NC0003417_J15060003 Report_20150805

+ DUKE Analytical Laboratory
ENERGY
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone:[phone] Fax:[phone]
Order Summary Report
Order Number: J15060003
Project Name: HF LEE PLANT - AB GW ASSESSMENT SOIL
Customer Name(s): Tim Hunsucker, Judd Mahan, Kathy Webb, John Toepfer
Customer Address: 1677 Old Smithfield Rd
Goldsboro NC 27530,
Lab Contact: Margaret Galvin -Karr Phone: [phone]
`\ MXG4644 (101161)
Report Authorized B h` 2015.06.26 14:55:38
p v� U R Y,..-oa�oo� Date:
(Signature)
Margaret Galvin -Karr
Program Comments:
Please contact the Program Manager (Margaret Galvin -Karr) with any questions regarding this report.
Data Flags & Calculations:
6/26/2015
1 of 56
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions: 2 of 56
Collection
Sample ID Plant/Station Date and Time Collected By Sample Description
2015016707
HF LEE PLANT
29-May-15 10:45 AM
ILLEGIBLE
S-10
2015016708
HF LEE PLANT
29-May-15 9:55 AM
ILLEGIBLE
S-16
2015016709
HF LEE PLANT
29-May-15 11:30 AM
ILLEGIBLE
ASW-NR1
3 Total Samples

3 of 56
Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals Yes No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes❑ No
All laboratory QA/QC requirements are acceptable.❑ Yes ❑ No
Report Sections Included:
U Job Summary Report
❑ Sample Identification
n Technical Validation of Data Package
❑ Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
66 Chain of Custody
[I/0] Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Margaret Galvin -Karr Date: 6/26/2015

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060003
Site: S-10
Collection Date: 29-May-15 10:45 AM
Analyte Result Units Qualifiers RDL DF
PERCENT SOLIDS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
DIONEX ANIONS BY VENDOR - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
PH IN SOIL - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
SEDIMENT ANALYSIS - (Analysis Performed by Access Analytical)
Vendor Parameter Complete
TOTAL ORGANIC CARBON IN SOILS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
4 of 56
Sample #: 2015016707
Matrix: SOIL
Method Analysis Date/Time Analyst
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_A.Analytical
Vendor Method V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060003
Site: S-16
Collection Date: 29-May-15 9:55 AM
Analyte Result Units Qualifiers RDL DF
PERCENT SOLIDS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
DIONEX ANIONS BY VENDOR - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
PH IN SOIL - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
SEDIMENT ANALYSIS - (Analysis Performed by Access Analytical)
Vendor Parameter Complete
TOTAL ORGANIC CARBON IN SOILS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
5 of 56
Sample #: 2015016708
Matrix: SOIL
Method Analysis Date/Time Analyst
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_A.Analytical
Vendor Method V_PACE

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060003
Site: ASW-NR1
Collection Date: 29-Mav-15 11:30 AM
Analyte Result Units Qualifiers RDL DF
PERCENT SOLIDS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
DIONEX ANIONS BY VENDOR - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
PH IN SOIL - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
SEDIMENT ANALYSIS - (Analysis Performed by Access Analytical)
Vendor Parameter Complete
TOTAL ORGANIC CARBON IN SOILS - (Analysis Performed by Pace Laboratories)
Vendor Parameter Complete
6 of 56
Sample #: 2015016709
Matrix: SOIL
Method Analysis Date/Time Analyst
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_PACE
Vendor Method V_A.Analytical
Vendor Method V_PACE
-- Additional Information --
Samples were delivered out of temperature. Temperature at receipt was 9.8 degrees C ACS 6/1/15

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Ki, c.8yMie. Suite 100
Huntersville, INC 28078
[phone]
June 26, 2015
Program Manager
Duke Energy
13339 Hagers Ferry Road
Bldg.7405 MG30A2
Huntersville, NC 28078
RE: Project: J 15060003
Pace Project No.: 92252370
Dear Program Manager:
Enclosed are the analytical results for sample(s) received by the laboratory on June 01, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
HORIZON Database Administrator
Enclosures
cc: Marge Galvin -Karr, Duke Energy
Program Manager, Duke Energy
Mary Ann Ogle, Duke Energy
Rodney Wilke, Duke Energy
p«FO
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
lqe� ��� without the written consent of Pace Analytical Services, Inc..
BRAT,
Page 1 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kigg8yMe. Suite 100
Huntersville, NC 28078
[phone]
Project: J15060003
Pace Project No.: 92252370
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification M PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate M 05007
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Green Bay Certification IDs
1241 Bellevue Street, Green Bay, WI 54302
Florida/NELAP Certification #: E87948
Illinois Certification #: 200050
Kentucky Certification #: 82
Louisiana Certification #: 04168
Minnesota Certification #: 055-999-334
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification M E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification #: 2958
New Jersey Certification #: FL765
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
Pennsylvania Certification #: 68-00547
Puerto Rico Certification M FLO1264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Washington Certification #: C955
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
North Dakota Certification #: R-150
South Carolina Certification #: 83006001
Texas Certification #: T104704529-14-1
US Dept of Agriculture #: S-76505
Wisconsin Certification #: 405132750
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification M 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kig%yMie. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: J15060003
Pace Project No.: 92252370
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92252370001
2015016707
Solid
05/29/1510:45
06/01/1518:40
92252370002
2015016708
Solid
05/29/15 09:55
06/01/15 18:40
92252370003
2015016709
Solid
05129/1511:30
06/01/1518:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 ffli�c&fie. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
J15060003
92252370
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92252370001
2015016707
EPA 6010
TAP
16
PASI-0
EPA 6020
CRT
8
PASI-O
EPA 7471
TAP
1
PASI-O
ASTM D2974-87
MLO
1
PASI-O
EPA 9045
MLS
1
PASI-A
EPA 9056
CMB
2
PASI-O
EPA 9056
CMB
1
PASI-O
EPA 9060
TJJ
6
PASI-G
92252370002
2015016708
EPA 6010
TAP
16
PASI-0
EPA 6020
CRT
8
PASI-O
EPA 7471
TAP
1
PASI-O
ASTM D2974-87
MLO
1
PASI-O
EPA 9045
MAB
1
PASI-A
EPA 9056
CMB
2
PASI-O
EPA 9056
CMB
1
PASI-O
EPA 9060
TJJ
6
PASI-G
92252370003
2015016709
EPA 6010
TAP
16
PASI-0
EPA 6020
CRT
8
PASI-O
EPA 7471
TAP
1
PASI-O
ASTM D2974-87
MLO
1
PASI-O
EPA 9045
MAB
1
PASI-A
EPA 9056
CMB
2
PASI-O
EPA 9056
CMB
1
PASI-O
EPA 9060
TJJ
6
PASI-G
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 fflin� c&fie. Suite 100
Huntersville, NC 28078
[phone]
Project: J15060003
Pace Project No.: 92252370
Lab Sample ID Client Sample ID
Method Parameters
SUMMARY OF DETECTION
Result Units Report Limit Analyzed Qualifiers
92252370001
2015016707
EPA 6010
Aluminum
4990
mg/kg
46.1
06/07/15 20:33
EPA 6010
Barium
48.5
mg/kg
4.6
06/07/15 20:33
EPA 6010
Beryllium
0.31 J
mg/kg
0.46
06/07/15 20:33
EPA 6010
Calcium
574
mg/kg
230
06/07/15 20:33
EPA 6010
Chromium
8.0
mg/kg
2.3
06/07/15 20:33
EPA 6010
Copper
5.8
mg/kg
2.3
06/07/15 20:33
EPA 6010
Iron
8520
mg/kg
18.4
06/07/15 20:33
EPA 6010
Magnesium
811
mg/kg
230
06/07/15 20:33
EPA 6010
Manganese
401
mg/kg
2.3
06/07/15 20:33
EPA 6010
Nickel
3.0
mg/kg
2.3
06/07/15 20:33
EPA 6010
Potassium
408J
mg/kg
461
06/07/15 20:33
EPA 6010
Strontium
5.8
mg/kg
4.6
06/07/15 20:33
EPA 6010
Zinc
26.6
mg/kg
9.2
06/07/15 20:33
EPA 6020
Lead
7.9J
mg/kg
9.2
06/10/15 09:29
EPA 6020
Vanadium
14.2
mg/kg
9.2
06/10/15 09:29
EPA 7471
Mercury
0.037
mg/kg
0.014
06/09/15 14:29
ASTM D2974-87
Percent Moisture
43.9
%
0.10
06/09/15 08:56
EPA 9045
pH at 25 Degrees C
6.8
Std. Units
0.10
06/07/15 14:55
EPA 9060
Total Organic Carbon
13900
mg/kg
1080
06/25/15 08:21
EPA 9060
Total Organic Carbon
13100
mg/kg
1070
06/25/15 08:27
EPA 9060
Total Organic Carbon
13300
mg/kg
1070
06/25/15 08:34
EPA 9060
Total Organic Carbon
12400
mg/kg
1070
06/25/15 08:39
EPA 9060
Mean Total Organic Carbon
13100
mg/kg
1070
06/25/15 08:21
EPA 9060
RSD%
4.6
%
06/25/15 08:21
92252370002
2015016708
EPA 6010
Aluminum
8470
mg/kg
54.9
06/07/15 20:37
EPA 6010
Barium
88.6
mg/kg
5.5
06/07/15 20:37
EPA 6010
Beryllium
0.56
mg/kg
0.55
06/07/15 20:37
EPA 6010
Calcium
1010
mg/kg
275
06/07/15 20:37
EPA 6010
Chromium
13.5
mg/kg
2.7
06/07/15 20:37
EPA 6010
Copper
12.4
mg/kg
2.7
06/07/15 20:37
EPA 6010
Iron
13800
mg/kg
22.0
06/07/15 20:37
EPA 6010
Magnesium
1410
mg/kg
275
06/07/15 20:37
EPA 6010
Manganese
841
mg/kg
2.7
06/07/15 20:37
EPA 6010
Nickel
5.6
mg/kg
2.7
06/07/15 20:37
EPA 6010
Potassium
666
mg/kg
549
06/07/15 20:37
EPA 6010
Strontium
9.7
mg/kg
5.5
06/07/15 20:37
EPA 6010
Zinc
56.0
mg/kg
11.0
06/07/15 20:37
EPA 6020
Cobalt
8.OJ
mg/kg
11.0
06/10/15 09:31
EPA 6020
Lead
15.6
mg/kg
11.0
06/10/15 09:31
EPA 6020
Vanadium
27.7
mg/kg
11.0
06/10/15 09:31
EPA 7471
Mercury
0.056
mg/kg
0.016
06/09/15 14:31
ASTM D2974-87
Percent Moisture
52.3
%
0.10
06/09/15 08:56
EPA 9045
pH at 25 Degrees C
6.7
Std. Units
0.10
06/05/15 14:55
EPA 9060
Total Organic Carbon
14500
mg/kg
1260
06/25/15 09:34
EPA 9060
Total Organic Carbon
15600
mg/kg
1260
06/25/15 09:39
EPA 9060
Total Organic Carbon
14800
mg/kg
1260
06/25/15 09:45
REPORT OF LABORATORY ANALYSIS
1g
1g
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 ffii�c&fie. Suite 100
Huntersville, NC 28078
[phone]
Project: J15060003
Pace Project No.: 92252370
Lab Sample ID
Method
Client Sample ID
Parameters
92252370002
2015016708
EPA 9060
Total Organic Carbon
EPA 9060
Mean Total Organic Carbon
EPA 9060
RSD%
92252370003
2015016709
EPA 6010
Aluminum
EPA 6010
Barium
EPA 6010
Beryllium
EPA 6010
Calcium
EPA 6010
Chromium
EPA 6010
Copper
EPA 6010
Iron
EPA 6010
Magnesium
EPA 6010
Manganese
EPA 6010
Nickel
EPA 6010
Potassium
EPA 6010
Strontium
EPA 6010
Zinc
EPA 6020
Cobalt
EPA 6020
Lead
EPA 6020
Vanadium
EPA 7471
Mercury
ASTM D2974-87
Percent Moisture
EPA 9045
pH at 25 Degrees C
EPA 9056
Sulfate
EPA 9060
Total Organic Carbon
EPA 9060
Total Organic Carbon
EPA 9060
Total Organic Carbon
EPA 9060
Total Organic Carbon
EPA 9060
Mean Total Organic Carbon
EPA 9060
RSD%
SUMMARY OF DETECTION
Result
Units
Report Limit
Analyzed Qualifiers
15800
mg/kg
1270
06/25/15 09:51
15200
mg/kg
1260
06/25/15 09:34
4.2
%
06/25/15 09:34
6800
mg/kg
43.8
06/07/15 20:42
67.6
mg/kg
4.4
06/07/15 20:42
0.42J
mg/kg
0.44
06/07/15 20:42
840
mg/kg
219
06/07/15 20:42
10.3
mg/kg
2.2
06/07/15 20:42
7.0
mg/kg
2.2
06/07/15 20:42
11300
mg/kg
17.5
06/07/15 20:42 1g
1030
mg/kg
219
06/07/15 20:42
602
mg/kg
2.2
06/07/15 20:42
4.0
mg/kg
2.2
06/07/15 20:42
495
mg/kg
438
06/07/15 20:42
8.2
mg/kg
4.4
06/07/15 20:42
38.6
mg/kg
8.8
06/07/15 20:42
6.OJ
mg/kg
8.8
06/10/15 09:33
10.2
mg/kg
8.8
06/10/15 09:33
19.3
mg/kg
8.8
06/10/15 09:33
0.037
mg/kg
0.015
06/09/1514:33
44.7
%
0.10
06/09/15 08:56
7.0
Std. Units
0.10
06/08/15 15:55
2450
mg/kg
443
06/06/1510:29 D3
10700
mg/kg
1080
06/25/15 09:57
11100
mg/kg
1080
06/25/1510:03
11700
mg/kg
1080
06/25/1510:09
11600
mg/kg
1090
06/25/1510:14
11300
mg/kg
1080
06/25/15 09:57
4.0
%
06/25/15 09:57
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 ffli�c&fie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15060003
Pace Project No.: 92252370
Method: EPA 6010
Description: 6010 MET ICP
Client: Duke Energy
Date: June 26, 2015
General Information:
3 samples were analyzed for EPA 6010. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3050 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
QC Batch: MPRP/24564
CH: The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased high.
• MS (Lab ID: 1234522)
• Iron
• MSD (Lab ID: 1234523)
• Iron
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MPRP/24564
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92252110014
M1: Matrix spike recovery exceeded QC limits.
• MS (Lab ID: 1234522)
• Aluminum
• Iron
• Manganese
• MSD (Lab ID: 1234523)
• Aluminum
• Iron
• Manganese
Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 fflic&fie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15060003
Pace Project No.: 92252370
Method: EPA 6010
Description: 6010 MET ICP
Client: Duke Energy
Date: June 26, 2015
Additional Comments:
Batch Comments:
Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
• QC Batch: ICP / 15002
Analyte Comments:
QC Batch: MPRP/24564
1g: Analyte was detected in the continueing calibration verification low level (CCVL). All associated samples had concentrations of at
least ten times greater than the CCVL or were below the reporting limit.
•2015016707 (Lab ID:92252370001)
• Iron
•2015016708 (Lab ID:92252370002)
• Iron
•2015016709 (Lab ID:92252370003)
• Iron
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 8 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 ffli�c&fie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15060003
Pace Project No.: 92252370
Method: EPA 6020
Description: 6020 MET ICPMS
Client: Duke Energy
Date: June 26, 2015
General Information:
3 samples were analyzed for EPA 6020. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3050 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MPRP/24565
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92252110014
M6: Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
• MS (Lab ID: 1234526)
• Arsenic
• Selenium
• Vanadium
• MSD (Lab ID: 1234527)
• Arsenic
• Vanadium
Additional Comments:
Batch Comments:
Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
• QC Batch: ICPM / 9947
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 9 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 ffii�c&fie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15060003
Pace Project No.: 92252370
Method: EPA 6020
Description: 6020 MET ICPMS
Client: Duke Energy
Date: June 26, 2015
Analyte Comments:
QC Batch: MPRP/24565
N2: The lab does not hold TNI accreditation for this parameter.
•2015016707 (Lab ID:92252370001)
• Antimony
•2015016708 (Lab ID:92252370002)
• Antimony
•2015016709 (Lab ID:92252370003)
• Antimony
• BLANK (Lab ID: 1234524)
• Antimony
• LCS (Lab ID: 1234525)
• Antimony
• MS (Lab ID: 1234526)
• Antimony
• MSD (Lab ID: 1234527)
• Antimony
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 10 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 fflic&fie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15060003
Pace Project No.: 92252370
Method: EPA 7471
Description: 7471 Mercury
Client: Duke Energy
Date: June 26, 2015
General Information:
3 samples were analyzed for EPA 7471. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 7471 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 11 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 ffligc&fie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15060003
Pace Project No.: 92252370
Method: EPA 9045
Description: 9045 pH Soil
Client: Duke Energy
Date: June 26, 2015
General Information:
3 samples were analyzed for EPA 9045. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch: WET/37839
D6: The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 1473422)
• pH at 25 Degrees C
QC Batch: WET/37905
D6: The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 1476410)
• pH at 25 Degrees C
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 12 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 ffli�c&fie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15060003
Pace Project No.: 92252370
Method: EPA 9056
Description: 9056 IC Anions
Client: Duke Energy
Date: June 26, 2015
General Information:
3 samples were analyzed for EPA 9056. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: WETA/47029
D3: Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
•2015016707 (Lab ID:92252370001)
• Chloride
• Sulfate
•2015016708 (Lab ID:92252370002)
• Chloride
• Sulfate
•2015016709 (Lab ID:92252370003)
• Chloride
• Sulfate
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 13 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KP�c&fie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15060003
Pace Project No.: 92252370
Method: EPA 9056
Description: 9056 IC Anions 48hr
Client: Duke Energy
Date: June 26, 2015
General Information:
3 samples were analyzed for EPA 9056. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
1­13: Sample was received or analysis requested beyond the recognized method holding time.
•2015016707 (Lab ID:92252370001)
•2015016708 (Lab ID:92252370002)
•2015016709 (Lab ID:92252370003)
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: WETA/47028
D3: Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
•2015016707 (Lab ID:92252370001)
• Nitrate as N
•2015016708 (Lab ID:92252370002)
• Nitrate as N
•2015016709 (Lab ID:92252370003)
• Nitrate as N
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 14 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 K�nic&fie. Suite 100
Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J15060003
Pace Project No.: 92252370
Method: EPA 9060
Description: Total Organic Carbon Quad
Client: Duke Energy
Date: June 26, 2015
General Information:
3 samples were analyzed for EPA 9060. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 15 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KP�c&fie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15060003
Pace Project No.: 92252370
Sample: 2015016707
Lab ID:
92252370001 Collected:
05/29/15 10:45
Received: 06/01/15 18:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical
Method: EPA 6010
Preparation
Method: EPA
3050
Aluminum
4990
mg/kg
46.1
23.0
5
06/06/15 15:46
06/07/15 20:33
7429-90-5
Barium
48.5
mg/kg
4.6
2.3
5
06/06/15 15:46
06/07/15 20:33
7440-39-3
Beryllium
0.31J
mg/kg
0.46
0.23
5
06/06/15 15:46
06/07/15 20:33
7440-41-7
Boron
ND
mg/kg
23.0
11.5
5
06/06/15 15:46
06/07/15 20:33
7440-42-8
Calcium
574
mg/kg
230
115
5
06/06/15 15:46
06/07/15 20:33
7440-70-2
Chromium
8.0
mg/kg
2.3
1.2
5
06/06/15 15:46
06/07/15 20:33
7440-47-3
Copper
5.8
mg/kg
2.3
1.2
5
06/06/15 15:46
06/07/15 20:33
7440-50-8
Iron
8520
mg/kg
18.4
9.2
5
06/06/15 15:46
06/07/15 20:33
7439-89-6
1g
Magnesium
811
mg/kg
230
115
5
06/06/15 15:46
06/07/15 20:33
7439-95-4
Manganese
401
mg/kg
2.3
1.2
5
06/06/15 15:46
06/07/15 20:33
7439-96-5
Molybdenum
ND
mg/kg
4.6
2.3
5
06/06/15 15:46
06/07/15 20:33
7439-98-7
Nickel
3.0
mg/kg
2.3
1.2
5
06/06/15 15:46
06/07/15 20:33
7440-02-0
Potassium
408J
mg/kg
461
230
5
06/06/15 15:46
06/07/15 20:33
7440-09-7
Sodium
ND
mg/kg
461
230
5
06/06/15 15:46
06/07/15 20:33
7440-23-5
Strontium
5.8
mg/kg
4.6
2.3
5
06/06/15 15:46
06/07/15 20:33
7440-24-6
Zinc
26.6
mg/kg
9.2
4.6
5
06/06/15 15:46
06/07/15 20:33
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020
Preparation
Method: EPA
3050
Antimony
ND
mg/kg
9.2
4.6
100
06/06/15 15:46
06/10/15 09:29
7440-36-0
N2
Arsenic
ND
mg/kg
9.2
4.6
100
06/06/15 15:46
06/10/15 09:29
7440-38-2
Cadmium
ND
mg/kg
1.1
0.55
100
06/06/15 15:46
06/10/15 09:29
7440-43-9
Cobalt
ND
mg/kg
9.2
4.6
100
06/06/15 15:46
06/10/15 09:29
7440-48-4
Lead
7.9J
mg/kg
9.2
4.6
100
06/06/15 15:46
06/10/15 09:29
7439-92-1
Selenium
ND
mg/kg
9.2
4.6
100
06/06/15 15:46
06/10/15 09:29
7782-49-2
Thallium
ND
mg/kg
9.2
4.6
100
06/06/15 15:46
06/10/15 09:29
7440-28-0
Vanadium
14.2
mg/kg
9.2
4.6
100
06/06/15 15:46
06/10/15 09:29
7440-62-2
7471 Mercury
Analytical
Method: EPA 7471
Preparation
Method: EPA
7471
Mercury
0.037
mg/kg 0.014
0.0069
1
06/06/1516:00
06/09/1514:29
7439-97-6
Percent Moisture
Analytical
Method: ASTM D2974-87
Percent Moisture
43.9
%
0.10
0.10
1
06/09/15 08:56
9045 pH Soil
Analytical
Method: EPA 9045
pH at 25 Degrees C
6.8
Std. Units
0.10
0.10
1
06/07/15 14:55
9056 IC Anions
Analytical
Method: EPA 9056
Chloride
ND
mg/kg
439
219
5
06/06/15 09:47
16887-00-6
D3
Sulfate
ND
mg/kg
439
219
5
06/06/15 09:47
14808-79-8
D3
9056 IC Anions 48hr
Analytical
Method: EPA 9056
Nitrate as N
ND
mg/kg
43.9
21.9
5
06/06/15 09:47
14797-55-8
D3,H3
Date: 06/26/2015 12:34 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 16 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KP�c&fie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15060003
Pace Project No.: 92252370
Sample: 2015016707
Lab ID:
92252370001
Collected:
05/29/15 10:45
Received: 06/01/15 18:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
Total Organic Carbon Quad
Analytical
Method: EPA 9060
Total Organic Carbon
13900
mg/kg
1080
540
1
06/25/15 08:21
7440-44-0
Total Organic Carbon
13100
mg/kg
1070
537
1
06/25/15 08:27
7440-44-0
Total Organic Carbon
13300
mg/kg
1070
534
1
06/25/15 08:34
7440-44-0
Total Organic Carbon
12400
mg/kg
1070
536
1
06/25/15 08:39
7440-44-0
Mean Total Organic Carbon
13100
mg/kg
1070
537
1
06/25/15 08:21
7440-44-0
Surrogates
RSD%
4.6
%
1
06/25/15 08:21
Date: 06/26/2015 12:34 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 17 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KPc&fie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15060003
Pace Project No.: 92252370
Sample: 2015016708
Lab ID:
92252370002 Collected:
05/29/15 09:55
Received: 06/01/15 18:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical
Method: EPA 6010
Preparation
Method: EPA
3050
Aluminum
8470
mg/kg
54.9
27.5
5
06/06/15 15:46
06/07/15 20:37
7429-90-5
Barium
88.6
mg/kg
5.5
2.7
5
06/06/15 15:46
06/07/15 20:37
7440-39-3
Beryllium
0.56
mg/kg
0.55
0.27
5
06/06/15 15:46
06/07/15 20:37
7440-41-7
Boron
ND
mg/kg
27.5
13.7
5
06/06/15 15:46
06/07/15 20:37
7440-42-8
Calcium
1010
mg/kg
275
137
5
06/06/15 15:46
06/07/15 20:37
7440-70-2
Chromium
13.5
mg/kg
2.7
1.4
5
06/06/15 15:46
06/07/15 20:37
7440-47-3
Copper
12.4
mg/kg
2.7
1.4
5
06/06/15 15:46
06/07/15 20:37
7440-50-8
Iron
13800
mg/kg
22.0
11.0
5
06/06/15 15:46
06/07/15 20:37
7439-89-6
1g
Magnesium
1410
mg/kg
275
137
5
06/06/15 15:46
06/07/15 20:37
7439-95-4
Manganese
841
mg/kg
2.7
1.4
5
06/06/15 15:46
06/07/15 20:37
7439-96-5
Molybdenum
ND
mg/kg
5.5
2.7
5
06/06/15 15:46
06/07/15 20:37
7439-98-7
Nickel
5.6
mg/kg
2.7
1.4
5
06/06/15 15:46
06/07/15 20:37
7440-02-0
Potassium
666
mg/kg
549
275
5
06/06/15 15:46
06/07/15 20:37
7440-09-7
Sodium
ND
mg/kg
549
275
5
06/06/15 15:46
06/07/15 20:37
7440-23-5
Strontium
9.7
mg/kg
5.5
2.7
5
06/06/15 15:46
06/07/15 20:37
7440-24-6
Zinc
56.0
mg/kg
11.0
5.5
5
06/06/15 15:46
06/07/15 20:37
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020
Preparation
Method: EPA
3050
Antimony
ND
mg/kg
11.0
5.5
100
06/06/15 15:46
06/10/15 09:31
7440-36-0
N2
Arsenic
ND
mg/kg
11.0
5.5
100
06/06/15 15:46
06/10/15 09:31
7440-38-2
Cadmium
ND
mg/kg
1.3
0.66
100
06/06/15 15:46
06/10/15 09:31
7440-43-9
Cobalt
8.OJ
mg/kg
11.0
5.5
100
06/06/15 15:46
06/10/15 09:31
7440-48-4
Lead
15.6
mg/kg
11.0
5.5
100
06/06/15 15:46
06/10/15 09:31
7439-92-1
Selenium
ND
mg/kg
11.0
5.5
100
06/06/15 15:46
06/10/15 09:31
7782-49-2
Thallium
ND
mg/kg
11.0
5.5
100
06/06/15 15:46
06/10/15 09:31
7440-28-0
Vanadium
27.7
mg/kg
11.0
5.5
100
06/06/15 15:46
06/10/15 09:31
7440-62-2
7471 Mercury
Analytical
Method: EPA 7471
Preparation
Method: EPA
7471
Mercury
0.056
mg/kg 0.016
0.0082
1
06/06/1516:00
06/09/1514:31
7439-97-6
Percent Moisture
Analytical
Method: ASTM D2974-87
Percent Moisture
52.3
%
0.10
0.10
1
06/09/15 08:56
9045 pH Soil
Analytical
Method: EPA 9045
pH at 25 Degrees C
6.7
Std. Units
0.10
0.10
1
06/05/15 14:55
9056 IC Anions
Analytical
Method: EPA 9056
Chloride
ND
mg/kg
525
262
5
06/06/1510:08
16887-00-6
D3
Sulfate
ND
mg/kg
525
262
5
06/06/1510:08
14808-79-8
D3
9056 IC Anions 48hr
Analytical
Method: EPA 9056
Nitrate as N
ND
mg/kg
52.5
26.2
5
06/06/15 10:08
14797-55-8
D3,H3
Date: 06/26/2015 12:34 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 18 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KP�c&fie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15060003
Pace Project No.: 92252370
Sample: 2015016708
Lab ID:
92252370002
Collected:
05/29/15 09:55
Received: 06/01/15 18:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
Total Organic Carbon Quad
Analytical
Method: EPA 9060
Total Organic Carbon
14500
mg/kg
1260
630
1
06/25/15 09:34
7440-44-0
Total Organic Carbon
15600
mg/kg
1260
629
1
06/25/15 09:39
7440-44-0
Total Organic Carbon
14800
mg/kg
1260
628
1
06/25/15 09:45
7440-44-0
Total Organic Carbon
15800
mg/kg
1270
634
1
06/25/15 09:51
7440-44-0
Mean Total Organic Carbon
15200
mg/kg
1260
630
1
06/25/15 09:34
7440-44-0
Surrogates
RSD%
4.2
%
1
06/25/15 09:34
Date: 06/26/2015 12:34 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 19 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 K��c&fie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15060003
Pace Project No.: 92252370
Sample: 2015016709
Lab ID:
92252370003 Collected:
05/29/15 11:30
Received: 06/01/15 18:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
6010 MET ICP
Analytical
Method: EPA 6010
Preparation
Method: EPA 3050
Aluminum
6800
mg/kg
43.8
21.9
5
06/06/15 15:46
06/07/15 20:42
7429-90-5
Barium
67.6
mg/kg
4.4
2.2
5
06/06/15 15:46
06/07/15 20:42
7440-39-3
Beryllium
0.42J
mg/kg
0.44
0.22
5
06/06/15 15:46
06/07/15 20:42
7440-41-7
Boron
ND
mg/kg
21.9
11.0
5
06/06/15 15:46
06/07/15 20:42
7440-42-8
Calcium
840
mg/kg
219
110
5
06/06/15 15:46
06/07/15 20:42
7440-70-2
Chromium
10.3
mg/kg
2.2
1.1
5
06/06/15 15:46
06/07/15 20:42
7440-47-3
Copper
7.0
mg/kg
2.2
1.1
5
06/06/15 15:46
06/07/15 20:42
7440-50-8
Iron
11300
mg/kg
17.5
8.8
5
06/06/15 15:46
06/07/15 20:42
7439-89-6
1g
Magnesium
1030
mg/kg
219
110
5
06/06/15 15:46
06/07/15 20:42
7439-95-4
Manganese
602
mg/kg
2.2
1.1
5
06/06/15 15:46
06/07/15 20:42
7439-96-5
Molybdenum
ND
mg/kg
4.4
2.2
5
06/06/15 15:46
06/07/15 20:42
7439-98-7
Nickel
4.0
mg/kg
2.2
1.1
5
06/06/15 15:46
06/07/15 20:42
7440-02-0
Potassium
495
mg/kg
438
219
5
06/06/15 15:46
06/07/15 20:42
7440-09-7
Sodium
ND
mg/kg
438
219
5
06/06/15 15:46
06/07/15 20:42
7440-23-5
Strontium
8.2
mg/kg
4.4
2.2
5
06/06/15 15:46
06/07/15 20:42
7440-24-6
Zinc
38.6
mg/kg
8.8
4.4
5
06/06/15 15:46
06/07/15 20:42
7440-66-6
6020 MET ICPMS
Analytical
Method: EPA 6020
Preparation
Method: EPA 3050
Antimony
ND
mg/kg
8.8
4.4
100
06/06/15 15:46
06/10/15 09:33
7440-36-0
N2
Arsenic
ND
mg/kg
8.8
4.4
100
06/06/15 15:46
06/10/15 09:33
7440-38-2
Cadmium
ND
mg/kg
1.1
0.53
100
06/06/15 15:46
06/10/15 09:33
7440-43-9
Cobalt
6.OJ
mg/kg
8.8
4.4
100
06/06/15 15:46
06/10/15 09:33
7440-48-4
Lead
10.2
mg/kg
8.8
4.4
100
06/06/15 15:46
06/10/15 09:33
7439-92-1
Selenium
ND
mg/kg
8.8
4.4
100
06/06/15 15:46
06/10/15 09:33
7782-49-2
Thallium
ND
mg/kg
8.8
4.4
100
06/06/15 15:46
06/10/15 09:33
7440-28-0
Vanadium
19.3
mg/kg
8.8
4.4
100
06/06/15 15:46
06/10/15 09:33
7440-62-2
7471 Mercury
Analytical
Method: EPA 7471
Preparation
Method: EPA 7471
Mercury
0.037
mg/kg 0.015
0.0073
1
06/06/1516:00
06/09/1514:33
7439-97-6
Percent Moisture
Analytical
Method: ASTM D2974-87
Percent Moisture
44.7
%
0.10
0.10
1
06/09/15 08:56
9045 pH Soil
Analytical
Method: EPA 9045
pH at 25 Degrees C
7.0
Std. Units
0.10
0.10
1
06/08/15 15:55
9056 IC Anions
Analytical
Method: EPA 9056
Chloride
ND
mg/kg
443
221
5
06/06/1510:29
16887-00-6
D3
Sulfate
2450
mg/kg
443
221
5
06/06/1510:29
14808-79-8
D3
9056 IC Anions 48hr
Analytical
Method: EPA 9056
Nitrate as N
ND
mg/kg
44.3
22.1
5
06/06/15 10:29
14797-55-8
D3,H3
Date: 06/26/2015 12:34 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 20 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 K�c&fie. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J15060003
Pace Project No.: 92252370
Sample: 2015016709
Lab ID:
92252370003
Collected:
05/29/15 11:30
Received: 06/01/15 18:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample
size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
Total Organic Carbon Quad
Analytical
Method: EPA 9060
Total Organic Carbon
10700
mg/kg
1080
540
1
06/25/15 09:57
7440-44-0
Total Organic Carbon
11100
mg/kg
1080
538
1
06/25/15 10:03
7440-44-0
Total Organic Carbon
11700
mg/kg
1080
539
1
06/25/15 10:09
7440-44-0
Total Organic Carbon
11600
mg/kg
1090
543
1
06/25/15 10:14
7440-44-0
Mean Total Organic Carbon
11300
mg/kg
1080
540
1
06/25/15 09:57
7440-44-0
Surrogates
RSD%
4.0
%
1
06/25/15 09:57
Date: 06/26/2015 12:34 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 21 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KPgc&fie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15060003
Pace Project No.: 92252370
QC Batch: MERP/5823
Analysis Method: EPA 7471
QC Batch Method: EPA 7471
Analysis Description: 7471
Mercury
Associated Lab Samples: 92252370001, 92252370002,
92252370003
METHOD BLANK: 1234528
Matrix: Solid
Associated Lab Samples: 92252370001, 92252370002,
92252370003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Mercury mg/kg
ND 0.0081
06/09/1513:50
LABORATORY CONTROL SAMPLE: 1234529
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Mercury mg/kg
.082 0.089
108 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1234530 1234531
MS MSD
92252110014
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD RPD Qual
Mercury mg/kg ND
.102 .0987 0.097
0.087 93 87 80-120 11 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/26/2015 12:34 PM without the written consent of Pace Analytical Services, Inc..
Page 22 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 K��c&fie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15060003
Pace Project No.: 92252370
QC Batch: MPRP/24564 Analysis Method: EPA 6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET Solid
Associated Lab Samples: 92252370001, 92252370002, 92252370003
METHOD BLANK: 1234520 Matrix:
Associated Lab Samples: 92252370001, 92252370002, 92252370003
Blank
Parameter Units Result
Solid
Reporting
Limit
Analyzed
Aluminum
mg/kg
ND
5.2
06/07/1518:49
Barium
mg/kg
ND
0.52
06/07/1518:49
Beryllium
mg/kg
ND
0.052
06/07/1518:49
Boron
mg/kg
ND
2.6
06/07/1518:49
Calcium
mg/kg
ND
25.8
06/07/1518:49
Chromium
mg/kg
ND
0.26
06/07/1518:49
Copper
mg/kg
ND
0.26
06/07/1518:49
Iron
mg/kg
ND
2.1
06/07/1518:49
Magnesium
mg/kg
ND
25.8
06/07/1518:49
Manganese
mg/kg
ND
0.26
06/07/1518:49
Molybdenum
mg/kg
ND
0.52
06/07/1518:49
Nickel
mg/kg
ND
0.26
06/07/1518:49
Potassium
mg/kg
ND
51.5
06/07/1518:49
Sodium
mg/kg
ND
51.5
06/07/1518:49
Strontium
mg/kg
ND
0.52
06/07/1518:49
Zinc
mg/kg
ND
1.0
06/07/1518:49
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1234521
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Aluminum
mg/kg
126
118
93
80-120
Barium
mg/kg
12.6
11.8
94
80-120
Beryllium
mg/kg
1.3
1.2
92
80-120
Boron
mg/kg
126
117
93
80-120
Calcium
mg/kg
629
594
94
80-120
Chromium
mg/kg
12.6
11.5
92
80-120
Copper
mg/kg
12.6
11.5
91
80-120
Iron
mg/kg
126
115
91
80-120
Magnesium
mg/kg
629
583
93
80-120
Manganese
mg/kg
12.6
11.7
93
80-120
Molybdenum
mg/kg
12.6
11.5
92
80-120
Nickel
mg/kg
12.6
11.7
93
80-120
Potassium
mg/kg
629
574
91
80-120
Sodium
mg/kg
629
594
94
80-120
Strontium
mg/kg
12.6
11.6
92
80-120
Zinc
mg/kg
62.9
57.9
92
80-120
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/26/2015 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 23 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 K��c&fie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15060003
Pace Project No.: 92252370
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1234522
1234523
MS
MSD
92252110014
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Aluminum
mg/kg
3080
157
149
4100
3850
650
518
75-125
6
20 M1
Barium
mg/kg
13.4
15.7
14.9
27.2
26.9
88
91
75-125
1
20
Beryllium
mg/kg
0.43
1.52
1.52
1.8
1.8
90
90
75-125
4
20
Boron
mg/kg
9.6J
157
149
151
145
90
91
75-125
4
20
Calcium
mg/kg
239
787
748
1010
961
98
97
75-125
5
20
Chromium
mg/kg
5.5
15.7
14.9
20.0
18.8
92
89
75-125
6
20
Copper
mg/kg
1.9
15.7
14.9
16.2
15.5
90
91
75-125
4
20
Iron
mg/kg
10400
157
149
9260
8860
-729
-1040
75-125
4
20 CH,M1
Magnesium
mg/kg
500
787
748
1190
1190
88
92
75-125
0
20
Manganese
mg/kg
90.9
15.7
14.9
96.0
83.6
32
-49
75-125
14
20 M1
Molybdenum
mg/kg
4.5
15.7
14.9
18.5
17.9
89
89
75-125
4
20
Nickel
mg/kg
1.8
15.7
14.9
17.5
16.7
100
100
75-125
5
20
Potassium
mg/kg
338
787
748
999
1000
84
89
75-125
0
20
Sodium
mg/kg
ND
787
748
784
717
100
96
75-125
9
20
Strontium
mg/kg
4.5
15.7
14.9
19.6
18.4
95
93
75-125
6
20
Zinc
mg/kg
5.9J
78.7
74.8
79.4
77.3
93
95
75-125
3
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/26/2015 12:34 PM without the written consent of Pace Analytical Services, Inc..
Page 24 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 K3nlc&fie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15060003
Pace Project No.: 92252370
QC Batch: MPRP/24565 Analysis Method: EPA 6020
QC Batch Method: EPA 3050 Analysis Description: 6020 MET SOLID
Associated Lab Samples: 92252370001, 92252370002, 92252370003
METHOD BLANK: 1234524
Matrix:
Solid
Associated Lab Samples:
92252370001, 92252370002,
92252370003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Antimony
mg/kg
ND
0.051
06/10/15 08:38 N2
Arsenic
mg/kg
ND
0.051
06/10/15 08:38
Cadmium
mg/kg
ND
0.0061
06/10/15 08:38
Cobalt
mg/kg
ND
0.051
06/10/15 08:38
Lead
mg/kg
ND
0.051
06/10/15 08:38
Selenium
mg/kg
ND
0.051
06/10/15 08:38
Thallium
mg/kg
ND
0.051
06/10/15 08:38
Vanadium
mg/kg
ND
0.051
06/10/15 08:38
LABORATORY CONTROL SAMPLE:
Parameter
1234525
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
mg/kg
2.5
2.6
102
80-120 N2
Arsenic
mg/kg
2.5
2.6
102
80-120
Cadmium
mg/kg
.25
0.26
102
80-120
Cobalt
mg/kg
2.5
2.6
103
80-120
Lead
mg/kg
2.5
2.6
104
80-120
Selenium
mg/kg
2.5
2.6
103
80-120
Thallium
mg/kg
2.5
2.7
105
80-120
Vanadium
mg/kg
2.5
2.6
103
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1234526
1234527
MS
MSD
92252110014
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
Antimony
mg/kg
ND
3.29
3.16
ND
ND
90
78
75-125
20 N2
Arsenic
mg/kg
49.5
3.29
3.16
47.8
42.3
-53
-225
75-125
12 20 M6
Cadmium
mg/kg
ND
.329
.316
ND
ND
84
82
75-125
20
Cobalt
mg/kg
ND
3.29
3.16
5.5J
5.3J
82
78
75-125
20
Lead
mg/kg
ND
3.29
3.16
4.5J
4.3J
87
83
75-125
20
Selenium
mg/kg
ND
3.29
3.16
4.6J
3.6J
132
103
75-125
20 M6
Thallium
mg/kg
ND
3.29
3.16
3.6J
3.3J
101
92
75-125
20
Vanadium
mg/kg
10.4
3.29
3.16
12.4
12.3
62
58
75-125
1 20 M6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/26/2015 12:34 PM without the written consent of Pace Analytical Services, Inc..
Page 25 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 K��c&fie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15060003
Pace Project No.: 92252370
QC Batch: PMST/3626
Analysis Method:
ASTM
D2974-87
QC Batch Method: ASTM D2974-87
Analysis Description:
Dry Weight/Percent Moisture
Associated Lab Samples: 92252370001,
92252370002, 92252370003
SAMPLE DUPLICATE: 1236448
35190638001
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Percent Moisture
%
23.8
22.8
5
10
SAMPLE DUPLICATE: 1236449
92252369003
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Percent Moisture
%
47.8
54.2
13
10 D6
SAMPLE DUPLICATE: 1236450
35191113002
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Percent Moisture
%
15.9
15.2
5
10
SAMPLE DUPLICATE: 1236451
35191437001
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Percent Moisture
%
15.1
16.3
8
10
SAMPLE DUPLICATE: 1236452
35191894001
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Percent Moisture
%
10.2
10.6
3
10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/26/2015 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 26 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 K3c&fie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15060003
Pace Project No.: 92252370
QC Batch: WET/37839 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 92252370001
SAMPLE DUPLICATE: 1473421
Parameter
pH at 25 Degrees C
SAMPLE DUPLICATE: 1473422
Parameter
pH at 25 Degrees C
92252023001 Dup Max
Units Result Result RPD RPD Qualifiers
Std. Units 8.0 8.1 1 10
92252110007 Dup Max
Units Result Result RPD RPD Qualifiers
Std. Units 6.4 6.5 2 10 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/26/2015 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 27 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 K3c&fie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15060003
Pace Project No.: 92252370
QC Batch: WET/37840 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 92252370002
SAMPLE DUPLICATE: 1473429
Parameter
pH at 25 Degrees C
SAMPLE DUPLICATE: 1473430
Parameter
pH at 25 Degrees C
92250905001 Dup Max
Units Result Result RPD RPD Qualifiers
Std. Units 7.9 7.9 0 10
92251844002 Dup Max
Units Result Result RPD RPD Qualifiers
Std. Units 7.5 7.6 0 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/26/2015 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 28 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 K��c&fie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15060003
Pace Project No.: 92252370
QC Batch: WET/37905 Analysis Method: EPA 9045
QC Batch Method: EPA 9045 Analysis Description: 9045 pH
Associated Lab Samples: 92252370003
SAMPLE DUPLICATE: 1476410
Parameter
pH at 25 Degrees C
SAMPLE DUPLICATE: 1476411
Parameter
pH at 25 Degrees C
92252908001 Dup Max
Units Result Result RPD RPD Qualifiers
Std. Units 5.1 4.9 3 10 D6
92252908010 Dup Max
Units Result Result RPD RPD Qualifiers
Std. Units 6.0 6.1 2 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/26/2015 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 29 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 K��c&fie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15060003
Pace Project No.: 92252370
QC Batch: WETA/47029 Analysis Method: EPA 9056
QC Batch Method: EPA 9056 Analysis Description: 9056 IC Anions
Associated Lab Samples: 92252370001, 92252370002, 92252370003
METHOD BLANK: 1233607 Matrix: Solid
Associated Lab Samples:
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chloride mg/kg ND 49.8 06/06/15 06:55
Sulfate mg/kg ND 49.8 06/06/15 06:55
LABORATORY CONTROL SAMPLE:
1233608
Parameter
Units
Chloride
mg/kg
Sulfate
mg/kg
MATRIX SPIKE SAMPLE:
1233610
Parameter
Units
Chloride
mg/kg
Sulfate
mg/kg
SAMPLE DUPLICATE: 1233609
Parameter
Chloride
Sulfate
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
496 510 103 80-120
496 507 102 80-120
92252369001 Spike MS MS % Rec
Result Conc. Result % Rec Limits Qualifiers
ND 1310 1240 76 80-120 M 1
ND 1310 1300 84 80-120
92252369001 Dup
Units Result Result
mg/kg ND ND
mg/kg ND ND
Max
RPD RPD Qualifiers
20
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/26/2015 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 30 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 K�c&fie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15060003
Pace Project No.: 92252370
QC Batch: WETA/47028
Analysis Method:
EPA 9056
QC Batch Method: EPA 9056
Analysis Description:
9056 IC Anions
Associated Lab Samples: 92252370001, 92252370002, 92252370003
METHOD BLANK: 1233603
Matrix: Solid
Associated Lab Samples:
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Nitrate as N
mg/kg
ND 5.0
06/06/15 06:55
LABORATORY CONTROL SAMPLE:
1233604
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Nitrate as N
mg/kg
49.6 52.7
106
80-120
MATRIX SPIKE SAMPLE:
1233606
92252369001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Nitrate as N
mg/kg
ND 131
123
92 80-120 H3
SAMPLE DUPLICATE: 1233605
92252369001 Dup
Max
Parameter
Units
Result Result
RPD
RPD
Qualifiers
Nitrate as N
mg/kg
ND ND
20 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/26/2015 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 31 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 K�gc&fie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J15060003
Pace Project No.: 92252370
QC Batch: WETA/29146
Analysis Method: EPA 9060
QC Batch Method: EPA 9060
Analysis Description: 9060 TOC Average
Associated Lab Samples: 92252370001, 92252370002,
92252370003
METHOD BLANK: 1180915
Matrix: Solid
Associated Lab Samples:
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Mean Total Organic Carbon mg/kg
ND 600
06/25/15 07:35
LABORATORY CONTROL SAMPLE: 1180916
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Mean Total Organic Carbon mg/kg
120000 111000
93 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1180917 1180918
MS MSD
92252370001
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD RPD Qual
Mean Total Organic Carbon mg/kg 13100
10700 10700 23800
22800 100 90 50-150 5 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/26/2015 12:34 PM without the written consent of Pace Analytical Services, Inc..
Page 32 of 37

Pace Analytical Services, Inc
aceAnalXical ® 9800 Suite tr��c&rr�e.100
Huntersville, NC 28078078
www.pacelabs.com [phone]
QUALIFIERS
Project: J15060003
Pace Project No.: 92252370
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-G Pace Analytical Services - Green Bay
PASI-O Pace Analytical Services - Ormond Beach
BATCH QUALIFIERS
Batch: ICP/15002
Ill Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
Batch: ICPM/9947
Ill Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
ANALYTE QUALIFIERS
1g Analyte was detected in the continueing calibration verification low level (CCVL). All associated samples had
concentrations of at least ten times greater than the CCVL or were below the reporting limit.
CH The continuing calibration for this compound is outside of Pace Analytical acceptance limits. The results may be biased
high.
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/26/2015 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 33 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Suite 100
Huntersville, INC 28078
[phone]
QUALIFIERS
Project: J15060003
Pace Project No.: 92252370
ANALYTE QUALIFIERS
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
N2 The lab does not hold TIN accreditation for this parameter.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/26/2015 12:34 PM without the written consent of Pace Analytical Services, Inc.. Page 34 of 37

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 1inlc&fie. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: J15060003
Pace Project No.: 92252370
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92252370001
2015016707
EPA 3050
MPRP/24564
EPA 6010
92252370002
2015016708
EPA 3050
MPRP/24564
EPA 6010
92252370003
2015016709
EPA 3050
MPRP/24564
EPA 6010
92252370001
2015016707
EPA 3050
MPRP/24565
EPA 6020
92252370002
2015016708
EPA 3050
MPRP/24565
EPA 6020
92252370003
2015016709
EPA 3050
MPRP/24565
EPA 6020
92252370001
2015016707
EPA 7471
MERP/5823
EPA 7471
92252370002
2015016708
EPA 7471
MERP/5823
EPA 7471
92252370003
2015016709
EPA 7471
MERP/5823
EPA 7471
92252370001
2015016707
ASTM D2974-87
PMST/3626
92252370002
2015016708
ASTM D2974-87
PMST/3626
92252370003
2015016709
ASTM D2974-87
PMST/3626
92252370001
2015016707
EPA 9045
WET/37839
92252370002
2015016708
EPA 9045
WET/37840
92252370003
2015016709
EPA 9045
WET/37905
92252370001
2015016707
EPA 9056
WETA/47029
92252370002
2015016708
EPA 9056
WETA/47029
92252370003
2015016709
EPA 9056
WETA/47029
92252370001
2015016707
EPA 9056
WETA/47028
92252370002
2015016708
EPA 9056
WETA/47028
92252370003
2015016709
EPA 9056
WETA/47028
92252370001
2015016707
EPA 9060
WETA/29146
92252370001
2015016707
EPA 9060
WETA/29147
92252370002
2015016708
EPA 9060
WETA/29146
92252370002
2015016708
EPA 9060
WETA/29147
92252370003
2015016709
EPA 9060
WETA/29146
92252370003
2015016709
EPA 9060
WETA/29147
Date: 06/26/2015 12:34 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
ICP/15002
ICP/15002
ICP/15002
ICPM/9947
ICPM/9947
ICPM/9947
MERC/5810
MERC/5810
MERC/5810
Page 35 of 37

e ��ceAnalyilc��la
Document Name:
le Condition Upon Recei
Document Number:
F-CHR-CS-003-rev.16
Document Revised: May 18, 2015
SCUR Page 1 of 2*
Issuing Authority: 42 of 56
Pace Huntersville Quality Office
Client Name:
Courier: ❑ Fed Ex ❑ UPS❑ USPS❑ Client❑ CommercialD" Pace Other
Custody Seal on Cooler/Box Present: ❑ yes rj no Seals intact: ❑ ves
Packing Material: ❑ Bubble v[jp ❑ Bubble Bags ❑ None ❑ Other
Thermometer Used: IR Gun T1401 Type of lee: jDetBlue None
Temn Correction Factor T1401 No Correction
• Page 2 of 2 is for Internal Use Only
❑ no
„]-Samples on ice, cooling process has begun
i
Corrected Cooler Temp.: �� •C
Biological Tissue is Frozen: Yes No NIA
Date and I itl Is of pe sa f
contents �j�f�amining
�f ---,
Temp should be above freezing to 6°C
Comments:
Chain of Custody Present:
©Yes
ONO
❑NIA
1.
Chain of Custody Filled Out:
C es
ON,
❑NIA
2.
Chain of Custody Relinquished:
a es
ONO
❑NIA
3.
Sampler Name & Signature on COC:
s
ONO
❑NIA
4.
Samples Arrived within Hold Time:
Y6s
ONO
❑NIA
5.
Short Hold Time Analysis (<72hr):
❑Yes
OHO
❑NIA
6.
Rush Turn Around Time Requested:
❑Yes
❑ o
❑NIA
7,
Sufficient Volume:
9'"®s
ON,
❑NIA
8.
Correct Containers Used:
❑Yes
ONO
❑NIA
9.
-Pace Containers Used:
LlYes
O'No
❑NIA
Containers Intact:
P-Yes
ONO
❑NIA
10,
Filtered volume received for Dissolved tests
❑Yes
❑No
CENIA
11.
Sample Labels match COC:
!]fes
ONO
❑NIA
12.
-Includes date/lime/ID/Analysis Matrix:
All containers needing preservation have been checked.
❑Yes
ONO
17lA
13.
All containers needing preservation are found to be in
Dyes
ONO
f❑NSA
compliance with EPA recommendation,
/
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water)
❑Yes
[--]No
Samples checked for dechlorination:
❑Yes
ONO
Ej NA
14,
Headspace in VOA Vials ( >6mm):
1--]Yes
ONO
RNK
15.
Trip Blank Present:
El Yes
ONO
❑NIA
16,
Trip Blank Custody Seals Present
❑Yes
ONO
❑NIA
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution: Field Data Required? Y I N
Person Contacted: Date/Time:
Comments/ Resolution:
SCURF Review: latt iDate: I (Q �i/S
SRF Review: I vat Date: 3 l5
Note: Whenever there is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( Le out of hold, incorrect preservative, out of temp,
incorrect containers)
WOtt : 92252370
II111121131111111111111111I�
Page 36 of 37

43 of 56
U
ro
S
N
o 1I
a i a
S I
C„slam er 3o aan+plola appropri la C011AIns to right
3 � �
n
a Y n
m
o+ 1 . a 'n
V
4 (D 3, a a
s
m 3
X 7 h n
d cr
�D > o 1
U)
�� I�rlf I-kkf kl l Ht��l
0
77 CS`
o` S
4'inlanicr moil Comryf�te ,
r-n Cz
W M d �
m
O
e 7<a
i
r t
> I I
i
!y1 i
O V y t
IV f W QiE
v .. _.Y too
4, fA i
I C
i
! i %
© N 1 i
ro
rrD00
c f]1
I o
N �
r y I
d
Ln U i
I
"Comp, "Ar alys s
,a
i
i t `
a!>
Grab Req Ire
��j—
y�
y r.
Total Metals, Anions,
CIL"
(U_7
PH
" 1, 8 oz Jar (PACE)
r
r
era S'clrgl�
I
j
J TOC I- 4 oz jar
a
o!jo
0 1
(PACE)
4
M
w itt
SPLP Total Metals and
`— + n
m.
0!
Anions 2 - 8
! --n
oz jars (PACE)
9
Sediment specific tests
N 2 -8 oz Jar (ACCESSn
ANALYTICAL)
5 �
m
i
i
i
ro
i
i
"Total # of Containers
.j.
rt
d
$
O
-D
o
.{{ A
G7
al
t -y
0 C a
v
.a
rao�
ili
0
rn
� Z
h #
Page 37 of 37

44 of 56
Acass
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Duke Energy
13339 Hagers Ferry Rd.
Huntersville NC 28078
ATTENTION
Marge Galvin -Karr
PROJECT ID
J15060003
LABORATORY REPORT NUMBER
1506303
DATE
June 15, 2015
Primary Data Review By Secondary Data Review By
Ashley Amick
Chantelle Kanhai Project Manager, Access Analytical
Project Manager, AES [e-mail]
PLEASE NOTE:
- Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA 30340.
- AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582,
NELAP certified laboratory # E87582
- Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243
Page 1 of 7

Anal
ytk
LaS
7-DIXF if-r
;
- - -:
: .
i�
�
lracodaM(Buiding Taos) work artir13339g F�+Y RaERG%HM 28076
._._..,•
�
tsso) 8754245 I iL090" By �DMe a 1 m.
1)ProjecrNamo----._--._...-..Fax:.(9gpl&75.43a9 i i
A8 Grovntlw - .....; I
Ater Assessment Soil z}Pha . Na. -
3)CH.nr
�1•-1 �— t et I4}Foe NO; j Pace
t t 4 As �w !! PO 1142081
}BrnlrieaC Linl[; ' MP
6IPrOJoc[iD: v yN
7WAp COtla- Anali tI�
P�C�
6) Operatlhq Unk: }�� y� Ca�
9lAcinrlty rD� �Q)?rocvaa lD aO NIl'r"b6r 114205
14 :.
zos�
.., specmc accountJng - . -
Presery d
atJvas when used rnust be Or added within is minutes of sample
i LAq USE ONLY I
coFFection
i Matriz
1
i
Leh ID ! j3oii, So —M, Ash} 15
le Descry lion or ID
Sediment
1
r G 1 4l
/VRi
r
i
r
i
1
I
'--�� WATER EQUIPMENT Bt ANK (1 PER DAY1
r7Ralirwuien.n a.. _ �,
a
30—
>
Inr ED
I? abora#ory ilsa Onfv _-_._.._.-._._.-----•-
m-x: SOIL
NC �gyn k,e Ori Imh S x_ ! Pacp 1 Of 1
From aH` DISTRISU'nON
2 ORIGINAL to LAB,
i
SAMPLE PRaGRAM � yy3ier r COFY to CL}ENT
�) Na1ES Other
r_i5 . %/ip
meals: Al, Sb, As, Ba, Be, 0nuul'1
Aniona; C!, Nitrate-N, SO4 a Pbr Mg, Mn , Hi, K, Se,
Sediment S Na. Sr, 77, y, Zn, Marco
ry, pH
1 t L �c��� f�Cific Pawr»eter3; CEC, Particle Size Distribution, Rotlox Potential
^nWe5t0U Turnaround
,y is Days
J 7 Days
•4s�a e 2c� of 7 � I
jiso lD oovs
1
i
Leh ID ! j3oii, So —M, Ash} 15
le Descry lion or ID
Sediment
1
r G 1 4l
/VRi
r
i
r
i
1
I
'--�� WATER EQUIPMENT Bt ANK (1 PER DAY1
r7Ralirwuien.n a.. _ �,
a
30—
>
Inr ED
I? abora#ory ilsa Onfv _-_._.._.-._._.-----•-
m-x: SOIL
NC �gyn k,e Ori Imh S x_ ! Pacp 1 Of 1
From aH` DISTRISU'nON
2 ORIGINAL to LAB,
i
SAMPLE PRaGRAM � yy3ier r COFY to CL}ENT
�) Na1ES Other
r_i5 . %/ip
meals: Al, Sb, As, Ba, Be, 0nuul'1
Aniona; C!, Nitrate-N, SO4 a Pbr Mg, Mn , Hi, K, Se,
Sediment S Na. Sr, 77, y, Zn, Marco
ry, pH
1 t L �c��� f�Cific Pawr»eter3; CEC, Particle Size Distribution, Rotlox Potential
^nWe5t0U Turnaround
,y is Days
J 7 Days
•4s�a e 2c� of 7 � I
jiso lD oovs

Analytical Environmental Services, Inc
Date: 15-Jun-1546 of 56
Client: Duke Energy
Project: J15060003 Case Narrative
Lab ID: 1506303
REDOX POTENTIAL
1506303-001
134.5 mV
92.4 mV
132.5 mV
1506303-002
86.8 mV
70.3 mV
63.5 mV
1506303-003
255.7 mV
255.2 mV
239.8 My
Page 3 of 7

47 of 56
Analytical Environmental Services, Inc
Date: 15-Jun-15
Client:
Duke Energy
Client Sample ID:
S-10
Project Name:
J15060003
Collection Date:
5/29/2015 10:45:00 AM
Lab ID:
1506303-001
Matrix:
Sediment
Reporting Dilution
Analyses Result Qual Units BatchID Date Analyzed Analyst
Limit Factor
CEC of Soils (Na Saturation) SW9081
Cation Exchange Capacity
Qualifiers: r Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
(SW9081)
9.9 1.0 meq/100g 208358 1 06/09/2015 00:37 TA
E
Estimated (value above quantitation range)
S
Spike Recovery outside limits due to matrix
Nan
See case narrative
NC
Not confirmed
<
Less than Result value
J
Estimated value detected below Reporting Limit
Page 4 of 7

48 of 56
Analytical Environmental Services, Inc
Date: 15-Jun-15
Client:
Duke Energy
Client Sample ID:
S-16
Project Name:
J15060003
Collection Date:
5/29/2015 9:55:00 AM
Lab ID:
1506303-002
Matrix:
Sediment
Reporting Dilution
Analyses Result Qual Units BatcbID Date Analyzed Analyst
Limit Factor
CEC of Soils (Na Saturation) SW9081
Cation Exchange Capacity
Qualifiers: r Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
(SW9081)
10 1.0 meq/100g 208358 1 06/09/2015 00:40 TA
E
Estimated (value above quantitation range)
S
Spike Recovery outside limits due to matrix
Nan
See case narrative
NC
Not confirmed
<
Less than Result value
J
Estimated value detected below Reporting Limit
Page 5 of 7

49 of 56
Analytical Environmental Services, Inc
Date: 15-Jun-15
Client:
Duke Energy
Client Sample ID:
ASW-NR1
Project Name:
J15060003
Collection Date:
5/29/2015 11:30:00 AM
Lab ID:
1506303-003
Matrix:
Sediment
Reporting Dilution
Analyses Result Qual Units BatcbID Date Analyzed Analyst
Limit Factor
CEC of Soils (Na Saturation) SW9081
Cation Exchange Capacity
Qualifiers: r Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
(SW9081)
6.8 1.0 meq/100g 208358 1 06/09/2015 00:42 TA
E
Estimated (value above quantitation range)
S
Spike Recovery outside limits due to matrix
Nan
See case narrative
NC
Not confirmed
<
Less than Result value
J
Estimated value detected below Reporting Limit
Page 6 of 7

Analytical Environmental Services, Ine.
Sample/Cooler Receipt Checklist
Client k,c I Work Order Number (' 060Du'
Checklist completed by (ol h
Signature Date
Carrier name: FedEY UPS _ Courier _ Client— US Mail Other
Shipping container/cooler in good condition? Yes No _ Not Present
Custody seats intact on shipping container/cooler? Yes No _ Not Present
Custody seals intact on sample bottles? Yes No _ Not Present
Container/Tenrp Blank temperature in compliance? (0°<6°C)* Yes / No
Cooler Al 3.5 ' Cooler 92 Cooler #3 Cooler 94 Cooler95 Cooler #6
/
Chain of custody present?
Yes
No
Chain of custody signed when relinquished and received?
Yes
r
No
Chain of custody agrees with sample labels?
Yes
!
No
Samples in proper containerlbottle?
Yes
No —
Sample containers intact?
Yes
No
/
Sufficient sample volume for indicated test?
Yes
/
No
All samples received within holding time?
Yes
No
Was TAT marked on the COC?
Yes
No
Proceed with Standard TAT as per project history?
Yes
T
No
Water - VOA vials have zero headspace? No VOA vials submitted ! Yes
Water - pH acceptable upon receipt? Yes _ No
Adjusted?
Sample Condition: Good/ Other(Etplaia)
(For diffusive samples or AIHA lead) is a known blank included?
See Case Narrative for resolution of the Non -Conformance.
Checked by
Yes
Not Applicable /
No
Not Applicable
No
* Samples do not have to comply with the given range for certain parameters.
Mes server111Sample ReceiptVvly Documents\COCs and pH Adjustment SheetlSample_Cooler_Recipt_Checklist Revl.rtf
Page 7 of 7

51 of 56
June 15, 2015
Access Analytical
7478 Carlisle Street
Irmo, South Carolina 29063
Attn: Mr. Ashley Amick
Re: Summary of Laboratory Testing
AB Groundwater Assessment
Terracon Project No. 73075016 (WOJ15060003)
Dear Mr. Amick:
Irerracon
Terracon has performed the requested laboratory testing program indicated by your Chain of
Custody Record, dated 06/04/15. The correspondence indicated hydrometer testing for
Samples S-10, S-16, and ASW-NR1.
The results have been electronically forwarded to you in PDF format at
[e-mail], as instructed. If there are any questions regarding the results
or if we can be of additional service, please contact us.
Sincerely,
Terracon Consultants, Inc.
xl--- --
Rebecca Simms, CET
Laboratory Manager
Attachments
Copies:
1xc: Above (PDF via email)
1xc: File
RS/PM
Phillit
iso P.E.
Geo artment Manager
Terracon Consultants, Inc. 521 Clemson Road Columbia, South Carolina 29229
P [803] 741 9000 F [803] 741 9900 terracon.com

GRAIN SIZE DISTRIBUTION
52 of 56
ASTM D422
U.S. SIEVE OPENING IN INCHES U.S. SIEVE NUMBERS I HYDROMETER
6 4 3 2 1.5 1 3/4 1/23/8 3 4 6 810 1416 20 30 40 50 60 100 140 200
100
95
-
90
85
-
80
75
70
65
w 60
>- 55
m
w
-
50
z
LL
-
I— 45
z
40
w
0
35
30
25
20
15
-
10
-
5
0
-
100 10 1 0.1 0.01 0.001
GRAIN SIZE IN MILLIMETERS
LCOBBLES
GRAVEL
SAND
SILT OR CLAY
coarse
fine
coarse
medium
fine

GRAIN SIZE DISTRIBUTION
53 of 56
ASTM D422
U.S. SIEVE OPENING IN INCHES U.S. SIEVE NUMBERS I HYDROMETER
6 4 3 2 1.5 1 3/4 1/23/8 3 4 6 810 1416 20 30 40 50 60 100 140 200
100
95
-
90
85
-
80
75
70
65
w 60
>- 55
m
w
-
50
z
LL
-
I— 45
z
40
w
0
35
30
25
20
15
-
10
-
5
0
-
100 10 1 0.1 0.01 0.001
GRAIN SIZE IN MILLIMETERS
LCOBBLES
GRAVEL
SAND
SILT OR CLAY
coarse
fine
coarse
medium
fine

GRAIN SIZE DISTRIBUTION
54 of 56
ASTM D422
U.S. SIEVE OPENING IN INCHES U.S. SIEVE NUMBERS I HYDROMETER
6 4 3 2 1.5 1 3/4 1/23/8 3 4 6 810 1416 20 30 40 50 60 100 140 200
100
95
-
90
85
-
80
75
70
65
w 60
>- 55
m
w
-
50
z
LL
-
I— 45
z
40
w
0
35
30
25
20
15
-
10
-
5
0
-
-71
100 10 1 0.1 0.01 0.001
GRAIN SIZE IN MILLIMETERS
LCOBBLES
GRAVEL
SAND
SILT OR CLAY
coarse
fine
coarse
medium
fine

w�
-
�} cc) Li (III N �' m
J < 10
o o dZ F s0 E g
L 4
EL
Q m mrZ
-� cO a -� �mm a
xnV trRy 3 roaL
a c c
�
o an q c m u c
y 3 A-
z m � a.c.4 c39.
o - N o= m C m it C U 1d V-
® U nuQi ac Q 1c2cc) H
L (� y 6 b O R C Q
mZo
c y 11 tl V 0 61 in G I
aoe¢ tyu iog :9
L
O
W
Q
/�
V
O
O
4'
U
Q
1
V/
Yf
V
818d'Ou8 �3(.4@fSS ?1_&A1�6SiE 915a�8�1E' 9P&d�l'li@ flL{SE[IC 59YdtLwe �913�.IEpC SjSfi�81
T TTrit ti'tiz.I �"? ?f�a?:r�ti
P'-flab P rc, F-IMP P"IW PTI-Em F mt" Par.H P
v r •dzu
r5
o
y•
�..
)
I
ce EL
F-
w
m
d
a
t45
� U 1
v o`
V°
o
Z Z Z Z
3C
U
u
n
C
O
M
7
C
u
TS
�
�
U
fU
�
Ci
In
L
H
i
O
w
6r
L
c�
m
�
�
m
N
cr
d
u
r
QCIO
y
u
U
y
'�
V
a;
.N
{% k�A

7.�7y
■I�,�rr■��rr����r
0, ono
no
Eno
loans
Total iN$tef Ani
PH
' 1 - a Oz Jar (PACE)
ba
rLP - Total Metals Aad
'lama 2.8
Ora (PAGE)
Sadirniont Specific teat,
2 { 8 of fair (ACCIES
ANALYT)CAL)
20x��,-m
N �
n
n