NC0003417_J15050639report_20150805

+ DUKE Analytical Laboratory
ENERGY
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
Order Number: J15050639
Project Name: HF LEE PLANT - AB GW ASSESSMENT WATER
Customer Name(s): Tim Hunsucker, Judd Mahan, Kathy Webb, John Toepfer
Customer Address: 1677 Old Smithfield Rd
Goldsboro NC 27530,
Lab Contact: Mary Ann Oqle Phone: [phone]
I �� / � � Mary Ann Ogle
Report Authorized By: % "(7:N�kY.-04'00'
� 2015.06.1013:40:32pate:
(Signature)
Mary Ann Ogle
Program Comments:
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
6/9/2015
Page 1 of 51
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Collection
Sample ID Plant/Station Date and Time
Collected By
Sample Description
2015015807
HF LEE PLANT
20-May-15 2:10 PM
Judd Mahan
AMW-14BC
2015015808
HF LEE PLANT
20-May-15 1:50 PM
Judd Mahan
AMW-14S
2015015809
HF LEE PLANT
20-May-15 5:45 PM
Judd Mahan
AMW-156C
2015015810
HF LEE PLANT
21-May-15 10:20 AM
Judd Mahan
AMW-15S
2015015811
HF LEE PLANT
21-May-15 3:25 PM
Judd Mahan
AMW-4BC
2015015814
HF LEE PLANT
20-May-15 10:25 AM
Judd Mahan
Filter Blank
2015015815
HF LEE PLANT
20-May-15 10:25 AM
Judd Mahan
Equipment Blank
2015015816
HF LEE PLANT
21-May-15 1:30 PM
Judd Mahan
Equipment Blank
2015015817
HF LEE PLANT
21-May-15 1:30 PM
Judd Mahan
Filter Blank
9 Total Samples
Page 2 of 51

Page 3 of 51
Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals Yes No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes❑ No
All laboratory QA/QC requirements are acceptable.❑ Yes ❑ No
Report Sections Included:
U Job Summary Report
❑ Sample Identification
n Technical Validation of Data Package
❑ Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
66 Chain of Custody
[I/0] Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Peggy Kendall Date: 6/9/2015

Certificate of Laboratory Analysis Page 4 of 51
This report shall not be reproduced, except in full.
Order # J15050639
Site: AMW-14BC
Collection Date: 20-May-15 2:10 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.019
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
18
mg/L
1
Sulfate
31
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.006
mg/L
0.005
Barium (Ba)
0.059
mg/L
0.005
Boron (B)
0.227
mg/L
0.05
Iron (Fe)
1.99
mg/L
0.01
Manganese (Mn)
0.119
mg/L
0.005
Strontium (Sr)
0.120
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
17.5
mg/L
0.01
Magnesium (Mg)
5.44
mg/L
0.005
Potassium (K)
4.90
mg/L
0.1
Sodium (Na)
30.9
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.109
mg/L
0.005
Barium (Ba)
0.060
mg/L
0.005
Boron (B)
0.224
mg/L
0.05
Iron (Fe)
2.09
mg/L
0.01
Manganese (Mn)
0.121
mg/L
0.005
Strontium (Sr)
0.117
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015015807
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
05/29/2015 14:56
LSTARL1
10
EPA 300.0
05/28/2015 18:24
BGN9034
10
EPA 300.0
05/28/2015 18:24
BGN9034
1
EPA 245.1
05/29/2015 12:09
ACPAYNE
1
EPA 245.1
06/01/2015 15:07
ACPAYNE
1
EPA 200.7
05/28/2015 11:16
MHALL3
1
EPA 200.7
05/28/2015 11:16
MHALL3
1
EPA 200.7
05/28/2015 11:16
MHALL3
1
EPA 200.7
05/28/2015 11:16
MHALL3
1
EPA 200.7
05/28/2015 11:16
MHALL3
1
EPA 200.7
05/28/2015 11:16
MHALL3
1
EPA 200.7
05/28/2015 11:16
MHALL3
1
EPA 200.7
05/28/2015 12:15
MHH7131
1
EPA 200.7
05/28/2015 12:15
MHH7131
1
EPA 200.7
05/28/2015 12:15
MHH7131
1
EPA 200.7
05/28/2015 12:15
MHH7131
1
EPA 200.7
05/27/2015 14:33
MHALL3
1
EPA 200.7
05/27/2015 14:33
MHALL3
1
EPA 200.7
05/27/2015 14:33
MHALL3
1
EPA 200.7
05/27/2015 14:33
MHALL3
1
EPA 200.7
05/27/2015 14:33
MHALL3
1
EPA 200.7
05/27/2015 14:33
MHALL3
1
EPA 200.7
05/27/2015 14:33
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050639
Site: AMW-14BC
Collection Date: 20-May-15 2:10 PM
Analyte
Result
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
2.38
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
2.33
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
0.402
Vanadium (V) Low Level
< 0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
180
Total Carbon
TOC
0.535
TOTAL SUSPENDED SOLIDS
TSS
11
Page 5 of 51
Sample #:
2015015807
Matrix:
GW_WW
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
06/05/2015 14:26
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:26
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:26
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:26
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:26
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:26
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:26
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:26
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:26
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:26
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:26
JAHERMA
ug/L
0.2
1
EPA 200.8
06/05/2015 14:26
JAHERMA
ug/L
0.3
1
EPA 200.8
06/05/2015 14:26
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 10:57
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 10:57
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 10:57
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 10:57
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 10:57
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 10:57
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 10:57
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 10:57
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 10:57
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 10:57
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 10:57
JAHERMA
ug/L
0.2
1
EPA 200.8
06/06/2015 10:57
JAHERMA
ug/L
0.3
1
EPA 200.8
06/06/2015 10:57
JAHERMA
Vendor Method
V_SHEALY
Vendor Method
V_ELE1
mg/L
25
1
SM2540C
05/26/201515:35
AGIBBS5
mg/L
0.1
1
SM5310C/EPA9060A
06/02/201513:44
TJA7067
mg/L
5
1
SM2540D
05/26/201510:27
AGIBBS5

Certificate of Laboratory Analysis Page 6 of 51
This report shall not be reproduced, except in full.
Order # J15050639
Site: AMW-14S
Collection Date: 20-May-15 1:50 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.021
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
19
mg/L
1
Sulfate
29
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.022
mg/L
0.005
Barium (Ba)
0.063
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
10.7
mg/L
0.01
Manganese (Mn)
0.136
mg/L
0.005
Strontium (Sr)
0.058
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
7.23
mg/L
0.01
Magnesium (Mg)
3.40
mg/L
0.005
Potassium (K)
6.93
mg/L
0.1
Sodium (Na)
11.4
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.490
mg/L
0.005
Barium (Ba)
0.074
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
12.7
mg/L
0.01
Manganese (Mn)
0.159
mg/L
0.005
Strontium (Sr)
0.067
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015015808
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
05/29/2015 14:57
LSTARL1
10
EPA 300.0
05/28/2015 18:41
BGN9034
10
EPA 300.0
05/28/2015 18:41
BGN9034
1
EPA 245.1
05/29/2015 12:11
ACPAYNE
1
EPA 245.1
06/01/2015 15:10
ACPAYNE
1
EPA 200.7
05/28/2015 11:20
MHALL3
1
EPA 200.7
05/28/2015 11:20
MHALL3
1
EPA 200.7
05/28/2015 11:20
MHALL3
1
EPA 200.7
05/28/2015 11:20
MHALL3
1
EPA 200.7
05/28/2015 11:20
MHALL3
1
EPA 200.7
05/28/2015 11:20
MHALL3
1
EPA 200.7
05/28/2015 11:20
MHALL3
1
EPA 200.7
05/28/2015 12:27
MHH7131
1
EPA 200.7
05/28/2015 12:27
MHH7131
1
EPA 200.7
05/28/2015 12:27
MHH7131
1
EPA 200.7
05/28/2015 12:27
MHH7131
1
EPA 200.7
05/27/2015 14:44
MHALL3
1
EPA 200.7
05/27/2015 14:44
MHALL3
1
EPA 200.7
05/27/2015 14:44
MHALL3
1
EPA 200.7
05/27/2015 14:44
MHALL3
1
EPA 200.7
05/27/2015 14:44
MHALL3
1
EPA 200.7
05/27/2015 14:44
MHALL3
1
EPA 200.7
05/27/2015 14:44
MHALL3

Certificate of Laboratory Analysis Page 7 of 51
This report shall not be reproduced, except in full.
Order # J15050639
Site: AMW-14S
Sample #: 2015015808
Collection Date: 20-May-15 1:50 PM
Matrix: GW_WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:30
JAHERMA
Arsenic (As)
1.41
ug/L
1
1
EPA 200.8
06/05/2015 14:30
JAHERMA
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:30
JAHERMA
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:30
JAHERMA
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:30
JAHERMA
Cobalt (Co)
4.26
ug/L
1
1
EPA 200.8
06/05/2015 14:30
JAHERMA
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:30
JAHERMA
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:30
JAHERMA
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:30
JAHERMA
Nickel (Ni)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:30
JAHERMA
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:30
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
06/05/2015 14:30
JAHERMA
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
06/05/2015 14:30
JAHERMA
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 10:43
JAHERMA
Arsenic (As)
1.72
ug/L
1
1
EPA 200.8
06/06/2015 10:43
JAHERMA
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 10:43
JAHERMA
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 10:43
JAHERMA
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 10:43
JAHERMA
Cobalt (Co)
4.91
ug/L
1
1
EPA 200.8
06/06/2015 10:43
JAHERMA
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 10:43
JAHERMA
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 10:43
JAHERMA
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 10:43
JAHERMA
Nickel (Ni)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 10:43
JAHERMA
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 10:43
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
06/06/2015 10:43
JAHERMA
Vanadium (V) Low Level
0.605
ug/L
0.3
1
EPA 200.8
06/06/2015 10:43
JAHERMA
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
100
mg/L
25
1
SM2540C
05/26/201515:35
AGIBBS5
Total Carbon
TOC
2.4
mg/L
0.1
1
SM5310C/EPA9060A
06/02/201513:44
TJA7067
TOTAL SUSPENDED SOLIDS
TSS
22
mg/L
5
1
SM2540D
05/26/201510:27
AGIBBS5

Certificate of Laboratory Analysis Page 8 of 51
This report shall not be reproduced, except in full.
Order # J15050639
Site: AMW-15BC
Collection Date: 20-May-15 5:45 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.032
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
11
mg/L
1
Sulfate
18
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.005
mg/L
0.005
Barium (Ba)
0.055
mg/L
0.005
Boron (B)
0.176
mg/L
0.05
Iron (Fe)
1.61
mg/L
0.01
Manganese (Mn)
0.097
mg/L
0.005
Strontium (Sr)
0.095
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
13.9
mg/L
0.01
Magnesium (Mg)
5.94
mg/L
0.005
Potassium (K)
5.78
mg/L
0.1
Sodium (Na)
25.6
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.264
mg/L
0.005
Barium (Ba)
0.058
mg/L
0.005
Boron (B)
0.177
mg/L
0.05
Iron (Fe)
1.86
mg/L
0.01
Manganese (Mn)
0.097
mg/L
0.005
Strontium (Sr)
0.097
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015015809
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
05/29/2015 14:59
LSTARL1
10
EPA 300.0
05/28/2015 18:57
BGN9034
10
EPA 300.0
05/28/2015 18:57
BGN9034
1
EPA 245.1
05/29/2015 12:13
ACPAYNE
1
EPA 245.1
06/01/2015 15:12
ACPAYNE
1
EPA 200.7
05/28/2015 11:24
MHALL3
1
EPA 200.7
05/28/2015 11:24
MHALL3
1
EPA 200.7
05/28/2015 11:24
MHALL3
1
EPA 200.7
05/28/2015 11:24
MHALL3
1
EPA 200.7
05/28/2015 11:24
MHALL3
1
EPA 200.7
05/28/2015 11:24
MHALL3
1
EPA 200.7
05/28/2015 11:24
MHALL3
1
EPA 200.7
05/28/2015 12:31
MHH7131
1
EPA 200.7
05/28/2015 12:31
MHH7131
1
EPA 200.7
05/28/2015 12:31
MHH7131
1
EPA 200.7
05/28/2015 12:31
MHH7131
1
EPA 200.7
05/27/2015 14:48
MHALL3
1
EPA 200.7
05/27/2015 14:48
MHALL3
1
EPA 200.7
05/27/2015 14:48
MHALL3
1
EPA 200.7
05/27/2015 14:48
MHALL3
1
EPA 200.7
05/27/2015 14:48
MHALL3
1
EPA 200.7
05/27/2015 14:48
MHALL3
1
EPA 200.7
05/27/2015 14:48
MHALL3

Certificate of Laboratory Analysis Page 9 of 51
This report shall not be reproduced, except in full.
Order # J15050639
Site: AMW-15BC
Sample #: 2015015809
Collection Date: 20-May-15 5:45 PM
Matrix: GW_WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:35
JAHERMA
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:35
JAHERMA
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:35
JAHERMA
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:35
JAHERMA
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:35
JAHERMA
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:35
JAHERMA
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:35
JAHERMA
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:35
JAHERMA
Molybdenum (Mo)
1.27
ug/L
1
1
EPA 200.8
06/05/2015 14:35
JAHERMA
Nickel (Ni)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:35
JAHERMA
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:35
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
06/05/2015 14:35
JAHERMA
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
06/05/2015 14:35
JAHERMA
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:02
JAHERMA
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:02
JAHERMA
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:02
JAHERMA
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:02
JAHERMA
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:02
JAHERMA
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:02
JAHERMA
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:02
JAHERMA
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:02
JAHERMA
Molybdenum (Mo)
1.16
ug/L
1
1
EPA 200.8
06/06/2015 11:02
JAHERMA
Nickel (Ni)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:02
JAHERMA
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:02
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
06/06/2015 11:02
JAHERMA
Vanadium (V) Low Level
0.311
ug/L
0.3
1
EPA 200.8
06/06/2015 11:02
JAHERMA
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
150
mg/L
25
1
SM2540C
05/26/201515:35
AGIBBS5
Total Carbon
TOC
0.488
mg/L
0.1
1
SM5310C/EPA9060A
06/02/201513:44
TJA7067
TOTAL SUSPENDED SOLIDS
TSS
23
mg/L
5
1
SM2540D
05/26/201510:27
AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050639
Site: AMW-15S
Collection Date: 21-May-15 10:20 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.014
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
12
mg/L
1
Sulfate
22
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.025
mg/L
0.005
Barium (Ba)
0.055
mg/L
0.005
Boron (B)
0.149
mg/L
0.05
Iron (Fe)
3.33
mg/L
0.01
Manganese (Mn)
0.064
mg/L
0.005
Strontium (Sr)
0.072
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
6.12
mg/L
0.01
Magnesium (Mg)
2.43
mg/L
0.005
Potassium (K)
3.99
mg/L
0.1
Sodium (Na)
7.78
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.286
mg/L
0.005
Barium (Ba)
0.057
mg/L
0.005
Boron (B)
0.149
mg/L
0.05
Iron (Fe)
3.49
mg/L
0.01
Manganese (Mn)
0.066
mg/L
0.005
Strontium (Sr)
0.073
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015015810
Matrix: GW_WW
Page 10 of 51
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
05/29/2015 15:00
LSTARL1
10
EPA 300.0
05/28/2015 22:30
BGN9034
10
EPA 300.0
05/28/2015 22:30
BGN9034
1
EPA 245.1
05/29/2015 12:25
ACPAYNE
1
EPA 245.1
06/01/2015 15:15
ACPAYNE
1
EPA 200.7
05/28/2015 11:27
MHALL3
1
EPA 200.7
05/28/2015 11:27
MHALL3
1
EPA 200.7
05/28/2015 11:27
MHALL3
1
EPA 200.7
05/28/2015 11:27
MHALL3
1
EPA 200.7
05/28/2015 11:27
MHALL3
1
EPA 200.7
05/28/2015 11:27
MHALL3
1
EPA 200.7
05/28/2015 11:27
MHALL3
1
EPA 200.7
05/28/2015 12:35
MHH7131
1
EPA 200.7
05/28/2015 12:35
MHH7131
1
EPA 200.7
05/28/2015 12:35
MHH7131
1
EPA 200.7
05/28/2015 12:35
MHH7131
1
EPA 200.7
05/27/2015 14:52
MHALL3
1
EPA 200.7
05/27/2015 14:52
MHALL3
1
EPA 200.7
05/27/2015 14:52
MHALL3
1
EPA 200.7
05/27/2015 14:52
MHALL3
1
EPA 200.7
05/27/2015 14:52
MHALL3
1
EPA 200.7
05/27/2015 14:52
MHALL3
1
EPA 200.7
05/27/2015 14:52
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050639
Site: AMW-15S
Collection Date: 21-May-15 10:20 AM
Analyte
Result
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
1.23
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
1.21
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
1.75
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
77
Total Carbon
TOC
2.9
TOTAL SUSPENDED SOLIDS
TSS
< 5
Page 11 of 51
Sample #:
2015015810
Matrix:
GW_WW
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
06/05/2015 14:40
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:40
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:40
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:40
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:40
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:40
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:40
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:40
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:40
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:40
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 14:40
JAHERMA
ug/L
0.2
1
EPA 200.8
06/05/2015 14:40
JAHERMA
ug/L
0.3
1
EPA 200.8
06/05/2015 14:40
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 11:06
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 11:06
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 11:06
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 11:06
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 11:06
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 11:06
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 11:06
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 11:06
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 11:06
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 11:06
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 11:06
JAHERMA
ug/L
0.2
1
EPA 200.8
06/06/2015 11:06
JAHERMA
ug/L
0.3
1
EPA 200.8
06/06/2015 11:06
JAHERMA
Vendor Method
V_SHEALY
Vendor Method
V_ELE1
mg/L
25
1
SM2540C
05/27/201514:10
AGIBBS5
mg/L
0.1
1
SM5310C/EPA9060A
06/02/201513:44
TJA7067
mg/L
5
1
SM2540D
05/28/2015 08:28
AGIBBS5

Certificate of Laboratory Analysis Page 12 of 51
This report shall not be reproduced, except in full.
Order # J15050639
Site: AMW-413C
Collection Date: 21-May-15 3:25 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.028
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
41
mg/L
1
Sulfate
22
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.017
mg/L
0.005
Barium (Ba)
0.182
mg/L
0.005
Boron (B)
0.109
mg/L
0.05
Iron (Fe)
5.45
mg/L
0.01
Manganese (Mn)
0.110
mg/L
0.005
Strontium (Sr)
0.201
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
36.3
mg/L
0.01
Magnesium (Mg)
11.8
mg/L
0.005
Potassium (K)
3.76
mg/L
0.1
Sodium (Na)
24.7
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.070
mg/L
0.005
Barium (Ba)
0.200
mg/L
0.005
Boron (B)
0.115
mg/L
0.05
Iron (Fe)
6.19
mg/L
0.01
Manganese (Mn)
0.118
mg/L
0.005
Strontium (Sr)
0.215
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015015811
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
05/29/2015 15:01
LSTARL1
10
EPA 300.0
05/28/2015 23:20
BGN9034
10
EPA 300.0
05/28/2015 23:20
BGN9034
1
EPA 245.1
05/29/2015 12:32
ACPAYNE
1
EPA 245.1
06/01/2015 15:26
ACPAYNE
1
EPA 200.7
05/28/2015 11:46
MHALL3
1
EPA 200.7
05/28/2015 11:46
MHALL3
1
EPA 200.7
05/28/2015 11:46
MHALL3
1
EPA 200.7
05/28/2015 11:46
MHALL3
1
EPA 200.7
05/28/2015 11:46
MHALL3
1
EPA 200.7
05/28/2015 11:46
MHALL3
1
EPA 200.7
05/28/2015 11:46
MHALL3
1
EPA 200.7
05/28/2015 13:11
MHH7131
1
EPA 200.7
05/28/2015 13:11
MHH7131
1
EPA 200.7
05/28/2015 13:11
MHH7131
1
EPA 200.7
05/28/2015 13:11
MHH7131
1
EPA 200.7
05/27/2015 14:55
MHALL3
1
EPA 200.7
05/27/2015 14:55
MHALL3
1
EPA 200.7
05/27/2015 14:55
MHALL3
1
EPA 200.7
05/27/2015 14:55
MHALL3
1
EPA 200.7
05/27/2015 14:55
MHALL3
1
EPA 200.7
05/27/2015 14:55
MHALL3
1
EPA 200.7
05/27/2015 14:55
MHALL3

Certificate of Laboratory Analysis Page 13 of 51
This report shall not be reproduced, except in full.
Order # J15050639
Site: AMW-413C
Sample #: 2015015811
Collection Date: 21-May-15 3:25 PM
Matrix: GW_WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:44
JAHERMA
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:44
JAHERMA
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:44
JAHERMA
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:44
JAHERMA
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:44
JAHERMA
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:44
JAHERMA
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:44
JAHERMA
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:44
JAHERMA
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:44
JAHERMA
Nickel (Ni)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 14:44
JAHERMA
Selenium (Se)
2.65
ug/L
1
1
EPA 200.8
06/05/2015 14:44
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
06/05/2015 14:44
JAHERMA
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
06/05/2015 14:44
JAHERMA
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:11
JAHERMA
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:11
JAHERMA
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:11
JAHERMA
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:11
JAHERMA
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:11
JAHERMA
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:11
JAHERMA
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:11
JAHERMA
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:11
JAHERMA
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:11
JAHERMA
Nickel (Ni)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:11
JAHERMA
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 11:11
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
06/06/2015 11:11
JAHERMA
Vanadium (V) Low Level
0.521
ug/L
0.3
1
EPA 200.8
06/06/2015 11:11
JAHERMA
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
240
mg/L
25
1
SM2540C
05/27/201514:10
AGIBBS5
Total Carbon
TOC
1.9
mg/L
0.1
1
SM5310C/EPA9060A
06/02/201513:44
TJA7067
TOTAL SUSPENDED SOLIDS
TSS
19
mg/L
5
1
SM2540D
05/28/2015 08:28
AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050639
Site: Filter Blank
Collection Date: 20-May-15 10:25 AM
Analyte
Result
Units
Qualifiers RDL
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
0.022
mg/L
0.005
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015015814
Matrix: GW_WW
Page 14 of 51
DF
Method
Analysis Date/Time
Analyst
1
EPA 245.1
06/01/2015 15:33
ACPAYNE
1
EPA 200.7
05/28/2015 11:58
MHALL3
1
EPA 200.7
05/28/2015 11:58
MHALL3
1
EPA 200.7
05/28/2015 11:58
MHALL3
1
EPA 200.7
05/28/2015 11:58
MHALL3
1
EPA 200.7
05/28/2015 11:58
MHALL3
1
EPA 200.7
05/28/2015 11:58
MHALL3
1
EPA 200.7
05/28/2015 11:58
MHALL3
1
EPA 200.8
06/05/2015 14:49
JAHERMA
1
EPA 200.8
06/05/2015 14:49
JAHERMA
1
EPA 200.8
06/05/2015 14:49
JAHERMA
1
EPA 200.8
06/05/2015 14:49
JAHERMA
1
EPA 200.8
06/05/2015 14:49
JAHERMA
1
EPA 200.8
06/05/2015 14:49
JAHERMA
1
EPA 200.8
06/05/2015 14:49
JAHERMA
1
EPA 200.8
06/05/2015 14:49
JAHERMA
1
EPA 200.8
06/05/2015 14:49
JAHERMA
1
EPA 200.8
06/05/2015 14:49
JAHERMA
1
EPA 200.8
06/05/2015 14:49
JAHERMA
1
EPA 200.8
06/05/2015 14:49
JAHERMA
1
EPA 200.8
06/05/2015 14:49
JAHERMA

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050639
Site: Equipment Blank
Collection Date: 20-May-15 10:25 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.016
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
< 0.1
mg/L
0.1
Sulfate
< 0.1
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
UNDIGESTED METALS BY ICP
Calcium (Ca)
< 0.01
mg/L
0.01
Magnesium (Mg)
< 0.005
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
< 0.05
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Page 15 of 51
Sample #: 2015015815
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2
05/29/2015 15:07
LSTARL1
1 EPA 300.0
05/28/2015 23:36
BGN9034
1 EPA 300.0
05/28/2015 23:36
BGN9034
1 EPA 245.1
05/29/2015 12:35
ACPAYNE
1 EPA 200.7
05/28/2015 12:43
MHH7131
1 EPA 200.7
05/28/2015 12:43
MHH7131
1 EPA 200.7
05/28/2015 12:43
MHH7131
1 EPA 200.7
05/28/2015 12:43
MHH7131
1 EPA 200.7
05/27/2015 14:59
MHALL3
1 EPA 200.7
05/27/2015 14:59
MHALL3
1 EPA 200.7
05/27/2015 14:59
MHALL3
1 EPA 200.7
05/27/2015 14:59
MHALL3
1 EPA 200.7
05/27/2015 14:59
MHALL3
1 EPA 200.7
05/27/2015 14:59
MHALL3
1 EPA 200.7
05/27/2015 14:59
MHALL3
1 EPA 200.8
06/06/2015 11:16
JAHERMA
1 EPA 200.8
06/06/2015 11:16
JAHERMA
1 EPA 200.8
06/06/2015 11:16
JAHERMA
1 EPA 200.8
06/06/2015 11:16
JAHERMA
1 EPA 200.8
06/06/2015 11:16
JAHERMA
1 EPA 200.8
06/06/2015 11:16
JAHERMA
1 EPA 200.8
06/06/2015 11:16
JAHERMA
1 EPA 200.8
06/06/2015 11:16
JAHERMA
1 EPA 200.8
06/06/2015 11:16
JAHERMA
1 EPA 200.8
06/06/2015 11:16
JAHERMA
1 EPA 200.8
06/06/2015 11:16
JAHERMA
1 EPA 200.8
06/06/2015 11:16
JAHERMA
1 EPA 200.8
06/06/2015 11:16
JAHERMA
METHANE - (Analysis Performed by Shealy Labs
Methane (CH4) Complete
Vendor Method V_SHEALY

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050639
Site: Equipment Blank
Collection Date: 20-May-15 10:25 AM
Analyte Result Units Qualifiers RDL DF
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete
TOTAL DISSOLVED SOLIDS
TDS < 25 mg/L 25 1
Total Carbon
Sample #: 2015015815
Matrix: GW WW
Page 16 of 51
Method Analysis Date/Time Analyst
Vendor Method
V_ELE1
SM2540C 05/26/201515:35 AGIBBS5
TOC 0.141 mg/L 0.1 1 SM5310C/EPA9060A 06/02/201513:44 TJA7067
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L 5 1 SM2540D 05/26/2015 10:27 AGIBBS5

Certificate of Laboratory Analysis Page 17 of 51
This report shall not be reproduced, except in full.
Order # J15050639
Site: Equipment Blank
Collection Date: 21-May-15 1:30 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.013
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
< 0.1
mg/L
0.1
Sulfate
< 0.1
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
UNDIGESTED METALS BY ICP
Calcium (Ca)
0.017
mg/L
0.01
Magnesium (Mg)
< 0.005
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
< 0.05
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015015816
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2
05/29/2015 15:12
LSTARL1
1 EPA 300.0
05/28/2015 23:52
BGN9034
1 EPA 300.0
05/28/2015 23:52
BGN9034
1 EPA 245.1
05/29/2015 12:37
ACPAYNE
1 EPA 200.7
05/28/2015 12:47
MHH7131
1 EPA 200.7
05/28/2015 12:47
MHH7131
1 EPA 200.7
05/28/2015 12:47
MHH7131
1 EPA 200.7
05/28/2015 12:47
MHH7131
1 EPA 200.7
05/27/2015 15:03
MHALL3
1 EPA 200.7
05/27/2015 15:03
MHALL3
1 EPA 200.7
05/27/2015 15:03
MHALL3
1 EPA 200.7
05/27/2015 15:03
MHALL3
1 EPA 200.7
05/27/2015 15:03
MHALL3
1 EPA 200.7
05/27/2015 15:03
MHALL3
1 EPA 200.7
05/27/2015 15:03
MHALL3
1 EPA 200.8
06/06/2015 11:20
JAHERMA
1 EPA 200.8
06/06/2015 11:20
JAHERMA
1 EPA 200.8
06/06/2015 11:20
JAHERMA
1 EPA 200.8
06/06/2015 11:20
JAHERMA
1 EPA 200.8
06/06/2015 11:20
JAHERMA
1 EPA 200.8
06/06/2015 11:20
JAHERMA
1 EPA 200.8
06/06/2015 11:20
JAHERMA
1 EPA 200.8
06/06/2015 11:20
JAHERMA
1 EPA 200.8
06/06/2015 11:20
JAHERMA
1 EPA 200.8
06/06/2015 11:20
JAHERMA
1 EPA 200.8
06/06/2015 11:20
JAHERMA
1 EPA 200.8
06/06/2015 11:20
JAHERMA
1 EPA 200.8
06/06/2015 11:20
JAHERMA
METHANE - (Analysis Performed by Shealy Labs
Methane (CH4) Complete
Vendor Method V_SHEALY

Certificate of Laboratory Analysis Page 18 of 51
This report shall not be reproduced, except in full.
Order # J15050639
Site: Equipment Blank
Collection Date: 21-Mav-15 1:30 PM
Analyte Result Units Qualifiers RDL DF
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete
TOTAL DISSOLVED SOLIDS
TDS < 25 mg/L 25 1
Total Carbon
Sample #: 2015015816
Matrix: GW WW
Method Analysis Date/Time Analyst
Vendor Method
V_ELE1
SM2540C 05/27/201514:10 AGIBBS5
TOC 0.198 mg/L 0.1 1 SM5310C/EPA9060A 06/02/201513:44 TJA7067
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L 5 1 SM2540D 05/28/2015 08:28 AGIBBS5

Certificate of Laboratory Analysis Page 19 of 51
This report shall not be reproduced, except in full.
Order # J15050639
Site: Filter Blank
Collection Date: 21-May-15 1:30 PM
Analyte
Result
Units
Qualifiers RDL
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
0.035
mg/L
0.005
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015015817
Matrix: GW_WW
DF
Method
Analysis Date/Time
Analyst
1
EPA 245.1
06/01/2015 15:36
ACPAYNE
1
EPA 200.7
05/28/2015 12:02
MHALL3
1
EPA 200.7
05/28/2015 12:02
MHALL3
1
EPA 200.7
05/28/2015 12:02
MHALL3
1
EPA 200.7
05/28/2015 12:02
MHALL3
1
EPA 200.7
05/28/2015 12:02
MHALL3
1
EPA 200.7
05/28/2015 12:02
MHALL3
1
EPA 200.7
05/28/2015 12:02
MHALL3
1
EPA 200.8
06/05/2015 14:53
JAHERMA
1
EPA 200.8
06/05/2015 14:53
JAHERMA
1
EPA 200.8
06/05/2015 14:53
JAHERMA
1
EPA 200.8
06/05/2015 14:53
JAHERMA
1
EPA 200.8
06/05/2015 14:53
JAHERMA
1
EPA 200.8
06/05/2015 14:53
JAHERMA
1
EPA 200.8
06/05/2015 14:53
JAHERMA
1
EPA 200.8
06/05/2015 14:53
JAHERMA
1
EPA 200.8
06/05/2015 14:53
JAHERMA
1
EPA 200.8
06/05/2015 14:53
JAHERMA
1
EPA 200.8
06/05/2015 14:53
JAHERMA
1
EPA 200.8
06/05/2015 14:53
JAHERMA
1
EPA 200.8
06/05/2015 14:53
JAHERMA

Page 20 of 51
Element One Inc.
6319-D Carolina Beach Rd.
Wilmington, NC 28412
Rhone: 910 793-0128
Fax: [phone]
el lab@el lab com
eDe vemtOne
REPORT OF ANALYSES
Duke Energy
June 2, 2015
Laboratory Services
Client Project Name
AB GW Assessment water (wells)
13339 Hagers Ferry Road Bld. MG03A
Client Project Number J15050639
Huntersville, NC 28078
PO Number
Sample Matrix
Sample Type Grab
Date Received
05/26/2015
Date Analyzed 05/26/2015
Method
SM 4500 S2- D
Time Received
1400
Delivered by Fed Ex
Received by
JRC
eOne ID Duke Energy ID
Parameter
Result Unit
Dil DL Date
Time
Sampled
Sampled
24846-1* AMW-14 BC
Sulfide
< 0.2 mg/L
2 0.1 05/20/15
1410
24846-2 AMW-14 S
Sulfide
< 0.1 mg/L
1 0.1 05/20/15
1350
24846-3* AMW-15 BC
Sulfide
< 1.0 mg/L
10 0.1 05/20/15
1745
24846-4 AMW-15 S
Sulfide
0.105 mg/L
1 0.1 05/21/15
1020
24846-5 AMW-4 BC
Sulfide
0.142 mg/L
1 0.1 05/21/15
1525
24846-6 Equipment Blank
Sulfide
< 0.1 mg/L
1 0.1 05/20/15
1025
24846-7 Equipment Blank
Sulfide
< 0.1 mg/L
1 0.1 05/21/15
1330
*Sample spike recovery outside of QA limits of 85-115%; dilution necessary to meet laboratory QA limits.
Ken Smith, Laboratory Director
24846 Duke Report Packet Compiled by
NC Certifications: DW 37788 and DWQ DENR 604

Page 21 of 51
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elementOne
SAMPLE SUBMISSION FORM
Lab Ibge 2N946
Hold Time Expiration 05.27.15 @ 1350
Client: Duke Energy
LIMS No J15050639
Project ID HF Lee
Analysis Due Date 05.26.15
Report Due Date 06.04.15
Date Rec: 05.26.15
Time Rec: 1400
Rec By JRC
H >9 Y No
Tem <_ 60C a No
Ref. Method:
SM4500 S2 D
If No, Record
I If No, Record d
Sample Identification & Collection Information
Lab ID
I Client ID
Collection Date
Collection Time
Analysis Requested
1
AMW-14 BC
05/20/15
1410
fide
2
AMW-14 S
05/20/15
1350
3
4
5
AMW-15 BC _
AMW-15 S
AMW-4 BC
05/20/15
05/21/15
05/21/15
1745
1020
1525
Sulfi
Su i
i
6
Equipment Blank
05/20/15
1025
ulfide
7
Equipment Blank
05/21/15
1330
ulfi
NOTE for Sulfide The MS/MSD spike should approximate 2 to 3 times the sample concentration. If no sulfide detected
at 100 pg/L spike the sample to render the final spike concentration at — 500 pg/L
Lab Communications
All AB Groundwater Assessment
SS Page 1 of 1
SS by
5/26/201 3:22:35 PM
need a RL of 0.1
Prep By / Date 9, �-65 ' � 5 �\
Labeled By / Date S - z
I D Verification By /Date F cAf'` 5— a G f S

Page 23 of 51
METHOD:
SM 4500,S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
u /mL
DETECTION LIMIT (uq)
1.000
CLIENT:
Duke
SPK LEVELJuM
5
Lab ID#
24846
Na2S•9H2O Lot #
40721
MAX ALIQUOT
10.00
Date:
5/26/15
STANDARD conc(ppm)
X
Time Analysis Begun
15:52
Cal Std Lot: WC2-83-2
10
Time Analysis Ended
1700
JQC Std Lot: WC2-83-3
10
Analyst:
KAM
ISTID ABSORPTION
Y
X
Y
0eoo -
ug STD
SOLUTION
STD
ABS
08M
01�
- -
0600
6,
_ _o�
0.00
1.00
2.50
5.00
7.5t)
10.00
0.000
0.097
0.234
0.451'i
0.627
0.819
0.500
y
1,01
661
-sue
o,aoo
0+00
0�,0
2.00 400 800 8,00 woo 1200
X
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
Slope 0.081426374
Correlation 0.998678972'
ALI in mL
TAKEN
RESULTS
u /mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std, B. 0.00
0.000
0.0000
10
10
10
<
0
Std. B. 1.00
0.099
0.8016
10
10
10
<
80.16%
1
Std. B. 2.50
0.212
1 2.2671
10
10
10
0.227
90.68%
2.5
Std. B. 5.00
0.436
5.1719
10
10
10
0.517
103.44%
5
Std. B. 7.50
0.632
7.7137
10
10
10
0.771
102.85%
7.5
Std. B. 10.00
0.787
9.7238
10
10
10
0.972
97.24%
10
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.428
5.0682
10
10
10
0.507
102%
5.0
QC
0.426
5.0423
10
10
10
0.504
101 %
5.0
24946-1
0.018
-0.2488
10
10
10
<
24846-1 spk
0.343
3.9659
10
10
10
0.397
79%
5.0
24846-2
0.021
-0.2099
10
1 10
10
24846-2 dup
0.021
-0.2099
10
10
10
< 0.1
24846-2 spk
0.435
5.1590
10
10
10
0.516
103%
5.0
24846-3
0.035
-0.0283
10
10
10
<
24846-3 spk
0.190
1.9818
10
10
10
0.198
40%
5.0
24846-4
0.118
1.0480
10
1 10
10
Q.
24846-4 spk
0.518
6.2353
10
10
10
0.624
104%
5.0
24846-5
0.147
1.4241
10
10
10
24846-5 s k
0.541
6.5336
10
10
10
0.653
102%
5.0
24846-6
0.000
0.0000
10
10
10
24846-6 spk
0.416
4.9126
10
10
10
0.491
98%
5.0
24846-7
-0.004
0.0000
10
10
10
24846-7 spk
0.427
5.0552
10
10
10
0.506
101 %
5.0
24946-1
0.012
-0.3266
10 1
10
5
24846-1 spk
0.369
4.3031
10
10
5
0.861
86%
5.0
24846-3
0.015
-0.2877
10
10
5
<
24846-3 spk
0.261
2.9025
10
10
5
0.581
58%
5.0
Blank
0.000
0.0000
10
10
10
<
QC
0.425
5.0293
10
10
10
0.503
101 %
5.0
Submitted for QA/QC-
Date: 5/26/15
By: (Print)
KAM
(sign): '
Page 1 of 2

Page 24 of 51
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
Na2S•9H2O Lot #
40721
UNITS OF ANSWER
u /mL
DETECTION LIMIT (uM
1.000
CLIENT:
Lab ID#
Duke
24846
SPK LEVEL (uM
MAX ALIQUOT
5
10.00
Date:
5/26/15
STANDARD conc(ppm)
X
Time Analysis Begun
15:52
Cal Std Lot: WC2-83-2
10
Time Analysis Ended
1700
QC Std Lot: WC2-83-3
10
Analyst:
KAM
STD ABSORPTION
Y
X
Y
ug STD
SOLUTION
STD
ABS
6600
0700
-
---
--
--
-°°°
0'00
1.00
1.00
2.50
5.00
7.50
10.00
0.000
0.097
0.234
0.451
0.627
0.819
osoo
Y
0400
061
oso
2:
°'°°
0.100
°°°00 700 400 6.00 600 1000 12M
x
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
Sloe 0.081426374`
Correlation 0.998678972
ALI in mL
TAKEN
RESULTS
u /mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0
Std. B. 1.00
0.099
0.8016
10
10
10
<
80.16%
1
Std. B. 2.50
0.212
2.2671
10
10
10
0.227
90.68%
2.5
Std. B. 5.00
0.436
5.1719
10
10
10
0.517
103.44%
5
Std. B. 7.50
0.632
7.7137
10
10
10
0.771
102.85%
7.5
Std. B. 10.00
0.787
9.7238
10
10
10
0.972
97.24%
10
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.428
5.0682
10
10
10
0.507
102%
5.0
QC
0.426
5.0423
10
10
10
0.504
5.0
24846-3
0.000
0.0000
10
10
2
<
24846-3 s k
0.348
4.0307
10
10
2
2.015
81 %
5.0
24846-3
-0.003
0.0000
10
10
1
-
24846-3 s k
0.383
4.4846
10
10
1
4.485
90%
5.0
#VALUE!
#VALUE!
#VALUE!
#VALUE!
#VALUE!
#VALUE!
#VALUE!
#VALUE!
Blank
0.000
0.0000
10
10
10
<
QC
0.425
5.0293
10
10
10
0.503
101 %
5.0
Submitted for QA/QC-
Date: 5/26/15
By: (Print)
KAM
(sign):
Page 2 of 2

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
Project Name: AB GW Assessment Water (Wells)
Project Number:J15050639
Lot Number:QE22060
Date Completed:06/01/2015
Grant Wilton
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
* QE22060*
Shealy Environmental Services, Inc. Page: 1 of 18
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SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Duke Energy
Lot Number: QE22060
Project Name: AB GW Assessment Water (Wells)
Project Number: J15050639
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 18
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QE22060
Project Name: AB GW Assessment Water (Wells)
Project Number: J15050639
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
2015015807
Aqueous
05/20/20151410
05/22/2015
002
2015015808
Aqueous
05/20/20151350
05/22/2015
003
2015015809
Aqueous
05/20/20151745
05/22/2015
004
2015015810
Aqueous
05/21/20151020
05/22/2015
005
2015015811
Aqueous
05/21/20151525
05/22/2015
006
2015015815
Aqueous
05/20/20151025
05/22/2015
007
2015015816
Aqueous
05/21/20151330
05/22/2015
(7 samples)
Shealy Environmental Services, Inc. Page: 3 of 18
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SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QE22060
Project Name: AB GW Assessment Water (Wells)
Project Number: J15050639
Sample Sample ID
Matrix
Parameter Method
Result Q
Units
Page
001
2015015807
Aqueous
Alkalinity SM 2320B-
84
mg/L
5
001
2015015807
Aqueous
Bicarbonate Alkalinity SM 2320B-
84
mg/L
5
001
2015015807
Aqueous
Methane RSK - 175
74
ug/L
6
002
2015015808
Aqueous
Alkalinity SM 2320B-
23
mg/L
7
002
2015015808
Aqueous
Bicarbonate Alkalinity SM 2320B-
23
mg/L
7
003
2015015809
Aqueous
Alkalinity SM 2320B-
87
mg/L
9
003
2015015809
Aqueous
Bicarbonate Alkalinity SM 2320B-
87
mg/L
9
004
2015015810
Aqueous
Alkalinity SM 2320B-
15
mg/L
11
004
2015015810
Aqueous
Bicarbonate Alkalinity SM 2320B-
15
mg/L
11
004
2015015810
Aqueous
Methane RSK - 175
11
ug/L
12
005
2015015811
Aqueous
Alkalinity SM 2320B-
120
mg/L
13
005
2015015811
Aqueous
Bicarbonate Alkalinity SM 2320B-
120
mg/L
13
(12 detections)
Shealy Environmental Services, Inc. Page: 4 of 18
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QE22060-001
Description: 2015015807 Matrix: Aqueous
Date Sampled:05/20/2015 1410 Project Name: AB GW Assessment Water
Date Received:05/22/2015 Project Number: J15050639
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/28/2015 2320
HMA 76015
1
(Bicarbonate ) SM 2320B-2011
1 05/28/2015 2320
HMA
1
(Carbonate Al) SM 2320B-2011
1 05/28/2015 2320
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
84
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
84
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE22060-001
Description: 2015015807 Matrix: Aqueous
Date Sampled:05/20/2015 1410 Project Name: AB GW Assessment Water
Date Received:05/22/2015 Project Number: J15050639
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/28/2015 2208 JJG 76030
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 74 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE22060-002
Description: 2015015808 Matrix: Aqueous
Date Sampled:05/20/2015 1350 Project Name: AB GW Assessment Water
Date Received:05/22/2015 Project Number: J15050639
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/28/2015 2326
HMA 76015
1
(Bicarbonate ) SM 2320B-2011
1 05/28/2015 2326
HMA
1
(Carbonate Al) SM 2320B-2011
1 05/28/2015 2326
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
23
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
23
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 18
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Methane
Client: Duke Energy Laboratory ID: QE22060-002
Description: 2015015808 Matrix: Aqueous
Date Sampled:05/20/2015 1350 Project Name: AB GW Assessment Water
Date Received:05/22/2015 Project Number: J15050639
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/28/2015 2218 JJG 76030
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 8 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE22060-003
Description: 2015015809 Matrix: Aqueous
Date Sampled:05/20/2015 1745 Project Name: AB GW Assessment Water
Date Received:05/22/2015 Project Number: J15050639
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/28/2015 2346
HMA 76015
1
(Bicarbonate ) SM 2320B-2011
1 05/28/2015 2346
HMA
1
(Carbonate Al) SM 2320B-2011
1 05/28/2015 2346
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
87
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
87
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QE22060-003
Description: 2015015809 Matrix: Aqueous
Date Sampled:05/20/2015 1745 Project Name: AB GW Assessment Water
Date Received:05/22/2015 Project Number: J15050639
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/28/2015 2231 JJG 76030
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 10 of 18
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QE22060-004
Description: 2015015810 Matrix: Aqueous
Date Sampled:05/21/2015 1020 Project Name: AB GW Assessment Water
Date Received:05/22/2015 Project Number: J15050639
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/28/2015 2351
HMA 76015
1
(Bicarbonate ) SM 2320B-2011
1 05/28/2015 2351
HMA
1
(Carbonate Al) SM 2320B-2011
1 05/28/2015 2351
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
15
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
15
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QE22060-004
Description: 2015015810 Matrix: Aqueous
Date Sampled:05/21/2015 1020 Project Name: AB GW Assessment Water
Date Received:05/22/2015 Project Number: J15050639
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/28/2015 2254 JJG 76030
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 11 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QE22060-005
Description: 2015015811 Matrix: Aqueous
Date Sampled:05/21/2015 1525 Project Name: AB GW Assessment Water
Date Received:05/22/2015 Project Number: J15050639
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/28/2015 2357
HMA 76015
1
(Bicarbonate ) SM 2320B-2011
1 05/28/2015 2357
HMA
1
(Carbonate Al) SM 2320B-2011
1 05/28/2015 2357
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
120
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
120
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QE22060-005
Description: 2015015811 Matrix: Aqueous
Date Sampled:05/21/2015 1525 Project Name: AB GW Assessment Water
Date Received:05/22/2015 Project Number: J15050639
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/28/2015 2305 JJG 76030
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 14 of 18
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QE22060-006
Description: 2015015815 Matrix: Aqueous
Date Sampled:05/20/2015 1025 Project Name: AB GW Assessment Water
Date Received:05/22/2015 Project Number: J15050639
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/29/2015 0002
HMA 76015
1
(Bicarbonate ) SM 2320B-2011
1 05/28/2015 0002
HMA
1
(Carbonate Al) SM 2320B-2011
1 05/28/2015 0002
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QE22060-006
Description: 2015015815 Matrix: Aqueous
Date Sampled:05/20/2015 1025 Project Name: AB GW Assessment Water
Date Received:05/22/2015 Project Number: J15050639
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/28/2015 2315 JJG 76030
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 16 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE22060-007
Description: 2015015816 Matrix: Aqueous
Date Sampled:05/21/2015 1330 Project Name: AB GW Assessment Water
Date Received:05/22/2015 Project Number: J15050639
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/29/2015 0006
HMA 76015
1
(Bicarbonate ) SM 2320B-2011
1 05/28/2015 0006
HMA
1
(Carbonate Al) SM 2320B-2011
1 05/28/2015 0006
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 17 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE22060-007
Description: 2015015816 Matrix: Aqueous
Date Sampled:05/21/2015 1330 Project Name: AB GW Assessment Water
Date Received:05/22/2015 Project Number: J15050639
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/28/2015 2325 JJG 76030
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 18 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: QE22060
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - Ii
Sample ID: QQ76015-001 Matrix: Aqueous
Batch: 76015
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 05/28/2015 2226
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE22060
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - LCS
Sample ID: QQ76015-002 Matrix: Aqueous
Batch: 76015
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 99 1 99 90-110 05/28/2015 2233
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE22060
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ76030-001 Matrix: Aqueous
Batch:76030
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 05/28/20151924
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE22060
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ76030-002 Matrix: Aqueous
Batch:76030
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 130 1 87 70-130 05/28/20151818
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE22060
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ76030-003 Matrix: Aqueous
Batch:76030
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 130 1 86 1.6 70-130 30 05/28/20151829
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE22060
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Peggy I of t
Shealy 516loorwrltaLSC Gzt-.li}C' "Ccs Raie: ttr0'J%la
C,X ..e,lt Kur. 5er. F-A11-0IG PfrixU. *Ew4r 0-V3QV11
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Sample Receipt. CheCkh ,t ( KQ
Client, niwc..or_ _ _ Cooler Inspected byJdate,'k`^t�-�,�i#,
A�frns taf receipt: ❑ SEa ❑ Client ❑ UPS ❑ F'edEx ❑ r'irkrorne $xp grOther
Yes
No
1_' "ere cust-Ody seals ixSEiyt on the coolor?
Ycv
1`ao
NA
2. if c11-afn }+ Teals wile preselult, were they hatact and anbrn cn?
Cooler Il3;CiriO nal temperature upon receiptTcrived (correded) tcmperatmc uPnn receipt.
1► ethad; ❑ Terrtperature 131an1t Against Botllcs IR Gun ID-,— M G-un � omectiui) Factor �
od of coolant. Wet lee ❑ )�Itte Ioo ❑ Li lc� ❑ None
tYes
3� It temgcrature of any craol� r rxoeeddd 6,4°C:, wss project Ivisrtaer notified?
rM notified by SRC, Phone, ricate (circle canc), other_
❑ No ❑ NA
or c�plers received -via cotn.t emial courier. PMs we to be TiaLi ed
it,�mcdtatel ,)
Yes ❑F—
the commelncial etaurier s $skin slip atttaoked#o this form?
Yes
NaVvere
c er tasted ^ mceduros (relin uishvdh�cceived €oTlo wed?
Yea
❑No
Sa Were sarn les reLwished t) client DO ocarnm�tial o9urier�?
6_ Were sarrl a IDs li6W on the CQC?
ides
7. ' Vert Sample IDs listed nn all slsrltple COrtt€tinets?
Yes
g. Was collectir n date & time listed on the CAC?
y�
9. as c[,1lectior<date & time listed oln all s
yesis
VN0 ❑
IO. I3id all cula(aiiker label infarmatiok, (ID date, time agree with the CCU?
�(es
No
11. W ere tests to be perfomied listed on the COO
'es
Ida
12. Did all salm Ics arrive in The rta r Cunt3ir1Er8 far e8efr #est?
a
Ala
13. Did all oontainers arrive iin cod Ct]Rtl�ht5n unbrvkem lids tart dw ;�s
ly
Na ❑
14. Was uate sa 1C vvlLmc ar►raSLatble7
1 S- Were all samples r eivEd within !/a the holding time or 48 hours, whichever
Yes ❑
comes first?
Yes ❑ old'
16. Were an 5-arn ley frtaium, liussing?
Yes No
NA
17, Wert there an excess sarn lcs not listed on t:OC?
1 Were bubbles e:nt =„ ea -size" ,-or tsrni7l in diameter} in any 'TC]A vim?
Yes ❑ 1+Ta
Yes ❑ N� Nt4
.
19. Were a metalsJU&GJHr,NUiiul.neiit sam: les rcceiaed at a H {if {2?
Wcre all n� aside and/or sullide samples re ive>d at a H >12?
1HLlTlCN/cyamidephcaiol (<i1.21ngiI.) saniples� fmc of
NyesNo20-
No ❑ NA[.21Wereallapplicable
22. Were 0DIUl cti4tl temperatures docul nted on the C fOr C' sariiples?
No ❑ i'•]A
3. Were client reirtaIl4S+PI`equests (i.C, requested &Fitiian.3. MSoMSD designatiottiF,
Yes �] I* o ❑ N A
etc.. _ 1 acorl l transcribed Flogs the COC itim the t wiiaent section in L IM `"
Yes ❑ lYta
2. �74Fas tltc ucte nunrkter ustd taken from the cotttsiner label?
wimple Pr serviltlon (i+. U_ be cclmpleted frrr any samplc(s) iucorrectlar pruscrvcd Or with headspace.)
were rcxacived incorrectly preserved arm were adjusted
Pl .s —
swug SR
CG[3rik1R ly in Sam— IGI�eIYLng with ( 2 Q4,HNQ3,HC Nat]Fi ll91i]
were reoeiva3 with laubiles mrn in diatoaeter_
Samples)
were ridded with TRC ill 2 #21 is PTO
Sam le s
SC F)ril 071-ft Water projrTct slnple(sj pT3 verified t be f 2 + _ mate-
Sam I
were not rrve3vcd at a pH of <2 and were adjusted alccordin uslti SR
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tyFrLfted lay: Tate,
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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

._._._._._._._._._._---------------- CHAIN OF CUSTODY RECORD AND - A
- ANALYSIS REQUEST FORM
oratory -----'---._._._._._._._._._.-.-._._._._._._.- Ana _ Analytical LaDora._._.uN.O
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Analytical Laboratory ._._. -.__._._._._._._._.-._._._._._._._._.-
DUIC@ En@f9Y Duke Energy Analytic-! Laboratory
cod. MG03A2 B.Nin i 74os ! !Order # Matrix GWW W NO
13339 Hagen Fury Rd sa.Fb• O gin•e p F an sc—
Chain of Custody a Hunter..., N. C. 28073 y ate Time
Sample Log t7041a75S24a ry� ' �t �/ SAMPLE PROGRAM
_ _ _ _ _ _ _ Fa._ a 67a3096 I:/w\ ram(. 0 6 Ground Water NPDES
f N0" a AB GW Assessment water No: t1 Drinking Water— UST_
resell i SHEALY V' RCRAWaete—
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900-87S-5032 PO 1142089 itration (0,46 um) b Unfiltered
inesS Unk: POOeif: Nola C" °if To: Preservative t- k. ice . k.
t ID: Acavay ID: Mae Coe.: H280..ox
MG03A3 C l e) (I C) I l l Volume (ml-) 2000 40 ml 300 125 Soo S00
Bey. abk t. Pn 1142133 Dntainer Type PET glass PET PET PET PET
Page 51 �51
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Page _1_ of 1
DISTRIBUTION
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ATE 1/22/2015
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ELEMENTS by ICP (TRM): AI, Ba, B, Fe, Mn, Sr, Zn ICP Undigested Ca, Mg, K, Na Mg by 245.1 0 "Other ASAP
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Dissolved metals: all metals ICP, IMS,Hg
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