WQ0000485_Monitoring - 07-2023_20230824 (4)

Monitoring Report Submittal
Permit Number#*
Name of Facility:*
Month:* July
Report Information
Type *
Revised - GW-59
Confirmation Email Address:
Name of Submitter: *
Signature:
Date of submittal:
WQ0000485
Darling Ingredients - Rose Hill
Year:* 2023
Upload Document*
scan 2023-07 WQ0000485 GW-59 DIRH- 3.82MB
REVISED.pdf
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
[e-mail]
Corey Lanier
C'!'t!ffliYlPt
Initial Review
..............................
Reviewer: Wanda.Gerald
8/24/2023
This will be filled in automatically

Is the project number correct?* WQ0000485
Is the monitoring report accepted?* Yes No
Regional Office* Wilmington
Reviewer: _anonymous
Review Date: 9/8/2023

DARLING
INGREDIENTS
August 18, 2023
Division of Water Resources
Attn: Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: Ground Water Quality Monitoring Report (GWQMR)
Darling Ingredients — Rose Hill
Permit W00000485
To whom it may concern,
Please find enclosed the Groundwater Quality Monitoring Compliance Report for
Surface Irrigation for the month of July 2023 for our Rose Hill Division.
Should you require any additional information or wish to discuss this matter,
please feel free to contact me at 910.289.2083 x 25119.
Sincerely,
b 4 4Y'`i
Larry Holt
General Manager
cc: DI Regional Corporate Office
!.k�:•u `_Ctiii iJrrv. ;F�a! uifiiaidJ art HEALTH • NUTRIEIJT. • RIOFNERF • SEPVICES

GW-59A COMPLIANCE REPORT FORM ?ermit # W00000485
(Sabmh gag each monitoring period with GW-59 jorms.)
I
Enter date monitoring resuiis were due. (01113'512023) Will this monitoring report (GIN-69 and GW-59A)
be submitted after the established due dale?
No
2
Was any required information missing on the GW-59 report forms?
No
IF the answer to question 1 or is 'YES". list in the space provided below the well identification numbar(s) and explain the
problems encountered in obtaining the required information.
MW-BA was damaged by farm equipment and is scheduled to be closed and replaced by Register Well Co, INC; moving the
replacement well 10' due North perDEQ direction.
3
Am soy of the monitor wells in need of repair or maintro*_(damaged casior, unlocktd or missing cap, missingidentincalion
plate, area overgrown, etc)? Ifthe onswer is -yes,,. contact the Regional Office forsuidance_
No
4
Are any monitored constituents equal to or above the established standards?
YES
It the answer to question 4 is'NO , sidp to section 8.
Ifthe answer to question 4 is "YES" list the affected wells individually with consttluent(s) and concentration(s) exceeding
standards In the space provided below.
SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR E,(CEEDANCE HISTORYREPORT
5
For the constituents identified In question 4 above, have standards been exceeded previously for the same
con6lttuant(s) In the same welt(s) In the last two years?
YES
Ifthe answer to question 5Is'NO", skip to section 8
Ifthe answer to question 5 is "YES", list in the space provided below, each well with constituents) exceeding standards,
concentrations) reported, and sample collection date for each occurrence (for the last two years).
SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT
6
Are the monitoring wells listed In section 5located at or beyond the review boundary?
YES
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE
IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the
,Regional Office.
7
Is the parmlttee implementing previously approved actions required by the Division Involving this groundwater quality
problem?
YES
If the answerto question 7 is 'YES", describe those actions in the space provided below
If the answerfa question 7 is "NO" contact the Re io a/ ofillice within 90 days; an evaluation rnay be
required to determine the impact the waste disposal system is having of the review and compliance
boundaries surrounding this facility. Failure to do so may sub act the permiffee to a Notice of Violation,
fines. andbr penalties.
Additional monitoring was performed to identify constituents of TOG in MW No.9. The facility has been
communicating with Mr. Geoff Kegley in the Wilmington Regional Office.
8
The person completing this portion (GW.59A) of the monitoring report should sign below and submit this form with
G W-59 forms for required wells to the address provided at the top of the current G Ws9 form.
I hereby acknowledge that the above Information was evaluated and the information submitted in this report
(Cc mpliance Report GW59A) Is true and complete to the best of my knowledge.
Ill-2o�3
Signature of Pe ataa (or Autronced Aga nt) Date
GW-59A 12/9/2003

Valley Proteins, Inc - Rose Hill (WQ0000485) Groundwater Monitoring Well 2 Year Exceedance History Report
TDS 500
10A
14A
July-23
816
1270
March-23
804
1310
November-22
833
944
July-22
772
1280
March-22
783
1100
November-21
801
1230
July-21
706
1010
pH 6.5-8.5
1
2
4
7A
8A
9
10A I
11A
12B
13A
14A
July-23
5.20
5.50
5.80
5.30
5.10
6.30
3.70
5.40
4.60
4.70
4.70
March-23
6.40
6.30
6.30
3.86
4.50
6.70
4.10
4.50
4.20
4.80
5.00
November-22
5.60
6.30
3.86
4.20
6.00
3.67
4.10
3.70
4.40
4.70
July-22
6.40
6.40
6.3
5.1
5.3
6.4
4.2
4.6
4
5.1
4.9
March-22
6.40
5.9
4.7
4.6
4.6
4.4
4.2
4.7
5.2
November-21
5.50
4.30
4.50
6.30
4.00
4.30
4.20
4.20
5.00
July-21
5.00
6.10
5.60
4.90
1 4.60
5.90
4.70
4.60
5.40
5.00
TOC 10
9
July-23
46.9
March-23
33
November-22
27.6
July-22
45.1
March-22
34.9
November-21
26.4
July-21
25.9
Chloride 250
10A
14A
July-23
337
361
March-23
350
November-22
305
350
July-22
261
356
March-22
294
325
November-21
353
July-21
425
275
Sulfate 250
14A
July-23
357
March-23
375
November-22
July-22
287
March-22
277
November-21
322
July-21

SUBMIT FORM ON YELLOW PAPER ONLY
OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
EDEPARTMENT
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Pnnt Clearly or Type
PERMIT Number: WQ0000485 Expiration Date: 3/31/2025
Facility Name:
Valley Proteins Inc.- Rose Hill
Non -Discharge UIC
Permit Name (if different):
NPDES Other
Facility Address:
469 Yellow
Cut Rd.
TYPE
OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Rose Hill, NC 28458 County Duplin
0,
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name
No. of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Other
(from Peiml
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-1
Date sample collected: 7/18/2023
FIELD ANALYSES:
WAS
Well Depth: 12.46 ft.
Well Diameter: 2 in.
pH4500HB 5.20 units Temp. 000lo: 28•6 °C
DRY at
Depth to Water Level 62546: 2.1
Screened Interval: 12.46 ft.
to 2.46 ft.
Spec. Cond. 00094 µMhos
time of
Measuring Point Is 1.17 ft. above land surface
Relative M.P. Elevation:
ft.
Odor 00065: None
sampling,
Volume of water pumped/bailed before sampling:
5.0
gallons
Appearance Clear
chech�
]
Sam les for metals were collected unfiltered.
X YES
NO and field acidified X YES
NO
er :
LABORATORY INFORMATION
Date sample analyzed: 07/1812023-08/10/202-3
Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L
Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1.0
/100mL.
Nitrate (NO3) as N 00620 0.35
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus: Total as P 00665 0.06
mg/L
(Note Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 123.00
mg/L
Al Aluminum 01105
mg/L
Sodium 6.2 mg/L
pH (Lab) 00403 5.20
units
Ba - Barium 01007
ug/L
TOC oosao 0.8
mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 6
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GCIMS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 60
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? 0 Yes (0) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium oo937
mg/L
VOC 78732: method # SM 6200C
Total Ammonia oo6lo <0.2
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
method #
TKN as N 00625 <0.5
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs mglL tmuent i otai vvl,s. "'ar" •—
1.
Larry Holt - General Manager
PermrtteE for Aothon7ed Agent) Name and Title - Please print or type
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
ME1617
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
MAIL SERVICE CENTER, RALEIGH, NC 27699-1817 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: W00000485 Expiration Date 3/31/2025
Facility Name:
Valley Proteins Inc.- Rose Hill
Non -Discharge UIC
NPDES Other
Permit Name (if different):
Facility Address:
469 Yellow Cut Rd.
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Rose Hill, NC 28458 County Duplin
(zip)
X Spray Field Remediation:
Contact Person: Corey Lanier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name
No. of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Other:
(from Permd
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-2
Date sample collected: 7/18/2023
FIELD ANALYSES:
WAS
Well Depth: 31.00 It
Well Diameter: 2 in.
pH4500HB 5.50 units Temp. 000lo: 22A °C
DRY at
Depth to Water Level 02546: 12.8 ft. below measuring point
Screened Interval: 30.15 ft. to 20.1 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 000m: None
check
Volume of water um ed/bailed before sampling:
p p p 9:
5.0
gallons
9
Appearance Clear
here:
Samples for metals were collected unfiltered:
X YES 0
NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 07118/2023-08/1012023
Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead o1051 ug1L
Coliform: MF Fecal 31616 <1.0
/100mL
Nitrate (NO3) as N 00620 0.14
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus: Total as P 00665 0.11
mg/L
(Note Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units)
issolved Solids:Total 70300 350.00
mg/L
Al - Aluminum 01105
mg/L Sodium 11.8 mg/L
pH (Lab) 00403 5.50
units
Ba - Barium 01007
uglL.
TOC 00680 0.9
mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 11
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GCWS, HPLC)
Phenol 32730
ug1L
Fe - Iron 01045
ug/L (Specify test and method N. ATTACH LAB REPORT.)
Sulfate 00945 30
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? N Yes (0) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 78732: method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625 <0.5
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L tmueri I Dial vuus: „1yrL. -111-s
GW-59 Rev.812013

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Prim Clearly or Type
Facility Name Valley Proteins Inc.- Rose Hill
Permit Name (if different):
Facility Address. 469 Yellow Cut Rd,
Rose Hill, NC 28458
(31'R.I
County Duplin
Contact Person Corey Lanier Telephone#: [phone]
Well Location/Site Name No, of wells to be sampled: 11
(from Permit)
UtTMENT OF ENVIRONMENT Nl NATURAL RESOURCES
{ION OF WATER RESOURCES • INFORMATION PROCESSING UNIT
MAIL SERVICE CENTER, RALEIGR NC 27699-1617 Phone: B10.007-6306
ERMIT Number: W00000485 Expiration Date: 3/3112025
on -Discharge UIC
PDES Other
YPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-4
Date sample collected:
7/18/2023
FIELD ANALYSES:
25.7 °C
WAS
DRY at
Well Depth: 28.93 ft.
Well Diameter:
2 in.
pH4500HB 5.80 units
Temp. 000lo:
time of
Depth to Water Level 82546 4 7 ft. below measuring point
Screened Interval:
28.93 ft. to 18.93ft.
Spec. Cond. 00094:
µMhos
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation
ft.
Odor 00085
None
check
Volume of water pumped/bailed before sampling: 5.0
gallons
Appearance
Clear
here:
Samples for metals were collected unfiltered: X YES ❑
NO and field acidified. X YES f j NO
LABORATORY INFORMATION
Date sample analyzed 07118/2023-08/10/2023
Laboratory Name:
Environmental Chemists. Inc.
Certification No. DWO#94
PARAMETERS NOTE: Values should reflect dissolved and
colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
<0.02 mg/L
Pb - Lead oio51
ug/L
Coliform: MF Fecal 31616 <1 /100mL
Nitrate (NO3) as N 00620
<0.02 mg/L
Zn - Zinc 01092
mg/L
Coliform: MF Total 31504 1100mL Phosphorus Total as P 00665
(Note Use MPN method for highly turbid samples)
issolved Solids:Total 70300
224.00
mg/L
pH (Lab) 00403
5.80
units
TOC 00680
<0.5
mg/L
Chloride 00940
5
mg/L
Arsenic 01002
ug/L
Grease and Oils 00552
mg1L
Phenol 32730
ug/L
Sulfate 00945
<5.0
mg/L
specific Conductance 00095
µMhos
Total Ammonia ooslo
<0.2
mg/L
(Ammonia Nitrogen; NH3 as N; Ammonia
Nitrogen, Total)
TKN as N 00625
<0.5
mg/L
For Remediation Systems Only (Attach Lab Reports):
GW-59 Rev.8/2013
Orthophosphate 70607
Al - Aluminum o1105
Ba - Barium 01007
Ca - Calcium oog16
Cd - Cadmium o1o27
Chromium: Total 01034
Cu - Copper 01042
Fe - Iron 01045
Hg - Mercury 71900
K - Potassium 00937
Mg - Magnesium 00927
Mn - Manganese 01055
Ni - Nickel 01067
Influent Total VOCs:
0.18 mg/L
mg/L
mg/L
ug/L
mg/L
ug/L
uglL.
mg/L
ug/L
ug/L
mg/L
mg/L
ug/L
ug/L
mg/L
Other (Specify Compounds and Concentration Units)
Sodium 8.50 m /L
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? 0 Yes (0) ❑ No (0)
VOC 78732: method # SM 6200C
method #
method #
method #
Effluent Total VOCs:
mg/L VOC Removal%

NDWATER QUALITY MONITORING:
LIANCE REPORT FORM
Name:
Name (if different):
Address:
Rose Hill, NC 28458
Please Print Clearly or Type
Valley Proteins Inc.- Rose Hill
469 Yellow Cut Rd.
County Duplin
act Person: Corey -Lanier Telephone#: [phone]
Location/Site Name: No. of wells to be sampled: 11
(from Pennll)
OF WATER RESOURCES -INFORMATION PROCESSING UNrr
LSERVICE CENTER, RALAGN,NCXUll-l617 Phons:0/9-l011t4M
Non -Discharge UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation Infiltration Gallery
X Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-7A
Date sample collected: 7/18/2023
FIELD ANALYSES:
WAS
Well Depth 16 ft.
Well Diameter. 2 in.
PI-W4101,13 5 30 units Temp. 000lo: 275 oC
DRY at
time of
Depth to Water Level e2w: 4.6 ft. below measuring point
Screened Interval: 16 ft. to 6 ft.
Spec. Cord cco5,1 uMhos
sampling,
Measuring Point Is 2.42 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00086: None
check
Volume of water pumped/bailed before sampling: 5.0 gallons
Appearance Clear
here:
Samples for metals were collected unfiltered X YES M NO
and Feld acidified: X YES ❑ NO
Date sample analyzed:
07/1812023-08/10/2023
Laboratory Name:
Environmental Chemists. Inc. Certification No. DWQ#94
PARAMETERS NOTE: Values
should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NOz) as N 00615
<0.02 mg/L
Pb - Lead o1051 ug/L
Coliform: MF Fecal31616
<1
Nitrate (N%) as N 00620
<0.02 mg/L
Zn - Zinc01092 mg/L
Coliform: MF Total 31504
_/100mL
/100mL
Phosphorus: Total as P oo665
0.07 mg/L
(Note Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units)
Dissolved Solids:Total 70300
194.00
mg/L
Al - Aluminum ol1o5
mg/L
Sodium 15.7 mg/L
pH (Lab) 00403
5.30
units
Ba - Barium 01007
ug/L
TOC oo68o
<0.5
mg/L
Ca - Calcium o0916
mg/L
Chloride 00940
68
mg/L
Cd - Cadmium 01027
uglL
Arsenic oto02
uglL
Chromium: Total o1o34
ug/L
Grease and Oils00552
mg/L
Cu - Copper oto42
mg/L
ORGANICS: (by GC, GC/MS, FiPLC)
Phenol 32730
ug/L
Fe - Iron 01045
uglL
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
17
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? 0 Yes (0) ❑ No (0)
Specific Conductance 000g5
PMhos
K - Potassium 00937
mg/L
VOC 78732 method # SM 6200C
Total Ammonia oo6lo
<0.2
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen NFtas N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
, method #
TKN as N 00625
<0.5
mg/L
Ni - Nickel 01057
ug/L
method #

DEPARTMENT OF ENVIRONMENT 8. NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 276994617 Phone: [phone]
FACILITY INFORMATION
Please Pent Clearly or Type
PERMIT Number: VV00000485 Expiratior Date: 31311202
Facility Name:
Valley Proteins Inc.- Rose Hill
Non -Discharge UIC
Permit Name (if different):
NPDES Other _
Facility Address:
469 Yellow Cut Rd.
TYPE OF PERMITTED OPERATION BEING 1`00Nl i oRI-D
91l
Rose Hill, NC 28458
County Duplin
❑ Lagoon ❑ Remediation Infitration Gallery
lc'•o tS'Ar,.i ;z,vt
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Appl cation uI Slu:i it
Well Location/Site Name Field 5 - damaged by
farm equip I to replace No. of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Other
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit):
MW-8A
Date sample collected: 7/18/2023
FIELD ANALYSES:
WAS
Well Depth: 16 ft.
Well Diameter: 2 in.
pH4500H8 5.10 units Temp. oD010 27.a aC
DRY at
time of
Depth to Water Level 82546: 5.2 ft. below
measuring point
Screened Interval: 16 ft. to
6 ft. Spec. Cond. 00094: µMhos
sampling,
Measuring Point is 2.5 ft. above land surface
Relative M.P. Elevation: ft,
Odor D0085: None
check
Volume of water pumped/bailed before Sam
0 5.0
gallons
Appearance Clear
here:❑
Samples for metals were collected unfiltered:
X YES QNO
and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 07/18/2023-08/10/2023
Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N co615 <0.02
mg/L Pb - Lead o1o51 ug/L
Colifonn: MF Fecal 31616 5
/100mL
Nitrate (NO3) as N 00620 0.23
mg/L Zn - Zinc 01092 mg/L
Colifonn: MF Total 31504
/100mL Phosphorus: Total as P ooe65 0.05
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units).
issolved Solids:Total 70300 58.00
mg/L
AI - Aluminumot tor)
mg/L Sediurn 1,48 mg/L
pH (Lab) 00403 5.10
units
Ba - Barium otom
ug/L
TOC 00680 0.80
mg/L
Ca - Calcium oogte
mg/L
Chloride oog4o <5
mg/L
Cd - Cadmium oto27
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper o1o42
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 21
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? N Yes (0) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 78732: method # SM_ 6200C
_
Total Ammonia oo6io <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
method #
(Ammonia Nitrogen; Ngas N; Ammonia Nitrogen, Total)
Mn - Manganese o1o55
ug/L ,
TKN as N 00625 <0.5
mg/L
Ni - Nickel 01067
ug/L method #
_
t
s rrrb
influent For Remediation Systems Only (Attach tab Reports): otal vvtrr� —_
Larry Holt - General Manager
Permdtee (or Authorized Agent) Name and Ti9e - Please print or type

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print clear,, 01 rypc
Facility Name: Valley Proteins Inc.- Rose Hill
Permit Name (if different):
Facility Address: 469 Yellow Cut Rd.
Rose Hill, NC 28458 County Duplin
0
Contact Person: Corey Lanier Telephone#: [phone]
Well Location/Site Name No. of wells to be sampled: 11
(from Permit)
ID NUMBER (from Permit): Ill Date sample collected
7/18/2023
DEPARTMENT OF ENVIRONMENT 6 NATURAL RESOURCES
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
Depth: 13.73 ft. Well Diameter: 2 in.
It to Water Level 82546: 3.8 ft. below measuring point Screened Interval: 13.73 ft. to 3.73 ft.
curing Point is 3.80 ft. above land surface Relative M.P. Elevation: ft.
me of water pumped/bailed before sampling: 5.0 gallons
Dies for metals were collected unfihered: X YES ❑ NO and field acidified: X YES ❑ NO
Number.
3/3112025
Dn-Discharge UIC
:)DES Other
(PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: infiltration Gallery
X Spray Field ❑ Remediation
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD ANALYSES:
pH45ooHu 6.30 units
Spec. Cond 00094
Temp.00olo: 25.4 eC
µMhos
at
of
Odor 00065: None 5ampully,
Appearance Tan checl_,
here:
Date sample analyzed: 07118/2023-08/10/2023
Laboratory Name:
Environmental Chemists, Inc.
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N oo615
0.06 mg/L Pb - Lead o1051
Coliforn: MF Fecal 31616 73
t100mL
Nitrate (NO3) as N o0620
<0.02 mg/L Zn - Zinc 01092
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
0.06 mg/L
Certification No. DWQ#94
ug/L
mg/L
(Note Use MPN method for highly turb d samples)
Orthophosphate70507
mg/L
Other (Specify Compounds and Concentration Units):
)issolved Solids:Total 70300
198.00
mg/L
Al - Aluminum o11os
mg/L
Sodium 3.45 mg/L
pH (Lab) 00403
6.30
units
Ba - Barium 01007
ug/L
TOC 00680
46.9
mg/L
Ca - Calcium 00916
mg/L
Chloride o094o
<5
mg/L
Cd - Cadmium 01027
uglL
Arsenic 01002
ug/L
Chromium: Total olo34
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron o1045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate oo945
6
mg1L
Hg - Mercury 71900
ug/L
Lab Report Attached? 0 Yes (0) ❑ No (0)
Specific Conductance 00095
uMhos
K - Potassium oo937
mg/L
VOC 7e732: , method # SM 6200C
Total Ammonia ooslo
<0.2
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; Nyas N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
_ , method #
TKN as N 00625
1.5
mg/L
Ni - Nickel 01067
ug/L
method #
Mg/t VOC Removal%
r-eimmee tOr AUMDnZtla 1jtl Li — �'- - - � - - 11---- r, • -3—

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION PfeesePrintCleadyorType
Facility Name: Valley Proteins Inc.- Rose Hill
Permit Name (if different).
Facility Address: 469 Yellow Cut Rd.
Rose Hill, NC 28458 County Duplin
Zn
(slate)
Contact Person: Corey Lanier Telephone#: [phone]
Well Location/Site Name No. of wells to be sampled: 11
(from Perm t)
DIVISION OF WATER RESOURCES . INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27691 1817 Phone: [phone]
PERMIT Number: W00000485 Expiration Date 3/31/2025
Non -Discharge UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediat`on• Infiltration Gallery
X Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
L ID NUMBER (from Permit): MW-10A
Date sample collected: 7/18/2023
FIELD ANALYSES:
WAS
Depth- 16 ft
Well Diameter. 2 in.
pH45mHe 3 70 units Temp. Doo1c 28.5 oC
DRY at
h to Water Level 82546: 3.4 ft. below measuring point
Screened Interval: 16 ft. to 6 ft.
Spec i Douse µMhos
time of
sampling,
wring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor oli None
cheep,
ne of water pumped/bailed before sampling: 5.0
gallons
Appearance Clear
here'
Dies for metals were collected unfiltered: X YES n
NO and field acidified X YES I -1 NO
late sample analyzed:
07118/2023-08/10/2023
Laboratory Name
Environmental Chemists, Inc. Certification No, DWQ#94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD oo335
mg/L
Nitrite (NO2) as N oli
<0.02 mg/L
Pb - Lead otio51 ug/L
Coliform: MF Fecal 31616
<1
/100ml-
Nitrate (NO3) as N 00620
<0 02 mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
1100mL
Phosphorus Total as P 00665
0.04 mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units)
ssolved Solids:Total 7o3oo
816.00
mg/L
Al - Aluminum o11o5
mg/L
Sodium 109 ni
pH (Lab) 00403
3.70
units
Ba - Barium olo07
ii
TOC 00680
4.1
ni
Ca - Calcium ooli
ni
Chloride 00940
337
ni
Cd - Cadmium 01027
ug/L
Arsenic 01002
11
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
ni
ORGANICS: (by GC, GCIMS, HPLC)
Phenol 32730
ug/L
Fe - Iron o1o45
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
140
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? E Yes (0) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 78732 method # SM 6200C
Total Ammonia 00610
0.40
mg/L
Mg - Magnesium oo927
ni
method #
(Ammonia Nitrogen; Ny as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
, method #
method #
TKN as N 00625
1.00
mg/L
Ni - Nickel 01067
ug/L
Larry Holt - General Managi
Pennittee (or Aulhorzed Agent) Name and Title i'iease print or type
Ssgnulure OT "rmmee i
(Date)

Mail e ri g in 11 DEPARTMENT OF ENVIRONMENT & NATURAL RttiUURLtS I
GROUNDWATER QUALITY MONITORING: e DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM and I e 1617MAIL S,ERVICECE,MTER,RALEIGH,Ncr>•e9s•1st7 Phone:[phone]-eaoe
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Valley Proteins Inc.- Rose Hill
Permit Name (if different):
Facility Address: 469 Yellow Cut Rd
Rose Hill. NC 28458 County Duplin
act Person: Corey Lanier Telephone#: [phone]
Location/Site Name No. of wells to be sampled: 11
(from Perms )
Non -Discharge UIC
N PDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
WELL ID NUMBER (from Permit): MW-11A Date sample collected: 7/18/2023
Well Depth 16 ft, Well Diameter: 2 in.
Depth to Water Level 02546: 4.9 Screened Interval: 16 ft. to 6 ft.
Measuring Point is 3.3 ft. above land surface Relative M.P. Elevation: ft.
Volume of water pumpedlbailed before sampling: 5.0 gallons
Samoles for metals were collected unfiltered. X YES rl NO and field acidified. X YES M NO
FIELD ANALYSES:
WAS
pH45o0He 5.40 units Temp.00o1( 27.6 eC
DRY at
Spec. Cond 00094 µMhos
time of
Odor 000m None
sampling,
Appearance Clear
the ft ,
here.
ate sample analyzed: 07/16/2023-08110/2023 Laboratory Name: Environmental Chemists, Inc.
ARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead most
Coliform: MF Fecal 31616 5 I100mL Nitrate (NO3) as N 00620 0.62 mg/L Zn - Zinc 01092,
Col'rfo—a RAF Total 315D4 /100mL Phosphorus: Total as P 00665 0.2 mg/L
Certification No. DWQ#94
ug/L
mg1L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
ssolved Solids:Total 70300
463.00
mg/L
AI -Aluminum o1105
mg1L
Sodium 60 7 mg/L
pH (Lab) 00403
5.40
units
Ba - Barium 01007
ug/L
TOC oo66o
2.40
mg/L
Ca - Calcium 00916
mg/L
Chloride oo94o
120
mg/L
Cd - Cadmium 01027
ug/L
Arsenicolooz
uglL
mg/L
Chromium: Total 01034
Cu - Copper 01042
uglL
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Grease and Oils 00552
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Phenol 32730
Sulfate 00945
151.0
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ■ Yes (0) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937.
mg/L
VOC 7e732: method # SM 6200C
method #
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L
ug/L
, method #
(Ammorde Nitrogen; NF)as N; Ammonia
Nltrogen, Total)
Mn -Manganese o1o55
ug/L
method #
TKN as N oo625
1.3
mg/L
Ni - Nickel 01067
rerr"I a tu, nuu w.- nyon,,,. o,,,.. ... �.. ...._ ..___-r••••--• -,r-

ROUNDWATER QUALITY MONITORING:
DMPLIANCE REPORT FORM
TY INFORMATION Please Pdnt Clearly or Type
Name: Valley Proteins Inc: Rose Hill
Name (if different):
Address: 469 Yellow Cut Rd.
County Duplin
,r.nn tr.�aa
act Person: Corey Lanier Telephone#: [phone]
Location/Site Name- No. of wells to be sampled: 11
(from Permit)
L ID NUMBER (from Permit): MW-12B
Depth: 16 ft.
h to Water Level 82546: 5.2 ft. below measuring point
:wring Point is 3 ft. above land surface
ne of water pumped/bailed before sampling: 5.0
oles for metals were collected unfiltered: X YES F
DIVISION OF WATER RESOURCES - INFORMA71ON PROCESSING UNIT
1817 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone:[phone]
PERMIT Number: WQ0000485 Expiration Dale. 3/31/2025
Non -Discharge UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
Date sample collected: 7/18/2023
Well Diameter: 2 in.
Screened Interval: 20 ft. to 10 ft.
Relative M.P. Elevation: ft.
gallons
NO and field acadified. X YES l l NO
FIELD ANALYSES: IWAS
pH4500HB. 4_60 units Temp. 00010: 26.9 eC DRY at
Spec. Cond. oom. µMhos time of
Odor 00085: None samplin
Appearance Clear cheo r
Date sample analyzed: 07/18/2023-08/10/2023 Laboratory Name: Environmental Chemists. Inc
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N oo615
<0.02 mg/L
Coliform: MF Fecal 31616
<1
/100mL
Nitrate (NO3) as N 00620
0.07 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
0.20 mg/L
(Nole Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
)issolved Solids:Total 70300
204.00
mg/L
Al - Aluminum mini
mg/L
pH (Lab) 00403
4.60
units
Be - Barium o1oo7
ug/L
TOC ool
1.40
mg/L
Ca - Calcium oo916
mg/L
Chloride oog4o
63
mg/L
Cd - Cadmium 01027_
uglL
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
Phenol 32730
ug/L
Fe - Iron o1o45
uglL
Sulfate oog45
56
mg/L
Hg - Mercury 71900
ul lL
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
Total Ammonia 00610
<0.2
mg/L
Mg - Magnesium 00927
mg/L
(Ammonia Nitrogen; NKas N; Ammonia Nitrogen. TotaQ
Mn - Manganese mo55 _
ug/L
TKN as N 00625
<0.5
mg/L
Ni - Nickel 01067
ug/L
Pb - Lead olo51
Zn - Zinc of o92
Certification No. DWQ#94
ug/L
mg/L
Other (Specify Compounds and Concentration Units).
Sodium 35.7 mglL
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? E Yes (0) ❑ No (0)
VOC 78732: method # SM 6200C
method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOIDS: mg/L Effluent Total VOCS rnpr VOC Removal'4,
Larry Holt- General N,ar'agt
P°:+n,nee(or Authorized Nr+mr_„ndNie Please print or type
(Date)

e DEPARTMENT OF ENVIRONMENT 6 NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM a 1(17MAIL SERVICE CENTER. RALEIGH,NC27699.1617 Phone:[phone]
FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WOCCOD485 Expiration Dale 313112025
Facility Name: Valley Proteins Inc: Rose Hill Non -Discharge UIC
Permit Name (if different) 77
NPDES Other _
Facility Address: 469 Yellow Cut Rd. TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill, NC 28458 County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediabon.
Contact Person: Corey Lanier Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-13A
Date sample collected: 7/18/2023
FIELD ANALYSES:
WAS
Vdell Depth: 16 ft.
Well Diameter: 2 in.
pH4500HB 4.70 units Temp. OD010: 27.7 eC
DRY at
time of
Depth to Water Level 82546: 4.2 tt. below measuring point
Screened Interval: 16 ft. to 6 ft.
Spec. Cond. 000g4: NMhos
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor00095 None
check
Volume of water pumped/bailed before sampling- 5.0 gallons
Appearance Clear/Wht tint
here:
Samoles for metals were collected unfiltered: X YES ❑ NO
and field acidified: X YES F I NO
Date sample analyzed.
07116/2023-0811012023
Laboratory Name:
Environmental Chemists, Inc.
PARAMETERS NOTE: Values
should reflect dissolved
and colloidal concentrations.
COD oo335
mg/L
Nitrite (1402) as N oo615
0.04 mg/L Pb - Lead oloei
Coliform: MF Fecal 3161s
<1 /100mL
Nitrate (NO3) as N oDs2o
<0.02 mg/L Zn - Zinc olo92
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P OD665
0.05 mg/L
Certification No. DWQ#94
ug/L
mg&
(Note Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
Jlssolveu Sollds:Total 70300
39.00
mg/L
AI - Aluminum o11o5
mg/L
Sodium 3.52 mg/L
pH (Lab) oo4o3
4.70
units
Be - Barium oloo7
ug/L
TOG Dome
<0.5
mg/L
Ca - Calcium oD916
mg/L
Chloride oo946
<5
mglL
Cd - Cadmium oto27
ug/L
Arsenic otoo2
ug/L
Chromium: Total olo34
ug/L
Grease and Oils oos52
mg/L
Cu - Coppero1o42
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
uglL
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
6.00
mg/L
Hg - Mercury 71900
_ ug/L
Lab Report Attached? 0 Yes (0) ❑ No (0)
Specific Conductance 00095
VMhos
K - Potassium oog37
mg/L
VOC 78732: method # SM 6200C
method #
Total Ammonia oD610 <0.20
mg/L
Mg - Magnesium 00927
Manganese
mg/L
ug/L
method #
(Ammonia Nitrogen; Nil as N; Ammonia
Nitrogen, Total)
Mn - oloss
,
method #
TKN as N 00625
<0.50
mg/L
Ni - Nickel o1o67
ug/L
For Remediation Systems Only (Attach Lab Reports): influent I otai VUGs mgrL cnMern I Umt vvw -1 - - - -
Larry Holt - General Manager
Penntltee (or Authorized Agent) Name and Title -Please print or type
Signature of Permnlee (or

TER QUALITY MONITORING:
E REPORT FORM
Facility Name:
Permit Name (if different):
Facility Address:
Rose Hill, NC 28458
Please Pnnt t:leany or type
illev Proteins Inc.- Rose Hill
469 Yellow Cut Rd.
County Duplin
Contact Person: Corey Lanier Telephone#: [phone],,,
Well Location/Site Name No. of wells to be sampled: 11
(from Pemdt)
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27899-1617 Phono: 919-0g7.8308
PERMIT Number: WQ0000485 Expiration Date: 3/31/2025
Non -Discharge UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
ELL ID NUMBER (from Permit): MW-14A
ell Depth: 16 ft.
tpfh to Water Level ersas: 3.6 ft. below measuring point
:asuring Point is 3 ft. above land surface
flume/ba of water pumpediled before sampling: 5.0
imples for metals were collected unfiltered: X YES M
Date sample collected: 7/18/2023
Well Diameter: 2 in
Screened Interval: 10 ft. to
Relative M.P. Elevation: ft.
gallons
NO and field acidified: X YES F1 NO
2 5 ft.
FIELD ANALYSES:
pH45DOHi3 4.70 units Temp. OOD1l: 2e.5 °C
Spec. Cond. 00094 ^µMhos
Odor 000es None
Appearance Clearrran
WAS
DRY at
time of
sampling,
checI
here:
1BORATORY INFORMATION
ite sample analyzed: 07/18/2023-08/10/2023
Laboratory Name:
Environmental Chemists. Inc. Certification No. DWQ#94
1RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N Das15
<0.02
mg/L
Pb - Lead olos1 ug/L
Coliform: MF Fecal 31616 <1.0
/100mL
Nitrate (NO3) as N oos2o
1.93
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 315o4
/100ml- Phosphorus: Total as P 00665
<0.04
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units)
;solved Solids:Total 70300 1270.00
mg/L
Al -Aluminum oilm
mg/L
Sodium 132 mg/L
pH (Lab) 00403_ 4.70
units
Be - Barium atom
ug/L
TOC oo6eo 4.20
mg/L
Ca - Calcium oo918
mg/L
Chloride oog4o 361
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron o1o45
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 357
mg/L
Hg - Mercury 71900
ug1L
Lab Report Attached? N Yes (0) ❑ No (0)
iecific Conductance ooDgs
µMhos
K - Potassium oo937
mg/L
VOC 711732: method # SM 6200C
Total Ammonia ooslo <0.20
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH as N. Ammonia Nitrogen, Total)
Mn - Manganese 01055
_
ug/L
, method #
TKN as N 00625 0.50
mg/L
Ni - Nickel 01OB7
ug/L
method #
=nr acmarliatinn Svstpms Only (Attach Lab Reports): Influent I otal VOCS mg/L Effluent Total VOCS: mg1L VOC Removal%
Larry Holt - General Manager
Permlftee (or Authorized Agent) Name and Title - Please print or type
Signature of Pe"Itlee (or Authorized

Environmental Chemists, Inc.
Alit-.
6602 Windmill. Way, Wilmington, NC 28405 a 910.392-0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28%0 • 910.347.5843Lab/Fax
ANALYTICAL A CONSULTING CHEMISTS
info�la environmentalchemismeom
Darling Ingredients - Rose Hill
Date of Report: Aug 15, 2023
Post Office Box 1026
Customer PO 0:
Rose Hill NC 28458
Customer ID: 08100027
Attention:
Report #: 2023-15377
Project ID: July- Monitoring Wells
Lab ID Sample ID:
Collect Dateffime Matrix Sampled by
23-38004 Site: MW-1
7/18/2023 12:50 PM Water jcb/envirochem
Test
Method Results Date Analyzed
Color
cdlor Clear 07/18/2023
Depth to water, ft.
Depth to water, Ft 2.1 feet 07/18/2023
Sodium
EPA200.7, Rev4.4.1994 6.20 mg/L 08/10/2023
Sulfate
EPA 300.0. Rev. 2.1,1993 60 mg/L 07/25/2023
Ammonia Nitrogen
EPA 350.1, Rev. 2.0.1993 < 0.2 mg/L 07/20/2023
Gallons bailed before sampling
GdonsBaled before samprng 5.0gallons 07/18/2023
Odor
oualtabe None 07/18/2023
Total Dissolved Solids (TDS)
SM2540C-2015 123 mg/L 07/1W023
Temperature
SM 2550 B-2010 28.8 C 07/18/2023
pH
SM 4500 H B-2011 5.2 units 07/18/2023
Total Phosphorus
SM 4W P (F-H)-2011 0.06 mg/L 08/03/2023
Total Organic Carbon (TOC)
SM 5310 B-2014 0.8 mg/L 07/25/2023
Fecal Coliform
SM 9222 D-2015 MF <1 Colonies/100ml- 07/13/2023
Chloride
SWSW CI E-2011 6 mg/L 08/10/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. zo,1993
< 0,02 mg/L
07/19/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.35 mg/L
07/25/2023
Nitrate Nitrogen
Subtmobon Method
0.35 mg/L
08/03/2023
Total Nitrogen (Caic)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev. 2.0,1993
<0.5 mg/L
08/01/2023
Total Nitrogen
Tots) Nitropen
<0.5 mg/L
08/10/2023
Report tf: 2023.15377 Page 1 of 11

Environmental Chemists, Inc*
7
• / 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
ANALYTICAL A CONSULTING CHEMISTS [e-mail]
Darling ingredients - Rose Hill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Date of Report: Aug 15, 2023
Customer PO 0:
Customer ID: 08100027
Report #: 2023.15377
Project ID: July - Monitoring Wells
Lab ID Sample ID:
Collect Datefnme Matrix Sampled by
23-38006 Site: MW-2
7/18/2023
12:35 PM Water jcb/envirochem
Test
Method
Results Date Analyzed
Color
Color
Clear
07/18/2023
Depth to water, ft.
Depth to water, Ft.
12.8 feet
07/18/2023
Sodium
EPA200.7, Rev4.4, 1994
11.8 mg/L
08/10/2023
Sulfate
EPA 300.0, Rev 2.1,1993
30 mg/L
07/25/2023
Ammonia Nitrogen
EPA 350.1, Rev. 2.0.1993
< 0.2 mg/L
07/20/2023
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
07/18/2023
Odor
Qualltafive
None
07/18/2023
Total Dissolved Solids (TDS)
SM2640C-2015
350 mg/L
07/19/2023
Temperature
SM 2550 9-2010
22.4 C
07/18/2023
pH
SM 4500 H B-2011
5.5 units
07/1812C23
Total Phosphorus
SM 45W P (F-H)-2011
0.11 mg/L
08/0312023
Total Organic Carbon (TOC)
sM53108-2014
0.9mg/L
07125/2023
Fecal Coliform
SM 9222 D-2015 MF
<1 Colonies/100ml- 07/18/2023
Chloride
SM45M G E-2011
11 mg/L
08/10/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2, Rev, 20.1993
< 0.02 mg/L
07/19/2023
N-itrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2 0.1993
0.14 mg/L
07/25/2023
Nitrate Nitrogen
Subtraction Method
0.14 mg/L
08/03/2023
Total Nitrogen (Cale)
Total lQeldahl Nitrogen (TKN)
EPA 351.2. Rev, 2.0, 1993
<0.5 mg/L
08/01/2023
Total Nitrogen
Total Nitrogen
<0.5 mg/L
08/10/2023
Report P.; 2023-15377 Page 2 of 11

:enviroodhen-i
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 -a 910.347.5943 Lab/Fax
info@environmentalchemismcom
Darling Ingredients - Rose hill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Date of Report: Aug 15, 2023
Customer PO #:
Customer ID: 08100027
Report #: 2023-15377
Project ID: July - Monitoring Wells
Lab ID Sample ID:
Collect DatelTime matrix Sampled by
23-38006 Site: MW-4
7/18/2023
12:00 PM Water jcb/envirochem
Test
Method
Results Date Analyzed
Color
Color
Clear
07/18/2023
Depth to water, ft,
Depth to water. Ft
4.7 feet
07118/2023
Sodium
EPA 200.7,ReV4A.1994
8.50mg/L
08/10/2023
Sulfate
EPA300.0, Rev. Z1.1993
<5 mg/L
07/26/2023
Ammonia Nitrogen
EPA 360.1, Rev. 2.0.1003
< 0.2 mg/L
07/20/2023
Gallons bailed before sampling
Gsrons Balled before sampling
5.0 gallons
07/18/2023
Odor
Qualtathre
None
07/18/2023
Total Dissolved Solids (TDS)
SM 2540 C-2015
224 mg/L
07/19/2023
Temperature
SM 2550 B-2010
25.7 C
07/18/2023
pH
SM 4500 H B-2011
5.8 units
0711812023
Total Phosphorus
SM 4500 P (F-H)-2011
0.18 mg/L
08103/2023
Total Organic Carbon (TOC)
SM 5310 &2014
<0.5 mg/L
07/25/2023
Fecal Coliform
SM 9=2 D-2015 MF
<1 Cotonies/100ml- 07/18/2023
Chloride
SM4500 Cl E-2011
< 5 mg/L
08/10/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA363.2. Rev. 2.0,1993
< 0.02 mg/L
07/19/2023
Nitrate+Nitrite-Nitrogen
EPA 353 Z. Rev. 7-0.1993
< 0.02 mg/L
07/2512023
Nitrate Nitrogen
SuWactin Method
<0.02 mg/L
08/03/2023
Total Nitrogen (Cale)
Total lgeldahl Nitrogen (TKN)
EPA351.2, Rev. 20.1903
<0.5 mg/L
08/01/2023
Total Nitrogen
Total Nitrogen
<0.5 mg/L
08/1012023
Report ft.; 2023.15377 Pape 3 of 11

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223Lab • 910392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252A73.5702 Lab/Fax
255-A Wilmington Highway, Jacksonvilie, NC 28540 • 910.347.5843 Lab/Fax
infoCa environmentalchemists.com
Darling Ingredients - Rose Hill Date of Report: Aug 15, 2023
Post Office Box 1026 Customer PO #:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Report #: 2023-15377
Project ID: July - Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-38007 Site: MW-7A 7/18/2023 1:25 PM Water jcb/envirochem
Test Method Results Date Analyzed
Color
color
Clear
07/18/2023
Depth to water, ft.
Depth to Water. FL
4.6 feet
07/18/2023
Sodium
EPA 200.7, Rev 4A. 1094
15.7 mg/L
08/10/2023
Sulfate
EPA 3W.0, Rev. 2.1.1993
17 mg/L
07/25/2023
Ammonia Nitrogen
EPA350.1, Rev. 20,1993
< 0.2 mg/L
07/20/2023
Gallons bailed before sampling
Gallons Bailed beroresemp9ng
5.0 gallons
07/18/2023
Odor
Quartagve
None
07/18/2023
Total Dissolved Solids (TDS)
SM 2540 C-2015
194 mg/L
07/19/2023
Temperature
SM 25H B-2010
27.5 C
07/18/2023
pH
SM 4500 N B-2011
5.3 units
07/18/2023
Total Phosphorus
SM 4500 P (F-I)-2011
0.07 mg/L
08/03/2023
Total Organic Carbon (TOC)
SM 5310 8-2014
<0.5 mg/L
07/25/2023
Fecal Coliform
SM 9222 D-2015 MF
<1 Colonies/100ml- 07/18/2023
Chloride
SM4500 CI E-2011
68 mg/L
08/10/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev, 2.0, 1993
< 0.02 mg/L
07/19/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev.10, 1993
< 0.02 mg/L
07P2512023
Nitrate Nitrogen
subtraction Method
<0.02 mg/L
08/03/2023
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351 2. Rev. 2.0,1993
<0.5 mg/L
08/01/2023
Total Nitrogen
Tel Nitrogen
40.5 mg/L
08110/2023
Report E: 2023-15377 Page 4 of 11

ro"W7
ANALYTICAL& CONSULTING CHEMISTS
Darling Ingredients • Rose Hill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Lab ID Sample ID:
23-38008 Site: MW-8A
Test
Color
Depth to water, ft.
Sodium
Sulfate
Ammonia Nitrogen
Gallons bailed before sampling
Odor
Total Dissolved Solids (TDS)
Temperature
pH
Total Phosphorus
Total Organic Carbon (TOC)
Fecal Coliform
Chloride
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
Nitrate+Nitrite-Nitrogen
Nitrate Nitrogen
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
Total Nitrogen
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.4735702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info@,cavironmentalchemists com
Date of Report: Aug 15, 2023
Customer PO d:
Customer ID: 08100027
Report 9: 2023-15377
Project ID: July - Monitoring Wells
Collect Date/Time Matrix
7/18/2023 1:35 PM Water
Method
Color
Depth to water. FL
EPA 200.7. Rev 4A. 1994
EPA 30D.0, Rev, 2.1. 1993
EPA 35D.1, Rev, 7-0.1993
Galms BeOed before saropring
oualitative
SM 2540 C-2016
SM 2550 B-2010
SM 4500 H 11-2011
SM 4500 P (F4i)-2011
SM 5310 B-2014
SM 0222 D-2016 MF
SM45W CI E-2011
EPA 353.2. Rev_ 20.1003
EPA 353.2, Rev. 20.1993
Subtraction Method
EPA 3612. Rev, 2.0.1093
Total Nitrogen
Results
Sampled by
jcb/envirochem
Date Analyzed
Clear
07/18/2023
5.2 feet
07/18/2023
1.48 mg/L
08/10/2023
21 mg/L
07/25/2023
< 0.2 mg/L
07/2012023
5.0 gallons
07/18/2023
None
07118/2023
58 mg/L
07/19/2023
27.4 C
07/18/2023
5.1 units
07/1812023
0.05 mg/L
08/03/2023
0.8 mg/L
07/25/2023
5 Colonies/100ml- 07/18/2023
< 5 mg/L
08/10/2023
< 0,02 mglL
07/19/2023
0.23 mg/L
07/2512023
0.23 mg/L
08/03/2023
<0.5 mg/L 08/01/2023
<0.5 mg/L 08/10/2023
Report�; 2023-16377 Page 5 of 11

r�
ANALYTICAL & CONSULTING CHEMIST'S
Darling Ingredients - Rose HIII
Post Office Box 1026
Rose Hill NC 28458
Attention:
Lab ID Sample ID:
23-38009 Site: MW 9
Test
Color
Depth to water, ft
Sodium
Sulfate
Ammonia Nitrogen
Gallons bailed before sampling
Odor
Total Dissolved Solids (TDS)
Temperature
pH
Total Phosphorus
Total Organic Carbon (TOC)
Fecal Coliform
Chloride
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
Nitrate+Nitrite-Nitrogen
Nitrate Nitrogen
Total Nitrogen (Cale)
Total Kjeldahl Nitrogen (TKN)
Total Nitrogen
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.02-23 Lab • 910.392.4424 Fax
71013owsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info@environmentalchemistscom
Date of Report: Aug 15, 2023
Customer PO 0:
Customer ID: 08100027
Report4: 2023-15377
Project ID: July - Monitoring Wells
Collect Date/7ime Matrix
7/18/2023 12:15 PM Water
Method
Color
Depth to Water. Ft.
EPA 200.7. Rev4A,1094
EPA 300.0. Rev 2.1.1993
EPA 350.1. Rev 2.0. 1993
Gallons Satkd before sempring
Qualitative
SM 2540 C-2015
SM 2550 B 2010
SM 45W H B-2011
SM 4600 P (F-H)-2011
SM 5310 8.2014
SM 0222 D2015 MF
SM4500 CI E-2011
EPA 353.2, Rev. 2 0, 1993
EPA 353.2. Rev. 20. 1993
SWtractim Method
EPA 351.2, Rev. 2.0. 1993
Total Nitrogen
Results
Sampled by
job/envirochem
Date Analyzed
Tan
07/18/2023
3.8 feet
07/18/2023
3.45 mglL
08/10/2023
6 mg/L
07/25/2023
< 0.2 mg/L
07/20/2023
5.0 gallons
07/18/2023
None
07/18/2023
198 mg/L
07119/2023
25.4 C
07/18/2023
6.3 units
07/18/2023
0.06 mg/L
08/03/2023
46.9 mg/L
07/26/2023
73 Colonies/100mL 07/18/2023
< 5 mg/L
08/10/2023
0.06 mg/L
07/19/2023
< 0.02 mg/L
07/25/2023
<0.02 mg/L
08/03/2023
1.5 mg/L 08/01/2023
1.5 mg/L 08/10/2023
Reporit: 2023-15377 Page 6 o111

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington,, NC 28405 u 910.392.0223 Lab • 910,392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 , 252,473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULInNO CHEMISTS info®environmentalchemists.com
Darling Ingredients - Rose HIII
Post Office Box 1026
Rose Hill NC 28458
Attention:
Date of Report: Aug 15, 2023
Customer PO #:
Customer ID: 08100027
Report #: 2023-15377
Project ID: July - Monitoring Wells
Lab ID Sample ID:
Collect DateITime Matrix Sampled by
23-38010 Site: MW-10A
7/1812023
11:35 AM Water jcb/envirochem
Test
Method
Results Date Analyzed
Color
color
Clear
07/18/2023
Depth to water, IL
Depth to wafer. Ft.
3.4 feet
07/18/2023
Sodium
EPA 200.7, Rev 4A 1904
109 mg/L
08/10/2023
Sulfate
EPA 3W.0, Rev. 2.1. IM
140 mg/L
07/25/2023
Ammonia Nitrogen
EPA350.1. Rev. 2.0.1093
0.4 mg/L
07/20/2023
Gallons bailed before sampling
canons Balled before san03kg
5.0 gallons
07118/2023
Odor
Qualtelive
None
07/18/2023
Total Dissolved Solids (TDS)
SM 254o C-2015
816 mg/L
07119/2023
Temperature
SM 2550 6-2010
28,5 C
07/18/2023
pH
SM 4500 H B-2011
3.7 units
07/18/2023
Estimate: result Is outside calibration range.
Total Phosphorus
SM 4600 P (F-H)-2011
0.04 mg/L
08/03/2023
Total Organic Carbon (TOC)
SM $310 B-2014
4.1 mg1L
07/26/2023
Fecal Coifform
SM a222 D-2015 MF
41 Colonies/100mL
07/18/2023
Chloride
SM45M Ci E-2011
337 mg/L
08/10/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2. Rev. 20.1993
< 0.02 mg/L
07/19/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0,1a03
< 0.02 mg/L
07/25/2023
Nitrate Nitrogen
Subtnacllon Method
<0.02 mg/L
08/03/2023
Total Nitrogen (Cale)
Total Kjeldahl Nitrogen (TKN)
EPA351.2. Rev. 2.0, 180
1.0 mg/L
08/01/2023
Total Nitrogen
Total NHrogen
1.0 mg/L
08/10/2023
Report ft 2=-15377 Page 7 of 11

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab • 910.392,4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473,5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Darling Ingredients - Rose Hill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Date of Report: Aug 15, 2023
Customer PO #:
Customer ID: 08100027
Report 9: 2023-15377
Project 10: July - Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-38011 Site: MW-11A
7/18/2023
11:05 AM Water jcb/envirochem
Test
Method
Results Date Analyzed
Color
color
Clear
07/18/2023
Depth to water, ft.
Depth to water. Ft
4.9 feet
07118/2023
Sodium
EPA200.7. PAW 4A.1994
60.7 mg/L
08/10/2023
Sulfate
EPA3W.0. Rev. 2.1.1993
151 mg/L
07/2512023
Ammonia Nitrogen
EPA 3501, Rev. 2.0,1e93
< 0.2 mg/L
07/20/2023
Gallons bailed before sampling
Galons Bailed before sampling
5,0 gallons
07/18/2023
Odor
ouardarwe
None
07/18/2023
Total Dissolved Solids (TOS)
SM 2540 C-2015
463 mg/L
07/19/2023
Temperature
SM 2550 B-2010
27.8 C
07/18/2023
PH
SM 4500 H 11-2011
5.4 units
07/18/2023
Total Phosphorus
SM 4500 P (F-H)-2011
0.20 mg/L
08/03/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
2.4 mg/L
07/26/2023
Fetal Coliform
SM =2 0-2015 MF
5 Colonies/100ml- 07/18/2023
Chloride
SM4s00 Cl E-2011
120 mg/L
08/10/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA353.2, Rev. 2.0. 1993
< 0.02 mg/L
07/19/2023
Nltrate+N-ttrite-Nitrogen
EPA 353.2, Rev. 2.0.1903
0.62 mg/L
07125/2023
Nitrate Nitrogen
Subtraction Mathod
0.62 mg/L
08/03/2023
Total Nitrogen (Cale)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2. Rev.2.0, 1993
1.3 mg/L
08/0112023
Total Nitrogen
Total Nitrogen
1.9 mg/L
08/10/2023
Repodk 2023-15377 Page 9 of 11

Environmental Chemists, Inc.
41MC4 6602 Windmill Way, Wilmington, NC 29405 a 910.392.0223 Lab . 910.392.4424 Fax
710 BOWSeitown Road, Manteo, NC 27954 o 252,473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Darling Ingredients - Rose Hill Date of Report: Aug 15, 2023
Post Office Box 1026 Customer PO #:
Rose hill NC 28458 Customer ID: 08100027
Attention: Report #: 2023-15377
Project ID: July - Monitoring Wells
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
23-38012 Site: MW-12B 7/18/2023 11:15 AM Water jcb/envirochem
Test Method Results Date Analyzed
Color
Color
Clear
07/18/2023
Depth to water, ft.
Depth to we*, Ft.
5.2 feet
07118/2023
Sodium
EPA2a0.7. Rev 4A.1994
35.7 mg/L
08/10/2023
Sulfate
EPA 300.0, Rev. 2.1,1093
56 mg/L
07/25/2023
Ammonia Nitrogen
EPA 350.1, Rev.2.0. t993
< 0.2 mg/L
07/20/2023
Gallons bailed before sampling
Gallons Balled before samplino
5.0 gallons
07/18/2023
Odor
Qualitedve
None
07118MO23
Total Dissolved Solids (TDS)
SM 2540 C-2015
204 mg/L
07/19/2023
Temperature
SM 2550 B-2010
26.9 C
07/18/2023
pH
SM 4500 H B-2011
4.6 units
07/18/2023
Total Phosphorus
SM 4500 P (F.H).2011
0.20 mg/L
08/03/2023
Total Organic Carbon (TOC)
SM 5310 6.2014
1.4 mg/L
07/26/2023
Fecal Coliform
SM 9222 0.2015 MF
<1 Colonies/100mL 07/18/2023
Chloride
SM4000 CA E-2011
63 mg/L
08/1012023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353Z Rev. 2.0,1993
< 0.02 mg/L
07/19/2023
Nitrate+Nitrite-Nitrogen
EPA353.2. Rev. 2.0, 1993
0.07 mg/L
07/2512023
Nitrate Nitrogen
Subtraction Me"
0.07 mg/L
08/03/2023
Total Nitrogen (Calo)
Total K]eldahl Nitrogen (TKN)
EPA 351.2. Rev. 2-0. 1993
<0.5 mg/L
08/01/2023
Total Nitrogen
Total Nitrogen
<0.5 mg/L
08/10/2023
Report 41:: 2023.15377 Pape a or 11

F"POP7 -77
envirochem
ANALYTICAL & CONSULTING CHEMISTS
Darling Ingredients - Rose Hill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab ■ 910,392,4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910,347.5843 Lab/Fax
[e-mail]
Date of Report: Aug 15, 2023
Customer PO #:
Customer ID: 08100027
Report #: 2023-15377
Project ID: July - Monitoring Wells
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
23-38013 Site: MW 13A
7/18/2023 11:25 AM Water jcb/envirochem
Test
Method Results Date Analyzed
Color
color Clear/W ht.tint 07/1812023
Depth to water, ft.
oepth to water, Ft 4.2 feet 07/18/2023
Sodium
EPA 200 7, Rev 4A, 1994 3.52 mg/L 08/10/2023
Sulfate
EPA300.0, Rev, 2,1.1993 5 mg/L 07/25/2023
Ammonia Nitrogen
EPA 350.1, Rev, 2 0,1993 < 0.2 mg/L 07/20/2023
Gallons bailed before sampling
Gallons SBW before sampling 5.0 gallons 07/18/2023
Odor
Qualitative None 07/18/2023
Total Dissolved Solids (TDS)
SM 2540 C-2015 39 mg/L 07/19/2023
Temperature
SM 2550 e-2010 27.7 C 07/18/2023
pH
Styr 4eoa K e-2011 4.7 units 07/18/2023
Total Phosphorus
Sid 4500 P (F4+2011 0.05 mg/L 08/03/2023
Total Organic Carbon (TOC)
SM 6310 9.2014 <0.5 mg/L 07125/2023
Fecal Coliform
SM 0=2 0.2015 MF <1 Colonies/100ml- 07/18/2023
Chloride
SM4500 CI E-2011 < 5 mg/L 08/10/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2. Rev 2,0, 1993 0.04 mg/L 07/19/2023
Nlirate+Nitrite-Nitrogen
EPA 353 2, Rev 2 0. 1993 < 0.02 mg/L 07/25/2023
Nitrate Nitrogen
Subtraction Method <0.02 mg/L 08/03/2023
Total Nitrogen (Cale)
Total Keldahl Nitrogen (TKN)
EPA 351.2, Rev_ 29,1993 <0.5 mg/L 08/01/2023
Total Nitrogen
Tatar Nitrogen <0.5 mg/L 08/10/2023
Report*: 2023.15377 Page 1 o of 11

ANALYTICAL 8 CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910,392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Pax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
info®environmentalchemists.com
Darling Ingredients - Rose Hill Date of Report: Aug 15, 2023
Post Office Box 1026 Customer PO #:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Report 0: 2023-15377
Project ID: July - Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrbt Sampled by
23-38014 Site: MW 14A 7/18/2023 1:10 PM Water jcb/envirochem
Test Method Results Date Analyzed
Color
Color
ClearfTan
07/1812023
Depth to water, ft.
Depth to Vfter• Ft
3.6 feet
07/18/2023
Sodium
EPA 200.7, Rev 4A,1904
132 mg/L
08/10/2023
Sulfate
EPA 300.0. Rev. 2 1. 1003
357 mg/L
07/25/2023
Ammonia Nitrogen
EPA 360.1. Rev.2.0.1993
< 0.2 mg/L
07/20/2023
Gallons bailed before sampling
Gafwes eeWed befaesarnpOrq
5.0 gallons
07/18/2023
Odor
ouawtive
None
07/18/2023
Total Dissolved Solids (TDS)
SM 2540 C-2015
1270 mg/L
07/19/2023
Temperature
SM 2ssa 8-2010
28.5 C
07/18/2023
PH
SM 4500 H e-2011
4.7 units
07/18/2023
Total Phosphorus
SM 4500 P (F-H)•2011
<0.04 mg/L
08/03/2023
Total Organic Carbon (TOC)
SM 5310 6-2014
4.2 mg/L
07/25/2023
Fecal Coliform
SM 9222 D-2015 MF
<1 Colonies/100ml- 07/18/2023
Chloride
W450 Ct E-2011
361 mg/L
08/10/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.02 mg/L
07/19/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev_ 2A,1923
1.93 mg/L
07/25/2023
Nitrate Nitrogen
Subbadon Method
1,93 mg/L
08/03/2023
Total Nitrogen (Cale)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev, 2.0,1993
0.5 mg/L
08/01/2023
Total Nitrogen
Total Nitrogen
2.4 mg/L
08/10/2023
Comment:
Reviewed by:
Report 1k.: 2023-15377 Page 11 of 11

Environmental Chemist, lnc., Wilmington, NC Lab #94
Sample Receipt Checklist
Client: Date: -7 lg 123 Report Number:
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Receipt of sample:
fLHEM Pickup Client Delivery ❑ JUPS ❑ FedEx ❑ Other E3
❑ YES ❑ NO
N/A
11. Were custody seals present on the cooler?
❑ YES ❑ NO
N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt Corrected temperature upon receipt 'C
How temperature taken:
❑ Temperature Blank K Against Bottles
iR Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
YES
E7 NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
0 NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑ NO
5. Were sample ID's listed on the COC?
YES
YES
❑ NO
❑ NO
6. Were samples ID's listed on sample containers?
7. Were collection date and time listed on the COC?
YES
❑ NO
B. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive in proper containers for each test?
TS[ YES
Cl NO
10. Did samples arrive in good condition for each test?
YES
❑ NO
11. Was adequate sample volume available?'
YES
❑ NO
12. Were samples received within proper holding time for requested tests?
YES
O YES
❑ NO
❑ NO
13. Were acid preserved samples received at a pH of <2?
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
1S. Were sulfide samples received at a pH >9?
YES
❑ YES
❑ NO
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2504 HNO3 HCI NaOH
rime of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain anew sample or
notify the state lab if directed to a naWed by the customer. Who was notified, date and time:
Volatiles Sample(s) Were received with headenara
COMMENTS:
DOC. QA.002 Rev 1

00 —4
oma
a e.0
% rg
9
7
a
M
ro
rA m
a
o
�
m
a
a
m
71
3
o
w
61
S
�`
V
W
o
a
4
3
0)
Sample
Type
composite
G�0G)0
)000G)nQn.n
or
,1)000
(crab
1
0
�
017
0
0-u
C)
-0
G)
In
-V
G)
-U
M
I
ner
or G}
(p or G)
I
Chlorine
�
mgll
f9
LAB lD
•
�
NUMBER
)(
NOW
-0
x
HOL
x
x
HZS00
N
rn
x
HNO3
C
f
a
x
7HI0
Z
ar
OTHER
o 0
o
0
0
1
Z
_ 0
O
ro W
a
Z
o
z
rN-n
[o
� �
c
m
IMA
M
�
o
M
�Z
X
p
D Z
m
3
M
O Z
Z
�2 D
r
S
w 0
O
wM
CA
m
r
O
z (n
# y
W _
Z
y

0 0
3
0
o
m
3
v
m
a
o
s
so
a
m
a
a
Q
m
m
�
z
3
{
�
J
v
�o
0
0
r
�
Sample
Type
Conlpaite
G�nL)0QC)Qn�O�nOn�0G)n
or
Grab
Container
G7
G)
o
Li
Gi
'd
0G7
o
Gi
'O
(Pore)
�
m
Chlorine
p
nwL
I
3
c
_..
1°
t�►B ro
�
iIT
NUMBER
11
�(
NONE
IT
a
C
X
HG T
X
X
N:804 Cal
rn u
1A.
NAON _
O 0
X
I
OL
TNIO Z li
1
oniElt r
t
m m
0
0
0
0
0
0
n
9}
t
O =
�
z 1
Q
N
rr
G
G z C
5D
L
N
r
j
Z
to f
m
a
� i
0 o Z m
O -4 -4 n C)
z
0 3 3
m o
3 O
7
m
d
L
0
O
r
z
O
n
Z
O
In
m
zZ
v
z
po
e z
m
I
m
am
Z
�r
O
S 0
l7 =,
M
CA
O
z
V
rli
mz
y

O a
m �
CL
O
O
N
7
7
1
H
a
CL
-4
l
m
A
^
K
v
n
m
t
3
-
L
o
a
c
OP
a
C
�
Semple
Type
Composite
O
n
0
0
0
n
O
n
O
n
O
n
G)
1. C)
O
n
G)
or ;
Grab
\
O-oner
O-0O-0O-9O-0O0O-0O
O'G
(Por6)
(P or
t
m
Chlorine
�
N
��
LAB ID
�
NUMBER �
�(
NONE
.�
HCL
'
X
�(
HM04
rn
;0
x
1�
HNO3
C
NAOH
<
a
x
I
Two
o
Z
a
3
m
'e
OTHER
m
O O
d
O
O
U
0 0
a"i
W
N
Z
n
Z
3
0
2
N
CL z
CD
to
°
3
Z
(7
N N
0
70
C
3
A
o
d m y
� � 5
Cto
v
g
t
3 3 �
C
_ 7
A �
O tb
N
M
zZ
v
iiv I—
�
O p0
O
o o m m Z
10 (D) 0 n T
M
Z id
3 y
0 M !n z at
v
0 C) n r m =
o D z
�• Z
M O o =
-n y m
n m
y C
o3i 0 F) U)
o 'A
2
Z V
C
V�
40 Z
n
x0 O my
Z Z O
�t � 3 -e CD
z �+ N
O
c m
ao3
M Q�
�T3
I sp
3 n
N

Z
W
O
o
IL
faD
K
m
G
S
g
EL
CD
y
3 eat
C
rL
s
w
�
3
v
N
•
o
3
J�
g
o
o
0
m
3
n
C
m
Semple
Type
CompoeHe
4)
0
Q
0
G)
0G)
0
0
0G)
00G7
n
0
0orGrob
I
G)vG)-0G)-0C)-0
-0
G)'OG)-uG)v
f
C(P or Por6)r ;
i
Chlarlee
mplL
I�
m
�LAB
ID
NUMBER
�(
NONE
X
"CL
X
X
N2804
en
m
�{
HNo3
C
KWH
0
r
a
X
nro
z
-"
0
0
0
0
I
0
.-Z
n
z
0
a
m
r
y
O
3
Z
0
(A
to
[n
m
c
o
7p
9
V

N
j
Ci
a
Z
W.
�
C
=r
ip
CL
a
g
p
16
�C
y
lotm
01
X
M
®
w
�
.O
3
r
a
a
Di
e
sample
Type
Compoalte I
G)
0
G)
0
O
0
O
0
G)
0
O
A
III
O
O
G)
0
I
G)
0
or 7
Grab
G)
-0
G)L-u
G)
Gi
G)
G)
G)
G)
-o
G)
Contal
(P ar G) G)
ChloNne
lf�
-g)L
3
�
LAS ID
O�
NUMBER
X
NONE
HOL
T
X
x ,
X
X
H2304
M
HNO3
x
Ipp�
A
NAG"
Di
I `
Z
a
X
THtO
m
OTHER
•
O
O
m
d
O
O
l
0
0
fd
N
Z
z
0
0;
3
o
CL
m
y
z
`
.Z
o
:3
(A
H
m
v
D
n
m
N
O1
7
�
3
c�
Q
E
7
C
3
7
NNN
�
m
2
n
x
0
v
0
O
m
0
M
o
<
0
m
v
n
0
0
--4
�
Q
z
m
rn
00
2
O
Q
C)
in
:
7
i�
0_
z
O
M
0
3
�
d
O
C
O
p
Z �
� Z
O 0
Lri A
z
0
M
zZ
$C
tx
o
s
A
�z
Z
0
Z
Z
v
x 0
y
v
'M
A
m
T
C/ ch
z
at
41
Z
0

�l
W
N
a
o 10
x
d
�
n
c
o
9 z
m
n
O
� R
i
a
•
m
w
m G
Ilk
S
�
J
v
�
�
O
N
i
A
A
m
�
o
ti
z
v�
a
3
m
�
Sampla
Type
Composite i
C�
G)
0
G)
n
Q
n
G)
n
G)
n
0
n
G)
n
G)
n
or
Grab
�
Container .
(Pore) ;
�
v
4
Chlorine
lit
nuyL
O
LAB ID
NUMM
)(
NONE
"Cf.
O
�(
M .
X
X
Hum
M
m
1C
NN03
M
<
O
N
Naw
�
aX
Z
1.
TMp
OTHER
�O
-n
Z
Z
O
m
O
O
n
C)}
Z
s
0
o
x
Q
O
T
CL
N
H
m
�
�
m
o
m
z
C
O
z
3
m
z
D
r
0
i
m
g
CA
//� I
W
z
0

G]
c.
8=
m
m
3
o
0CD
s
_
9 Z
m
n
a"
p
a
d
-�
m
J
�
R
A
l
�
Semple
Type
Campaelta
G)A
,nA
00000000000000
or
Grab
I
Q���G)�O-00m0
oAroAMA,D
I
ontainer
(Pore) (P or 0)
I
0
`
d
Chlorine
kA
mqfL
A
�d4
LAB ID
NUMBER 'I
�(
NONE
�(
HCl
m
:0
X
X
112SDA
m
){
��
HNO3
s
NAOH
.
z
a
X
TRIO
OTHER
m
O
O
O
O
A
A
W
W
Z
A
Z
0
m
aCD>�
p
W
O
Q
Z
m
O
3
Z
(n
N
c
D
d
CAm
Am
3
m
9
m
0<
Z-
A 0
pZ
m
ic
m
oZ
z
zrf7
a
x 0 f=d
N m
m
r —
O
z
V
m Z
y

n
n
m
0
N+
a
d
=
d
m
4t
rn
g
3
acn
R
S
a
m
FL cu
a
d
H71
o
O
n
�
m
it
t.
g
m
0
�
�
a
'a
3
m
Sample
ryI»
Composlb C.
0
n
0
0
0
n
O
n
O
n
O
n
O
n
O
n
0
n
or 3
Grob
r
m
G»O-uO-0L)'o0-00m0-0
vO�
Contslner
(PorG)
�
m
Chlorine .q
I
mglL
C
3
Jt
m
LAB ID
NUMBER
IT
X
NONE
Hm
c
k
r�
k
x
N2SO4
Vj
m N
x
r
"NO]
G m
�I
NAG"
�
ou
a
X
Two
Z u
iO3
OTHER
a
O O m
m
O
O
o
0 0 0
�
N
<
!
z 0
z
�
t
0
m
2
W
Z C
r
i
C
N
o
Z
O
rA I
f1
CA
L
mSS
c10
O
a
m r
m
ml
2,
m
=z
T
�O
fl Z
m
r
>m
o Z
Z
# D
Z
A
0
Z 0 S
C
�M
A
m
a
o
Z
4h V
COW
Z
0

s
m
I
o
tag
m
y
3
a
a G
m
N13
n
•_
1
wy
T
7
Q
m
n
�
o
v
m
C)
=r
O
CL
m
T�
Sfimple
Type
Comp-1w I
G)
n
G)
n
G)
n
ID
0
G)
A
G)
n
G)
n
G)
0
G)
n
or
Grab
I
G1
G)
v
G)
'v
G)
To
G)
"a
G)
v
G)
-0
G)
-0
G)
I
ner
l alp
I
�O
C7
Chloflne
mg/
o
LAB IC
�'
NUMBER
)(
NONE
NCL
O
x
x
yc
xssoa
w
HNO3
m
C
{�
I ,
v
MACH
Ai
I
Z
x
TUC
ai
OTHER
m
O
O
o
0
0
C)
R
W
N
Z
n
Z
n
CD
o
a
IT
r
o
oCh
z
a
D
0
�
o
m
�Z
m C
.Z'a!,
�o
m Z
r
5s m
Z
O
Z J
a.
z�
2
H0
o =,
wm
n
T
D
2
* V
toZ
0

o 0 m
� c
K
I
Af
CL
I N
+
c)
0
=
o
S
CO)
m
�
•a
o
�
v
a
M.
m
FL
06
o
r.
A
~
Is
m
c
r
m
CL
�'
0
SEMPM
Type
Composite
0A60AG)AG�AG)AOAG�A0000
or
Grab
O
G)
O
O
0'v
O-0
0-0
0-0
O'0
Container
(P or G)
d
chlodue
in
OWL
ro
s�
LAB ID
V
NUMBER
)(
NONE
i(
NCL
'D
X
)!
H2604
m
rn
m
�(
hi
I
m
HM03
C
A
r
NAOH
CL
m
TWO
z
X
r
OTHER
<
-n
2
z
z
O
O
O
n
n
m
o
w
o
CL
:0
r
--I
y
O
3ICA
p
�i
to
p
o
c
c
W
D
0
z
D•
EO
0
a
�
CL
m
s
m
of
W
o
a
w
s
x
m
=Z
e
0
z
O A30
o?
C-
o
Z
m L
o
G
m
5
z
a
O s m
z
Ort
�•
3
o
= Q
i
>
m
—
'(a M
A
�
m
G �
�•1
r
/�
2 +
y
O
w
N
�o
3
Z
O
m
r
Z
Z
O
O
��
m 0
m
3 N
641
ei N
w
Qi
O 4 ?
9 N n

A �
m
3
4c
m
a
c)
p .0
R
rt U
� � 0
C �Z
z 57,
a
� N�
z Uj
c
y� C
1 3
N�
o
N
w 3
to
a
m
Q
n
m
Q,
L
�
3
�
m
o
a
c
N
(43
m
m
+`
o
Sample
Type
Com{walte (p
G)
0
,)
n
Q
n
G)
n
Q
n
G)
0
G)
n
n
G)
C)
or a
3
Grab
Conte "Ior
(PorG)
m
o
U�
Chlorine
11
nw
c
Q'
LAB 1s 3
r
NUMBER
IT
x
u
�(
NONE
HCL
C
X
X
y(
H2804
HNO3
C
X
r
I�
NAOH�i
i
Q V
�
at
a
>C
TM10
z tl
�
�
OTHER
U
4
'
o o co 03
o
o
3
n n
w
w
Z n
z
0
1
N O
to
a
A C
N
j
Z
N
SO <
pzsN
m i
m
O
a
m
A Z
v
zra
a
�0
O
m z
DM
z
n r
i
s 0
(n _
CJ
m
a ch
a
Z V)
V
V �
Z
W