/15/2015 19:48
BGN9034
1
EPA 245.1
06/18/2015 11:55
ACPAYNE
1
EPA 245.1
06/16/2015 11:18
ACPAYNE
1
EPA 200.7
06/12/2015 13:47
MHALL3
1
EPA 200.7
06/12/2015 13:47
MHALL3
1
EPA 200.7
06/12/2015 13:47
MHALL3
1
EPA 200.7
06/12/2015 13:47
MHALL3
1
EPA 200.7
06/12/2015 13:47
MHALL3
1
EPA 200.7
06/12/2015 13:47
MHALL3
1
EPA 200.7
06/12/2015 13:47
MHALL3
1
EPA 200.7
06/17/2015 10:31
MHALL3
1
EPA 200.7
06/17/2015 10:31
MHALL3
1
EPA 200.7
06/17/2015 10:31
MHALL3
1
EPA 200.7
06/17/2015 10:31
MHALL3
1
EPA 200.7
06/13/2015 15:13
MHALL3
1
EPA 200.7
06/13/2015 15:13
MHALL3
1
EPA 200.7
06/13/2015 15:13
MHALL3
1
EPA 200.7
06/13/2015 15:13
MHALL3
1
EPA 200.7
06/13/2015 15:13
MHALL3
1
EPA 200.7
06/13/2015 15:13
MHALL3
1
EPA 200.7
06/13/2015 15:13
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: AMW-12S
Collection Date: 10-Jun-15 4:53 PM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
2.93
ug/L
1
Copper (Cu)
6.52
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
3.70
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
0.289
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
3.17
ug/L
1
Copper (Cu)
5.61
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
4.21
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
RADIOLOGICAL - (Analysis Performed by GEL)
Vendor Parameter
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS 56 mg/L 25
Total Carbon
TOC 0.390 mg/L 0.1
Sample #: 2015018394
Matrix: GW WW
Analytical Lab
Page 19 of 84
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/22/2015 18:51
SLS2560
1
EPA 200.8
06/22/2015 18:51
SLS2560
1
EPA 200.8
06/22/2015 18:51
SLS2560
1
EPA 200.8
06/22/2015 18:51
SLS2560
1
EPA 200.8
06/22/2015 18:51
SLS2560
1
EPA 200.8
06/22/2015 18:51
SLS2560
1
EPA 200.8
06/22/2015 18:51
SLS2560
1
EPA 200.8
06/22/2015 18:51
SLS2560
1
EPA 200.8
06/22/2015 18:51
SLS2560
1
EPA 200.8
06/22/2015 18:51
SLS2560
1
EPA 200.8
06/22/2015 18:51
SLS2560
1
EPA 200.8
06/22/2015 18:51
SLS2560
1
EPA 200.8
06/22/2015 18:51
SLS2560
1
EPA 200.8
06/20/2015 22:30
JAHERMA
1
EPA 200.8
06/20/2015 22:30
JAHERMA
1
EPA 200.8
06/20/2015 22:30
JAHERMA
1
EPA 200.8
06/20/2015 22:30
JAHERMA
1
EPA 200.8
06/20/2015 22:30
JAHERMA
1
EPA 200.8
06/20/2015 22:30
JAHERMA
1
EPA 200.8
06/20/2015 22:30
JAHERMA
1
EPA 200.8
06/20/2015 22:30
JAHERMA
1
EPA 200.8
06/20/2015 22:30
JAHERMA
1
EPA 200.8
06/20/2015 22:30
JAHERMA
1
EPA 200.8
06/20/2015 22:30
JAHERMA
1
EPA 200.8
06/20/2015 22:30
JAHERMA
1
EPA 200.8
06/20/2015 22:30
JAHERMA
Vendor Method V_SHEALY
Vendor Method v GEL
Vendor Method V_ELE1
1 SM2540C 06/15/201510:03 AGIBBS5
1 SM5310C/EPA9060A 06/24/201514:12 GHUTCHI

Analytical Lab
Certificate of Laboratory Analysis Page 20 of 84
This report shall not be reproduced, except in full.
Order # J15060347
Site: AMW-12S Sample #: 2015018394
Collection Date: 10-Jun-15 4:53 PM Matrix: GW WW
Analyte Result Units Qualifiers RDL DF Method Analysis Date/Time Analyst
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L 5 1 SM2540D 06/12/2015 09:12 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: AMW-12BC
Collection Date: 10-Jun-15 3:41 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.025
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
8.6
mg/L
0.1
Sulfate
8.4
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.025
mg/L
0.005
Barium (Ba)
0.012
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
12.2
mg/L
0.01
Manganese (Mn)
0.278
mg/L
0.005
Strontium (Sr)
0.033
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
6.21
mg/L
0.01
Magnesium (Mg)
2.28
mg/L
0.005
Potassium (K)
0.875
mg/L
0.1
Sodium (Na)
11.3
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.031
mg/L
0.005
Barium (Ba)
0.013
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
12.6
mg/L
0.01
Manganese (Mn)
0.287
mg/L
0.005
Strontium (Sr)
0.034
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015018395
Matrix: GW WW
Analytical Lab
Page 21 of 84
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2
06/17/2015 12:18
LSTARLI
1 EPA 300.0
06/15/2015 20:04
BGN9034
1 EPA 300.0
06/15/2015 20:04
BGN9034
1 EPA 245.1
06/16/2015 11:39
ACPAYNE
1 EPA 245.1
06/16/2015 11:39
ACPAYNE
1 EPA 200.7
06/12/2015 13:59
MHALL3
1 EPA 200.7
06/12/2015 13:59
MHALL3
1 EPA 200.7
06/12/2015 13:59
MHALL3
1 EPA 200.7
06/12/2015 13:59
MHALL3
1 EPA 200.7
06/12/2015 13:59
MHALL3
1 EPA 200.7
06/12/2015 13:59
MHALL3
1 EPA 200.7
06/12/2015 13:59
MHALL3
1 EPA 200.7
06/17/2015 13:21
MHALL3
1 EPA 200.7
06/17/2015 13:21
MHALL3
1 EPA 200.7
06/17/2015 13:21
MHALL3
1 EPA 200.7
06/17/2015 13:21
MHALL3
1 EPA 200.7
06/13/2015 15:17
MHALL3
1 EPA 200.7
06/13/2015 15:17
MHALL3
1 EPA 200.7
06/13/2015 15:17
MHALL3
1 EPA 200.7
06/13/2015 15:17
MHALL3
1 EPA 200.7
06/13/2015 15:17
MHALL3
1 EPA 200.7
06/13/2015 15:17
MHALL3
1 EPA 200.7
06/13/2015 15:17
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: AMW-12BC
Collection Date: 10-Jun-15 3:41 PM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
RADIOLOGICAL - (Analysis Performed by GEL)
Vendor Parameter
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS 87 mg/L 25
Total Carbon
TOC 0.579 mg/L 0.1
Sample #: 2015018395
Matrix: GW WW
Analytical Lab
Page 22 of 84
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/22/2015 18:58
SLS2560
1
EPA 200.8
06/22/2015 18:58
SLS2560
1
EPA 200.8
06/22/2015 18:58
SLS2560
1
EPA 200.8
06/22/2015 18:58
SLS2560
1
EPA 200.8
06/22/2015 18:58
SLS2560
1
EPA 200.8
06/22/2015 18:58
SLS2560
1
EPA 200.8
06/22/2015 18:58
SLS2560
1
EPA 200.8
06/22/2015 18:58
SLS2560
1
EPA 200.8
06/22/2015 18:58
SLS2560
1
EPA 200.8
06/22/2015 18:58
SLS2560
1
EPA 200.8
06/22/2015 18:58
SLS2560
1
EPA 200.8
06/22/2015 18:58
SLS2560
1
EPA 200.8
06/22/2015 18:58
SLS2560
1
EPA 200.8
06/20/2015 22:37
JAHERMA
1
EPA 200.8
06/20/2015 22:37
JAHERMA
1
EPA 200.8
06/20/2015 22:37
JAHERMA
1
EPA 200.8
06/20/2015 22:37
JAHERMA
1
EPA 200.8
06/20/2015 22:37
JAHERMA
1
EPA 200.8
06/20/2015 22:37
JAHERMA
1
EPA 200.8
06/20/2015 22:37
JAHERMA
1
EPA 200.8
06/20/2015 22:37
JAHERMA
1
EPA 200.8
06/20/2015 22:37
JAHERMA
1
EPA 200.8
06/20/2015 22:37
JAHERMA
1
EPA 200.8
06/20/2015 22:37
JAHERMA
1
EPA 200.8
06/20/2015 22:37
JAHERMA
1
EPA 200.8
06/20/2015 22:37
JAHERMA
Vendor Method V_SHEALY
Vendor Method v GEL
Vendor Method V_ELE1
1 SM2540C 06/15/201514:29 AGIBBS5
1 SM5310C/EPA9060A 06/24/201514:12 GHUTCHI

Analytical Lab
Certificate of Laboratory Analysis Page 23 of 84
This report shall not be reproduced, except in full.
Order # J15060347
Site: AMW-12BC Sample #: 2015018395
Collection Date: 10-Jun-15 3:41 PM Matrix: GW WW
Analyte Result Units Qualifiers RDL DF Method Analysis Date/Time Analyst
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L 5 1 SM2540D 06/12/2015 09:12 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: Filter Blank
Collection Date: 10-Jun-15 8:04 AM
Analyte
Result
Units
Qualifiers RDL
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015018396
Matrix: GW WW
Analytical Lab
Page 24 of 84
DF
Method
Analysis Date/Time
Analyst
1
EPA 245.1
06/16/2015 11:27
ACPAYNE
1
EPA 200.7
06/12/2015 14:03
MHALL3
1
EPA 200.7
06/12/2015 14:03
MHALL3
1
EPA 200.7
06/12/2015 14:03
MHALL3
1
EPA 200.7
06/12/2015 14:03
MHALL3
1
EPA 200.7
06/12/2015 14:03
MHALL3
1
EPA 200.7
06/12/2015 14:03
MHALL3
1
EPA 200.7
06/12/2015 14:03
MHALL3
1
EPA 200.8
06/22/2015 19:05
SLS2560
1
EPA 200.8
06/22/2015 19:05
SLS2560
1
EPA 200.8
06/22/2015 19:05
SLS2560
1
EPA 200.8
06/22/2015 19:05
SLS2560
1
EPA 200.8
06/22/2015 19:05
SLS2560
1
EPA 200.8
06/22/2015 19:05
SLS2560
1
EPA 200.8
06/22/2015 19:05
SLS2560
1
EPA 200.8
06/22/2015 19:05
SLS2560
1
EPA 200.8
06/22/2015 19:05
SLS2560
1
EPA 200.8
06/22/2015 19:05
SLS2560
1
EPA 200.8
06/22/2015 19:05
SLS2560
1
EPA 200.8
06/22/2015 19:05
SLS2560
1
EPA 200.8
06/22/2015 19:05
SLS2560

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: Equipment Blank
Collection Date: 10-Jun-15 8:04 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
< 0.1
mg/L
0.1
Sulfate
< 0.1
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
UNDIGESTED METALS BY lCP
Calcium (Ca)
0.027
mg/L
0.01
Magnesium (Mg)
< 0.005
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
< 0.05
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Analytical Lab
Page 25 of 84
Sample #: 2015018397
Matrix: GW WW
DF Method Analysis Date/Time Analyst
Vendor Method V_SHEALY
1 EPA 353.2
06/17/2015 12:19
LSTARLI
1 EPA 300.0
06/15/2015 17:36
BGN9034
1 EPA 300.0
06/15/2015 17:36
BGN9034
1 EPA 245.1
06/18/2015 12:00
ACPAYNE
1 EPA 200.7
06/17/2015 09:57
MHALL3
1 EPA 200.7
06/17/2015 09:57
MHALL3
1 EPA 200.7
06/17/2015 09:57
MHALL3
1 EPA 200.7
06/17/2015 09:57
MHALL3
1 EPA 200.7
06/13/2015 15:21
MHALL3
1 EPA 200.7
06/13/2015 15:21
MHALL3
1 EPA 200.7
06/13/2015 15:21
MHALL3
1 EPA 200.7
06/13/2015 15:21
MHALL3
1 EPA 200.7
06/13/2015 15:21
MHALL3
1 EPA 200.7
06/13/2015 15:21
MHALL3
1 EPA 200.7
06/13/2015 15:21
MHALL3
1 EPA 200.8
06/20/2015 22:44
JAHERMA
1 EPA 200.8
06/20/2015 22:44
JAHERMA
1 EPA 200.8
06/20/2015 22:44
JAHERMA
1 EPA 200.8
06/20/2015 22:44
JAHERMA
1 EPA 200.8
06/20/2015 22:44
JAHERMA
1 EPA 200.8
06/20/2015 22:44
JAHERMA
1 EPA 200.8
06/20/2015 22:44
JAHERMA
1 EPA 200.8
06/20/2015 22:44
JAHERMA
1 EPA 200.8
06/20/2015 22:44
JAHERMA
1 EPA 200.8
06/20/2015 22:44
JAHERMA
1 EPA 200.8
06/20/2015 22:44
JAHERMA
1 EPA 200.8
06/20/2015 22:44
JAHERMA
1 EPA 200.8
06/20/2015 22:44
JAHERMA
METHANE - (Analysis Performed by Shealy Labs
Methane (CH4) Complete
Vendor Method V_SHEALY

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060347
Site: Equipment Blank
Collection Date: 10-Jun-15 8:04 AM
Analyte Result Units Qualifiers RDL DF
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete
TOTAL DISSOLVED SOLIDS
TDS < 25 mg/L 25 1
Total Carbon
Sample #: 2015018397
Matrix: GW WW
Analytical Lab
Page 26 of 84
Method Analysis Date/Time Analyst
Vendor Method
V_ELE1
SM2540C 06/15/201514:29 AGIBBS5
TOC 0.276 mg/L 0.1 1 SM5310C/EPA9060A 06/24/201514:12 GHUTCHI
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L 5 1 SM2540D 06/12/2015 09:12 AGIBBS5
Qualifiers:
M2 Matrix spike recovery was Low: the associated Laboratory Control Spike (LCS) was acceptable.
R1 Relative Percent Difference exceeded method acceptance limits, see additional notes.
-- Additional Information --
R1 - RPD for MS/MSD of this sample was greater than the control limits for Iron (24.7% difference). The sample
concentration was disproportionate to the spiking concentration.

Analytical Lab
Page 27 of 84
Element One Onc.
6319-D Carolina Beach Rd.
Wilmington, NC 28412
Phone: [phone]
Fax: [phone]
[e-mail]
REPORT OF ANALYSES
Duke Energy
June 16, 2015
Laboratory Services
Client Project Name AB GW Assessment water (wells) HF Lee
13339 Hagers Ferry Road Bld. MG03A Client Project Number J15060347
Huntersville, NC 28078
PO Number
Sample Matrix GW WW
Sample Type Grab Date Received
06/12/2015
Date Analyzed 06/15/2015
Method SM 4500 S2- D Time Received
1345
Delivered by FedEx
Received by
JRC
eOne ID Duke Energy ID
Parameter Result Unit Dil DL Date
Sampled
Time
Sampled
25054-1 IABMW-1 S
Sulfide < 0.1 mg/L 1 0.1 06/10/15
1105
25054-2*
IABMW-1
Sulfide
< 0.2
mg/L
2
0.1
06/10/15
1030
25054-3
AMW-13S
Sulfide
< 0.1
mg/L
1
0.1
06/10/15
1522
25054-4
AMW-1313C
Sulfide
< 0.1
mg/L
1
0.1
06/10/15
1600
25054-5*
IABMW-3S
Sulfide
< 0.2
mg/L
2
0.1
06/10/15
1025
25054-6
IABMW-2S
Sulfide
< 0.1
mg/L
1
0.1
06/10/15
1305
25054-7
AMW-12S
Sulfide
< 0.1
mg/L
1
0.1
06/10/15
1653
25054-8
AMW-1213C
Sulfide
0.201
mg/L
1
0.1
06/10/15
1541
*Sample spike recovery outside of QA limits of 85-115%; dilution necessary to meet laboratory QA limits.
Ken mith, Laboratory Director
25054 Duke Report Packet Compiled by �
NC Certifications: DW 37788 and DWQ DENR 604

Analytical Lab
Page 28 of 84
lemerlt• _
REPORT OF ANALYSES
Elernent One lace
6319-D Carolina Beach Rd.
Wilmington, VAC 28412
Phone: [phone]
Fax: [phone]
[e-mail]
Duke Energy
June 16, 2015
Laboratory Services
Client Project Name AB GW Assessment water (wells) HF Lee
13339 Hagers Ferry Road Bld. MG03A
Client Project Number J15060347
Huntersville, NC 28078
PO Number
Sample Matrix GW WW
Sample Type Grab Date Received
06/12/2015
Date Analyzed 06/15/2015
Method SM 4500 S2- D Time Received
1345
Delivered by FedEx
Received by
JRC
eOne ID Duke Energy ID
Parameter Result Unit Dil DL Date
Sampled
Time
Sampled
25054-9 Equipment Blank
Sulfide < 0.1 mg/L 1 0.1 06/10/15
0804
1-1
(4/cjw-
Ken Smith, Laboratory Director
25054 Duke Report Packet Compiled by '1-`
NC Certifications: DW 37788 and DWQ DENR 604

Analytical Lab
Page 29 of 84
W
m
L
i
Q!
C
jaulajuOO g lejO.L
O
O
O
O
O
O
O
O
O O O P
O
m O
O
N
N
Lu
�
_I
4
J 11 81B{aUl
i O N pan osios s as
_ �
I
_
-�
--
N
O a w
Is z aas)sle;alry
-�
,
\
N
— r
y o
I
E Q 3
o
T
....................
--4
i
—
w-13`J-A
N i WE PUB SZZ)
wnlpeal%qal
—t
N
j
Wlml E a a w (43uawe13-A)
spUlnS
o r ewuoyep
'Aluumv
J
ewMN
m: m a
I
1
N
zx M n '4oS 'I7
$ tl O
fit
E „ AIeemsA (SLt
£ I1 SS1
^�
E
. V
N
x
X
R
ec
o q..a
a
m
y
r •dwo 3
Cq si o N r" 1
z
m N
o a
J Y
JJ c
111
F
J A
T ((�� a
C
l
a v
V1 N
i
V i V
00
tE
N
3 a o
o
'Jt�
'a
^1
d
�i�
In
b'
I
�I'
In
p
r�l CD C N U
m a L 0 o
�yE'
8
�•
Z U
°
'�
a
u
og _ • N d W
a
9 Zak : Iz I,lu g c
Xi
g mupax
a u
: o
E
m
s T"8 a
uz SSG
3
= a
o f
a
o `S
a o
f'.indi L y
��
1 W
d
p
w $
I' �
��
° a a
O 8
E
I I I
I
_
a o. ..
U U„
' N
T T
YY
i
N (n
Z 2 d
Q
dl T (7 1
wui 1n
J J
J
$y
ZVI
{_MI
T
`{
9qr
e
€
a� n g
2 m e L
O
c
c
n �
1
Ii
- m
..._..i
_.
_ _.._.
_.._..�.._...._..
.....
1.-
_.l_.._..._..l
_ ._.._.

elementOne SAMPLE SUBMISSION FORM
TAT 5 BD RUSH
Hold Time Expiration 06.17.15 @ 0804
Client: Duke Energy
LIMS No J15060347
Project ID HF Lee
Analytical Lab
Lab I6ge 1964
Analysis Due Date 06.15.15
Report Due Date 06.17.15
Date Rec:
06.12.15
Time Rec:
1345
Rec By
JRC
H >9 d:e:j2' No
Temp:5 6°C C�a No
Ref. Method:
SM4500 S2 D
If No, Record
if No, Record
bampie luentitication & Collection Information
Lab ID
Client ID
Collection Date
Collection Time
Analysis Requested
1
IABMW-1 S
06/10/15
1105
S-UTf 5 6
2
IABMW-1
06/10/15
1030
u �If
3
AMW-1 3S
06/10/15
1522
4
AMW-13BC
- - ------- - -
06/10/15
1600
5
IABMW-3S
06/10/15
1025
6
1 A BMW-2 S
06/10/15
1305
7
AMW-12S
06/10/15
1653
ulf
8
AMW-12BC
06/10/15
1541
9
Equipment Blank 06/10/15
0804
u I
NOTE for
Sulfide
The MS/MSD spike should approximate 2 to 3
times the sample concentration. If no sulfide detected
at 100 pg/L spike the sample to render the final
spike concentration at
- 500 pg/L
SS Page 1 of 1 Prep By / Date
SS by. Orf Labeled By / Date
6/12/2015 4'49-3-0 PM ID Verification By /Date vWks z/, - 15,

Analytical Lab
Page 31 of 84
METHOD:
SM 4500 S2- D
ELEMENT ASSAY:
Sulfide
CLIENT:
Duke
Lab ID#
25053/ 054/ 055/ 056/ 057/ 063/ 069/
070
Date:
06/15/15
Time Analysis Begun
10:45
Time Analysis Ended
17:20
Analyst:
KAM
X
y
----_
ug STD
STD
SOLUTION
ABS
0.00
0.000
1.00
0.098
2.50
0.227
5.00
750
0.428
0 614
5
10.00
X
10
10
Y I
250
• Y.00 000 am 8.00 low MO
10.00 0.795 x
ELEMENT ONE
Spectrophotometer UNITS OF ANSWER
Wave Length 664 DETECTION LIMIT u
SPK LEVELLugj
MAX ALIQUOT
Na2S•9H2O Lot # STANDARD conc(ppm)
40721 ICal Std Lot: SD-05•
QC Std Lot: SD-05•
STD ABSORPTION
ALI in mL
ANALYZED
PREP
VOL in mL
Sloe 0.079013187
ALI in mL RESULTS
TAKEN ug/mL
Correlation 0.999089305
LESS THAN SPIKE
% SPK REC LEVEL
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.098
0.8713
10
10
10
<
87.13%
1.0
Std. B. 2.50
0.233
2.6529
10
10
10
0.265
106.12%
2.5
Std. B. 5.00
0.440
5.3847
10
10
10
0.538
107.69%
5.0
Std. B. 7.50
0.635
7.9582
10
10
10
0.796
106.11 %
7.5
Std, B. 10.00
0.829
10.5184
10
10
10
1.052
105.18%
10.0
LRB
0.000
0.0000
10
10
10
<
0.0
LRB SPK
0.423
5.1604
10
10
10
0.516
103%
5.0
QC
0.451
5.5299
10
10
10
0.553
111 %
5.0
25053-1
0.032
0.0003
10
10
10
<
25053-1 s k
0.340
4.0650
10
10
10
0.406
81 %
5.0
25053-2
0.047
0.1982
10
10
10,01;
_m
25053-2 dup
0.015
-0.2241
10
10
10
p;
25053-2 spk
0.392
4.7512
10
10
10
0.475
95%
5.0
25053-3
0.005
-0.3561
10
10
10
0 f'
25053-3 s k
0.424
5.1736
10
10
10
0.517
103%
5.0
25053-4
0.008
-0.3165
10
10
10
25053-4 s k
0.427
5.2131
10
10
10
0.521
104%
5.0
25054-1
0.023
-0.1185
10
10
10
75
25054-1 spk
0.388
4.6985
10
10
10
0.470
94%
5.0
25054-2
0.107
0.9900
10
10
10
<
25054-2 s k
0.481
5.9258
10
10
10
0.593
119%
5.0
25054-3
0.007
-0.3297
10
10
10
0:1 "i
25054-3 s k
0.417
5.0812
10
10
10
0.508
102%
5.0
25054-4
0.065
0.4358
10
10
10
.
25054-4 s k
0.462
5.6750
10
10
10
0.568
114%
5.0
25054-5
0.047
0.1982
10
10
10
<
25054-5 s k
0.483
5.9522
10
10
10
0.595
119%
5.0
Blank
0.000
0.0000
10
10
10
<
QC 0.451 5.5299 10
Submitted f6r QA/QC- Date: 06/15/15
10
By: (Print)
10 1 0.553
KAM
111 % 5.0
(sign):
Page 1 of 5

Analytical Lab
Page 32 of 84
METHOD:
SM 4500 S2- D
ELEMENT ASSAY:
Sulfide
CLIENT:
Duke
Lab ID#
25053/ 054/ 055/ 056/ 057/ 063
070
Date:
06/15/15'
Time Analysis Begun
10:45
Time Analysis Ended
17:20
Analyst:
KAM
X
Y
-- ---
°
ug STD
STD
SOLUTION
ABS
0.00
0.000
1.00
0.098
2.50
0.227
5.00
0.428
7.50
0.614
ELEMENT ONE
Wave Length 664
Na2S•9H2O Lot # STANDARD
40721 C�StdLot:Q
STD ABS OF
0.700
0.600
0.
O a00
------------
----- -- "-----
-- .d38_
0.
0.200
.22
0100
o....
060
z.�
10.00 0.795
8.00 9.00 lo- 12.M
x
X
10
ALI in mL
ANALYZED
10
10
10
10
10
10
Sloe 0.079013187
Correlation 0.999089305
SAMPLE
I.D.
Std. B. 0.00
Std. B. 1.00
Std. B. 2.50
Std. B. 5.00
Std. B. 7.50
Std. B. 10.00
SAMP
ABS
0.000
0.098
0.233
0.440
0.635
0.829
ug PER
ALIQUOT
0.0000
0.8713
2.6529
5.3847
7.9582
10.5184
PREP
VOL in mL
10
10
10
10
10
10
ALI in mL
TAKEN
10
10
10
10
10
10
RESULTS
u /mL
<
<
0.265
0.538
0.796
1.052
LESS THAN
% SPK REC
87.13%
106.12%
107.69%
106.11 %
105.18%
SPIKE
LEVEL
0.0
1.0
2.5
5.0
7.5
10.0
LRB
0.000
0.0000
10
10
10
<
0.0
LRB SPK
0.423
5.1604
10
10
10
0.516
103%
5.0
QC
0.451
5.5299
10
10
10
0.553
111 %
5.0
25054-6
0.090
0.7657
10
10
10
25054-6 s k
0.428
5.2263
10
10
10
0.523
105%
5.0
25054-7
0.005
1 -0.3561
10
10
10
25054-7 dup
0.005
-0.3561
10
10
10
< 0.1
25054-7 spk
0.442
5.4111
10
10
10
0.541
108%
5.0
25054-8
0.184
2.0062
10
10
10
0 241
25054-8 s k
0.576
7.1795
10
10
10
0.718
103%
5.0
25054-9
0.004
-0.3693
10
10
10
c0¢
25054-9 s k
0.425
5.1868
10
10
10
0.519
104%
5.0
25055-1
0.019
-0.1713
10
10
10
11
25055-1 s k
0.395
4.7908
10
10
10
0.479
96%
5.0
25055-2
0.011
-0.2769
10
10
10
25055-2 s k
0.392
4.7512
10
10
10
0.475
95%
5.0
25055-3
0.013
-0.2505
10
10
10
25055-3 s k
0.385
4.6589
10
10
10
0.466
93%
5.0
25055-4
0.010
-0.2901
10
10
10
25055-4 spk
0.394
4.7776
10
10
10
0.478
96%
5.0
25056-1
0.008
-0.3165
10
10
10
d:1�
25056-1 s k
0.370
4.4609
10
10
10
0.446
89%
5.0
Blank
0.000
0.0000
10
10
10
<
QC 0.450 5.5167 10
Submlfted fOr QA/QC- Date: 06/15/15
10
By: (Print)
10 0.552
KAM
1100/05.0
(sign):
Page 2 of 5 ��

Analytical Lab
Page 33 of 84
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
ug/mL
DETECTION LIMIT u
1.000'
CLIENT:
Duke
SPK LEVEL u
5
Lab ID#
25053/ 054/ 055/ 056/ 057/ 063/ 069/
070 MAX ALIQUOT
06/15/15 Na2S•9H2O Lot # STANDARD conc(ppm)
10:45 40721 Cal Std Lot: SD-05-3
17:20 QC Std Lot: SD-054
KAM _ - STD ABSORPTION
Y o.�o
10.00
Date:
X
Time Analysis Begun
10
Time Analysis Ended
10
Analyst:
Y
X
ug STD
SOLUTION
STD mo
ABS om0.00
0.fi00
1.00
2.50
5.00
7.50
10.00
0.098
° °°°
---- ---
---------------------
o'°°
0.227
ozro
:
0.428
o,ao
-- --
--- - - -
--
ooao
--
- -
-
0.614
0.795
C,0 zoo °.ao a.ao 8.00 m.ao ,zao
■
I
j..," a,
,.
Sloe 0.079013187
Correlation 0.999089305
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.098
0.8713
10
10
10
<
87.13%
1.0
Std. B. 2.50
0.233
2.6529
10
10
10
0.265
106.12%
2.5
Std. B. 5.00
0.440
5.3847
10
10
10
0.538
107.69%
5.0
Std. B. 7.50
0.635
7.9582
10
10
10
0.796
106.11 %
7.5
Std. B. 10.00
0.829
10.5184
10
10
10
1.052
105.18%
10.0
LRB
0.000
0.0000
10
10
10
<
0.0
LRB SPK
0.423
5.1604
10
10
10
0.516
103%
5.0
QC
0.451
5.5299
10
10
10
0.553
111 %
5.0
25056-2
0.011
-0.2769
10
10
10
25056-2 s k
0.360
4.3289
10
10
10
0.433
87%
5.0
25056-3
0.005
-0.3561
10
10
10�'i
25056-3 spk
0.421
5.1340
10
10
10
0.513
103%
5.0
25057
0.007
-0.3297
10
10
10
<0,,
25057 dup
0.007
-0.3297
10
10
10
< 0.1
25057 s k
0.426
5.1999
10
10
10
0.520
104%
5.0
25063
0.015
-0.2241
10
10
10
<
25063 s k
0.112
1.0560
10
10
10
0.106
21 %
5.0
24186 - 19.2 QC
0.273
3.1808
10
10
1
3.181
TV= 4.23
25053-1
0.015
-0.2241
10
10
5
25053-1 s k
0.386
4.6721
10
10
5
0.934
93%
5.0
25054-2
0.057
0.3302
10
10
5
25054-2 s k
0.462
5.6750
10 1
10
5
1.135
114%
5.0
25054-5
0.024
-0.1053
10
10
5
<:0:
25054-5 s k
0.441
5.3979
10
10
5
1.080
108%
5.0
25063
0.020
-0.1581
10
10
5
<
25063 s k
0.163
1.7291
10
10
5
0.346
35%
5.0
25063
0.021
-0.1449
10
10
2
<
25063 spk
0.223
2.5209
10
10
2
1.260
50%
5.0
Blank
0.000
0.0000
10
10
10 1
<
QC 0.450 5.5167 10
Submitted fOY QA/QC- Date: 06/15/15
10
By: (Print)
10 1 0.552 1
KAM
110% 5.0
(sign): '
Page 3 of 5

Analytical Lab
Page 34 of 84
METHOD:
SM 4500 S2- D
ELEMENT ASSAY:
Sulfide
CLIENT:
Duke
Lab ID#
25053/ 054/ 055/ 056/ 057/ 063/
070
Date:
06/15/15
Time Analysis Begun
10:45
Time Analysis Ended
17:20
X
Y
ug STD
STD
SOLUTION
ABS
0.00
0.000
1.00
0.098
2.50
0.227
5.00
0.428
7.50
0.614
10.00
0.795
ELEMENT ONE
pectrophotometer UNITS OF ANSWER
Wave Length 664 DETECTION LIMIT u
SPK LEVEL u
MAX ALIQUOT
Na2S•9H2O Lot # STANDARD conc(ppm)
40721 Cal Std Lot: SD-05-3
QC Std Lot: SD-05-4
STD ABSORPTION
Imp M
BOD B.pO 10.00 12M
5
10.00
X
A 5'�
ug PER ALI in mL
ALIQUOT ANALYZED
a _.
PREP
VOL in mL
Sloe 0.079013187
Correlation 0.999089306
SAMPLE
I.D.
SAMP
ABS
ALI in mL
TAKEN
RESULTS
u /mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.098
0.8713
10
10
10
<
87.13%
1.0
Sid. B. 2.50
0.233
2.6529
10
10
10
0.265
106.12%
2.5
Std. B. 5.00
0.440
5.3847
10
10
10
0.538
107.69%
5.0
Std. B. 7.50
0.635
7.9582
10
10
10
0.796
106.11 %
7.5
Std. B. 10.00
0.829
10.5184
10
10
10
1.052
105.18%
10.0
LRB
0.000
0.0000
10
10
10
<
0.0
LRB SPK
0.423
5.1604
10
10
10
0.516
103%
5.0
QC
0.451
5.5299
10
10
10
0.553
111 %
5.0
25063
0.013
-0.2505
10
10
1
<
25063 s k
0.313
3.7087
10
10
1
3.709
74%
5.0
25063
0.007
-0.3297
10
10
0.5
<
25063 s k
0.345
4.1310
10
10
0.5
8.262
83%
5.0
25063
0.003
-0.3825
10
10
0.25
4;tJ
25063 s k
0.385
4.6589
10
10
0.25
18.635
93%
5.0
24186-19.2 QC
0.307
3.6295
10
10
1
3.629
86%
TV=4.23
25069-1
0.006
-0.3429
10
10
10
t}
25069-1 s k
0.418
5.0944
10
10
10
0.509
102%
5.0
25069-2
0.011
-0.2769
10
10
10�,�
25069-2 dup
0.011
-0.2769
10
10
10
< 0.1
25069-2 s k
0.372
4.4873
10
10
10
0.449
90%
5.0
25069-3
0.003
-0.3825
10
10
10
25069-3 s ki
0.434
5.3055
10
10
10
0.531
106%
5.0
25070-5
0.0041
-0.3693
10
10
10
<
25070-5 s k
0.344 1
4.1178
10
10
10
0.412
82%
5.0
25070-6
0.003
-0.3825
10
10
10
25070-6 s k
0.428
5.2263
10
10
10
0.523
105%
5.0
25070-7
0.002
-0.3957
10
10
10'0;v
25070-7 s k
0.434
5.3055
10
10
10
0.531
106%
5.0
Blank
0.000 1
0.0000
10
10
10
<
QC
0.450
5.5167
10
10
10
0.552
1100/
5.0
Submitted for QA/QC- Date: 06/15/15 -7f
By: (Print)
KAM
(sign):
Page 4 of 5 /Z

Analytical Lab
Page 35 of 84
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
.Duke
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
CLIENT:
DETECTION LIMIT u
SPK LEVEL u
1.0005
Lab ID#
25053/ 054/ 055/ 056/ 057/ 063/ 069/
070
06/15/15 Na2S•9H2O Lot #
1045 40721
17:20
KAM
-------- ------ _ _
MAX ALIQUOT
STANDARD conc(ppm)
10.00
x
Date:
Time Analysis Begun
Time Analysis Ended
Cal Std Lot: SD-05-3
10
QC Std Lot: SD-05-4
10
Analyst:
STD ABSORPTION
_ -- ----
Y
Xy
ug STD
STD
SOLUTION
ABS
0.00
0.000
1.00
0.098
2.50
0.227
5.00
0.428
7.50
0.614
10.00
0.795
B'0° low +zro
x i
Sloe 0.079013187 Correlation 0.999089306
ug PER ALI in mL PREP ALI in mL RESULTS LESS THAN SPIKE
ALIQUOT ANALYZED VOL in mL TAKEN u /mL % SPK REC LEVEL
0.0000 10 10 10 <
-77
SAMPLE
1.D.
Std. B. 0.00
SAMP
ABS
0.000
B. 1.00
Std��ffttd.
B. 2.50
B. 5.00
Std. B. 7.50
Std. B. 10.00
0.098
0.233
0.440
0.635
0.829
0.8713
2.6529
5.3847
7.9582
10.5184
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
<
0.265
0.538
0.796
1.052
87.13%
106.12%
107.69%
106.11 %
105.18%
0.0
1.0
2.5
5.0
7.5
10.0
LRB
0.000
0.0000
10
10
10
<
0.0
LRB SPK
0.423
5.1604
10
10
10
0.516
103%
5.0
5.0
QC
0.451
5.5299
10
10
10
0.553
111 %
25070-8
0.004
-0.3693
10
10
10�"
<'r?
5.0
25070-8 s k
25070-9
0.426
0.011
5.1999
-0.2769
10
10
10
10
10
10.p,
0.520
104%
25070-9 s k
0.404
4.9096
10
10
10
0.491
98%
5.0
25070-5
0.015
-0.2241
10
10
10
<y2
25070-5 spk
24186-19.2 QC
0.365
0.308
4.3949
3.6427
10
10
10 ]:::::5!_
10
0.879
3.643
88%
5.0
86%
TV= 4.23
flank 0.000 0.0000 1 10 10 10 <
QC 0.450 5.5167 10 10 10 El 0.552 110%
3d fOr "QC- Date: 06/15/15 By: (Print) KAM
(sign):
Page 5 of 5 77

® Laboratories LLc
nalytical Lab
36of84
a member of The GEL Group IN'.
Po Box 30712 Charleston, SC 29417
2040 Savage Road Charlestan. SC 25407
F 843.556.8171
F 843.766.1178
gel.com
June 23, 2015
Mary Ann Ogle
Duke Energy Analytical Laboratory
13339 Hagers Ferry Road
Mail Code: MGO3A2
Huntersville, North Carolina 28078
Re: AB GW Assessment Water
Work Order: 374990
SDG: J15060347
Dear Mary:
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the
sample(s) we received on June 12, 2015. This original data report has been prepared and reviewed in accordance
with GEL's standard operating procedures.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs
on time every time. We trust that you will find everything in order and to your satisfaction. If you have any
questions, please do not hesitate to call me at [phone], ext. 4443.
Sincerely,
'Le
En�Trrent for
Lindsay Fabra
Project Manager
Purchase Order: 1142110
Enclosures
Pa 11111111111111111111111111111111111111111111111111111111111111

Analytical Lab
Page 37 of 84
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis Report
for
DUP0002 Duke Energy
Client SDG: J15060347 GEL Work Order: 374990
The Qualifiers in this report are defined as follows:
* A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a Tracer compound
** Analyte is a surrogate compound
J Value is estimated
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the Certificate of Analysis.
The designation ND, if present, appears in the result column when the analyte concentration is not detected above
the limit as defined in the 'U' qualifier above.
This data report has been prepared and reviewed in accordance with GEL Laboratories LLC
standard operating procedures. Please direct any questions to your Project Manager, Lindsay Fabra.
Reviewed by
Page 2 of 13

Analytical Lab
GEL LABORATORIES LLC Page 38 of 84
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis
Company:
Duke Energy Analytical Laboratory
Address :
13339 Hagers Ferry Road
Mail Code: MG03A2
Huntersville, North Carolina 28078
Contact:
Mary Ann Ogle
Project:
AB GW Assessment Water
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
2015018388
374990001
Ground Water
10-JUN-15 11:05
12-JUN-15
Client
Report Date: June 23, 2015
Project: DUKE00225
Client ID: DUP0002
Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method
Metals Analysis-ICP-MS
SW846 3010A/6020A Liquid "As Received"
Uranium-238 0.000465
0.000067
0.0002
ug/mL
1
SKJ 06/17/15
1535 1485528 1
Uranium-233 U 0.00
0.00001
0.00005
ug/mL
1
SKJ 06/18/15
0931 1485528 2
Uranium-234 U 0.00
0.00001
0.00005
ug/mL
1
Uranium-236 U 1.00E-06
0.00001
0.00005
ug/mL
1
Rad Gas Flow Proportional Counting
GFPC, Ra228, Liquid "As Received"
Radium-228 U 1.13
1.33
3.00
pCi/L
AXM6 06/19/15
1134 1485645 3
Rad Radium-226
Lucas Cell, Ra226, liquid "As Received"
Radium-226 0.979
0.524
1.00
pCi/L
CXP3 06/19/15
0800 1485267 4
The following Prep Methods were performed:
Method Description
Analyst
Date
Time Prep Batch
SW846 3010A SW 846 3010 Acid Digestion
JP1
06/12/15
1810
1485527
The following Analytical Methods were performed:
Method Description Analyst Comments
1 SW846 3010A/6020A
2 SW846 3010A/6020A
3 EPA 904,0/SW846 9320 Modified
4 EPA 903.1 Modified
Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits
Barium-133 Tracer GFPC, Ra228, Liquid "As Received" 96.3 (15%-125%)
Notes:
Page 3 of 13

Analytical Lab
GEL LABORATORIES LLC Page 39 of 84
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis
Company:
Duke Energy Analytical Laboratory
Address :
13339 Hagers Ferry Road
Mail Code: MG03A2
Huntersville, North Carolina 28078
Contact:
Mary Ann Ogle
Project:
AB GW Assessment Water
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
2015018389
374990002
Ground Water
10-JUN-15 10:30
12-JUN-15
Client
Report Date: June 23, 2015
Project: DUKE00225
Client ID: DUP0002
Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method
Metals Analysis-ICP-MS
SW846 3010A/6020A Liquid "As Received"
Uranium-238 0.0135
0.000067
0.0002
ug/mL
1
SKJ 06/17/15
1543 1485528 1
Uranium-233 U 0.00
0.00001
0.00005
ug/mL
1
SKJ 06/18/15
0936 1485528 2
Uranium-234 U 1.00E-06
0.00001
0.00005
ug/mL
1
Uranium-236 U 0.00
0.00001
0.00005
ug/mL
1
Rad Gas Flow Proportional Counting
GFPC, Ra228, Liquid "As Received"
Radium-228 U 1.50
1.67
3.00
pCi/L
AXM6 06/19/15
1305 1485645 3
Rad Radium-226
Lucas Cell, Ra226, liquid "As Received"
Radium-226 1.12
0.789
1.00
pCi/L
CXP3 06/19/15
0800 1485267 4
The following Prep Methods were performed:
Method Description
Analyst
Date
Time Prep Batch
SW846 3010A SW 846 3010 Acid Digestion
JP1
06/12/15
1810
1485527
The following Analytical Methods were performed:
Method Description Analyst Comments
1 SW846 3010A/6020A
2 SW846 3010A/6020A
3 EPA 904,0/SW846 9320 Modified
4 EPA 903.1 Modified
Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits
Barium-133 Tracer GFPC, Ra228, Liquid "As Received" 90.6 (15%-125%)
Notes:
Page 4 of 13

Analytical Lab
GEL LABORATORIES LLC Page 40 of 84
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis
Company:
Duke Energy Analytical Laboratory
Address :
13339 Hagers Ferry Road
Mail Code: MG03A2
Huntersville, North Carolina 28078
Contact:
Mary Ann Ogle
Project:
AB GW Assessment Water
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
2015018394
374990003
Ground Water
10-JUN-15 16:53
12-JUN-15
Client
Report Date: June 23, 2015
Project: DUKE00225
Client ID: DUP0002
Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method
Metals Analysis-ICP-MS
SW846 3010A/6020A Liquid "As Received"
Uranium-238 0.00224
0.000067
0.0002
ug/mL
1
SKJ 06/17/15
1544 1485528 1
Uranium-233 U 0.00
0.00001
0.00005
ug/mL
1
SKJ 06/18/15
0938 1485528 2
Uranium-234 U 0.00
0.00001
0.00005
ug/mL
1
Uranium-236 U 0.00
0.00001
0.00005
ug/mL
1
Rad Gas Flow Proportional Counting
GFPC, Ra228, Liquid "As Received"
Radium-228 11.4
2.34
3.00
pCi/L
AXM6 06/23/15
1243 1485645 3
Rad Radium-226
Lucas Cell, Ra226, liquid "As Received"
Radium-226 12.0
0.719
1.00
pCi/L
CXP3 06/19/15
0800 1485267 4
The following Prep Methods were performed:
Method Description
Analyst
Date
Time Prep Batch
SW846 3010A SW 846 3010 Acid Digestion
JP1
06/12/15
1810
1485527
The following Analytical Methods were performed:
Method Description Analyst Comments
1 SW846 3010A/6020A
2 SW846 3010A/6020A
3 EPA 904,0/SW846 9320 Modified
4 EPA 903.1 Modified
Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits
Barium-133 Tracer GFPC, Ra228, Liquid "As Received" 77.5 (15%-125%)
Notes:
Page 5 of 13

Analytical Lab
GEL LABORATORIES LLC Page41 of84
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis
Company:
Duke Energy Analytical Laboratory
Address :
13339 Hagers Ferry Road
Mail Code: MG03A2
Huntersville, North Carolina 28078
Contact:
Mary Ann Ogle
Project:
AB GW Assessment Water
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
2015018395
374990004
Ground Water
10-JUN-15 15:41
12-JUN-15
Client
Report Date: June 23, 2015
Project: DUKE00225
Client ID: DUP0002
Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method
Metals Analysis-ICP-MS
SW846 3010A/6020A Liquid "As Received"
Uranium-238 U 0.0000201
0.000067
0.0002
ug/mL
1
SKJ 06/17/15
1546 1485528 1
Uranium-233 U 0.00
0.00001
0.00005
ug/mL
1
SKJ 06/18/15
0939 1485528 2
Uranium-234 U 0.00
0.00001
0.00005
ug/mL
1
Uranium-236 U 0.00
0.00001
0.00005
ug/mL
1
Rad Gas Flow Proportional Counting
GFPC, Ra228, Liquid "As Received"
Radium-228 U 1.04
1.38
3.00
pCi/L
AXM6 06/19/15
1134 1485645 3
Rad Radium-226
Lucas Cell, Ra226, liquid "As Received"
Radium-226 U 0.537
0.551
1.00
pCi/L
CXP3 06/19/15
0800 1485267 4
The following Prep Methods were performed:
Method Description
Analyst
Date
Time Prep Batch
SW846 3010A SW 846 3010 Acid Digestion
JP1
06/12/15
1810
1485527
The following Analytical Methods were performed:
Method Description Analyst Comments
1 SW846 3010A/6020A
2 SW846 3010A/6020A
3 EPA 904,0/SW846 9320 Modified
4 EPA 903.1 Modified
Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits
Barium-133 Tracer GFPC, Ra228, Liquid "As Received" 91.3 (15%-125%)
Notes:
Page 6of13

Analytical Lab
Page 42 of 84
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
QC Summary
Duke Energy Analytical Laboratory
13339 Hagers Ferry Road
Mail Code: MG03A2
Huntersville, North Carolina
Contact: Mary Ann Ogle
Workorder: 374990
Report Date: June 23, 2015
Page 1 of 3
Parmname
NOM
Sample
Qual
QC
Units
RPD%o
REC%
Range Anlst
Date Time
Metals Analysis - ICPMS
Batch 1485528
QC1203336713
374990001
DUP
Uranium-233
U
ND
U
ND
ug/mL
N/A
SKJ
06/18/15 09:32
Uranium-234
U
ND
U
ND
ug/mL
N/A
Uranium-236
U
ND
U
ND
ug/mL
N/A
Uranium-238
0.000465
0.000486
ug/mL
4.31 ^
(+/-0.0002)
06/17/1515:37
QC1203336712
LCS
Uranium-238
0.0496
0.0518
ug/mL
104
(80%-120%)
06/17/1515:31
QC1203336718
LCS
Uranium-233
0.0005
0.000524
ug/mL
105
(80%-120%)
06/18/15 09:29
Uranium-234
0.00055
0.000556
ug/mL
101
(80%-120%)
Uranium-236
0.005
0.0057
ug/mL
114
(80%-120%)
QC1203336711
MB
Uranium-233
U
ND
ug/mL
06/18/15 09:28
Uranium-234
U
ND
ug/mL
Uranium-236
U
ND
ug/mL
Uranium-238
U
ND
ug/mL
06/17/1515:30
QC1203336714
374990001
MS
Uranium-238
0.0496
0.000465
0.0545
ug/mL
109
(75%-125%)
06/17/1515:38
QC1203336717
374990001
MS
Uranium-233
0.0005
U
ND
0.000533
ug/mL
107
(75%-125%)
06/18/15 09:34
Uranium-234
0.00055
U
ND
0.000558
ug/mL
101
(75%-125%)
Uranium-236
0.005
U
ND
0.0058
ug/mL
116
(75%-125%)
QC1203336715
374990001
SDILT
Uranium-233
U
ND
U
ND
ug/L
N/A
06/18/15 09:35
Page 7of13

Analytical Lab
Page 43 of 84
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
QC Summary
Workorder: 374990
Page 2 of 3
Parmname
NOM Sample
Qual
QC
Units
RPD% REC%
Range Anlst Date Time
Metals Analysis - ICPMS
Batch 1485528
Uranium-234
U ND
U
ND
ug/L
N/A
Uranium-236
U ND
U
ND
ug/L
N/A
(0%-10%) SKJ 06/18/15 09:35
Uranium-238
0.465
J
0.103
ug/L
10.4
(0%-10%) 06/17/1515:39
Rad Gas Flow
Batch 1485645
QC1203337062 374990003 DUP
Radium-228 11.4 9.97 pCi/L 13.7 (0% - 100%) AXM6 06/23/15 12:43
QC1203337063 LCS
Radium-228 30.8 26.8 pCi/L 87.1 (75%-125%) 06/19/1511:35
QC1203337061 MB
Radium-228 U 0.918 pCi/L 06/19/1511:35
Rad Ra-226
Batch 1485267
QC1203336043 374876001 DUP
Radium-226 0.814
0.765 pCi/L 6.23
(0% - 100%) CXP3 06/19/15 08:35
QC1203336045 LCS
Radium-226 24.7
26.1 pCi/L
106 (75%-125%) 06/19/15 08:35
QC1203336042 MB
Radium-226 U
0.193 pCi/L
06/19/15 08:00
QC1203336044 374876001 MS
Radium-226 124 0.814
125 pCi/L
101 (75%-125%) 06/19/15 08:35
Notes:
The Qualifiers in this report are defined as follows:
** Analyte is a Tracer compound
< Result is less than value reported
> Result is greater than value reported
BD Results are either below the MDC or tracer recovery is low
E %difference of sample and SD is >10%. Sample concentration must meet flagging criteria
FA Failed analysis.
FB Mercury was found present at quantifiable concentrations in field blanks received with these samples.
Data associated with the blank are deemed
invalid for reporting to regulatory agencies
H Analytical holding time was exceeded
Page 8 of 13

Analytical Lab
Page 44 of 84
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
QC Summary
Workorder: 374990
Parmname NOM Sample Qual QC Units RPD%o REC'%
Page 3 of 3
Range Anlst Date Time
J Value is estimated
K Analyte present. Reported value may be biased high. Actual value is expected to be lower.
L Analyte present. Reported value may be biased low. Actual value is expected to be higher.
M M if above MDC and less than LLD
M REMP Result > MDC/CL and < RDL
N Metals --The Matrix spike sample recovery is not within specified control limits
N/A RPD or %Recovery limits do not apply.
N1 See case narrative
ND Analyte concentration is not detected above the detection limit
NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
R Sample results are rejected
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma Spectroscopy --Uncertain identification
UJ Gamma Spectroscopy --Uncertain identification
UL Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.
X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Y Other specific qualifiers were required to properly define the results. Consult case narrative.
^ RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
h Preparation or preservation holding time was exceeded
N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable.
^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than
five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the
RL is used to evaluate the DUP result.
* Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the QC Summary.
Page 9 of 13

Analytical Lab
Page 45 of 84
LU
m
�7
Cu
Nzz Pug fizz)
Lunlpeu lUIOI
IUOU1813 A)
9pUlnS
A
IvUOCp a
"0
OVAIN
-81VAIN'301
6jve4S-A (SU
'Asm)
11'ss
cc)
r-111
C
0
Yl
Y)
-21 C
76
kn Ld �j
D
0
C 0
...... .....
...... .....
Page 10 of 13

STRAIGHT BILL OF LADING — SHORT FORM 'A
Date Bill of LadingAndytical Lab
NOTICE: Shippers of hazardous: materials must enter 24-hour Emergency Page 46 of 84
response telephone number under "Emergency Response Phone Number. Shipper No.
Memorandum V\ i, 1'­� ��'i -Carrier No.
70—. FROM: il'/' , 1, f
I " 'r -� , Shipper i
Consignee
treet
Street
Orio­ t�l V Zip Code
Destination V i Zip Code Emergency Response
Route: Vehicle No. SCAC �Phone Number
No.
Shipping
Units
+HM
Kind of Packaging, Description of Articles Cqn-inerefities requiring special or additional care or attention in handling or
slowing must be so marked and packaged as to ensure safe transportation with
Special Marks and Exceptions ordinary care. See section 2(e) of National Motor Freight Classification. Item 360.
[Srubpeigfit ql; to
ri)�
Rate or Class
CHARGES
it
ports
*If the shipment moves between two ports by a
carrier by water, the law requireolthat, the bfil�lof :10inp
, g
state whether weight,is "carrier's or shipper's weighe �
REMIT
C.O.D.O:
ADDRESS
0
�7
C.O.D.
mt.
Amt. $
C.O.D. FEE: TOTAL
4 I 0
PREPAID 0
COLL CTO $ CHARGES: $
COLLECTO $
Note -Where the rate is dependent on value, shippers are required to
state specifically in writing the agreed or declared value of the property.
The agreed or declared value of the property is hereby specifically stated
by the shipper to be not exceeding
$ per
Subject to Section 7 of the conditions, if this shipment is to be delivered to the consignee vvit without
recourse on the consignor, the consignor shall sign the following statement. l
a
The carrier shall not make delivery of this shipment without payment of frPight and 11 other
charges.
FREIGHT CHARGES
Check Appropriate Box
171 Freight prepaid
I El Collect
except as noted (conten
(signature of Consignor)
-r , ­_ r> . ­­, flP ,ihei ah—a in aorsirent road order,
RECEIVED, subject to the classifications and bimuity rhea Lanus In LITUGL — 1— word carrier being understood throughout this contract as meaning any perst
and condition of contents of packages unknown), marked, consigned, and destined as indicated above which said carrier (the w, if on its route, otherwise to deliver to another carrier on the route to sE
or corporation in possession of the property under the contract] agrees to carry to its usual place of delivery at said destination, is to each party at any time interested in all or any of said prc
destination. It is mutually agreed as to each carrier of all or any of, said property over all or any portion of said route to destination and E
arty, that every service to be performed hereunder shall be subject to all the terms and conditions of the Uniform Domestic Straight Bill of Lading setforth(1) in Uniform Fraipt Classifications in affect i
the date hereof, if this is a rail or a rail -water shipment or (2) in the applicable motor carrier classification or tariff, if this is a motor carrier shipment. Shipper hereby cardias that he is familiar with
�hm�n� and conditions of the said bill of lading, set forth in the classification or tariff which governs the transportation of this shipment, and the said terms and conditions are hereby agreed to by t
A ­--i f­ hi —If and his assigns.
Mark with `RQ` if appropriate to designate Hazardous Materials as defined in the U.S. Department of
Transportation Regulations governing the transportation of hazardous materials. The use of this column is
an optional method for identifying hazardous materials on Bills of Lading per 172.201(a](1) (iij) of Title 49
Code of Federal Regulations. Also when shipping hazardous materials, the shipper's certification statement
prescribed in section 172.204(a) of the Federal Regulations. as indicated an the Bill of Lading does apply.
.­­ . ­­ir, --ti— from the reauirinnent is provided in the Regulation for a particular material.
01 I
The format and content of hazardous item list is the responsibility of individual cam- Note: Liability limitation for lo!
parry interpretation of requirements as described in 49 Code of Federal Regulations or damage in this shipme
172. Subpart 0-Shipping Papers,
Such description consists of the following per Sec- may be applicable. See
tions 172.201 (Hazardous Material Table) and Sections 172,202 and 172.2a3.
Proper shipping,name, hazardous class. UN identification number, packing group. United States Code, Sectioi
and subsidiary class(es). I 4706(c (1 )(A) and (B).
This is to certify that the above named materials are properly classified, packaged, Carrier acknowledges receipt of packages and any required placards. Caryier certifies emergency response intern
marked, and labeled, and are in proper condition for transportation according to the Lion was made available and/or carrier has the U.S. Department of Transportation emergency response guidebc
or equivalent documentation in the vehicle. Property described above is received in good order, except as noted.
applicable regulations of the U.S. Department of Transportation.
Page 11 of 13

Analytical Lab
Page 47 of 84
j LaboratorieS L LC
SAMPLE RECEIPT & REVIEW FORM
Client: 'I z,
SDG/AWCOC[WorkOrder: C190
Received By:
Date Received: & / `
Suspected Hazard Information
o *If Net Counts > I00cpm on samples not marked "radioactive", contact the Radiation Safety Group for further
>1
investigation.
COC/Samples marked as radioactive?
Le Maximum Net Counts Observed* (Observed Counts - Area Background Counts):
Classified Radioactive 11 or fit by RSO?
14f yes, Were swipes taken of sample containers < action levels?
COC/Samples marked containing PCBs?
Package, COC, and/or Samples marked as
beryllium or asbestos containing?
Ifyes, samples are to be segregated as Safety Controlled Samples, and opened by the GEL Safety Group.
Shipped as a DOT Hazardous?
w Hazard Class Shipped: UN#:
Samples identified as Foreign Soil?
Sample Receipt Criteria
Comments/Qualifiers (Required for Non -Conforming Items)
Shipping containers received intact
Circle Applicable:
I
and sealed?
Seals broken Damaged container Leaking container Other (describe)
2
Samples requiring cold preservation
Preservation Method* Icebags Blue ice Dry ice one Other(describe)
within (0 < 6 deg. C)?*
1 t® all temperatures are recorded in Celsius
2a
Daily check performed and passed on
Temperature Device Serial IT:
Secondary Temperature Device Serial It(If Applicable): C{J (j 3
IR temperature gun?
3
Chain of custody documents included
with shipment?
Circle Applicable:
4
Sample containers intact and sealed?
Seals broken Damaged container Leaking container Other (describe)
Samples requiring chemical
Sample ID's, containers affected and observed pH:
5
preservation at proper pH?
If Preservation added .o #:
Do Low Level Perchlorate samples
Sample to's and containers affected:
6
(EPA 6850) have headspace as
required?
VOA vials free of headspace (defined
i
Sample ID's and containers affected:
7
as < 6mm bubble)?
`*''�
(If yes, immediately deliver to Volatiles laboratory)
8
Are Encore containers present?
Samples received within holding
ID's and tests affected:
9
time?
14
Sample ID's on COC match ID's on
Sample ID's and containers affected:
bottles?
Date & time on COC thatch date &
Sample ID's affected:
11
time on bottles?
Number of containers received match
Sample ID's affected:
12
number indicated on COC?
13
Are sample containers identifiable as
GEL provided?
14
COC form is properly signed in
relinquished/received sections?
Circle Applicable: _
FedEx Air FedF_x Ground UPS Field Services Courier Other
15
Carrier and tracking number.
Comments (Use Continuation Form if needed):
PM (or PMA) review: Initials Date I� Page S of -f— GL-CHL-SR-001 Rev 1
Page 12 of 13

Analytical Lab
Page 48 of 84
List of current GEL Certifications as of 23 June 2015
State
Certification
Alaska
UST-110
Arkansas
88-0651
CLIA
42D0904046
California
2940 Interim
Colorado
SC00012
Connecticut
PH-0169
Delaware
SC000122013-10
DoD ELAP/ ISO17025 A2LA
2567.01
Florida NELAP
E87156
Foreign Soils Permit
P330-12-00283, P330-12-00284
Georgia
SC00012
Georgia SDWA
967
Hawaii
SC000122013-10
Idaho Chemistry
SC00012
Idaho Radiochemistry
SC00012
Illinois NELAP
200029
Indiana
C—SC-01
Kansas NELAP
E-10332
Kentucky SDWA
90129
Kentucky Wastewater
90129
Louisiana NELAP
03046 (A133904)
Louisiana SDWA
LA150001
Maryland
270
Massachusetts
M—SC012
Michigan
9976
Mississippi
SC000122013-10
Nebraska
NE—OS-26-13
Nevada
SC000122014-1
New Hampshire NELAP
2054
New Jersey NELAP
SC002
New Mexico
SC00012
New York NELAP
11501
North Carolina
233
North Carolina SDWA
45709
Oklahoma
9904
Pennsylvania NELAP
68-00485
Plant Material Permit
PDEP-12-00260
S.Carolina Radchem
10120002
South Carolina Chemistry
10120001
Tennessee
TN 02934
Texas NELAP
T104704235-15-10
Utah NELAP
SC000122015-17
Vermont
VT87156
Virginia NELAP
460202
Washington
C780
West Virginia
997404
Page 13 of 13

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
Project Name: AB GW Assessment Water - HF Lee
Project Number:J15060347
Lot Number:QF12010
Date Completed:06/17/2015
Grant Wilton
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
* QF1 201 0*
Shealy Environmental Services, Inc. Page: 1 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Duke Energy
Lot Number: QF12010
Project Name: AB GW Assessment Water - HF Lee
Project Number: J15060347
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QF12010
Project Name: AB GW Assessment Water - HF Lee
Project Number: J15060347
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
2015018388
Aqueous
06/10/20151105
06/12/2015
002
2015018389
Aqueous
06/10/20151030
06/12/2015
003
2015018390
Aqueous
06/10/20151522
06/12/2015
004
2015018391
Aqueous
06/10/20151600
06/12/2015
005
2015018392
Aqueous
06/10/20151025
06/12/2015
006
2015018393
Aqueous
06/10/20151305
06/12/2015
007
2015018394
Aqueous
06/10/20151653
06/12/2015
008
2015018395
Aqueous
06/10/20151541
06/12/2015
009
2015018397
Aqueous
06/10/2015 0804
06/12/2015
(9 samples)
Shealy Environmental Services, Inc. Page: 3 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QF12010
Project Name: AB GW Assessment Water - HF Lee
Project Number: J15060347
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
2015018388
Aqueous
Alkalinity
SM 2320B-
300
mg/L
5
001
2015018388
Aqueous
Bicarbonate Alkalinity
SM 2320B-
300
mg/L
5
001
2015018388
Aqueous
Methane
RSK - 175
63
ug/L
6
002
2015018389
Aqueous
Alkalinity
SM 2320B-
580
mg/L
7
002
2015018389
Aqueous
Bicarbonate Alkalinity
SM 2320B-
580
mg/L
7
003
2015018390
Aqueous
Alkalinity
SM 2320B-
26
mg/L
9
003
2015018390
Aqueous
Bicarbonate Alkalinity
SM 2320B-
26
mg/L
9
004
2015018391
Aqueous
Alkalinity
SM 2320B-
100
mg/L
11
004
2015018391
Aqueous
Bicarbonate Alkalinity
SM 2320B-
100
mg/L
11
004
2015018391
Aqueous
Methane
RSK - 175
30
ug/L
12
005
2015018392
Aqueous
Alkalinity
SM 2320B-
120
mg/L
13
005
2015018392
Aqueous
Bicarbonate Alkalinity
SM 2320B-
120
mg/L
13
005
2015018392
Aqueous
Methane
RSK - 175
420
ug/L
14
006
2015018393
Aqueous
Alkalinity
SM 2320B-
350
mg/L
15
006
2015018393
Aqueous
Bicarbonate Alkalinity
SM 2320B-
350
mg/L
15
006
2015018393
Aqueous
Methane
RSK - 175
16
ug/L
16
007
2015018394
Aqueous
Methane
RSK - 175
10
ug/L
18
008
2015018395
Aqueous
Alkalinity
SM 2320B-
38
mg/L
19
008
2015018395
Aqueous
Bicarbonate Alkalinity
SM 2320B-
38
mg/L
19
008
2015018395
Aqueous
Methane
RSK - 175
14
ug/L
20
(20 detections)
Shealy Environmental Services, Inc. Page: 4 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF12010-001
Description: 2015018388 Matrix: Aqueous
Date Sampled:06/10/2015 1105 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060347
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/16/2015 1915
HMA 77407
1
(Bicarbonate ) SM 2320B-2011
1 06/16/2015 1915
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/16/2015 1915
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
300
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
300
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF12010-001
Description: 2015018388 Matrix: Aqueous
Date Sampled:06/10/2015 1105 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060347
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/16/2015 1545 DCS 77379
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 63 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF12010-002
Description: 2015018389 Matrix: Aqueous
Date Sampled:06/10/2015 1030 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060347
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/16/2015 1944
HMA 77407
1
(Bicarbonate ) SM 2320B-2011
1 06/16/2015 1944
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/16/2015 1944
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
580
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
580
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF12010-002
Description: 2015018389 Matrix: Aqueous
Date Sampled:06/10/2015 1030 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060347
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/16/2015 1848 JJG 77428
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 8 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF12010-003
Description: 2015018390 Matrix: Aqueous
Date Sampled:06/10/2015 1522 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060347
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/16/2015 1950
HMA 77407
1
(Bicarbonate ) SM 2320B-2011
1 06/16/2015 1950
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/16/2015 1950
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
26
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
26
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF12010-003
Description: 2015018390 Matrix: Aqueous
Date Sampled:06/10/2015 1522 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060347
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/16/2015 1911 JJG 77428
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 10 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF12010-004
Description: 2015018391 Matrix: Aqueous
Date Sampled:06/10/2015 1600 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060347
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/16/2015 1956
HMA 77407
1
(Bicarbonate ) SM 2320B-2011
1 06/16/2015 1956
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/16/2015 1956
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
100
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
100
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 11 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF12010-004
Description: 2015018391 Matrix: Aqueous
Date Sampled:06/10/2015 1600 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060347
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/16/2015 1926 JJG 77428
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 30 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 12 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF12010-005
Description: 2015018392 Matrix: Aqueous
Date Sampled:06/10/2015 1025 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060347
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/16/2015 2003
HMA 77407
1
(Bicarbonate ) SM 2320B-2011
1 06/16/2015 2003
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/16/2015 2003
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
120
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
120
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 13 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF12010-005
Description: 2015018392 Matrix: Aqueous
Date Sampled:06/10/2015 1025 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060347
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/16/2015 1936 JJG 77428
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 420 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 14 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF12010-006
Description: 2015018393 Matrix: Aqueous
Date Sampled:06/10/2015 1305 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060347
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/16/2015 2011
HMA 77407
1
(Bicarbonate ) SM 2320B-2011
1 06/16/2015 2011
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/16/2015 2011
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
350
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
350
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 15 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF12010-006
Description: 2015018393 Matrix: Aqueous
Date Sampled:06/10/2015 1305 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060347
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/16/2015 1951 JJG 77428
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 16 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 16 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF12010-007
Description: 2015018394 Matrix: Aqueous
Date Sampled:06/10/2015 1653 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060347
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/16/2015 2015
HMA 77407
1
(Bicarbonate ) SM 2320B-2011
1 06/16/2015 2015
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/16/2015 2015
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 17 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF12010-007
Description: 2015018394 Matrix: Aqueous
Date Sampled:06/10/2015 1653 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060347
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/16/2015 2004 JJG 77428
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 10 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 18 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF12010-008
Description: 2015018395 Matrix: Aqueous
Date Sampled:06/10/2015 1541 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060347
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/16/2015 2033
HMA 77407
1
(Bicarbonate ) SM 2320B-2011
1 06/16/2015 2033
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/16/2015 2033
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
38
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
38
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 19 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF12010-008
Description: 2015018395 Matrix: Aqueous
Date Sampled:06/10/2015 1541 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060347
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/16/2015 2015 JJG 77428
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 14 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 20 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF12010-009
Description: 2015018397 Matrix: Aqueous
Date Sampled:06/10/2015 0804 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060347
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/16/2015 2039
HMA 77407
1
(Bicarbonate ) SM 2320B-2011
1 06/16/2015 2039
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/16/2015 2039
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 21 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF12010-009
Description: 2015018397 Matrix: Aqueous
Date Sampled:06/10/2015 0804 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060347
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/16/2015 2037 JJG 77428
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 22 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: QF12010
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MB
Sample ID: QQ77407-001 Matrix: Aqueous
Batch:77407
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 06/16/20151902
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF12010
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - LCS
Sample ID: QQ77407-002 Matrix: Aqueous
Batch:77407
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 93 1 93 90-110 06/16/20151908
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF12010
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MS
Sample ID: QF12010-001 MS Matrix: Aqueous
Batch:77407
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 300 100 350 N 1 55 70-130 06/16/20151924
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF12010
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MSD
Sample ID: QF12010-001 MD Matrix: Aqueous
Batch:77407
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Alkalinity 300 100 360 N 1 56 0.28 70-130 20 06/16/20151932
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF12010
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ77379-001 Matrix: Aqueous
Batch:77379
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 06/16/20151207
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF12010
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ77379-002 Matrix: Aqueous
Batch:77379
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 50 43 1 86 70-130 06/16/20151142
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF12010
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ77379-003 Matrix: Aqueous
Batch:77379
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 50 50 1 99 14 70-130 30 06/16/20151156
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF12010
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ77428-001 Matrix: Aqueous
Batch:77428
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 06/16/20151701
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF12010
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ77428-002 Matrix: Aqueous
Batch:77428
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 50 43 1 85 70-130 06/16/20151632
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF12010
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ77428-003 Matrix: Aqueous
Batch:77428
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 50 44 1 87 2.2 70-130 30 06/16/20151646
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF12010
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC
c
0
�
[
\
�iq
.
L
\
�
ƒ
�
§
C r.4
--- �2
q
�
-
;■ !
�§&�
E
:
.i
Jj
�■$��$qLU
�
i
I ■ ,
�$ )|
El
�
�
�
Shealy Environmental Services, Inc.
106 GA# Point »e West Columbia, SC 29172 A% a,- m Fax A% a,au, www.shealylab.com Level 1 Report «,

SHEALY ENVIRONMENTAL SERVICES, INC.
'Stiealy rmvm mama] scrv6•.Cz, ln� Pegs I of I
Dm-wT WNµrnb%.F-AP-014 Repl.,Ltsnow 1IM704
Pwixian Number.. 17 EJIL%ti s+c Dwe{Id13l I5
Sample Receipt C1lecklist (:SRC)
C'licnt: UYt- O-et9iL Cooler Inspected by"'date. "r5P—S . Lot#: I t:7 t C]
Me= of rcccipl: Sf:Si ❑ Client ❑ UPS ❑ FedFx ❑ Airborne Rip L241hur
Yes ❑ No
1. Were cusiodywals prcscillit an the cool
Yes 1 No NA 2. If cu=dy sesls were prcscip, were they intact and unbroken?
Cooler ID106 irral temperature upon receiptI riN (cormted) w1ap€rai I,m 111an receipt:
Method, ❑ Temperature qbak Against Bottles IR Cue 1LI: ' _ 1R Gun Corrtction FaetDr: 43 °C
' Method of coolant; &Vet Ice Blue Ice El Dry lot [l Nme
Yes ❑
NO ❑
---
NAc2oPM
I If temperaEure of any cooler exceeded 6.01C, was Pray-1 Ma=ger notified?
(notified by SRC, phone, ante (circle one), other:
;For coolers received via cnmmerctal courier, FM are to be nod —bed
imjjaediat�lw.
Yea ❑NO
NA
4. Is the commcrciall courier's packiag slip attached to this form?
r:4
NO
❑
Were Proper oustody pro=durcs (reli uished,{received) followed?
Yes ❑
❑ I
NA
Sa Were smPles ref' 'shred b • client to commercial couric r?
Yes
. a
❑
6, Were sample IDs listed un the CQC°?
YCS
No
❑
7, Wcrc sample IDs listed on all sample containers?
Yes
No
❑
$. W collection eta! It 6 lisped on the
Yes
o
Q
q, Was enller-doi l date & time listed on all ram le contairte,x?
Yes
M..
a
❑
10. Did all contairur label mfatranatien (ID, date, time) Agree v ith the COC?
Yes
n
❑
11. ll = tests to be perfi?rmaxl listed on the Cam 7
Y
o
®
I2. Did all saaWlez arrive is the prqper eoutainers for each test'!
Yes210
❑
13_ Did all containers aujvc in good coDditien u1 brokean. lids can etc.)?
No
14.. Was adequate sain le volume availablav?
Yes ❑
Noy
15.'4'cre all samples rmci%rd vdthin !/x the holding time or 48 hours, whichever
comes first?
Ys"
No
16, Were any sir les containers miss° ?
Yes ❑
No Ef
17, Weire there Lny excess samples not listed on, CMG?
Yes ❑
No `
NALJ
19. Wcre bubbles cscnt �i Ica -sire°' (W or 6mm in diamer) in any VOA vials?
Yes 0
No ❑
NA
1 J_ Were s1I =4a1!V(D&G/FEFMlnutrien1 samples rcocived at -a pH of <2?
Yes ❑
No ❑ TNA
7
20. Were all cyanide and'or sulfide sa bes recei wed at a 2H >127
Yes ❑
No ❑
Nei
21. 'Were all applicable NH3JKNlcyatudeipwhew1(<{)_2mVL) samples free of
residual chlorine?
Yes ❑
No ❑
NA 2n
22, Were col leuion temperatures documented an the CCC fir NC samples?
Yes [I
No ❑
NA!rL24,Tm
3. Ware client Tomarks!requests (Le- requested dilutions, MS.MSD designatious,
csomectl transcribed from the C'DC into the r ent section is LIMS?
Ye4 ❑
No
the quote number used txjken fram the contai= label?
Sample Preservation (Must be oompletW for any sample(s) inct rroody pruu; r -cd air viitb bcadsspaec.)
samples) %vre received incorrectly XtuT.ved and were adjusted
3oc(vrdiagly in sawn le receiving wit11 S0.HNQj.H Na0H using S1t #
Sawn le(s) were received with bubbles >6 mm in diarncter,
Stun lu . were received with TRC >0_2. m I If R21 is. No
SC Drinkitng Water Project Saniple(s) pH verified to bc: =' 2 by Date,
Sam. lc(a;) were ncA avp=ivted at a pH of '' 2 and w= adi uated according] i ..SRO
ample Zalrels a lia:d b}: Verified by, ]Late:-1 --
Comments
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM
AnalytcliVrifterra EDD
Duke Energy Analytical Laboratory Analytical Laborato Use On Page 04 OT tf4
Duke Energy Page_1_of_1_
Mal CodeMGOSA2 eua9g7maJ ! !Order# Matrix GW_WW NC_
Analytical 13339Hager,FerryRtl sc_ DISTRIBUTION
Chain of Custody a Halltil le, N. C. xaor9 !Logged By a rimeI j ORIGINAL to LAB, COPY to CLIENT
Sample Log (79q a7sstas SAMPLE PROGRAM
) J J Ground Water _ NPDES _
_
Pr.jeat Nan --_---AB GW Assessment water Plane No: -- - r (� Drinking Water_ UST_
RCRA Waste COC REV DATE 1/22/2015
L , Fax No: _.._.._. CooMr Tome.���.._.._...._.._.._.._.............................. ................... ........ .._�
Client ._ 980675s0 Shealy tration (0.45 um) Unfiltered !1 filer"°
P01142.Oi�9 �M-
BuainessUnit: vree.ee: a.ay.cnfrro Preservative k» ke ke x Ice I=
all
ProJaor IM Al ID: Mail Code. emn A0 ml 300 in Soo Soo 2L 600 250
MG03A3
9eay: i-ea Elelrentl ' GEL
lass PET PET PET PET HDPE HOPE HOPE
P011421331 PO E Z 1142110
m
.
Sample Description or ID N
S 10 > V
ana deo ,r.w�. •" ml �l ,�.
W 9 m call o »
cc
UJ
Collection Information a to (,� a
I UJI m el
GPS Location C u e vl I
g y n O o F
v
Date Time Signature o n H .- U H Z ¢ 'm Li > wn Z t- > 0 E
_
itVils61Q �i�i�x
W
/�
�i
X
1
2
1
1
1
1
1
1
11
3w
-
y&
Q3o
'A
r
/
/
/
e
310
-
_) 0
5'
1
!
I
%
I
o
W-13
a s
16�
I
2
1
1
J
/
)
0
D
0
, 0-
)
l
1
J
/
3a5
MO
o
0
Filter Blank
)CLAS
R09
1
1
31 j
Euipment Blank
, p )+5
1
2
1
1
1
1
1
8
0
TOTAL
2
4
2
2
2
2
2
0
0
0
2
2
0
20
Relinquia
DateR'ime
Atcepjbd By:
DatalTime
m
m
Requested Tumaro nd
E
Relinquished By DatelTime
cepted By: DatelTi
741
alc
n P
14 Days
7 Days
RelinquiA By DaterTime
sh}
Acce By: Da m
E
c a
ek d By Datarrime
SeakMlLock Opened By Date rime
i
�
o m
E n
•- d
v
'48Hr
afiy
ELEMENTS by ICP MS (TRM): As, Be, Cd, Cc, Cr, Cu, Mo, NI, Pb, Sb, Se, TI (ILL), V (LL)
o
*Other ASAP
AP
ELEMENTS by Ill(TRM): Al, Be, B. Fe, Mn, Sr, 2n
ICP Undigested Ca, Mg, K, Na
Hg by 245.1
m
•Add. Cost Apply
Dissolved metals: all metals ICP, IMS,Hg
U
Total 20