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HomeMy WebLinkAboutNC0090140_Permit (Issuance)_20230831 North Carolina Department of Environmental Quality  Division of Water Resources 512 North Salisbury Street  1617 Mail Service Center  Raleigh, North Carolina 27699-1617 -- 919.707.9000 ROY COOPER Governor ELISABETH S. BISER Secretary RICHARD E. ROGERS , JR. Director South End Charlotte Owner, LLC Michael McNally, SVP 3990 Hillsboro Pike, Ste 400, Nashville TN 37215 c/o Bo Cappleman, PC, Project Manager Heart/Hickman, H&H Job No. SLC.001 2923 South Tryon Street, Suite100 Charlotte, North Carolina 28203 Subject: Issuance of New NPDES Permit NC0090140 Fulbright Laboratories Brownfields Property 1919, 1923, and 1933 South Boulevard, Charlotte Brownfields Project No. 25073-21-060 WWTP WPCS Grade PCNC Mecklenburg County Mr. Chappleman: The Division of Water Resources (the Division or DWR) hereby issues the attached NPDES permit update for the subject facility. We issue this pursuant to the requirements of North Carolina General Statute 143-215.1 and the Memorandum of Agreement between North Carolina and the U.S. Environmental Protection Agency dated October 15, 2007, or as subsequently amended. Scope of Work: The Division understands that South End Charlotte Owner, LLC [herein South End or Permittee] proposes to construct foundations and infrastructure at the subject Brownfields properties with intent to: 1. install temporary groundwater dewatering wells, 2. advance excavations below the local groundwater surface, 3. install a remediation system to treat groundwater prior to discharge, and 4. avoid long-term dewatering / treatment by applying robust waterproofing to permanent subsurface facilities. Monthly Report Submittals: Federal regulations require electronic submittal of all program reports and Monthly Discharge Monitoring Reports (DMRs). Please note that South End must successfully register for the Electronic Discharge Monitoring Report (eDMR) program. In addition, you must also fill out and submit to DWQ an Electronic Signature Agreement. By so doing, you forgo the need to submit DMR hardcopy as back-up to the eDMR [see Permit Condition A. (3.)]. DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 8/31/2023 Bo Cappleman, PC, Project Manager Heart/Hickman Issuance of Permit, July 2023 Establishing Contaminants of Concern (COCs) The Division understands that the current chemical evaluation of local groundwater is limited to site assessment data only with no treated effluent data available. Based on your application therefore, DWR has identified a list of contaminants of concern (COCs) to include those identified as detected and those thought to be present. We have also included two broader-scoped, but less frequent tests, as EPA 624.1 and 625.1, anticipating the potential need to report so-far undetected COCs [see Section A. (1.)]. For your ease of reporting, we provide a COC list as permit Section A. (4.). Lastly, we include Whole Effluent Toxicity (WET) testing [TAA6C], Monthly, as Monitor and Report only. If any parts, measurement frequencies or sampling requirements contained in this permit are unacceptable, you have the right to an adjudicatory hearing upon written request submitted within thirty (30) days following receipt of this letter. This request must take the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings (6714 Mail Service Center, Raleigh, North Carolina 27699-6714). Unless such demand is made, this decision shall be final and binding. Please note that this permit is not transferable except after notice to the Division. The Division may modify, revoke, and/or reissue this permit. This permit does not affect the Permittee’s legal obligation to obtain other permits required by the Division of Water Resources, the Division of Land Resources, the Coastal Area Management Act, or any other federal or local governments. If you have questions, or if we may provide addition assistance, please email Joe R. Corporon, P.G. of my staff at [joe.corporon@ncdenr.gov]. Sincerely, _____________________________ for Richard E. Rogers, Jr., Director Division of Water Resources Enclosure: NPDES Permit NC0090140 (Issuance of new permit) ec: DWR/NPDES Program Files Laserfiche DWR/OCU, Maureen Kinney DWR/MRO, Ed Watson, Wes Bell ATB, Cindy Moore Southern Land, Michael McNally, SVP [michael.mcnally@southernland.com] H&H, Bo Cappleman, PC Project Manager, [rcappleman@harthickman.com] DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit NC0090140 Page 1 of 13 STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES PERMIT TO DISCHARGE WASTEWATER UNDER THE NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM (NPDES) In compliance with the provisions of North Carolina General Statute 143-215.1, other lawful standards and regulations promulgated and adopted by the North Carolina Environmental Management Commission, and the Federal Water Pollution Control Act, as amended, South End Charlotte Owner, LLC Fulbright Laboratories Brownfields Property 1919, 1923, and 1933 South Blvd, Charlotte Brownfields Project Number 25073-21-060 Excavation Dewatering GW-REM Mecklenburg County to a receiving waterbody designated as an unnamed tributary (UT) to Little Sugar Creek within the Catawba River Basin, in accordance with effluent limitations, monitoring requirements, and other conditions set forth in Parts I, II, III, and IV hereof. The permit shall become effective This permit and the authorization to discharge shall expire at midnight on June 30, 2025. Signed this day for Richard E. Rogers, Jr., Director Division of Water Resources By Authority of the Environmental Management Commission DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 October 1, 2023 August 31, 2023 NPDES Permit NC0090140 Page 2 of 13 SUPPLEMENT TO PERMIT COVER SHEET [new NPDES Permit – no previous permits] South End Charlotte Owner, LLC Fulbright Laboratories Brownfields Property 1919, 1923, and 1933 South Blvd, Charlotte Brownfields Project Number 25073-21-060 is hereby authorized to: 1. install and begin operating a wastewater treatment system designed to treat contaminated groundwater generated during excavation and construction of habitable structures and new storm sewer advanced below the groundwater table, this system operating at a flow rate not to exceed 0.075 MGD with treatment facilities consisting of, but not limited to: • one (1) each equalization tank (proposed 6,000-gallon to 21,000-gallon) • one (1) each bag filter (Rain for Rent BF100 or equivalent); max flow 100 gpm / 10 micron • one (1) filter for heavy metals [HS-200 liquid phase organoclay (i.e., zeolite)] • one (1) each filter for VOCs [granular activated carbon (GAC)]; 1,900 lbs • one (1) each filter for VOCs [granular activated carbon (GAC)]; 1,000 lbs • one (1) each effluent totalizing flow meter. • appurtenant piping to the outfall these treatment facilities located at 1919, 1923, and 1933 South Blvd, Charlotte, Mecklenburg County, and 2. begin discharging from said treatment works via Outfall 00l, a designated storm-sewer inlet located SE of the sight on Weston Street (see attached map), thence to an unnamed tributary (UT) to Dairy Branch [Stream Index 11-137-8-3], a waterbody currently classified C waters within hydrological unit 03-08-34 [HUC: 030501030102] of the Catawba River Basin. DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit NC0090140 Page 3 of 13 PART I A. (1.) EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS [15A NCAC 02B .0400 et seq., 02B .0500 et seq.] WPCS Grade PC/NC [15A NCAC 08G .0302] During the period beginning on the effective date of this permit and lasting until completion, the Permittee is authorized to discharge via Outfall 001 [stormsewer inlet]. Such discharges shall be limited, monitored, and reported 1 by the Permittee as specified below: EFFLUENT CHARACTERISTICS [CAS number / Parameter Code] MONITORING CONDTIONS 2 MONITORING REQUIREMENTS Monthly Average Daily Maximum Measurement Frequency Sample Type Sample Location Flow (MGD) 50050 0.075 0.075 Episodic Recording Effluent pH (Standard Units) 00400 Not < 6.0 or > 9.0 s. u. Daily Grab Effluent Total Lead 2 (7439-92-1) 01051 0.54 ug/L 13.88 ug/L Weekly Grab Effluent Total Chromium 2 (7440-47-3) CO034 24 µg/L 183 µg/L Weekly Grab Effluent Total Arsenic 2 (7440-38-2) 01000 150 µg/L 340 µg/L Weekly Grab Effluent 1,1-dichloroethane (75-34-3) 34496 100 µg/L 100 µg/L Weekly Grab Effluent 1,1-dichloroethylene (75-35-4) 34501 3,200 ug/L 3,200 ug/L Weekly Grab Effluent Tetrachloroethylene (127-18-4) 78389 3.3 ug/L 3.3 ug/L Weekly Grab Effluent Toluene (108-88-3) 34010 11 ug/L 11 ug/L Weekly Grab Effluent Trichloroethylene (79-01-6) 39180 30 ug/L 30 ug/L Weekly Grab Effluent Vinyl chloride (75-01-4) 39175 2.4 ug/L 2.4 ug/L Weekly Grab Effluent Chloroform (67-66-3) 32106 Monitor and Report Weekly Grab Effluent 1,2-trans-dichloroethylene (156-60-5) 34546 Monitor and Report Weekly Grab Effluent Total Hardness (mg/L) 2 [CaCO3 or Ca + Mg] 00900 Monitor and Report Monthly Grab Effluent WET-testing, Acute 3 TAA6C Monitor and Report Monthly Grab Effluent Organics, Total Purgeable (VOCs) 4 (µg/L), EPA Method 624.1 76029 Monitor and report Monthly Grab Effluent Base Neutrals & Acids Semi-VOCs 4 (µg/L), EPA Method 625.1 76028 Monitor and report Monthly Grab Effluent Total PAHs (µg/L) 4 (EPA Method 8270D) CO456 Monitor and Report Monthly Grab Effluent Table 3 Footnotes: 1. The Permittee shall submit monthly Discharge Monitoring Reports (DMRs) electronically using the Division’s eDMR application system [see Condition A. (3.)]. 2. Laboratory analyses of these metals require concurrent sampling for Total Hardness. Limits reflect 15A NCAC 02B Water Quality Standards for Surface Waters. DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit NC0090140 Page 4 of 13 3. Whole Effluent Toxicity (WET) Test, Monthly [TAA6C], Acute, Monitor and Report, 48-hour static test, Pass/Fail using species Fathead Minnow (Pimephales promelas) [See Section A. (2.)]. 4. For detailed reporting requirements and options for analytes detected by EPA test Methods 8270, 624.1, and 625.1, see Special Condition A. (4.) Permit Conditions: • Chemical analyses [as limited by technology] shall be conducted at a sufficiently sensitive laboratory practical quantitation level (PQL) to determine its compliance to NC surface water quality standard, if any. • Permit limits apply at end-of-pipe [NCAC 02B. 0211(21]. Compliance problems shall be addressed through Best Management Practices [NCAC 02B. 0202]. • For the duration of this permit, the Permittee shall maintain (available for DWR inspection) all internal sampling logs and laboratory analyses conducted to verify contaminant breakthrough of internal system treatment-component. • System effluent samples shall be collected down stream of treatment, i.e., …before the effluent joins or is diluted by any other wastestream, body of water, or substance (Part II, Section D 1.); [40 CFR 122.41(j)]. A. (2.) ACUTE TOXICITY – MONITOR ONLY (Monthly) [15A NCAC 02B .0500 et seq.] The permittee shall conduct acute toxicity tests on a Monthly basis using protocols defined as definitive in EPA Document EPA-821-R-02-012 entitled Methods for Measuring the Acute Toxicity of Effluents and Receiving Waters to Freshwater and Marine Organisms. The monitoring shall be performed as a Fathead Minnow (Pimephales promelas) 48-hour static test. Effluent samples for self-monitoring purposes must be obtained during representative effluent discharge and shall be performed at the NPDES permitted final effluent discharge below all waste treatment processes. The parameter code for Pimephales promelas is TAA6C. All toxicity testing results required as part of this permit condition will be entered electronically using the Division’s eDMR system for the month in which it was performed, using the appropriate parameter code. Additionally, DWR Form AT-1 (original) is to be sent to the following address: North Carolina Division of Water Resources Water Sciences Section/Aquatic Toxicology Branch 1621 Mail Service Center Raleigh, NC 27699-1621 Or, results can be sent to the email, ATForms.ATB@ncdenr.gov. Completed Aquatic Toxicity Test Forms shall be filed with the Water Sciences Section no later than 30 days after the end of the reporting period for which the report is made. Test data shall be complete, accurate, include all supporting chemical/physical measurements and all concentration/response data, and be certified by laboratory supervisor and ORC or approved designate signature. DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit NC0090140 Page 5 of 13 Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for disinfection of the waste stream. Should there be no discharge of flow from the facility during any month, the permittee will complete the information located at the top of the aquatic toxicity (AT) test form indicating the facility name, permit number, pipe number, county, and the month/year of the report with the notation of “No Flow” in the comment area of the form. The report shall be submitted to the Water Sciences Section at the address cited above. Should any test data from either these monitoring requirements or tests performed by the North Carolina Division of Water Resources indicate potential impacts to the receiving stream, this permit may be re- opened and modified to include alternate monitoring requirements or limits. NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism survival and appropriate environmental controls, shall constitute an invalid test and will require immediate follow-up testing to be completed no later than the last day of the month following the month of the initial monitoring. A. (3.) ELECTRONIC REPORTING OF MONITORING REPORTS [NCGS 143-215.1 (b)] Federal regulations require electronic submittal of all discharge monitoring reports (DMRs) and program reports. The final NPDES Electronic Reporting Rule was adopted and became effective on December 21, 2015. NOTE: This special condition supplements or supersedes the following sections within Part II of this permit (Standard Conditions for NPDES Permits): • Section B. (11.) Signatory Requirements • Section D. (2.) Reporting • Section D. (6.) Records Retention • Section E. (5.) Monitoring Reports 1. Reporting Requirements [Supersedes Section D. (2.) and Section E. (5.) (a)] The permittee shall report discharge monitoring data electronically using the NC DWR’s Electronic Discharge Monitoring Report (eDMR) internet application. Monitoring results obtained during the previous month(s) shall be summarized for each month and submitted electronically using eDMR. The eDMR system allows permitted facilities to enter monitoring data and submit DMRs electronically using the internet. The eDMR system may be accessed at: https://deq.nc.gov/about/divisions/water-resources/edmr. If a permittee is unable to use the eDMR system due to a demonstrated hardship or due to the facility being physically located in an area where less than 10 percent of the households have broadband access, then a temporary waiver from the NPDES electronic reporting requirements may be granted and discharge monitoring data may be submitted on paper DMR forms (MR 1, 1.1, 2, 3) or alternative forms approved by the Director. Duplicate signed copies shall be submitted to the following address: NC DEQ / Division of Water Resources / Water Quality Permitting Section ATTENTION: Central Files 1617 Mail Service Center DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit NC0090140 Page 6 of 13 Raleigh, North Carolina 27699-1617 See “How to Request a Waiver from Electronic Reporting” section below Regardless of the submission method, the first DMR is due on the last day of the month following the issuance of the permit or in the case of a new facility, on the last day of the month following the commencement of discharge. Starting on December 21, 2025, the permittee must electronically report the following compliance monitoring data and reports, when applicable: • Sewer Overflow/Bypass Event Reports; • Pretreatment Program Annual Reports; and • Clean Water Act (CWA) Section 316(b) Annual Reports. The permittee may seek an electronic reporting waiver from the Division (see “How to Request a Waiver from Electronic Reporting” section below). 2. Electronic Submissions In accordance with 40 CFR 122.41(l)(9), the permittee must identify the initial recipient at the time of each electronic submission. The permittee should use the EPA’s website resources to identify the initial recipient for the electronic submission. Initial recipient of electronic NPDES information from NPDES-regulated facilities means the entity (EPA or the state authorized by EPA to implement the NPDES program) that is the designated entity for receiving electronic NPDES data [see 40 CFR 127.2(b)]. EPA plans to establish a website that will also link to the appropriate electronic reporting tool for each type of electronic submission and for each state. Instructions on how to access and use the appropriate electronic reporting tool will be available as well. Information on EPA’s NPDES Electronic Reporting Rule is found at: https://www.federalregister.gov/documents/2015/10/22/2015-24954/national-pollutant- discharge-elimination-system-npdes-electronic-reporting-rule Electronic submissions must start by the dates listed in the “Reporting Requirements” section above. 3. How to Request a Waiver from Electronic Reporting The permittee may seek a temporary electronic reporting waiver from the Division. To obtain an electronic reporting waiver, a permittee must first submit an electronic reporting waiver request to the Division. Requests for temporary electronic reporting waivers must be submitted in writing to the Division for written approval at least sixty (60) days prior to the date the facility would be required under this permit to begin submitting monitoring data and reports. The duration of a temporary waiver shall not exceed 5 years and shall thereupon expire. At such time, monitoring data and reports shall be submitted electronically to the Division unless the permittee re-applies for and is granted a new temporary electronic reporting waiver by the Division. Approved electronic reporting waivers are not transferrable. Only permittees with an approved reporting waiver request may submit monitoring data and reports on paper to the Division for the period that the approved reporting waiver request is effective. Information on eDMR and the application for a temporary electronic reporting waiver are found on the following web page: http://deq.nc.gov/about/divisions/water-resources/edmr Signatory Requirements [Supplements Section B. (11.) (b) & Supersedes Section B. (11.) (d)] All eDMRs submitted to the permit issuing authority shall be signed by a person described in Part II, Section B. (11.)(a) or by a duly authorized representative of that person as described in Part II, Section DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit NC0090140 Page 7 of 13 B. (11.)(b). A person, and not a position, must be delegated signatory authority for eDMR reporting purposes. For eDMR submissions, the person signing and submitting the DMR must obtain an eDMR user account and login credentials to access the eDMR system. For more information on North Carolina’s eDMR system, registering for eDMR and obtaining an eDMR user account, please visit the following web page: http://deq.nc.gov/about/divisions/water-resources/edmr Certification. Any person submitting an electronic DMR using the state’s eDMR system shall make the following certification [40 CFR 122.22]. NO OTHER STATEMENTS OF CERTIFICATION WILL BE ACCEPTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Records Retention [Supplements Section D. (6.)] The permittee shall retain records of all Discharge Monitoring Reports, including eDMR submissions. These records or copies shall be maintained for a period of at least 3 years from the date of the report. This period may be extended by request of the Director at any time [40 CFR 122.41]. A. (4.) ADDITIONAL MONITORING AND REPORTING [G.S. 143-215.1(B)] (a.) EPA Method 624.1 – Organics, Total Purgeables (VOCs). The permittee shall conduct Monthly effluent pollutant scans using protocols as defined in E.P.A. Document EPA 821-R-16-008 entitled “Method 624.1: Purgeables by GC/MS”. The parameter code for reporting EPA Method 624.1 is 76029. Parameter codes for reporting analytes associated with this method are listed in EPA Method 624.1: Tables 1 and 2 below. (b.) EPA Method 625.1 – Base Neutrals & Acids (Semi-VOCs). The permittee shall conduct Monthly effluent pollutant scans using protocols as defined in E.P.A. Document EPA 821-R-16-007 entitled “Method 625.1: Base/Neutrals and Acids by GC/MS”. The parameter code for reporting EPA Method 625.1 is 76028. Parameter codes for reporting analytes associated with this method are listed in EPA Method 625.1: Tables 1, 2 and 3 below. (c.) Standard Conditions. Analytical methods shall be in accordance with 40 CFR Part 136 and shall be sufficiently sensitive to determine whether parameters are present in concentrations greater than applicable standards and criteria (See Part II. Section D. 4.). Laboratory reports shall be kept on file in accordance with records retention requirements found in Part II. Section D. 6. (d.) Effluent Scan Reporting. • For the eDMR application system, under the parameter code for the pollutant scan, indicate whether the test was performed by entering “1” for “yes” and “0” for “no”. DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit NC0090140 Page 8 of 13 • Any detection of analytes shall be entered in eDMR, using the appropriate parameter code listed in the tables below. Once an analyte is detected, the parameter should be reported in eDMR at the same monitoring frequency as the pollutant scan until further notice by the Division. • Parameter codes noted with “+” in the tables below may not currently be allowed in eDMR and will need to be added by the eDMR administrator. Please submit requests to add parameters to the appropriate eDMR contacts with the Division. • Any analytes in the tables below that do not have an assigned parameter code are noted as “No Code”. These parameters shall be noted in the comments section of eDMR by noting the analyte detected, the CAS Registry No. and the reported concentration. • A current List of Parameters Allowed for DMRs can be found at the following webpage: https://deq.nc.gov/about/divisions/water-resources/edmr/user-documentation. EPA Method 624.1: Table 1 – Purgeables * All the analytes in this table are Priority Pollutants (40 CFR part 423, appendix A). Analyte [alternative nomenclature] CAS Registry No. Parameter Code Analyte CAS Registry No. Parameter Code Acrolein 107-02-8 34210 1,3-Dichlorobenzene [meta-dichlorobenzene, 1,3-DCB] 541-73-1 34566 Acrylonitrile 107-13-1 34215 1,4-Dichlorobenzene [para-dichlorobenzene, 1,4-DCB] 106-46-7 34571 Benzene 71-43-2 34030 1,1-Dichloroethane 75-34-3 34496 Bromodichloromethane [Dichlorobromomethane] 75-27-4 32101 1,2-Dichloroethane 107-06-2 32103 Bromoform 75-25-2 32104 1,1-Dichloroethene [1,1-Dichloroethylene] 75-35-4 34501 Bromomethane [Methyl Bromide] 74-83-9 34413 trans-1,2-Dichloroethene [trans-1,2-Dichloroethylene] 156-60-5 34546 Carbon tetrachloride 56-23-5 32102 1,2-Dichloropropane 78-87-5 CO541 Chlorobenzene 108-90-7 34301 cis-1,3-Dichloropropene 10061-01-5 34704 Chloroethane 75-00-3 85811 trans-1,3-Dichloropropene 10061-02-6 34699 2-Chloroethyl vinyl ether (mixed) 110-75-8 34576 Ethyl benzene 100-41-4 34371 Chloroform 67-66-3 32106 Methylene chloride [Dichloromethane] 75-09-2 34423 Chloromethane (Methyl Chloride) 74-87-3 34418 1,1,2,2-Tetrachloroethane 79-34-5 34516 Dibromochloromethane [Chlorodibromomethane] 124-48-1 32105 Tetrachloroethene [PERC] [Tetrachloroethylene] 127-18-4 34475 1,2-Dichlorobenzene [ortho-dichlorobenzene, 1,2-DCB] 95-50-1 34536 Toluene 108-88-3 34010 EPA Method 624.1: Table 2 – Additional Purgeables Analyte [alternative nomenclature] CAS Registry No. Parameter Code Analyte CAS Registry No. Parameter Code Acetone 67-64-1 81552 Ethyl methacrylate 97-63-2 73570+ Acetonitrile [Methyl cyanide] 64047 73207 Ethylene oxide 75-21-8 76999 Acrolein 107-02-8 34210 Hexachlorobutadiene 87-63-3 CO702 Acrylonitrile 107-13-1 34215 Hexachloroethane 67-72-1 34396 Allyl alcohol [2-Propen-1-ol] 107-18-6 73505+ 2-Hexanone 591-78-6 75166+ Allyl chloride [3-Chloropropene] 107-05-1 78109+ Iodomethane 74-88-4 No Code t-Amyl ethyl ether [TAEE] 919-94-8 No Code Isobutyl alcohol 78-83-1 77033 t-Amyl methyl ether [TAME] [Tert-Amyl Methyl Ether] 994-05-8 22421 Isopropylbenzene 98-82-8 77223 Benzyl chloride 100-44-7 73128+ p-Isopropyltoluene [4-Isopropyltoluene] 99-87-6 03980+ Bromoacetone 598-31-2 No Code Methacrylonitrile 126-98-7 81593+ Bromobenzene 108-86-1 81555+ Methanol 67-56-1 77885 Bromochloromethane 74-97-5 70009+ Malonitrile 109-77-3 No Code 1,3-Butadiene 106-99-0 51695+ Methyl acetate 79-20-9 77032 n-Butanol [1-Butanol] 71-36-3 45265 Methyl acrylate 96-33-3 51010 2-Butanone [MEK] 78-93-3 78356 Methyl cyclohexane 108-87-2 No Code t-Butyl alcohol [tert-Butyl alcohol] [TBA] 75-65-0 51008 Methyl iodide 74-88-4 No Code n-Butylbenzene 104-51-8 77342 Methyl methacrylate 80-62-6 81597 sec-Butylbenzene 135-98-8 77350 4-Methyl-2-pentanone [MIBK] [Methyl isobutyl ketone] 108-10-1 78133+ t-Butylbenzene [Tert-butylbenzene] 72477 77353 Methyl-t-butyl ether [MTBE] [Methyl tert-butyl ether] 1634-04-4 22417 DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit NC0090140 Page 9 of 13 EPA Method 624.1: Table 2 – Additional Purgeables Analyte [alternative nomenclature] CAS Registry No. Parameter Code Analyte CAS Registry No. Parameter Code [Propane, 2-methoxy-2-methyl] t-Butyl ethyl ether [ETBE] [Ethyl-Tert Butyl Ether] 637-92-3 22422+ Naphthalene 91-20-3 34696 Carbon Disulfide 75-15-0 77041 Nitrobenzene 98-95-3 34447 Chloral hydrate 302-17-0 39108+ N-Nitroso-di-n-butylamine [N-Nitrosodibutylamine] 924-16-3 73609 Chloroacetonitrile 107-14-2 No Code 2-Nitropropane 79-46-9 No Code 1-Chlorobutane 109-69-3 No Code Paraldehyde 123-63-7 No Code Chlorodifluoromethane [Freon 22] 75-45-6 45028+ Pentachloroethane 76-01-7 No Code 2-Chloroethanol 107-07-3 77046+ Pentafluorobenzene 363-72-4 No Code bis (2-Chloroethyl) sulfide [Mustard Gas] 505-60-2 No Code 2-Pentanone 107-19-7 No Code 1-Chlorohexanone 20261-68-1 No Code 2-Picoline [2-Methylpyridine] 109-06-8 77088+ Chloroprene [2-chloro-1,3-butadiene] 126-99-8 81520+ 1-Propanol [n-Propyl alcohol] 71-23-8 77018+ 3-Chloropropene [Allyl chloride] 107-05-1 78109+ 2-Propanol [Isopropanol] 67-63-0 77015 3-Chloropropionitrile 542-76-7 No Code Propargyl alcohol 107-19-7 No Code 2-Chlorotoluene [Orthochlorotoluene] 95-49-8 38681 beta-Propiolactone 57-57-8 No Code 4-Chlorotoluene [p-Chlorotoluene] 106-43-4 61227+ Propionitrile [ethyl cyanide] 107-12-0 51466 Crotonaldehyde 123-73-9 77028 n-Propylamine 107-10-8 No Code Cyclohexanone 108-94-1 77097+ n-Propylbenzene 103-65-1 77224 1,2-Dibromo-3-chloropropane [Dibromochloropropane] 96-12-8 49146 Pyridine 110-86-1 77045 1,2-Dibromoethane [Ethylene dibromide] 106-93-4 73292+ Styrene 100-42-5 81708 Dibromomethane [Methylene Bromide] 74-95-3 38679 1,1,1,2-Tetrachloroethane 630-20-6 77562+ cis-1,4-Dichloro-2-butene 1476-11-5 No Code Tetrahydrofuran 109-99-9 81607 trans-1,4-Dichloro-2-butene 110-57-6 49263+ o-Toluidine 95-53-4 77142 cis-1,2-Dichloroethene [cis-1,2-DCE] [cis-1,2-Dichloroethylene] 156-59-2 77093 1,2,3-Trichlorobenzene 87-61-6 77613+ Dichlorodifluoromethane 75-71-8 34668 Trichlorofluoromethane [Freon 11] 75-69-4 34488+ 1,3-Dichloropropane 142-28-9 77173+ 1,2,3-Trichloropropane 96-18-4 77443+ 2,2-Dichloropropane 594-20-7 46366+ 1,2,3-Trimethylbenzene 526-73-8 51565+ 1,3-Dichloro-2-propanol 96-23-1 No Code 1,2,4-Trimethylbenzene 95-63-6 77222+ 1,1-Dichloropropene 563-58-6 77168+ 1,3,5-Trimethylbenzene 108-67-8 77226+ cis-1,3-Dichloropropene 10061-01-5 34704+ Vinyl acetate 108-05-4 77057+ 1:2,3:4-Diepoxybutane 1464-53-5 No Code m-Xylene [1,3-Xylene] 108-38-3 81710+ Diethyl ether [ethoxyethane] 60-29-7 81576 o-Xylene [1,2-Xylene] 95-47-6 81711+ Diisopropyl ether [DIPE] [Isopropyl ether] 108-20-3 81577 p-Xylene [1,4-Xylene] 106-42-3 34728 1,4-Dioxane [Dioxane] 123-91-1 82388 m+o- Xylene 179601-22-0 No Code Epichlorohydrin 106-89-8 81679+ m+p- Xylene 179601-23-1 85795+ Ethanol 64-17-5 77004 o+p- Xylene 136777-61-2 78121+ Ethyl acetate 141-78-6 81585 Xylene (mix of m+o+p) NA 81551 EPA Method 625.1: Table 1 – Non-Pesticide/PCB Base/Neutral Extractables * All the analytes in this table are Priority Pollutants (40 CFR part 423, appendix A). Analyte [alternative nomenclature] CAS Registry No. Parameter Code Analyte CAS Registry No. Parameter Code Acenaphthene 83-32-9 34205 3,3’-Dichlorobenzidine 91-94-1 34631 Acenaphthylene 208-96-8 34200 Diethyl phthalate 84-66-2 34336 Anthracene 120-12-7 CO220 Dimethyl phthalate 131-11-3 34341 Benzidine 92-87-5 39120 2,4-Dinitrotoluene 121-14-2 34611 Benzo(a)anthracene 56-55-3 CO526 2,6-Dinitrotoluene 606-20-2 CO626 Benzo(a)pyrene 50-32-8 34247 Di-n-octylphthalate 117-84-0 34596 Benzo(b)fluoranthene 205-99-2 34230 Fluoranthene 206-44-0 CO376 Benzo(k)fluoranthene 207-08-9 34242 Fluorene 86-73-7 34381 Benzo(ghi)perylene 191-24-2 34521 Hexachlorobenzene 118-74-1 CO700 Benzyl butyl phthalate [Butyl Benzyl Phthalate] 85-68-7 34292 Hexachlorobutadiene 87-68-3 CO702 bis(2-Chloroethoxy)methane 111-91-1 34278 Hexachloroethane 67-72-1 34396 bis(2-Ethylhexyl)phthalate 117-81-7 CO100 Indeno(1,2,3-cd)pyrene 193-39-5 34403 bis(2-Chloroisopropyl) ether [2,2’-Oxybis(1-chloropropane)] 108-60-1 34283 Isophorone 78-59-1 34408 DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit NC0090140 Page 10 of 13 EPA Method 625.1: Table 1 – Non-Pesticide/PCB Base/Neutral Extractables * All the analytes in this table are Priority Pollutants (40 CFR part 423, appendix A). Analyte [alternative nomenclature] CAS Registry No. Parameter Code Analyte CAS Registry No. Parameter Code 4-Bromophenyl phenyl ether 101-55-3 34636 Naphthalene 91-20-3 34696 2-Chloronaphthalene 91-58-7 34581 Nitrobenzene 98-95-3 34447 4-Chlorophenyl phenyl ether 7005-72-3 34641 N-Nitrosodi-n-propylamine 621-64-7 34428 Chrysene 218-01-9 34320 Phenanthrene 85-01-8 34461 Dibenz(a,h)anthracene 53-70-3 34556 Pyrene 129-00-0 34469 Di-n-butylphthalate 84-74-2 39110 1,2,4-Trichlorobenzene 120-82-1 CO551 EPA Method 625.1: Table 2 – Acid Extractables * All the analytes in this table are Priority Pollutants (40 CFR part 423, appendix A). Analyte (alternative nomenclature) CAS Registry No. Parameter Code Analyte CAS Registry No. Parameter Code 4-Chloro-3-methylphenol 59-50-7 70012 2-Nitrophenol 88-75-5 34591 2-Chlorophenol 95-57-8 34586 4-Nitrophenol 100-02-7 34646 2,4-Dichlorophenol 120-83-2 34601 Pentachlorophenol 87-86-5 39032 2,4-Dimethylphenol 105-67-9 34606 Phenol 108-95-2 34694 2,4-Dinitrophenol 51-28-5 34616 2,4,6-Trichlorophenol 88-06-2 34621 2-Methyl-4,6-dinitrophenol [4,6-dinitro-o-cresol] 534-52-1 34657 EPA Method 625.1: Table 3 – Additional Extractable Analytes Analytes noted as “*” in this table are Priority Pollutants (40 CFR part 423, appendix A). Analyte (alternative nomenclature) CAS Registry No. Parameter Code Analyte CAS Registry No. Parameter Code Acetophenone 98-86-2 81553 2,2’,4,4’,5’,6-Hexachlorobiphenyl 60145-22-4 No Code 2-Acetylaminofluorene [2-Acetyl aminoflourcene] 53-96-3 82204 Hexachlorocyclopentadiene * 77-47-4 34386+ 1-Acetyl-2-thiourea 591-08-2 No Code Hexachlorophene 70-30-4 51541+ Alachlor 15972-60-8 39161+ Hexachloropropene 1888-71-7 No Code Aldrin * 309-00-2 39330 Hexamethylphosphoramide [HMPA] 680-31-9 82196+ Ametryn 834-12-8 38402+ Hexanoic acid 142-62-1 77190+ 2-Aminoanthraquinone 117-79-3 No Code Hexazinone 51235-04-2 30264+ Aminoazobenzene 60-09-3 No Code Hydroquinone 123-31-9 77165+ 4-Aminobiphenyl [p-Aminobiphenyl] 92-67-1 77581+ Isodrin 465-73-6 51527+ 3-Amino-9-ethylcarbazole 132-32-1 No Code 2-Isopropylnaphthalene 2027-17-0 No Code Anilazine 101-05-3 No Code Isosafrole 120-58-1 No Code Aniline 62-53-3 77089 Kepone 143-50-0 81281+ o-Anisidine 90-04-0 No Code Leptophos 21609-90-5 51382+ Aramite 140-57-8 No Code Longifolene 475-20-7 No Code Atraton 1610-17-9 No Code Malachite green 569-64-2 51478+ Atrazine 1912-24-9 39033+ Malathion 121-75-5 39530 Azinphos-methyl (Guthion) 86-50-0 82616+ Maleic anhydride 108-31-6 No Code Barban 101-27-9 38418+ Merphos 150-50-5 30009+ Benzanthrone 82-05-3 No Code Mestranol 72-33-3 No Code Benzenethiol 108-98-5 No Code Methapyrilene 91-80-5 No Code Benzoic acid 65-85-0 77247 Methoxychlor 72-43-5 39480 2,3-Benzofluorene 243-17-4 No Code 2-Methylbenzothioazole 120-75-2 No Code p-Benzoquinone 106-51-4 No Code 3-Methylcholanthrene 56-49-5 61225+ Benzyl alcohol 100-51-6 77147+ 4,4’-Methylenebis(2-chloroaniline) 101-14-4 78123+ alpha-BHC * 319-84-6 39336 4,4’-Methylenebis(N,N-dimethylaniline) 101-61-1 No Code beta-BHC * 319-85-7 39338 4,5-Methylenephenanthrene 203-64-5 No Code gamma-BHC [Lindane] * 58-89-9 39344 1-Methylfluorene 1730-37-6 No Code delta-BHC * 319-86-8 34198 Methyl methanesulfonate 66-27-3 No Code Biphenyl 92-52-4 81513+ 2-Methylnaphthalene 91-57-6 77416 Bromacil 314-40-9 30311+ Methylparaoxon 950-35-6 No Code 2-Bromochlorobenzene 694-80-4 No Code Methyl parathion 298-00-0 39600+ 3-Bromochlorobenzene 108-37-2 No Code 1-Methylphenanthrene 832-69-9 No Code Bromoxynil 1689-84-5 51136 2-(Methylthio)benzothiazole 615-22-5 51079+ Butachlor 2318-4669 77860 Metolachlor 51218-45-2 39356+ Butylate [Sutan] 2008-41-5 81410+ Metribuzin 21087-64-9 82630+ n-C10 [n-decane] 124-18-5 77427 Mevinphos 7786-34-7 39600+ n-C12 [n-undecane] 1120-21-4 No Code Mexacarbate 315-18-4 38506+ n-C14 [n-tetradecane] 629-59-4 77691+ MGK 264 [Pyrodone] 113-48-4 No Code DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit NC0090140 Page 11 of 13 EPA Method 625.1: Table 3 – Additional Extractable Analytes Analytes noted as “*” in this table are Priority Pollutants (40 CFR part 423, appendix A). Analyte (alternative nomenclature) CAS Registry No. Parameter Code Analyte CAS Registry No. Parameter Code n-C16 [n-hexadecane] 544-76-3 77757+ Mirex 2385-85-5 39755 n-C18 [n-octadecane] 593-45-3 77804 Molinate [Ordram] 2212-67-1 49562+ n-C20 [n-eicosane] 112-95-8 77830+ Monocrotophos 6923-22-4 51385+ n-C22 [n-docosane] 629-97-0 77859+ Naled 300-76-5 38855+ n-C24 [n-tetracosane] 646-31-1 No Code Napropamide [Devrinol] 15299-99-7 49564+ n-C26 [n-hexacosane] 630-01-3 77901+ 1,4-Naphthoquinone 130-15-4 No Code n-C28 [n-octacosane] 630-02-4 No Code 1-Naphthylamine 134-32-7 No Code n-C30 [n-triacontane] 638-68-6 No Code 2-Naphthylamine 91-59-8 82191+ Captafol 2425-06-1 No Code 1,5-Naphthalenediamine 2243-62-1 No Code Captan 133-06-2 39640+ Nicotine 54-11-5 No Code Carbaryl [Sevin] 63-25-2 39750 5-Nitroacenaphthene 602-87-9 No Code Carbazole 86-74-8 77571 2-Nitroaniline 88-74-4 78306+ Carbofuran 1563-66-2 81405+ 3-Nitroaniline 99-09-2 78300+ Carboxin 5234-68-4 No Code 4-Nitroaniline 100-01-6 78870+ Carbophenothion [Trithion] 786-19-6 51042+ 5-Nitro-o-anisidine 99-59-2 No Code Chlordane * 57-74-9 51032+ 4-Nitrobiphenyl 92-93-3 No Code bis(2-Chloroethyl) ether * 111-44-4 34273 Nitrofen 1836-75-5 No Code Chloroneb 2675-77-6 51139+ 5-Nitro-o-toluidine 99-55-8 No Code 4-Chloroaniline 106-47-8 50312+ Nitroquinoline-1-oxide 56-57-5 No Code Chlorobenzilate 510-15-6 39460+ N-Nitrosodi-n-butylamine [N-Nitrosodibutylamine] 924-16-3 73609 Chlorfenvinphos 470-90-6 04083+ N-Nitrosodiethylamine 55-18-5 78200+ 4-Chloro-2-methylaniline 95-69-2 No Code N-Nitrosodimethylamine [NDMA] * 62-75-9 34438 3-(Chloromethyl)pyridine hydrochloride 6959-48-4 No Code N-Nitrosodiphenylamine * 86-30-6 34433 4-Chloro-2-nitroaniline 89-63-4 No Code N-Nitrosomethylethylamine 10595-95-6 No Code Chlorpropham 101-21-3 81322+ N-Nitrosomethylphenylamine 614-00-6 No Code Chlorothalonil [Daconil (C8Cl4N2)] 1897-45-6 51140+ N-Nitrosomorpholine [Morpholine, 4-nitroso-] 59-89-2 73617+ 1-Chloronaphthalene 90-13-1 No Code N-Nitrosopiperidine [1-Nitrosopiperidine] 100-75-4 73619+ 3-Chloronitrobenzene 121-73-3 No Code N-Nitrosopyrrolidine 930-55-2 78206+ 4-Chloro-1,2-phenylenediamine 95-83-0 No Code trans-Nonachlor [Chlordane - Nonachlor, Trans] 39765-80-5 39071+ 4-Chloro-1,3-phenylenediamine 5131-60-2 No Code Norflurazon 27314-13-2 51151+ 2-Chlorobiphenyl 2051-60-7 No Code 2,2’,3,3’,4,5’,6,6’-Octachlorobiphenyl 40186-71-8 No Code Chlorpyrifos 2921-88-2 81403+ Octamethyl pyrophosphoramide 152-16-9 No Code Coumaphos 56-72-4 81293+ 4,4’-Oxydianiline 101-80-4 No Code m+p-Cresol 15831-10-4 No Code Parathion [Ethyl parathion] 56-38-2 39540+ o-Cresol [ortho-Cresol] [2-Methylphenol] 95-48-7 78395 PCB-1016 [Arochlor 1016] * 12674-11-2 34671 p-Cresidine 120-71-8 No Code PCB-1221 [Arochlor 1221] * 11104-28-2 39488 Crotoxyphos [Ciodrin] 7700-17-6 82565+ PCB-1232 [Arochlor 1232] * 11141-16-5 39492 2-Cyclohexyl-4,6-dinitro-phenol 131-89-5 No Code PCB-1242 [Arochlor 1242] * 53469-21-9 39496 Cyanazine 21725-46-2 04041+ PCB-1248 [Arochlor 1248] * 12672-29-6 39500 Cycloate 1134-23-2 81892+ PCB-1254 [Arochlor 1254] * 11097-69-1 39504 p-Cymene [4-Isopropyltoluene] 99-87-6 03908 PCB-1260 [Arochlor 1260] * 11096-82-5 39508 Dacthal [DCPA] 1861-32-1 39770+ PCB-1268 [Arochlor 1268] * 11100-14-4 51581+ 4,4’-DDD * 72-54-8 39310 Pebulate 1114-71-2 49563+ 4,4’-DDE * 72-55-9 39320 Pentachlorobenzene 608-93-5 77793+ 4,4’-DDT * 50-29-3 39300 Pentachloronitrobenzene [PCNB] 82-68-8 49206+ Demeton-O 298-03-3 No Code 2,2’,3,4’,6-Pentachlorobiphenyl 68194-05-8 No Code Demeton-S 126-75-0 No Code Pentachloroethane 76-01-7 81501+ Diallate (cis or trans) 2303-16-4 No Code Pentamethylbenzene 700-12-9 No Code 2,4-Diaminotoluene [2,4-Toluenediamine] 95-80-7 78888+ Perylene 198-55-0 77801+ Diazinon 333-41-5 39570 Phenacetin 62-44-2 73183+ Dibenz(a,j)acridine 224-42-0 73542+ cis-Permethrin 61949-76-6 No Code Dibenzofuran 132-64-9 81302+ trans-Permethrin 61949-77-7 No Code Dibenzo(a,e)pyrene 192-65-4 51737+ Phenobarbital 50-06-6 No Code Dibenzothiophene 132-65-0 No Code Phenothiazene 92-84-2 No Code 1,2-Dibromo-3-chloropropane [Dibromochloropropane] 96-12-8 49146 1,4-Phenylenediamine 624-18-0 No Code 3,5-Dibromo-4-hydroxybenzonitrile [Bromoxynil] 1689-84-5 51136+ 1-Phenylnaphthalene 605-02-7 No Code 2,6-Di-tert-butyl-p-benzoquinone 719-22-2 No Code 2-Phenylnaphthalene 612-94-2 No Code DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit NC0090140 Page 12 of 13 EPA Method 625.1: Table 3 – Additional Extractable Analytes Analytes noted as “*” in this table are Priority Pollutants (40 CFR part 423, appendix A). Analyte (alternative nomenclature) CAS Registry No. Parameter Code Analyte CAS Registry No. Parameter Code Dichlone 117-80-6 39150+ Phorate 298-02-2 46313+ 2,3-Dichloroaniline 608-27-5 77533 Phosalone 2310-17-0 81291+ 2,3-Dichlorobiphenyl 16605-91-7 No Code Phosmet [Imidan] 732-11-6 51154+ 2,6-Dichloro-4-nitroaniline [Dichloran] 99-30-9 38446+ Phosphamidon 13171-21-6 78881+ 2,3-Dichloronitrobenzene 3209-22-1 No Code Phthalic anhydride 85-44-9 77453+ 1,3-Dichloro-2-propanol 96-23-1 No Code alpha-Picoline [2-Methylpyridine] 109-06-8 77088+ 2,6-Dichlorophenol [2,4-Dichlorophenol] 120-83-2 34601 Piperonyl sulfoxide 120-62-7 No Code Dichlorvos [2,2-Dichlorovinyldimethyl phosphate] 62-73-7 39109 Prometon 1610-18-0 51155+ Dicrotophos 141-66-2 04310+ Prometryn 7287-19-6 51156+ Dieldrin * 60-57-1 39380 Pronamide 23950-58-5 51157+ 1,2:3,4-Diepoxybutane 1464-53-5 No Code Propachlor 1918-16-7 51158+ Di(2-ethylhexyl) adipate [Bis(2-ethylhexyl) adipate] 103-23-1 51174+ Propazine 139-40-2 51159+ Diethylstilbestrol 56-53-1 82192+ Propylthiouracil 51-52-5 No Code Diethyl sulfate 64-67-5 No Code Pyridine 110-86-1 77045 Dilantin [Phenytoin] [5,5-Diphenylhydantoin] 57-41-0 51744+ Resorcinol [1,3-Benzenediol] 108-46-3 77164+ Dimethoate 60-51-5 46314+ Safrole 94-59-7 77545+ 3,3’-Dimethoxybenzidine 119-90-4 51769+ Simazine 122-34-9 39055+ Dimethylaminoazobenzene [p-Dimethylaminoazobenzene] 60-11-7 73179+ Simetryn 1014-70-6 No Code 7,12-Dimethylbenz(a)anthracene 57-97-6 No Code Squalene 7683-64-9 No Code 3,3’-Dimethylbenzidine 119-93-7 51647+ Stirofos [Tetrachlorvinphos] 22248-79-9 38686 N,N-Dimethylformamide 68-12-2 77110+ Strychnine 57-24-9 No Code 3,6-Dimethylphenathrene 1576-67-6 No Code Styrene 100-42-5 81708 alpha, alpha-Dimethylphenethylamine 122-09-8 No Code Sulfallate 95-06-7 No Code Dimethyl sulfone 67-71-0 No Code Tebuthiuron 34014-18-1 51160+ 1,2-Dinitrobenzene 528-29-0 No Code Terbacil 5902-51-2 30234+ 1,3-Dinitrobenzene 99-65-0 45622+ Terbufos 13071-79-9 51462+ 1,4-Dinitrobenzene 100-25-4 No Code Terbutryn 886-50-0 51162+ Dinocap 39300-45-3 No Code alpha-Terpineol 98-55-5 77493 Dinoseb [Dinitrobutyl phenol] [2-sec-Butyl-4,6-dinitrophenol] 88-85-7 30191+ 1,2,4,5-Tetrachlorobenzene 95-94-3 77734+ Diphenylamine 122-39-4 77579+ 2,2’,4,4’-Tetrachlorobiphenyl 2437-79-8 No Code Diphenyl ether 101-84-8 No Code 2,3,7,8-Tetrachlorodibenzo-p-dioxin [Dioxin] [TCDD] 1746-01-6 34675 1,2-Diphenylhydrazine 122-66-7 34346 2,3,4,6-Tetrachlorophenol 58-90-2 77770 Diphenamid 957-51-7 78004+ Tetrachlorvinphos 22248-79-9 38686+ Diphenyldisulfide 882-33-7 No Code Tetraethyl dithiopyrophosphate [Sulfotepp] 3689-24-5 82201+ Disulfoton 298-04-4 39010 Tetraethyl pyrophosphate [TEPP] 107-49-3 39620+ Disulfoton sulfoxide 2497-07-6 No Code Thianaphthene [2,3-Benzothiophene] 95-15-8 No Code Disulfoton sulfone 2497-06-5 No Code Thioacetamide 62-55-5 No Code Endosulfan I * 959-98-8 34361 Thionazin 297-97-2 51381+ Endosulfan II * 33213-65-9 34356 Thiophenol [Benzenethiol] 108-98-5 No Code Endosulfan sulfate * 1031-07-8 34351 Thioxanthone 492-22-8 No Code Endrin * 72-20-8 39390 Toluene-1,3-diisocyanate 26471-62-5 No Code Endrin aldehyde * 7421-93-4 34366 Toluene-2,4-diisocyanate 584-84-9 78144+ Endrin ketone, in water * 53494-70-5 78008 o-Toluidine 95-53-4 77142 EPN 2104-64-5 81290+ Toxaphene * 8001-35-2 39400 EPTC [Eradicane] [S-Ethyl dipropylthiocarbamate] 759-94-4 81894+ Triadimefon, organic pesticide 43121-43-3 51163+ Ethion 563-12-2 39398+ 1,2,3-Trichlorobenzene 87-61-6 77613+ Ethoprop 13194-48-4 81758+ 2,4,5-Trichlorobiphenyl 15862-07-4 No Code Ethyl carbamate 51-79-6 No Code 2,3,6-Trichlorophenol 933-75-5 No Code Ethyl methanesulfonate 62-50-0 73184+ 2,4,5-Trichlorophenol 95-95-4 77687 Ethylene thiourea 96-45-7 38928+ Tricyclazole 41814-78-2 No Code Etridiazole 2593-15-9 No Code Trifluralin 1582-09-8 39030+ Ethynylestradiol-3-methyl ether 72-33-3 No Code 1,2,3-Trimethoxybenzene 634-36-6 No Code Famphur 52-85-7 38462+ 2,4,5-Trimethylaniline 137-17-7 No Code Fenamiphos 22224-92-6 No Code Trimethyl phosphate 512-56-1 No Code Fenarimol 60168-88-9 51145+ Triphenylene 217-59-4 No Code Fensulfothion 115-90-2 30004 Tripropyleneglycolmethyl ether 20324-33-8 No Code Fenthion 55-38-9 30006+ 1,3,5-Trinitrobenzene 99-35-4 73653+ DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit NC0090140 Page 13 of 13 EPA Method 625.1: Table 3 – Additional Extractable Analytes Analytes noted as “*” in this table are Priority Pollutants (40 CFR part 423, appendix A). Analyte (alternative nomenclature) CAS Registry No. Parameter Code Analyte CAS Registry No. Parameter Code Fluchloralin 33245-39-5 No Code Tris(2,3-dibromopropyl) phosphate 126-72-7 22410+ Fluridone 59756-60-4 51588+ Tri-p-tolyl phosphate 78-32-0 No Code Heptachlor * 76-44-8 39410 O,O,O-Triethyl phosphorothioate [Phosphorothioic acid, O,O,O-triethyl ester] 126-68-1 73652+ Heptachlor epoxide * 1024-57-3 39420 Trithiane 3325-33-5 No Code 2,2’,3,3’,4,4’,6-Heptachlorobiphenyl 52663-71-5 No Code Vernolate 1929-77-7 82200+ DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 South End Charlotte Owner, LLC Fulbright Labs Brownfields Property 1919, 1923, and 1933 South Blvd, Charlotte Excavation & Permanent-Structure Dewatering North State Grid/Quad: G15 NE / Charlotte East 12-Digit HUC:03050103030102 Receiving Stream:UT to Dairy Branch Stream Class: C Drainage Basin: Catawba River Basin Sub-Basin:03-08-34 Stream Segment: 11-137-8-1 NPDES Permit NC0090140 Mecklenburg County Facility Location not to scale US HWY I-77 Outfall 001 Storm Sewer (Flows SE to Dairy Branch) South Blvd Location -Figure 1 DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 South End Charlotte Owner, LLC Fulbright Labs Brownfields Property 1919, 1923, and 1933 South Blvd, Charlotte North State Grid/Quad: G15 NE / Charlotte East 12-Digit HUC:03050103030102 Receiving Stream:UT to Dairy Branch Stream Class: C Drainage Basin: Catawba River Basin Sub-Basin:03-08-34 Stream Segment: 11-137-8-1 NPDES Permit NC0090140 Mecklenburg County Facility Location not to scale US HWY I-77 Outfall 001 Storm Sewer (Flows SE to Little Sugar Creek) South Blvd Figure 2Site Detail DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 North NPDES Permit NC0090140 Mecklenburg County Facility Location [not to scale] Storm Drain Pathway Outfall 001 (flows North) Stormsewer Drainage Pathway Figure 3 State Grid/Quad: G15 NE / Charlotte East 12-Digit HUC:03050103030102 Receiving Stream:UT to Dairy Branch Stream Class: C Drainage Basin: Catawba River Basin Sub-Basin:03-08-34 Stream Segment: 11-137-8-1 South End Charlotte Owner, LLC Fulbright Labs Brownfields Property 1919, 1923, and 1933 South Blvd, Charlotte DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit Standard Conditions Page 1 of 18 Version 11/09/2011 PART II STANDARD CONDITIONS FOR NPDES PERMITS Section A. Definitions 2/Month Samples are collected twice per month with at least ten calendar days between sampling events. These samples shall be representative of the wastewater discharged during the sample period. 3/Week Samples are collected three times per week on three separate calendar days. These samples shall be representative of the wastewater discharged during the sample period. Act or "the Act" The Federal Water Pollution Control Act, also known as the Clean Water Act (CWA), as amended, 33 USC 1251, et. seq. Annual Average The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar year. In the case of fecal coliform, the geometric mean of such discharges. Arithmetic Mean The summation of the individual values divided by the number of individual values. Bypass The known diversion of waste streams from any portion of a treatment facility including the collection system, which is not a designed or established or operating mode for the facility. Calendar Day The period from midnight of one day until midnight of the next day. However, for purposes of this permit, any consecutive 24-hour period that reasonably represents the calendar day may be used for sampling. Calendar Week The period from Sunday through the following Saturday. Calendar Quarter One of the following distinct periods: January through March, April through June, July through September, and October through December. Composite Sample A sample collected over a 24-hour period by continuous sampling or combining grab samples of at least 100 mL in such a manner as to result in a total sample representative of the wastewater discharge during the sample period. The Director may designate the most appropriate method (specific number and size of aliquots necessary, the time interval between grab samples, etc.) on a case-by-case basis. Samples may be collected manually or automatically. Composite samples may be obtained by the following methods: (1) Continuous: a single, continuous sample collected over a 24-hour period proportional to the rate of flow. (2) Constant time/variable volume: a series of grab samples collected at equal time intervals over a 24 hour period of discharge and combined proportional to the rate of flow measured at the time of individual sample collection, or (3) Variable time/constant volume: a series of grab samples of equal volume collected over a 24 hour period with the time intervals between samples determined by a preset number of gallons passing the sampling point. Flow measurement between sample intervals shall be determined by use of a flow recorder and totalizer, and the preset gallon interval between sample collection fixed at no greater than 1/24 of the expected total daily flow at the treatment system, or DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit Standard Conditions Page 2 of 18 Version 11/09/2011 (4) Constant time/constant volume: a series of grab samples of equal volume collected over a 24-hour period at a constant time interval. Use of this method requires prior approval by the Director. This method may only be used in situations where effluent flow rates vary less than 15 percent. The following restrictions also apply: Influent and effluent grab samples shall be of equal size and of no less than 100 milliliters Influent samples shall not be collected more than once per hour. Permittees with wastewater treatment systems whose detention time < 24 hours shall collect effluent grab samples at intervals of no greater than 20 minutes apart during any 24-hour period. Permittees with wastewater treatment systems whose detention time exceeds 24 hours shall collect effluent grab samples at least every six hours; there must be a minimum of four samples during a 24-hour sampling period. Continuous flow measurement Flow monitoring that occurs without interruption throughout the operating hours of the facility. Flow shall be monitored continually except for the infrequent times when there may be no flow or for infrequent maintenance activities on the flow device. Daily Discharge The discharge of a pollutant measured during a calendar day or any 24-hour period that reasonably represents the calendar day for purposes of sampling. For pollutants measured in units of mass, the "daily discharge" is calculated as the total mass of the pollutant discharged over the day. For pollutants expressed in other units of measurement, the “daily discharge” is calculated as the average measurement of the pollutant over the day. (40 CFR 122.2; see also “Composite Sample,” above.) Daily Maximum The highest “daily discharge” during the calendar month. Daily Sampling Parameters requiring daily sampling shall be sampled 5 out of every 7 days per week unless otherwise specified in the permit. Sampling shall be conducted on weekdays except where holidays or other disruptions of normal operations prevent weekday sampling. If sampling is required for all seven days of the week for any permit parameter(s), that requirement will be so noted on the Effluent Limitations and Monitoring Page(s). DWQ or “the Division” The Division of Water Quality, Department of Environment and Natural Resources. Effluent Wastewater discharged following all treatment processes from a water pollution control facility or other point source whether treated or untreated. EMC The North Carolina Environmental Management Commission EPA The United States Environmental Protection Agency Facility Closure Cessation of all activities that require coverage under this NPDES permit. Completion of facility closure will allow this permit to be rescinded. Geometric Mean The Nth root of the product of the individual values where N = the number of individual values. For purposes of calculating the geometric mean, values of “0” (or “< [detection level]”) shall be considered = 1. Grab Sample Individual samples of at least 100 mL collected over a period of time not exceeding 15 minutes. Grab samples can be collected manually. Grab samples must be representative of the discharge (or the receiving stream, for instream samples). DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit Standard Conditions Page 3 of 18 Version 11/09/2011 Hazardous Substance Any substance designated under 40 CFR Part 116 pursuant to Section 311 of the CWA. Instantaneous flow measurement The flow measured during the minimum time required for the flow measuring device or method to produce a result in that instance. To the extent practical, instantaneous flow measurements coincide with the collection of any grab samples required for the same sampling period so that together the samples and flow are representative of the discharge during that sampling period. Monthly Average (concentration limit) The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar month. In the case of fecal coliform or other bacterial parameters or indicators, the geometric mean of such discharges. Permit Issuing Authority The Director of the Division of Water Quality. Quarterly Average (concentration limit) The arithmetic mean of all samples taken over a calendar quarter. Severe property damage Substantial physical damage to property, damage to the treatment facilities which causes them to become inoperable, or substantial and permanent loss of natural resources which can reasonably be expected to occur in the absence of a bypass. Severe property damage excludes economic loss caused by delays in production. Toxic Pollutant: Any pollutant listed as toxic under Section 307(a)(1) of the CWA. Upset An incident beyond the reasonable control of the Permittee causing unintentional and temporary noncompliance with permit effluent limitations and/or monitoring requirements. An upset does not include noncompliance caused by operational error, improperly designed treatment facilities, inadequate treatment facilities, lack of preventive maintenance, or careless or improper operation. Weekly Average (concentration limit) The arithmetic mean of all "daily discharges" of a pollutant measured during the calendar week. In the case of fecal coliform or other bacterial parameters or indicators, the geometric mean of such discharges. Section B. General Conditions l. Duty to Comply The Permittee must comply with all conditions of this permit. Any permit noncompliance constitutes a violation of the CWA and is grounds for enforcement action; for permit termination, revocation and reissuance, or modification; or denial of a permit renewal application [40 CFR 122.41]. a. The Permittee shall comply with effluent standards or prohibitions established under section 307(a) of the CWA for toxic pollutants and with standards for sewage sludge use or disposal established under section 405(d) of the CWA within the time provided in the regulations that establish these standards or prohibitions or standards for sewage sludge use or disposal, even if the permit has not yet been modified to incorporate the requirement. b. The CWA provides that any person who violates section[s] 301, 302, 306, 307, 308, 318 or 405 of the Act, or any permit condition or limitation implementing any such sections in a permit issued under section 402, or any requirement imposed in a pretreatment program approved under sections 402(a)(3) or 402(b)(8) of the Act, is subject to a civil penalty not to exceed $37,500 per day for each violation. [33 USC 1319(d) and 40 CFR 122.41(a)(2)] c. The CWA provides that any person who negligently violates sections 301, 302, 306, 307, 308, 318, or 405 of the Act, or any condition or limitation implementing any of such sections in a permit issued under section 402 of the Act, or any requirement imposed in a pretreatment program approved under section 402(a)(3) or 402(b)(8) of the Act, is subject to criminal penalties of $2,500 to $25,000 per day of violation, or DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit Standard Conditions Page 4 of 18 Version 11/09/2011 imprisonment of not more than 1 year, or both. In the case of a second or subsequent conviction for a negligent violation, a person shall be subject to criminal penalties of not more than $50,000 per day of violation, or by imprisonment of not more than 2 years, or both. [33 USC 1319(c)(1) and 40 CFR 122.41(a)(2)] d. Any person who knowingly violates such sections, or such conditions or limitations is subject to criminal penalties of $5,000 to $50,000 per day of violation, or imprisonment for not more than 3 years, or both. In the case of a second or subsequent conviction for a knowing violation, a person shall be subject to criminal penalties of not more than $100,000 per day of violation, or imprisonment of not more than 6 years, or both. [33 USC 1319(c)(2) and 40 CFR 122.41(a)(2)] e. Any person who knowingly violates section 301, 302, 303, 306, 307, 308, 318 or 405 of the Act, or any permit condition or limitation implementing any of such sections in a permit issued under section 402 of the Act, and who knows at that time that he thereby places another person in imminent danger of death or serious bodily injury, shall, upon conviction, be subject to a fine of not more than $250,000 or imprisonment of not more than 15 years, or both. In the case of a second or subsequent conviction for a knowing endangerment violation, a person shall be subject to a fine of not more than $500,000 or by imprisonment of not more than 30 years, or both. An organization, as defined in section 309(c)(3)(B)(iii) of the CWA, shall, upon conviction of violating the imminent danger provision, be subject to a fine of not more than $1,000,000 and can be fined up to $2,000,000 for second or subsequent convictions. [40 CFR 122.41(a)(2)] f. Under state law, a civil penalty of not more than $25,000 per violation may be assessed against any person who violates or fails to act in accordance with the terms, conditions, or requirements of a permit. [North Carolina General Statutes § 143-215.6A] g. Any person may be assessed an administrative penalty by the Administrator for violating section 301, 302, 306, 307, 308, 318 or 405 of this Act, or any permit condition or limitation implementing any of such sections in a permit issued under section 402 of this Act. Administrative penalties for Class I violations are not to exceed $16,000 per violation, with the maximum amount of any Class I penalty assessed not to exceed $37,500. Penalties for Class II violations are not to exceed $16,000 per day for each day during which the violation continues, with the maximum amount of any Class II penalty not to exceed $177,500. [33 USC 1319(g)(2) and 40 CFR 122.41(a)(3)] 2. Duty to Mitigate The Permittee shall take all reasonable steps to minimize or prevent any discharge or sludge use or disposal in violation of this permit with a reasonable likelihood of adversely affecting human health or the environment [40 CFR 122.41(d)]. 3. Civil and Criminal Liability Except as provided in permit conditions on "Bypassing" (Part II.C.4), “Upsets” (Part II.C.5) and "Power Failures" (Part II.C.7), nothing in this permit shall be construed to relieve the Permittee from any responsibilities, liabilities, or penalties for noncompliance pursuant to NCGS 143-215.3, 143-215.6 or Section 309 of the Federal Act, 33 USC 1319. Furthermore, the Permittee is responsible for consequential damages, such as fish kills, even though the responsibility for effective compliance may be temporarily suspended. 4. Oil and Hazardous Substance Liability Nothing in this permit shall be construed to preclude the institution of any legal action or relieve the Permittee from any responsibilities, liabilities, or penalties to which the Permittee is or may be subject to under NCGS 143- 215.75 et seq. or Section 311 of the Federal Act, 33 USG 1321. Furthermore, the Permittee is responsible for consequential damages, such as fish kills, even though the responsibility for effective compliance may be temporarily suspended. 5. Property Rights The issuance of this permit does not convey any property rights in either real or personal property, or any exclusive privileges, nor does it authorize any injury to private property or any invasion of personal rights, nor any infringement of Federal, State or local laws or regulations [40 CFR 122.41(g)]. 6. Onshore or Offshore Construction This permit does not authorize or approve the construction of any onshore or offshore physical structures or facilities or the undertaking of any work in any navigable waters. DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit Standard Conditions Page 5 of 18 Version 11/09/2011 7. Severability The provisions of this permit are severable. If any provision of this permit, or the application of any provision of this permit to any circumstances, is held invalid, the application of such provision to other circumstances, and the remainder of this permit, shall not be affected thereby [NCGS 150B-23]. 8. Duty to Provide Information The Permittee shall furnish to the Permit Issuing Authority, within a reasonable time, any information which the Permit Issuing Authority may request to determine whether cause exists for modifying, revoking and reissuing, or terminating this permit or to determine compliance with this permit. The Permittee shall also furnish to the Permit Issuing Authority upon request, copies of records required by this permit [40 CFR 122.41(h)]. 9. Duty to Reapply If the Permittee wishes to continue an activity regulated by this permit after the expiration date of this permit, the Permittee must apply for and obtain a new permit [40 CFR 122.41(b)]. 10. Expiration of Permit The Permittee is not authorized to discharge after the expiration date. In order to receive automatic authorization to discharge beyond the expiration date, the Permittee shall submit such information, forms, and fees as are required by the agency authorized to issue permits no later than 180 days prior to the expiration date unless permission for a later date has been granted by the Director. (The Director shall not grant permission for applications to be submitted later than the expiration date of the existing permit.) [40 CFR 122.21(d)] Any Permittee that has not requested renewal at least 180 days prior to expiration, or any Permittee that does not have a permit after the expiration and has not requested renewal at least 180 days prior to expiration, will subject the Permittee to enforcement procedures as provided in NCGS 143-215.6 and 33 USC 1251 et. seq. 11. Signatory Requirements All applications, reports, or information submitted to the Permit Issuing Authority shall be signed and certified [40 CFR 122.41(k)]. a. All permit applications shall be signed as follows: (1) For a corporation: by a responsible corporate officer. For the purpose of this Section, a responsible corporate officer means: (a) a president, secretary, treasurer or vice president of the corporation in charge of a principal business function, or any other person who performs similar policy or decision making functions for the corporation, or (b) the manager of one or more manufacturing, production, or operating facilities, provided, the manager is authorized to make management decisions which govern the operation of the regulated facility including having the explicit or implicit duty of making major capital investment recommendations, and initiating and directing other comprehensive measures to assure long term environmental compliance with environmental laws and regulations; the manager can ensure that the necessary systems are established or actions taken to gather complete and accurate information for permit application requirements; and where authority to sign documents has been assigned or delegated to the manager in accordance with corporate procedures . (2) For a partnership or sole proprietorship: by a general partner or the proprietor, respectively; or (3) For a municipality, State, Federal, or other public agency: by either a principal executive officer or ranking elected official [40 CFR 122.22]. b. All reports required by the permit and other information requested by the Permit Issuing Authority shall be signed by a person described in paragraph a. above or by a duly authorized representative of that person. A person is a duly authorized representative only if: (1) The authorization is made in writing by a person described above; (2) The authorization specified either an individual or a position having responsibility for the overall operation of the regulated facility or activity, such as the position of plant manager, operator of a well or well field, superintendent, a position of equivalent responsibility, or an individual or position having overall responsibility for environmental matters for the company. (A duly authorized representative may thus be either a named individual or any individual occupying a named position.); and (3) The written authorization is submitted to the Permit Issuing Authority [40 CFR 122.22] DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit Standard Conditions Page 6 of 18 Version 11/09/2011 c. Changes to authorization: If an authorization under paragraph (b) of this section is no longer accurate because a different individual or position has responsibility for the overall operation of the facility, a new authorization satisfying the requirements of paragraph (b) of this section must be submitted to the Director prior to or together with any reports, information, or applications to be signed by an authorized representative [40 CFR 122.22] d. Certification. Any person signing a document under paragraphs a. or b. of this section shall make the following certification [40 CFR 122.22]. NO OTHER STATEMENTS OF CERTIFICATION WILL BE ACCEPTED: "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 12. Permit Actions This permit may be modified, revoked and reissued, or terminated for cause. The filing of a request by the Permittee for a permit modification, revocation and reissuance, or termination, or a notification of planned changes or anticipated noncompliance does not stay any permit condition [40 CFR 122.41(f)]. 13. Permit Modification, Revocation and Reissuance, or Termination The issuance of this permit does not prohibit the permit issuing authority from reopening and modifying the permit, revoking and reissuing the permit, or terminating the permit as allowed by the laws, rules, and regulations contained in Title 40, Code of Federal Regulations, Parts 122 and 123; Title 15A of the North Carolina Administrative Code, Subchapter 02H .0100; and North Carolina General Statute 143.215.1 et. al. 14. Annual Administering and Compliance Monitoring Fee Requirements The Permittee must pay the annual administering and compliance monitoring fee within thirty days after being billed by the Division. Failure to pay the fee in a timely manner in accordance with 15A NCAC 02H .0105(b)(2) may cause this Division to initiate action to revoke the permit. Section C. Operation and Maintenance of Pollution Controls 1. Certified Operator Owners of classified water pollution control systems must designate operators, certified by the Water Pollution Control System Operators Certification Commission (WPCSOCC), of the appropriate type and grade for the system, and, for each classification must [T15A NCAC 08G .0201]: a. designate one Operator In Responsible Charge (ORC) who possesses a valid certificate of the type and grade at least equivalent to the type and grade of the system; b. designate one or more Back-up Operator(s) in Responsible Charge (Back-up ORCs) who possesses a valid certificate of the type of the system and no more than one grade less than the grade of the system, with the exception of no backup operator in responsible charge is required for systems whose minimum visitation requirements are twice per year; and c. submit a signed completed "Water Pollution Control System Operator Designation Form" to the Commission (or to the local health department for owners of subsurface systems) countersigned by the designated certified operators, designating the Operator in Responsible Charge (ORC) and the Back-up Operator in Responsible Charge (Back-up ORC): (1) 60 calendar days prior to wastewater or residuals being introduced into a new system; or (2) within 120 calendar days following: receiving notification of a change in the classification of the system requiring the designation of a new Operator in Responsible Charge (ORC) and Back-up Operator in Responsible Charge (Back-up ORC) of the proper type and grade; or a vacancy in the position of Operator in Responsible Charge (ORC) or Back-up Operator in Responsible Charge (Back-up ORC). DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit Standard Conditions Page 7 of 18 Version 11/09/2011 (3) within seven calendar days of vacancies in both ORC and Back-up ORC positions replacing or designating at least one of the responsibilities. The ORC of each Class I facility (or the Back-up ORC, when acting as surrogate for the ORC) must: Visit the facility as often as is necessary to insure proper operation of the treatment system; the treatment facility must be visited at least weekly Comply with all other conditions of 15A NCAC 08G .0204. The ORC of each Class II, III and IV facility (or the Back-up ORC, when acting as surrogate for the ORC) must: Visit the facility as often as is necessary to insure proper operation of the treatment system; the treatment facility must be visited at least five days per week, excluding holidays Properly manage and document daily operation and maintenance of the facility Comply with all other conditions of 15A NCAC 08G .0204. 2. Proper Operation and Maintenance The Permittee shall at all times properly operate and maintain all facilities and systems of treatment and control (and related appurtenances) which are installed or used by the Permittee to achieve compliance with the conditions of this permit. Proper operation and maintenance also includes adequate laboratory controls and appropriate quality assurance procedures. This provision requires the Permittee to install and operate backup or auxiliary facilities only when necessary to achieve compliance with the conditions of the permit [40 CFR 122.41(e)]. NOTE: Properly and officially designated operators are fully responsible for all proper operation and maintenance of the facility, and all documentation required thereof, whether acting as a contract operator [subcontractor] or a member of the Permittee’s staff. 3. Need to Halt or Reduce not a Defense It shall not be a defense for a Permittee in an enforcement action that it would have been necessary to halt or reduce the permitted activity in order to maintain compliance with the condition of this permit [40 CFR 122.41(c)]. 4. Bypassing of Treatment Facilities a. Bypass not exceeding limitations [40 CFR 122.41(m)(2)] The Permittee may allow any bypass to occur which does not cause effluent limitations to be exceeded, but only if it also is for essential maintenance to assure efficient operation. These bypasses are not subject to the provisions of Paragraphs b. and c. of this section. b. Notice [40 CFR 122.41(m)(3)] (1) Anticipated bypass. If the Permittee knows in advance of the need for a bypass, it shall submit prior notice, if possible at least ten days before the date of the bypass; including an evaluation of the anticipated quality and effect of the bypass. (2) Unanticipated bypass. The Permittee shall submit notice of an unanticipated bypass as required in Part II.E.6. (24-hour notice). c. Prohibition of Bypass (1) Bypass from the treatment facility is prohibited and the Permit Issuing Authority may take enforcement action against a Permittee for bypass, unless: (A) Bypass was unavoidable to prevent loss of life, personal injury or severe property damage; (B) There were no feasible alternatives to the bypass, such as the use of auxiliary treatment facilities, retention of untreated wastes or maintenance during normal periods of equipment downtime. This condition is not satisfied if adequate backup equipment should have been installed in the exercise of reasonable engineering judgment to prevent a bypass which occurred during normal periods of equipment downtime or preventive maintenance; and (C) The Permittee submitted notices as required under Paragraph b. of this section. (2) Bypass from the collection system is prohibited and the Permit Issuing Authority may take enforcement action against a Permittee for a bypass as provided in any current or future system-wide collection system permit associated with the treatment facility. DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit Standard Conditions Page 8 of 18 Version 11/09/2011 (3) The Permit Issuing Authority may approve an anticipated bypass, after considering its adverse effects, if the Permit Issuing Authority determines that it will meet the three conditions listed above in Paragraph c. (1) of this section. 5. Upsets a. Effect of an upset [40 CFR 122.41(n)(2)]: An upset constitutes an affirmative defense to an action brought for noncompliance with such technology based permit effluent limitations if the requirements of paragraph b. of this condition are met. No determination made during administrative review of claims that noncompliance was caused by upset, and before an action for noncompliance, is final administrative action subject to judicial review. b. Conditions necessary for a demonstration of upset: Any Permittee who wishes to establish the affirmative defense of upset shall demonstrate, through properly signed, contemporaneous operating logs, or other relevant evidence that: (1) An upset occurred and that the Permittee can identify the cause(s) of the upset; (2) The Permittee facility was at the time being properly operated; and (3) The Permittee submitted notice of the upset as required in Part II.E.6.(b) of this permit. (4) The Permittee complied with any remedial measures required under Part II.B.2. of this permit. c. Burden of proof [40 CFR 122.41(n)(4)]: The Permittee seeking to establish the occurrence of an upset has the burden of proof in any enforcement proceeding. 6. Removed Substances Solids, sludges, filter backwash, or other pollutants removed in the course of treatment or control of wastewaters shall be utilized/disposed of in accordance with NCGS 143-215.1 and in a manner such as to prevent any pollutant from such materials from entering waters of the State or navigable waters of the United States except as permitted by the Commission. The Permittee shall comply with all applicable state and Federal regulations governing the disposal of sewage sludge, including 40 CFR 503, Standards for the Use and Disposal of Sewage Sludge; 40 CFR Part 258, Criteria For Municipal Solid Waste Landfills; and 15A NCAC Subchapter 2T, Waste Not Discharged To Surface Waters. The Permittee shall notify the Permit Issuing Authority of any significant change in its sludge use or disposal practices. 7. Power Failures The Permittee is responsible for maintaining adequate safeguards (as required by 15A NCAC 02H .0124) to prevent the discharge of untreated or inadequately treated wastes during electrical power failures either by means of alternate power sources, standby generators or retention of inadequately treated effluent. Section D. Monitoring and Records l. Representative Sampling Samples collected and measurements taken, as required herein, shall be representative of the permitted discharge. Samples collected at a frequency less than daily shall be taken on a day and time that is representative of the discharge for the period the sample represents. All samples shall be taken at the monitoring points specified in this permit and, unless otherwise specified, before the effluent joins or is diluted by any other wastestream, body of water, or substance. Monitoring points shall not be changed without notification to and the approval of the Permit Issuing Authority [40 CFR 122.41(j)]. 2. Reporting Monitoring results obtained during the previous month(s) shall be summarized for each month and reported on a monthly Discharge Monitoring Report (DMR) Form (MR 1, 1.1, 2, 3) or alternative forms approved by the Director, postmarked no later than the last calendar day of the month following the completed reporting period. The first DMR is due on the last day of the month following the issuance of the permit or in the case of a new facility, on the last day of the month following the commencement of discharge. Duplicate signed copies of these, and all other reports required herein, shall be submitted to the following address: DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit Standard Conditions Page 9 of 18 Version 11/09/2011 NC DENR / Division of Water Quality / Surface Water Protection Section ATTENTION: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 3. Flow Measurements Appropriate flow measurement devices and methods consistent with accepted scientific practices shall be selected and used to ensure the accuracy and reliability of measurements of the volume of monitored discharges. The devices shall be installed, calibrated and maintained to ensure that the accuracy of the measurements is consistent with the accepted capability of that type of device. Devices selected shall be capable of measuring flows with a maximum deviation of less than 10% from the true discharge rates throughout the range of expected discharge volumes. Flow measurement devices shall be accurately calibrated at a minimum of once per year and maintained to ensure that the accuracy of the measurements is consistent with the accepted capability of that type of device. The Director shall approve the flow measurement device and monitoring location prior to installation. Once-through condenser cooling water flow monitored by pump logs, or pump hour meters as specified in Part I of this permit and based on the manufacturer's pump curves shall not be subject to this requirement. 4. Test Procedures Laboratories used for sample analysis must be certified by the Division. Permittees should contact the Division’s Laboratory Certification Section (919 733-3908 or http://portal.ncdenr.org/web/wq/lab/cert) for information regarding laboratory certifications. Facilities whose personnel are conducting testing of field-certified parameters only must hold the appropriate field parameter laboratory certifications. Test procedures for the analysis of pollutants shall conform to the EMC regulations (published pursuant to NCGS 143-215.63 et. seq.), the Water and Air Quality Reporting Acts, and to regulations published pursuant to Section 304(g), 33 USC 1314, of the CWA (as amended), and 40 CFR 136; or in the case of sludge use or disposal, approved under 40 CFR 136, unless otherwise specified in 40 CFR 503, unless other test procedures have been specified in this permit [40 CFR 122.41]. To meet the intent of the monitoring required by this permit, all test procedures must produce minimum detection and reporting levels that are below the permit discharge requirements and all data generated must be reported down to the minimum detection or lower reporting level of the procedure. If no approved methods are determined capable of achieving minimum detection and reporting levels below permit discharge requirements, then the most sensitive (method with the lowest possible detection and reporting level) approved method must be used. 5. Penalties for Tampering The CWA provides that any person who falsifies, tampers with, or knowingly renders inaccurate, any monitoring device or method required to be maintained under this permit shall, upon conviction, be punished by a fine of not more than $10,000 per violation, or by imprisonment for not more than two years per violation, or by both. If a conviction of a person is for a violation committed after a first conviction of such person under this paragraph, punishment is a fine of not more than $20,000 per day of violation, or by imprisonment of not more than 4 years, or both [40 CFR 122.41]. 6. Records Retention Except for records of monitoring information required by this permit related to the Permittee’s sewage sludge use and disposal activities, which shall be retained for a period of at least five years (or longer as required by 40 CFR 503), the Permittee shall retain records of all monitoring information, including: all calibration and maintenance records all original strip chart recordings for continuous monitoring instrumentation copies of all reports required by this permit copies of all data used to complete the application for this permit These records or copies shall be maintained for a period of at least 3 years from the date of the sample, measurement, report or application. This period may be extended by request of the Director at any time [40 CFR 122.41]. DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit Standard Conditions Page 10 of 18 Version 11/09/2011 7. Recording Results For each measurement or sample taken pursuant to the requirements of this permit, the Permittee shall record the following information [40 CFR 122.41]: a. The date, exact place, and time of sampling or measurements; b. The individual(s) who performed the sampling or measurements; c. The date(s) analyses were performed; d. The individual(s) who performed the analyses; e. The analytical techniques or methods used; and f. The results of such analyses. 8. Inspection and Entry The Permittee shall allow the Director, or an authorized representative (including an authorized contractor acting as a representative of the Director), upon the presentation of credentials and other documents as may be required by law, to; a. Enter, at reasonable times, upon the Permittee's premises where a regulated facility or activity is located or conducted, or where records must be kept under the conditions of this permit; b. Have access to and copy, at reasonable times, any records that must be kept under the conditions of this permit; c. Inspect at reasonable times any facilities, equipment (including monitoring and control equipment), practices, or operations regulated or required under this permit; and d. Sample or monitor at reasonable times, for the purposes of assuring permit compliance or as otherwise authorized by the CWA, any substances or parameters at any location [40 CFR 122.41(i)]. Section E Reporting Requirements l. Change in Discharge All discharges authorized herein shall be consistent with the terms and conditions of this permit. The discharge of any pollutant identified in this permit more frequently than or at a level in excess of that authorized shall constitute a violation of the permit. 2. Planned Changes The Permittee shall give notice to the Director as soon as possible of any planned physical alterations or additions to the permitted facility [40 CFR 122.41(l)]. Notice is required only when: a. The alteration or addition to a permitted facility may meet one of the criteria for new sources at 40 CFR 122.29(b); or b. The alteration or addition could significantly change the nature or increase the quantity of pollutants discharged. This notification applies to pollutants subject neither to effluent limitations in the permit, nor to notification requirements under 40 CFR 122.42(a)(1); or c. The alteration or addition results in a significant change in the Permittee’s sludge use or disposal practices, and such alteration, addition or change may justify the application of permit conditions that are different from or absent in the existing permit, including notification of additional use or disposal sites not reported during the permit application process or not reported pursuant to an approved land application plan. 3. Anticipated Noncompliance The Permittee shall give advance notice to the Director of any planned changes to the permitted facility or other activities that might result in noncompliance with the permit [40 CFR 122.41(l)(2)]. 4. Transfers This permit is not transferable to any person without prior written notice to and approval from the Director in accordance with 40 CFR 122.61. The Director may condition approval in accordance with NCGS 143-215.1, in particular NCGS 143-215.1(b)(4)b.2., and may require modification or revocation and reissuance of the permit, or a minor modification, to identify the new permittee and incorporate such other requirements as may be necessary under the CWA [40 CFR 122.41(l)(3), 122.61] or state statute. DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit Standard Conditions Page 11 of 18 Version 11/09/2011 5. Monitoring Reports Monitoring results shall be reported at the intervals specified elsewhere in this permit [40 CFR 122.41(l)(4)]. a. Monitoring results must be reported on a Discharge Monitoring Report (DMR) (See Part II.D.2) or forms provided by the Director for reporting results of monitoring of sludge use or disposal practices. b. If the Permittee monitors any pollutant more frequently than required by this permit using test procedures approved under 40 CFR Part 136 and at a sampling location specified in this permit or other appropriate instrument governing the discharge, the results of such monitoring shall be included in the calculation and reporting of the data submitted on the DMR. 6. Twenty-four Hour Reporting a. The Permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the Permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the Permittee becomes aware of the circumstances. The written submission shall contain a description of the noncompliance, and its cause; the period of noncompliance, including exact dates and times, and if the noncompliance has not been corrected, the anticipated time it is expected to continue; and steps taken or planned to reduce, eliminate, and prevent reoccurrence of the noncompliance [40 CFR 122.41(l)(6)]. b. The Director may waive the written report on a case-by-case basis for reports under this section if the oral report has been received within 24 hours. c. Occurrences outside normal business hours may also be reported to the Division’s Emergency Response personnel at (800) 662-7956, (800) 858-0368 or (919) 733-3300. 7. Other Noncompliance The Permittee shall report all instances of noncompliance not reported under Part II.E.5 and 6. of this permit at the time monitoring reports are submitted. The reports shall contain the information listed in Part II.E.6. of this permit [40 CFR 122.41(l)(7)]. 8. Other Information Where the Permittee becomes aware that it failed to submit any relevant facts in a permit application, or submitted incorrect information in a permit application or in any report to the Director, it shall promptly submit such facts or information [40 CFR 122.41(l)(8)]. 9. Noncompliance Notification The Permittee shall report by telephone to either the central office or the appropriate regional office of the Division as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Any occurrence at the water pollution control facility which results in the discharge of significant amounts of wastes which are abnormal in quantity or characteristic, such as the dumping of the contents of a sludge digester; the known passage of a slug of hazardous substance through the facility; or any other unusual circumstances. b. Any process unit failure, due to known or unknown reasons, that render the facility incapable of adequate wastewater treatment such as mechanical or electrical failures of pumps, aerators, compressors, etc. c. Any failure of a pumping station, sewer line, or treatment facility resulting in a by-pass without treatment of all or any portion of the influent to such station or facility. Persons reporting such occurrences by telephone shall also file a written report within 5 days following first knowledge of the occurrence. Also see reporting requirements for municipalities in Part IV.C.2.c. of this permit. 10. Availability of Reports Except for data determined to be confidential under NCGS 143-215.3 (a)(2) or Section 308 of the Federal Act, 33 USC 1318, all reports prepared in accordance with the terms shall be available for public inspection at the offices of the Division. As required by the Act, effluent data shall not be considered confidential. Knowingly making any false statement on any such report may result in the imposition of criminal penalties as provided for in NCGS 143- 215.1(b)(2) or in Section 309 of the Federal Act. DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit Standard Conditions Page 12 of 18 Version 11/09/2011 11. Penalties for Falsification of Reports The CWA provides that any person who knowingly makes any false statement, representation, or certification in any record or other document submitted or required to be maintained under this permit, including monitoring reports or reports of compliance or noncompliance shall, upon conviction, be punished by a fine of not more than $25,000 per violation, or by imprisonment for not more than two years per violation, or by both [40 CFR 122.41]. 12. Annual Performance Reports Permittees who own or operate facilities that collect or treat municipal or domestic waste shall provide an annual report to the Permit Issuing Authority and to the users/customers served by the Permittee (NCGS 143-215.1C). The report shall summarize the performance of the collection or treatment system, as well as the extent to which the facility was compliant with applicable Federal or State laws, regulations and rules pertaining to water quality. The report shall be provided no later than sixty days after the end of the calendar or fiscal year, depending upon which annual period is used for evaluation. The report shall be sent to: NC DENR / Division of Water Quality / Surface Water Protection Section ATTENTION: Central Files 1617 Mail Service Center Raleigh, North Carolina 27699-1617 DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit Standard Conditions Page 13 of 18 Version 11/09/2011 PART III OTHER REQUIREMENTS Section A. Construction a. The Permittee shall not commence construction of wastewater treatment facilities, nor add to the plant's treatment capacity, nor change the treatment process(es) utilized at the treatment plant unless (1) the Division has issued an Authorization to Construct (AtC) permit or (2) the Permittee is exempted from such AtC permit requirements under Item b. of this Section. b. In accordance with NCGS 143-215.1(a5) [SL 2011-394], no permit shall be required to enter into a contract for the construction, installation, or alteration of any treatment work or disposal system or to construct, install, or alter any treatment works or disposal system within the State when the system’s or work’s principle function is to conduct, treat, equalize, neutralize, stabilize, recycle, or dispose of industrial waste or sewage from an industrial facility and the discharge of the industrial waste or sewage is authorized under a permit issued for the discharge of the industrial waste or sewage into the waters of the State. Notwithstanding the above, the permit issued for the discharge may be modified if required by federal regulation. c. Issuance of an AtC will not occur until Final Plans and Specifications for the proposed construction have been submitted by the Permittee and approved by the Division. Section B. Groundwater Monitoring The Permittee shall, upon written notice from the Director, conduct groundwater monitoring as may be required to determine the compliance of this NPDES permitted facility with the current groundwater standards. Section C. Changes in Discharges of Toxic Substances The Permittee shall notify the Permit Issuing Authority as soon as it knows or has reason to believe (40 CFR 122.42): a. That any activity has occurred or will occur which would result in the discharge, on a routine or frequent basis, of any toxic pollutant which is not limited in the permit, if that discharge will exceed the highest of the following "notification levels"; (1) One hundred micrograms per liter (100 g/L); (2) Two hundred micrograms per liter (200 g/L) for acrolein and acrylonitrile; five hundred micrograms per liter (500 g/L) for 2,4-dinitrophenol and for 2-methyl-4 ,6-dinitrophenol; and one milligram per liter (1 mg/L) for antimony; (3) Five times the maximum concentration value reported for that pollutant in the permit application. b. That any activity has occurred or will occur which would result in any discharge, on a non-routine or infrequent basis, of a toxic pollutant which is not limited in the permit, if that discharge will exceed the highest of the following "notification levels"; (1) Five hundred micrograms per liter (500 g/L); (2) One milligram per liter (1 mg/L) for antimony; (3) Ten times the maximum concentration value reported for that pollutant in the permit application. Section D. Facility Closure Requirements The Permittee must notify the Division at least 90 days prior to the closure of any wastewater treatment system covered by this permit. The Division may require specific measures during deactivation of the system to prevent adverse impacts to waters of the State. This permit cannot be rescinded while any activities requiring this permit continue at the permitted facility. DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit Standard Conditions Page 14 of 18 Version 11/09/2011 PART IV SPECIAL CONDITIONS FOR MUNICIPAL FACILITIES Section A. Definitions In addition to the definitions in Part II of this permit, the following definitions apply to municipal facilities: Indirect Discharge or Industrial User Any non-domestic source that discharges wastewater containing pollutants into a POTW regulated under section 307(b), (c) or (d) of the CWA. [40 CFR 403.3 (i) and (j) and 15A NCAC 02H .0903(b)(11)] Interference Inhibition or disruption of the POTW treatment processes; operations; or its sludge process, use, or disposal which causes or contributes to a violation of any requirement of the Permittee's (or any satellite POTW's if different from the Permittee) NPDES, collection system, or non-discharge permit or prevents sewage sludge use or disposal in compliance with specified applicable State and Federal statutes, regulations, or permits. [15A NCAC 02H .0903(b)(14)] Pass Through A discharge which exits the POTW into waters of the State in quantities or concentrations which, alone or with discharges from other sources, causes a violation, including an increase in the magnitude or duration of a violation, of the Permittee's (or any satellite POTW's, if different from the Permittee) NPDES, collection system, or non-discharge permit. [15A NCAC 02H .0903(b)(23)] Publicly Owned Treatment Works (POTW) A treatment works as defined by Section 212 of the CWA, which is owned by a State or local government organization. This definition includes any devices and systems used in the storage, treatment, recycling and reclamation of municipal sewage or industrial wastes of a liquid nature. It also includes the collection system, as defined in 15A NCAC 2T .0402, only if it conveys wastewater to a POTW treatment plant. The term also means the local government organization, or municipality, as defined in section 502(4) of the CWA, which has jurisdiction over indirect discharges to and the discharges from such a treatment works. In this context, the organization may be the owner of the POTW treatment plant or the owner of the collection system into which an indirect discharger discharges. This second type of POTW may be referred to as a "satellite POTW organization." [15A NCAC 02H .0903(b)(26)] "Significant Industrial User" or "SIU" An Industrial User that discharges wastewater into a publicly owned treatment works and that [15A NCAC 02H .0903(b)(33)]: 1. Discharges an average of 25,000 gallons per day or more of process wastewater to the POTW (excluding sanitary, noncontact cooling and boiler blowdown wastewaters); or 2. Contributes process wastewater which makes up five percent or more of the NPDES or non-discharge permitted flow limit or organic capacity of the POTW treatment plant. In this context, organic capacity refers to BOD, TSS and ammonia; or 3. Is subject to categorical standards under 40 CFR Part 403.6 and 40 CFR Parts 405-471; or 4. Is designated as such by the Permittee on the basis that the Industrial User has a reasonable potential for adversely affecting the POTW's operation or for violating any pretreatment standard or requirement, or the POTW's effluent limitations and conditions in its NPDES or non-discharge permit, or to limit the POTW's sludge disposal options; 5. Subject to approval under 15A NCAC 02H .0907(b), the Permittee may determine that an Industrial User meeting the criteria in paragraphs 1 or 2 of this definition above has no reasonable potential for adversely affecting the POTW's operation or for violating any pretreatment standard or requirement, the POTW's effluent limitations and conditions in its NPDES or non-discharge permit, or to limit the POTW's sludge disposal options, and thus is not a Significant Industrial User (SIU); or 6. Subject to approval under 15A NCAC 02H .0907(b), the Permittee may determine that an Industrial User meeting the criteria in paragraph 3 of this definition above meets the requirements of 40 CFR Part 403.3(v)(2) and thus is a non-significant categorical Industrial User. Section B. Publicly Owned Treatment Works (POTWs) DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit Standard Conditions Page 15 of 18 Version 11/09/2011 All POTWs must provide adequate notice to the Director of the following [40 CFR 122.42(b)]: 1. Any new introduction of pollutants into the POTW from an indirect discharger, regardless of the means of transport, which would be subject to section 301 or 306 of CWA if it were directly discharging those pollutants; and 2. Any substantial change in the volume or character of pollutants being introduced by an indirect discharger as influent to that POTW at the time of issuance of the permit. 3. For purposes of this paragraph, adequate notice shall include information on (1) the quality and quantity of effluent introduced into the POTW, and (2) any anticipated impact that may result from the change of the quantity or quality of effluent to be discharged from the POTW. Section C. Municipal Control of Pollutants from Industrial Users. 1. Effluent limitations are listed in Part I of this permit. Other pollutants attributable to inputs from Industrial Users discharging to the POTW may be present in the Permittee's discharge. At such time as sufficient information becomes available to establish limitations for such pollutants, this permit may be revised to specify effluent limitations for any or all of such other pollutants in accordance with best practicable technology or water quality standards. 2. Prohibited Discharges a. The Permittee shall develop and enforce their Pretreatment Program to implement the prohibition against the introduction of pollutants or discharges into the waste treatment system or waste collection system which cause or contribute to Pass Through or Interference as defined in 15A NCAC 02H .0900 and 40 CFR 403. [40 CFR 403.5(a)(1)] b. The Permittee shall develop and enforce their Pretreatment Program to implement the prohibitions against the introduction of the following wastes in the waste treatment or waste collection system [40 CFR 403.5(b)]: (1) Pollutants which create a fire or explosion hazard in the POTW, including, but not limited to, wastestreams with a closed cup flashpoint of less than 140 degrees Fahrenheit or 60 degrees Centigrade using the test methods specified in 40 CFR 261.21; (2) Pollutants which cause corrosive structural damage to the POTW, but in no case discharges with pH lower than 5.0, unless the works is specifically designed to accommodate such discharges; (3) Solid or viscous pollutants in amounts which cause obstruction to the flow in the POTW resulting in Interference; (4) Any pollutant, including oxygen demanding pollutants (BOD, etc.) released in a Discharge at a flow rate and/or pollutant concentration which will cause Interference with the POTW; (5) Heat in amounts which will inhibit biological activity in the POTW resulting in Interference, but in no case heat in such quantities that the temperature at the POTW Treatment Plant exceeds 40°C (104°F) unless the Division, upon request of the POTW, approves alternate temperature limits; (6) Petroleum oil, non-biodegradable cutting oil, or products of mineral oil origin in amounts that will cause Interference or Pass Through; (7) Pollutants which result in the presence of toxic gases, vapors, or fumes within the POTW in a quantity that may cause acute worker health and safety problems; or (8) Any trucked or hauled pollutants, except at discharge points designated by the POTW. c. The Permittee shall investigate the source of all discharges into the POTW, including slug loads and other unusual discharges, which have the potential to adversely impact the Permittee's Pretreatment Program and/or the operation of the POTW. The Permittee shall report such discharges into the POTW to the Director or the appropriate Regional Office. Any information shall be provided orally within 24 hours from the time the Permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the Permittee becomes aware of the circumstances. The written submission shall contain a description of the discharge; the investigation into possible sources; the period of the discharge, including exact dates and times; if the discharge has not ceased, the anticipated time it is expected to continue; and steps taken or planned to reduce, eliminate, and prevent reoccurrence of the noncompliance, DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit Standard Conditions Page 16 of 18 Version 11/09/2011 3. With regard to the effluent requirements listed in Part I of this permit, it may be necessary for the Permittee to supplement the requirements of the Federal Pretreatment Standards (40 CFR, Part 403) to ensure compliance by the Permittee with all applicable effluent limitations. Such actions by the Permittee may be necessary regarding some or all of the industries discharging to the municipal system. 4. The Permittee shall require any Industrial User (IU) discharging to the POTW to meet Federal Pretreatment Standards developed under Section 307(b) of the Act as amended (which includes categorical standards and specific local limits, best management practices and narrative requirements). Prior to accepting wastewater from any Significant Industrial User (SIU), the Permittee shall either develop and submit to the Division a new Pretreatment Program or, as necessary, a modification of an existing Pretreatment Program, for approval as required under section D below as well as 15A NCAC 02H .0907(a) and (b). [40 CFR 122.44(j)(2)] 5. This permit shall be modified, or alternatively, revoked and reissued, to incorporate or modify an approved POTW Pretreatment Program or to include a compliance schedule for the development of a POTW Pretreatment Program as required under Section 402 (b)(8) of the CWA and implementing regulations or by the requirements of the approved State pretreatment program, as appropriate. Section D. Pretreatment Programs Under authority of sections 307 (b) and (c) and 402(b)(8) of the CWA and implementing regulations 40 CFR 403, North Carolina General Statute 143-215.3(14) and implementing regulations 15A NCAC 02H .0900, and in accordance with the approved pretreatment program, all provisions and regulations contained and referenced in the pretreatment program submittal are an enforceable part of this permit. [40 CFR 122.44(j)(2)] The Permittee shall operate its approved pretreatment program in accordance with Section 402(b)(8) of the CWA, 40 CFR 403, 15A NCAC 02H .0900, and the legal authorities, policies, procedures, and financial provisions contained in its pretreatment program submission and Division approved modifications thereof. Such operation shall include but is not limited to the implementation of the following conditions and requirements. Terms not defined in Part II or Part IV of this permit are as defined in 15A NCAC 02H .0903 and 40 CFR 403.3. 1. Sewer Use Ordinance (SUO) The Permittee shall maintain adequate legal authority to implement its approved pretreatment program. [15A NCAC 02H .0903(b)(32), .0905 and .0906(b)(1); 40 CFR 403.8(f)(1) and 403.9(b)(1) and (2)] 2. Industrial Waste Survey (IWS) The Permittee shall implement an IWS consisting of the survey of users of the POTW collection system or treatment plant, as required by 40 CFR 403.8(f)(2)(i-iii) and 15A NCAC 02H .0905 [also 40 CFR 122.44(j)(1)], including identification of all Industrial Users that may have an impact on the POTW and the character and amount of pollutants contributed to the POTW by these Industrial Users and identification of those Industrial Users meeting the definition of SIU. Where the Permittee accepts wastewater from one or more satellite POTWs, the IWS for the Permittee shall address all satellite POTW services areas, unless the pretreatment program in those satellite service areas is administered by a separate Permittee with an approved Pretreatment Program. The Permittee shall submit a summary of its IWS activities to the Division at least once every five years, and as required by the Division. The IWS submission shall include a summary of any investigations conducted under paragraph C.2.c. of this Part. [15A NCAC 02H .0903(b)(13), .0905 and .0906(b)(2); 40 CFR 403.8(f)(2) and 403.9] 3. Monitoring Plan The Permittee shall implement a Division-approved Monitoring Plan for the collection of facility specific data to be used in a wastewater treatment plant Headworks Analysis (HWA) for the development of specific pretreatment local limits. Effluent data from the Plan shall be reported on the DMRs (as required by Parts II.D and II.E.5.). [15A NCAC 02H .0903(b)(16), .0906(b)(3) and .0905] 4. Headworks Analysis (HWA) and Local Limits The Permittee shall obtain Division approval of a HWA at least once every five years, and as required by the Division. Within 180 days of the effective date of this permit (or any subsequent permit modification) the Permittee shall submit to the Division a written technical evaluation of the need to revise local limits (i.e., an updated HWA or documentation of why one is not needed) [40 CFR 122.44]. The Permittee shall develop, in accordance with 40 CFR 403.5(c) and 15A NCAC 02H .0909, specific Local Limits to implement the prohibitions listed in 40 CFR 403.5(a) and (b) and 15A NCAC 02H .0909. Pursuant to 40 CFR 403.5, local limits are DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit Standard Conditions Page 17 of 18 Version 11/09/2011 enforceable Pretreatment Standards as defined by 40 CFR 403.3(1). [15A NCAC 02H .0903(b)(10), .0905, and .0906(b)(4)] 5. Industrial User Pretreatment Permits (IUP) & Allocation Tables In accordance with NCGS 143-215.1, the Permittee shall issue to all Significant Industrial Users, permits for operation of pretreatment equipment and discharge to the Permittee's collection system or treatment works. These permits shall contain limitations, sampling protocols, reporting requirements, appropriate standard and special conditions, and compliance schedules as necessary for the installation of treatment and control technologies to assure that their wastewater discharge will meet all applicable pretreatment standards and requirements. The Permittee shall maintain a current Allocation Table (AT) which summarizes the results of the HWA and the limits from all IUPs. Permitted IUP loadings for each parameter cannot exceed the treatment capacity of the POTW as determined by the HWA. [15A NCAC 02H .0906(b)(6), .0909, .0916, and .0917; 40 CFR 403.5, 403.8(f)(1)(iii); NCGS 143-215.67(a)] 6. Authorization to Construct (AtC) The Permittee shall ensure that an Authorization to Construct permit (AtC) is issued to all applicable Industrial Users for the construction or modification of any pretreatment facility. Prior to the issuance of an AtC, the proposed pretreatment facility and treatment process must be evaluated for its capacity to comply with all Industrial User Pretreatment Permit (IUP) limitations. [15A NCAC 02H .0906(b)(7) and .0905; NCGS 143- 215.1(a)(8)] 7. POTW Inspection & Monitoring of their IUs The Permittee shall conduct inspection, surveillance, and monitoring activities as described in its Division approved pretreatment program in order to determine, independent of information supplied by Industrial Users, compliance with applicable pretreatment standards. [15A NCAC 02H .0908(e); 40 CFR 403.8(f)(2)(v)] The Permittee must: a. Inspect all Significant Industrial Users (SIUs) at least once per calendar year; b. Sample all Significant Industrial Users (SIUs) at least once per calendar year for all SIU permit-limited parameters including flow except as allowed under 15A NCAC .0908(e); and c. At least once per year, document an evaluation of any non-significant categorical Industrial User for compliance with the requirements in 40 CFR 403.3(v)(2), and either continue or revoke the designation as non- significant. 8. IU Self Monitoring and Reporting The Permittee shall require all Industrial Users to comply with the applicable monitoring and reporting requirements outlined in the Division-approved pretreatment program, the industry's pretreatment permit, or in 15A NCAC 02H .0908. [15A NCAC 02H .0906(b)(5) and .0905; 40 CFR 403.8(f)(1)(v) and (2)(iii); 40 CFR 122.44(j)(2) and 40 CFR 403.12] 9. Enforcement Response Plan (ERP) The Permittee shall enforce and obtain appropriate remedies for violations of all pretreatment standards promulgated pursuant to section 307(b) and (c) of the CWA (40 CFR 405 et. seq.), prohibitive discharge standards as set forth in 40 CFR 403.5 and 15A NCAC 02H .0909, specific local limitations, and other pretreatment requirements. All remedies, enforcement actions and other, shall be consistent with the Enforcement Response Plan (ERP) approved by the Division. [15A NCAC 02H .0903(b)(7), .0906(b)(8) and .0905; 40 CFR 403.8(f)(5)] 10. Pretreatment Annual Reports (PAR) The Permittee shall report to the Division in accordance with 15A NCAC 02H .0908. In lieu of submitting annual reports, Modified Pretreatment Programs developed under 15A NCAC 02H .0904 (b) may be required to submit a partial annual report or to meet with Division personnel periodically to discuss enforcement of pretreatment requirements and other pretreatment implementation issues. For all other active pretreatment programs, the Permittee shall submit two copies of a Pretreatment Annual Report (PAR) describing its pretreatment activities over the previous calendar year to the Division at the following address: DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138 NPDES Permit Standard Conditions Page 18 of 18 Version 11/09/2011 NC DENR / Division of Water Quality / Surface Water Protection Section Pretreatment, Emergency Response, and Collection Systems (PERCS) Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 These reports shall be submitted by March 1 of each year and shall contain the following: a. Narrative A narrative summary detailing actions taken, or proposed, by the Permittee to correct significant non- compliance and to ensure compliance with pretreatment requirements; b. Pretreatment Program Summary (PPS) A pretreatment program summary (PPS) on forms or in a format provided by the Division; c. Significant Non-Compliance Report (SNCR) A list of Industrial Users (IUs) in significant noncompliance (SNC) with pretreatment requirements, and the nature of the violations on forms or in a format provided by the Division; d. Industrial Data Summary Forms (IDSF) Monitoring data from samples collected by both the POTW and the Significant Industrial Users (SIUs). These analytical results must be reported on Industrial Data Summary Forms (IDSF) or on other forms or in a format provided by the Division; e. Other Information Copies of the POTW's allocation table, new or modified enforcement compliance schedules, public notice of IUs in SNC, a summary of data or other information related to significant noncompliance determinations for IUs that are not considered SIUs, and any other information, upon request, which in the opinion of the Director is needed to determine compliance with the pretreatment implementation requirements of this permit; 11. Public Notice The Permittee shall publish annually a list of Industrial Users (IUs) that were in significant noncompliance (SNC) as defined in the Permittee's Division-approved Sewer Use Ordinance with applicable pretreatment requirements and standards during the previous twelve month period. This list shall be published within four months of the applicable twelve-month period. [15A NCAC 02H .0903(b)(34), .0908(b)(5) and .0905 and 40 CFR 403.8(f)(2)(viii)] 12. Record Keeping The Permittee shall retain for a minimum of three years records of monitoring activities and results, along with support information including general records, water quality records, and records of industrial impact on the POTW and shall retain all other Pretreatment Program records as required by 15A NCAC 02H .0908(f). [15A NCAC 02H .0908(f); 40 CFR 403.12(o)] 13. Pretreatment Program Resources The Permittee shall maintain adequate funding and qualified personnel to accomplish the objectives of its approved pretreatment program. and retain a written description of those current levels of inspection. [15A NCAC 02H .0906(b)(9) and (10) and .0905; 40 CFR 403.8(f)(3), 403.9(b)(3)] 14. Modification to Pretreatment Programs Modifications to the approved pretreatment program including but not limited to local limits modifications, POTW monitoring of their Significant Industrial Users (SIUs), and Monitoring Plan modifications, shall be considered a permit modification and shall be governed by 40 CFR 403.18, 15 NCAC 02H .0114 and 15A NCAC 02H .0907. DocuSign Envelope ID: 7BBE1705-8F8C-42E3-9053-B7F66EF45138