NC0003417_J15030544 Report_20150805

Lab
DUI E Analytical Laboratory APagel1aof477
ENERGY
Order Number:
Project Name:
Customer Name(s):
Customer Address:
Lab Contact:
Report Authorized By:
(Signature)
Program Comments:
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
J15030544
HF LEE PLANT - AB GW ASSESSMENT WATER
Tim Hunsucker, Judd Mahan, Kathy Webb, John Toepfer
1677 Old Smithfield Rd
Goldsboro NC 27530,
Mary Ann Ogle
Phone: [phone]
r �� / Mary Ann Ogle
i "'f%6 C✓95 2015.04.15 12:12:08 Date:
(/-04'00'
Mary Ann Ogle
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
4/15/2015
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Collection
Sample ID Plant/Station Date and Time
2015007941
2015007942
2015007943
2015007944
4 Total Samples
Collected By
Sample Description
HF LEE PLANT
19-Mar-15 9:50 AM
ILLEGIBLE
ABMW-1S
HF LEE PLANT
19-Mar-15 11:09 AM
ILLEGIBLE
ABMW-1
HF LEE PLANT
19-Mar-15 11:51 AM
ILLEGIBLE
Equipment Blank
HF LEE PLANT
19-Mar-15 11:51 AM
ILLEGIBLE
Filter Blank
Analytical Lab
Page 2 of 47

Analytical Lab
Page 3 of 47
Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals 0 Yes ❑ No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes 0 No
All laboratory QA/QC requirements are acceptable. 0 Yes ❑ No
Report Sections Included:
E%-'] Job Summary Report
❑� Sample Identification
Technical Validation of Data Package
❑� Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
❑d Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
❑� Chain of Custody
❑� Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Mary Ann Ogle Date: 4/15/2015

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030544
Site: ABMW-1 S
Collection Date: 19-Mar-15 9:50 AM
Analyte
Result
Units
Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.1
mg-N/L
0.1
INORGANIC IONS BY IC
Chloride
41
mg/L
1
Sulfate
39
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.020
mg/L
0.005
Barium (Ba)
0.563
mg/L
0.005
Boron (B)
2.61
mg/L
0.05
Iron (Fe)
20.2
mg/L
0.01
Manganese (Mn)
1.16
mg/L
0.005
Strontium (Sr)
4.29
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
139
mg/L
M4
0.1
Magnesium (Mg)
17.8
mg/L
M4
0.005
Potassium (K)
10.8
mg/L
0.1
Sodium (Na)
32.3
mg/L
M4
0.5
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.269
mg/L
0.005
Barium (Ba)
0.574
mg/L
0.005
Boron (B)
2.66
mg/L
0.05
Iron (Fe)
19.9
mg/L
0.01
Manganese (Mn)
1.16
mg/L
0.005
Strontium (Sr)
4.32
mg/L
0.005
Zinc (Zn)
0.007
mg/L
0.005
Sample #: 2015007941
Matrix: GW WW
Analytical Lab
Page 4 of 47
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
10
EPA 353.2
03/24/2015 16:00
TLINN
10
EPA 300.0
03/25/2015 00:20
BGN9034
10
EPA 300.0
03/25/2015 00:20
BGN9034
1
EPA 245.1
03/31/2015 16:22
ACPAYNE
1
EPA 245.1
03/25/2015 17:46
ACPAYNE
1
EPA 200.7
03/24/2015 11:52
MHALL3
1
EPA 200.7
03/24/2015 11:52
MHALL3
1
EPA 200.7
03/24/2015 11:52
MHALL3
1
EPA 200.7
03/24/2015 11:52
MHALL3
1
EPA 200.7
03/24/2015 11:52
MHALL3
1
EPA 200.7
03/24/2015 11:52
MHALL3
1
EPA 200.7
03/24/2015 11:52
MHALL3
10
EPA 200.7
03/24/2015 14:07
MHALL3
1
EPA 200.7
03/24/2015 14:07
MHALL3
1
EPA 200.7
03/24/2015 14:07
MHALL3
10
EPA 200.7
03/24/2015 14:07
MHALL3
1
EPA 200.7
03/25/2015 12:06
MHALL3
1
EPA 200.7
03/25/2015 12:06
MHALL3
1
EPA 200.7
03/25/2015 12:06
MHALL3
1
EPA 200.7
03/25/2015 12:06
MHALL3
1
EPA 200.7
03/25/2015 12:06
MHALL3
1
EPA 200.7
03/25/2015 12:06
MHALL3
1
EPA 200.7
03/25/2015 12:06
MHALL3

Analytical Lab
Certificate of Laboratory Analysis Page 5 of 47
This report shall not be reproduced, except in full.
Order # J15030544
Site: ABMW-1 S
Sample #: 2015007941
Collection Date: 19-Mar-15 9:50 AM
Matrix: GW
WW
Analyte
Result
Units
Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
DISSOLVED METALS BY lCP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/14/2015 13:37
JAHERMA
Arsenic (As)
761
ug/L
M4
5
5
EPA 200.8
04/14/2015 13:37
JAHERMA
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/14/2015 13:37
JAHERMA
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/14/2015 13:37
JAHERMA
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
04/14/2015 13:37
JAHERMA
Cobalt (Co)
5.99
ug/L
1
1
EPA 200.8
04/14/2015 13:37
JAHERMA
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
04/14/2015 13:37
JAHERMA
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/14/2015 13:37
JAHERMA
Molybdenum (Mo)
34.5
ug/L
1
1
EPA 200.8
04/14/2015 13:37
JAHERMA
Nickel (Ni)
1.16
ug/L
1
1
EPA 200.8
04/14/2015 13:37
JAHERMA
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/14/2015 13:37
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/14/2015 13:37
JAHERMA
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/14/2015 13:37
JAHERMA
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/13/2015 14:57
JAHERMA
Arsenic (As)
745
ug/L
M4
20
20
EPA 200.8
04/13/2015 14:57
JAHERMA
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/13/2015 14:57
JAHERMA
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/13/2015 14:57
JAHERMA
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
04/13/2015 14:57
JAHERMA
Cobalt (Co)
6.17
ug/L
1
1
EPA 200.8
04/13/2015 14:57
JAHERMA
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
04/13/2015 14:57
JAHERMA
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/13/2015 14:57
JAHERMA
Molybdenum (Mo)
32.2
ug/L
1
1
EPA 200.8
04/13/2015 14:57
JAHERMA
Nickel (Ni)
1.32
ug/L
1
1
EPA 200.8
04/13/2015 14:57
JAHERMA
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/13/2015 14:57
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/13/2015 14:57
JAHERMA
Vanadium (V) Low Level
0.512
ug/L
0.3
1
EPA 200.8
04/13/2015 14:57
JAHERMA
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
510
mg/L
25
1
SM2540C
03/24/201511:00
AGIBBS5
Total Carbon
TOC
1.0
mg/L
N1
0.1
1
SM5310C/EPA9060A
03/31/201516:16
TJA7067
TOTAL SUSPENDED SOLIDS
TSS
150
mg/L
6.3
1
SM2540D
03/23/201514:45
AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030544
Site: ABMW-1
Collection Date: 19-Mar-15 11:09 AM
Analyte
Result
Units
Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.072
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
27
mg/L
1
Sulfate
11
mg/L
1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
0.024
mg/L
0.005
Barium (Ba)
1.06
mg/L
0.005
Boron (B)
2.55
mg/L
0.05
Iron (Fe)
21.2
mg/L
0.02
Manganese (Mn)
1.38
mg/L
0.005
Strontium (Sr)
6.36
mg/L
0.005
Zinc (Zn)
0.007
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
174
mg/L
M4
0.1
Magnesium (Mg)
24.0
mg/L
M4
0.05
Potassium (K)
16.1
mg/L
0.1
Sodium (Na)
39.3
mg/L
M4
0.5
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.098
mg/L
0.005
Barium (Ba)
1.08
mg/L
0.005
Boron (B)
2.55
mg/L
0.05
Iron (Fe)
19.6
mg/L
0.01
Manganese (Mn)
1.35
mg/L
0.005
Strontium (Sr)
6.25
mg/L
0.005
Zinc (Zn)
0.009
mg/L
0.005
Sample #: 2015007942
Matrix: GW WW
Analytical Lab
Page 6 of 47
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
03/24/2015 15:58
TLINN
10
EPA 300.0
03/25/2015 00:38
BGN9034
10
EPA 300.0
03/25/2015 00:38
BGN9034
1
EPA 245.1
03/31/2015 16:24
ACPAYNE
1
EPA 245.1
03/25/2015 17:56
ACPAYNE
1
EPA 200.7
03/24/2015 11:56
MHALL3
1
EPA 200.7
03/24/2015 11:56
MHALL3
1
EPA 200.7
03/24/2015 11:56
MHALL3
2
EPA 200.7
03/24/2015 11:56
MHALL3
1
EPA 200.7
03/24/2015 11:56
MHALL3
1
EPA 200.7
03/24/2015 11:56
MHALL3
1
EPA 200.7
03/24/2015 11:56
MHALL3
10
EPA 200.7
03/24/2015 14:11
MHALL3
10
EPA 200.7
03/24/2015 14:11
MHALL3
1
EPA 200.7
03/24/2015 14:11
MHALL3
10
EPA 200.7
03/24/2015 14:11
MHALL3
1
EPA 200.7
03/25/2015 12:17
MHALL3
1
EPA 200.7
03/25/2015 12:17
MHALL3
1
EPA 200.7
03/25/2015 12:17
MHALL3
1
EPA 200.7
03/25/2015 12:17
MHALL3
1
EPA 200.7
03/25/2015 12:17
MHALL3
1
EPA 200.7
03/25/2015 12:17
MHALL3
1
EPA 200.7
03/25/2015 12:17
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030544
Site: ABMW-1
Collection Date: 19-Mar-15 11:09 AM
Analyte
Result
DISSOLVED METALS BY lCP-MS
Antimony (Sb)
< 1
Arsenic (As)
197
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
1.27
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
8.37
Nickel (Ni)
2.49
Selenium (Se)
< 1
Thallium (TI) Low Level
0.524
Vanadium (V) Low Level
3.05
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
182
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
1.41
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
8.01
Nickel (Ni)
3.07
Selenium (Se)
< 1
Thallium (TI) Low Level
0.789
Vanadium (V) Low Level
3.76
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
640
Total Carbon
TOC
1.1
TOTAL SUSPENDED SOLIDS
TSS
51
Sample #: 2015007942
Matrix: GW WW
Analytical Lab
Page 7 of 47
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
04/14/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:52
JAHERMA
ug/L
0.2
1
EPA 200.8
04/14/2015 13:52
JAHERMA
ug/L
0.3
1
EPA 200.8
04/14/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
04/13/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/13/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/13/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/13/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/13/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/13/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/13/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/13/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/13/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/13/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/13/2015 15:14
JAHERMA
ug/L
0.2
1
EPA 200.8
04/13/2015 15:14
JAHERMA
ug/L
0.3
1
EPA 200.8
04/13/2015 15:14
JAHERMA
Vendor Method
V_SHEALY
mg/L 25
mg/L N1 0.1
mg/L N2 5
Vendor Method
V_ELE1
1 SM2540C 03/24/201511:00
AGIBBS5
1 SM5310C/EPA9060A 03/31/201516:16
TJA7067
1 SM2540D 03/27/201513:24
AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030544
Site: Equipment Blank
Collection Date: 19-Mar-15 11:51 AM
Analyte
Result
Units
Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
< 0.1
mg/L
0.1
Sulfate
< 0.1
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
UNDIGESTED METALS BY lCP
Calcium (Ca)
< 0.01
mg/L
M4
0.01
Magnesium (Mg)
< 0.005
mg/L
M4
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
< 0.05
mg/L
M4
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Analytical Lab
Page 8 of 47
Sample #: 2015007943
Matrix: GW WW
DF Method Analysis Date/Time Analyst
Vendor Method V_SHEALY
1 EPA 353.2
03/24/2015 15:52
TLINN
1 EPA 300.0
03/24/2015 22:15
BGN9034
1 EPA 300.0
03/24/2015 22:15
BGN9034
1 EPA 245.1
03/31/2015 16:27
ACPAYNE
1 EPA 200.7
03/24/2015 14:26
MHALL3
1 EPA 200.7
03/24/2015 14:26
MHALL3
1 EPA 200.7
03/24/2015 14:26
MHALL3
1 EPA 200.7
03/24/2015 14:26
MHALL3
1 EPA 200.7
03/25/2015 13:11
MHALL3
1 EPA 200.7
03/25/2015 13:11
MHALL3
1 EPA 200.7
03/25/2015 13:11
MHALL3
1 EPA 200.7
03/25/2015 13:11
MHALL3
1 EPA 200.7
03/25/2015 13:11
MHALL3
1 EPA 200.7
03/25/2015 13:11
MHALL3
1 EPA 200.7
03/25/2015 13:11
MHALL3
1 EPA 200.8
04/13/2015 15:19
JAHERMA
1 EPA 200.8
04/13/2015 15:19
JAHERMA
1 EPA 200.8
04/13/2015 15:19
JAHERMA
1 EPA 200.8
04/13/2015 15:19
JAHERMA
1 EPA 200.8
04/13/2015 15:19
JAHERMA
1 EPA 200.8
04/13/2015 15:19
JAHERMA
1 EPA 200.8
04/13/2015 15:19
JAHERMA
1 EPA 200.8
04/13/2015 15:19
JAHERMA
1 EPA 200.8
04/13/2015 15:19
JAHERMA
1 EPA 200.8
04/13/2015 15:19
JAHERMA
1 EPA 200.8
04/13/2015 15:19
JAHERMA
1 EPA 200.8
04/13/2015 15:19
JAHERMA
1 EPA 200.8
04/13/2015 15:19
JAHERMA
METHANE - (Analysis Performed by Shealy Labs
Methane (CH4) Complete
Vendor Method V_SHEALY

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030544
Site: Equipment Blank
Collection Date: 19-Mar-15 11:51 AM
Analyte Result Units Qualifiers RDL DF
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete
TOTAL DISSOLVED SOLIDS
TDS < 25 mg/L 25 1
Total Carbon
Sample #: 2015007943
Matrix: GW WW
Analytical Lab
Page 9 of 47
Method Analysis Date/Time Analyst
Vendor Method
V_ELE1
SM2540C 03/24/201511:00 AGIBBS5
TOC 0.117 mg/L N1 0.1 1 SM5310C/EPA9060A 03/31/201516:16 TJA7067
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L N2 5 1 SM2540D 03/27/2015 13:24 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030544
Site: Filter Blank
Collection Date: 19-Mar-15 11:51 AM
Analyte Result
Mercury Dissolved (cold vapor) in Water (Filtered
Mercury (Hg)
< 0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
< 0.005
Barium (Ba)
< 0.005
Boron (B)
< 0.05
Iron (Fe)
< 0.01
Manganese (Mn)
< 0.005
Strontium (Sr)
< 0.005
Zinc (Zn)
< 0.005
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper(Cu)
<1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
Sample #: 2015007944
Matrix: GW WW
Analytical Lab
Page 10 of 47
Units
Qualifiers RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
0.05
1
EPA 245.1
03/25/2015 17:58
ACPAYNE
mg/L
0.005
1
EPA 200.7
03/24/2015 12:58
MHALL3
mg/L
0.005
1
EPA 200.7
03/24/2015 12:58
MHALL3
mg/L
0.05
1
EPA 200.7
03/24/2015 12:58
MHALL3
mg/L
0.01
1
EPA 200.7
03/24/2015 12:58
MHALL3
mg/L
0.005
1
EPA 200.7
03/24/2015 12:58
MHALL3
mg/L
0.005
1
EPA 200.7
03/24/2015 12:58
MHALL3
mg/L
0.005
1
EPA 200.7
03/24/2015 12:58
MHALL3
ug/L
1
1
EPA 200.8
04/14/2015 13:57
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:57
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:57
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:57
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:57
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:57
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:57
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:57
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:57
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:57
JAHERMA
ug/L
1
1
EPA 200.8
04/14/2015 13:57
JAHERMA
ug/L
0.2
1
EPA 200.8
04/14/2015 13:57
JAHERMA
ug/L
0.3
1
EPA 200.8
04/14/2015 13:57
JAHERMA
Qualifiers:
M4 The spike recovery value was unusable since the analyte concentration in the sample was disproportionate to
the spike level. The associated Laboratory Control Spike recovery was acceptable.
N1 See additional information listed below.
-- Additional Information --
These sample were stored in a refrigerator that malfunctioned causing the sample to freeze. The state was notified
and the results may be reported for compliance purposes as long as the data is flagged. Any parameter requiring
preservation at < 6C and that was tested after 3/25/2015 at 15:45 when the refrigerator was documented to be in
compliance are flagged with N1. N2 - TSS samples for 2015007942 and 2015007943 were repeated on 3/27/15 due
to a potential lab error. This data is reported past holding time, and should be considered as estimated values.

Analytical Lab
Page 11 of 47
EDement One Inc.
6319-D Carolina Beach Rd.
Wilmington, IBC 28412
Rhone: 910 793-0128
Fax: [phone]
e11ab aLie1 lab
.corm
eDtB�untOne
REPORT OF ANALYSES
Duke Energy March 27, 2015
Laboratory Services Client Project Name AB GW Assessment Water Synterra
13339 Hagers Ferry Road Bld. MG03A Client Project Number J15030544
Huntersville, NC 28078 PO Number
Sample Matrix
GW WW
Date Analyzed
03/25/2015
Delivered by
FedEx
eOne ID
Duke Energy ID
24347-1* ABMW-1S
24347-2* ABMW-1
24347-3 Equipment Blank
Sample Type Grab
Method SM 4500 S2- D
Parameter Result Unit Dil
Date Received
03/25/2015
Time Received
0940
Received by
LLB
DL Date
Time
Sampled
Sampled
Sulfide < 10.0 mg/L 100 0.1 03/19/15 0950
Sulfide < 10.0 mg/L 100 0.1 03/19/15 1109
Sulfide < 0.1 mg/L 1 0.1 03/19/15 1151
*Sample spike recovery outside of QA limits of 85-115%; dilution necessary to meet laboratory QA limits.
``7� ,O� �
Ken Smith, Laboratory Director
c
24347 Duke Report Packet Compiled by)
NC Certifications: DW 37788 and DWQ DENR 604

Analytical Lab
Page 12 of 47
V $
1� �J
c \
r-
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elementOne SAMPLE SUBMISSION FORM
TAT 7 131)
Hold Time Expiration 03.26.15 @ 0950 AM
Client: Duke Energy
LIMS No J15030544
Project ID AB GW Assessment Water - Synterra
Analytical Lab
Page 13 of 47
Lab ID 24347
Analysis Due Date 03.25.15
Report Due Date 04.03.15
Date Rec: 03.25.15
Time Rec: 0940
Rec By I I R
pH >9 (yes No Temn:5 No Ref. Method:
d
If No, Record 1. If No, Record
�SM4500 S2 D
Sam le — Identification & Collection Information
Lab ID Client ID Collection Date Collection Time Analysis Requested
1 ABMW-1S 03.19.15
0950 Am Sulfide
2 ABMW-1 03.19.15
1109 AM Sulfide
3 Equipment Blank 03.19.15 1151 AM Sulfide
NOTE for Sulfide The MS/MSD spike should approximate 2 to 3 times the sample concentration. If no sulfide detected
at 100 pg/L spike the sample to render the final spike concentration at — 500 pg/L

Analytical Lab
Page 14 of 47
METHOD: SM 4500 S2- D ELEMENT ONE
ELEMENT ASSAY: Sulfide Spectrophotometer UNITS OF ANSW
DETECTION LIMI
Wave Length 664 CLIENT: Duke Lab ID# 24347/348/349/350/351 SPK LEVEL uMAX ALIQUOT
Date: 03/25/15 Na2S•9H2O Lot # STANDARD conc
Time Analysis Begun 14:30 40721
Time Analysis Ended 17:25
Analyst: KAM STD ABSORPTIC
ug 5TU
SOLUTION
STD
ABS
0.00
0.000
1.00
0.07
2.50
0.172
5.00
0.351
7.50
0.504
10.00
0.697
Dim
o eoo
wF
D.m
ram
m0
.ml
2m
en
,noo
w
mo
o.
X
=>co ill
0.00 Bm
0m 1200
X
SAMPLE SAMP ug PER ALI in n1L PREP
I.D. ABS ALIQUOT ANALYZED VOL in mL
Sloe 0.06898022
ALI in mL RESULTS
TAKEN u /mL
LRB
0.00
10
10
10
<
LRB SPK
0.367
5.3278
10
10
10
0.533
24347-1
0.007
0.0631
10
10
10
<
24347-1 s k
0.079
1.1160
10
10
10
0.112
24347-2
0.003
0.0046
10
10
10
<
24347-2 dup
0.001
-0.0246
10
10
10
<
24347-2 s k
0.116
1.6571
10
10
10
0.166
24347-3
-0.001
0.0000
10
10
10
< 0.1
24347-3 s k
0.368
5.3424
10
10
10
0.534
24347-1
0.005
0.0339
10
10
2
<
24347-1 s k
0.194
2.7978
10
10
2
1.399
24347-2
0.002
-0.0100
10
10
2
<
24347-2 s k
0.128
1.8326
10
10
2
0.916
24347-1
0.003
0.0046
10
10
1
<
24347-11clup
0
0.0000
10
10
1
<
24347-1 s k
0.236
3.4120
10
10
1
3.412
24347-2
0.005
0.0339
10
10
1
<
24347-2 s k
0.173
2.4907
10
10
1
2.491
24347-1
0.001
-0.0246
10
10
0.5
<
24347-1 s k
24347-2
0.270
0.005
3.9092
0.0339
10
10
10
10
0.5
0.5
7.818
<
24347-2 s k
0.220
3.1780
10
10
0.5
6.356
Blank
0
0.0000
10
10
10
<
QC 0.338 1 4.9037 10
Submitted for Q QC- Date: 3/25/15
10
By: (Print)
10 0.490
KAM
('
% SPK REC
LEVI
107%
5.0
22%
5.0
33% 5.0
107% s n
5.0
37%
6S"7o
5.0
50%
5.0
78%
5.0
64%
5.0
98% 5.0
;iqn):

Analytical Lab
Page 15 of 47
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide Spectrophotometer UNITS OF ANSWER
Wave Length 664 DETECTION LIMIT u
Duke SPK LEVEL u
24347/348/349/350/351 MAX ALIQUOT
03/25/15 Na2S•9H2O Lot # STANDARD conc(ppm)
14:30 40721
17:25
KAM STD ABSORPTION
- --
y - - ---
GeDo
ug/mL
1.000
5
CLIENT:
Lab ID#
10.00
X
Date:
Time Analysis Begun
10
Time Analysis Ended
Analyst:
Y
X
ug STD
SOLUTION
STD o �o
ABS 0500
0.00
1.00
2.50
5.00
7.50
10.00
0.000 o5oo
0.07
I o
ml
0.172
am
-
0.351 0+�
o
1M
0.504 o.00 u
1 0.697
w zoo a oo a o0 eoo Joao 12oo
I x
SAMPLE SAMPY ug PER ALI in mL PREP
I.D. ABS ALIQUOT ANALYZED VOL in mL
Sloe 0.06898022
ALI in mL RESULTS
TAKEN ug/mL
Correlation 0.999628195
LESS THAN SPIKE
% SPK REC LEVEL
LRB
0.00
10
10
10
<
0
LRB SPK
0.367
5.3278
10
10
10
0.533
107%
5.0
24347-1
0.002
-0.0100
10
10
0.1
< 10.0
24347-1 s k
0.322 T
4.6697
10
10
0.1
46.697
93%
5.0
24347-2
0.001
-0.0246
10
10
0.1
< 10.0
24347-2 s k
0.305
4.4211
10
10
0.1
44.211
88%
5.0
24348-1
0.004
0.0192
10
10
10
< 0.1
5.0
24348-1 du
0.001
-0.0246
10
10
10
< 0.1
24348-1 s k
0.314
4.5527
10
10
10
0.455
91 %
24348-2
0.003
0.0046
10
10
10
<
24348-2 s k
0.01
0.1070
10
10
10
<
2%
5.0
24348-3
0.002
-0.0100
10
10
10
<
24348-3 s k
24348-4
0.012
0.01
0.1362
0.1070
10
10
10
10
10
10
<
<
3%
5.0
24348-4 s k
24349-1
0.084
0.01
1.1892
0.1070
10
10
10
10
10
10
0.119
<
24%
5.0
24349-1 du
0.005
0.0339 --i10
10
10
<
24349-1 s k
0.226
3.2658
10
10
10
0.327
65%
5.0
24349-2
0.031
0.4141
10
10
10
<
24349-2 s k
0.218
3.1488
10
10
10
0.315
63%
5.0
24349-3
0.001
-0.0246
10
10
10
<
24349-3S k
0.206
2.9733
10
10
10
0.297
59%
5.0
24349-4
0.002
-0.0100
10
10
10
<
24349-4 s k
Blank
0.178
0
2.5638
0.0000
10
10
10
10
10 0.256
10 <
10 0.496
KAM
51 %
5.0
QC
Submitted r Q Q
0.342
C - Date:
4.9622
3/25/15
10
10
By: (Print)
99%
5.0
(sign):

Analytical Lab
Page 16 of 47
METHOD: SM 4500 S2- D
ELEMENT ASSAY: Sulfide Spectrophotomete
CLIENT: Duke Wave Length 664
Lab ID# 24347/348/349/350/351
Date: 03/25/15 Na2S•91-12O Lot #
Time Analysis Begun 14:30 40721
Time Analysis Ended 17:25
Analyst: KAM
X y
ug STD
STD
SOLUTION
ABS
0.00
0.000
1.00
0.07
2.50
0.172
5.00
0.351
7.50
0.504
ELEMENT ONE
ANDARD
o eoo
0-]00
0,000
0.6.
014.
0,300
.361
0,200
0.100
.Ol
iM
0 000
060
200
1
X
400 ­0 3.00 low 12M
10.00 1 0.697 x
SAMPLE SAMP ug PER ALI M mL PREP
I.D. ABS ALIQUOT ANALYZED VOL in mL
LRB 0.000 0.0000 10 10
No 0.06898022
ALI in mL RESULTS
TAKEN u /mL
10 <
Correlation 0.99962819E
LESS THAN SPIKE
% SPK REC LEVEL
0
LRB SPK
24349-5
0.367
0.001
5.3278
1 -0.0246
10
10
10
10
10
10
0.533
< 0.1
107%
5.0
24349-5 s k
0.330
4.7867
10
10
10
0.479
96%
5.0
24350
0.098
1.3939
10
10
10
0.139
24350 dup
0.075
1.0575
10
10
10
0.106
24350 s k
0.059
0.8236
10
10
10
<
-5%
5.0
24351
0.004
0.0192
10
10
10
<
24351 s k
Blank
0,206
I 0.000
2.9733
1 0.0000
10
10
10
10
10
10
0.297
<
59%
5.0
QC
0.342
4.9622
10
10
10
0.496
99%
5.0
I VNNI//1agwu /Vr wAfwt,- Date:3/25/15 B Print
Y (Print) KAM ��;,.,�.

Analytical Lab
Page 17 of 47
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
ug/mL
DETECTION LIMIT &
2.500
CLIENT:
SPK LEVELL&
5
Lab ID#
Na2S•9H2OLot#
0 06 as � a711
MAX ALIQUOT
25.00-
Date:
I'Lo5o/14351 i
STANDARD conc(ppm)
X
Time Analysis Begun
10
Time Analysis Ended
Analyst:
1!t
Y
ug STD
SOLUTION
STD
ABS
00
r 0.00 -a
.50' 10•
00
1O' 7,0
c�,o©
0,010
t7
d6 504�
©.� 7
V.60D
6.600
,So
a400
0100
0000
W 200 400 600 B00 000 i00
x
SAMPLE SAMP
I.D. ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
s rt
PREP
VOL in mL
Slope #DIV/0'!
Correlation #DIWOI
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
LRB
U,Ur)0
k 10
1
1
<
0
LRB SPK
2,5 10
1
1
<
0%
5.0
'a 1— r
6.0197
t 0
i t3
t o
<
0.076P
I
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f//%pa0/2
<
#VALUE!
(-
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. 5<
#VALUE!
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<
a 5
1
aaa
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—_.—
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#VALUE!
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0, UGj
0.0000
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1
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11
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0%1
5.0
Submitted for QA/QC-
Date: • S< (S
By: (Print)
(sign):
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68
S(> [
PA. (

Analytical Lab
Page 18 of 47
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
u /mL
DETECTION LIMu
ITSPK
2.500
CLIENT:
LEVEL u
5
Lab ID#
MAX ALIQUOT 25.00
Na2S•9H2OLot# STANDARD conc(ppm) X
N13 7. \ 10
1 00 ti G `(0 , �`
^ I STD ABSORPTION Y
Y
12M
Date:
Time Analysis Begun
Time Analysis Ended
Analyst:
X
ug STD
SOLUTION
STD
000
ABS
—�
.00
5. l] a.5
7. 5�.
10.00 ie
t0
10&r,
0.171
o2w
0,3/St
0000W
—
--
�W/[
06
0.6 q,7
200 4,00 6w e00 10m 12W
x
SAMPLE
I.D.
SAMP ug PER ALI in mL7VOLin
ABS ALIQUOT ANALYZED
Slope #DIV/0!
Correlation #DIV/O!
ALI in mL
TAKEN
RESULTS
u /mL
LESS THAN
% SPK REC
SPIKE
LEVEL
LRB
L),UU
10
10
<
0
LRB SPK
t 0
10
<
0%
5.0
)V - (
O,oO�-
(0
t 0
<
0,32
f
S�d
o, G 1
(
<
#VALUE!
S h
L7,3q5
.1
<
0 . 00
<
— i
,06 C
<
#VALUE!
1
<
(2,01 d1
<
#VALUE!
<
o- 010
<
#VALUE!
—1-! 5PA
0 0
<
a L(3 Ltd0.00
<
1
.Odd
<
#VALUE!
<
<
<
#VALUE!
i'<
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<
<
#VALUE!
Blank
0.0000
1 25
1
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l0,3qzl
1 25
1
1
<
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5.0
Submitted for QA/QC-
Date: a S LS
By: (Print)
(sign):
I LI 3 L(8 - ),
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Analytical Lab
Page 19 of 47
METHOD:
SM 4500'S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
ug/mL
DETECTION LIMIT u
2.500.
CLIENT:
v
SPK LEVEL_LuM
5
Lab ID#
Na2S•9H2OLot#
00000 ` j��a` i
MAX ALIQUOT
25.00
Date:
Y Wasp aLt351
STANDARD conc(ppm)
X
Time Analysis Begun
I k
10
Time Analysis Ended
Pfl- t X1'#— 4
Analyst:
STD ABSORPTION
Y
X
Y
z�
ug STD
SOLUTION
STD
ABS
a�
j 00
` 50 1
5. 0
7. I>tpL
10. -1 %5
100
CJ d f1
,17j�
�/8t43}7�,.1y(
o m 1
C116aj
Q�
0�
0,200
-
� W
O.00 200 .00 600 8.00 low,200
,
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SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
Project Name: AB GW Assessment Water - HF Lee
Project Number:J15030544
Lot Number:QC23045
Date Completed:03/31/2015
Grant Wilton
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
* QC23045*
Shealy Environmental Services, Inc. Page: 1 of 10
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SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Duke Energy
Lot Number: QC23045
Project Name: AB GW Assessment Water - HF Lee
Project Number: J15030544
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 10
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QC23045
Project Name: AB GW Assessment Water - HF Lee
Project Number: J15030544
Sample Number Sample ID Matrix Date Sampled Date Received
001 2015007941 Aqueous 03/19/2015 0950 03/23/2015
002 2015007942 Aqueous 03/19/20151109 03/23/2015
003 2015007943
(3 samples)
Aqueous 03/19/20151151 03/23/2015
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SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QC23045
Project Name: AB GW Assessment Water - HF Lee
Project Number: J15030544
Sample Sample ID
Matrix Parameter Method
Result Q
Units
Page
001
2015007941
Aqueous Alkalinity SM 2320B-
340
mg/L
5
001
2015007941
Aqueous Bicarbonate Alkalinity SM 2320B-
340
mg/L
5
001
2015007941
Aqueous Methane RSK - 175
790
ug/L
6
002
2015007942
Aqueous Alkalinity SM 2320B-
490
mg/L
7
002
2015007942
Aqueous Bicarbonate Alkalinity SM 2320B-
490
mg/L
7
002
2015007942
Aqueous Methane RSK - 175
670
ug/L
8
003
2015007943
Aqueous Methane RSK - 175
10
ug/L
10
(7 detections)
Shealy Environmental Services, Inc. Page: 4 of 10
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QC23045-001
Description: 2015007941 Matrix: Aqueous
Date Sampled:03/19/2015 0950 Project Name: AB GW Assessment Water -
Date Received:03/23/2015 Project Number: J15030544
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 03/27/2015 1838
HMA 71143
1
(Bicarbonate ) SM 2320B-2011
1 03/27/2015 1838
BWS 03/27/2015 1838
1
(Carbonate Al) SM 2320B-2011
1 03/27/2015 1838
BWS 03/27/2015 1838
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
340
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
340
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 10
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Methane
Client: Duke Energy Laboratory ID: QC23045-001
Description: 2015007941 Matrix: Aqueous
Date Sampled:03/19/2015 0950 Project Name: AB GW Assessment Water -
Date Received:03/23/2015 Project Number: J15030544
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 RSK - 175 2 03/24/2015 2030 DCS 70960
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 790 20 ug/L 2
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 10
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QC23045-002
Description: 2015007942 Matrix: Aqueous
Date Sampled:03/19/2015 1109 Project Name: AB GW Assessment Water -
Date Received:03/23/2015 Project Number: J15030544
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 03/30/2015 1712
BWS 71282
1
(Bicarbonate ) SM 2320B-2011
1 03/30/2015 1712
BWS 03/30/2015 1712
1
(Carbonate Al) SM 2320B-2011
1 03/30/2015 1712
BWS 03/30/2015 1712
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
490
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
490
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 10
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Methane
Client: Duke Energy Laboratory ID: QC23045-002
Description: 2015007942 Matrix: Aqueous
Date Sampled:03/19/2015 1109 Project Name: AB GW Assessment Water -
Date Received:03/23/2015 Project Number: J15030544
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 RSK - 175 2 03/27/2015 1710 DCS 71295
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 670 20 ug/L 2
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 8 of 10
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QC23045-003
Description: 2015007943 Matrix: Aqueous
Date Sampled:03/19/2015 1151 Project Name: AB GW Assessment Water -
Date Received:03/23/2015 Project Number: J15030544
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 03/30/2015 1717
BWS 71282
1
(Bicarbonate ) SM 2320B-2011
1 03/30/2015 1717
BWS 03/30/2015 1717
1
(Carbonate Al) SM 2320B-2011
1 03/30/2015 1717
BWS 03/30/2015 1717
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 of 10
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Methane
Client: Duke Energy Laboratory ID: QC23045-003
Description: 2015007943 Matrix: Aqueous
Date Sampled:03/19/2015 1151 Project Name: AB GW Assessment Water -
Date Received:03/23/2015 Project Number: J15030544
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 03/27/2015 1656 DCS 71148
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 10 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 10 of 10
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QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: QC23045
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - Ii
Sample ID: QQ71143-001 Matrix: Aqueous
Batch: 71143
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 03/27/20151656
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC23045
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - LCS
Sample ID: QQ71143-002 Matrix: Aqueous
Batch: 71143
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 99 1 99 90-110 03/27/20151703
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC23045
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - Ii
Sample ID: QQ71282-001 Matrix: Aqueous
Batch: 71282
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 03/30/20151508
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC23045
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - LCS
Sample ID: QQ71282-002 Matrix: Aqueous
Batch: 71282
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 95 1 95 90-110 03/30/20151514
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC23045
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ70960-001 Matrix: Aqueous
Batch:70960
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 03/24/20151843
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC23045
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ70960-002 Matrix: Aqueous
Batch:70960
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 50 40 1 79 70-130 03/24/20151758
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC23045
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ70960-003 Matrix: Aqueous
Batch:70960
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 50 36 1 72 10 70-130 30 03/24/20151817
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC23045
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ71148-001 Matrix: Aqueous
Batch: 71148
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 03/27/20151407
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC23045
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ71148-002 Matrix: Aqueous
Batch: 71148
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 150 1 99 70-130 03/27/20151342
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC23045
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ71148-003 Matrix: Aqueous
Batch: 71148
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 190 1 128 26 70-130 30 03/27/20151355
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC23045
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ71295-001 Matrix: Aqueous
Batch: 71295
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 03/27/20151407
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC23045
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ71295-002 Matrix: Aqueous
Batch: 71295
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 150 1 99 70-130 03/27/20151342
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC23045
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ71295-003 Matrix: Aqueous
Batch: 71295
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 190 1 128 26 70-130 30 03/27/20151355
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC23045
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

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Lhxumi�u[ Numlwr VAa•016
Roxision AlurAnrr. 16
Face I of]
RCFIBCCs. LALe M15n4
Eftev-dvc: DW: 11/07114
Sample Receipt Checklist (SRC)
Client: U ve, ii r '+. C;oolcr inapectecl by/date- atjO /� 5Lnt 9; -2,3 —
Means of receipt- rsT ❑ CLient 0 LT ❑ FedEx [] .Airb=e Fxp 5ffier
"Yes ❑ I Nc 1. WM eurtody seals preRent on -the oa,oler?
Yes LI I No NA 2r L2. If custody seals w Wit, were the intact and unbroken?
Cooler ID/Original teinperat= upon reccipVDeri%red (enrected) tempe1-4ture upon receipt.
l .0 J 2 aC f 44 aC } } QD { I OC
Method.. ❑ Temperqturu Bl Against Bottles IR G-an ID_ 44 IRGun Cerrection Factor. 0.°C
Method e•fc;oolsnt; ct10C ❑ Btue lee n D,v fee n None.
Yas ❑
No ❑
NA
3. rftemperaturc. of any coolu excecded 6_0'C, was PMicct Manager noticed?
PM nolircd by SRC, phorie, note (circle one), ocbcr; ---.
(For 000lers rcccivcd via oo nmercia,l Courier, pMs art tc'P ba notified
intmediatel .
Yes ❑
No
NA ❑
4, is Iha commercial courier's packing. slip attached to this f&m'?
Yes
'D
S. Were rp ercustod e procedures(re lin ui shedIrmei ved) followod?
Yes
a
RTA E]
5a Were qwnpks relin uished by chizit to nommerei al eouricO
Yces
Nc, ❑
6. Wcre sample 10s listed on the CCtC"
o ❑
7. Wcrc sample IDs listed on all sample c9nuillers?
o ❑
S. Was collection d & time listed cart the COCv?
I
o
9. Was corll t:ic is date & time listed on all S5 M le containers?
o Q
10. Dtdall cotudner label information T.D 1�1°- Iv. Ii nc a with the C DC?
+ o it
11 - Were tests to k!e Lbnned listed on the CIOC?
YtS
o ❑
12. Did all samples arrive W (be er unntainr rs for each test's
Yes
o
13, Did all cvntainc:rs arrive in good oondition unbroken, lids on, ete. ?
'Yes
lorry ❑
14. Was adequate saMplo volume avaAable?
Yes ❑
No
15. Were 01 samples received within % the holding time or 48 .hours, wrhichcvcr
Comes tint?
16- Were ary samples containers missing?
Yes L] No
Yes ❑
NO
IT Were there any excess samples ncrt listed om COG?
18, WIC bubbles prcwmt : ' a S1Ze" 'f,"OY btitrrl in $iam to in any VOA vials'
YrN ❑ Na TEA ❑
Yes ❑
No ❑
NA
19, Wem rill me(alh C)&GyUFMjnutrietn sample~s i ccci4 eil at a H of �2`?
Yes ❑
No ❑
NA
20. Were all c snide 9rWor sulfide sarfi les received at a pH >127
Y'es ❑
No ❑
NAWf
2 1 - Were all applicable NHI7I Nii2yanirlclphcnol (-QO.2mgIL) samples &w o
residual chlarinc?
Yes i❑I
No ©
NA
2. Were Wilectio�n Tern eratures documented on Or, C for NC: sam trs?
Yes ❑
No ❑
,4
23. Were cheat remarlcsdregquests (i.e. rcqucstcd dilution£, M.W- d] 4ie-si rions,
etc- I c+orrectl uansf nbed from the COC' into the oamanent section in l.ljvT!P
Yes Cl
NO 23 1
124.
Was the quote number used taken from the container label?
Ssrnale Preservatiu■ fkfus
bu cornolctcd for arty samnlef0 ithenrrer.Ily r«re-.srrvM nr with hemd- nrr 1
l �arrnnlp,fcl vvara ra,�aivari i.-�r�:3n���=r1,: r,.,r•��dr.k.l ,.1 ,.....v .,.,1..,.,a..a

CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM
-- --------------------- ---------------- - ------
Dulte En" ATmly*W Laborejory
Duko Erkomy
- --------------------------- -------------------------------------------
i j ArlmlyUclal Lumbers ilea avily-_
Analytical Laboratory rAp, C�A. wcltvl� fflwldl�q mAI
IIJ39 K.". F—V Rd
!Order# Matrix GW-WW
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rx
sc.—
Chain ol Custody ZL "UrdwrAlt. N. C. 28078
SonVdc Log MQ676452idmr
-ri
'�:- III
L
SAMPLE PlWdRM
- -----------------------
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GMUnd VftW
WOES—
RrmkirNrprA8 GW Asseasllmll Water 'Ph�dk�
rm
!VftKlr
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Eldn" Wq1mr
Ln7
RCRA Wamic
PO 1142 133 I—"&Dn (0." um)
Unfiltered
Business Unrt; Pe—: R'P.c6rd.'Tq;
'MRA
P
lee
I-allumip (MLI 2WO
SHEALY
i-sIc
4 1 MH3
too 500
AmIlmar Type.' PET
PO 1142089
glass PET
Per PEI PET
samplIG ription or I D
19
w
----------
E
(2PS Locafion
"I-ndll
Dal* I Time 619M&Wre
g a wl
0
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Pall'! i of I
DISTRIBU-FPUiN
ORIGINAL to J'-:' {fir i,y w ci r N I
COO REV DATE 1r'22J2015
Soo 290
ME
Em
Rsy. 3L4110TIM? By:
- 4f
7—
Requested Tui-natuand
-a—womme CIO ptid BY: Owt mig
Ca
'9
14 rin ys
"V-11mished By flne
DaterriAweWd By- vmwn'llme
A
Q. 2
'10-ILew i;�-ca
E
c m
7 Duy!L
By Unwilm SesladA-bek CPp*ncd Sy
'4B l-If
ELEMENTS by ICP - MS (TR M): As, Be. Cd, Go, Cr. Cu. Mo. 5 b. Se, TI (LL), V (I-L)
UEMENTS by ICP (TPZJA): Al. 13a, 8, Fe, Mn, Sr, Zn ICIP-1.1ndloastod Ca, Mg. K, Na Hg by 245.1
49
'Oth(" ASAF
all metals iCP.JmS,H5j
Add. Qoal V-1111 Apply