NC0003417_J15040235 Report_20150805

DUE Analytical Laboratory
ENERGY
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
Order Number: J15040235
Project Name: HF LEE PLANT - AB GW ASSESSMENT WATER
Customer Name(s): Tim Hunsucker, Judd Mahan, Kathy Webb, John Toepfer
Customer Address: 1677 Old Smithfield Rd
Goldsboro NC 27530,
Lab Contact: Mary AnnjOgle Mary Ann Ogle Phone: [phone]
Report Authorized By: �7 2015.04.27 Date:
(Signature) 14:38:06-04'00'
Mary Ann Ogle
Program Comments:
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
4/27/2015
Analytical Lab
Page 1 of 41
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Collection
Sample ID Plant/Station Date and Time
2015010231
2015010232
2015010233
2015010234
2015010235
2015010236
6 Total Samples
Collected By
Sample Description
HF LEE PLANT
09-Apr-15 4:30 PM
Synterra
IABMW-1S
HF LEE PLANT
09-Apr-15 2:10 PM
Synterra
IABMW-2S
HF LEE PLANT
09-Apr-15 11:10 AM
Synterra
IABMW-3S
HF LEE PLANT
09-Apr-15 12:20 PM
Synterra
IABMW-3
HF LEE PLANT
09-Apr-15 10:00 AM
Synterra
Filter Blank
HF LEE PLANT
09-Apr-15 10:00 AM
Synterra
Equipment Blank
Analytical Lab
Page 2 of 41

Analytical Lab
Page 3 of 41
Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals 0 Yes ❑ No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes 0 No
All laboratory QA/QC requirements are acceptable. 0 Yes ❑ No
Report Sections Included:
E%-'] Job Summary Report
❑� Sample Identification
Technical Validation of Data Package
❑� Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
❑d Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
❑� Chain of Custody
❑� Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Mary Ann Ogle Date: 4/27/2015

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040235
Site: IABMW-1 S
Collection Date: 09-Apr-15 4:30 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
13
mg/L
1
Sulfate
11
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
M2 0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.031
mg/L
0.005
Barium (Ba)
0.164
mg/L
0.005
Boron (B)
0.251
mg/L
0.05
Iron (Fe)
27.8
mg/L
0.1
Manganese (Mn)
4.96
mg/L
0.005
Strontium (Sr)
0.465
mg/L
0.005
Zinc (Zn)
0.006
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
58.6
mg/L
0.1
Magnesium (Mg)
29.5
mg/L
0.05
Potassium (K)
0.792
mg/L
0.1
Sodium (Na)
15.9
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.093
mg/L
0.005
Barium (Ba)
0.173
mg/L
0.005
Boron (B)
0.253
mg/L
0.05
Iron (Fe)
30.4
mg/L
0.05
Manganese (Mn)
5.19
mg/L
0.005
Strontium (Sr)
0.486
mg/L
0.005
Zinc (Zn)
0.016
mg/L
0.005
Sample #: 2015010231
Matrix: GW_WW
Analytical Lab
Page 4 of 41
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
04/15/2015 15:03
LSTARLI
10
EPA 300.0
04/15/2015 18:06
BGN9034
10
EPA 300.0
04/15/2015 18:06
BGN9034
1
EPA 245.1
04/15/2015 12:34
ACPAYNE
1
EPA 245.1
04/15/2015 13:43
ACPAYNE
1
EPA 200.7
04/13/2015 09:17
MHH7131
1
EPA 200.7
04/13/2015 09:17
MHH7131
1
EPA 200.7
04/13/2015 09:17
MHH7131
10
EPA 200.7
04/13/2015 09:17
MHH7131
1
EPA 200.7
04/13/2015 09:17
MHH7131
1
EPA 200.7
04/13/2015 09:17
MHH7131
1
EPA 200.7
04/13/2015 09:17
MHH7131
10
EPA 200.7
04/13/2015 10:46
MHH7131
10
EPA 200.7
04/13/2015 10:46
MHH7131
1
EPA 200.7
04/13/2015 10:46
MHH7131
1
EPA 200.7
04/13/2015 10:46
MHH7131
1
EPA 200.7
04/15/2015 13:24
MHH7131
1
EPA 200.7
04/15/2015 13:24
MHH7131
1
EPA 200.7
04/15/2015 13:24
MHH7131
5
EPA 200.7
04/15/2015 13:24
MHH7131
1
EPA 200.7
04/15/2015 13:24
MHH7131
1
EPA 200.7
04/15/2015 13:24
MHH7131
1
EPA 200.7
04/15/2015 13:24
MHH7131

Analytical Lab
Certificate of Laboratory Analysis Page 5 of 41
This report shall not be reproduced, except in full.
Order # J15040235
Site: IABMW-1 S
Sample #: 2015010231
Collection Date: 09-Apr-15 4:30
PM
Matrix: GW_WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:05
DJSULL1
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:05
DJSULL1
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:05
DJSULL1
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:05
DJSULL1
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:05
DJSULL1
Cobalt (Co)
34.7
ug/L
1
1
EPA 200.8
04/20/2015 14:05
DJSULL1
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:05
DJSULL1
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:05
DJSULL1
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:05
DJSULL1
Nickel (Ni)
5.30
ug/L
1
1
EPA 200.8
04/20/2015 14:05
DJSULL1
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:05
DJSULL1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/20/2015 14:05
DJSULL1
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/20/2015 14:05
DJSULL1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:25
JAHERMA
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:25
JAHERMA
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:25
JAHERMA
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:25
JAHERMA
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:25
JAHERMA
Cobalt (Co)
35.6
ug/L
1
1
EPA 200.8
04/15/2015 15:25
JAHERMA
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:25
JAHERMA
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:25
JAHERMA
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:25
JAHERMA
Nickel (Ni)
4.95
ug/L
1
1
EPA 200.8
04/15/2015 15:25
JAHERMA
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:25
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/15/2015 15:25
JAHERMA
Vanadium (V) Low Level
0.361
ug/L
0.3
1
EPA 200.8
04/15/2015 15:25
JAHERMA
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
370
mg/L
25
1
SM2540C
04/14/201514:33
AGIBBS5
Total Carbon
TOC
3.3
mg/L
0.1
1
SM5310C/EPA9060A
04/16/201511:47
GHUTCHI
TOTAL SUSPENDED SOLIDS
TSS
11
mg/L
5
1
SM2540D
04/13/2015 08:15
AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040235
Site: IABMW-2S
Collection Date: 09-Apr-15 2:10 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.017
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
19
mg/L
1
Sulfate
110
mg/L
2
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
0.182
mg/L
0.005
Boron (B)
1.27
mg/L
0.05
Iron (Fe)
5.27
mg/L
0.01
Manganese (Mn)
2.84
mg/L
0.005
Strontium (Sr)
1.84
mg/L
0.005
Zinc (Zn)
0.007
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
85.2
mg/L
0.1
Magnesium (Mg)
49.4
mg/L
0.05
Potassium (K)
1.26
mg/L
0.1
Sodium (Na)
18.6
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.027
mg/L
0.005
Barium (Ba)
0.214
mg/L
0.005
Boron (B)
1.55
mg/L
0.05
Iron (Fe)
13.4
mg/L
0.01
Manganese (Mn)
4.19
mg/L
0.005
Strontium (Sr)
2.62
mg/L
0.005
Zinc (Zn)
0.005
mg/L
0.005
Sample #: 2015010232
Matrix: GW_WW
Analytical Lab
Page 6 of 41
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
04/15/2015 15:04
LSTARLI
10
EPA 300.0
04/16/2015 10:11
BGN9034
20
EPA 300.0
04/16/2015 10:11
BGN9034
1
EPA 245.1
04/15/2015 12:44
ACPAYNE
1
EPA 245.1
04/15/2015 13:50
ACPAYNE
1
EPA 200.7
04/13/2015 09:21
MHH7131
1
EPA 200.7
04/13/2015 09:21
MHH7131
1
EPA 200.7
04/13/2015 09:21
MHH7131
1
EPA 200.7
04/13/2015 09:21
MHH7131
1
EPA 200.7
04/13/2015 09:21
MHH7131
1
EPA 200.7
04/13/2015 09:21
MHH7131
1
EPA 200.7
04/13/2015 09:21
MHH7131
10
EPA 200.7
04/13/2015 10:50
MHH7131
10
EPA 200.7
04/13/2015 10:50
MHH7131
1
EPA 200.7
04/13/2015 10:50
MHH7131
1
EPA 200.7
04/13/2015 10:50
MHH7131
1
EPA 200.7
04/15/2015 13:28
MHH7131
1
EPA 200.7
04/15/2015 13:28
MHH7131
1
EPA 200.7
04/15/2015 13:28
MHH7131
1
EPA 200.7
04/15/2015 13:28
MHH7131
1
EPA 200.7
04/15/2015 13:28
MHH7131
1
EPA 200.7
04/15/2015 13:28
MHH7131
1
EPA 200.7
04/15/2015 13:28
MHH7131

Analytical Lab
Certificate of Laboratory Analysis Page 7 of 41
This report shall not be reproduced, except in full.
Order # J15040235
Site: IABMW-2S
Sample #: 2015010232
Collection Date: 09-Apr-15 2:10
PM
Matrix: GW_WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:10
DJSULL1
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:10
DJSULL1
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:10
DJSULL1
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:10
DJSULL1
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:10
DJSULL1
Cobalt (Co)
32.9
ug/L
1
1
EPA 200.8
04/20/2015 14:10
DJSULL1
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:10
DJSULL1
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:10
DJSULL1
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:10
DJSULL1
Nickel (Ni)
6.08
ug/L
1
1
EPA 200.8
04/20/2015 14:10
DJSULL1
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:10
DJSULL1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/20/2015 14:10
DJSULL1
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/20/2015 14:10
DJSULL1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:52
JAHERMA
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:52
JAHERMA
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:52
JAHERMA
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:52
JAHERMA
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:52
JAHERMA
Cobalt (Co)
52.7
ug/L
1
1
EPA 200.8
04/15/2015 15:52
JAHERMA
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:52
JAHERMA
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:52
JAHERMA
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:52
JAHERMA
Nickel (Ni)
4.57
ug/L
1
1
EPA 200.8
04/15/2015 15:52
JAHERMA
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:52
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/15/2015 15:52
JAHERMA
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/15/2015 15:52
JAHERMA
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
530
mg/L
25
1
SM2540C
04/14/201514:33
AGIBBS5
Total Carbon
TOC
3.0
mg/L
0.1
1
SM5310C/EPA9060A
04/16/201511:47
GHUTCHI
TOTAL SUSPENDED SOLIDS
TSS
8.0
mg/L
5
1
SM2540D
04/13/2015 08:15
AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040235
Site: IABMW-3S
Collection Date: 09-Apr-15 11:10 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
9.8
mg/L
1
Sulfate
29
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.010
mg/L
0.005
Barium (Ba)
0.182
mg/L
0.005
Boron (B)
0.554
mg/L
0.05
Iron (Fe)
52.6
mg/L
0.1
Manganese (Mn)
1.09
mg/L
0.005
Strontium (Sr)
0.365
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
25.0
mg/L
0.1
Magnesium (Mg)
9.42
mg/L
0.05
Potassium (K)
1.31
mg/L
0.1
Sodium (Na)
12.3
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.027
mg/L
0.005
Barium (Ba)
0.202
mg/L
0.005
Boron (B)
0.603
mg/L
0.05
Iron (Fe)
56.7
mg/L
0.05
Manganese (Mn)
1.18
mg/L
0.005
Strontium (Sr)
0.405
mg/L
0.005
Zinc (Zn)
0.009
mg/L
0.005
Sample #: 2015010233
Matrix: GW_WW
Analytical Lab
Page 8 of 41
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
04/15/2015 15:08
LSTARLI
10
EPA 300.0
04/15/2015 18:42
BGN9034
10
EPA 300.0
04/15/2015 18:42
BGN9034
1
EPA 245.1
04/15/2015 12:46
ACPAYNE
1
EPA 245.1
04/15/2015 13:53
ACPAYNE
1
EPA 200.7
04/13/2015 09:25
MHH7131
1
EPA 200.7
04/13/2015 09:25
MHH7131
1
EPA 200.7
04/13/2015 09:25
MHH7131
10
EPA 200.7
04/13/2015 09:25
MHH7131
1
EPA 200.7
04/13/2015 09:25
MHH7131
1
EPA 200.7
04/13/2015 09:25
MHH7131
1
EPA 200.7
04/13/2015 09:25
MHH7131
10
EPA 200.7
04/13/2015 10:54
MHH7131
10
EPA 200.7
04/13/2015 10:54
MHH7131
1
EPA 200.7
04/13/2015 10:54
MHH7131
1
EPA 200.7
04/13/2015 10:54
MHH7131
1
EPA 200.7
04/15/2015 13:33
MHH7131
1
EPA 200.7
04/15/2015 13:33
MHH7131
1
EPA 200.7
04/15/2015 13:33
MHH7131
5
EPA 200.7
04/15/2015 13:33
MHH7131
1
EPA 200.7
04/15/2015 13:33
MHH7131
1
EPA 200.7
04/15/2015 13:33
MHH7131
1
EPA 200.7
04/15/2015 13:33
MHH7131

Analytical Lab
Certificate of Laboratory Analysis Page 9 of 41
This report shall not be reproduced, except in full.
Order # J15040235
Site: IABMW-3S
Sample #: 2015010233
Collection Date: 09-Apr-15 11:10
AM
Matrix: GW_WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:14
DJSULL1
Arsenic (As)
3.10
ug/L
1
1
EPA 200.8
04/20/2015 14:14
DJSULL1
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:14
DJSULL1
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:14
DJSULL1
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:14
DJSULL1
Cobalt (Co)
1.22
ug/L
1
1
EPA 200.8
04/20/2015 14:14
DJSULL1
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:14
DJSULL1
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:14
DJSULL1
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:14
DJSULL1
Nickel (Ni)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:14
DJSULL1
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 14:14
DJSULL1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/20/2015 14:14
DJSULL1
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/20/2015 14:14
DJSULL1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:56
JAHERMA
Arsenic (As)
3.67
ug/L
1
1
EPA 200.8
04/15/2015 15:56
JAHERMA
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:56
JAHERMA
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:56
JAHERMA
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:56
JAHERMA
Cobalt (Co)
1.36
ug/L
1
1
EPA 200.8
04/15/2015 15:56
JAHERMA
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:56
JAHERMA
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:56
JAHERMA
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:56
JAHERMA
Nickel (Ni)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:56
JAHERMA
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/15/2015 15:56
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/15/2015 15:56
JAHERMA
Vanadium (V) Low Level
0.616
ug/L
0.3
1
EPA 200.8
04/15/2015 15:56
JAHERMA
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
240
mg/L
25
1
SM2540C
04/14/201514:33
AGIBBS5
Total Carbon
TOC
3.7
mg/L
0.1
1
SM5310C/EPA9060A
04/16/201511:47
GHUTCHI
TOTAL SUSPENDED SOLIDS
TSS
15
mg/L
5
1
SM2540D
04/13/2015 08:15
AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040235
Site: IABMW-3
Collection Date: 09-Apr-15 12:20 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.072
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
9.2
mg/L
0.1
Sulfate
87
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.028
mg/L
0.005
Barium (Ba)
0.133
mg/L
0.005
Boron (B)
0.619
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
0.025
mg/L
0.005
Strontium (Sr)
1.24
mg/L
0.005
Zinc (Zn)
0.014
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
56.1
mg/L
0.1
Magnesium (Mg)
19.9
mg/L
0.05
Potassium (K)
12.7
mg/L
0.1
Sodium (Na)
10.7
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.700
mg/L
0.005
Barium (Ba)
0.174
mg/L
0.005
Boron (B)
0.926
mg/L
0.05
Iron (Fe)
0.245
mg/L
0.01
Manganese (Mn)
0.045
mg/L
0.005
Strontium (Sr)
2.00
mg/L
0.005
Zinc (Zn)
0.015
mg/L
0.005
Sample #: 2015010234
Matrix: GW_WW
Analytical Lab
Page 10 of 41
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
04/15/2015 15:09
LSTARLI
1
EPA 300.0
04/15/2015 21:41
BGN9034
10
EPA 300.0
04/15/2015 21:41
BGN9034
1
EPA 245.1
04/15/2015 12:49
ACPAYNE
1
EPA 245.1
04/15/2015 13:55
ACPAYNE
1
EPA 200.7
04/13/2015 09:29
MHH7131
1
EPA 200.7
04/13/2015 09:29
MHH7131
1
EPA 200.7
04/13/2015 09:29
MHH7131
1
EPA 200.7
04/13/2015 09:29
MHH7131
1
EPA 200.7
04/13/2015 09:29
MHH7131
1
EPA 200.7
04/13/2015 09:29
MHH7131
1
EPA 200.7
04/13/2015 09:29
MHH7131
10
EPA 200.7
04/13/2015 10:58
MHH7131
10
EPA 200.7
04/13/2015 10:58
MHH7131
1
EPA 200.7
04/13/2015 10:58
MHH7131
1
EPA 200.7
04/13/2015 10:58
MHH7131
1
EPA 200.7
04/15/2015 13:37
MHH7131
1
EPA 200.7
04/15/2015 13:37
MHH7131
1
EPA 200.7
04/15/2015 13:37
MHH7131
1
EPA 200.7
04/15/2015 13:37
MHH7131
1
EPA 200.7
04/15/2015 13:37
MHH7131
1
EPA 200.7
04/15/2015 13:37
MHH7131
1
EPA 200.7
04/15/2015 13:37
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040235
Site: IABMW-3
Collection Date: 09-Apr-15 12:20 PM
Analyte
Result
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
6.01
Arsenic (As)
4.40
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
3.55
Cobalt (Co)
2.73
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
24.7
Nickel (Ni)
10.4
Selenium (Se)
613
Thallium (TI) Low Level
2.58
Vanadium (V) Low Level
18.0
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
8.71
Arsenic (As)
9.89
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
3.37
Cobalt (Co)
4.03
Copper (Cu)
1.27
Lead (Pb)
< 1
Molybdenum (Mo)
57.7
Nickel (Ni)
15.0
Selenium (Se)
1100
Thallium (TI) Low Level
2.85
Vanadium (V) Low Level
28.7
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Total Carbon
TOC
1.7
Sample #: 2015010234
Matrix: GW_WW
Analytical Lab
Page 11 of 41
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
04/20/2015 14:19
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 14:19
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 14:19
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 14:19
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 14:19
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 14:19
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 14:19
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 14:19
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 14:19
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 14:19
DJSULL1
ug/L
20
20
EPA 200.8
04/20/2015 14:19
DJSULL1
ug/L
0.2
1
EPA 200.8
04/20/2015 14:19
DJSULL1
ug/L
0.3
1
EPA 200.8
04/20/2015 14:19
DJSULL1
ug/L
1
1
EPA 200.8
04/15/2015 16:01
JAHERMA
ug/L
1
1
EPA 200.8
04/15/2015 16:01
JAHERMA
ug/L
1
1
EPA 200.8
04/15/2015 16:01
JAHERMA
ug/L
1
1
EPA 200.8
04/15/2015 16:01
JAHERMA
ug/L
1
1
EPA 200.8
04/15/2015 16:01
JAHERMA
ug/L
1
1
EPA 200.8
04/15/2015 16:01
JAHERMA
ug/L
1
1
EPA 200.8
04/15/2015 16:01
JAHERMA
ug/L
1
1
EPA 200.8
04/15/2015 16:01
JAHERMA
ug/L
1
1
EPA 200.8
04/15/2015 16:01
JAHERMA
ug/L
1
1
EPA 200.8
04/15/2015 16:01
JAHERMA
ug/L
50
50
EPA 200.8
04/15/2015 16:01
JAHERMA
ug/L
0.2
1
EPA 200.8
04/15/2015 16:01
JAHERMA
ug/L
0.3
1
EPA 200.8
04/15/2015 16:01
JAHERMA
Vendor Method
V_SHEALY
Vendor Method
V_ELE1
mg/L
0.1
1
SM5310C/EPA9060A
04/16/201511:47
GHUTCHI

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040235
Site: Filter Blank
Collection Date: 09-Apr-15 10:00 AM
Analyte
Result
Units
Qualifiers RDL
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 2
ug/L
2
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.6
ug/L
0.6
Sample #: 2015010235
Matrix: GW_WW
Analytical Lab
Page 12 of 41
DF
Method
Analysis Date/Time
Analyst
1
EPA 245.1
04/15/2015 13:57
ACPAYNE
1
EPA 200.7
04/13/2015 09:34
MHH7131
1
EPA 200.7
04/13/2015 09:34
MHH7131
1
EPA 200.7
04/13/2015 09:34
MHH7131
1
EPA 200.7
04/13/2015 09:34
MHH7131
1
EPA 200.7
04/13/2015 09:34
MHH7131
1
EPA 200.7
04/13/2015 09:34
MHH7131
1
EPA 200.7
04/13/2015 09:34
MHH7131
1
EPA 200.8
04/20/2015 14:46
DJSULL1
1
EPA 200.8
04/20/2015 14:46
DJSULL1
2
EPA 200.8
04/20/2015 14:46
DJSULL1
1
EPA 200.8
04/20/2015 14:46
DJSULL1
1
EPA 200.8
04/20/2015 14:46
DJSULL1
1
EPA 200.8
04/20/2015 14:46
DJSULL1
1
EPA 200.8
04/20/2015 14:46
DJSULL1
1
EPA 200.8
04/20/2015 14:46
DJSULL1
1
EPA 200.8
04/20/2015 14:46
DJSULL1
1
EPA 200.8
04/20/2015 14:46
DJSULL1
1
EPA 200.8
04/20/2015 14:46
DJSULL1
1
EPA 200.8
04/20/2015 14:46
DJSULL1
2
EPA 200.8
04/20/2015 14:46
DJSULL1

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040235
Site: Equipment Blank
Collection Date: 09-Apr-15 10:00 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
< 0.1
mg/L
0.1
Sulfate
< 0.1
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
UNDIGESTED METALS BY lCP
Calcium (Ca)
0.011
mg/L
0.01
Magnesium (Mg)
< 0.005
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
< 0.05
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Analytical Lab
Page 13 of 41
Sample #: 2015010236
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method V_SHEALY
1 EPA 353.2
04/15/2015 15:10
LSTARLI
1 EPA 300.0
04/15/2015 19:18
BGN9034
1 EPA 300.0
04/15/2015 19:18
BGN9034
1 EPA 245.1
04/15/2015 12:51
ACPAYNE
1 EPA 200.7
04/13/2015 11:02
MHH7131
1 EPA 200.7
04/13/2015 11:02
MHH7131
1 EPA 200.7
04/13/2015 11:02
MHH7131
1 EPA 200.7
04/13/2015 11:02
MHH7131
1 EPA 200.7
04/15/2015 13:48
MHH7131
1 EPA 200.7
04/15/2015 13:48
MHH7131
1 EPA 200.7
04/15/2015 13:48
MHH7131
1 EPA 200.7
04/15/2015 13:48
MHH7131
1 EPA 200.7
04/15/2015 13:48
MHH7131
1 EPA 200.7
04/15/2015 13:48
MHH7131
1 EPA 200.7
04/15/2015 13:48
MHH7131
1 EPA 200.8
04/15/2015 16:06
JAHERMA
1 EPA 200.8
04/15/2015 16:06
JAHERMA
1 EPA 200.8
04/15/2015 16:06
JAHERMA
1 EPA 200.8
04/15/2015 16:06
JAHERMA
1 EPA 200.8
04/15/2015 16:06
JAHERMA
1 EPA 200.8
04/15/2015 16:06
JAHERMA
1 EPA 200.8
04/15/2015 16:06
JAHERMA
1 EPA 200.8
04/15/2015 16:06
JAHERMA
1 EPA 200.8
04/15/2015 16:06
JAHERMA
1 EPA 200.8
04/15/2015 16:06
JAHERMA
1 EPA 200.8
04/15/2015 16:06
JAHERMA
1 EPA 200.8
04/15/2015 16:06
JAHERMA
1 EPA 200.8
04/15/2015 16:06
JAHERMA
METHANE - (Analysis Performed by Shealy Labs
Methane (CH4) Complete
Vendor Method V_SHEALY

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040235
Site: Equipment Blank
Collection Date: 09-Apr-15 10:00 AM
Analyte Result Units Qualifiers RDL DF
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete
TOTAL DISSOLVED SOLIDS
TDS < 25 mg/L 25 1
Total Carbon
Sample #: 2015010236
Matrix: GW_WW
Analytical Lab
Page 14 of 41
Method Analysis Date/Time Analyst
Vendor Method
V_ELE1
SM2540C 04/14/201514:33 AGIBBS5
TOC 0.186 mg/L 0.1 1 SM5310C/EPA9060A 04/16/201511:47 GHUTCHI
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L 5 1 SM2540D 04/13/2015 08:15 AGIBBS5
Qualifiers:
M2 Matrix spike recovery was Low: the associated Laboratory Control Spike (LCS) was acceptable.

Analytical Lab
Page 15 of 41
el,
elementOne
Duke Energy
Laboratory Services
13339 Hagers Ferry Road Bid. MG03A
Huntersville, NC 28078
Sample Matrix GW WW
Date Analyzed 04/14/2015
Delivered by FedEx
eOne ID Duke Energy ID
24497-1 IABMW-1 S
24497-2
IABMW-2S
24497-3
IABMW-3S
24497-4*
IABMW-3
24497-5
Equipment Blank
Element One Inc.
6319-D Carolina Beach Rd.
Wilmington, NC 28412
Phone: [phone]
Fax: [phone]
[e-mail]
REPORT OF ANALYSES
April 16, 2015
Client Project Name AB GW Assessment Water— HF Lee
Client Project Number J15040235
PO Number
Sample Type
Grab
Date Received
04/14/2015
Method
SM 4500 S2- D
Time Received
1115
Received by
JRC
Parameter
Result
Unit
Dil
DL Date
Time
Sampled
Sampled
Sulfide
< 0.1
mg/L
1
0.1 04/09/15
1630
Sulfide
< 0.1
mg/L
1
0.1 04/09/15
1410
Sulfide
< 0.1
mg/L
1
0.1 04/09/15
1110
Sulfide
< 0.2
mg/L
2
0.1 04/09/15
1220
Sulfide
< 0.1
mg/L
1
0.1 04/09/15
1000
*Sample spike recovery outside of QA limits of 85-115%; dilution necessary to meet laboratory QA limits.
Ka4 Strickla A Coordinator
24497 Duke Report Packet Compiled by
NC Certifications: DW 37788 and DWQ DENR 604

Analytical Lab
Page 16 of 41
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win
w f5
T
m

Analytical Lab
e ementOne SAMPLE SUBMISSION FORM Lab Ityge 124497
TAT 7 BD Analysis Due Date 04.15.15
Hold Time Expiration 04.16.15 @ 1000 AM Report Due Date 04.23.15
Client: Duke Energy Date Rec: 04.14.15
LIMS No J15040235 Time Rec: 1115
Project ID HF Lee-----,Rec By JRC
H >9 <_ Yes No Tem 6°C Yes No Ref. Method:
If No, Record If No, Record SM4500 S2 D
Samale Identification & Collection Information
Lab ID
Client ID
Collection Date
Collection Time
Analysis Requested
1
IABMW-1 S
O4.09.15
1630
fid
Ru
2
IABMW-2S
O4.09.15
1410
ul i
3
4
5
IABMW-3S
IABMW-3
Equipment Blank
O4.09.15
04.09.15
04.09.15
1110
1220
1011
Su f
Sul I
Sulfi
NOTE for Sulfide
The MS/MSD spike should approximate 2 to 3 times the sample concentra ion. If no sulfide detected
at 100 dig/L spike the sample to render the final spike concentration at — 500 dig/L
All AB Groundwater Assessment jobs need a RL of 0.1
Lab Communications
SS Page 1 of 1 Prep By / Date kAJ''` 1-1 ` I L-1 o
SS by .f Labeled By / Date cam- _ 4 • I S - 1:5
4/14/20 12:19:53 PM ID Verification By/Date k L/,1grIS

Analytical Lab
Page 18 of 41
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
ug/mL
DETECTION LIMIT(uq)
1.000
CLIENT:
Duke
SPK LEVEL w*
5
Lab ID#
24497 / 24498
Na2S•9H2O Lot #
40721
MAX ALIQUOT
10.00
Date:
4/14/15
STANDARD conc(ppm)
X
Time Analysis Begun
13:30
Cal Std Lot:
10
Time Analysis Ended
16:00
QC Std Lot:
Analyst:
KAM
STD ABSORPTION
Y
X
Y
--.
ug STD
SOLUTION
STD
01-
'00
ABS 0
0.000 1.
0
0.097 I °."°°
0.209
0.423 °.+wop
0.00
1.00
2.50
5.00
7.50
10.00
__ _
a
4Z .
---
---
0006w
0.599 zW 4.W 6A° em iom ,too
0.765 ! X
..�..
...e.
Slope 0.07658022
Correlation 0.998642417
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Sulfide Std. B. 0.00
0
0.0000
10
10
10
<
0
Sulfide Std. B. 1.00
0.094
0.8250
10
10
10
<
82.50%
1.0
Sulfide Std. B. 2.50
0.206
2.3669
10
10
10
0.237
94.68%
2.5
Sulfide Std. B. 5.00
0.399
5.0240
10
10
10
0.502
100.48%
5.0
Sulfide Std. B. 7.50
0.608
1 7.9013
10
10
10
0.790
105.35%
7.5
Sulfide Std. B. 10.00
0.729
9.5672
10
10
10
0.957
95.67%
10.0
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.437
5.5471
10
10
10
0.555
111 %
5.0
QC
0.422
5.3406
10
10
10
0.534
107%
5.0
24497-1
0.005
1 -0.4003
10
10
10
< 0.1
24497-1 spk
0.355
4.4182
10
10
10
0.442
88%
5.0
24497-2
0.015
-0.2626
10
10
10
< 0.1
24497-2 dup
0.011
-0.3177
10
10
10
<0.1
24497-2 spk
0.375
4.6936
10
10
10
0.469
94%
5.0
24497-3
0.032
-0.0286
10
10
10
< 0.1
24497-3 spk
0.420
5.3131
10
10
10
0.531
106%
5.0
24497-4
0.013
-0.2902
10
10
10
<0.1
24497-4 spk
0.462
5.8913
10
10
10
0.589
118%
5.0
24497-5
0.000
0.0000
10
10
10
< 0.1
24497-5 spk
0.425
5.3819
10
10
10
0.538
108%
5.0
24498-1
0.004
-0.4141
10
10
10
< 0.1
24498-1 spk
0.432
5.4783
10
10
10
0.548
110%
5.0
24498-2
0.005
-0.4003
10
10
10
< 0.1
24498-2 spk
0.435
5.5196
10
10
10
0.552
110%
5.0
24498-3
0.019
-0.2076
10
10
10
< 0.1
24498-3 spk
0.405
5.1066
10
10
10
0.511
102%
5.0
24497-4
0.010
-0.3315
10
10
5
< 0.2
24497-4 spk
0.444
5.6435
10
10
5
1.129
113%
5.0
1000ppm Std. QC
0.419
5.2993
10
10
10
0.530
106%
5.0
Blank
0.000
0.0000
10
10 1
10
<
QC
0.417
5.2718
10
10
10
0.527
105%
5.0
Submitted for QA/QC-
Date: 4/14/15
By: (Print)
KAM
(sign

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
Project Name: AB GW Assessment Water - HF Lee
Project Number:J15040235
Lot Number:QD14016
Date Completed:04/24/2015
Grant Wilton
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
*QD14016*
Shealy Environmental Services, Inc. Page: 1 of 14
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SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Duke Energy
Lot Number: QD14016
Project Name: AB GW Assessment Water - HF Lee
Project Number: J15040235
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 14
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QD14016
Project Name: AB GW Assessment Water - HF Lee
Project Number: J15040235
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
2015010231
Aqueous
04/09/20151630
04/14/2015
002
2015010232
Aqueous
04/09/20151410
04/14/2015
003
2015010233
Aqueous
04/09/20151110
04/14/2015
004
2015010234
Aqueous
04/09/20151220
04/14/2015
005
2015010236
Aqueous
04/09/20151000
04/14/2015
(5 samples)
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SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QD14016
Project Name: AB GW Assessment Water - HF Lee
Project Number: J15040235
Sample Sample ID
Matrix Parameter Method
Result Q
Units
Page
001
2015010231
Aqueous Alkalinity SM 2320B-
300
mg/L
5
001
2015010231
Aqueous Bicarbonate Alkalinity SM 2320B-
300
mg/L
5
001
2015010231
Aqueous Methane RSK - 175
82
ug/L
6
002
2015010232
Aqueous Alkalinity SM 2320B-
340
mg/L
7
002
2015010232
Aqueous Bicarbonate Alkalinity SM 2320B-
340
mg/L
7
003
2015010233
Aqueous Alkalinity SM 2320B-
95
mg/L
9
003
2015010233
Aqueous Bicarbonate Alkalinity SM 2320B-
95
mg/L
9
003
2015010233
Aqueous Methane RSK - 175
490
ug/L
10
004
2015010234
Aqueous Alkalinity SM 2320B-
140
mg/L
11
004
2015010234
Aqueous Bicarbonate Alkalinity SM 2320B-
140
mg/L
11
(10 detections)
Shealy Environmental Services, Inc. Page: 4 of 14
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QD14016-001
Description: 2015010231 Matrix: Aqueous
Date Sampled:04/09/2015 1630 Project Name: AB GW Assessment Water -
Date Received:04/14/2015 Project Number: J15040235
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/22/2015 1627
HMA 72555
1
(Bicarbonate ) SM 2320B-2011
1 04/22/2015 1730
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/22/2015 1730
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
300
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
300
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 14
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Methane
Client: Duke Energy Laboratory ID: QD14016-001
Description: 2015010231 Matrix: Aqueous
Date Sampled:04/09/2015 1630 Project Name: AB GW Assessment Water -
Date Received:04/14/2015 Project Number: J15040235
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 04/14/2015 1743 DCS 72503
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 82 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 14
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QD14016-002
Description: 2015010232 Matrix: Aqueous
Date Sampled:04/09/2015 1410 Project Name: AB GW Assessment Water -
Date Received:04/14/2015 Project Number: J15040235
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/22/2015 1627
HMA 72555
1
(Bicarbonate ) SM 2320B-2011
1 04/22/2015 1739
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/22/2015 1739
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
340
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
340
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QD14016-002
Description: 2015010232 Matrix: Aqueous
Date Sampled:04/09/2015 1410 Project Name: AB GW Assessment Water -
Date Received:04/14/2015 Project Number: J15040235
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 04/14/2015 1758 DCS 72503
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QD14016-003
Description: 2015010233 Matrix: Aqueous
Date Sampled:04/09/2015 1110 Project Name: AB GW Assessment Water -
Date Received:04/14/2015 Project Number: J15040235
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/22/2015 1627
HMA 72555
1
(Bicarbonate ) SM 2320B-2011
1 04/22/2015 1752
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/22/2015 1752
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
95
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
95
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QD14016-003
Description: 2015010233 Matrix: Aqueous
Date Sampled:04/09/2015 1110 Project Name: AB GW Assessment Water -
Date Received:04/14/2015 Project Number: J15040235
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 04/14/2015 2115 DCS 72503
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 490 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QD14016-004
Description: 2015010234 Matrix: Aqueous
Date Sampled:04/09/2015 1220 Project Name: AB GW Assessment Water -
Date Received:04/14/2015 Project Number: J15040235
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/22/2015 1627
HMA 72555
1
(Bicarbonate ) SM 2320B-2011
1 04/22/2015 1758
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/22/2015 1758
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
140
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
140
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QD14016-004
Description: 2015010234 Matrix: Aqueous
Date Sampled:04/09/2015 1220 Project Name: AB GW Assessment Water -
Date Received:04/14/2015 Project Number: J15040235
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 04/14/2015 2143 DCS 72503
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QD14016-005
Description: 2015010236 Matrix: Aqueous
Date Sampled:04/09/2015 1000 Project Name: AB GW Assessment Water -
Date Received:04/14/2015 Project Number: J15040235
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/22/2015 1627
HMA 72555
1
(Bicarbonate ) SM 2320B-2011
1 04/22/2015 1802
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/22/2015 1802
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QD14016-005
Description: 2015010236 Matrix: Aqueous
Date Sampled:04/09/2015 1000 Project Name: AB GW Assessment Water -
Date Received:04/14/2015 Project Number: J15040235
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 04/14/2015 2054 DCS 72503
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: QD14016
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - Ii
Sample ID: QQ72555-001 Matrix: Aqueous
Batch: 72555
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 04/22/20151627
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD14016
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - LCS
Sample ID: QQ72555-002 Matrix: Aqueous
Batch: 72555
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 110 1 109 90-110 04/22/20151627
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD14016
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ72503-001 Matrix: Aqueous
Batch: 72503
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 04/14/20151535
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD14016
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ72503-002 Matrix: Aqueous
Batch: 72503
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 130 1 88 70-130 04/14/20151456
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD14016
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ72503-003 Matrix: Aqueous
Batch: 72503
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 140 1 91 4.1 70-130 30 04/14/20151507
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD14016
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Shtvly Fsvmmnrntal Scnirs fac. NO 1 Of 1
LXF.-,u "daNur*rr.F-..APi!16 RepkncisAube:U7i1S-'I$
R"iiEina N n - 16 JOele. i 1,V17'i14
Sample Receipt Checklist (SRC)
slit t: Cooler Inspected byldatesXYy,� i_nt
Means-ofreaccipt: ❑ SEST [I Client ❑ UPS FrdEtix ❑ airborne Vxp 0 Otber
Yes Z
I No El 1 1. Wem custod sDals pjmsent on the cooler?
YO
ISO ❑ Itil= 2. If t. li"d �ls tgroprysmj, wcm thcy intact and unbroken'?
n'?
Cooler il)/ lriginal lemplGrature upon rucciptMerived (corwwd.) temperature upon. moeipt-
Method_ ennperattm Blank ❑ Against Botties IR Gun TT3 94 IR Mn CorrecliU® Factor. 0..�
Method of coo latit--Z Wet lee: ❑ Blue Ice ❑ Di-� rce ❑ Newic
Yes ❑
No ❑
NA
3. Tf 1e mperlature of any cooler e,,wcede d f _O C, wag Project MaElXlger nal Bred?
PM notified by Slit,, phone, note (circle ogle), oilier:
(For cooler received via commercial o ourier, PM& are to be; noti fi l
immediately.)
Yes ❑
No
NA El
1 4, Is ihe; o0tnnl=ial viurier's parking slip attached to this form?
Yes
NO ❑
5. Were proper tod edure5 (jzlmq Lahhadlrcomycd followed?
Yes
No ❑
NA ❑
5a Wcre sarn las rulinquiibed b • c.liEnt to commercial courier"'
Yes
No [ I
& Were sample IDs listed on the COO?
7. Were s le RN listed o a fall sam lc contain rs?
Yes
NV Q
Wac 11eCtli5la d#1te time listed the y9.
Was callecticn date time Iixwd on all wria le c�oniainen?
10. Did all aantainer label infonnatinn , date, time a with the COC.?
t_
11. Were tests to be crforined listed oa the` COC7
12. Did all sam les arrive ire the ar container . for e-9ch test?
13, Did all containers arriN�e in good cnndit%nn (unbroken, I ida ern, etc -I?
14. Was adr tiate 82MIe volume availabin?
Yes V
No U
yes El
N+
15,'Y4'ene all samples receis�i within �5 the holding time or 48 bours, whichevET
comes. filrst?
Yes ET
No 1
16,Wcre un 1es containers mi
Yrs- ❑
No
17, Were there Mexms - les not listed on CO ?
Y6s ❑
No 2r
V.A ❑
18,'Wcrcbubbles prcamit> ea -size" (3r4"or 61YM in diameter in any VOA vial&?
Yeg ❑
No ❑
NA.
19. Were all metallss.10&.a1HE,M1niArient gam less received at a ph of <2?
Yes ❑
Na ❑
N,-k F7,
20. Wcre all cyanide m Vor s ul ride samples received at s pFT > 12?
Yes ❑
No ❑
NA �
21. Were: a applicable NHI TKN/cyanida phe nol (<l0lrng)T-) samples free of
residual chlorine
Yes
No ❑
NA Rr
22. Were collection temperatures doctimented on that CDC for NC 5 les?
Yeas ❑
No ®
NA E!�
23. Were client remarl-9 requests (i.e. regh,esLed dilutions, MSeMSD dessign.ations,
etc...) correctly tran8cribod From the COC into the wrnmcn( Nectiun in Ll S'
'Yes El'No
l
24- Was the quotp, nwtm er used taken from the container label?
Sample P'reservatian (Must
be cwWleted for any sample(s) incorrectly preserved or with headspace,)
5ample(s)! . _.. were received incorrectly preserved and were adjusted
ac Dudin ly ' sam lc rcaci with (L-S0,,,HNO3,HCI,Na0H) using SR #
S L 6 were recoiled with bubbles >6 mm in diameter.
I s wiLrr rew vcsl with TRC >Um "I, rf #21 is lwlo
SIC Dr lolang Water Projcct Samplc(s) pH vcri63d to be;- 2 by Date,
saulplv(s) were not rmcivcd at a pH -of =:2 and wcm adjusted accordingly using SR#
Sam Ise label! applied lry: ``ter Verified by: Date,
Comments:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

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