WQ0000485_Monitoring - 07-2023_20230824 (3)

Monitoring Report Submittal
Permit Number#*
Name of Facility:*
Month:* July
Report Information
Type *
GW-59
Confirmation Email Address:
Name of Submitter: *
Signature:
Date of submittal:
Initial Review
WQ0000485
Darling Ingredients - Rose Hill
Year:* 2023
Upload Document*
scan 2023-07 WQ0000485 GW-59 DIRH.pdf 3.84MB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
[e-mail]
Corey Lanier
Reviewer: Wanda.Gerald
8/24/2023
This will be filled in automatically

Is the project number correct?* WQ0000485
Is the monitoring report accepted?* Yes No
Regional Office* Wilmington
Reviewer: _anonymous
Review Date: 9/6/2023

DARLING
INGREDIENTS
August 18, 2023
Division of Water Resources
Attn: Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: Ground Water Quality Monitoring Report (GWQMR)
Darling Ingredients — Rose Hill
Permit WQ0000485
To whom it may concern,
Please find enclosed the Groundwater Quality Monitoring Compliance Report for
Surface Irrigation for the month of July 2023 for our Rose Hill Division.
Should you require any additional information or wish to discuss this matter,
please feel free to contact me at 910.289.2083 x 25119.
Sincerely,
i
Larry Holt
General Manager
cc: DI Regional Corporate Office

Permit # W00000485
(Su, one
]
Enter date monitoring results were due. (0813112023) Will this monitoring report (GW-59 and GW-59A)
be submitted after the established due date?
No
2
Was any required information missing on the GW-59 report forms?
No
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the
problems encountered in obtaining the required information.
VW--8A was damaged by farm equipment and is scheduled to be closed and replaced by Register Well Co, INC; moving the
replacement well 10' due North per DEQ direction.
3
.Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missingidentification
(plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Office for guidance
No
4
Are any monitored constituents equal to or above the established standards?
YES
If the answer to question 4 is "NO", skip to section 8
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentrations) exceeding
standards in the space provided below.,
SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR F,(CEEDANCE HISTORY REPORT
5
For the constituents identified in question 4 above, have standards been exceeded previously for the same
constituent(s) in the same well(s) In the last two years?
YES
If the answer to question 5 is "NO", skip to section 8
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards,
concentration(s) reported, and sample collection date for each occurrence (for the last two years).
SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE
IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the
Regional Office.
7
Is the permlttee implementing previously approved actions required by the Division involving this groundwater quality
problem?
YES
If the answer to question 7 is 'YES", describe those actions in the space provided below.
If the answer to question 7 is "NO". contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the oermittee to a Notice of Violation.
fines. and/or penalties.
Additional monitoring was performed to identify constituents of TOC in MW No.9 The facility has been
communicating with Mr. Geoff Kegley in the Wilmington Regional Office
8
The person completing this portion (G W-59A) of the monitoring report should sign below and submit this form with
G W-59 forms for required wells to the address provided at the top of the current G W-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this report
(Compliance Report GW-59A) istrueand complete to the best of my knowledge.
Signature of Per itteo (or Authorized Agent) Date

Valley Proteins, Inc - Rose Hill (WQ0000485) Groundwater Monitoring Well 2 Year Exceedance History Report
TDS 500
10A
July-23
816
March-23
804
November-22
833
July-22
772
March-22
783
November-21
801
July-21
706
pH 6.5-8.5
1
2
4
7A
8A
9
10A
11A
12B
13A
14A
July-23
5.20
5.50
5.80
5.30
5.10
6.30
3.70
5.40
4.60
4.70
4.70
March-23
6.40
6.30
6.30
3.86
4.50
6.70
4.10
4.50
4.20
4.80
5.00
November-22
5.60
6.30
3.86
4.20
6.00
3.67
4.10
3.70
4.40
4.70
July-22
6.40
6.40
6.3
5.1
1 5.3
6.4
4.2
4.6
4
5.1
4.9
March-22
6.40
5.9
4.7
4.6
4.6
4.4
4.2
4.7
5.2
November-21
5.50
4.30
4.50
6.30
4.00
4.30
4.20
4.20
5.00
July-21
5.00
i 6.10
5.60
4.90
4.60
5.90
4.70
4.60
5.40
5.00
TOC 10
9
July-23
46.9
March-23
33
November-22
27.6
July-22
45.1
March-22
34.9
November-21
26.4
July-21
25.9
Chloride 250
10A
14A
July-23
337
361
March-23
350
November-22
305
350
July-22
261
356
March-22
294
325
November-21
353
July-21
425
275
Sulfate 250
14A
July-23
357
March-23
375
November-22
July-22
287
March-22
277
November-21
322
July-21

SUBMIT FORM ON YELLOW PAPER ONLY
.
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
a
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: WQ0000485 Expiration Date: 3/31/2025
Facility Name:
Valley Proteins Inc.- Rose Hill
Non -Discharge UIC
NPDES Other
Permit Name (if different):
Facility Address:
469
Yellow Cut Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Rose Hill, NC 28458 County Duplin
X Spray Field El Remediation:
Contact Person Corey Lanier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name
No of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-1
Date sample collected: 7/18/2023
FIELD ANALYSES:
WAS
Well Depth: 12.46 ft.
Well Diameter: 2 in.
pH4500HB 5.20 units Temp. 000lo: 28.8 °C
DRY at
Depth to Water Level 82546: 2.1
Screened Interval: 12.46 ft. to 2.46 ft. Spec. Cond. 00094 µMhos
time of
Measuring Point is 1.17 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085 None
sampling,
Volume of water pumped/bailed before sampling:
5.0
gallons
Appearance Clear
check 7
Samples for metals were collected unfiltered:
X YES M NO and field acidified: X YES NO
here:
LABORATORY INFORMATION
Date sample analyzed: 07/18/2023-08/10/2023
Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1.0
/100mL
Nitrate (NO3) as N 00620 035
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 0.06
mg/L
(Note. Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 123.00
mg/L
Al - Aluminum 01105
mg/L Sodium 6.2 mg/L
pH (Lab) 00403 5.20
units
Ba - Barium 01007
ug/L
TOC 00680 0.8
mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 6
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 60
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? 0 Yes (0) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 78732 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625 <0.5
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.812013

SUBMIT FORM ON YELLOW PAPER ONLY
• •
•
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• •
•
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: W00000485 Expiration Date 3/31/2025
Facility Name:
Valley Proteins
Inc.- Rose Hill
Non -Discharge UIC
NPDES Other
Permit Name (if different):
Facility Address:
469 Yellow Cut Rd.
TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill, NC 28458
County Duplin
❑ Lagoon ❑ Remediation: Infiltration Gallery
(state)
(zip)
X Spray Field ❑ Remediation:
Contact Person. Corey Lanier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name
No. of wells to be sampled 11
❑ Water Source Heat Pump ❑ Other:
(from Permd
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-2
Date sample collected 7/18/2023
FIELD ANALYSES:
WAS
Well Depth: 31.00 ft.
Well Diameter: 2 in.
pH4500HB 5.50 units Temp. 000lo: 22.4 oC
DRY at
Depth to Water Level 82546: 12.8 ft. below measuring point
Screened Interval: 30.15 ft. to 20.15ft.
Spec. Cond. 00094 µMhos
time of
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft
Odor 00085 None
sampling,
check
Volume of water pumped/bailed before sampling:
5.0
gallons
Appearance Clear
here: El
Samples for metals were collected unfiltered:
X YES ❑
NO and field acidified. X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed. 07/18/2023-08/10/2023
Laboratory Name Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1.0
/100mL
Nitrate (NO3) as N 00620 0.14
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus:
Total as P 00665 0.11
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 350.00
mg/L
Al - Aluminum 01105
mg/L Sodium 11.8 mg/L
pH (Lab) 00403 5.50
units
Ba - Barium 01007
ug/L
TOC 00680 0.9
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 11
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 30
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? N Yes (0) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 78732: method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nilroga s N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625 <0.5
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Larry Holt - General Manager
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
• 11•
DEPARTMENT OF ENVIRONMENT s, NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
•,• •
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: W00000485 Expiration Date 3/31/2025
Facility Name:
Valley Proteins Inc.- Rose Hill
Non -Discharge UIC
NPDES Other
Permit Name (if different):
Facility Address:
469 Yellow Cut Rd.
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Rose Hill, NC 28458 County
Duplin
(zip)
X Spray Field ❑ Remediation:
Contact Person Corey Lanier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name
No. of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-4
Date sample collected:
7/18/2023 FIELD ANALYSES:
WAS
Well Depth: 28.93 ft.
Well Diameter:
2 in. pH4500HB 5.80 units Temp. 000lo 25.7 °C
DRY at
Depth to Water Level 82546: 4.7 ft. below measuring point Screened Interval
28 93 ft. to 18.93 ft. Spec. Cond. 00094 µMhos
time of
sampling,
Measuring Point is 3 _ ft. above land surface
Relative M.P. Elevation
ft. Odor 00085 None
check
Volume of water pumped/bailed before sampling:
5.0
gallons
Appearance Clear
here:
Samples for metals were collected unfiltered.
X YES ❑ NO and field acidified- X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed07/18/2023-08/10/2023
Laboratory Name:
Environmental Chemists, Inc Certification No. DWQ#94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
<0.02 mg/L Pb - Lead 01051 uglL
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620
<0.02 mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/1001
Phosphorus: Total as P 00665
0.18 mg/L
(Note Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 224.00
mg/L
Al -Aluminum olim
mg/L Sodium 8 50 mg/L
pH (Lab) 00403 5.80
units
Ba - Barium 01007
ug/L
TOC 00680 <0.5
mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 5
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
1
Chromium: Total 01034
1
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
uglL
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5.0
mg/L
Hg - Mercury 71900
11 Lab Report Attached? E Yes (0) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 78732: method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
ri method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
Ug/L , method #
TKN as N 00625 <0.5
mg/L
Ni - Nickel 01067
uglL method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Larry Holt - General Manager
Permittee (or Authorized Aqent) Name and Title - Please print or i
GW-59 Rev.8/2013

❑EPARTMENJ OF ENVIRONMENT& NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISIONOFWATERRESOURCES-INFORMATIONPROCESSINGUNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: W00000485 Expiration Date: 3/31/2025
Facility Name:
Valley Proteins Inc.- Rose Hill
Non -Discharge UIC
NPDES Other
Permit Name (if different):
Facility Address:
469 Yellow Cut Rd.
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Rose Hill, NC 28458 County Duplin
-` °'
X Spray Field ❑ Remediation:
Contact Person Corey Lanier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-7A
Date sample collected: 7/18/2023
FIELD ANALYSES:
WAS
Well Depth: 16 ft.
Well Diameter: 2 in.
pH4sixitta 5.30 units Temp. 00010: 27 5 °C
DRY at
Depth to Water Level 82546: 4.6 ft. below measuring
point
Screened Interval: 16 ft. to
6 ft. Spec. Cond. 00094 uMhos
time of
Measuring Point is 2.42 ft. above land surface
Relative M.P Elevation: ft.
Odor 00085: None
sampling,
Volume of water pumped/bailed before sampling:
5.0
gallons
Appearance Clear
check
here:❑
Samples for metals were collected unfiltered:
X YES i
NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 07/18/2023-08/10/2023
Laboratory Name: Environmental Chemists. Inc. Certification No. DWQ#94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus: Total as P 00665 0.07
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units)
issolved Solids:Total 70300 194.00
mg/L
At -Aluminum 01105
mg/L Sodium 15.7 mg/L
pH (Lab) 00403 5.30
units
Ba - Barium 01007
ug/L
TOC 00680 <0.5
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 68
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 17
mg/L
Hg - Mercury71900
ug/L Lab Report Attached? NYes (0) ❑ No (0)
Specific Conductance 00095
rtMhos
K - Potassium 00937
mg/L VOC 78732: method # SM 6200C
Total Ammonia oo6lo <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen, NFSas N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 <0.5
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs. mg/L Effluent I otal VUcs: mg/L vut, Kemovar7o
Larry Holt - General Manager
Permillee (or Authorized Agent) Name and Title - Please print or type

DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES- INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
16W MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: WQ0000485 Expiration Date: 3/3112025
Facility Name: Valley Proteins Inc.- Rose Hill
Non -Discharge UIC
NPDES Other
Permit Name (if different):
Facility Address: 469 Yellow Cut Rd.
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Rose Hill, NC 28458 County Duplin
." (state)
X Spray Field ❑ Remediation:
Contact Person Corey Lanier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name Field 5 - damaged by farm equip / to replace No. of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-8A
Date sample collected: 7/18/2023
FIELD ANALYSES:
WAS
Well Depth 16 ft.
Well Diameter: 2 in.
pH4500HB 5.10 units Temp. 00010: 27A °C
DRY at
Depth to Water Level 82546: 5.2 ft. below measuring point Screened Interval: 16 ft. to
6 ft. Spec. Cond. 00094 µMhos
time of
Measuring Point is 2.5 ft above land surface
Relative M.P. Elevation:
Odor 00065 None
sampling,
Volume of water pumped/bailed before Sam 0 5.0
-ft.
gallons
Appearance Clear
check
here:❑
Samples for metals were collected unfiltered: X YES L J NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 07/18/2023-08/10/2023
Laboratory Name: Environmental Chemists, Inc Certification No. DWQ#94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 5 /100mL
Nitrate (NO3) as N 00620 0.23
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665 0.05
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units)
issolved Solids:Total 70300 58.00 mg/L
Al - Aluminum oil o5
mg/L Sodium 1 48 mg/L
pH (Lab) 00403 5.10 units
Ba - Barium 01007
ug/L
TOC 00680 0.80 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 <5 mg/L
Col - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 21 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? 0 Yes (0) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L VOC 78732: method # SM 6200C
Total Ammonia 00610 <0.2 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; Nyas N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 <0.5 mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Ettluent I otal vOus: mg/L VOC memovaiw

• •
•
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
• •
•
DIVISION OF WATER RESOURCES- INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: WQ0000485 Expiration Date: 3/31/2025
Facility Name:
Valley Proteins Inc.- Rose Hill
Non -Discharge UIC
NPDES Other
Permit Name (if different):
Facility Address:
469 Yellow Cut Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Rose Hill, NC 28458 County Duplin
(Cily1
X Spray Field El Remediation:
Contact Person: Corey Lanier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name
No. of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-9
Date sample collected. 7/18/2023
FIELD ANALYSES:
WAS
Well Depth: 13.73 ft.
Well Diameter: 2 in.
pH4500HB 6.30 units Temp. 000lo 25.4 °C
DRY at
Depth to Water Level 82546: 3.8 ft. below measuring
point
Screened Interval: 13.73 ft. to
3.73 ft. Spec. Cond. 00094: µMhos
time of
Measuring Point is 3.80 ft. above land surface
Relative M.P Elevation: ft.
Odor 00085: None
sampling,
Volume of water pumped/bailed before sampling:
50
gallons
Appearance Tan
check
here:❑
Samples for metals were collected unfiltered.
X YES
NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 07/18/2023-08/10/2023
Laboratory Name: Environmental Chemists, Inc Certification No. DWQ#94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.06
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 73
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus: Total as P 00665 0.06
mg/L
(Note. Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units)
issolved Solids:Total 70300 198.00
mg/L
Al -Aluminum 01105
mg/L Sodium 3.45 mg/L
pH (Lab) 00403 6.30
units
Ba - Barium 01007
ug/L
TOC 00680 46.9
mg/L
Ca - Calcium 00916
ni
Chloride 00940 <5
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 6
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? N Yes (0) ❑ No (0)
Specific Conductance 00095
uMhos
K - Potassium 00937
mg/L VOC 78732: method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
1 method #
(Ammonia Nitrogen; Nljas N, Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 1.5
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L t-nluent i otai vuus ni VOC memoval-i.
Larry Holt - General Manager
Permittee (or Authorized Agent) Name and Title - Please print or type

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name:
Permit Name (if different):
Facility Address
Please Print Clearly or Type
Fallev Proteins Inc.- Rose Hill
469 Yellow Cut Rd.
Rose Hill, NC 28458
(State) r�^
Contact Person: Corey Lanier
Well Location/Site Name
ID NUMBER (from Permit):
MW-10A
Well Depth: 16 ft.
Depth to Water Level 82546: 3.4 ft. below measuring point
Measuring Point is 3 ft. above land surface
Volume of water pumped/bailed before sampling: 5.0
Samoles for metals were collected unfiltered: X YES
County Duplin
Telephone#: [phone]
No. of wells to be sampled: 11
(from Permit)
Date sample collected:
Well Diameter:
Screened Interval:
Relative M.P. Elevation:
7/18/2023
iEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
IVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
Non -Discharge UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
2 in.
16 ft. to 6 ft.
ft.
gallons
NO and field acidified X YES M NO
FIELD ANALYSES:
pH4500HB 3.70 units
Spec. Cond. 00094:
Temp. 000l( 28.5 oC
Odor 00085: None
Appearance Clear
uMhos
late sample analyzed
07/18/2023-08/10/2023
Laboratory Name:
Environmental Chemists, Inc. Certification No DWQ#94
ARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
<0.02 mg/L
Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616
<1
/100i
Nitrate (NO3) as N 00620
<0.02 mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/1001
Phosphorus Total as P 00665
0.04 mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units)
ssolved Solids:Total 70300
816.00
mg/L
Al - Aluminum 01105
mg/L
Sodium 109 mg/L
pH (Lab) 00403
3.70
units
Ba - Barium 01007
ug/L
TOC 00680
4.1
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940
337
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
140
mg/L
Hg - Mercury 71900
uglL
Lab Report Attached? EYes (0) ❑ No (0)
pecific Conductance 00095
uMhos
K - Potassium 00937
mg/L
VOC 78732: method # SM 6200C
Total Ammonia 00610
0.40
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NFJas N, Ammonia Nitrogen, Total)
Mn - Manganese o1o55
ug/L
, method #
TKN as N 00625
1.00
mg/L
Ni - Nickel 01067
ug/L
method #
:or Remediation Svstems Only (Attach Lab Reports):
Influent Total VOCs:
mgil Effluent
Total VOCs: mg/L VOC Removal%
WAS
DRY at
time of
sampling,

DEPARTMENT OF ENVIRONMENT S NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
,
• 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: W00000485Expiration Date. 3/31/2025
Facility Name:
Valley Proteins Inc.- Rose Hill
Non -Discharge UIC
NPDES Other
Permit Name (if different):
Facility Address:
469 Yellow Cut Rd.
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Rose Hill, NC 28458 County Duplin
, (State)
(zip)
X Spray Field ❑ Remediation:
Contact Person Corey Lanier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name
No. of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-11A
Date sample collected: 7/18/2023
FIELD ANALYSES:
WAS
Well Depth 16 ft.
Well Diameter: 2 in.
pH450oNe 5 40 units Temp. 000u 27.8 oC
DRY at
Depth to Water Level 82546: 4.9
Screened Interval: 16 ft. to
6 ft. Spec. Cond 00094 µMhos
time of
Measuring Point Is 3.3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00065 None
sampling,
Volume of water pumped/bailed before sampling:
5.0
gallons
Appearance Clear
check
here:❑
Samples for metals were collected unfiltered
X YES
NO and field acidified: X YES NO
LABORATORY INFORMATION
Date sample analyzed 07/18/2023-08/10/2023
Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE: Values should reflect dissolved and
colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 5
/100mL
Nitrate (NO3) as N 00620 0.62
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus: Total as P 00665 0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 463.00
mg/L
Al -Aluminum 01105
mg/L Sodium 60.7 mq/L
pH (Lab) 00403 5.40
units
Ba - Barium 01007
ug/L
TOC 00660 2.40
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 120
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 151.0
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? N Yes (0) ❑ No(0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 78732: method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NFias N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625 1.3
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Intluent Iotal VUGs: mg/L tTTuleni imat vuls: IrIy+L V�1' RCIIIVva. /n
Larry Holt - General Manager
Permittee (or Authorized Agent) Name and Title - Please print or type

DEPARTMENT OF ENVIRONMENT S NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: WQ0000485 Expiration Date: 3/31/2025
Facility Name:
Valley Proteins Inc.- Rose Hill
Non -Discharge UIC
NPDES Other
Permit Name (if different):
Facility Address:
469 Yellow Cut Rd.
TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill, NC 28458
County Duplin
❑ Lagoon ❑ Remediation, Infiltration Gallery
tcityl e„.,
-r
X Spray Field ❑ Remediation:
Contact Person. Corey Lanier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-12B
Date sample collected: 7/18/2023
FIELD ANALYSES:
WAS
Well Depth: 16 ft.
Well Diameter: 2 in.
pH4500HB: 4.60 units Temp. 000lo: 26.9 °C
DRY at
Depth to Water Level 82546: 5.2 ft. below measuring point
Screened Interval: 20 ft. to
10 ft. Spec. Cond. 00094: µMhos
time of
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: None
sampling,
Volume of water pumped/bailed before sampling:
5.0
gallons
Appearance Clear
check
Samples for metals were collected unfiltered:
X YES M
NO and field acidified: X YES NO
here:
LABORATORY INFORMATION
Date sample analyzed: 07/18/2023-08/10/2023
Laboratory Name: Environmental Chemists. Inc. Certification No. DWQ#94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0 02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.07
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus: Total as P 00665 0.20
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 204.00
mg/L
At - Aluminum oilo5
mg/L Sodium 35.7 mg/L
pH (Lab) 00403 4.60
units
Ba - Barium 01007
ug/L
TOC 00680 1.40
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 63
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 56
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? 0 Yes (0) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 78732: method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 <0.5
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mglL. wu Removal mo
Larry Holt - General Manager
Permittee (or Authorized Agent) Name and Title - Please print or type

DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
,
1617 MAIL SERVICE CENTER. RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: W00000485Expiration Date: 3/31/2025
Facility Name:
Valley Proteins Inc.- Rose Hill
Non -Discharge UIC
NPDES Other
Permit Name (if different):
Facility Address:
469 Yellow Cut Rd.
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Rose Hill, NC 28458 County Duplin
(City) iSf.w
Op'
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name
No. of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-13A
Date sample collected: 7/18/2023
FIELD ANALYSES:
WAS
Well Depth: 16 ft.
Well Diameter: 2 in.
pH4500HB 4.70 units Temp. 000lo: 27.7 oC
DRY at
Depth to Water Level 82546: 4.2 ft. below measuring point
Screened Interval: 16 ft. to
6 ft. Spec. Cond. 00094 omhos
time of
Measuring Point Is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085 None
sampling,
Volume of water pumped/bailed before sampling
5.0
gallons
Appearance Clear/Wht. tint
check
here:
Samples for metals were collected unfiltered:
x YES 7
NO and field acidified: X YES NO
LABORATORY INFORMATION
Date sample analyzed: 07/18/2023-08/1012023
Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.04
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus: Total as P 00665 0.05
mg/L
(Note Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 39.00
mg/L
Al - Aluminum 01105
mg/L Sodium 3.52 mg/L
pH (Lab) 00403 4.70
units
Ba - Barium 01007
ug/L
TOC 00680 <0.5
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 <5
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 5.00
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? E Yes (0) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 78732: method # SM 6200C
Total Ammonia 00610 <0.20
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NFtas N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 <0.50
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent I otal VUGS rng/L tmuent I otal vvt�s: my/L vU%- I[fflimuvdm 7n
Larry Holt - General Manager
Pennittee (or Authorized Agent) Name and Title - Please print or type

• •
DEPARTMENT OF ENVIRONMENT 8 NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
• • •
•
DIVISION OF WATER RESOURCES-INFORMATIONPROCESSINGUNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: W00000485 Expiration Date: 3/31/2025
Facility Name:
Valley Proteins
Inc.- Rose Hill
Non -Discharge UIC
NPDES Other
Permit Name (if different):
Facility Address:
469 Yellow Cut Rd.
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation Infiltration Gallery
Rose Hill, NC 28458 County Duplin
(City) (State,
X Spray Field El Remediation:
Contact Person: Corey Lanier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name
No. of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit):
MW-14A
Date sample collected: 7/18/2023
FIELD ANALYSES:
WAS
Well Depth: 16 ft.
Well Diameter: 2 in.
pH4500HB 4.70 units Temp. 000l( 28.5 °C
DRY at
Depth to Water Level 82546: 3.6 ft. below
measuring point
Screened Interval: 10 ft. to
2.5 ft. Spec. Cond. 00094 µMhos
time of
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft
Odor 00085 None
sampling,
Volume of water pumped/bailed before sampling:
5.0
gallons
Appearance Clear/Tan
check _
here:
Samples for metals were collected unfiltered:
X YES I —I
NO and field acidified: X YES NO
LABORATORY INFORMATION
Date sample analyzed: 07/18/2023-08/10/2023
Laboratory Name: Environmental Chemists. Inc Certification No DWQ#94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1.0
/100mL
Nitrate (NO3) as N 00620 1.93
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus: Total as P 00665 <0.04
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units)
issolved Solids:Total 70300 1270.00
mg/L
Al -Aluminum 01105
mg/L Sodium 132 mg/L
pH (Lab) 00403 4.70
units
Ba - Barium 01007
ug/L
TOC 00680 4.20
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 361
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 357
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? 0 Yes (0) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 78732 method # SM 6200C
Total Ammonia 00610 <0.20
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; Nljas N, Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 0.50
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs mgtL Effluent I otal VUL;s: mg/L Vvc Kenr i•
Larry Holt - General Manager
Permittee (or Authorized Agent) Name and Title - Please print or type

ANALYTICAL & CONSULTING CHEMISTS
F00,00-7 -71
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28%0 a 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Date of Report: Aug 15, 2023
Customer PO #:
Customer ID: 08100027
Report #: 2023-15377
Project ID: July - Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-38004 Site: MW-1
7/18/2023
12:50 PM Water jcb/envirochem
Test
Method
Results Date Analyzed
Color
Color
Clear
07/18/2023
Depth to water, ft.
Depth to Water. Ft
2.1 feet
07/18/2023
Sodium
EPA 200.7. Rev 4.4. 1994
6.20 mg/L
08/10/2023
Sulfate
EPA 300.0, Rev. 2.1, 1993
60 mg/L
07/25/2023
Ammonia Nitrogen
EPA 350.1. Rev. 2.0. 1993
< 0.2 mg/L
07/20/2023
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
07/18/2023
Odor
oualitaGve
None
07/18/2023
Total Dissolved Solids (TDS)
SM 2540 C-2015
123 mg/L
07/19/2023
Temperature
SM 2550 B-2010
28.8 C
07/18/2023
pH
SM 4500 H B-2011
5.2 units
07/18/2023
Total Phosphorus
SM 4500 P (F-H)-2011
0.06 mg/L
08/03/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
0.8 mg/L
07/25/2023
Fecal Coliform
SM 9222 D-2015 MF
<1 Colonies/100ml-
07/18/2023
Chloride
SM45M Cl E-2011
6 mg/L
08/10/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0,1993
< 0.02 mg/L
07/19/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.35 mg1L
07/25/2023
Nitrate Nitrogen
Subtraction Method
0.35 mg/L
08/03/2023
Total Nitrogen (Cale)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev. 2.0, 1993
<0.5 mg/L
08/01/2023
Total Nitrogen
Total Nitrogen
<0.5 mg/L
08/10/2023
Report 9..: 2023-15377 Page 1 of 11

:"enviro e-hem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Darling ingredients - Rose Hill Date of Report: Aug 15, 2023
Post Office Box 1026 Customer PO #:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Report #: 2023-15377
Project ID: July - Monitoring Wells
Lab ID Sample ID: Coliect Date/Time Matrix Sampled by
23-38005 Site: MW-2 7/18/2023 12:35 PM Water jcb/envirochem
Test Method Results Date Analyzed
Color
Color
Clear
07/18/2023
Depth to water, ft.
Depth to Water, Ft.
12.8 feet
07/18/2023
Sodium
EPA200.7, Rev 4.4,1994
11.8 mg/L
08/10/2023
.Sulfate
EPA 300.0, Rev 2.1. 1993
30 mg/L
07/25/2023
Ammonia Nitrogen
EPA 350.1. Rev. 2.0. 1993
< 0.2 mg/L
07/20/2023
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
07/18/2023
Odor
Qualitative
None
07/18/2023
Total Dissolved Solids (TDS)
SM2540C-2015
350 mg/L
07/19/2023
Temperature
SM 2550 B-2010
22.4 C
07/18/2023
pH
SM 4500 H B-2011
5.5 units
07/1812023
Total Phosphorus
SM 4500 P (F-H)-2011
0.11 mg/L
08/03/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
0.9 mg/L
07/25/2023
Fecal Coliform
SM 9222 D-2015 MF
<1 Colonies1100mL
07/18/2023
Chloride
SM4500 Cl E-2011
11 mg/L
08/10/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2, Rev, 20. 1993
< 0.02 mg/L
07/19/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2 0, 1993
0.14 mg/L
07/25/2023
Nitrate Nitrogen
subtraction Method
0.14 mg/L
08/03/2023
Total Nitrogen (Cale)
Total Kieldahl Nitrogen (TKN)
EPA 351.2, Rev, 20, 1993
<0.5 mg/L
08/01/2023
Total Nitrogen
Total Nitrogen
<0.5 mg/L
08/10/2023
ReportiF:; 2023-15377 Page 2 of i 1

F"pp--. Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/i ax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Darling Ingredients - Rose Bill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Date of Report: Aug 15, 2023
Customer PO #:
Customer ID: 08100027
Report #: 2023-15377
Project ID: July - Monitoring Wells
Lab ID Sample ID:
Collect Daterrime Matrix Sampled by
23-38006 Site: MW-4
7/18/2023
12:00 PM Water jcb/envirochem
Test
Method
Results Date Analyzed
Color
Color
Clear
07/18/2023
Depth to water, ft.
Depth to Water. Ft.
4.7 feet
07/18/2023
Sodium
EPA 200.7, Rev 4.4.1994
8.50 mgtL
08/10/2023
Sulfate
EPA 300.0, Rev. 2.1, 1993
<5 mg/L
07/25/2023
Ammonia Nitrogen
EPA 350.1, Rev. 2.0. 1903
< 0.2 mg/L
07/20/2023
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
07/18/2023
Odor
Qualitative
None
07/18/2023
Total Dissolved Solids (TDS)
SM 2540 C-2015
224 mg/L
07/19/2023
Temperature
SM 2550 B-2010
25.7 C
07/18/2023
pH
SM 4500 H B-2011
5.8 units
07/18/2023
Total Phosphorus
SM 4500 P (F-H)-2011
0.18 mg/L
08/03/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
<0.5 mg/L
07/25/2023
Fecal Coliform
SM 92220-2015 MF
<1 Colonies/100ml-
07/18/2023
Chloride
SM4500 Cl E-2011
< 5 mg/L
08/10/2023
Nitrate Nitrogen (Caic)
Nitrite Nitrogen
EPA 363.2. Rev. 2.0.1993
< 0.02 mg/L
07/19/2023
Nitrate+Nitrite-Nitrogen
EPA 353 2, Rev. 20.1993
< 0.02 mg/L
07/25/2023
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
08/03/2023
Total Nitrogen (Caic)
Total Kjeldahl Nitrogen (TKN)
EPA351,2, Rev. 2.0, 1093
<0.5 mg/L
08/01/2023
Total Nitrogen
Total Nitrogen
<0.5 mg/L
08/10/2023
Report V.-: 2023.16377 Page 3 of 11

[envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392,0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252A73.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
info`kenvironmentalchemists.com
Darling Ingredients - Rose Hill Date of Report: Aug 15, 2023
Post Office Box 1026 Customer PO #:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Report #: 2023-15377
Project ID: July - Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-38007 Site: MW-7A 7/18/2023 1:25 PM Water jcb/envirochem
Test Method Results Date Analyzed
Color
color
Clear
07/18/2023
Depth to water, ft.
Depth to Water. FL
4.6 feet
07/18/2023
Sodium
EPA 200.7, Rev 4A, 1994
15.7 mg/L
08/10/2023
Sulfate
EPA 300.0, Rev, 2.1, 1993
17 mg/L
07/25/2023
Ammonia Nitrogen
EPA350.1, Rev. 20, 1993
< 0.2 mg/L
07/20/2023
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
07/18/2023
Odor
Qualitative
None
07/18/2023
Total Dissolved Solids (TDS)
SM 2540 C-2015
194 mg/L
07/19/2023
Temperature
SM 2550 B-2010
27.5 C
07/18/2023
pH
SM 4500 H B-2011
5.3 units
07/18/2023
Total Phosphorus
SM 4500 P (F-H).2011
0.07 mg/L
08/03/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
<0.5 mg/L
07/25/2023
Fecal Coliform
SM 9222 D-2015 MF
<1 Colonies/100mL 07/18/2023
Chloride
SM4500 CI E-2011
68 mg/L
08/10/2023
Nitrate Nitrogen (Caic)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
< 0.02 mg/L
07/19/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2. Rev. 2.0, 1993
< 0.02 mg/L
07/25/2023
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
08/03/2023
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 3512. Rev. 2.0,1093
<0.5 mg/L
08/01/2023
Total Nitrogen
Total Nitrogen
40.5 mg/L
08/10/2023
Report #_: 2023-15377 Page 4 of 11

envirochem
ANALYTICAL 8 CONSULTING CHEMISTS
F"007 -747
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill
Date of Report:
Aug 15, 2023
Post Office Box 1026
Customer PO #:
Rose Hill NC 28458
Customer ID:
08100027
Attention:
Report #:
2023-15377
Project ID: July
- Monitoring Wells
Lab 1D Sample ID:
Collect Date/Time Matrix
Sampled by
23-38008 Site: MW-8A
7/18/2023 1:35 PM Water
jcb/envirochem
Test Method Results Date
Color
Color
Clear
07/18/2023
Depth to water, ft.
Depth to water. Ft.
5.2 feet
07/18/2023
Sodium
EPA 200.7, Rev 4A. 1994
1.48 mg/L
08/10/2023
Sulfate
EPA30D.0, Rex 2.1, 1993
21 mg/L
07/25/2023
Ammonia Nitrogen
EPA 350.1, Rev, 2.0, 1993
< 0.2 mg/L
07/20/2023
Gallons bailed before sampling
Gallons BaDed before sampling
5.0 gallons
07/18/2023
Odor
oualitative
None
07/18/2023
Total Dissolved Solids (TDS)
SM 2540 C-2015
58 mg/L
07/19/2023
Temperature
SM 255D 13-2010
27.4 C
07/18/2023
pH
SM 4500 H B-2011
5.1 units
07/18/2023
Total Phosphorus
SM 4500 P (F-H)-2011
0.05 mg/L
08/03/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
0.8 mg/L
07/25/2023
Fecal Coliform
SM 9222 D-2015 MF
5 Colonies/100mL 07/18/2023
Chloride
SM4500 Cl E-2011
< 5 mg/L
08/10/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2. Rev_ ZD. 1993
< 0,02 mg/L
07/19/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2. Rev. 2.0, 1993
0.23 mg/L
07/25/2023
Nitrate Nitrogen
Subtractlon Method
0.23 mg/L
08/03/2023
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 3512. Rev, 2.0. 1093
<0.5 mg/L
08/01/2023
Total Nitrogen
Total Nitrogen
<0.5 mg/L
08/10/2023
Report #.-, 2023-15377 Page 5 of 11

Environmental Chemists, Inc.
enviroche 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info*cnvironmentalchemistscom
Darling Ingredients - Rose Hill
Date of Report:
Aug 15, 2023
Post Office Box 1026
Customer PO #:
Rose Hill NC 28458
Customer ID:
08100027
Attention:
Report #:
2023-15377
Project ID: July
- Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix
Sampled by
23-38009 Site: MW-9
7/18/2023 12:15 PM Water
jcb/envirochem
Test Method Results Date Analyzed
Color
Color
Tan
07/18/2023
Depth to water, ft.
Depth to Water, Ft.
3.8 feet
07/18/2023
Sodium
EPA 200.7, Rev 4A, 1994
3.45 mg/L
08/10/2023
Sulfate
EPA 300.0, Rev 2.1. 1993
6 mg/L
07/25/2023
Ammonia Nitrogen
EPA 350.1. Rev 2.0, 1993
< 0.2 mg/L
07/20/2023
Gallons bailed before sampling
Gallons Balled before sempling
5.0 gallons
07/18/2023
Odor
Qualitative
None
07/18/2023
Total Dissolved Solids (TDS)
SM 2540 C-2015
198 mg/L
07/19/2023
Temperature
SM 2550 B-2010
25.4 C
07/18/2023
pH
SM 4500 H B-2011
6.3 units
07/18/2023
Total Phosphorus
SM 4500 P (F-H).2011
0.06 mg/L
08/03/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
46.9 mg/L
07/26/2023
Fecal Coliform
SM e222 D-2015 MF
73 Colonies/100mL 07/18/2023
Chloride
SM4500 Cl E-2011
< 5 mg/L
08/10/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2 0,1993
0.06 mg/L
07/19/2023
Nitrate+Nitrite-Nitrogen
EPA353.2. Rev.2.o, 1993
< 0.02 mg/L
07/25/2023
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
08/03/2023
Total Nitrogen (Cale)
Total Kjeldahl Nitrogen (TKN)
EPA351.2, Rev. 2.0. 1993
1.5 mg/L
08/01/2023
Total Nitrogen
Total Nitrogen
1.5 mg/L
08/10/2023
Report #:: 2023-15377 Page 6 of 11

`. ■■ ■
����� ■y
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Date of Report: Aug 15, 2023
Customer PO #:
Customer ID: 08100027
Report #: 2023-15377
Project ID: July - Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-38010 Site: MW-10A
7/18/2023
11:35 AM Water jcb/envirochem
Test
Method
Results Date Analyzed
Color
Color
Clear
07/18/2023
Depth to water, ft.
Depth to Water. Ft.
3.4 feet
07/18/2023
Sodium
EPA 200.7, Rev 4.4, 1994
109 mg/L
08/10/2023
Sulfate
EPA 300.0, Rev. 2.1,1993
140 mg/L
07/25/2023
Ammonia Nitrogen
EPA 350.1, Rev. 2.0, 1993
0.4 mg/L
07/20/2023
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
07/18/2023
Odor
Qualitative
None
07/18/2023
Total Dissolved Solids (TDS)
SM 2640 C-7015
816 mg/L
07/19/2023
Temperature
SM 2550 B-2010
28.5 C
07/18/2023
pH
SM 4500 H B-2011
3,7 units
07/18/2023
Estimate: result Is outside calibration range.
Total Phosphorus
SM 4500 P (F-H)-2011
0.04 mg/L
08/03/2023
Total Organic Carbon (TOC)
SM 5310 8-2014
4.1 mg/L
07/26/2023
Fecal Coliform
SM 9222 D-2015 MF
<1 Colonies/100ml-
07/18/2023
Chloride
SM4500 Cl E-2011
337 mg/L
08/10/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353,2, Rev. 20, 1993
< 0.02 mg/L
07/19/2023
Nitrate+Nitrite-Nitrogen
EPA 353,2, Rev. 2.0,1993
< 0.02 mg/L
07/25/2023
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
08/03/2023
Total Nitrogen (Cale)
Total Kleldahl Nitrogen (TKN)
EPA351.2. Rev. 2.0,1993
1.0 mg/L
08/01/2023
Total Nitrogen
Total Nitrogen
1.0 mg/L
08/10/2023
Report 6.: 2023.15377 Page 7 of 11

[envi7roehem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info 5environmentalchemists.com
Darling Ingredients - Rose Hill Date of Report: Aug 15, 2023
Post Office Box 1026 Customer PO #:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Report #: 2023-15377
Project ID: July - Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-38011 Site: MW-11A 7/18/2023 11:05 AM Water jcb/envirochem
Test Method Results Date Analyzed
Color
color
Clear
07/18/2023
Depth to water, ft.
Depth to Water. Ft.
4.9 feet
0711812023
Sodium
EPA200.7. Rev4.4.1994
60.7 mg/L
08/10/2023
Sulfate
EPA300.0. Rev.2.1, 1993
151 mg/L
07/25/2023
Ammonia Nitrogen
EPA 3501, Rev. 2.0. 1993
< 0.2 mg/L
07/20/2023
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
07/18/2023
Odor
Qualitative
None
07/18/2023
Total Dissolved Solids (TDS)
SM 2540 C-2016
463 mg/L
07/19/2023
Temperature
SM 2550 B-201 a
27.8 C
07/18/2023
pH
SM 4500 H B-2011
5.4 units
07/18/2023
Total Phosphorus
SM 4500 P (F-H)-2011
0.20 mg/L
08/03/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
2.4 mg/L
07/26/2023
Fecal Coliform
SM 9222 D-2015 MF
5 Colonies/100mL 07/18/2023
Chloride
SM4500 Cl E-2011
120 mg/L
08/10/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2. Rev. 2.0. 1993
< 0.02 mg/L
07/19/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.62 mg/L
07/25/2023
Nitrate Nitrogen
Subtraction Method
0.62 mg/L
08/03/2023
Total Nitrogen (Cale)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev. 20, 1993
1.3 mg/L
08/01 /2023
Total Nitrogen
Total Nitrogen
1.9 mg/L
08/10/2023
Report k 202345377 Page a of 11

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
info @4environ mentalchernists.com
Darling Ingredients - Rose Hill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Date of Report: Aug 15, 2023
Customer PO #:
Customer ID: 08100027
Report #: 2023-15377
Project ID: July - Monitoring Wells
Lab ID Sample ID:
Collect DateMme Matrix Sampled by
23-38012 Site: MW-12B
7/18/2023
11:15 AM Water jcb/envirochem
Test
Method
Results Date Analyzed
Color
Color
Clear
07/18/2023
Depth to water, ft.
Depth to Water, Ft.
5.2 feet
07/18/2023
Sodium
EPA200.7, RW4.4, 1994
35.7 mg/L
08/10/2023
Sulfate
EPA 300,0, Rev. 2.1, 1993
56 mg/L
07/25/2023
Ammonia Nitrogen
EPA 350,1, Rev. 2.0,1993
< 0.2 mg/L
07/20/2023
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
07/18/2023
Odor
Qualitative
None
07/18/2023
Total Dissolved Solids (TDS)
SM 2540 c-2015
204 mg/L
07/19/2023
Temperature
SM 2550 B-2010
26.9 C
07/18/2023
pH
SM 4500 H B-2011
4.6 units
07/18/2023
Total Phosphorus
SM 4500 P (F-H)-2011
0.20 mg/L
08/03/2023
Total Organic Carbon (TOC)
SM 5310 8-2014
1.4 mg/L
07/26/2023
Fecal Coliform
SM 9222 D-2015 MF
<1 Colonies/100ml-
07/18/2023
Chloride
SM45W CA E-2011
63 mg/L
08/10/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 3532. Rev 2.0, 1993
< 0.02 mg/L
07/19/2023
Nitrate+Nitrite-Nitrogen
EPA3532. Rev. z0, 1993
0.07 mg/L
07/25/2023
Nitrate Nitrogen
Subtraction Method
0.07 mg/L
08/03/2023
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2. Rev. 2.0, 1993
<0.5 mg/L
08/01/2023
Total Nitrogen
Total Nitrogen
<0.5 mg/L
08/10/2023
Report #:: 2023.15377 Page 9 of 11

ANALYTICAL & CONSULTING CHEMISTS
F"007- -,,"7
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392,4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info[ oenvironmentalchemists.com
Darling Ingredients - Rose Hill
Date of Report:
Aug 15, 2023
Post Office Box 1026
Customer PO #:
Rose Hill NC 28458
Customer ID:
08100027
Attention:
Report #:
2023-15377
Project ID: July
- Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix
Sampled by
23-38013 Site: MW-13A
7/18/2023 11:25 AM Water
jcb/envirochem
Test Method Results Date Analyzed
Color
color
Clear/Wht.tint
07/18/2023
Depth to water, ft.
Depth to Water, Ft,
4.2 feet
07/18/2023
Sodium
EPA 200 7, Rev 4A, 1994
3.52 mg/L
08/10/2023
Sulfate
EPA 300.0. Rev, 2,1. 1993
5 mg/L
07/25/2023
Ammonia Nitrogen
EPA 350,1, Rev, 2,0,1993
< 0.2 mg/L
07/20/2023
Gallons bailed before sampling
Gallons Bailed before sampling
5.Ogallons
07/18/2023
Odor
QualitatIve
None
07/18/2023
Total Dissolved Solids (TDS)
SM 2540 C-2015
39 mg/L
07/19/2023
Temperature
SM 2550 B-2010
27.7 C
07/18/2023
pH
SM 4500 H B-2011
4.7 units
07/18/2023
Total Phosphorus
SM 4500 P (F-H)-2011
0.05 mg/L
08/03/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
<0.5 mg/L
07/25/2023
Fecal Coliform
SM 9222 0-2015 MF
<1 Colonies/100mL 07/18/2023
Chloride
SM4500 cl E-2011
< 5 mg/L
08/10/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2, Rev 2,0,1993
0.04 mg/L
07/19/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev 2.0,1993
< 0.02 mg/L
07/25/2023
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
08/03/2023
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2. Rev_ 20, 1993
<0.5 mg/L
08/01/2023
Total Nitrogen
Total Nitrogen
<0.5 mg/L
08/10/2023
Report #': 2023-15377 Page 10 of 11

ANALYTICAL S CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 a 910,392.0223 Lab o 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Date of Report: Aug 15, 2023
Customer PO #:
Customer ID: 08100027
Report #: 2023-15377
Project ID: July - Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-38014 Site: MW-14A
7/18/2023
1:10 PM Water jcb/envirochem
Test
Method
Results Date Analyzed
Color
color
Clear/Tan
07/18/2023
Depth to water, ft.
Depth to Water. Ft.
3.6 feet
07/18/2023
Sodium
EPA 200.7, Rev4A, 1994
132 mg/L
08/10/2023
Sulfate
EPA 300.0. Rev. 2 i, 1993
357 mg/L
07/25/2023
Ammonia Nitrogen
EPA350.1, Rev, 20. 1993
< 0.2 mg/L
07/20/2023
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
07/18/2023
Odor
Qualitative
None
07/18/2023
Total Dissolved Solids (TDS)
SM 2540 C-2015
1270 mg/L
07/19/2023
Temperature
SM 2550 a-2010
28.5 C
07/18/2023
pH
SM 4500 H B-2011
4.7 units
07/18/2023
Total Phosphorus
SM 4500 P (F-H).2011
<0.04 mg/L
08/03/2023
Total Organic Carbon (TOC)
SM 5310 8•2014
4.2 mg/L
07/25/2023
Fecal Coliform
SM 9222 D-2015 MF
<1 Colonies/100mi-
07/18/2023
Chloride
SM4500 G E-2011
361 mg/L
08/10/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
< 0.02 mg/L
07/19/2023
Nitrate+ Nitrite-N itroge n
EPA 353.2, Rev_ 2.0, 1993
1.93 mg/L
07/26/2023
Nitrate Nitrogen
Subtraction Method
1,93 mg/L
08/03/2023
Total Nitrogen (Cale)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev, 2.0, 1993
0.6 mg/L
08/01/2023
Total Nitrogen
Total Nitrogen
2.4 mg/L
08/10/2023
Comment:
Reviewed by:
Reportif.- 2023-16377 Page 111 of 11

Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client:- i( Date: Report Number: 23_l 53-77
Receipt of sample:
❑ YES ❑
HEM Pickup Client Delivery ❑ JUPS ❑ FedEx ❑ Other ❑
NO
N/A 1. Were custody seals present on the cooler?
❑ YES ❑ NO N/A 2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt_ °C
How temperature taken:
Corrected temperature upon receipt
❑ Temperature Blank Against Bottles
I Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction Factor °C: 0.0
YES
❑
NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
� YES
❑
NO
4. Were proper custody procedures (relinquished/received) followed?
NO
5. Were sample ID's listed on the COC?
r
❑
NO
6. Were samples ID's listed on sample containers?
❑
NO
7. Were collection date and time listed on the COC?
❑
NO
8. Were tests to be performed listed on the COC?
YES
❑
NO
9. Did samples arrive in proper containers for each test?
YES
❑
NO
10. Did samples arrive in good condition for each test?
YES
❑
NO
11. Was adequate sample volume available?'
EYES
❑
NO
12. Were samples received within proper holding time for requested tests?
❑
NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑
NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑
NO
15. Were sulfide samples received at a pH >9?
YES
❑
NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑
N 118,
Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
Sample(s)
by adding (circle one):
(Must be completed for any sample(s) incorrectly preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain anew sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
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