NC0003417_J15060348report_20150805

DUE Analytical Laboratory
ENERGY
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
Order Number: J15060348
Project Name: HF LEE PLANT - AB GW ASSESSMENT SURFACE
Customer Name(s): Tim Hunsucker, Judd Mahan, Kathy Webb, John Toepfer
Customer Address: 1677 Old Smithfield Rd
Goldsboro NC 27530,
Lab Contact: RA—, Ann r)M. Mary Ann Og1ePhone: 980-875-5274
`(._ 2015.06.26
Report Authorized By: 16:37:03-0400, Date:
(Signature)
Mary Ann Ogle
Program Comments:
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
6/26/2015
Analytical Lab
Page 1 of 54
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Collection
Sample ID Plant/Station Date and Time
2015018398
2015018399
2015018400
2015018401
2015018402
2015018403
2015018404
7 Total Samples
Collected By
Sample Description
HF LEE PLANT
10-Jun-15 10:55 AM
ILLEGIBLE
S-16
HF LEE PLANT
10-Jun-15 11:40 AM
ILLEGIBLE
S-10
HF LEE PLANT
10-Jun-15 11:50 AM
ILLEGIBLE
S-10 Dup
HF LEE PLANT
10-Jun-15 12:40 PM
ILLEGIBLE
ASW-NR1
HF LEE PLANT
10-Jun-15 5:34 PM
ILLEGIBLE
Filter Blank
HF LEE PLANT
10-Jun-15 5:40 PM
ILLEGIBLE
Field Blank
HF LEE PLANT
10-Jun-15 5:34 PM
ILLEGIBLE
Trip Blank
Analytical Lab
Page 2 of 54

Analytical Lab
Page 3 of 54
Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals 0 Yes ❑ No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes 0 No
All laboratory QA/QC requirements are acceptable. 0 Yes ❑ No
Report Sections Included:
E%-'] Job Summary Report
❑� Sample Identification
Technical Validation of Data Package
❑� Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
❑d Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
❑� Chain of Custody
❑� Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Mary Ann Ogle Date: 6/26/2015

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060348
Site: S-16
Collection Date: 10-Jun-15 10:55 AM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.650
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
21
mg/L
1
Sulfate
15
mg/L
1
MERCURY IN WATER - (Analysis Performed by
Prism Labs)
Vendor Parameter
Complete
DISSOLVED METALS BY ICP
Aluminum (AI)
0.133
mg/L
0.005
Barium (Ba)
0.027
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.483
mg/L
0.01
Manganese (Mn)
0.064
mg/L
0.005
Strontium (Sr)
0.064
mg/L
0.005
Zinc (Zn)
0.008
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
7.86
mg/L
0.01
Magnesium (Mg)
3.23
mg/L
0.005
Potassium (K)
4.58
mg/L
0.1
Sodium (Na)
20.7
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.545
mg/L
0.005
Barium (Ba)
0.032
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
1.25
mg/L
0.01
Manganese (Mn)
0.106
mg/L
0.005
Strontium (Sr)
0.063
mg/L
0.005
Zinc (Zn)
0.006
mg/L
0.005
Sample #: 2015018398
Matrix: GW WW
Analytical Lab
Page 4 of 54
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2 06/17/2015 12:23 LSTARLI
10 EPA 300.0 06/12/2015 12:45 BGN9034
10 EPA 300.0 06/12/2015 12:45 BGN9034
Vendor Method V_PRISM
1 EPA 200.7
06/12/2015 10:55
MHALL3
1 EPA 200.7
06/12/2015 10:55
MHALL3
1 EPA 200.7
06/12/2015 10:55
MHALL3
1 EPA 200.7
06/12/2015 10:55
MHALL3
1 EPA 200.7
06/12/2015 10:55
MHALL3
1 EPA 200.7
06/12/2015 10:55
MHALL3
1 EPA 200.7
06/12/2015 10:55
MHALL3
1 EPA 200.7
06/13/2015 13:53
MHALL3
1 EPA 200.7
06/13/2015 13:53
MHALL3
1 EPA 200.7
06/13/2015 13:53
MHALL3
1 EPA 200.7
06/13/2015 13:53
MHALL3
1 EPA 200.7
06/17/2015 10:21
MHH7131
1 EPA 200.7
06/17/2015 10:21
MHH7131
1 EPA 200.7
06/17/2015 10:21
MHH7131
1 EPA 200.7
06/17/2015 10:21
MHH7131
1 EPA 200.7
06/17/2015 10:21
MHH7131
1 EPA 200.7
06/17/2015 10:21
MHH7131
1 EPA 200.7
06/17/2015 10:21
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060348
Site: S-16
Collection Date: 10-Jun-15 10:55 AM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
1.07
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
1.20
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
1.31
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
1.10
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
2.02
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
110
mg/L
25
Total Carbon
TOC
5.5
mg/L
0.2
TOTAL SUSPENDED SOLIDS
TSS
18
mg/L
5
Sample #: 2015018398
Matrix: GW WW
Analytical Lab
Page 5 of 54
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/22/2015 23:33
SLS2560
1
EPA 200.8
06/22/2015 23:33
SLS2560
1
EPA 200.8
06/22/2015 23:33
SLS2560
1
EPA 200.8
06/22/2015 23:33
SLS2560
1
EPA 200.8
06/22/2015 23:33
SLS2560
1
EPA 200.8
06/22/2015 23:33
SLS2560
1
EPA 200.8
06/22/2015 23:33
SLS2560
1
EPA 200.8
06/22/2015 23:33
SLS2560
1
EPA 200.8
06/22/2015 23:33
SLS2560
1
EPA 200.8
06/22/2015 23:33
SLS2560
1
EPA 200.8
06/22/2015 23:33
SLS2560
1
EPA 200.8
06/22/2015 23:33
SLS2560
1
EPA 200.8
06/22/2015 23:33
SLS2560
1
EPA 200.8
06/21/2015 13:43
SLS2560
1
EPA 200.8
06/21/2015 13:43
SLS2560
1
EPA 200.8
06/21/2015 13:43
SLS2560
1
EPA 200.8
06/21/2015 13:43
SLS2560
1
EPA 200.8
06/21/2015 13:43
SLS2560
1
EPA 200.8
06/21/2015 13:43
SLS2560
1
EPA 200.8
06/21/2015 13:43
SLS2560
1
EPA 200.8
06/21/2015 13:43
SLS2560
1
EPA 200.8
06/21/2015 13:43
SLS2560
1
EPA 200.8
06/21/2015 13:43
SLS2560
1
EPA 200.8
06/21/2015 13:43
SLS2560
1
EPA 200.8
06/21/2015 13:43
SLS2560
1
EPA 200.8
06/21/2015 13:43
SLS2560
Vendor Method
V_SHEALY
Vendor Method V_ELE1
1 SM2540C 06/15/201514:29 AGIBBS5
2 SM5310C/EPA9060A 06/22/201515:17 GHUTCHI
1 SM2540D 06/12/2015 09:12 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060348
Site: S-10
Collection Date: 10-Jun-15 11:40 AM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.550
mg-N/L M2
0.01
INORGANIC IONS BY IC
Chloride
21
mg/L
1
Sulfate
14
mg/L
1
MERCURY IN WATER - (Analysis Performed by
Prism Labs)
Vendor Parameter
Complete
DISSOLVED METALS BY ICP
Aluminum (AI)
0.184
mg/L
0.005
Barium (Ba)
0.028
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.571
mg/L
0.01
Manganese (Mn)
0.074
mg/L
0.005
Strontium (Sr)
0.064
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
7.84
mg/L
0.01
Magnesium (Mg)
3.23
mg/L
0.005
Potassium (K)
4.57
mg/L
0.1
Sodium (Na)
20.4
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.546
mg/L
0.005
Barium (Ba)
0.031
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
1.21
mg/L
0.01
Manganese (Mn)
0.102
mg/L
0.005
Strontium (Sr)
0.062
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015018399
Matrix: GW WW
Analytical Lab
Page 6 of 54
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2 06/17/2015 13:37 LSTARLI
10 EPA 300.0 06/12/2015 13:02 BGN9034
10 EPA 300.0 06/12/2015 13:02 BGN9034
Vendor Method V_PRISM
1 EPA 200.7
06/12/2015 10:59
MHALL3
1 EPA 200.7
06/12/2015 10:59
MHALL3
1 EPA 200.7
06/12/2015 10:59
MHALL3
1 EPA 200.7
06/12/2015 10:59
MHALL3
1 EPA 200.7
06/12/2015 10:59
MHALL3
1 EPA 200.7
06/12/2015 10:59
MHALL3
1 EPA 200.7
06/12/2015 10:59
MHALL3
1 EPA 200.7
06/13/2015 13:57
MHALL3
1 EPA 200.7
06/13/2015 13:57
MHALL3
1 EPA 200.7
06/13/2015 13:57
MHALL3
1 EPA 200.7
06/13/2015 13:57
MHALL3
1 EPA 200.7
06/17/2015 10:34
MHH7131
1 EPA 200.7
06/17/2015 10:34
MHH7131
1 EPA 200.7
06/17/2015 10:34
MHH7131
1 EPA 200.7
06/17/2015 10:34
MHH7131
1 EPA 200.7
06/17/2015 10:34
MHH7131
1 EPA 200.7
06/17/2015 10:34
MHH7131
1 EPA 200.7
06/17/2015 10:34
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060348
Site: S-10
Collection Date: 10-Jun-15 11:40 AM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
1.23
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
1.43
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
1.50
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
1.88
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
110
mg/L
25
Total Carbon
TOC
5.5
mg/L
0.2
TOTAL SUSPENDED SOLIDS
TSS
15
mg/L
5
Sample #: 2015018399
Matrix: GW WW
Analytical Lab
Page 7 of 54
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/22/2015 23:11
SLS2560
1
EPA 200.8
06/22/2015 23:11
SLS2560
1
EPA 200.8
06/22/2015 23:11
SLS2560
1
EPA 200.8
06/22/2015 23:11
SLS2560
1
EPA 200.8
06/22/2015 23:11
SLS2560
1
EPA 200.8
06/22/2015 23:11
SLS2560
1
EPA 200.8
06/22/2015 23:11
SLS2560
1
EPA 200.8
06/22/2015 23:11
SLS2560
1
EPA 200.8
06/22/2015 23:11
SLS2560
1
EPA 200.8
06/22/2015 23:11
SLS2560
1
EPA 200.8
06/22/2015 23:11
SLS2560
1
EPA 200.8
06/22/2015 23:11
SLS2560
1
EPA 200.8
06/22/2015 23:11
SLS2560
1
EPA 200.8
06/21/2015 13:21
SLS2560
1
EPA 200.8
06/21/2015 13:21
SLS2560
1
EPA 200.8
06/21/2015 13:21
SLS2560
1
EPA 200.8
06/21/2015 13:21
SLS2560
1
EPA 200.8
06/21/2015 13:21
SLS2560
1
EPA 200.8
06/21/2015 13:21
SLS2560
1
EPA 200.8
06/21/2015 13:21
SLS2560
1
EPA 200.8
06/21/2015 13:21
SLS2560
1
EPA 200.8
06/21/2015 13:21
SLS2560
1
EPA 200.8
06/21/2015 13:21
SLS2560
1
EPA 200.8
06/21/2015 13:21
SLS2560
1
EPA 200.8
06/21/2015 13:21
SLS2560
1
EPA 200.8
06/21/2015 13:21
SLS2560
Vendor Method
V_SHEALY
Vendor Method V_ELE1
1 SM2540C 06/15/201514:29 AGIBBS5
2 SM5310C/EPA9060A 06/22/201515:17 GHUTCHI
1 SM2540D 06/12/2015 09:12 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060348
Site: S-10 Dup
Collection Date: 10-Jun-15 11:50 AM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.522
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
20
mg/L
1
Sulfate
14
mg/L
1
MERCURY IN WATER - (Analysis Performed by
Prism Labs)
Vendor Parameter
Complete
DISSOLVED METALS BY ICP
Aluminum (AI)
0.186
mg/L
0.005
Barium (Ba)
0.028
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.585
mg/L
0.01
Manganese (Mn)
0.070
mg/L
0.005
Strontium (Sr)
0.063
mg/L
0.005
Zinc (Zn)
0.005
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
7.84
mg/L
0.01
Magnesium (Mg)
3.23
mg/L
0.005
Potassium (K)
4.60
mg/L
0.1
Sodium (Na)
20.5
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.515
mg/L
0.005
Barium (Ba)
0.031
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
1.16
mg/L
0.01
Manganese (Mn)
0.099
mg/L
0.005
Strontium (Sr)
0.061
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015018400
Matrix: GW WW
Analytical Lab
Page 8 of 54
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2 06/17/2015 13:38 LSTARLI
10 EPA 300.0 06/12/2015 13:18 BGN9034
10 EPA 300.0 06/12/2015 13:18 BGN9034
Vendor Method V_PRISM
1 EPA 200.7
06/12/2015 11:03
MHALL3
1 EPA 200.7
06/12/2015 11:03
MHALL3
1 EPA 200.7
06/12/2015 11:03
MHALL3
1 EPA 200.7
06/12/2015 11:03
MHALL3
1 EPA 200.7
06/12/2015 11:03
MHALL3
1 EPA 200.7
06/12/2015 11:03
MHALL3
1 EPA 200.7
06/12/2015 11:03
MHALL3
1 EPA 200.7
06/13/2015 14:00
MHALL3
1 EPA 200.7
06/13/2015 14:00
MHALL3
1 EPA 200.7
06/13/2015 14:00
MHALL3
1 EPA 200.7
06/13/2015 14:00
MHALL3
1 EPA 200.7
06/17/2015 10:38
MHH7131
1 EPA 200.7
06/17/2015 10:38
MHH7131
1 EPA 200.7
06/17/2015 10:38
MHH7131
1 EPA 200.7
06/17/2015 10:38
MHH7131
1 EPA 200.7
06/17/2015 10:38
MHH7131
1 EPA 200.7
06/17/2015 10:38
MHH7131
1 EPA 200.7
06/17/2015 10:38
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060348
Site: S-10 Dup
Collection Date: 10-Jun-15 11:50 AM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
1.15
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
1.42
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
1.35
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
1.77
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
110
mg/L
25
Total Carbon
TOC
5.6
mg/L
0.2
TOTAL SUSPENDED SOLIDS
TSS
13
mg/L
5
Sample #: 2015018400
Matrix: GW WW
Analytical Lab
Page 9 of 54
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/22/2015 23:40
SLS2560
1
EPA 200.8
06/22/2015 23:40
SLS2560
1
EPA 200.8
06/22/2015 23:40
SLS2560
1
EPA 200.8
06/22/2015 23:40
SLS2560
1
EPA 200.8
06/22/2015 23:40
SLS2560
1
EPA 200.8
06/22/2015 23:40
SLS2560
1
EPA 200.8
06/22/2015 23:40
SLS2560
1
EPA 200.8
06/22/2015 23:40
SLS2560
1
EPA 200.8
06/22/2015 23:40
SLS2560
1
EPA 200.8
06/22/2015 23:40
SLS2560
1
EPA 200.8
06/22/2015 23:40
SLS2560
1
EPA 200.8
06/22/2015 23:40
SLS2560
1
EPA 200.8
06/22/2015 23:40
SLS2560
1
EPA 200.8
06/21/2015 13:50
SLS2560
1
EPA 200.8
06/21/2015 13:50
SLS2560
1
EPA 200.8
06/21/2015 13:50
SLS2560
1
EPA 200.8
06/21/2015 13:50
SLS2560
1
EPA 200.8
06/21/2015 13:50
SLS2560
1
EPA 200.8
06/21/2015 13:50
SLS2560
1
EPA 200.8
06/21/2015 13:50
SLS2560
1
EPA 200.8
06/21/2015 13:50
SLS2560
1
EPA 200.8
06/21/2015 13:50
SLS2560
1
EPA 200.8
06/21/2015 13:50
SLS2560
1
EPA 200.8
06/21/2015 13:50
SLS2560
1
EPA 200.8
06/21/2015 13:50
SLS2560
1
EPA 200.8
06/21/2015 13:50
SLS2560
Vendor Method
V_SHEALY
Vendor Method V_ELE1
1 SM2540C 06/15/201514:29 AGIBBS5
2 SM5310C/EPA9060A 06/22/201515:17 GHUTCHI
1 SM2540D 06/12/2015 09:12 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060348
Site: ASW-NR1
Collection Date: 10-Jun-15 12:40 PM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.524
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
21
mg/L
1
Sulfate
15
mg/L
1
MERCURY IN WATER - (Analysis Performed by
Prism Labs)
Vendor Parameter
Complete
DISSOLVED METALS BY ICP
Aluminum (AI)
0.201
mg/L
0.005
Barium (Ba)
0.029
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.633
mg/L
0.01
Manganese (Mn)
0.135
mg/L
0.005
Strontium (Sr)
0.073
mg/L
0.005
Zinc (Zn)
0.016
mg/L
0.005
UNDIGESTED METALS BY lCP
Calcium (Ca)
8.14
mg/L
0.01
Magnesium (Mg)
3.23
mg/L
0.005
Potassium (K)
4.58
mg/L
0.1
Sodium (Na)
20.6
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.464
mg/L
0.005
Barium (Ba)
0.031
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
1.18
mg/L
0.01
Manganese (Mn)
0.126
mg/L
0.005
Strontium (Sr)
0.070
mg/L
0.005
Zinc (Zn)
0.052
mg/L
0.005
Sample #: 2015018401
Matrix: GW WW
Analytical Lab
Page 10 of 54
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2 06/17/2015 13:39 LSTARLI
10 EPA 300.0 06/12/2015 13:35 BGN9034
10 EPA 300.0 06/12/2015 13:35 BGN9034
Vendor Method V_PRISM
1 EPA 200.7
06/12/2015 11:07
MHALL3
1 EPA 200.7
06/12/2015 11:07
MHALL3
1 EPA 200.7
06/12/2015 11:07
MHALL3
1 EPA 200.7
06/12/2015 11:07
MHALL3
1 EPA 200.7
06/12/2015 11:07
MHALL3
1 EPA 200.7
06/12/2015 11:07
MHALL3
1 EPA 200.7
06/12/2015 11:07
MHALL3
1 EPA 200.7
06/13/2015 14:04
MHALL3
1 EPA 200.7
06/13/2015 14:04
MHALL3
1 EPA 200.7
06/13/2015 14:04
MHALL3
1 EPA 200.7
06/13/2015 14:04
MHALL3
1 EPA 200.7
06/17/2015 10:42
MHH7131
1 EPA 200.7
06/17/2015 10:42
MHH7131
1 EPA 200.7
06/17/2015 10:42
MHH7131
1 EPA 200.7
06/17/2015 10:42
MHH7131
1 EPA 200.7
06/17/2015 10:42
MHH7131
1 EPA 200.7
06/17/2015 10:42
MHH7131
1 EPA 200.7
06/17/2015 10:42
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060348
Site: ASW-NR1
Collection Date: 10-Jun-15 12:40 PM
Analyte Result Units Qualifiers RDL
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
1.18
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
1.01
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
1.57
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
1.03
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
1.34
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
1.04
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
2.23
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
110
mg/L
25
Total Carbon
TOC
5.5
mg/L
0.2
TOTAL SUSPENDED SOLIDS
TSS
13
mg/L
5
Sample #: 2015018401
Matrix: GW WW
Analytical Lab
Page 11 of 54
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/22/2015 23:47
SLS2560
1
EPA 200.8
06/22/2015 23:47
SLS2560
1
EPA 200.8
06/22/2015 23:47
SLS2560
1
EPA 200.8
06/22/2015 23:47
SLS2560
1
EPA 200.8
06/22/2015 23:47
SLS2560
1
EPA 200.8
06/22/2015 23:47
SLS2560
1
EPA 200.8
06/22/2015 23:47
SLS2560
1
EPA 200.8
06/22/2015 23:47
SLS2560
1
EPA 200.8
06/22/2015 23:47
SLS2560
1
EPA 200.8
06/22/2015 23:47
SLS2560
1
EPA 200.8
06/22/2015 23:47
SLS2560
1
EPA 200.8
06/22/2015 23:47
SLS2560
1
EPA 200.8
06/22/2015 23:47
SLS2560
1
EPA 200.8
06/21/2015 13:58
SLS2560
1
EPA 200.8
06/21/2015 13:58
SLS2560
1
EPA 200.8
06/21/2015 13:58
SLS2560
1
EPA 200.8
06/21/2015 13:58
SLS2560
1
EPA 200.8
06/21/2015 13:58
SLS2560
1
EPA 200.8
06/21/2015 13:58
SLS2560
1
EPA 200.8
06/21/2015 13:58
SLS2560
1
EPA 200.8
06/21/2015 13:58
SLS2560
1
EPA 200.8
06/21/2015 13:58
SLS2560
1
EPA 200.8
06/21/2015 13:58
SLS2560
1
EPA 200.8
06/21/2015 13:58
SLS2560
1
EPA 200.8
06/21/2015 13:58
SLS2560
1
EPA 200.8
06/21/2015 13:58
SLS2560
Vendor Method
V_SHEALY
Vendor Method V_ELE1
1 SM2540C 06/15/201514:29 AGIBBS5
2 SM5310C/EPA9060A 06/22/201515:17 GHUTCHI
1 SM2540D 06/12/2015 09:12 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060348
Site: Filter Blank
Collection Date: 10-Jun-15 5:34 PM
Analyte Result Units Qualifiers RDL DF
DISSOLVED METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
Barium (Ba)
< 0.005
mg/L
Boron (B)
< 0.05
mg/L
Iron (Fe)
< 0.01
mg/L
Manganese (Mn)
< 0.005
mg/L
Strontium (Sr)
< 0.005
mg/L
Zinc (Zn)
< 0.005
mg/L
TOTAL RECOVERABLE METALS
BY ICP-MS (DISSOLVED)
Antimony (Sb)
< 1
ug/L
Arsenic (As)
< 1
ug/L
Beryllium (Be)
< 1
ug/L
Cadmium (Cd)
< 1
ug/L
Chromium (Cr)
< 1
ug/L
Cobalt (Co)
< 1
ug/L
Copper (Cu)
< 1
ug/L
Lead (Pb)
< 1
ug/L
Molybdenum (Mo)
< 1
ug/L
Nickel (Ni)
< 1
ug/L
Selenium (Se)
< 1
ug/L
Thallium (TI) Low Level
< 0.2
ug/L
Vanadium (V) Low Level
< 0.3
ug/L
Sample #: 2015018402
Matrix: GW WW
Analytical Lab
Page 12 of 54
Method Analysis Date/Time Analyst
0.005
1
EPA 200.7
06/12/2015 11:11
MHALL3
0.005
1
EPA 200.7
06/12/2015 11:11
MHALL3
0.05
1
EPA 200.7
06/12/2015 11:11
MHALL3
0.01
1
EPA 200.7
06/12/2015 11:11
MHALL3
0.005
1
EPA 200.7
06/12/2015 11:11
MHALL3
0.005
1
EPA 200.7
06/12/2015 11:11
MHALL3
0.005
1
EPA 200.7
06/12/2015 11:11
MHALL3
1
1
EPA 200.8
06/22/2015 23:54
SLS2560
1
1
EPA 200.8
06/22/2015 23:54
SLS2560
1
1
EPA 200.8
06/22/2015 23:54
SLS2560
1
1
EPA 200.8
06/22/2015 23:54
SLS2560
1
1
EPA 200.8
06/22/2015 23:54
SLS2560
1
1
EPA 200.8
06/22/2015 23:54
SLS2560
1
1
EPA 200.8
06/22/2015 23:54
SLS2560
1
1
EPA 200.8
06/22/2015 23:54
SLS2560
1
1
EPA 200.8
06/22/2015 23:54
SLS2560
1
1
EPA 200.8
06/22/2015 23:54
SLS2560
1
1
EPA 200.8
06/22/2015 23:54
SLS2560
0.2
1
EPA 200.8
06/22/2015 23:54
SLS2560
0.3
1
EPA 200.8
06/22/2015 23:54
SLS2560

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060348
Site: Field Blank
Collection Date: 10-Jun-15 5:40 PM
Analyte Result Units Qualifiers RDL DF
MERCURY IN WATER - (Analysis Performed by Prism Labs)
Vendor Parameter Complete
Analytical Lab
Page 13 of 54
Sample #: 2015018403
Matrix: GW WW
Method Analysis Date/Time Analyst
Vendor Method V_PRISM

Site: Trip Blank
Collection Date: 10-Jun-15 5:34 PM
Analytical Lab
Certificate of Laboratory Analysis Page 14 of 54
This report shall not be reproduced, except in full.
Order # J15060348
Sample #: 2015018404
Matrix: GW WW
Analyte Result Units Qualifiers RDL DF Method Analysis Date/Time Analyst
MERCURY IN WATER - (Analysis Performed by Prism Labs)
Vendor Parameter Complete Vendor Method V_PRISM
Qualifiers:
M2 Matrix spike recovery was Low: the associated Laboratory Control Spike (LCS) was acceptable.

Analytical Lab
Page 15 of 54
(WI
Uernernt One Mc.
6319-D Carolina Beach Rd.
Mlming>ton, VAC 28412
Phone: [phone]
Fax: [phone]
el lab@el lab com
,seentOne
REPORT OF ANALYSES
Duke Energy
June 16, 2015
Laboratory Services
Client Project Name AB GW Assessment Surface
water HF Lee
13339 Hagers Ferry Road Bld. MG03A Client Project Number J15060348
Huntersville, NC 28078
PO Number
Sample Matrix GW WW
Sample Type Grab
Date Received
06/12/2015
Date Analyzed 06/15/2015
Method SM 4500 S2- D
Time Received
1345
Delivered by FedEx
Received by
JRC
eOne ID Duke Energy ID
Parameter Result Unit
Dil DL Date
Time
Sampled
Sampled
25055-1 S-16
Sulfide < 0.1 mg/L
1 0.1 06/10/15
1055
25055-2 S-10
Sulfide < 0.1 mg/L
1 0.1 06/10/15
1140
25055-3 S-10 Dup
Sulfide < 0.1 mg/L
1 0.1 06/10/15
1150
25055-4 ASW-NR1
Sulfide < 0.1 mg/L
1 0.1 06/10/15
1240
Ken S it , Laboratory Director
25055 Duke Report Packet Compiled by-�?
NC Certifications: DW 37788 and DWQ DENR 604

W
Analytical Lab
Page 16 of 54
euleyuo0 p 1e70l
��
�
o
0
0
0
0
0
0
o e
o
o
g
a
o
w
u
e o sle;aw
_IV
o N = panlossl❑
o o o eeolaq
oI
eas sIe3a W
a
A
II 1,
gm'
mN0 b
ao
I
,e
E a
F N3
a1 0
JLD
o
N T
p
a m = ma
E (�IBBgS N
'a a a4C94 BH
a
N
e
w�0I m 4VIO-013-A)
_
.ate i I IY n d BPUInS
�z
III � C p (RIQagS A
_ W O ppI i yj O a1000QJY'J
oiinnleunn I: .-
�•�II`I acv 11 III•,l i•
I
_
I
a S 1 N 1 'aivuogjv'JIe
'
1
.Rtilwlnlltl
I.
Ixx
0 X w OWUN
vai .1` o X. a 'OMMN '001
O
13,
E m aU
_
H a Sa1'SS1
EZT
I
9 ill u
x
,�
x
quAD
r O
ci
d
a
Q E m
31
C �i
CD 3 a > c
C IF l •Y. i .` .. O
z
J Y
S. �_I LL G C
I:
> m
a '
m am �..
l
F-
`>I =
�m LLI O Cu O U
~
�'
u
a a'
f
'.
10
CL
'gym U
!
u z „i rc s c
CO
m
E`
E
E
E
mwf
q�Y a a1
�a� w n
�
—
=' f
8\
S
amp
0
e LL 3 N
<<
3
LL i
LL
- 0
—
ma d
�F-
c
F-
r:
a
U u N
�a
2 2 w w m
J I Q
d S a m I m m
W W w
. _. _
._.._
-----
.._.._.:_.._
- .�. :.----
._
u la ._. _.
E
W W °
Ym
`
e
5q1
€
�.._.._...
�'.
.�
..... A.....
......
.....
..... i._.._.I......
...........
._.._.
_.'.._,_..
•e

eennentOne SAMPLE SUBMISSION FORM
ETAT 5 BD RUSH
Hold Time Expiration 06.17.15 @ 1055
Client: Duke Energy
LIMS No J15060348
Project ID HF Lee
Analytical Lab
Lab Ibge litd.5
Analysis Due Date 06.15.15
Report Due Date 06.17.15
Date Rec:
06.12.15
Time Rec:
1345
Rec By
JRC
H >9 No Tem <_ 6°C e No Ref. Method:
If No, Record I If No, Record I SM4500 S2 D
Sample Identification & Collection Information
Lab ID
Client ID
Collection Date
Collection Time
Analysis Requested
1
S-16
06/10/15
1055
i e
2
S-10
06/10/15
1140
u i
3
S-10 Dup
06/10/15
1150
ulfi -
4
ASW NR1
06/10/15
1240
NOTE for Sulfide The MS/MSD spike should approximate 2 to 3 times the sample concentration. If no sulfide detected
at 100 pg/L spike the sample to render the final spike concentration at — 500 pg/L
SS Page 1 of 1 Prep By / Date iv¢,--� 6-� � I S ' IS
SS by Labeled By / Date -
6/12/2015 :18 PM ID Verification By /Date uI�✓t� I S. /

Analytical Lab
Page 18 of 54
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
u /mL
DETECTION LIMIT u
1.000
CLIENT:
Duke
SPK LEVEL u
5
Lab ID#
25053/ 054/ 055/ 056/ 057/ 063/ 069/
070
06/15/15
10:45
17:20
KAM
Y
MAX ALIQUOT
Na2S•9H2O Lot # STANDARD conc(ppm)
40721 Cal Std Lot: SD-05-3
QC Std Lot: SD-05-4
STD ABSORPTION
10.00
X
10
10
Y
Date:
Time Analysis Begun
Time Analysis Ended
Analyst:
ug STD
STD
SOLUTION
ABS
0.00
0.000
1.00
0.098
2.50
0.227
5.00
0.428
7.50
0.614
�oao
8.00 tom 1200
10.00 0.795 ■
ALI in mL
ANALYZED
Sloe 0.079013187
Correlation 0.999089306
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
u /mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.098
0.8713
10
10
10
<
87.13%
1.0
Std. B. 2.50
Std. B. 5.00
Std. B. 7.50
Std. B. 10.00
0.233
0.440
0.635
0.829
2.6529
5.3847
7.9582
10.5184
10
10
10
10
10
10
10
10
10
10
10
10
0.265
0.538
0.796
1.052
106.12%
107.69%
106.11 %
105.18%
2.5
5.0
7.5
10.0
LRB
0.000
0.0000
10
10
10
<
0.0
LRB SPK
0.423
5.1604
10
10
10
0.516
103%
5.0
QC
0.451
5.5299
10
10
10
0.553
111 %
5.0
25053-1
0.032
0.0003
10
10
10
<
25053-1 s k
0.340
4.0650
10
10
10
0.406
81 %
5.0
25053-2
0.047
0.1982
10
10
10
a Cad
25053-2 dup
0.015
-0.2241
10
10
10
0 t
25053-2 spk
0.392
4.7512
10
10
10
0.475
95%
5.0
25053-3
0.005
-0.3561
10
10
10
25053-3 s k
0.424
5.1736
10
10
10
0.517
103%
5.0
5053-4
0.008
-0.3165
10
10
10
. ,
c ¢:
25053-4 s k
0.427
5.2131
10
10
10
0.521
104%
5.0
25054-1
0.023
-0.1185
10
10
10
c 01
25054-1 s k
0.388
1 4.6985
10
10
10
0.470
94%
5.0
25054-2
0.107
0.9900
10
10
10
<
25054-2 s k
0.481
5.9258
10
10
10
0.593
119%
5.0
25054-3
0.007
-0.3297
10
10
10
25054-3 s k
0.417
5.0812
10
10
10
0.508
102%
5.0
25054-4
0.065
0.4358
10
10
10
25054-4 s k
0.462
5.6750
10
10
10
0.568
114%
5.0
25054-5
0.047
0.1982
10
10
10
<
25054-5 s k
0.483
5.9522
10
10
10
0.595
119%
5.0
Blank
0.000
0.0000
10
10
10
<
QC 1 0.451 5.5299 10
Submitted for QA- QC- Date: 06/15/15
10
By: (Print)
10 0.553
KAM
111 % 5.0
(sign):
Page 1 of 5

Analytical Lab
Page 19 of 54
METHOD:
SM 4500 S2- D
ELEMENT ASSAY:
Sulfide
CLIENT:
Duke
Lab ID#
25053/ 054/ 055/ 056/ 057/ OE
070
Date:
06/15/15
Time Analysis Begun
10:45
Time Analysis Ended
17:20
X
Y
ug STD
STD
SOLUTION
ABS
0.00
0.000
1.00
0.098
2.50
0.227
5.00
0.428
7.50
0.614
10.00
0.795 .
ELEMENT ONE
Spectrophotometer UNITS OF ANSWER
Wave Length 664 DETECTION LIMIT L_M
SPK LEVEL u
i9f
MAX ALIQUOT
Na2S•9H2O Lot # STANDARD conc(ppm)
40721 Cal Std Lot: SD-05-3
QC Std Lot: SD-05-4
STD ABSORPTION
10.0
X
Tee
0.00 8.00 10.00 1200
x
a
s
Sloe 0.0790131$7
Correlation 0:999089305
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.098
0.8713
10
10
10
<
87.13%
1.0
Std. B. 2.50
0.233
2.6529
10
10
10
0.265
106.12%
2.5
Std. B. 5.00
0.440
5.3847
10
10
10
0.538
107.69%
5.0
Std. B. 7.50
0.635
7.9582
10
10
10
0,796
106.11%
7.5
Std. B. 10.00
0.829
10.5184
10
10
10
1.052
105.18%
10.0
LRB
0.000
0.0000
10
10
10
<
0.0
LRB SPK
0.423
5.1604
10
1 10
10
0.516
103%
5.0
QC
0.451
5.5299
10
10
10
0.553
111 %
5.0
25054-6
0.090
0.7657
10
10
10
25054-6 spk
0.428
5.2263
10
10
10
0.523
105%
5.0
25054-7
0.005
-0.3561
10
10
10
25054-7 dup
0.005
-0.3561
10
10
10
< 0.1
25054-7 spk
0.442
5.4111
10
10
10
0.541
108%
5.0
25054-8
0.184
2.0062
10
10
10
()01
25054-8 s k
0.576
7.1795
10
10
10
0.718
103%
5.0
25054-9
0.004
-0.3693
10
10
1031
25054-9 s k
0.425
5.1868
10
10
10
0,519
104%
5.0
25055-1
0.019
-0.1713
10
10
10
'D 1 r
25055-1 spk
0.395
4.7908
10
10
10
0.479
96%
5.0
25055-2
0.011
-0.2769
10
10
10,0,
;
25055-2 s k
0.392
4.7512
10
10
10
0.475
95%
5.0
25055-3
0.013
-0.2505
10
10
10
Q_ a
25055-3 spk
0.385
4.6589
10
10
10
0.466
93%
5.0
25055-4
0.010
-0.2901
10
10
10;
25055-4 spk
0.394
4.7776
10
10
10
0.478
96%
5.0
25056-1
0.008
-0.3165
10
10
10
c p:
25056-1 spk
0.370
4.4609
10
10
10
0.446
89%
5.0
Blank
0.000
0.0000
10
10
10
<
QC 0.450 F 5.5167 10
Submitted for (?A/QC- Date: 06/15/15
10
By: (Print)
10 0.552
KAM
110% 5.0
(sign): '
Page 2 of 5 ��

Analytical Lab
Page 20 of 54
METHOD:
SM 4500 82- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
u /mL
DETECTION LIMIT u
SE K LEVEL u
1.000
5
CLIENT:
Duke
Lab ID#
25053/ 054/ 055/ 056/ 057/`063/ 069/
070
MAX ALIQUOT 10.00
Na2S•9H2O Lot # STANDARD conc(ppm) X
40721 Cal Std Lot: SD-05-3 10
QC Std Lot: SD-05-4 10
STD ABSORPTION Y
- -- - -.
Date:
06/15/15
Time Analysis Begun
10:45
Time Analysis Ended
17:20
Analyst:
KAM
XY
ug 5 I U
SOLUTION
STD 1
ABS
0.00
0.000
1.00
0.098
2.50
0.227
5.00
0.428
7.50
0.614
10.00
0.79Fi
_000
-sue
8.00 10.w 12W
x
x
SAMPLE SAMP
I.D. ABS
Std. B. 0.00 0.000
Std. B. 1.00 0.098
Std. B. 2.50 0.233
Std. B. 5.00 0.440
Std. B. 7.50 0.635
Std. B. 10.00 0.829
ug PER
ALIQUOT
0.0000
0.8713
2.6529
5.3847
7.9582
10.5184
ALI in mL PREP
ANALYZED VOL in mL
10 10
10 10
10 10
10 10
10 10
10 10
Sloe
0.079013187
Correlation
0.999089305
ALI in mL
TAKEN
10
10
10
10
10
10
RESULTS
u /mL
<
<
0.265
0.538
0.796
1.052
LESS THAN
% SPK REC
87.13%
106.12%
107.69%
106.11 %
105.18%
SPIKE
LEVEL
0.0
1.0
2.5
5.0
7.5
10.0
LRB
0.000
0.0000
10
10
10
<
0.0
LRB SPK
0.423
5.1604
10
10
10
0.516
103%
5.0
QC
0.451
5.5299
10
10
10
0.553
111 %
5.0
25056-2
0.011
-0.2769
10
10
101,
25056-2 s k
0.360
4.3289
10
10
10
0.433
87%
5.0
25056-3
0.005
-0.3561
10
10
10�"
25056-3 spk
0.421
5.1340
10
10
10
0.513
103%
5.0
25057
0.007
-0.3297
10
10
10
< t1
25057 dup
0.007
-0.3297
10
10
10
< 0.1
25057 s k
0.426
5.1999
10
10
10
0.520
104%
5.0
25063
0.015
-0.2241
10
10
10
<
25063 s k
0.112
1.0560
10
10
10
0.106
21 %
5.0
24186 - 19.2 QC
0.273
3.1808
10
10
1
3.181
TV= 4.23
25053-1
0.015
-0.2241
10
10
5
5l
25053-1 s k
0.386
4.6721
10
10
5
0,934
93%
5.0
25054-2
0.057
0.3302
10
10
50"
25054-2 s k
0.462
5.6750
10
10
5
1.135
114%
5.0
25054-5
0.024
-0.1053
10
10
5''
25054-5 s k
0.441
5.3979
10
10
5
1.080
108%
5.0
25063
0.020
-0.1581
10
10
5
<
25063 s k
0.163
1.7291
10
10
5
0.346
35%
5.0
25063
0.021
-0.1449
10
10
2
<
25063 spk
0.223
2.5209
10
10
2
1.260
50%
5.0
Blank
0.000
0.0000
10
10
10
<
QC 0.450 1 5.5167 10
Submitted for QA/QC- Date: 06/15/15
10
By: (Print)
10 0.552
K.AM
110% 5.0
(sign):
Page 3 of 5 '�

Analytical Lab
Page 21 of 54
METHOD: SM 4500 S2- D ELEMENT ONE
ELEMENT ASSAY: Sulfide Spectrophotometer UNITS OF ANSW
DETECTION LIMI
Wave Length 664 CLIENT: Duke SPK LEVEL u
25053/ 054/ 055/ 056/ 057/ 063/ 069/
Lab ID# 070 MAX ALIQUOT
Date.
06/15/15
Na2S•9H2O Lot #
STANDARD conc(ppm)
Time Analysis Be un
10:45
40721
Cal Std Lot: SD-05-3
Time Analysis Ended
17:20
QC Std Lot: SD-05-4
Analyst:
KAM
-------
--------
STD ABSORPTION
ug STD
SOLUTION
STD
ABS
0.00
0.000
1.00
0.098
2.50
0.227
5.00
0.428
7.50
0,614
10.00
0.795
o.�
o.�
Y
DAM
o.wo
0.200
227
0.100
D.=
000
�m
.....
_
1
X
10
10
Y
-rso
M 8.00 10A0 12.00
x
Slope 0.079013187
Correlation
0.999089306
SAMPLE
I.D.
Std. B. 0.00
Std. B. 1.00
Std. B. 2.50
Std. B. 5.00
Std. B. 7.50
Std. B. 10.00
SAMP
ABS
0.000
0.098
0.233
0.440
0.635
0.829
ug PER
ALIQUOT
0.0000
0.8713
2.6529
5.3847
7.9582
10.5184
ALI in mL
ANALYZED
10
10
10
10
10
10
PREP
VOL in mL
10
10
10
10
10
10
ALI in mL
TAKEN
10
10
10
10
10
10
RESULTS
u /mL
<
<
0.265
0.538
0.796
1.052
LESS THAN
% SPK REC
87.13%
106.12%
107.69%
106.11 %
105.18%
SPIKE
LEVEL
0.0
1.0
2.5
5.0
7.5
10.0
LRB
0.000
0.0000
10
10
10
<
0.0
LRB SPK
0,423
5.1604
10
10
10
0.516
103%
5.0
QC
0.451
5.5299
10
10
10
0.553
111 %
5.0
25063
0.013
-0.2505
10
10
1
<
25063 s k
0.313
3.7087
10
10
1
3.709
74%
5.0
25063
0.007
-0.3297
10
10
0.5
<
25063 spk
0.345
4.1310
10
10
0.5
8.262
83%
5.0
25063
0.003
-0.3825
10
10
0.25
<.0 4 � _'
w
25063 s k
0.385
4.6589
10
10
0.25
18.635
93%
5.0
24186-19.2 QC
25069-1
0.307
0.006
3.6295
-0.3429
10
10
10
10
1
10
3.629
�.r a
86%
TV=4.23
25069-1 spk
0.418
5.0944
10
10
10
0.509
102%
5.0
25069-2
0.011
-0.2769
10
10
10
25069-2 dup
0.011
-0.2769
10
10
10
< 0.1
25069-2 s k
0.372
4.4873
10
10
10
0.449
90%
5.0
25069-3
0.003
-0.3825
10
10
10
r'
5.0
25069-3 s ki
0.434
5.3055
10
10
10
0.531
106%
25070-5
0.004
-0.3693
10
10
10
<
25070-5 spk
0.344
4.1178
10
10
10
0.412
82%
5.0
25070-6
0.003
-0.3825
10
10
10
4;
25070-6 s k
0.428
5.2263
10
10
10
0.523
105%
5.0
25070-7
0.002
-0.3957
10
10
10
25070-7 s k
0.434
5.3055
10
10
10
0.531
106%
5.0
Blank
0.000 1
0.0000
10
10
10
<
17 QC
Submitted for QA/QC-
0.450 5.5167 10
Date: 06/15/15
10
By: (Print)
10 0.552
KAM
110°/ 5.0
(sign): r
Page 4 of 5

Analytical Lab
Page 22 of 54
METHOD:
SM 4500 S2- D
ELEMENT ASSAY:
Sulfide
CLIENT:
Lab ID#
Duke
25053/ 054/ 055/ 056/ 057/ 063/
070
Date:
06/15/15
Time Analysis Begun
10:45
Time Analysis Ended
17:20
X
Y
ug STD
STD
ELUTION
ABS
0.000
0.00
1.00
0.098
2.50
0.227
5.00
0.428
7.50
0.614
10.00
0.795
ELEMENT ONE
pectrophotometer UNITS OF ANSW
Wave Length 664 DETECTION LIMI
n r.v . - •r-. I
Na2S•9H2O Lot # STANDARD conc(ppm)
40721 Cal Std Lot: SD-05-3
QC Std Lot: SD-05-4
STD ABSORPTION
r
J
_-
5
10.00
X
10
10
Y
-_soon
BW BW +UW I2.W
X
SAMPLE SAMP ug PER
I.D. ABS ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
Slope 0.079013187
Correlation0:999.089305
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Sid. B. 1.00
0.098
0.8713
10
10
10
<
87.13%
1.0
Std. B. 2.50
0.233
2.6529
10
10
10
0.265
106.12%
2.5
Std. B. 5.00
0.440
5.3847
10
10
10
0.538
107.69%
5.0
Sid. B. 7.50
0.635
7.9582
10
10
10
0.796
106.11 %
7.5
Std. B. 10.00
0.829
10.5184
10
10
10
1.052
105.18%
10.0
LRB
0.000
0.0000
10
10
10
<
0.0
LRB SPK
0.423
5.1604
10
10
10
0.516
103%
5.0
QC
0.451
5.5299
10
10
10
0.553
111 %
5.0
25070-8
0.004
-0.3693
10
10
10
25070-8 s k
0.426
5.1999
10
10
10
0.520
104%
5.0
25070-9
0.011
-0.2769
10
10
10
Q;
25070-9 s k
0.404
4.9096
10
10
10
0.491
98%
5.0
25070-5
0.015
-0.2241
10
10
10
25070-5 spk
0.365
4.3949
10
10
5
0.879
88%
5.0
24186-19.2 QC
0.308
3.6427
10
10
1
3.643
86%
TV= 4.23
Blank
0.000
0.0000
10
10
10
<
QC 0.450 5.5167 10
Submitted for QA/QC- Date: 06/15/15
10
By: (Print)
10 0.552
KAM
110% 5.
(sign):
Page 5 of 5

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
Project Name: AB GW Assessment Water - HF Lee
Project Number:J15060348
Lot Number:QF12011
Date Completed:06/17/2015
Grant Wilton
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
* QF1 201 1 *
Shealy Environmental Services, Inc. Page: 1 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Duke Energy
Lot Number: QF12011
Project Name: AB GW Assessment Water - HF Lee
Project Number: J15060348
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QF12011
Project Name: AB GW Assessment Water - HF Lee
Project Number: J15060348
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
2015018398
Aqueous
06/10/20151055
06/12/2015
002
2015018399
Aqueous
06/10/20151140
06/12/2015
003
2015018400
Aqueous
06/10/20151150
06/12/2015
004
2015018401
Aqueous
06/10/20151240
06/12/2015
005
2015018403
Aqueous
06/10/20151740
06/12/2015
006
2015018404
Aqueous
06/10/20151734
06/12/2015
(6 samples)
Shealy Environmental Services, Inc. Page: 3 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES,
INC.
Executive Summary
Duke Energy
Lot Number: QF12011
Project Name: AB GW Assessment Water - HF Lee
Project Number: J15060348
Sample Sample ID
Matrix Parameter Method Result Q
Units
Page
001
2015018398
Aqueous Alkalinity SM 2320B-
33
mg/L
5
001
2015018398
Aqueous Bicarbonate Alkalinity SM 2320B-
33
mg/L
5
001
2015018398
Aqueous Methane RSK - 175
14
ug/L
6
002
2015018399
Aqueous Alkalinity SM 2320B-
34
mg/L
7
002
2015018399
Aqueous Bicarbonate Alkalinity SM 2320B-
33
mg/L
7
002
2015018399
Aqueous Methane RSK - 175
11
ug/L
8
003
2015018400
Aqueous Alkalinity SM 2320B-
34
mg/L
9
003
2015018400
Aqueous Bicarbonate Alkalinity SM 2320B-
34
mg/L
9
003
2015018400
Aqueous Methane RSK - 175
12
ug/L
10
004
2015018401
Aqueous Alkalinity SM 2320B-
35
mg/L
11
004
2015018401
Aqueous Bicarbonate Alkalinity SM 2320B-
35
mg/L
11
004
2015018401
Aqueous Methane RSK - 175
23
ug/L
12
(12 detections)
Shealy Environmental Services, Inc. Page: 4 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF12011-001
Description: 2015018398 Matrix: Aqueous
Date Sampled:06/10/2015 1055 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060348
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/16/2015 2045
HMA 77407
1
(Bicarbonate ) SM 2320B-2011
1 06/16/2015 2045
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/16/2015 2045
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
33
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
33
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF12011-001
Description: 2015018398 Matrix: Aqueous
Date Sampled:06/10/2015 1055 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060348
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/16/2015 2051 JJG 77428
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 14 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF12011-002
Description: 2015018399 Matrix: Aqueous
Date Sampled:06/10/2015 1140 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060348
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/16/2015 2051
HMA 77407
1
(Bicarbonate ) SM 2320B-2011
1 06/16/2015 2051
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/16/2015 2051
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
34
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
33
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF12011-002
Description: 2015018399 Matrix: Aqueous
Date Sampled:06/10/2015 1140 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060348
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/16/2015 2102 JJG 77428
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 11 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 8 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF12011-003
Description: 2015018400 Matrix: Aqueous
Date Sampled:06/10/2015 1150 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060348
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/16/2015 2057
HMA 77407
1
(Bicarbonate ) SM 2320B-2011
1 06/16/2015 2057
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/16/2015 2057
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
34
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
34
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF12011-003
Description: 2015018400 Matrix: Aqueous
Date Sampled:06/10/2015 1150 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060348
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/16/2015 2113 JJG 77428
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 12 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 10 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF12011-004
Description: 2015018401 Matrix: Aqueous
Date Sampled:06/10/2015 1240 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060348
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/16/2015 2103
HMA 77407
1
(Bicarbonate ) SM 2320B-2011
1 06/16/2015 2103
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/16/2015 2103
HMA
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
35
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
35
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 11 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF12011-004
Description: 2015018401 Matrix: Aqueous
Date Sampled:06/10/2015 1240 Project Name: AB GW Assessment Water -
Date Received:06/12/2015 Project Number: J15060348
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/16/2015 2129 JJG 77428
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 23 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 12 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: QF12011
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MB
Sample ID: QQ77407-001 Matrix: Aqueous
Batch:77407
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 06/16/20151902
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF12011
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - LCS
Sample ID: QQ77407-002 Matrix: Aqueous
Batch:77407
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 93 1 93 90-110 06/16/20151908
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF12011
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ77428-001 Matrix: Aqueous
Batch:77428
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 06/16/20151701
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF12011
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ77428-002 Matrix: Aqueous
Batch:77428
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 50 43 1 85 70-130 06/16/20151632
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF12011
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ77428-003 Matrix: Aqueous
Batch:77428
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 50 44 1 87 2.2 70-130 30 06/16/20151646
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF12011
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
W
C
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Shcal4 Ent-Imw Lnncel Services, ILta.
Doavmcw NjmL�r F-AD-016
RevisinnNumber: L7
Pace 1 of 1
"laces Dame, I1r07A4
EffeciiveDaze: Oq+' UflS
Sample Receipt Checklist (SRC)
Clicrit_ e- 1 F ii Cooler htspeczed by/datt- VkkQ rl(o-I -1S Lot 9: Q C)
Mtans of receipt: SESI ❑ Client ❑ M ❑ FCdEx ❑ A irbt►rric Exp 4 11, er
Yes NO 1. Wexc custody seals resant an the cooler?
Yes No aJs were Ment,w�ere they intact and unhrnken'?
Coulm lD/OrigbiA LrmperatLrre upon reed t,T)erived {corrected) temperature upon rt ipt;
AU lglo -C I '� I- -C i I - ac r I °C
Method- Q Temperature stl: A ftit5st Bottles lR CJirn ID_ Il? [,unCorrection t�L+ Ler: If
Method of coolant: �et lee f "I Blue Ice I —I nr,r ire
--
Yes Wr
No D
NA ®
3. If tcmperature of c�)oler exomded 6-0 "C, was Project Manager notified?
PM notified b) RC' phone, note (dircle ), other
(For mioicrs rccravcd via cS mmmiaLl Courier, PNIs are to lie nolificd
imT.n µali wly)
Yes ❑rio
❑
:fA
- Ls the Cummexia1 courier's pauking slip attarhed to thiis dorm?
Yes
No ❑
. Wcrc prupicr ousted pracedures (relin uishedlr eived) followed? -
5a Wcrc samples rclinquished by client to oo)natuercial courier?
Yeq Yn❑ NA
Yes
N0 ❑
6, Were sam to IDs listed on the COC?
Yes
_No ❑
7. Wue samele Ms listed on all sample conWaers?
Yes
No []
9- Was collection date & time. listed on Lhc COC?
yCS CXN0
❑
9. Was collection date & tm' a listed. on all sample containers'.+
Yes
YO ❑
ltl. Did ell container label infonnatian fO, date, lime) figrer with the LC{ .?
Yes
o ❑
11 - Were tests to be ome d listed on the COO
Yet
o ❑
12. Did all sour les arrive in the proper containers for each test?
'r`gR
e 0
13- Did all containers arrive in Z ood condition unbroken, lids �OrL, cl.c- ?
Yes
No ❑
14, Was aide Tote saurglo volume available'
Yes ❑
'No
_
15. " em a]I samples received within '6 the holding time or 4S hours, whichcwcr
Comes first?
Yes
No
16. WCro any.; ai los ca�lil3CM missiEI87
YeN ❑
No
_
NA
17, Were there any ex ms somplcs not listed on COO?
18. Were bubbles reseaut >« ea -size'* ' "Sir 6tiil¢�L ill diaia4 t�r� in an VOA vials'
Yes ® No
Yes ❑
1�10 ❑
1�1A
19.4c all asctalJD&GiEI4?nr�tricnt sour lcs received at a H df?
O- were al] c atlide ancVor su fide samples =eived at a >12?
Y,hs ❑ Mn ❑ NA
Yes ❑
No ❑
NA
21- V4Wece all applicable 11,R�ITKN/eyiarddelphenol (<13.2mg/L.) samples free of
residual chlorine?
Yes ❑
Igo ©
NA
22. Wert llocti+on to eratures documented ion the C for N Samples?
Yes ❑
Nr3 ❑
NAL
3. Were Client rerriarkslrequests (i.e. rcqucsted dilutions, lUi r SD designations,
rtcJ : r�rreMd tTuTtscrilad frorn 6t: 000 into the comment section in LIMS?
Yes ❑
N4
24. Was the uote su>mber used taken from the container label? -
am* Preservntton (blurt be cnttopletad for any sample(s) incorrectly preserved or with htadspace.)
Samples) _ were received incorrectly pmerved and were adjusted
accordingly in -.,-j-np Ic rocciving. with H2S ,HNO3,HCi,Na0H) using SR #
ram lc(s) vLrere received with bubbles >6 mm in diameter -
Sam lc(s) were receiNvd with TRC ,-O.2 m +L Uf 421 is No
SC DT rLking Water P3-Gjeci Sample(s)pH VCJ'L-.12d to l>e -�, 2 by Date:
Sara l s were not rcocivod al s p4 of <2 and were adjnstod accordingly using, SEA#
Sarnialr labels applied by: tA JkAo Verified by: Date. (a- LP -15
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

P R I S M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Duke Energy Corporation
Mary Ann Ogle
13339 Hagers Ferry Road
Huntersville, NC 28078
NC Certification No. 402
SC Certification No. 99012
NC Drinkinq Water Cert No. 37735
VA Certification No. 460211
DOD ELAP: L-A-B Accredited Certificate No. L2307
ISO/IEC 17025: L-A-BAccredited Certificate No. L2307
Project: Low Level Mercury Rushes
Project No.: J15060348
Lab Submittal Date: 06/24/2015
Prism Work Order: 5060448
nalytica ab
narrative
06/26/2015
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
I �� �L �_ I � (_ - &. I -
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 11

P R I IS M Full -Service Analytical s
Environmental Solutions
LABORATORIES, INC.
Sample Rec#i 4jfVtnmary
06/26/2015
Prism Work Order: 5060448
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
2015018398/S-16
5060448-01
Water
06/10/15
06/24/15
2015018399/S-10
5060448-02
Water
06/10/15
06/24/15
2015018400/S-10 Dup
5060448-03
Water
06/10/15
06/24/15
2015018401/ASW-NR1
5060448-04
Water
06/10/15
06/24/15
2015018403/Field Blank
5060448-05
Water
06/10/15
06/24/15
2015018404/Trip Blank
5060448-06
Water
06/10/15
06/24/15
Samples were received at 24.1 degrees C. See case narrative for further information.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 11

PRISMFull -Service Analytical Environmental Solutions
3 LABORATORIES, INC.
Duke Energy Corporation
Attn: Mary Ann Ogle
13339 Hagers Ferry Road
Huntersville, NC 28078
Labo tTY,,Report
06/26/2015
Project: Low Level Mercury Rushes
Client Sample ID: 2015018398/S-16
Prism Sample ID: 5060448-01
Project No.: J15060348
Prism Work Order: 5060448
Sample Matrix: Water
Time Collected: 06/10/15 10:55
Time Submitted: 06/24/15 09:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Total Metals
Mercury 1.4
ng/L 1.0 0.27 1 *1631E 6/25/15 21:58 BGM P51F0447
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 11

Laboi+c�eport
Full -Service Analytical &
P R S M
Page 46 0 54
/ Environmental Solutions
LABORATORIES INC.
06/26/2015
Duke Energy Corporation
Project: Low Level Mercury Rushes
Client Sample ID: 2015018399/S-10
Attn: Mary Ann Ogle
Prism Sample ID: 5060448-02
13339 Hagers Ferry Road
Project No.: J15060348
Prism Work Order: 5060448
Huntersville, NC 28078
Sample Matrix: Water
Time Collected: 06/10/15 11:40
Time Submitted: 06/24/15 09:30
Parameter Result
Units Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
Total Metals
Mercury 1.2
ng/L 1.0 0.27
1 *1631E 6/25/15 22:04 BGM P5F0447
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 11

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Duke Energy Corporation
Attn: Mary Ann Ogle
13339 Hagers Ferry Road
Huntersville, NC 28078
Project: Low Level Mercury Rushes
Project No.: J15060348
Sample Matrix: Water
Laboink" deport
Page 47 o 54
06/26/2015
Client Sample ID: 2015018400/S-10 Dup
Prism Sample ID: 5060448-03
Prism Work Order: 5060448
Time Collected: 06/10/15 11:50
Time Submitted: 06/24/15 09:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Total Metals
Mercury 1.5 ng/L 1.0 0.27 1 *1631E 6/25/15 22:31 BGM P5F0448
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 11

PR I S M Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Duke Energy Corporation
Attn: Mary Ann Ogle
13339 Hagers Ferry Road
Huntersville, NC 28078
Project: Low Level Mercury Rushes
Project No.: J15060348
Sample Matrix: Water
Laboini+c tReport
Page 48 o 54
06/26/2015
Client Sample ID: 2015018401/ASW-NR1
Prism Sample ID: 5060448-04
Prism Work Order: 5060448
Time Collected: 06/10/15 12:40
Time Submitted: 06/24/15 09:30
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Total Metals
Mercury 1.6 ng/L 1.0 0.27 1 *1631E 6/25/15 22:36 BGM P5F0448
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 11

Laboi+c�eport
Full -Service Analytical &
P R S M
Page 49 0 54
/ Environmental Solutions
LABORATORIES INC.
06/26/2015
Duke Energy Corporation
Project: Low Level Mercury Rushes
Client Sample ID: 2015018403/Field Blank
Attn: Mary Ann Ogle
Prism Sample ID: 5060448-05
13339 Hagers Ferry Road
Project No.: J15060348
Prism Work Order: 5060448
Huntersville, NC 28078
Sample Matrix: Water
Time Collected: 06/10/15 17:40
Time Submitted: 06/24/15 09:30
Parameter Result
Units Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
Total Metals
Mercury BRL
ng/L 1.0 0.27
1 '1631E 6/25/15 21:47 BGM P51`0447
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 11

t
Labo i+50
Full -Service Analytical &
P R S M
Page 50 0 54
oT54
/ Environmental Solutions
LABORATORIES INC.
06/26/2015
Duke Energy Corporation
Project: Low Level Mercury Rushes
Client Sample ID: 2015018404/Trip Blank
Attn: Mary Ann Ogle
Prism Sample ID: 5060448-06
13339 Hagers Ferry Road
Project No.: J15060348
Prism Work Order: 5060448
Huntersville, NC 28078
Sample Matrix: Water
Time Collected: 06/10/15 17:34
Time Submitted: 06/24/15 09:30
Parameter Result
Units Report MDL
Dilution Method Analysis Analyst Batch
Limit
Factor Date/Time ID
Total Metals
Mercury BRL
ng/L 1.0 0.27
1 '1631E 6/25/15 21:53 BGM P51`0447
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 11

Full -Service Analytical &
P R I IS M
Environmental Solutions
LABORATORIES, INC.
Duke Energy Corporation
Attn: Mary Ann Ogle
13339 Hagers Ferry Road
Huntersville, NC 28078
Total Metals - Quality Control
Analyte
Batch P5FO447 - 1631 E
Project: Low Level Mercury Rushes
Project No: J15060348
AneyeialLQC Report
Page 51 of 54 6/26/15
Prism Work Order: 5060448
Time Submitted: 6/24/2015 9:30:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P5F0447-BLK1)
Prepared &Analyzed: 06/25/15
Mercury
BRL 1.0 ng/L
Blank (P5F0447-BLK2)
Prepared & Analyzed: 06/25/15
Mercury
BRL 1.0 ng/L
LCS (P5F0447-BS1)
Prepared &Analyzed: 06/25/15
Mercury
4.40 1.0 ng/L 5.000 88 79-121
Batch P5F0448 - 1631 E
Blank (P5F0448-BLK1) Prepared & Analyzed: 06/25/15
Mercury BRL 1.0 ng/L
LCS (P5F0448-BS1) Prepared &Analyzed: 06/25/15
Mercury 4.91 1.0 ng/L 5.000 98 79-121
Matrix Spike (P5F0448-MS1) Source: 5060448-04 Prepared & Analyzed: 06/25/15
Mercury 15.2 1.1 ng/L 13.64 1.55 100 71-125
Matrix Spike Dup (P5F0448-MSD1) Source: 5060448-04 Prepared & Analyzed: 06/25/15
Mercury 12.4 1.1 ng/L 13.64 1.55 79 71-125 21 24
Sample Extraction Data
Prep Method: 1631E
Lab Number Batch Initial Final Date/Time
5060448-01
P51`0447
500
mL
500
mL
06/25/15
7:30
5060448-02
P5F0447
500
mL
500
mL
06/25/15
7:30
5060448-03
P5F0448
250
mL
250
mL
06/25/15
7:30
5060448-04
P5F0448
250
mL
250
mL
06/25/15
7:30
5060448-05
P51`0447
500
mL
500
mL
06/25/15
7:30
5060448-06
P5F0447
500
mL
500
mL
06/25/15
7:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 9 of 11

Analytical Lab
Page 9a&
*�
0 0 0 ^ P g\\OG]]

Analytical Lab
Page 53 of 54
Cyo
z
uj
(molaq
SMOW
ILI
aqJ
0
F
4M
2
all
G IUOW813
apigns
z
n
I
N'30J.
'vos'lo
i 0
E
'r
75
ioja
V,
Gai'ssi
>
'dw
C) 0 (L
>
V
V
LL
C
(Y)
M
C)o
4.,611
E
0
-LU
CL
IMU
(7
............
DZ
r
C
.5
w
C
C 0
- > ui ()
Ct
17L
E
gl!
rn
im
CL
E
lQ
0,
'0 r %
uj
'V
......
............
......
...
............
....
..
C
<
0
L)
0
C3
0.
Z.
_j
21
41
L) e
E
LY
t E
3
0 CC
E
Cp
LU W 0,
m CO
L
1 Page 1

CHAIN OF CUSTODY RECORD AND ANALYSIS_ REQUEST FORM
---'-'-' Duke Energy ._._._._
• i5je Energy Analytical Laboratory
-• I.--'-•-•---'---'---•-•-•-•—,-
.... ..Analytical -:--- Laboratory Use Onl-'--'---'-•-'-•-•----._._._._.-.-._._._._._._..
Analytical Laboratory
Mall Code MGOW (Building r4o3)
13339 Hagen Ferry Rd
Order
J _<�
X GW W W
KA—
5amplee orlginadnprrom sC_
Chain of Custody &
Sample Lo
P 9
Hunlersvnle, N. C. 21.1.
(�oq Ns22A6
i r�� .y �, - Dale t
r I �1,.
SAMPLE PROGRAM
i
:._._._._._.
Fax:sn.1 EH.W ..............
._._._._._._. _._. _.
! !
Ground Water NPDES
_._._._._._._._._._._._._._._.
Prgarr Naa a AS GW Assessment SURFACE PhO"f No'
r�
J
Drinking Water UST _
RCRAWeb
E r
Client
Fax No:
Elementl
p
......_.._.._.._.._.._.._.._.
s'
980475-5032
; p01142133
Filtration (0.45 um)
Unfiltered
E BOsiMSS Unit:
prgecss: R.P. Canby Tx
t
Preservative Ice
bar
Ice lee 11 elee +�ele
i Prolaat ax.
pedvlly lD:
NN Cpaa:
MG03A3
I
Cho ^_11r
ar Volume (mL)
%Ontainef TYPe
2000
40 ml
300
126
500
$00
40 mL
y: HF Lae
PET
SrIeSS
PET
PET
PET
PET
Blass
Analytical L b Synxerr•a EDD
Page 54 of 4
Page _1_ of
_1_
DISTRIBUTION
ORIGINAL to LAB, COPY
to CLIENT
OC REV DATE
1/22/2015
filtered
HDPEIHOPE
r-01142089
Sample Description or ID ate non
sna°e° areas.
Collection Information
GPS Location
Date Time nature
O
H
ryj
n
t-
X2,
U) m
m N
c>
t—
m n_
d'
0
M
v
r
A
Z N
'�
t- Z
g _
c 7o T
c° c y
'A m° s
x i y
a m ci >
d E
L d
t_ W
l
US Z
M d
{ L
U)
rn l
x Z
�A•,
N 3
O
d
N
0
N
•- m
0 EAb
o
U
o
~
A
n`
(P
X
1
2
,
1
1
1
2
1
1
11
—10
1
ll1/0
>t
I
2
1
I
I
f
Z.
r
I
9'
so
)(I
r
2
W- 1.
I2Y0
2
1
r
It
Z
r
r
0
0
0
0
0
0
0
0
0
0
Filter Blank
o !j
Field Blank
jfj
gil
1
Trip Blank
0
TOTAL
132
1
1
1 4
0
0
0
1
2
0
14
TtelTime
By:
ELEMENTS by ICP MS (TRM): As, Be, Cd, Co, Cr, Cu, Mo, Ni, Pb, Sb, Se, TI (ILL), V (LL)
ELEMENTS by ICP (TRM): All, Be, B, Fe, Mn, Sr, Zn ICP Undigested Ca, Mg, K, Na Hg by 245.1
Dissolved metals : all metals ICP, IMS,Hg
R
Requested Turnaround T
'14 Days
m
ns c
N 3
a o
c
7 Days
c �
m
0
°a S
48 Hr
E N
N
V
d
c
'Other _ASAP
' Add. Cost Will Apply
U
>tal E