NC0003417_J15050112report_20150805

+ DUKE Analytical Laboratory
ENERGY
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
Order Number: J15050112
Project Name: HF LEE PLANT - AB GW ASSESSMENT SURFACE
Customer Name(s): Tim Hunsucker, Judd Mahan, Kathy Webb, John Toepfer
Customer Address: 1677 Old Smithfield Rd
Goldsboro NC 27530,
Lab Contact: Mary Ann Ogle Phone: [phone]
�n Mary Ann Ogle
Report Authorized By: % 2015.05.22 12:50:40 Date: 5/20/2015
(Signature)-04'00'
Mary Ann Ogle
Program Comments:
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
Page 1 of 103
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Page 2 of 103
Sample ID Plant/Station
Collection
Date and Time Collected By
Sample Description
2015013503
HF LEE PLANT
04-May-15 2:30 PM
ILLEGIBLE
S-04
2015013504
HF LEE PLANT
04-May-15 4:45 PM
ILLEGIBLE
S-09
2015013505
HF LEE PLANT
04-May-15 3:35 PM
ILLEGIBLE
S-03A
2015013506
HF LEE PLANT
05-May-15 8:50 AM
ILLEGIBLE
S-24
2015013507
HF LEE PLANT
05-May-15 9:45 AM
ILLEGIBLE
S-06
2015013508
HF LEE PLANT
05-May-15 10:25 AM
ILLEGIBLE
S-01
2015013509
HF LEE PLANT
05-May-15 11:15 AM
ILLEGIBLE
ASW-BG
2015013510
HF LEE PLANT
05-May-15 1:55 PM
ILLEGIBLE
S-15
2015013511
HF LEE PLANT
05-May-15 2:45 PM
ILLEGIBLE
S-14
2015013512
HF LEE PLANT
05-May-15 3:00 PM
ILLEGIBLE
S-14 Dup
2015013513
HF LEE PLANT
05-May-15 3:50 PM
ILLEGIBLE
ISW-HMBREF
2015013514
HF LEE PLANT
Filter Blank
2015013515
HF LEE PLANT
Field Blank
2015013516
HF LEE PLANT
Trip Blank
14 Total Samples

Page 3 of 103
Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals Yes No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes❑ No
All laboratory QA/QC requirements are acceptable.❑ Yes ❑ No
Report Sections Included:
U Job Summary Report
❑ Sample Identification
n Technical Validation of Data Package
❑ Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
66 Chain of Custody
[I/0] Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Peggy Kendall Date: 5/20/2015

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050112
Site: S-04
Collection Date: 04-May-15 2:30 PM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
23
mg/L
1
Sulfate
54
mg/L
1
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
Vendor Parameter
Complete
DISSOLVED METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
0.289
mg/L
0.005
Boron (B)
1.54
mg/L
0.05
Iron (Fe)
0.174
mg/L
0.01
Manganese (Mn)
0.500
mg/L
0.005
Strontium (Sr)
2.85
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
105
mg/L
0.1
Magnesium (Mg)
12.3
mg/L
0.005
Potassium (K)
10.7
mg/L
0.1
Sodium (Na)
29.2
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.025
mg/L
0.005
Barium (Ba)
0.368
mg/L
0.005
Boron (B)
1.61
mg/L
0.05
Iron (Fe)
5.54
mg/L
0.01
Manganese (Mn)
0.651
mg/L
0.005
Strontium (Sr)
3.17
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Page 4 of 103
Sample #: 2015013503
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
05/07/2015 11:33
LSTARL1
10
EPA 300.0
05/11/2015 11:01
BGN9034
10
EPA 300.0
05/11/2015 11:01
BGN9034
Vendor Method
V_SHEALY
1
EPA 200.7
05/07/2015 13:04
MHALL3
1
EPA 200.7
05/07/2015 13:04
MHALL3
1
EPA 200.7
05/07/2015 13:04
MHALL3
1
EPA 200.7
05/07/2015 13:04
MHALL3
1
EPA 200.7
05/07/2015 13:04
MHALL3
1
EPA 200.7
05/07/2015 13:04
MHALL3
1
EPA 200.7
05/07/2015 13:04
MHALL3
10
EPA 200.7
05/07/2015 15:16
MHALL3
1
EPA 200.7
05/07/2015 15:16
MHALL3
1
EPA 200.7
05/07/2015 15:16
MHALL3
1
EPA 200.7
05/07/2015 15:16
MHALL3
1
EPA 200.7
05/08/2015 12:30
MHALL3
1
EPA 200.7
05/08/2015 12:30
MHALL3
1
EPA 200.7
05/08/2015 12:30
MHALL3
1
EPA 200.7
05/08/2015 12:30
MHALL3
1
EPA 200.7
05/08/2015 12:30
MHALL3
1
EPA 200.7
05/08/2015 12:30
MHALL3
1
EPA 200.7
05/08/2015 12:30
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050112
Site: S-04
Collection Date: 04-May-15 2:30 PM
Analyte
Result
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
77.8
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
1.01
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
72.4
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
387
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
1.49
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
86.7
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
0.259
Vanadium (V) Low Level
< 0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
410
Total Carbon
TOC
2.5
TOTAL SUSPENDED SOLIDS
TSS
11
Page 5 of 103
Sample #:
2015013503
Matrix:
GW_WW
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
05/13/2015 17:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:17
JAHERMA
ug/L
0.2
1
EPA 200.8
05/13/2015 17:17
JAHERMA
ug/L
0.3
1
EPA 200.8
05/13/2015 17:17
JAHERMA
ug/L
1
1
EPA 200.8
05/15/2015 12:39
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:39
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:39
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:39
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:39
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:39
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:39
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:39
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:39
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:39
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:39
DJSULL1
ug/L
0.2
1
EPA 200.8
05/15/2015 12:39
DJSULL1
ug/L
0.3
1
EPA 200.8
05/15/2015 12:39
DJSULL1
Vendor Method V SHEALY
Vendor Method
V_ELE1
mg/L
25 1 SM2540C
05/07/201510:20 AGIBBS5
mg/L
0.1 1 SM5310C/EPA9060A
05/07/201514:53 GHUTCHI
mg/L
5 1 SM2540D
05/06/2015 08:52 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050112
Site: S-09
Collection Date: 04-May-15 4:45 PM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.204
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
25
mg/L
1
Sulfate
37
mg/L
1
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
Vendor Parameter
Complete
DISSOLVED METALS BY ICP
Aluminum (AI)
0.017
mg/L
0.005
Barium (Ba)
0.123
mg/L
0.005
Boron (B)
2.44
mg/L
0.05
Iron (Fe)
0.152
mg/L
0.01
Manganese (Mn)
0.388
mg/L
0.005
Strontium (Sr)
1.83
mg/L
0.005
Zinc (Zn)
0.006
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
61.1
mg/L
0.01
Magnesium (Mg)
13.6
mg/L
0.005
Potassium (K)
8.45
mg/L
0.1
Sodium (Na)
23.5
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.361
mg/L
0.005
Barium (Ba)
0.135
mg/L
0.005
Boron (B)
2.44
mg/L
0.05
Iron (Fe)
3.47
mg/L
0.01
Manganese (Mn)
0.408
mg/L
0.005
Strontium (Sr)
1.89
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Page 7 of 103
Sample #: 2015013504
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
05/07/2015 11:34
LSTARL1
10
EPA 300.0
05/11/2015 11:55
BGN9034
10
EPA 300.0
05/11/2015 11:55
BGN9034
Vendor Method
V_SHEALY
1
EPA 200.7
05/07/2015 12:26
MHALL3
1
EPA 200.7
05/07/2015 12:26
MHALL3
1
EPA 200.7
05/07/2015 12:26
MHALL3
1
EPA 200.7
05/07/2015 12:26
MHALL3
1
EPA 200.7
05/07/2015 12:26
MHALL3
1
EPA 200.7
05/07/2015 12:26
MHALL3
1
EPA 200.7
05/07/2015 12:26
MHALL3
1
EPA 200.7
05/07/2015 15:52
MHALL3
1
EPA 200.7
05/07/2015 15:52
MHALL3
1
EPA 200.7
05/07/2015 15:52
MHALL3
1
EPA 200.7
05/07/2015 15:52
MHALL3
1
EPA 200.7
05/08/2015 12:41
MHALL3
1
EPA 200.7
05/08/2015 12:41
MHALL3
1
EPA 200.7
05/08/2015 12:41
MHALL3
1
EPA 200.7
05/08/2015 12:41
MHALL3
1
EPA 200.7
05/08/2015 12:41
MHALL3
1
EPA 200.7
05/08/2015 12:41
MHALL3
1
EPA 200.7
05/08/2015 12:41
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050112
Site: S-09
Collection Date: 04-May-15 4:45 PM
Analyte
Result
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
15.7
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
62.3
Nickel (Ni)
1.10
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
55.7
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
66.0
Nickel (Ni)
1.20
Selenium (Se)
< 1
Thallium (TI) Low Level
0.342
Vanadium (V) Low Level
0.656
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
320
Total Carbon
TOC
6.8
TOTAL SUSPENDED SOLIDS
TSS
32
Page 8 of 103
Sample #:
2015013504
Matrix:
GW_WW
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
05/13/2015 17:22
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:22
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:22
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:22
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:22
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:22
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:22
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:22
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:22
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:22
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:22
JAHERMA
ug/L
0.2
1
EPA 200.8
05/13/2015 17:22
JAHERMA
ug/L
0.3
1
EPA 200.8
05/13/2015 17:22
JAHERMA
ug/L
1
1
EPA 200.8
05/15/2015 12:25
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:25
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:25
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:25
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:25
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:25
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:25
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:25
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:25
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:25
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:25
DJSULL1
ug/L
0.2
1
EPA 200.8
05/15/2015 12:25
DJSULL1
ug/L
0.3
1
EPA 200.8
05/15/2015 12:25
DJSULL1
Vendor Method V SHEALY
Vendor Method
V_ELE1
mg/L
25 1 SM2540C
05/07/201510:20 AGIBBS5
mg/L
0.1 1 SM5310C/EPA9060A
05/07/201514:53 GHUTCHI
mg/L
5 1 SM2540D
05/06/2015 08:52 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050112
Site: S-03A
Collection Date: 04-May-15 3:35 PM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.427
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
11
mg/L
1
Sulfate
9.8
mg/L
1
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
Vendor Parameter
Complete
DISSOLVED METALS BY ICP
Aluminum (AI)
0.231
mg/L
0.005
Barium (Ba)
0.033
mg/L
0.005
Boron (B)
0.051
mg/L
0.05
Iron (Fe)
0.771
mg/L
0.01
Manganese (Mn)
0.045
mg/L
0.005
Strontium (Sr)
0.100
mg/L
0.005
Zinc (Zn)
0.006
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
7.65
mg/L
0.01
Magnesium (Mg)
2.59
mg/L
0.005
Potassium (K)
3.25
mg/L
0.1
Sodium (Na)
8.95
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
1.30
mg/L
0.005
Barium (Ba)
0.045
mg/L
0.005
Boron (B)
0.063
mg/L
0.05
Iron (Fe)
2.41
mg/L
0.01
Manganese (Mn)
0.119
mg/L
0.005
Strontium (Sr)
0.118
mg/L
0.005
Zinc (Zn)
0.007
mg/L
0.005
Page 10 of 103
Sample #: 2015013505
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
05/07/2015 11:39
LSTARL1
10
EPA 300.0
05/11/2015 12:13
BGN9034
10
EPA 300.0
05/11/2015 12:13
BGN9034
Vendor Method
V_SHEALY
1
EPA 200.7
05/07/2015 12:37
MHALL3
1
EPA 200.7
05/07/2015 12:37
MHALL3
1
EPA 200.7
05/07/2015 12:37
MHALL3
1
EPA 200.7
05/07/2015 12:37
MHALL3
1
EPA 200.7
05/07/2015 12:37
MHALL3
1
EPA 200.7
05/07/2015 12:37
MHALL3
1
EPA 200.7
05/07/2015 12:37
MHALL3
1
EPA 200.7
05/07/2015 15:41
MHALL3
1
EPA 200.7
05/07/2015 15:41
MHALL3
1
EPA 200.7
05/07/2015 15:41
MHALL3
1
EPA 200.7
05/07/2015 15:41
MHALL3
1
EPA 200.7
05/08/2015 12:45
MHALL3
1
EPA 200.7
05/08/2015 12:45
MHALL3
1
EPA 200.7
05/08/2015 12:45
MHALL3
1
EPA 200.7
05/08/2015 12:45
MHALL3
1
EPA 200.7
05/08/2015 12:45
MHALL3
1
EPA 200.7
05/08/2015 12:45
MHALL3
1
EPA 200.7
05/08/2015 12:45
MHALL3

Certificate of Laboratory Analysis Page 11 of 103
This report shall not be reproduced, except in full.
Order # J15050112
Site: S-03A
Sample #: 2015013505
Collection Date: 04-May-15 3:35 PM
Matrix: GW_WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 17:26
JAHERMA
Arsenic (As)
2.37
ug/L
1
1
EPA 200.8
05/13/2015 17:26
JAHERMA
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 17:26
JAHERMA
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 17:26
JAHERMA
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 17:26
JAHERMA
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 17:26
JAHERMA
Copper (Cu)
1.81
ug/L
1
1
EPA 200.8
05/13/2015 17:26
JAHERMA
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 17:26
JAHERMA
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 17:26
JAHERMA
Nickel (Ni)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 17:26
JAHERMA
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 17:26
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
05/13/2015 17:26
JAHERMA
Vanadium (V) Low Level
0.662
ug/L
0.3
1
EPA 200.8
05/13/2015 17:26
JAHERMA
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 12:43
DJSULL1
Arsenic (As)
5.57
ug/L
1
1
EPA 200.8
05/15/2015 12:43
DJSULL1
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 12:43
DJSULL1
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 12:43
DJSULL1
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 12:43
DJSULL1
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 12:43
DJSULL1
Copper (Cu)
2.24
ug/L
1
1
EPA 200.8
05/15/2015 12:43
DJSULL1
Lead (Pb)
1.49
ug/L
1
1
EPA 200.8
05/15/2015 12:43
DJSULL1
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 12:43
DJSULL1
Nickel (Ni)
1.08
ug/L
1
1
EPA 200.8
05/15/2015 12:43
DJSULL1
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 12:43
DJSULL1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
05/15/2015 12:43
DJSULL1
Vanadium (V) Low Level
2.52
ug/L
0.3
1
EPA 200.8
05/15/2015 12:43
DJSULL1
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
94
mg/L
25
1
SM2540C
05/07/201510:20
AGIBBS5
Total Carbon
TOC
6.9
mg/L
0.1
1
SM5310C/EPA9060A
05/07/201514:53
GHUTCHI
TOTAL SUSPENDED SOLIDS
TSS
25
mg/L
5
1
SM2540D
05/06/2015 08:52
AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050112
Site: S-24
Collection Date: 05-May-15 8:50 AM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.013
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
29
mg/L
1
Sulfate
24
mg/L
1
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
Vendor Parameter
Complete
DISSOLVED METALS BY ICP
Aluminum (AI)
0.021
mg/L
0.005
Barium (Ba)
0.366
mg/L
0.005
Boron (B)
2.14
mg/L
0.05
Iron (Fe)
21.8
mg/L
0.01
Manganese (Mn)
2.07
mg/L
0.005
Strontium (Sr)
4.25
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
115
mg/L
0.1
Magnesium (Mg)
15.9
mg/L
0.005
Potassium (K)
11.0
mg/L
0.1
Sodium (Na)
32.1
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.114
mg/L
0.005
Barium (Ba)
0.403
mg/L
0.005
Boron (B)
2.13
mg/L
0.05
Iron (Fe)
26.1
mg/L
0.01
Manganese (Mn)
2.09
mg/L
0.005
Strontium (Sr)
4.34
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Page 13 of 103
Sample #: 2015013506
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
05/07/2015 11:42
LSTARL1
10
EPA 300.0
05/11/2015 12:31
BGN9034
10
EPA 300.0
05/11/2015 12:31
BGN9034
Vendor Method
V_SHEALY
1
EPA 200.7
05/07/2015 12:30
MHALL3
1
EPA 200.7
05/07/2015 12:30
MHALL3
1
EPA 200.7
05/07/2015 12:30
MHALL3
1
EPA 200.7
05/07/2015 12:30
MHALL3
1
EPA 200.7
05/07/2015 12:30
MHALL3
1
EPA 200.7
05/07/2015 12:30
MHALL3
1
EPA 200.7
05/07/2015 12:30
MHALL3
10
EPA 200.7
05/07/2015 15:01
MHALL3
1
EPA 200.7
05/07/2015 15:01
MHALL3
1
EPA 200.7
05/07/2015 15:01
MHALL3
1
EPA 200.7
05/07/2015 15:01
MHALL3
1
EPA 200.7
05/08/2015 12:49
MHALL3
1
EPA 200.7
05/08/2015 12:49
MHALL3
1
EPA 200.7
05/08/2015 12:49
MHALL3
1
EPA 200.7
05/08/2015 12:49
MHALL3
1
EPA 200.7
05/08/2015 12:49
MHALL3
1
EPA 200.7
05/08/2015 12:49
MHALL3
1
EPA 200.7
05/08/2015 12:49
MHALL3

Certificate of Laboratory Analysis Page 14 of 103
This report shall not be reproduced, except in full.
Order # J15050112
Site: S-24
Sample #: 2015013506
Collection Date: 05-May-15 8:50 AM
Matrix: GW_WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 17:31
JAHERMA
Arsenic (As)
291
ug/L
1
1
EPA 200.8
05/13/2015 17:31
JAHERMA
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 17:31
JAHERMA
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 17:31
JAHERMA
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 17:31
JAHERMA
Cobalt (Co)
6.63
ug/L
1
1
EPA 200.8
05/13/2015 17:31
JAHERMA
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 17:31
JAHERMA
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 17:31
JAHERMA
Molybdenum (Mo)
20.8
ug/L
1
1
EPA 200.8
05/13/2015 17:31
JAHERMA
Nickel (Ni)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 17:31
JAHERMA
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 17:31
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
05/13/2015 17:31
JAHERMA
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
05/13/2015 17:31
JAHERMA
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 12:48
DJSULL1
Arsenic (As)
354
ug/L
1
1
EPA 200.8
05/15/2015 12:48
DJSULL1
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 12:48
DJSULL1
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 12:48
DJSULL1
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 12:48
DJSULL1
Cobalt (Co)
6.94
ug/L
1
1
EPA 200.8
05/15/2015 12:48
DJSULL1
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 12:48
DJSULL1
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 12:48
DJSULL1
Molybdenum (Mo)
22.2
ug/L
1
1
EPA 200.8
05/15/2015 12:48
DJSULL1
Nickel (Ni)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 12:48
DJSULL1
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 12:48
DJSULL1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
05/15/2015 12:48
DJSULL1
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
05/15/2015 12:48
DJSULL1
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
470
mg/L
25
1
SM2540C
05/11/201514:40
AGIBBS5
Total Carbon
TOC
1.8
mg/L
0.1
1
SM5310C/EPA9060A
05/07/201514:53
GHUTCHI
TOTAL SUSPENDED SOLIDS
TSS
78
mg/L
5
1
SM2540D
05/11/201511:28
AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050112
Site: S-06
Collection Date: 05-May-15 9:45 AM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.013
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
11
mg/L
1
Sulfate
5.1
mg/L
0.1
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
Vendor Parameter
Complete
DISSOLVED METALS BY ICP
Aluminum (AI)
0.597
mg/L
0.005
Barium (Ba)
0.041
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
2.14
mg/L
0.01
Manganese (Mn)
0.061
mg/L
0.005
Strontium (Sr)
0.028
mg/L
0.005
Zinc (Zn)
0.022
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
2.84
mg/L
0.01
Magnesium (Mg)
1.74
mg/L
0.005
Potassium (K)
5.58
mg/L
0.1
Sodium (Na)
6.03
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
1.22
mg/L
0.005
Barium (Ba)
0.048
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
3.60
mg/L
0.01
Manganese (Mn)
0.064
mg/L
0.005
Strontium (Sr)
0.030
mg/L
0.005
Zinc (Zn)
0.011
mg/L
0.005
Page 16 of 103
Sample #: 2015013507
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
05/07/2015 11:44
LSTARL1
10
EPA 300.0
05/11/2015 14:54
BGN9034
1
EPA 300.0
05/11/2015 14:54
BGN9034
Vendor Method
V_SHEALY
1
EPA 200.7
05/07/2015 13:23
MHALL3
1
EPA 200.7
05/07/2015 13:23
MHALL3
1
EPA 200.7
05/07/2015 13:23
MHALL3
1
EPA 200.7
05/07/2015 13:23
MHALL3
1
EPA 200.7
05/07/2015 13:23
MHALL3
1
EPA 200.7
05/07/2015 13:23
MHALL3
1
EPA 200.7
05/07/2015 13:23
MHALL3
1
EPA 200.7
05/07/2015 15:45
MHALL3
1
EPA 200.7
05/07/2015 15:45
MHALL3
1
EPA 200.7
05/07/2015 15:45
MHALL3
1
EPA 200.7
05/07/2015 15:45
MHALL3
1
EPA 200.7
05/08/2015 12:53
MHALL3
1
EPA 200.7
05/08/2015 12:53
MHALL3
1
EPA 200.7
05/08/2015 12:53
MHALL3
1
EPA 200.7
05/08/2015 12:53
MHALL3
1
EPA 200.7
05/08/2015 12:53
MHALL3
1
EPA 200.7
05/08/2015 12:53
MHALL3
1
EPA 200.7
05/08/2015 12:53
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050112
Site: S-06
Collection Date: 05-May-15 9:45 AM
Analyte
Result
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
1.14
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
1.09
Cobalt (Co)
1.02
Copper (Cu)
1.24
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
1.00
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
1.48
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
1.34
Cobalt (Co)
1.23
Copper (Cu)
1.45
Lead (Pb)
1.80
Molybdenum (Mo)
< 1
Nickel (Ni)
1.09
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
2.18
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
130
Total Carbon
TOC
19
TOTAL SUSPENDED SOLIDS
TSS
23
Page 17 of 103
Sample #:
2015013507
Matrix:
GW_WW
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
05/13/2015 17:35
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:35
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:35
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:35
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:35
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:35
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:35
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:35
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:35
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:35
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:35
JAHERMA
ug/L
0.2
1
EPA 200.8
05/13/2015 17:35
JAHERMA
ug/L
0.3
1
EPA 200.8
05/13/2015 17:35
JAHERMA
ug/L
1
1
EPA 200.8
05/15/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:52
DJSULL1
ug/L
0.2
1
EPA 200.8
05/15/2015 12:52
DJSULL1
ug/L
0.3
1
EPA 200.8
05/15/2015 12:52
DJSULL1
Vendor Method
V_SHEALY
mg/L
mg/L
mg/L
Vendor Method V_ELE1
41.7 1 SM2540C 05/11/201514:40 AGIBBS5
1
5
10 SM5310C/EPA9060A 05/07/201514:53 GHUTCHI
1 SM2540D 05/11/201511:28 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050112
Site: S-01
Collection Date: 05-May-15 10:25 AM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.014
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
13
mg/L
1
Sulfate
9.7
mg/L
1
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
Vendor Parameter
Complete
DISSOLVED METALS BY ICP
Aluminum (AI)
0.264
mg/L
0.005
Barium (Ba)
0.081
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
3.15
mg/L
0.01
Manganese (Mn)
0.044
mg/L
0.005
Strontium (Sr)
0.056
mg/L
0.005
Zinc (Zn)
0.196
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
4.03
mg/L
0.01
Magnesium (Mg)
2.34
mg/L
0.005
Potassium (K)
3.50
mg/L
0.1
Sodium (Na)
7.33
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.430
mg/L
0.005
Barium (Ba)
0.087
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
5.61
mg/L
0.01
Manganese (Mn)
0.045
mg/L
0.005
Strontium (Sr)
0.059
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Page 19 of 103
Sample #: 2015013508
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
05/07/2015 11:45
LSTARL1
10
EPA 300.0
05/11/2015 13:07
BGN9034
10
EPA 300.0
05/11/2015 13:07
BGN9034
Vendor Method
V_SHEALY
1
EPA 200.7
05/07/2015 13:15
MHALL3
1
EPA 200.7
05/07/2015 13:15
MHALL3
1
EPA 200.7
05/07/2015 13:15
MHALL3
1
EPA 200.7
05/07/2015 13:15
MHALL3
1
EPA 200.7
05/07/2015 13:15
MHALL3
1
EPA 200.7
05/07/2015 13:15
MHALL3
1
EPA 200.7
05/07/2015 13:15
MHALL3
1
EPA 200.7
05/07/2015 16:07
MHALL3
1
EPA 200.7
05/07/2015 16:07
MHALL3
1
EPA 200.7
05/07/2015 16:07
MHALL3
1
EPA 200.7
05/07/2015 16:07
MHALL3
1
EPA 200.7
05/08/2015 12:57
MHALL3
1
EPA 200.7
05/08/2015 12:57
MHALL3
1
EPA 200.7
05/08/2015 12:57
MHALL3
1
EPA 200.7
05/08/2015 12:57
MHALL3
1
EPA 200.7
05/08/2015 12:57
MHALL3
1
EPA 200.7
05/08/2015 12:57
MHALL3
1
EPA 200.7
05/08/2015 12:57
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050112
Site: S-01
Collection Date: 05-May-15 10:25 AM
Analyte
Result
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
0.833
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
1.70
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
79
Total Carbon
TOC
11
TOTAL SUSPENDED SOLIDS
TSS
38
Page 20 of 103
Sample #:
2015013508
Matrix:
GW_WW
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
05/13/2015 17:58
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:58
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:58
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:58
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:58
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:58
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:58
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:58
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:58
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:58
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 17:58
JAHERMA
ug/L
0.2
1
EPA 200.8
05/13/2015 17:58
JAHERMA
ug/L
0.3
1
EPA 200.8
05/13/2015 17:58
JAHERMA
ug/L
1
1
EPA 200.8
05/15/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 12:57
DJSULL1
ug/L
0.2
1
EPA 200.8
05/15/2015 12:57
DJSULL1
ug/L
0.3
1
EPA 200.8
05/15/2015 12:57
DJSULL1
Vendor Method V SHEALY
Vendor Method
V_ELE1
mg/L
25 1 SM2540C
05/11/201514:40 AGIBBS5
mg/L
1 10 SM5310C/EPA9060A
05/07/201514:53 GHUTCHI
mg/L
6.1 1 SM2540D
05/11/201511:28 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050112
Site: ASW-BG
Collection Date: 05-May-15 11:15 AM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.022
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
8.5
mg/L
0.1
Sulfate
2.4
mg/L
0.1
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
Vendor Parameter
Complete
DISSOLVED METALS BY ICP
Aluminum (AI)
0.270
mg/L
0.005
Barium (Ba)
0.047
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
1.32
mg/L
0.01
Manganese (Mn)
0.039
mg/L
0.005
Strontium (Sr)
0.029
mg/L
0.005
Zinc (Zn)
0.016
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
2.43
mg/L
0.01
Magnesium (Mg)
2.00
mg/L
0.005
Potassium (K)
2.81
mg/L
0.1
Sodium (Na)
2.80
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.319
mg/L
0.005
Barium (Ba)
0.049
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
1.72
mg/L
0.01
Manganese (Mn)
0.040
mg/L
0.005
Strontium (Sr)
0.029
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Page 22 of 103
Sample #: 2015013509
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2
05/07/2015 11:46
LSTARL1
1 EPA 300.0
05/11/2015 15:12
BGN9034
1 EPA 300.0
05/11/2015 15:12
BGN9034
Vendor Method
V_SHEALY
1 EPA 200.7
05/07/2015 12:22
MHALL3
1 EPA 200.7
05/07/2015 12:22
MHALL3
1 EPA 200.7
05/07/2015 12:22
MHALL3
1 EPA 200.7
05/07/2015 12:22
MHALL3
1 EPA 200.7
05/07/2015 12:22
MHALL3
1 EPA 200.7
05/07/2015 12:22
MHALL3
1 EPA 200.7
05/07/2015 12:22
MHALL3
1 EPA 200.7
05/07/2015 14:07
MHALL3
1 EPA 200.7
05/07/2015 14:07
MHALL3
1 EPA 200.7
05/07/2015 14:07
MHALL3
1 EPA 200.7
05/07/2015 14:07
MHALL3
1 EPA 200.7
05/08/2015 13:00
MHALL3
1 EPA 200.7
05/08/2015 13:00
MHALL3
1 EPA 200.7
05/08/2015 13:00
MHALL3
1 EPA 200.7
05/08/2015 13:00
MHALL3
1 EPA 200.7
05/08/2015 13:00
MHALL3
1 EPA 200.7
05/08/2015 13:00
MHALL3
1 EPA 200.7
05/08/2015 13:00
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050112
Site: ASW-BG
Collection Date: 05-May-15 11:15 AM
Analyte
Result
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
0.644
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
67
Total Carbon
TOC
17
TOTAL SUSPENDED SOLIDS
TSS
8.0
Page 23 of 103
Sample #:
2015013509
Matrix:
GW_WW
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
05/13/2015 18:12
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:12
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:12
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:12
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:12
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:12
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:12
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:12
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:12
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:12
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:12
JAHERMA
ug/L
0.2
1
EPA 200.8
05/13/2015 18:12
JAHERMA
ug/L
0.3
1
EPA 200.8
05/13/2015 18:12
JAHERMA
ug/L
1
1
EPA 200.8
05/15/2015 13:01
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:01
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:01
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:01
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:01
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:01
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:01
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:01
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:01
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:01
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:01
DJSULL1
ug/L
0.2
1
EPA 200.8
05/15/2015 13:01
DJSULL1
ug/L
0.3
1
EPA 200.8
05/15/2015 13:01
DJSULL1
Vendor Method V SHEALY
Vendor Method
V_ELE1
mg/L
25 1 SM2540C
05/11/201514:40 AGIBBS5
mg/L
1 10 SM5310C/EPA9060A
05/07/201514:53 GHUTCHI
mg/L
5 1 SM2540D
05/11/201511:28 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050112
Site: S-15
Collection Date: 05-May-15 1:55 PM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
1.3
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
9.8
mg/L
1
Sulfate
9.1
mg/L
0.1
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
Vendor Parameter
Complete
DISSOLVED METALS BY ICP
Aluminum (AI)
0.329
mg/L
0.005
Barium (Ba)
0.088
mg/L
0.005
Boron (B)
0.075
mg/L
0.05
Iron (Fe)
2.51
mg/L
0.01
Manganese (Mn)
0.122
mg/L
0.005
Strontium (Sr)
0.157
mg/L
0.005
Zinc (Zn)
0.013
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
9.70
mg/L
0.01
Magnesium (Mg)
3.50
mg/L
0.005
Potassium (K)
3.97
mg/L
0.1
Sodium (Na)
5.70
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.658
mg/L
0.005
Barium (Ba)
0.095
mg/L
0.005
Boron (B)
0.073
mg/L
0.05
Iron (Fe)
3.41
mg/L
0.01
Manganese (Mn)
0.125
mg/L
0.005
Strontium (Sr)
0.161
mg/L
0.005
Zinc (Zn)
0.007
mg/L
0.005
Page 25 of 103
Sample #: 2015013510
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
05/07/2015 11:47
LSTARL1
10
EPA 300.0
05/11/2015 15:29
BGN9034
1
EPA 300.0
05/11/2015 15:29
BGN9034
Vendor Method
V_SHEALY
1
EPA 200.7
05/07/2015 13:19
MHALL3
1
EPA 200.7
05/07/2015 13:19
MHALL3
1
EPA 200.7
05/07/2015 13:19
MHALL3
1
EPA 200.7
05/07/2015 13:19
MHALL3
1
EPA 200.7
05/07/2015 13:19
MHALL3
1
EPA 200.7
05/07/2015 13:19
MHALL3
1
EPA 200.7
05/07/2015 13:19
MHALL3
1
EPA 200.7
05/07/2015 15:13
MHALL3
1
EPA 200.7
05/07/2015 15:13
MHALL3
1
EPA 200.7
05/07/2015 15:13
MHALL3
1
EPA 200.7
05/07/2015 15:13
MHALL3
1
EPA 200.7
05/08/2015 13:04
MHALL3
1
EPA 200.7
05/08/2015 13:04
MHALL3
1
EPA 200.7
05/08/2015 13:04
MHALL3
1
EPA 200.7
05/08/2015 13:04
MHALL3
1
EPA 200.7
05/08/2015 13:04
MHALL3
1
EPA 200.7
05/08/2015 13:04
MHALL3
1
EPA 200.7
05/08/2015 13:04
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050112
Site: S-15
Collection Date: 05-May-15 1:55 PM
Analyte
Result
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
2.08
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
1.83
Copper (Cu)
1.10
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
1.25
Selenium (Se)
3.37
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
0.567
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
2.31
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
2.07
Copper (Cu)
1.22
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
1.40
Selenium (Se)
3.25
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
1.27
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
100
Total Carbon
TOC
14
TOTAL SUSPENDED SOLIDS
TSS
12
Page 26 of 103
Sample #:
2015013510
Matrix:
GW_WW
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
05/13/2015 18:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:17
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:17
JAHERMA
ug/L
0.2
1
EPA 200.8
05/13/2015 18:17
JAHERMA
ug/L
0.3
1
EPA 200.8
05/13/2015 18:17
JAHERMA
ug/L
1
1
EPA 200.8
05/15/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:06
DJSULL1
ug/L
0.2
1
EPA 200.8
05/15/2015 13:06
DJSULL1
ug/L
0.3
1
EPA 200.8
05/15/2015 13:06
DJSULL1
Vendor Method V SHEALY
Vendor Method
V_ELE1
mg/L
25 1 SM2540C
05/11/201514:40 AGIBBS5
mg/L
1 10 SM5310C/EPA9060A
05/07/201514:53 GHUTCHI
mg/L
5 1 SM2540D
05/11/201511:28 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050112
Site: S-14
Collection Date: 05-May-15 2:45 PM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
2.4
mg-N/L
0.1
INORGANIC IONS BY IC
Chloride
10
mg/L
1
Sulfate
6.4
mg/L
0.1
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
Vendor Parameter
Complete
DISSOLVED METALS BY ICP
Aluminum (AI)
0.456
mg/L
0.005
Barium (Ba)
0.096
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.568
mg/L
0.01
Manganese (Mn)
0.036
mg/L
0.005
Strontium (Sr)
0.037
mg/L
0.005
Zinc (Zn)
0.016
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
5.14
mg/L
0.01
Magnesium (Mg)
2.83
mg/L
0.005
Potassium (K)
4.46
mg/L
0.1
Sodium (Na)
4.73
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.791
mg/L
0.005
Barium (Ba)
0.102
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.897
mg/L
0.01
Manganese (Mn)
0.036
mg/L
0.005
Strontium (Sr)
0.037
mg/L
0.005
Zinc (Zn)
0.007
mg/L
0.005
Page 28 of 103
Sample #: 2015013511
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
10
EPA 353.2
05/07/2015 13:15
LSTARL1
10
EPA 300.0
05/11/2015 15:47
BGN9034
1
EPA 300.0
05/11/2015 15:47
BGN9034
Vendor Method
V_SHEALY
1
EPA 200.7
05/07/2015 12:34
MHALL3
1
EPA 200.7
05/07/2015 12:34
MHALL3
1
EPA 200.7
05/07/2015 12:34
MHALL3
1
EPA 200.7
05/07/2015 12:34
MHALL3
1
EPA 200.7
05/07/2015 12:34
MHALL3
1
EPA 200.7
05/07/2015 12:34
MHALL3
1
EPA 200.7
05/07/2015 12:34
MHALL3
1
EPA 200.7
05/07/2015 15:28
MHALL3
1
EPA 200.7
05/07/2015 15:28
MHALL3
1
EPA 200.7
05/07/2015 15:28
MHALL3
1
EPA 200.7
05/07/2015 15:28
MHALL3
1
EPA 200.7
05/08/2015 13:16
MHALL3
1
EPA 200.7
05/08/2015 13:16
MHALL3
1
EPA 200.7
05/08/2015 13:16
MHALL3
1
EPA 200.7
05/08/2015 13:16
MHALL3
1
EPA 200.7
05/08/2015 13:16
MHALL3
1
EPA 200.7
05/08/2015 13:16
MHALL3
1
EPA 200.7
05/08/2015 13:16
MHALL3

Certificate of Laboratory Analysis Page 29 of 103
This report shall not be reproduced, except in full.
Order # J15050112
Site: S-14
Sample #: 2015013511
Collection Date: 05-May-15 2:45 PM
Matrix: GW_WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 18:21
JAHERMA
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 18:21
JAHERMA
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 18:21
JAHERMA
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 18:21
JAHERMA
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 18:21
JAHERMA
Cobalt (Co)
1.25
ug/L
1
1
EPA 200.8
05/13/2015 18:21
JAHERMA
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 18:21
JAHERMA
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 18:21
JAHERMA
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 18:21
JAHERMA
Nickel (Ni)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 18:21
JAHERMA
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 18:21
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
05/13/2015 18:21
JAHERMA
Vanadium (V) Low Level
0.596
ug/L
0.3
1
EPA 200.8
05/13/2015 18:21
JAHERMA
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 13:11
DJSULL1
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 13:11
DJSULL1
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 13:11
DJSULL1
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 13:11
DJSULL1
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 13:11
DJSULL1
Cobalt (Co)
1.54
ug/L
1
1
EPA 200.8
05/15/2015 13:11
DJSULL1
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 13:11
DJSULL1
Lead (Pb)
1.16
ug/L
1
1
EPA 200.8
05/15/2015 13:11
DJSULL1
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 13:11
DJSULL1
Nickel (Ni)
1.03
ug/L
1
1
EPA 200.8
05/15/2015 13:11
DJSULL1
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 13:11
DJSULL1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
05/15/2015 13:11
DJSULL1
Vanadium (V) Low Level
1.12
ug/L
0.3
1
EPA 200.8
05/15/2015 13:11
DJSULL1
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
84
mg/L
25
1
SM2540C
05/11/201514:40
AGIBBS5
Total Carbon
TOC
12
mg/L
1
10
SM5310C/EPA9060A
05/07/201514:53
GHUTCHI
TOTAL SUSPENDED SOLIDS
TSS
15
mg/L
5
1
SM2540D
05/11/201511:28
AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050112
Site: S-14 Dup
Collection Date: 05-May-15 3:00 PM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
2.4
mg-N/L
0.1
INORGANIC IONS BY IC
Chloride
10
mg/L
1
Sulfate
6.9
mg/L
0.1
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
Vendor Parameter
Complete
DISSOLVED METALS BY ICP
Aluminum (AI)
0.441
mg/L
0.005
Barium (Ba)
0.094
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.551
mg/L
0.01
Manganese (Mn)
0.035
mg/L
0.005
Strontium (Sr)
0.037
mg/L
0.005
Zinc (Zn)
0.018
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
5.15
mg/L
0.01
Magnesium (Mg)
2.84
mg/L
0.005
Potassium (K)
4.45
mg/L
0.1
Sodium (Na)
4.71
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.861
mg/L
0.005
Barium (Ba)
0.104
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.913
mg/L
0.01
Manganese (Mn)
0.037
mg/L
0.005
Strontium (Sr)
0.038
mg/L
0.005
Zinc (Zn)
0.009
mg/L
0.005
Page 31 of 103
Sample #: 2015013512
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
10
EPA 353.2
05/07/2015 13:16
LSTARL1
10
EPA 300.0
05/11/2015 16:05
BGN9034
1
EPA 300.0
05/11/2015 16:05
BGN9034
Vendor Method
V_SHEALY
1
EPA 200.7
05/07/2015 13:35
MHALL3
1
EPA 200.7
05/07/2015 13:35
MHALL3
1
EPA 200.7
05/07/2015 13:35
MHALL3
1
EPA 200.7
05/07/2015 13:35
MHALL3
1
EPA 200.7
05/07/2015 13:35
MHALL3
1
EPA 200.7
05/07/2015 13:35
MHALL3
1
EPA 200.7
05/07/2015 13:35
MHALL3
1
EPA 200.7
05/07/2015 15:56
MHALL3
1
EPA 200.7
05/07/2015 15:56
MHALL3
1
EPA 200.7
05/07/2015 15:56
MHALL3
1
EPA 200.7
05/07/2015 15:56
MHALL3
1
EPA 200.7
05/08/2015 13:27
MHALL3
1
EPA 200.7
05/08/2015 13:27
MHALL3
1
EPA 200.7
05/08/2015 13:27
MHALL3
1
EPA 200.7
05/08/2015 13:27
MHALL3
1
EPA 200.7
05/08/2015 13:27
MHALL3
1
EPA 200.7
05/08/2015 13:27
MHALL3
1
EPA 200.7
05/08/2015 13:27
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050112
Site: S-14 Dup
Collection Date: 05-May-15 3:00 PM
Analyte
Result
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
1.32
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
1.03
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
0.544
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
1.54
Copper (Cu)
< 1
Lead (Pb)
1.21
Molybdenum (Mo)
< 1
Nickel (Ni)
1.01
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
1.09
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS
84
Total Carbon
TOC
12
TOTAL SUSPENDED SOLIDS
TSS
7.0
Page 32 of 103
Sample #:
2015013512
Matrix:
GW_WW
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
05/13/2015 18:26
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:26
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:26
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:26
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:26
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:26
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:26
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:26
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:26
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:26
JAHERMA
ug/L
1
1
EPA 200.8
05/13/2015 18:26
JAHERMA
ug/L
0.2
1
EPA 200.8
05/13/2015 18:26
JAHERMA
ug/L
0.3
1
EPA 200.8
05/13/2015 18:26
JAHERMA
ug/L
1
1
EPA 200.8
05/15/2015 13:37
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:37
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:37
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:37
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:37
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:37
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:37
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:37
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:37
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:37
DJSULL1
ug/L
1
1
EPA 200.8
05/15/2015 13:37
DJSULL1
ug/L
0.2
1
EPA 200.8
05/15/2015 13:37
DJSULL1
ug/L
0.3
1
EPA 200.8
05/15/2015 13:37
DJSULL1
Vendor Method V SHEALY
Vendor Method
V_ELE1
mg/L
25 1 SM2540C
05/11/201514:40 AGIBBS5
mg/L
1 10 SM5310C/EPA9060A
05/07/201514:53 GHUTCHI
mg/L
5 1 SM2540D
05/11/201511:28 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050112
Site: ISW-HMBREF
Collection Date: 05-May-15 3:50 PM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter
Complete
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)
0.087
mg-N/L
0.01
INORGANIC IONS BY IC
Chloride
9.7
mg/L
1
Sulfate
3.9
mg/L
0.1
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
Vendor Parameter
Complete
DISSOLVED METALS BY ICP
Aluminum (AI)
0.291
mg/L
0.005
Barium (Ba)
0.070
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.989
mg/L
0.01
Manganese (Mn)
0.036
mg/L
0.005
Strontium (Sr)
0.034
mg/L
0.005
Zinc (Zn)
0.017
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
3.87
mg/L
0.01
Magnesium (Mg)
2.27
mg/L
0.005
Potassium (K)
2.81
mg/L
0.1
Sodium (Na)
5.04
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.603
mg/L
0.005
Barium (Ba)
0.077
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
2.01
mg/L
0.01
Manganese (Mn)
0.037
mg/L
0.005
Strontium (Sr)
0.035
mg/L
0.005
Zinc (Zn)
0.006
mg/L
0.005
Page 34 of 103
Sample #: 2015013513
Matrix: GW_WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
05/07/2015 11:51
LSTARL1
10
EPA 300.0
05/12/2015 14:20
BGN9034
1
EPA 300.0
05/12/2015 14:20
BGN9034
Vendor Method
V_SHEALY
1
EPA 200.7
05/07/2015 13:27
MHALL3
1
EPA 200.7
05/07/2015 13:27
MHALL3
1
EPA 200.7
05/07/2015 13:27
MHALL3
1
EPA 200.7
05/07/2015 13:27
MHALL3
1
EPA 200.7
05/07/2015 13:27
MHALL3
1
EPA 200.7
05/07/2015 13:27
MHALL3
1
EPA 200.7
05/07/2015 13:27
MHALL3
1
EPA 200.7
05/07/2015 15:48
MHALL3
1
EPA 200.7
05/07/2015 15:48
MHALL3
1
EPA 200.7
05/07/2015 15:48
MHALL3
1
EPA 200.7
05/07/2015 15:48
MHALL3
1
EPA 200.7
05/08/2015 13:31
MHALL3
1
EPA 200.7
05/08/2015 13:31
MHALL3
1
EPA 200.7
05/08/2015 13:31
MHALL3
1
EPA 200.7
05/08/2015 13:31
MHALL3
1
EPA 200.7
05/08/2015 13:31
MHALL3
1
EPA 200.7
05/08/2015 13:31
MHALL3
1
EPA 200.7
05/08/2015 13:31
MHALL3

Certificate of Laboratory Analysis Page 35 of 103
This report shall not be reproduced, except in full.
Order # J15050112
Site: ISW-HMBREF
Sample #: 2015013513
Collection Date: 05-May-15 3:50 PM
Matrix: GW_WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 18:30
JAHERMA
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 18:30
JAHERMA
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 18:30
JAHERMA
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 18:30
JAHERMA
Chromium (Cr)
1.00
ug/L
1
1
EPA 200.8
05/13/2015 18:30
JAHERMA
Cobalt (Co)
1.26
ug/L
1
1
EPA 200.8
05/13/2015 18:30
JAHERMA
Copper (Cu)
1.18
ug/L
1
1
EPA 200.8
05/13/2015 18:30
JAHERMA
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 18:30
JAHERMA
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 18:30
JAHERMA
Nickel (Ni)
1.12
ug/L
1
1
EPA 200.8
05/13/2015 18:30
JAHERMA
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
05/13/2015 18:30
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
05/13/2015 18:30
JAHERMA
Vanadium (V) Low Level
0.469
ug/L
0.3
1
EPA 200.8
05/13/2015 18:30
JAHERMA
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 13:51
DJSULL1
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 13:51
DJSULL1
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 13:51
DJSULL1
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 13:51
DJSULL1
Chromium (Cr)
1.23
ug/L
1
1
EPA 200.8
05/15/2015 13:51
DJSULL1
Cobalt (Co)
1.32
ug/L
1
1
EPA 200.8
05/15/2015 13:51
DJSULL1
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 13:51
DJSULL1
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 13:51
DJSULL1
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 13:51
DJSULL1
Nickel (Ni)
1.18
ug/L
1
1
EPA 200.8
05/15/2015 13:51
DJSULL1
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
05/15/2015 13:51
DJSULL1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
05/15/2015 13:51
DJSULL1
Vanadium (V) Low Level
1.57
ug/L
0.3
1
EPA 200.8
05/15/2015 13:51
DJSULL1
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
79
mg/L
25
1
SM2540C
05/11/201514:40
AGIBBS5
Total Carbon
TOC
17
mg/L
1
10
SM5310C/EPA9060A
05/11/201515:29
TJA7067
TOTAL SUSPENDED SOLIDS
TSS
7.0
mg/L
5.6
1
SM2540D
05/11/201511:28
AGIBBS5

Certificate of Laboratory Analysis Page 37 of 103
This report shall not be reproduced, except in full.
Order # J15050112
Site: Filter Blank
Collection Date:
Analyte
Result
Units
Qualifiers RDL
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
DISSOLVED METALS BY ICP-MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015013514
Matrix: GW WW
DF
Method
Analysis Date/Time
Analyst
1
EPA 245.1
05/12/2015 12:53
ACPAYNE
1
EPA 200.7
05/07/2015 13:38
MHALL3
1
EPA 200.7
05/07/2015 13:38
MHALL3
1
EPA 200.7
05/07/2015 13:38
MHALL3
1
EPA 200.7
05/07/2015 13:38
MHALL3
1
EPA 200.7
05/07/2015 13:38
MHALL3
1
EPA 200.7
05/07/2015 13:38
MHALL3
1
EPA 200.7
05/07/2015 13:38
MHALL3
1
EPA 200.8
05/13/2015 18:35
JAHERMA
1
EPA 200.8
05/13/2015 18:35
JAHERMA
1
EPA 200.8
05/13/2015 18:35
JAHERMA
1
EPA 200.8
05/13/2015 18:35
JAHERMA
1
EPA 200.8
05/13/2015 18:35
JAHERMA
1
EPA 200.8
05/13/2015 18:35
JAHERMA
1
EPA 200.8
05/13/2015 18:35
JAHERMA
1
EPA 200.8
05/13/2015 18:35
JAHERMA
1
EPA 200.8
05/13/2015 18:35
JAHERMA
1
EPA 200.8
05/13/2015 18:35
JAHERMA
1
EPA 200.8
05/13/2015 18:35
JAHERMA
1
EPA 200.8
05/13/2015 18:35
JAHERMA
1
EPA 200.8
05/13/2015 18:35
JAHERMA

Certificate of Laboratory Analysis Page 38 of 103
This report shall not be reproduced, except in full.
Order # J15050112
Site: Field Blank
Collection Date:
Analyte Result Units Qualifiers RDL DF
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete
Sample #: 2015013515
Matrix: GW WW
Method Analysis Date/Time Analyst
Vendor Method V_SHEALY

Certificate of Laboratory Analysis Page 39 of 103
This report shall not be reproduced, except in full.
Order # J15050112
Site: Trip Blank
Collection Date:
Analyte Result Units Qualifiers RDL DF
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete
Sample #: 2015013516
Matrix: GW WW
Method Analysis Date/Time Analyst
Vendor Method V_SHEALY

Page 40 of 103
Eernent One Inc.
6319-D Carolina Beach Rd.
Wilmington, NC 28412
Rhone: 910 793-0128
Fax: [phone]
el lab@el lab corn
ntOne
REPORT OF ANALYSES
Duke Energy
May 8, 2015
Laboratory Services
Client Project
Name
AB
GW Assessment
Surface
13339 Hagers Ferry Road Bld. MG03A
water — Synterra Lee Plant
Huntersvilie, NC 28078
Client Project Number
J15050112
PO Number
Sample Matrix GW WW
Sample Type
Grab
Date Received
05/07/2015
Date Analyzed 05/07/2015
Method
SM 4500 S2- D
Time
Received
1100
Delivered by FedEx
Received by
LLB
eOne ID Duke Energy ID
Parameter
Result Unit
Dil
DL
Date
Time
Sampled
Sampled
24694-1 S-04
Sulfide
< 0.1 mg/L
1
0.1
05/04/15
1430
24694-2* S-09
Sulfide
< 0.5 mg/L
5
0.1
05/04/15
1645
24694-3* S-03A
Sulfide
< 0.2 mg/L
2
0.1
05/04/15
1535
24694-4 S-24
Sulfide
< 0.1 mg/L
1
0.1
05/05/15
0850
24694-5 S-06
Sulfide
< 0.1 mg/L
1
0.1
05/05/15
0945
24694-6 S-01
Sulfide
0.387 mg/L
1
0.1
05/05/15
1025
24694-7 ASW-BG
Sulfide
< 0.1 mg/L
1
0.1
05/05/15
1115
24694-8 S-15
Sulfide
< 0.1 mg/L
1
0.1
05/05/15
1355
*Sample spike recovery outside of QA limits of 85-115%; dilution necessary to meet laboratory QA limits.
k-- zlo*�-
IF t Z07�
Ken S ith, Laboratory Director
24694 Duke Report Packet Compiled by
NC Certifications: DW 37788 and DWQ DENR 604

Page 41 of 103
W
Element One Inc.
6319-D Carolina Beach Rd.
WHmington, NC 28412
Phone: [phone]
Fax: [phone]
el lab@el lab 1-c—
e%0ementOne
REPORT
OF ANALYSES
Duke Energy
May 8, 2015
Laboratory Services
Client Project
Name AB GW Assessment
Surface
13339 Hagers Ferry Road Bld.
MG03A
water — Synterra Lee Plant
Huntersville, NC 28078
Client Project Number J15050112
PO Number
Sample Matrix GW WW
Sample Type
Grab
Date Received
05/07/2015
Date Analyzed 05/07/2015
Method
SM 4500 S2- D
Time Received
1100
Delivered by FedEx
Received by
LLB
eOne ID Duke Energy ID
Parameter
Result Unit
Dil DL Date
Time
Sampled
Sampled
24694-9 S-14
Sulfide
< 0.1 mg/L
1 0.1 05/05/15
1445
24694-10 S-14 Dup
Sulfide
< 0.1 mg/L
1 0.1 05/05/15
1500
24694-11 1 SW-HMBREF
Sulfide
< 0.1 mg/L
1 0.1 05/05/15
1550
Ken Smit , Laboratory Director
24694 Duke Report Packet Compiled by�
NC Certifications: DW 37788 and DWQ DENR 604

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eoementOne SAMPLE SUBMISSION FORM Laba[13024694
TAT 7 BD
Hold Time Expiration 05.11.15 @ 1430
Client: Duke Energy
LIMS No J15050112
Project ID Lee
H >9 es No Tem <_ 60C
If No, Record If No, Record
Sample Identification & Collection Information
Analysis Due Date 05.08.15
Report Due Date 05.18.15
Date Rec: 05.07.15
Time Rec: 1100
Rec By LLB
No Ref. Method:
SM4500 S2 D
Lab ID
Client ID
Collection Date
Collection Time
Analysis Requested
1
S-04
05/04/15
1430
1 u fi
2
S-09
05/04/15
1645
ul i
3
S-03A
05/04/15
1535
ulfi
4
S-24
05/05/15
0850
ul i
5
S-06
05/05/15
0945
6
S-01 _
05/05/15
1025
ulfi
7
ASW-BG
05/05/15
1115
ulfi
8
S-15 _
05/05/15
1355
i e
9
S-14
2105/05/15
05/05/15
1445
ulfid
10
S-14 Dup
05/05/15
1500
Ifi
11
1 1 SW-HMBREF
1550
ulfide
NOTE for Sulfide
The MS/MSD spike should approximate 2 to 3 times the sample concentration. If no sulfide detected
at 100 pg/L spike the sample to render the final spike concentration at - 500 pg/L
Lab Communications
All AB Groundwater Assessment jobs need a RL of 0.1
SS Page 1 of 1 Prep By / DateM - 5
SS by Labeled By / Dated
5/7/2015 12: 1:06 PM ID Verification By /Date v Mlv\,

Page 44 of 103
METHOD: S'M 4500 S2- D
ELEMENT ASSAY: Sulfide
_ Date:
5/7/15
Time Analysis Begun
14:10
Time Analysis Ended
16 0S0
Analyst:
KAM
X
Y
ug STD
STD
SOLUTION
ABS
0.00
0.000
1.00
0.099
2.50
0.228
5.00
0.422
7.50
0.612
10.00
0.776
ELEMENT ONE
spectrophotometer
UNITS OF ANSWER
ug/mL
Wave Length 664
DETECTION LIMIT u
1.000
SPK LEYELLuM
5
MAX ALIQUOT
10.00
Na2S•9H2O Lot # STANDARD conc(ppm)
X
40721 Cal Std Lot: Wes. - -It -"
10
QC Std Lot: W C.-2 - -1$ - �(
STD ABSORPTION
Y
u.800
o.�
0�°
0,400411
-
0.2W
zza
-------
--
o.aoo
-o�
-i000
4A0 6.00 8.00 ,O.OD 12M
x
ug PER
ALIQUOT
Sloe 0.077389011
Correlation 0.998682271
SAMPLE
I.D.
SAMP
ABS
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0
Std. B. 1.00
0.100
0.8689
10
10
10
<
86.89%
1
Std. B. 2.50
0.227
2.5864
10
10
10
0.259
103.46%
2.5
Std. B. 5.00
Std. B. 7.50
Std. B. 10.00
0.421
0.612
0.783
5.2102
7.7933
10.1060
10
10
10
10
10
10
10
10
10
0.521
0.779
1.011
104.20%
103.91 %
101.06%
5
7.5
10
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.414
5.1155
10
10
10
0.512
103%
5.0
QC
0.394
4.8450
10
10
10
0.485
5.0
24692-1
0.008
-0.3754
10
10
10
c,p,
24692-1 s k
0.359
4.3717
10
10
10
0.437
87%
5.0
24692-2
0.009
-0.3619
10
10
10
<
24692-2 dup
0.017
-0.2537
10
10
10
<
24692-2 s k
0.285
3.3709
10
10
10
0.337
67%
5.0
24692-3
0.006
-0.4024
10
10
10
< 0
24692-3 s k
0.375
4.5880
10
10
10
0.459
92%
5.0
24692-4
0.003
-0.4430
10
10
10
< 0;1_
24692-4 s k
0.384
4.7098
10
10
10
0.471
94%
5.0
4692-5
0.006
-0.4024
10
10
10
p,
24692-5 s k
0.385
4.7233
10
10
10
0.472
94%
5.0
24692-6
0.006
-0.4024
10
10
10
Q;1
24692-6 s k
0.415
5.1290
10
10
10
0.513
103%
5.0
24693
0.002
-0.4565
10
10
10
Q:1.
24693 s k
0.407
5.0208
10
10
10
0.502
100%
5.0
24694-1
0.007
-0.3889
10
10
10
< 0.1
24694-1 s k
0.371 1
4.5339
10
10
10
0.453
91 %
5.0
24694-2
0.003
-0.4430
10
10
10
<
24694-2 s k
0.317
3.8036
10
10
10
0.380
76%
5.0
Blank
0.000
0.0000
10
10
10
<
QC 0.389
Submitted for QA/QC- I
4.7774 10
Date: 5/7/15
10
By: (Print)
10 0.478
KAM
96% 5.0
(sign):
Page 1 of 3

Page 45 of 103
METHOD:
SM 4500 S2- D
ELEMENT ASSAY:
Sulfide
CLIENT:
Duke
Lab ID#
24692 / 24693 / 24694
Date:
5/7/15
Time Analysis Begun
14:10
Time Analysis Ended
16:50
Analyst:
KAM _
X
Y
ug STD
STD
SOLUTION
ABS
0.00
0.000
1.00
0.099
2.50
0.228
5.00
0.422
7.50
0.612
10.00 0.776
ELEMENT ONE
Wave Length 664 VC I C\J I IVIV L11 11 I U
SPK LEVEL (ug)
MAX ALIQUOT
Na2S•9H2O Lot # STANDARD conc(ppm)
40721 Cal Std Lot: wt.1- -i Sr
P
--���
�, -w
1.000
5
10.00
X
10
Y
�o� I
-- I50
- UU
8W 9.m tOm 12W
x
Slope 0.077389011
Correlation 0.898582271
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0
Std. B. 1.00
0,100
0.8689
10
10
10
<
86.89%
1
Std. B. 2.50
0.227
2.5864
10
10
10
0.259
103.46%
2.5
Std. B. 5.00
0.421
5.2102
10
10
10
0.521
104.20%
5
Std. B. 7.50
0.612
7.7933
10
10
10
0.779
103.91 %
7.5
Std. B. 10.00
0.783
10.1060
10
10
10
1.011
101.06%
10
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.414
5.1155
10
10
10
0.512
103%
5.0
QC
0.394
4.8450
10
10
10
0.485
5.0
24694-3
0.020
-0.2131
10
10
10
<
24694-3 s k
0.346
4.1958
10
10
10
0.420
84%
5.0
24694-4
0.007
-0.3889
10
10
10
<
24694-4 dup
0.010
-0.3483
10
10
10
24694-4 s k
0.373
4.5610
10
10
10
0.456
91 %
5.0
24694-5
0.040
0.0574
10
10
10
24694-5 s k
0.391
4.8044
10
10
10
0.480
96%
5.0
24694-6
0.322
3.8713
10
10
10
4$7,
24694-6 s k
0.691
8.8617
10
10
10
0.886
100%
5.0
24694-7
0.032
-0.0508
10
10
10.p
1�
24694-7 s k
0.429
5.3184
10
10
10
0.532
106%
5.0
24694-8
0.014
-0.2942
10
10
10
24694-8 s k
0.382
4.6827
10
10
10
0.468
94%
5.0
24694-9
0.012
-0.3213
10
10
10
7777Et,1.
24694-9 s k
0.402
4.9532
10
10
10
0.495
99%
5.0
24694-10
0.018
-0.2401
10
10
10
24694-10 s k
0.387
4.7503
10
10
10
0.475
95%
5.0
24694-11
0.011
-0.3348
10
10
10
24694-11 s k
0.404
4.9802
10
10
10
0.498
100%
5.0
Blank
0.000
0.0000 1
10
10
10
<
QC
0.388
4.7639
10
10
10
0.476
95%
5.0
Submitted for QA/QC-
Date: 5/7/15
By: (Print)
KAM
(sign):
Page 2 of 3

Page 46 of 103
METHOD: SM 4500 S2- D
ELEMENT ASSAY: Sulfide
CLIENT: Duke
Lab ID# 24692 / 24693 / 24694
Date: 5/7/15
Time Analysis Begun 14:10
Time Analvsis Ended 16:50
ug STD
STD
)LUTION
ABS
0.00
0.000
1.00
0.099
2.50
0.228
5.00
0.422
7.50
0.612
10.00
0.776
ELEMENT ONE
Spectrophotometer UNITS OF ANSWER
Wave Length 664 DETECTION LIMIT (uo)
SPK LEVEL u
MAX ALIQUOT
Na2S•9H2O Lot # STANDARD conc(ppm)
40721 Cal Std Lot: WQ --71 3
QC Std Lot: WCZ --lg -y
STD ABSORPTION
DAM
0.700
0.�
--..---_.----------
--___--.__---__
- -_-.
0.500
0400
0.000
0.200
338
---_ __--
---- -_-
0100
Il
-._044
- i000
000 800 10.00 12.00
x
SAMPLE
I.D.
Std. B. 0.00
Std. B. 1.00
Std. B. 2.50
Std. B. 5.00
Std. B. 7.50
Std. B. 10.00
SAMP
ABS
0.000
0.100
0.227
0.421
0.612
0.783
ug PER ALI in mL
ALIQUOT ANALYZED
0.0000 10
0.8689 10
2.5864 10
5.2102 10
7.7933 10
10.1060 10
PREP
VOL in mL
10
10
10
10
10
10
Sloe 0.077389011
ALI in mL RESULTS
TAKEN u /mL
10 <
10 <
10 0.259
10 0.521
10 0.779
10 1.011
Correlation 0.998682271
LESS THAN SPIKE
% SPK REC LEVEL
0
86.89% 1
103.46% 2.5
104.20% 5
103.91 % 7.5
161.06% 10
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.414
5.1155
10
10
10
0.512
103%
5.0
QC
0.394
4.8450
10
10
10
0.485
97%
5.0
24692-2
0.010
-0.3483
10
10
5
<
24692-2 s k
0.328
3.9524
10
10
5
0.790
79%
5.0
24694-2
0.006
-0.4024
10
10
5
<
24694-2 s k
0.347
4.2094
10
10
5
0.842
84%
5.0
24694-3.
0.009
-0.3619
10
10
5
24694-3 s k
0.371
4.5339
10
10
5
0.907
91 %
5.0
24692-2
0.001
-0.4700
10
10
2
E 6,
24692-2 dup
0.005
-0.4159
10
10
2
<
24692-2 s k
0.357
4.3446
10
10
2
2.172
87%
5.0
24694-2
0.003
-0.4430
10
10
2;
24694-2 s k
0.382
4.6827
10
10
2
2.341
94%
5.0
purchased std. QC
0.415
5.1290
10
10
10
0.513
103%
5.0
Blank
0.000
0.0000
10
10
10
<
QC 0.385
Submitted for QAIQC-
4.7233 10
Date: 5/7/15
10
By: (Print)
10 0.472
KAM
94% 5.0
(sign) --
Page 3 of 3

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
Project Name: AB GW Assessment Surface Water -Sutton
Project Number:J15050112
Lot Number:QE07084
Date Completed:05/14/2015
Grant Wilton
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
* QE07084*
Shealy Environmental Services, Inc. Page: 1 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Duke Energy
Lot Number: QE07084
Project Name: AB GW Assessment Surface Water -Sutton
Project Number: J15050112
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QE07084
Project Name: AB GW Assessment Surface Water -Sutton
Project Number: J15050112
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
2015013503
Aqueous
05/04/20151430
05/07/2015
002
2015013504
Aqueous
05/04/20151645
05/07/2015
003
2015013505
Aqueous
05/04/20151535
05/07/2015
004
2015013506
Aqueous
05/05/2015 0850
05/07/2015
005
2015013507
Aqueous
05/05/2015 0945
05/07/2015
006
2015013508
Aqueous
05/05/20151025
05/07/2015
007
2015013509
Aqueous
05/05/20151115
05/07/2015
008
2015013510
Aqueous
05/05/20151355
05/07/2015
009
2015013511
Aqueous
05/05/20151445
05/07/2015
010
2015013512
Aqueous
05/05/20151500
05/07/2015
011
2015013513
Aqueous
05/05/20151550
05/07/2015
013
2015013515
Aqueous
05/05/20151445
05/07/2015
014
2015013516
Aqueous
05/05/20151445
05/07/2015
3 samples
Shealy Environmental Services, Inc. Page: 3 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QE07084
Project Name: AB GW Assessment Surface Water -Sutton
Project Number: J15050112
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
2015013503
Aqueous
Alkalinity
SM 2320B-
250
mg/L
5
001
2015013503
Aqueous
Bicarbonate Alkalinity
SM 2320B-
250
mg/L
5
001
2015013503
Aqueous
Methane
RSK - 175
79
ug/L
6
001
2015013503
Aqueous
Mercury (CVAFS)
1631E
0.543
ng/L
7
002
2015013504
Aqueous
Alkalinity
SM 2320B-
190
mg/L
8
002
2015013504
Aqueous
Bicarbonate Alkalinity
SM 2320B-
190
mg/L
8
002
2015013504
Aqueous
Methane
RSK - 175
11
ug/L
9
002
2015013504
Aqueous
Mercury (CVAFS)
1631E
1.94
ng/L
10
003
2015013505
Aqueous
Alkalinity
SM 2320B-
25
mg/L
11
003
2015013505
Aqueous
Bicarbonate Alkalinity
SM 2320B-
25
mg/L
11
003
2015013505
Aqueous
Methane
RSK - 175
19
ug/L
12
003
2015013505
Aqueous
Mercury (CVAFS)
1631E
4.27
ng/L
13
004
2015013506
Aqueous
Alkalinity
SM 2320B-
340
mg/L
14
004
2015013506
Aqueous
Bicarbonate Alkalinity
SM 2320B-
340
mg/L
14
004
2015013506
Aqueous
Methane
RSK - 175
580
ug/L
15
004
2015013506
Aqueous
Mercury (CVAFS)
1631E
0.712
ng/L
16
005
2015013507
Aqueous
Methane
RSK - 175
140
ug/L
18
005
2015013507
Aqueous
Mercury (CVAFS)
1631E
6.05
ng/L
19
006
2015013508
Aqueous
Methane
RSK - 175
160
ug/L
21
006
2015013508
Aqueous
Mercury (CVAFS)
1631E
2.71
ng/L
22
007
2015013509
Aqueous
Methane
RSK - 175
59
ug/L
24
007
2015013509
Aqueous
Mercury (CVAFS)
1631E
1.78
ng/L
25
008
2015013510
Aqueous
Alkalinity
SM 2320B-
21
mg/L
26
008
2015013510
Aqueous
Bicarbonate Alkalinity
SM 2320B-
21
mg/L
26
008
2015013510
Aqueous
Methane
RSK - 175
67
ug/L
27
008
2015013510
Aqueous
Mercury (CVAFS)
1631E
2.44
ng/L
28
009
2015013511
Aqueous
Methane
RSK - 175
41
ug/L
30
009
2015013511
Aqueous
Mercury (CVAFS)
1631E
1.96
ng/L
31
010
2015013512
Aqueous
Methane
RSK - 175
51
ug/L
33
010
2015013512
Aqueous
Mercury (CVAFS)
1631E
1.89
ng/L
34
011
2015013513
Aqueous
Methane
RSK - 175
51
ug/L
36
011
2015013513
Aqueous
Mercury (CVAFS)
1631E
2.24
ng/L
37
(32 detections)
Shealy Environmental Services, Inc. Page: 4 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE07084-001
Description: 2015013503 Matrix: Aqueous
Date Sampled:05/04/2015 1430 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/08/2015 2140
HMA 74435
1
(Bicarbonate ) SM 2320B-2011
1 05/08/2015 2140
HMA 05/08/2015 2140
1
(Carbonate Al) SM 2320B-2011
1 05/08/2015 2140
HMA 05/08/2015 2140
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
250
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
250
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE07084-001
Description: 2015013503 Matrix: Aqueous
Date Sampled:05/04/2015 1430 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/08/2015 2221 JJG 74442
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 79 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QE07084-001
Description: 2015013503 Matrix: Aqueous
Date Sampled:05/04/2015 1430 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 05/13/2015 1805 COH 05/12/2015 1705 74606
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 0.543 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE07084-002
Description: 2015013504 Matrix: Aqueous
Date Sampled:05/04/2015 1645 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/08/2015 2147
HMA 74435
1
(Bicarbonate ) SM 2320B-2011
1 05/08/2015 2147
HMA 05/08/2015 2147
1
(Carbonate Al) SM 2320B-2011
1 05/08/2015 2147
HMA 05/08/2015 2147
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
190
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
190
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 8 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE07084-002
Description: 2015013504 Matrix: Aqueous
Date Sampled:05/04/2015 1645 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/08/2015 2232 JJG 74442
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 11 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QE07084-002
Description: 2015013504 Matrix: Aqueous
Date Sampled:05/04/2015 1645 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 05/13/2015 1819 COH 05/12/2015 1705 74606
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 1.94 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 10 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE07084-003
Description: 2015013505 Matrix: Aqueous
Date Sampled:05/04/2015 1535 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/08/2015 2205
HMA 74435
1
(Bicarbonate ) SM 2320B-2011
1 05/08/2015 2205
HMA 05/08/2015 2205
1
(Carbonate Al) SM 2320B-2011
1 05/08/2015 2205
HMA 05/08/2015 2205
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
25
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
25
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 11 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE07084-003
Description: 2015013505 Matrix: Aqueous
Date Sampled:05/04/2015 1535 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/08/2015 2249 JJG 74442
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 19 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 12 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QE07084-003
Description: 2015013505 Matrix: Aqueous
Date Sampled:05/04/2015 1535 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 05/13/2015 1835 COH 05/12/2015 1705 74606
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 4.27 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 13 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE07084-004
Description: 2015013506 Matrix: Aqueous
Date Sampled:05/05/2015 0850 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/08/2015 2214
HMA 74435
1
(Bicarbonate ) SM 2320B-2011
1 05/08/2015 2214
HMA 05/08/2015 2214
1
(Carbonate Al) SM 2320B-2011
1 05/08/2015 2214
HMA 05/08/2015 2214
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
340
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
340
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 14 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE07084-004
Description: 2015013506 Matrix: Aqueous
Date Sampled:05/05/2015 0850 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/10/2015 1216 DCS 74477
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 580 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 15 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QE07084-004
Description: 2015013506 Matrix: Aqueous
Date Sampled:05/05/2015 0850 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 05/13/2015 1840 COH 05/12/2015 1705 74606
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 0.712 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 16 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE07084-005
Description: 2015013507 Matrix: Aqueous
Date Sampled:05/05/2015 0945 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/08/2015 2219
HMA 74435
1
(Bicarbonate ) SM 2320B-2011
1 05/08/2015 2219
HMA 05/08/2015 2219
1
(Carbonate Al) SM 2320B-2011
1 05/08/2015 2219
HMA 05/08/2015 2219
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 17 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE07084-005
Description: 2015013507 Matrix: Aqueous
Date Sampled:05/05/2015 0945 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/10/2015 1226 DCS 74477
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 140 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 18 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QE07084-005
Description: 2015013507 Matrix: Aqueous
Date Sampled:05/05/2015 0945 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 05/13/2015 1845 COH 05/12/2015 1705 74606
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 6.05 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 19 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE07084-006
Description: 2015013508 Matrix: Aqueous
Date Sampled:05/05/2015 1025 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/08/2015 2224
HMA 74435
1
(Bicarbonate ) SM 2320B-2011
1 05/08/2015 2224
HMA 05/08/2015 2224
1
(Carbonate Al) SM 2320B-2011
1 05/08/2015 2224
HMA 05/08/2015 2224
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 20 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE07084-006
Description: 2015013508 Matrix: Aqueous
Date Sampled:05/05/2015 1025 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/10/2015 1238 DCS 74477
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 160 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 21 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QE07084-006
Description: 2015013508 Matrix: Aqueous
Date Sampled:05/05/2015 1025 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 05/13/2015 1849 COH 05/12/2015 1705 74606
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 2.71 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 22 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE07084-007
Description: 2015013509 Matrix: Aqueous
Date Sampled:05/05/2015 1115 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/08/2015 2228
HMA 74435
1
(Bicarbonate ) SM 2320B-2011
1 05/08/2015 2228
HMA 05/08/2015 2228
1
(Carbonate Al) SM 2320B-2011
1 05/08/2015 2228
HMA 05/08/2015 2228
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 23 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE07084-007
Description: 2015013509 Matrix: Aqueous
Date Sampled:05/05/2015 1115 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/10/2015 1249 DCS 74477
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 59 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 24 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QE07084-007
Description: 2015013509 Matrix: Aqueous
Date Sampled:05/05/2015 1115 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 05/13/2015 1854 COH 05/12/2015 1705 74606
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 1.78 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 25 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE07084-008
Description: 2015013510 Matrix: Aqueous
Date Sampled:05/05/2015 1355 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/08/2015 2244
HMA 74435
1
(Bicarbonate ) SM 2320B-2011
1 05/08/2015 2244
HMA 05/08/2015 2244
1
(Carbonate Al) SM 2320B-2011
1 05/08/2015 2244
HMA 05/08/2015 2244
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
21
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
21
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 26 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE07084-008
Description: 2015013510 Matrix: Aqueous
Date Sampled:05/05/2015 1355 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/10/2015 1308 DCS 74477
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 67 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 27 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QE07084-008
Description: 2015013510 Matrix: Aqueous
Date Sampled:05/05/2015 1355 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 05/13/2015 1859 COH 05/12/2015 1705 74606
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 2.44 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 28 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE07084-009
Description: 2015013511 Matrix: Aqueous
Date Sampled:05/05/2015 1445 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/08/2015 2249
HMA 74435
1
(Bicarbonate ) SM 2320B-2011
1 05/08/2015 2249
HMA 05/08/2015 2249
1
(Carbonate Al) SM 2320B-2011
1 05/08/2015 2249
HMA 05/08/2015 2249
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 29 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE07084-009
Description: 2015013511 Matrix: Aqueous
Date Sampled:05/05/2015 1445 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/10/2015 1318 DCS 74477
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 41 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 30 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QE07084-009
Description: 2015013511 Matrix: Aqueous
Date Sampled:05/05/2015 1445 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 05/13/2015 1903 COH 05/12/2015 1705 74606
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 1.96 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 31 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE07084-010
Description: 2015013512 Matrix: Aqueous
Date Sampled:05/05/2015 1500 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/08/2015 2254
HMA 74435
1
(Bicarbonate ) SM 2320B-2011
1 05/08/2015 2254
HMA 05/08/2015 2254
1
(Carbonate Al) SM 2320B-2011
1 05/08/2015 2254
HMA 05/08/2015 2254
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 32 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE07084-010
Description: 2015013512 Matrix: Aqueous
Date Sampled:05/05/2015 1500 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/10/2015 1328 DCS 74477
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 51 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 33 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QE07084-010
Description: 2015013512 Matrix: Aqueous
Date Sampled:05/05/2015 1500 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 05/13/2015 1908 COH 05/12/2015 1705 74606
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 1.89 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 34 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE07084-011
Description: 2015013513 Matrix: Aqueous
Date Sampled:05/05/2015 1550 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/08/2015 2259
HMA 74435
1
(Bicarbonate ) SM 2320B-2011
1 05/08/2015 2259
HMA 05/08/2015 2259
1
(Carbonate Al) SM 2320B-2011
1 05/08/2015 2259
HMA 05/08/2015 2259
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 35 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE07084-011
Description: 2015013513 Matrix: Aqueous
Date Sampled:05/05/2015 1550 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/10/2015 1338 DCS 74477
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 51 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 36 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QE07084-011
Description: 2015013513 Matrix: Aqueous
Date Sampled:05/05/2015 1550 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 05/13/2015 1913 COH 05/12/2015 1705 74606
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 2.24 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 37 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QE07084-013
Description: 2015013515 Matrix: Aqueous
Date Sampled:05/05/2015 1445 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 05/13/2015 1936 COH 05/12/2015 1705 74606
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury(CVAFS) 7439-97-6 1631E ND 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 38 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QE07084-014
Description: 2015013516 Matrix: Aqueous
Date Sampled:05/05/2015 1445 Project Name: AB GW Assessment Surface
Date Received:05/07/2015 Project Number: J15050112
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 05/13/2015 1940 COH 05/12/2015 1705 74606
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury(CVAFS) 7439-97-6 1631E ND 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 39 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: QE07084
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - Ii
Sample ID: QQ74435-001 Matrix: Aqueous
Batch: 74435
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 05/08/20151937
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE07084
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - LCS
Sample ID: QQ74435-002 Matrix: Aqueous
Batch: 74435
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 94 1 94 90-110 05/08/20151943
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE07084
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MS
Sample ID: QE07084-002MS Matrix: Aqueous
Batch: 74435
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 190 100 250 N 1 66 70-130 05/08/2015 2154
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE07084
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MSD
Sample ID: QE07084-002MD Matrix: Aqueous
Batch: 74435
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Alkalinity 190 100 250 N 1 69 1.0 70-130 20 05/08/2015 2201
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE07084
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ74442-001 Matrix: Aqueous
Batch:74442
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 05/08/20151820
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE07084
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ74442-002 Matrix: Aqueous
Batch:74442
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 120 1 82 70-130 05/08/20151747
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE07084
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ74442-003 Matrix: Aqueous
Batch:74442
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 120 1 80 1.7 70-130 30 05/08/20151803
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE07084
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ74477-001 Matrix: Aqueous
Batch: 74477
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 05/10/20151201
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE07084
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ74477-002 Matrix: Aqueous
Batch: 74477
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 140 1 91 70-130 05/10/20151140
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE07084
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ74477-003 Matrix: Aqueous
Batch: 74477
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 140 1 90 1.6 70-130 30 05/10/20151150
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE07084
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS) - MB
Sample ID: QQ74606-001 Matrix: Aqueous
Batch:74606 Prep Method: 1631E
Analytical Method: 1631E Prep Date: 05/12/2015 1705
Parameter Result Q Dil PQL Units Analysis Date
Mercury (CVAFS) ND 1 0.500 ng/L 05/13/2015 1737
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE07084
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS) - LCS
Sample ID: QQ74606-002 Matrix: Aqueous
Batch:74606 Prep Method: 1631E
Analytical Method: 1631E Prep Date: 05/12/2015 1705
Spike
Amount Result % Rec
Parameter (ng/L) (ng/L) Q Dil % Rec Limit Analysis Date
Mercury (CVAFS) 5.00 5.42 1 108 75-125 05/13/2015 1742
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE07084
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS) - MS
Sample ID: QE07084-001MS
Matrix: Aqueous
Batch:74606
Prep Method: 1631E
Analytical Method: 1631E
Prep Date: 05/12/2015 1705
Sample
Spike
Amount
Amount
Result % Rec
Parameter
(ng/L)
(ng/L)
(ng/L) Q Dil % Rec Limit Analysis Date
Mercury (CVAFS)
0.543
5.00
5.05 1 90 71-125 05/13/2015 1810
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE07084
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS) - MSD
Sample ID: QE07084-001MD
Matrix: Aqueous
Batch:74606
Prep Method: 1631E
Analytical Method: 1631E
Prep Date: 05/12/2015 1705
Sample
Spike
Amount
Amount
Result % Rec % RPD
Parameter
(ng/L)
(ng/L)
(ng/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Mercury (CVAFS)
0.543
5.00
5.35 1 96 5.8 71-125 24 05/13/2015 1814
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE07084
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
S6raly Egiuimnmtnral Scrwicrs; ]nC Fag[ t r3F 1
C]ncuu►� nrTiumber: F-,hfi s 1 G R,¢laces Date: I ],9p7114
D=L3 ae Nurnbrr 17 Efftlfly Dais: O#r'� OJ 5
RcvisLSample Receipt Checklist (S Q
lie;n4: r1�� CoolerInspeetvd bydate; Lot #: � --
�ns vt-remipt: ❑ sF-si ❑ C.liont ❑ LTFS ❑ FedLx ❑ Agborne Exp ❑ Other
❑
No
1. Were custodseal
Eye-5
No
NA
2- if cu!j )dy Ovals were pieserrt, wcrc Lhcy intact and unbrokcn?
CCFDlsr ID/QriOal temperature upon rt-Ceiptoi)erived (corrected) temperaiCtl,tte aponmccipt:
. + L• _ . ) I -mac ,0 F._ rye
eratura lank ❑ Agaimt Bottles ER GtLn ILA:_ IR, Mull Correction Paclor cc -L3 IC
l4iethfld;nc-ool
14ieEhod oact: et Ice ❑ HluItt ❑ Iy ire None
3, iftemperatk= of any cuuler exoetded 6,0T, was Project Manager notified?
❑ A Qr F notified by SRC:, phcane, note (circle erne), other.
Y ❑ t*n
(For coolers roccived aria commercial courier, FMs are. to be notified
im,mediate:l .)
5� No El NA 4- Is the commcrrixl coariar's ackin�* slip ai[rlcited to this form?
Yes No ❑ S. Were Proper custrad pruccdures (lelinquished/received) follt?vred7
Y_, ❑ No E] NA 17 5a Wcre samples relinquished by client to comarmial courier?
'Yes tTo ❑ 6. Were sample IDs listcd on the COC.'
Yes No 7- wc= saniple )Ds listed ern all sample cQUWncm? _
i'e:s 1�To ❑ S_ Was collecriuju date &. time listed flu the COG?
Yes
,
g Was coUccaon date & time listed -0a all Sample containers?
Yes
NO
❑
10- Did all container label infoFT31ation ID date e a t r with runthe COC?
Yes
1
NO
❑
I I. Were tests to be crforialed listed can the COC?
Yes
t~1D ❑
12, Did all s uiY le s Arrive` in the LP 3Titairter fCTi each test?
Yes
No
l3. Did all tnnLaixtens xlmwe in ood coadition unbTr n, lids on, etc, .?
Yes
li9 ❑
l4. Was adcquate sample volume available?
YGS ❑
No
15. W'ere all smVie s received within Yi the h+alding time or 4$ fatiurs, whkheycr
Yes Nc
16- W= 13ny samples containers mtss+n
Yes � iv
17. W there nayexcess =m les not listed o� C-IOC?
AP Yea No I�d}i f
1$. V4'rre bubbl e:�,:�it °' a size'" 6ar fmim in diameter' in an VOA vials
Yes No ❑ NA
1 . Were: all metals &G,STF.M. nuirit�ut salnles rcr:civ'ed at a Hof ��?
Yes Na NA
20- Were au cyanide arxVor Sulfide ram Im received at a H >12?
21,'Were all applicable AIH3oTKN,'cyanide�' eno1(A.2ix L) samples free of
Yes. ❑ No Q '14A
r ideal r lnrint'?
No ❑ NA
22. Were collection tern erarures d ultneated rm the COC for NC seem les?'�y23.
Wwe cliesnt remarksfrequests (i.e. regneacd diludoil,5, MSIMSD designations,
gcEl.
No❑ A'A 5Xctt:.
- - oorrcc#1 transc6hed from the C,OC into die cQmrnent section in LIMS?
No
24- Wan the uoit riumber saved taken from the container label?
SamplPreservation (MTusl becompleted fGr any samples) incorz�ectly preser�ned cr with }readspaoc.}
were rcc4ived incarmi;tly preserved and were adjusted
Samples
accords ] y in sample rcccivin with (H230 ,k1NO3,HCJ.'NaOH) vs - SR #
sample(s)
wore received %vilh bubbles >6 minin di,amacr.
Salon lc(s.
- wine reserved ihith TI C; >0-2 mg1L (if421 is
C ]Drinking V atcr Fr je t 5amp1e(s) pH verified tc be> 2 by Date:
Sam le(s)
were not rcccive d at a pH of <2 and weye adjusted accordingly using SR #
Sam lc labela cl lied b .
Verified by Date;
mments:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

t,HAIN UP- LAJ,> IV U r tSC%+VRV MIYV mlvt`Li l Jr�l r♦ ._._._.___._._.__ _ ._._._. _._._._._._.___._._.
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Dissolved metals: all metals ICP, IMS,Hy V
Page _1_ of ,1_
DISTRIBUTION
ORIGINAL 1:0 LAB, COPY to CL
� Filtered
500 250
HOPE H.PE
0 q-° 1 0 1 , -I
Requested Turnaround
"14 Days f
7 pays
"48 Hr
*Other _ASAP
" Add. Cost Will Apply
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SYNTERRA EDD
Page 103 of 103
4
Totalr 14