WQ0003924_Shield Report on corrective Action bing taken_20210821

Report of
Laboratory Results of Pond and Tank Sampling
Celadon Recycling Solutions Facility
Lincolnton, North Carolina
Prepared for:
Linco Partnership
5200 Old Harding Rd
Nashville, Tennessee
Prepared by:
Shield Engineering, Inc.
4301 Taggart Creek Road
Charlotte, North Carolina
Shield Project No. 1210037-01
July 2021
SHIELD
ENGINEERING

SHIELD
ENGINEERING
July 23, 2021
Mr. Ron Buck
Linco Partnership
5200 Old Harding Road
Nashville, TN 37064
Subject: Laboratory Results of Pond and Tank Sampling
Celadon Recycling Solutions Facility
Lincointon, NC
Shield Project No. 1210037-01
Dear Mr. Buck,
Shield Engineering (Shield) is pleased to present our report of Laboratory Results of Pond and
Tank Sampling at the subject facility. The attached report contains Shield's methods of
investigation, findings and conclusions.
We appreciate the opportunity to provide our professional services on this matter. Please let
us know if you have any questions about this report or other aspects of this project.
Sincerely,
SHIELD ENGINEERING, INC.
Thomas W. Witner, P.G.
Prince
Robert L. Griffin, P.E.
President, CEO
Attachments:
Report
Photographs
Laboratory Reports
4301 Taggart Creek Road www.shieldengineeringcom Telephone [phone]
Charlotte, NC 28208 License No. F-0856

Results of Pond and Tank Sampling
Celadon Recycling Solutions
Shield Project No. 1210037-01
Intrnrillrtinn
July 23, 2021
Page 1
Linco Partnership has engaged Shield Engineering ("Shield") to provide technical services to aid
in developing a plan for addressing certain site conditions on its property in Lincolnton, NC. The
property at 288 Whitehouse Dr, Lincolnton, NC is the site where Celadon Recycling Services
formerly operated a Centralized Waste Treatment facility. Among other things, Shield was
engaged to investigate and characterize the water quality and sludge material in an 0.81 acre
pond ("Pond") and a 300,000 gallon open -top holding tank, referred to as the equalization tank
("Tank") on the property. See attached photographs. The effort, as described below, required
Shield to conduct a sampling program and obtain EPA -certified laboratory analysis of the Pond
water, sludge, and wastewater from the Tank. This report presents the results of the analytical
program related to those conditions on the property and describes site features, Shield's field
procedures, laboratory testing protocols and a summary of findings. Copies of the laboratory
results from eurofins TestAmerica are provided as an Attachment. Analytical Report ID 400-
203460-1 addresses water samples from the Pond (Sample ID W-1) and from the Tank (Sample
ID EQ-1). The second, Analytical Report ID 400-203461-1, addresses the results of a five -sample
composite sample of the sediment/sludge from the Pond (Sample ID S1-5 Composite).
SUMMARY FINDINGS
• Very few analyzed constituents were detected in the Tank and Pond samples. Detected
constituent concentrations in the samples are considered relatively low. No constituent
was found at amounts that would cause the waters to be considered hazardous waste.
No constituents were detected at levels that exceed common regulatory thresholds such
as US EPA Regional Screening Levels, US EPA Maximum Contaminant Levels, and North
Carolina surface and groundwater standards used for context.
• In general, as with the water samples, few analyzed constituents were detected in the
sludge. All the TCLP results for both organics and metals were reported as "ND" (Not
SHIELD
ENGINEERING

Results of Pond and Tank Sampling
Celadon Recycling Solutions
Shield Project No. 1210037-01
July 23, 2021
Page 2
Detected at the reporting limit) indicating that the sludge did not contain detectable
concentrations of D-Listed hazardous waste.
Sampling Methodologies/Volumes
Sampling of the Pond water, identified in the lab reports as "W-1", and the Tank, referred to as
"EQ-111, as well as sludge from the pond, referred to as "S1-5 Composite", was conducted on May
13, 2021. Sampling, sample handling, and chains of custody were conducted in accord with
standard methods. Water samples from the Pond were obtained in the nominal center at
approximately 1 foot below the surface by Shield's sampling crew working out of a flat -bottom
boat. The Tank, which is continuously mixed by pump recirculation therefore keeping solids in
suspension, was sampled at the top from the exterior access ladder.
The Pond bottom sludge samples were obtained by Shield's field crew at five representative
locations in the Pond and were taken from the boat and from the catwalk on the east end of the
Pond. The boat was held stable at each location by tethering to polypropylene ropes crossing
the water at fixed locations and tied to the security fence that surrounds the Pond. A stainless -
steel sampling dredge (clam shell sampler) was used to obtain each of the five sludge samples.
For volume calculations, using a graduated rod and measuring tape, representative water -depth
and sludge -thickness measurements were obtained at eight locations. The Pond water depth
was determined to be nominally 6 feet to the top of the sludge. Water volume of the Pond is
estimated to be 1.2 million gallons and is variable due to precipitation and evaporation. The
sludge measured approximately 6 inches deep across the Pond and is estimated to be about 500
cubic yards. The Tank contains approximately 300,000 gallons.
SHIELD
ENGINEERING

Results of Pond and Tank Sampling
Celadon Recycling Solutions
Shield Project No. 1210037-01
July 23, 2021
Page 3
In accordance with standard field sampling methods, the separate water samples were placed
into laboratory -prepared containers. The separate sludge samples were also placed in
laboratory -prepared containers and all samples were packed on ice in insulated containers and
sent overnight to a U.S. EPA -certified laboratory, eurofins TestAmerica. The sludge samples were
composited at the analytical laboratory into one sample. Both water and sludge samples were
laboratory analyzed for a wide spectrum of analytes as described below.
Laboratory Analyses
All laboratory analysis were conducted by U.S. EPA SW-846 for RCRA testing under 40 C.F.R. §
260.11. The water samples were analyzed for volatile organic compounds (VOCs) by EPA Method
8260D, semi -volatile organic compounds (SVOCs) by EPA Method 8270E. The eight RCRA metals
by EPA Method 6010D and Method 7470A (mercury), along with selected wastewater
parameters - pH, temperature, ammonia, biochemical oxygen demand (BOD), chemical oxygen
demand (COD) and total suspended solids (TSS). As a conservative measure to identify other
potential problematic analytes, we broadened the analysis to include organochlorine pesticides
by EPA Method 8081B, and herbicides by EPA Method 8151A.
The Pond sludge sample was also analyzed for a wide spectrum of analytes including VOCs,
SVOCs, pesticides, herbicides, and eight RCRA metals. In addition, the sludge sample was
analyzed using EPA Method 1311 Toxicity Characteristics Leachate Procedure (TCLP) for VOCs,
SVOCs, pesticides, herbicides, and metals. TCLP results provide leachable values that can be used
to determine if a waste is hazardous by the toxicity characteristic under 40 C.F.R. § 261.24.
Pond W-1 and Tank EQ-1 Water Lab Results Summary
As demonstrated, over 95 percent of the analytes, including the pesticides and herbicides, tested
in the waters were not detected above the reporting limit (non -detected or "ND.") Of the
SHIELD
ENGINEERING

Results of Pond and Tank Sampling
Celadon Recycling Solutions
Shield Project No. 1210037-01
July 23, 2021
Page 4
approximately 150 organic constituents analyzed, only seven were detected in the Pond sample
and nine in the Tank sample. Only two out of eight metals, mercury and barium, were detected
in the Pond and the Tank samples. The Tank and Pond results are generally similar with the
exception being that the Tank sample has higher TSS (due to constant recirculation of water) and
COD than the Pond sample. The results for these limited constituents that were detected and
comparison to US EPA Regional Screening Levels and various water quality standards for context
are presented in Table 1.
As illustrated in Table 1, detected organic constituent concentrations are considered low with all
but one result (benzoic acid) in the micrograms per liter (µg/I aka parts per billion (ppb)) range.
Numerous detections were so low that they triggered "J" qualifiers signifying the results, while
higher than the method detection limit, are below the reporting limit and, therefore, are
estimated values.
These results differ slightly in both constituents and amounts from results from samples
conducted by the North Carolina Department of Environmental Quality (NCDEQ) in January 2021.
However, the sampling locations and methods used for those investigations are not clear, and so
Shield relies on its more recent and documented sampling to reflect the current conditions.
Importantly, referring to Table 1, no constituent was found at amounts that would cause the
waters to be considered hazardous waste. Another conclusion of the testing program is, except
for benzoic acid exceeding the NCDEQ groundwater standard in sample EQ-1, the absence of any
constituent at levels that exceed common regulatory thresholds such as US EPA Regional
Screening Levels, US EPA Maximum Contaminant Levels, and other water quality standards. It is
important to note that benzoic acid as well as several other detected constituents have few or
no standards in the aforementioned programs, further indicating relatively low toxicity risk of
those constituents. Finally, while a few of the parameters (e.g., BOD, COD, and TSS) are at levels
that exceed the nominal local limits for discharge to the Lincolnton publicly owned treatment
SHIELD
ENGINEERING

Results of Pond and Tank Sampling
Celadon Recycling Solutions
Shield Project No. 1210037-01
July 23, 2021
Page 5
works, the levels are well within the range that could be accepted if done so with proper testing
on a planned schedule and payment structure.
Pond Sludge (S-1) Laboratory Results Summary
In general, as with the water samples, relatively few analyzed constituents were even detected
in the sludge. Of the approximately 150 organic constituents analyzed, only seven were detected
in the sludge composite sample, all at low levels. Metals detected were barium, chromium, lead
and mercury, again at low levels.
All the TCLP results for both organics and metals were reported as "ND" indicating that the sludge
did not contain detectable concentrations of D-Listed hazardous waste. 40 C.F.R. §261.24.
Furthermore, levels detected are below the EPA's Regional Screening Levels for industrial soil and
below the levels recognized by the NCDEQ standards for Industrial/Commercial Health -Based
Preliminary Soil Remediation Goals. The laboratory results and comparisons for the sludge
analysis are provided in Table 2.
Conclusions
In Shield's opinion, the minor detection of organic compounds and metals in both the water
samples and the sludge samples does not warrant these materials being characterized as
hazardous waste. The results show the water and sludge samples are within the limits generally
acceptable for disposal by discharge to a publicly owned treatment works (water) or in a
municipal, non -hazardous landfill (sludge), subject to the requirements of the Pretreatment
Coordinator or the landfill permit for water and sludge, respectively.
SHIELD
ENGINEERING

Results of Pond and Tank Sampling
Celadon Recycling Solutions July 23, 2021
Shield Project No. 1210037-01 Page 6
Photographs
Photo 1- 300,000 gallon wastewater tank near pond.
Photo 2 - Pond looking west.
SHIELD
ENGINEERING

Table 1: Summary of Analytical Results- Water Samples
Celadon Recycling
288 Whitehouse Drive, Lincolnton, North Carolina
Shield Project 1210037-01
Analytical Method-->
EPA 8260 D
EPA 8270 E
EPA 8151 A
EPA 6010 D
EPA 7470 A
EPA 350.1
Miscellaneous
4-
2-Butanone
Carbon
Isobutyl
Methyl
3 & 4
Ammonia
Biochemical Oxygen
Chemical Oxygen
Acetone
Benzene
(MEK)
disulfide
alcohol
Toluene
Trimethylbenz
Acetate
2-Methyl-2-Propanol
Methylphenol
Benzoic Acid- DL
Phenol
Dicamba
Barium
Mercury
(undistilled)
pH
Temperature
Total Suspended Solids
Demand (BOD)
Demand
ene
15A NCAC 2L.0202 Standard ->
6000
1
4000
700
NE
600
400
NE
NE
NE
30000
30
NE
700
1
NE
NE
NE
NE
NE
NE
15A NCAC 02B Standard ----->
NE
NE
NE
NE
NE
11
NE
NE
NE
NE
NE
NE
NE
NE
0.012
NE
6.0-9.0
Narrative
NE
NE
NE
Standard
EPA Regional Screening Levels --- >
1.40E+04
4.60E-01
5.60E+03
8.10E+02
5.90E+03
1.10E+03
5.60E+01
2.00E+04
NE
NE
7.50E+04
5.80E+03
5.70E+02
3.80E+03
6.30E-01
NE
NE
NE
NE
NE
NE
EPA Regional Screening Levels -
MCLs --->
NE
2.6
NE
NE
NE
690
NE
NE
NE
NE
NE
NE
NE
820
100
NE
NE
NE
NE
NE
NE
Lincolnton Wastewater Ordinance
§54.005Industrial Local Limits
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
0.003
NE
NE
NE
250
250
250
mg/L
Location
Date
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
mg/L
mg/I
mg/L
SU
Temp (C)
mg/L
mg/L
mg/L
W-1
5/13/2021
203
ND
9.741
15.1
ND
3.71
ND
ND
90.1
36.91
12100
27.81
5.89
0.0137
0.08621
7.97
7.57
20.2
44
68.2
609*
EQ-1
5/13/2021
866
0.6791
33.1
0.6821
35.6
0.4151
0.8531
4.771
116
ND
46400
1911
ND
0.0332
0.1531
70
7.29
20
2000*
684*
15800
Notes:
ug/L=Units in micrograms per liter
mg/I=Units in milligrams per liter
ND= Not detected at or above the method detection limit specified in the laboratory report
NE= Not Established
1=Detected but below the Reporting Limit; therefore, the result is an estimated concentration
SU=Standard Unit
15A. NCAC 2L.0202= North Carolina Administrative Code 2L Groundwater Standards
15A NCAC 02B= North Carolina Water Quality Standards for Surface Waters
EPA Regional Screening Levels= Environmental Protection Agency Regional Screening Levels calculated for Tapwater
Bold Values exceed the 2L Standards
Underlined Values exceed 02B Water Quality Standards
Italics values exceed EPA Regional Screening Levels
-values exceed EPA Regional Screening Levels-MCLs
* Values exceed Lincolnton Wastewater Ordinance
All other data can be seen in the attached laboratory report.

Table 2: Summary of Analytical Results- Pond Sludge Samples
Celadon Recycling
288 Whitehouse Drive, Lincolnton, North Carolina
Shield Project 1210037-01
Analytical Method-->
EPA 8260 D
EPA 8270 E
EPA 6010 D
EPA 7470 A
2-Butanone
1,2,4-
Bis (2-ethylhexyl)
Barium
Chromium
TCLP
Mercury
Acetone
Ethylbenzene
4-Isopropyltoluene
Toluene
2-Methyl-2-Propanol
Benzaldehyde
TCLP Barium
Lead (Total)
TCLP Lead
TCLP Mercury
(MEK)
Trimethyl benzene
phthalate
(Total)
(Total)*
Chromium
(Total)
NCDEQ PSRG- Industrial/Commercial ----->
1.40E+08
4.00E+07
2.70E+04
NE
9.70E+06
3.70E+05
NE
1.60E+05
8.20E+05
4.70E+04
NA
3.50E+05
NA
6.00E+01
NA
7.00E+01
NA
EPA Regional Screening Levels -Industrial Soil---
6.70E+08
1.90E+08
2.50E+04
NE
4.70E+07
1.80E+06
NE
1.60E+05
8.20E+05
2.20E+05
NA
1.80E+06
NA
8.00E+02
NA
3.50E+02
NA
Location
Date
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
ug/Kg
mg/kg
mg/I
mg/kg
mg/I
mg/kg
mg/I
mg/kg
mg/I
Sl COMPOSITE
5/13/2021
503
1221
5.011
8.261
155
9.991
1670
16400B
23601
71.3
ND
291
ND
14.4
ND
0.326
ND
Notes:
ug/Kg=Units in micrograms per kilograms (parts per million)
mg/kg=Units in milligrams per kilogram
mg/I=Units in milligrams per liter
NA= Not applicable
ND= Not detected at or above the method detection limit specified in the laboratory report
NE= Not Established
B= Compound detected within the blank and sample
1=Detected but below the Reporting Limit; therefore, the result is an estimated concentration
NCDEQ PSRG= North Carolina Preliminary Soil Remediation Goals (PSRG) for Industria Commercial
Underlined Values exceed Industrial/Commercial Health Based PSRG
Italics Values exceed EPA Regional Screening Levels
Double Underlined Values exceed EPA Regional Screening Levels -Industrial Soil
* Limits are for Chrome III
All other data can be seen in the attached laboratory report.

urofins
Environment Testing
America
ANALYTICAL REPORT
Eurofins TestAmerica, Pensacola
3355 McLemore Drive
Pensacola, FL 32514
Tel: [phone]
Laboratory Job ID: 400-203460-1
Client Project/Site: Celadon
Revision: 1
For:
Shield Engineering Inc
4301 Taggart Creek Road
Charlotte, North Carolina 28208
Attn: Tom Witner
Authorized for release by:
612212021 8:13:37 AM
Ken Hayes, Project Manager II
[phone]
[e-mail]
Designee for
John Andros, Project Manager 1
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: Shield Engineering Inc
Project/Site: Celadon
Table of Contents
Laboratory Job ID: 400-203460-1
Cover Page ..............................................
1
Table of Contents .........................................
2
Case Narrative ...........................................
3 L
Detection Summary ........................................
5
Sample Summary .........................................
6
Client Sample Results ......................................
7
Definitions .........................................
17
Surrogate Summary .......................................
19
QC Association ...........................................
21 C
QC Sample Results ........................................
24
Chronicle ................................................
40
Method Summary .........................................
46
Certification Summary ......................................
47
Chain of Custody ..........................................
48
Receipt Checklists .........................................
49
Eurofins TestAmerica, Pensacola
Page 2 of 49 6/22/2021 (Rev. 1)

Case Narrative
Client: Shield Engineering Inc
Project/Site: Celadon
Job ID: 400-203460-1
Laboratory: Eurofins TestAmerica, Pensacola
Narrative
Job Narrative
400-203460-1
Job ID: 400-203460-1
Revised Report: Revised to report Benzoic Acid at the client's request after initial Ireporting. This report replaces the one generated on
05/24/21 @ 15:30.
Comments
No additional comments.
Receipt
The samples were received on 5/15/2021 8:58 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 0.00 C.
GC/MS VOA
Method 8260D: The laboratory control sample (LCS) for analytical batch 400-532736 recovered outside control limits for the following
analyte: Hexachlorobutadiene. This analyte was biased high in the LCS and was not detected in the associated samples; therefore, the
data have been reported.
Method 8260D: The continuing calibration verification (CCV) associated with batch 400-532736 recovered above the upper control limit for
Bromomethane, Hexachlorobutadiene and n-Butylbenzene . The samples associated with this CCV were non -detects for the affected
analyte; therefore, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
Method 8270E: The following samples were diluted due to the nature of the sample matrix: W-1 (400-203460-1) and EQ-1
(400-203460-2). Elevated reporting limits (RLs) are provided.
Method 8270E: Surrogate recovery for the following sample was outside control limits: EQ-1 (400-203460-2). Evidence of matrix
interference is present; therefore, re -extraction and/or re -analysis was not performed.
Method 8270E: The continuing calibration verification (CCV) associated with batch 400-532781 recovered outside acceptance criteria, low
biased, for Bis(2-chloroethyl)ether, Caprolactam, Nitrobenzene, Isophorone, Phenol, and Bis(2-chloroethoxy)methane. A reporting limit
(RL) standard was analyzed, and the target analyte was detected. Since the associated samples were less than the reporting limit for this
analyte, the data have been reported.
Method 8270E: Six surrogates are used for this analysis. The laboratory's SOP allows one of these surrogates to be outside acceptance
criteria without performing re-extraction/re-analysis. The following sample contained an allowable number of surrogate compounds
outside limits: W-1 (400-203460-1). These results have been reported and qualified.
Method 8270E: The continuing calibration verification (CCV) associated with batch 400-532788 recovered above the upper control limit for
Carbazole and Bis(2-ethylhexyl) phthalate. The samples associated with this CCV were non -detects for the affected analytes; therefore,
the data have been reported. The associated samples are impacted: (CCVIS 400-532788/3) and (MB 400-532580/1-A).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC Semi VOA
Method 8081 B: The continuing calibration verification (CCV) associated with batch 400-532257 recovered above the upper control limit for
4,4'-DDT. The samples associated with this CCV were non -detects for the affected analytes; therefore, the data have been reported.
Method 8081 B: Two surrogates are used for this analysis. The laboratory's SOP allows one of these surrogates to be outside acceptance
criteria without performing re-extraction/re-analysis. The following samples contained an allowable number of surrogate compounds
outside limits: W-1 (400-203460-1) and EQ-1 (400-203460-2). These results have been reported and qualified.
Method 8081 B: The following sample was diluted due to the nature of the sample matrix: EQ-1 (400-203460-2). Elevated reporting limits
Eurofins TestAmerica, Pensacola
Page 3 of 49 6/22/2021 (Rev. 1)

Case Narrative
Client: Shield Engineering Inc
Project/Site: Celadon
Job ID: 400-203460-1 (Continued)
Laboratory: Eurofins TestAmerica, Pensacola (Continued)
(RLs) are provided.
Job ID: 400-203460-1
Method 8081 B: The laboratory control sample duplicate (LCSD) recovered above calibration range for the following analytes: 4,4'-DDT and
Methoxychlor. However, the percent recoveries (%R) are within acceptance limits; therefore, the data has been reported. (LCSD
400-532015/3-A)
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method 7470A: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 400-531709 and analytical batch
400-532149 were outside control limits. Sample matrix interference and/or non -homogeneity are suspected because the associated
laboratory control sample (LCS) recovery was within acceptance limits.
Method 6010D: Method required MS/MSD and/or duplicate QC were prepared and analyzed at required batch frequency for preparation
batch 400-532043 and analytical batch 400-532226 using samples from other sites, and are not reported with this project.
Method 6010D: The continuing calibration verification (CCV) associated with batch 400-532226 recovered above the upper control limit for
Arsenic, Chromium and Selenium. The samples associated with this CCV were non -detects for the affected analytes; therefore, the data
have been reported. The associated samples are impacted: W-1 (400-203460-1), EQ-1 (400-203460-2) and (MB 400-532043/1-A).
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
General Chemistry
Method SM 5220D: The following samples were diluted to bring the concentration of target analytes within the calibration range: W-1
(400-203460-1) and EQ-1 (400-203460-2). Elevated reporting limits (RLs) are provided.
Method SM 5220D: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for analytical batch 400-532002 were outside control
limits. Sample matrix interference and/or non -homogeneity are suspected because the associated laboratory control sample (LCS)
recovery was within acceptance limits.
Method 350.1: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for analytical batch 400-532312 were outside control limits.
Sample matrix interference and/or non -homogeneity are suspected because the associated laboratory control sample (LCS) recovery was
within acceptance limits.
Method 350.1: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for analytical batch 400-532313 were outside control limits.
Sample matrix interference and/or non -homogeneity are suspected because the associated laboratory control sample (LCS) recovery was
within acceptance limits.
Method 350.1: The following samples were diluted to bring the concentration of target analytes within the calibration range: W-1
(400-203460-1) and EQ-1 (400-203460-2). Elevated reporting limits (RLs) are provided.
Method SM 5210B: The glucose-glutamic acid standard (LCS) recovered outside the recovery limits specified in the method in batch
400-531930. The method holding time had expired, therefore the analysis was not repeated. The data was qualified and reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep
Method 3520C: The following sample is a cloudy milky like sample that formed emulsions during the extraction procedure: EQ-1
(400-203460-2). Gel like emulsification leaked through the extractor arm during the run time. Matrix interference is expected.
Method 3520C: The following sample is a cloudy milky sample that formed emulsions during the extraction procedure: EQ-1
(400-203460-2). Gel like emulsifications leaked through the extractor arm during the run time. Matrix interference is expected.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Eurofins TestAmerica, Pensacola
Page 4 of 49 6/22/2021 (Rev. 1)

Detection Summary
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Client Sample ID: W-1
Lab Sample ID: 400-203460-1
Analyte
Result
Qualifier
RL
MDL
Unit
Dil Fac D
Method
Prep Type
Acetone
203
25.0
10.0
ug/L
1
8260D
Total/NA '
2-Butanone (MEK)
9.74
J
25.0
2.60
ug/L
1
8260D
Total/NA
Carbon disulfide
15.1
1.00
0.500
ug/L
1
8260D
Total/NA
Toluene
3.71
1.00
0.410
ug/L
1
8260D
Total/NA
2-Methyl-2-propanol
90.1
10.0
4.90
ug/L
1
8260D
Total/NA
3 & 4 Methylphenol
36.9
J
115
6.00
ug/L
5
8270E
Total/NA
Phenol
27.8
J
57.7
15.0
ug/L
5
8270E
Total/NA
Benzoic acid - DL
12100
3460
842
ug/L
100
8270E
Total/NA
Dicamba
5.89
5.84
0.0661
ug/L
1
8151A
Total/NA
Barium
0.0137
0.0100
0.00300
mg/L
1
6010D
Total/NA
Mercury
0.0862
J
0.200
0.0700
ug/L
1
7470A
Total/NA
Ammonia (undistilled)
7.97
0.100
0.0480
mg/L
2
350.1
Total/NA
pH
7.57
HF
Su
1
9040C
Total/NA
Temperature
20.2
HF
Degrees C
1
9040C
Total/NA
Total Suspended Solids
44.0
10.0
10.0
mg/L
1
SM 2540D
Total/NA
Biochemical Oxygen Demand
68.2
«+
2.00
2.00
mg/L
1
SM 5210B
Total/NA
Chemical Oxygen Demand
609
100
64.0
mg/L
10
SM 5220D
Total/NA
Client Sample ID: EQ-1
Lab Sample ID: 400-203460-2
Analyte
Result
Qualifier
RL
MDL
Unit
Dil Fac D
Method
Prep Type
Acetone
866
25.0
10.0
ug/L
1
8260D
Total/NA
Benzene
0.679
J
1.00
0.380
ug/L
1
8260D
Total/NA
2-Butanone (MEK)
33.1
25.0
2.60
ug/L
1
8260D
Total/NA
Carbon disulfide
0.682
J
1.00
0.500
ug/L
1
8260D
Total/NA
Isobutyl alcohol
35.6
25.0
10.0
ug/L
1
8260D
Total/NA
Toluene
0.415
J
1.00
0.410
ug/L
1
8260D
Total/NA
1,2,4-Trimethylbenzene
0.853
J
1.00
0.820
ug/L
1
8260D
Total/NA
Methyl acetate
4.77
J
5.00
2.50
ug/L
1
8260D
Total/NA
2-Methyl-2-propanol
116
10.0
4.90
ug/L
1
8260D
Total/NA
Phenol
191
J
224
58.2
ug/L
20
8270E
Total/NA
Benzoic acid - DL
46400
6720
1630
ug/L
200
8270E
Total/NA
Barium
0.0332
0.0100
0.00300
mg/L
1
6010D
Total/NA
Mercury
0.153
J
0.400
0.140
ug/L
1
7470A
Total/NA
Ammonia (undistilled)
70.0
1.00
0.480
mg/L
20
350.1
Total/NA
pH
7.29
HF
Su
1
9040C
Total/NA
Temperature
20.0
HF
Degrees C
1
9040C
Total/NA
Total Suspended Solids
2000
20.0
20.0
mg/L
1
SM 2540D
Total/NA
Biochemical Oxygen Demand
684
«+
2.00
2.00
mg/L
1
SM 5210B
Total/NA
Chemical Oxygen Demand
15800
4000
2560
mg/L
400
SM 5220D
Total/NA
This Detection Summary does not include radiochemical test results.
Eurofins TestAmerica, Pensacola
Page 5 of 49 6/22/2021 (Rev. 1)

Sample Summary
Client: Shield Engineering Inc
Project/Site: Celadon
Job ID: 400-203460-1
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID
400-203460-1 W-1 Water 05/13/2111:45 05/15/2108:58
400-203460-2 EQ-1 Water 05/13/2115:15 05/15/2108:58
Eurofins TestAmerica, Pensacola
Page 6 of 49 6/22/2021 (Rev. 1)

Client Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
Job ID: 400-203460-1
Client Sample ID: W-1 Lab Sample ID: 400-203460-1
Date Collected: 05/13/21 11:45 Matrix: Water
Date Received: 05/15/21 08:58
Method: 8260D - Volatile Organic Compounds by GC/MS
Analyte
Result Qualifier
Acetone
203
Benzene
ND
Bromobenzene
ND
Chlorobromomethane
ND
Dichlorobromomethane
ND
Bromoform
ND
Bromomethane
ND
2-Butanone (MEK)
9.74 J
n-Butylbenzene
ND
sec- Butylbenzene
ND
tert-Butylbenzene
ND
Carbon disulfide
15.1
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroethane
ND
Chloroform
ND
Chloromethane
ND
3-Chloro-1-propene
ND
2-Chlorotoluene
ND
4-Chlorotoluene
ND
Chlorodibromomethane
ND
1,2-Dibromo-3-Chloropropane
ND
Ethylene Dibromide
ND
Dibromomethane
ND
1,2-Dichlorobenzene
ND
1,3-Dichlorobenzene
ND
1,4-Dichlorobenzene
ND
trans-1,4-Dichloro-2-butene
ND
Dichlorodifluoromethane
ND
1,1-Dichloroethane
ND
1,2-Dichloroethane
ND
cis-1,2-Dichloroethene
ND
trans- 1,2-Dichloroethene
ND
1,2-Dichloroethene, Total
ND
1,1-Dichloroethene
ND
1,2-Dichloropropane
ND
1,3-Dichloropropane
ND
2,2-Dichloropropane
ND
1,1-Dichloropropene
ND
cis-1,3-Dichloropropene
ND
trans- 1,3-Dichloropropene
ND
Ethylbenzene
ND
Ethyl methacrylate
ND
Hexachlorobutadiene
ND `+
2-Hexanone
ND
lodomethane
ND
Isobutyl alcohol
ND
Isopropylbenzene
ND
4-Isopropyltoluene
ND
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
25.0
10.0
ug/L
05/21/2112:48
1
1.00
0.380
ug/L
05/21/2112:48
1
1.00
0.540
ug/L
05/21/2112:48
1
1.00
0.520
ug/L
05/21/2112:48
1
1.00
0.500
ug/L
05/21/2112:48
1
5.00
0.710
ug/L
05/21/2112:48
1
1.00
0.980
ug/L
05/21/2112:48
1
25.0
2.60
ug/L
05/21/2112:48
1
1.00
0.760
ug/L
05/21/2112:48
1
1.00
0.700
ug/L
05/21/2112:48
1
1.00
0.630
ug/L
05/21/2112:48
1
1.00
0.500
ug/L
05/21/2112:48
1
1.00
0.500
ug/L
05/21/2112:48
1
1.00
0.500
ug/L
05/21/2112:48
1
1.00
0.760
ug/L
05/21/2112:48
1
1.00
0.600
ug/L
05/21/2112:48
1
1.00
0.830
ug/L
05/21/2112:48
1
5.00
1.00
ug/L
05/21/2112:48
1
1.00
0.570
ug/L
05/21/2112:48
1
1.00
0.560
ug/L
05/21/2112:48
1
1.00
0.500
ug/L
05/21/2112:48
1
5.00
1.50
ug/L
05/21/2112:48
1
1.00
0.500
ug/L
05/21/2112:48
1
5.00
0.590
ug/L
05/21/2112:48
1
1.00
0.500
ug/L
05/21/2112:48
1
1.00
0.540
ug/L
05/21/2112:48
1
1.00
0.640
ug/L
05/21/2112:48
1
5.00
1.00
ug/L
05/21/2112:48
1
1.00
0.850
ug/L
05/21/2112:48
1
1.00
0.500
ug/L
05/21/2112:48
1
1.00
0.500
ug/L
05/21/2112:48
1
1.00
0.500
ug/L
05/21/2112:48
1
1.00
0.500
ug/L
05/21/2112:48
1
10.0
0.640
ug/L
05/21/2112:48
1
1.00
0.500
ug/L
05/21/2112:48
1
1.00
0.500
ug/L
05/21/2112:48
1
1.00
0.500
ug/L
05/21/2112:48
1
1.00
0.500
ug/L
05/21/2112:48
1
1.00
0.500
ug/L
05/21/2112:48
1
5.00
0.500
ug/L
05/21/2112:48
1
5.00
0.500
ug/L
05/21/2112:48
1
1.00
0.500
ug/L
05/21/2112:48
1
1.00
0.600
ug/L
05/21/2112:48
1
5.00
0.900
ug/L
05/21/2112:48
1
25.0
3.10
ug/L
05/21/2112:48
1
1.00
0.900
ug/L
05/21/2112:48
1
25.0
10.0
ug/L
05/21/2112:48
1
1.00
0.530
ug/L
05/21/2112:48
1
1.00
0.710
ug/L
05/21/2112:48
1
0
Eurofins TestAmerica, Pensacola
Page 7 of 49 6/22/2021 (Rev. 1)

Client Sample Results
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Client Sample ID: W-1
Lab Sample
ID: 400-203460-1
Date Collected: 05/13/21 11:45
Matrix:
Water
Date Received: 05/15/21 08:58
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Methylene Chloride
ND
5.00
3.00
ug/L
05/21/21 12:48
1
4-Methyl-2-pentanone (MIBK)
ND
25.0
1.80
ug/L
05/21/21 12:48
1
Methyl tert-butyl ether
ND
1.00
0.740
ug/L
05/21/21 12:48
1
Naphthalene
ND
1.00
1.00
ug/L
05/21/21 12:48
1
N-Propylbenzene
ND
1.00
0.690
ug/L
05/21/21 12:48
1
Styrene
ND
1.00
1.00
ug/L
05/21/21 12:48
1
1,1,1,2-Tetrachloroethane
ND
1.00
0.520
ug/L
05/21/21 12:48
1
1,1,2,2-Tetrachloroethane
ND
1.00
0.500
ug/L
05/21/21 12:48
1
Tetrachloroethene
ND
1.00
0.580
ug/L
05/21/21 12:48
1
Toluene
3.71
1.00
0.410
ug/L
05/21/21 12:48
1
1,2,3-Trichlorobenzene
ND
1.00
0.700
ug/L
05/21/21 12:48
1
1,2,4-Trichlorobenzene
ND
1.00
0.820
ug/L
05/21/21 12:48
1
1,1,1-Trichloroethane
ND
1.00
0.500
ug/L
05/21/21 12:48
1
1,1,2-Trichloroethane
ND
5.00
0.500
ug/L
05/21/21 12:48
1
Trichloroethene
ND
1.00
0.500
ug/L
05/21/21 12:48
1
Trichlorofluoromethane
ND
1.00
0.520
ug/L
05/21/21 12:48
1
1,2,3-Trichloropropane
ND
5.00
0.840
ug/L
05/21/21 12:48
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.00
0.500
ug/L
05/21/21 12:48
1
1,2,4-Trimethylbenzene
ND
1.00
0.820
ug/L
05/21/21 12:48
1
1,3,5-Trimethylbenzene
ND
1.00
0.560
ug/L
05/21/21 12:48
1
Vinyl acetate
ND
25.0
2.00
ug/L
05/21/21 12:48
1
Vinyl chloride
ND
1.00
0.500
ug/L
05/21/21 12:48
1
o-Xylene
ND
5.00
0.600
ug/L
05/21/21 12:48
1
m-Xylene & p-Xylene
ND
5.00
1.60
ug/L
05/21/21 12:48
1
Xylenes, Total
ND
10.0
1.60
ug/L
05/21/21 12:48
1
Cyclohexane
ND
1.00
0.500
ug/L
05/21/21 12:48
1
Methyl acetate
ND
5.00
2.50
ug/L
05/21/21 12:48
1
Methylcyclohexane
ND
1.00
0.500
ug/L
05/21/21 12:48
1
Tetrahydrofuran
ND
5.00
1.50
ug/L
05/21/21 12:48
1
Hexane
ND
1.00
0.960
ug/L
05/21/21 12:48
1
Ethyl ether
ND
1.00
0.600
ug/L
05/21/21 12:48
1
n-Heptane
ND
1.00
0.700
ug/L
05/21/21 12:48
1
1,3-Dichloropropene, Total
ND
5.00
0.500
ug/L
05/21/21 12:48
1
Butadiene
ND
1.00
0.500
ug/L
05/21/21 12:48
1
Dichlorofluoromethane
ND
1.00
0.500
ug/L
05/21/21 12:48
1
2-Methyl-2-propanol
90.1
10.0
4.90
ug/L
05/21/21 12:48
1
1,4-Dioxane
ND
400
100
ug/L
05/21/21 12:48
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
4-Bromofluorobenzene
94
78 - 118
05121121 12:48
1
Dibromofluoromethane
102
81- 121
05121121 12:48
1
Toluene-d8 (Surr)
98
80 - 120
05121121 12:48
1
1,2-Dichloroethane-d4 (Surr)
98
67- 134
05121121 12:48
1
Method: 8270E - Semivolatile Organic Compounds
(GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Atrazine
ND
57.7
2.60
ug/L
05/20/2109:44
05/21/2121:11
5
4-Chloro-3-methylphenol
ND
57.7
21.9
ug/L
05/20/2109:44
05/21/2121:11
5
2-Chlorophenol
ND
57.7
12.7
ug/L
05/20/2109:44
05/21/2121:11
5
2,4-Dichlorophenol
ND
57.7
17.3
ug/L
05/20/2109:44
05/21/2121:11
5
0
Eurofins TestAmerica, Pensacola
Page 8 of 49 6/22/2021 (Rev. 1)

Client Sample Results
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Client Sample ID: W-1
Lab Sample
ID: 400-203460-1
Date Collected: 05/13/21 11:45
Matrix: Water
Date Received: 05/15/21 08:58
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
2,4-Dimethylphenol
ND
57.7
20.2
ug/L
05/20/21 09:44
05/21/21 21:11
5
4,6-Dinitro-2-methyl phenol
ND
57.7
11.5
ug/L
05/20/21 09:44
05/21/21 21:11
5 �.
2,4-Dinitrophenol
ND
173
19.6
ug/L
05/20/21 09:44
05/21/21 21:11
5
2-Methylphenol
ND
57.7
10.4
ug/L
05/20/21 09:44
05/21/21 21:11
5
3 & 4 Methylphenol
36.9 J
115
6.00
ug/L
05/20/21 09:44
05/21/21 21:11
5
2-Nitrophenol
ND
57.7
3.75
ug/L
05/20/21 09:44
05/21/21 21:11
5
4-Nitrophenol
ND
57.7
12.1
ug/L
05/20/21 09:44
05/21/21 21:11
5
Pentachlorophenol
ND
115
10.4
ug/L
05/20/21 09:44
05/21/21 21:11
5
Phenol
27.8 J
57.7
15.0
ug/L
05/20/21 09:44
05/21/21 21:11
5
2,4,5-Trichlorophenol
ND
57.7
21.3
ug/L
05/20/21 09:44
05/21/21 21:11
5
2,4,6-Trichlorophenol
ND
57.7
20.2
ug/L
05/20/21 09:44
05/21/21 21:11
5
Acenaphthene
ND
57.7
2.65
ug/L
05/20/21 09:44
05/21/21 21:11
5
Acenaphthylene
ND
57.7
3.23
ug/L
05/20/21 09:44
05/21/21 21:11
5
Acetophenone
ND
57.7
3.58
ug/L
05/20/21 09:44
05/21/21 21:11
5
Anthracene
ND
57.7
2.42
ug/L
05/20/21 09:44
05/21/21 21:11
5
Benzaldehyde
ND
57.7
7.50
ug/L
05/20/21 09:44
05/21/21 21:11
5
Benzo[a]anthracene
ND
57.7
1.96
ug/L
05/20/21 09:44
05/21/21 21:11
5
Benzo[a]pyrene
ND
57.7
2.48
ug/L
05/20/21 09:44
05/21/21 21:11
5
Benzo[k]fluoranthene
ND
57.7
2.19
ug/L
05/20/21 09:44
05/21/21 21:11
5
Benzo[k]fluoranthene
ND
57.7
3.12
ug/L
05/20/21 09:44
05/21/21 21:11
5
4-Bromophenyl phenyl ether
ND
57.7
1.85
ug/L
05/20/21 09:44
05/21/21 21:11
5
Butyl benzyl phthalate
ND
57.7
3.98
ug/L
05/20/21 09:44
05/21/21 21:11
5
Caprolactam
ND
57.7
21.9
ug/L
05/20/21 09:44
05/21/21 21:11
5
Carbazole
ND
57.7
5.02
ug/L
05/20/21 09:44
05/21/21 21:11
5
4-Chloroaniline
ND
57.7
19.6
ug/L
05/20/21 09:44
05/21/21 21:11
5
Bis(2-chloroethoxy)methane
ND
57.7
3.98
ug/L
05/20/21 09:44
05/21/21 21:11
5
Bis(2-chloroethyl)ether
ND
57.7
4.27
ug/L
05/20/21 09:44
05/21/21 21:11
5
2-Chloronaphthalene
ND
57.7
3.00
ug/L
05/20/21 09:44
05/21/21 21:11
5
4-Chlorophenyl phenyl ether
ND
57.7
11.5
ug/L
05/20/21 09:44
05/21/21 21:11
5
Chrysene
ND
57.7
2.83
ug/L
05/20/21 09:44
05/21/21 21:11
5
Dibenz(a,h)anthracene
ND
57.7
6.75
ug/L
05/20/21 09:44
05/21/21 21:11
5
Dibenzofuran
ND
57.7
3.00
ug/L
05/20/21 09:44
05/21/21 21:11
5
Di-n-butyl phthalate
ND
57.7
15.6
ug/L
05/20/21 09:44
05/21/21 21:11
5
Di-n-octyl phthalate
ND
57.7
2.54
ug/L
05/20/21 09:44
05/21/21 21:11
5
3,3'-Dichlorobenzidine
ND
57.7
15.0
ug/L
05/20/21 09:44
05/21/21 21:11
5
Diethyl phthalate
ND
57.7
4.04
ug/L
05/20/21 09:44
05/21/21 21:11
5
Dimethyl phthalate
ND
57.7
3.46
ug/L
05/20/21 09:44
05/21/21 21:11
5
2,4-Dinitrotoluene
ND
57.7
11.0
ug/L
05/20/21 09:44
05/21/21 21:11
5
2,6-Dinitrotoluene
ND
57.7
11.0
ug/L
05/20/21 09:44
05/21/21 21:11
5
1,1'-Biphenyl
ND
57.7
2.31
ug/L
05/20/21 09:44
05/21/21 21:11
5
Bis(2-ethylhexyl) phthalate
ND
57.7
28.8
ug/L
05/20/21 09:44
05/21/21 21:11
5
Fluoranthene
ND
57.7
4.44
ug/L
05/20/21 09:44
05/21/21 21:11
5
Fluorene
ND
57.7
3.23
ug/L
05/20/21 09:44
05/21/21 21:11
5
Hexachlorobenzene
ND
57.7
1.44
ug/L
05/20/21 09:44
05/21/21 21:11
5
Hexachlorobutadiene
ND
57.7
20.8
ug/L
05/20/21 09:44
05/21/21 21:11
5
Hexachlorocyclopentadiene
ND
115
15.0
ug/L
05/20/21 09:44
05/21/21 21:11
5
Hexachloroethane
ND
57.7
24.2
ug/L
05/20/21 09:44
05/21/21 21:11
5
Indeno[1,2,3-cd]pyrene
ND
57.7
5.89
ug/L
05/20/21 09:44
05/21/21 21:11
5
Isophorone
ND
57.7
3.29
ug/L
05/20/21 09:44
05/21/21 21:11
5
Eurofins TestAmerica, Pensacola
Page 9 of 49 6/22/2021 (Rev. 1)

Client Sample Results
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Client Sample ID: W-1
Lab Sample
ID: 400-203460-1
Date Collected: 05/13/21 11:45
Matrix:
Water
Date Received: 05/15/21 08:58
Method: 8270E - Semivolatile Organic Compounds
(GC/MS) (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Naphthalene
ND
57.7
3.63
ug/L
05/20/2109:44
05/21/2121:11
5
2-Methylnaphthalene
ND
57.7
3.12
ug/L
05/20/2109:44
05/21/2121:11
5
3-Nitroaniline
ND
57.7
10.4
ug/L
05/20/2109:44
05/21/2121:11
5
4-Nitroaniline
ND
57.7
14.3
ug/L
05/20/2109:44
05/21/2121:11
5
Nitrobenzene
ND
57.7
3.17
ug/L
05/20/2109:44
05/21/2121:11
5
n-Nitrosodiphenylamine(as
ND
57.7
2.71
ug/L
05/20/2109:44
05/21/2121:11
5
diphenylamine)
N-Nitrosodi-n-propylamine
ND
57.7
19.0
ug/L
05/20/2109:44
05/21/2121:11
5
Phenanthrene
ND
57.7
2.37
ug/L
05/20/2109:44
05/21/2121:11
5
Pyrene
ND
57.7
6.29
ug/L
05/20/2109:44
05/21/2121:11
5
2,2'-oxybis(1-chloropropane)
ND
57.7
4.67
ug/L
05/20/2109:44
05/21/2121:11
5
2-Nitroaniline
ND
57.7
12.7
ug/L
05/20/2109:44
05/21/2121:11
5
Benzo[g,h,i]perylene
ND
57.7
6.12
ug/L
05/20/2109:44
05/21/2121:11
5
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4, 6-Tribromophenol (Surr)
121
15 - 135
05120121 09:44
05121121 21:11
5
2-Fluorobiphenyl
61
34 - 120
05120121 09:44
05121121 21:11
5
2-Fluorophenol (Surr)
22
10 - 120
05120121 09:44
05121121 21:11
5
Nitrobenzene-d5 (Surr)
46
27- 120
05120121 09:44
05121121 21:11
5
Phenol-d5 (Surr)
54
10 - 120
05120121 09:44
05121121 21:11
5
Terphenyl-d14 (Surr)
41 S1-
53- 125
05120121 09:44
05121121 21:11
5
Method: 8270E - Semivolatile Organic Compounds
(GC/MS) - DL
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Benzoic acid
12100
3460
842
ug/L
05/20/21 09:44
06/18/21 20:52
100
Method: 8081B - Organochlorine
Pesticides (GC)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Aldrin
ND
0.0206
0.00124
ug/L
05/17/21 09:06
05/18/21 16:16
1
alpha-BHC
ND
0.0206
0.00149
ug/L
05/17/21 09:06
05/18/21 16:16
1
beta-BHC
ND
0.0206
0.00124
ug/L
05/17/21 09:06
05/18/21 16:16
1
delta-BHC
ND
0.0206
0.000867
ug/L
05/17/21 09:06
05/18/21 16:16
1
gamma-BHC (Lindane)
ND
0.0516
0.0103
ug/L
05/17/21 09:06
05/18/21 16:16
1
cis -Chlordane
ND
0.0206
0.00173
ug/L
05/17/21 09:06
05/18/21 16:16
1
trans -Chlordane
ND
0.0206
0.00132
ug/L
05/17/21 09:06
05/18/21 16:16
1
4,4'-DDD
ND
0.0206
0.00124
ug/L
05/17/21 09:06
05/18/21 16:16
1
4,4'-DDE
ND
0.0206
0.000908
ug/L
05/17/21 09:06
05/18/21 16:16
1
4,4'-DDT
ND
0.0206
0.00161
ug/L
05/17/21 09:06
05/18/21 16:16
1
Dieldrin
ND
0.0206
0.00124
ug/L
05/17/21 09:06
05/18/21 16:16
1
Endosulfan I
ND
0.0206
0.00124
ug/L
05/17/21 09:06
05/18/21 16:16
1
Endosulfan II
ND
0.0206
0.00305
ug/L
05/17/21 09:06
05/18/21 16:16
1
Endosulfan sulfate
ND
0.0206
0.000867
ug/L
05/17/21 09:06
05/18/21 16:16
1
Endrin
ND
0.0206
0.00124
ug/L
05/17/21 09:06
05/18/21 16:16
1
Endrin aldehyde
ND
0.0206
0.00116
ug/L
05/17/21 09:06
05/18/21 16:16
1
Endrin ketone
ND
0.0206
0.00157
ug/L
05/17/21 09:06
05/18/21 16:16
1
Heptachlor
ND
0.0206
0.00128
ug/L
05/17/21 09:06
05/18/21 16:16
1
Heptachlor epoxide
ND
0.0206
0.00132
ug/L
05/17/21 09:06
05/18/21 16:16
1
Methoxychlor
ND
0.0206
0.00169
ug/L
05/17/21 09:06
05/18/21 16:16
1
Toxaphene
ND
3.09
0.124
ug/L
05/17/21 09:06
05/18/21 16:16
1
Eurofins TestAmerica, Pensacola
Page 10 of 49 6/22/2021 (Rev. 1)

Client Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
F
Job ID: 400-203460-1
Client Sample ID: W-1 Lab Sample ID: 400-203460-1
Date Collected: 05/13/21 11:45 Matrix: Water
Date Received: 05/15/21 08:58
Surrogate %Recovery
Qualifier
DCB Decachlorobiphenyl
10
Tetrachloro-m-xylene
19
S1-
Method: 8151A - Herbicides (GC)
Analyte
Result
Qualifier
2,4,5-T
ND
2,4-D
ND
2,4-DB
ND
Dalapon
ND
Dicamba
5.89
Dichlorprop
ND
Dinoseb
ND
MCPA
ND
Silvex (2,4,5-TP)
ND
Mecoprop
ND
Surrogate %Recovery
Qualifier
DCAA
99
Method: 6010D - Metals (ICP)
Analyte
Result
Qualifier
Silver
ND
Arsenic
ND
A+
Barium
0.0137
Cadmium
ND
Chromium
ND
^+
Lead
ND
Selenium
ND
^+
Method: 7470A - Mercury (CVAA)
Analyte
Result
Qualifier
Mercury
0.0862
J
General Chemistry
Analyte
Result
Qualifier
pH
7.57
HF
Temperature
20.2
HF
Analyte
Result
Qualifier
Ammonia (undistilled)
7.97
Biochemical Oxygen Demand
68.2
*+
Chemical Oxygen Demand
609
Analyte
Result
Qualifier
Total Suspended Solids
44.0
Limits
Prepared
Analyzed
Dil Fac
10 - 130
05117121 09:06
05118121 16:16
1
43 - 130
05117121 09:06
05118121 16:16
1
Y
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
3.89
0.0389
ug/L
05/19/2108:17
05/20/2119:02
1
19.5
0.253
ug/L
05/19/2108:17
05/20/2119:02
1
19.5
0.311
ug/L
05/19/2108:17
05/20/2119:02
1
117
1.89
ug/L
05/19/2108:17
05/20/2119:02
1
5.84
0.0661
ug/L
05/19/2108:17
05/20/2119:02
1
13.6
0.233
ug/L
05/19/2108:17
05/20/2119:02
1
1.95
0.160
ug/L
05/19/2108:17
05/20/2119:02
1
3890
38.9
ug/L
05/19/2108:17
05/20/2119:02
1
3.89
0.0177
ug/L
05/19/2108:17
05/20/2119:02
1
3890
38.9
ug/L
05/19/2108:17
05/20/2119:02
1
Limits
Prepared
Analyzed
Dil Fac
30 - 142
05119121 08:17
05120121 19:02
1
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
0.00500
0.00100
mg/L
05/17/2110:44
05/17/2123:04
1
0.0100
0.00300
mg/L
05/17/2110:44
05/17/2123:04
1
0.0100
0.00300
mg/L
05/17/2110:44
05/19/2117:51
1
0.00500
0.00100
mg/L
05/17/2110:44
05/17/2123:04
1
0.0100
0.00500
mg/L
05/17/2110:44
05/17/2123:04
1
0.0100
0.00200
mg/L
05/17/2110:44
05/17/2123:04
1
0.0200
0.00800
mg/L
05/17/2110:44
05/17/2123:04
1
RL MDL Unit
0.200 0.0700 ug/L
NONE
NONE
Unit
Su
Degrees C
RL
MDL
Unit
0.100
0.0480
mg/L
2.00
2.00
mg/L
100
64.0
mg/L
RL
RL
Unit
10.0
10.0
mg/L
D Prepared Analyzed Dil Fac
05/17/2109:40 05/17/2113:48 1
D Prepared
Analyzed
Dil Fac
05/17/21 08:40
1
05/17/21 08:40
1
D Prepared
Analyzed
Dil Fac
05/18/2114:25
2
05/15/21 10:35
1
05/16/21 22:00
10
D Prepared
Analyzed
Dil Fac
05/17/21 12:08
1
Page 11 of 49
Eurofins TestAmerica, Pensacola
6/22/2021 (Rev. 1)

Client Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
Job ID: 400-203460-1
Client Sample ID: EQ-1 Lab Sample ID: 400-203460-2
Date Collected: 05/13/21 15:15 Matrix: Water
Date Received: 05/15/21 08:58
Method: 8260D - Volatile Organic Compounds by GC/MS
Analyte
Result Qualifier
Acetone
866
Benzene
0.679 J
Bromobenzene
ND
Chlorobromomethane
ND
Dichlorobromomethane
ND
Bromoform
ND
Bromomethane
ND
2-Butanone (MEK)
33.1
n-Butylbenzene
ND
sec- Butylbenzene
ND
tert-Butylbenzene
ND
Carbon disulfide
0.682 J
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroethane
ND
Chloroform
ND
Chloromethane
ND
3-Chloro-1-propene
ND
2-Chlorotoluene
ND
4-Chlorotoluene
ND
Chlorodibromomethane
ND
1,2-Dibromo-3-Chloropropane
ND
Ethylene Dibromide
ND
Dibromomethane
ND
1,2-Dichlorobenzene
ND
1,3-Dichlorobenzene
ND
1,4-Dichlorobenzene
ND
trans-1,4-Dichloro-2-butene
ND
Dichlorodifluoromethane
ND
1,1-Dichloroethane
ND
1,2-Dichloroethane
ND
cis-1,2-Dichloroethene
ND
trans- 1,2-Dichloroethene
ND
1,2-Dichloroethene, Total
ND
1,1-Dichloroethene
ND
1,2-Dichloropropane
ND
1,3-Dichloropropane
ND
2,2-Dichloropropane
ND
1,1-Dichloropropene
ND
cis-1,3-Dichloropropene
ND
trans- 1,3-Dichloropropene
ND
Ethylbenzene
ND
Ethyl methacrylate
ND
Hexachlorobutadiene
ND `+
2-Hexanone
ND
lodomethane
ND
Isobutyl alcohol
35.6
Isopropylbenzene
ND
4-Isopropyltoluene
ND
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
25.0
10.0
ug/L
05/21/2113:16
1
1.00
0.380
ug/L
05/21/2113:16
1
1.00
0.540
ug/L
05/21/2113:16
1
1.00
0.520
ug/L
05/21/2113:16
1
1.00
0.500
ug/L
05/21/2113:16
1
5.00
0.710
ug/L
05/21/2113:16
1
1.00
0.980
ug/L
05/21/2113:16
1
25.0
2.60
ug/L
05/21/2113:16
1
1.00
0.760
ug/L
05/21/2113:16
1
1.00
0.700
ug/L
05/21/2113:16
1
1.00
0.630
ug/L
05/21/2113:16
1
1.00
0.500
ug/L
05/21/2113:16
1
1.00
0.500
ug/L
05/21/2113:16
1
1.00
0.500
ug/L
05/21/2113:16
1
1.00
0.760
ug/L
05/21/2113:16
1
1.00
0.600
ug/L
05/21/2113:16
1
1.00
0.830
ug/L
05/21/2113:16
1
5.00
1.00
ug/L
05/21/2113:16
1
1.00
0.570
ug/L
05/21/2113:16
1
1.00
0.560
ug/L
05/21/2113:16
1
1.00
0.500
ug/L
05/21/2113:16
1
5.00
1.50
ug/L
05/21/2113:16
1
1.00
0.500
ug/L
05/21/2113:16
1
5.00
0.590
ug/L
05/21/2113:16
1
1.00
0.500
ug/L
05/21/2113:16
1
1.00
0.540
ug/L
05/21/2113:16
1
1.00
0.640
ug/L
05/21/2113:16
1
5.00
1.00
ug/L
05/21/2113:16
1
1.00
0.850
ug/L
05/21/2113:16
1
1.00
0.500
ug/L
05/21/2113:16
1
1.00
0.500
ug/L
05/21/2113:16
1
1.00
0.500
ug/L
05/21/2113:16
1
1.00
0.500
ug/L
05/21/2113:16
1
10.0
0.640
ug/L
05/21/2113:16
1
1.00
0.500
ug/L
05/21/2113:16
1
1.00
0.500
ug/L
05/21/2113:16
1
1.00
0.500
ug/L
05/21/2113:16
1
1.00
0.500
ug/L
05/21/2113:16
1
1.00
0.500
ug/L
05/21/2113:16
1
5.00
0.500
ug/L
05/21/2113:16
1
5.00
0.500
ug/L
05/21/2113:16
1
1.00
0.500
ug/L
05/21/2113:16
1
1.00
0.600
ug/L
05/21/2113:16
1
5.00
0.900
ug/L
05/21/2113:16
1
25.0
3.10
ug/L
05/21/2113:16
1
1.00
0.900
ug/L
05/21/2113:16
1
25.0
10.0
ug/L
05/21/2113:16
1
1.00
0.530
ug/L
05/21/2113:16
1
1.00
0.710
ug/L
05/21/2113:16
1
0
Eurofins TestAmerica, Pensacola
Page 12 of 49 6/22/2021 (Rev. 1)

Client Sample Results
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Client Sample ID: EQ-1
Lab Sample
ID: 400-203460-2
Date Collected: 05/13/21 15:15
Matrix:
Water
Date Received: 05/15/21 08:58
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Methylene Chloride
ND
5.00
3.00
ug/L
05/21/21 13:16
1
4-Methyl-2-pentanone (MIBK)
ND
25.0
1.80
ug/L
05/21/21 13:16
1
Methyl tert-butyl ether
ND
1.00
0.740
ug/L
05/21/21 13:16
1
Naphthalene
ND
1.00
1.00
ug/L
05/21/21 13:16
1
N-Propylbenzene
ND
1.00
0.690
ug/L
05/21/21 13:16
1
Styrene
ND
1.00
1.00
ug/L
05/21/21 13:16
1
1,1,1,2-Tetrachloroethane
ND
1.00
0.520
ug/L
05/21/21 13:16
1
1,1,2,2-Tetrachloroethane
ND
1.00
0.500
ug/L
05/21/21 13:16
1
Tetrachloroethene
ND
1.00
0.580
ug/L
05/21/21 13:16
1
Toluene
0.415
J
1.00
0.410
ug/L
05/21/21 13:16
1
1,2,3-Trichlorobenzene
ND
1.00
0.700
ug/L
05/21/21 13:16
1
1,2,4-Trichlorobenzene
ND
1.00
0.820
ug/L
05/21/21 13:16
1
1,1,1-Trichloroethane
ND
1.00
0.500
ug/L
05/21/21 13:16
1
1,1,2-Trichloroethane
ND
5.00
0.500
ug/L
05/21/21 13:16
1
Trichloroethene
ND
1.00
0.500
ug/L
05/21/21 13:16
1
Trichlorofluoromethane
ND
1.00
0.520
ug/L
05/21/21 13:16
1
1,2,3-Trichloropropane
ND
5.00
0.840
ug/L
05/21/21 13:16
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.00
0.500
ug/L
05/21/21 13:16
1
1,2,4-Trimethyl benzene
0.853
J
1.00
0.820
ug/L
05/21/21 13:16
1
1,3,5-Trimethylbenzene
ND
1.00
0.560
ug/L
05/21/21 13:16
1
Vinyl acetate
ND
25.0
2.00
ug/L
05/21/21 13:16
1
Vinyl chloride
ND
1.00
0.500
ug/L
05/21/21 13:16
1
o-Xylene
ND
5.00
0.600
ug/L
05/21/21 13:16
1
m-Xylene & p-Xylene
ND
5.00
1.60
ug/L
05/21/21 13:16
1
Xylenes, Total
ND
10.0
1.60
ug/L
05/21/21 13:16
1
Cyclohexane
ND
1.00
0.500
ug/L
05/21/21 13:16
1
Methyl acetate
4.77
J
5.00
2.50
ug/L
05/21/21 13:16
1
Methylcyclohexane
ND
1.00
0.500
ug/L
05/21/21 13:16
1
Tetrahydrofuran
ND
5.00
1.50
ug/L
05/21/21 13:16
1
Hexane
ND
1.00
0.960
ug/L
05/21/21 13:16
1
Ethyl ether
ND
1.00
0.600
ug/L
05/21/21 13:16
1
n-Heptane
ND
1.00
0.700
ug/L
05/21/21 13:16
1
1,3-Dichloropropene, Total
ND
5.00
0.500
ug/L
05/21/21 13:16
1
Butadiene
ND
1.00
0.500
ug/L
05/21/21 13:16
1
Dichlorofluoromethane
ND
1.00
0.500
ug/L
05/21/21 13:16
1
2-Methyl-2-propanol
116
10.0
4.90
ug/L
05/21/21 13:16
1
1,4-Dioxane
ND
400
100
ug/L
05/21/21 13:16
1
Surrogate
%Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
4-Bromofluorobenzene
112
78 - 118
05121121 13:16
1
Dibromofluoromethane
101
81- 121
05121121 13:16
1
Toluene-d8 (Surr)
103
80 - 120
05121121 13:16
1
1,2-Dichloroethane-d4 (Surr)
96
67- 134
05121121 13:16
1
Method: 8270E - Semivolatile Organic Compounds
(GC/MS)
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Atrazine
ND
224
10.1
ug/L
05/20/2109:44
05/21/2121:33
20
4-Chloro-3-methylphenol
ND
224
85.1
ug/L
05/20/2109:44
05/21/2121:33
20
2-Chlorophenol
ND
224
49.3
ug/L
05/20/2109:44
05/21/2121:33
20
2,4-Dichlorophenol
ND
224
67.2
ug/L
05/20/2109:44
05/21/2121:33
20
0
Eurofins TestAmerica, Pensacola
Page 13 of 49 6/22/2021 (Rev. 1)

Client Sample Results
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Client Sample ID: EQ-1
Lab Sample
ID: 400-203460-2
Date Collected: 05/13/21 15:15
Matrix:
Water
Date Received: 05/15/21 08:58
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
2,4-Dimethylphenol
ND
224
78.4
ug/L
05/20/21 09:44
05/21/21 21:33
20
4,6-Dinitro-2-methyl phenol
ND
224
44.8
ug/L
05/20/21 09:44
05/21/21 21:33
20 �.
2,4-Dinitrophenol
ND
672
76.1
ug/L
05/20/21 09:44
05/21/21 21:33
20
2-Methylphenol
ND
224
40.3
ug/L
05/20/21 09:44
05/21/21 21:33
20
3 & 4 Methylphenol
ND
448
23.3
ug/L
05/20/21 09:44
05/21/21 21:33
20
2-Nitrophenol
ND
224
14.6
ug/L
05/20/21 09:44
05/21/21 21:33
20
4-Nitrophenol
ND
224
47.0
ug/L
05/20/21 09:44
05/21/21 21:33
20
Pentachlorophenol
ND
448
40.5
ug/L
05/20/21 09:44
05/21/21 21:33
20
Phenol
191 J
224
58.2
ug/L
05/20/21 09:44
05/21/21 21:33
20
2,4,5-Trichlorophenol
ND
224
82.9
ug/L
05/20/21 09:44
05/21/21 21:33
20
2,4,6-Trichlorophenol
ND
224
78.4
ug/L
05/20/21 09:44
05/21/21 21:33
20
Acenaphthene
ND
224
10.3
ug/L
05/20/21 09:44
05/21/21 21:33
20
Acenaphthylene
ND
224
12.5
ug/L
05/20/21 09:44
05/21/21 21:33
20
Acetophenone
ND
224
13.9
ug/L
05/20/21 09:44
05/21/21 21:33
20
Anthracene
ND
224
9.41
ug/L
05/20/21 09:44
05/21/21 21:33
20
Benzaldehyde
ND
224
29.1
ug/L
05/20/21 09:44
05/21/21 21:33
20
Benzo[a]anthracene
ND
224
7.61
ug/L
05/20/21 09:44
05/21/21 21:33
20
Benzo[a]pyrene
ND
224
9.63
ug/L
05/20/21 09:44
05/21/21 21:33
20
Benzo[k]fluoranthene
ND
224
8.51
ug/L
05/20/21 09:44
05/21/21 21:33
20
Benzo[k]fluoranthene
ND
224
12.1
ug/L
05/20/21 09:44
05/21/21 21:33
20
4-Bromophenyl phenyl ether
ND
224
7.17
ug/L
05/20/21 09:44
05/21/21 21:33
20
Butyl benzyl phthalate
ND
224
15.5
ug/L
05/20/21 09:44
05/21/21 21:33
20
Caprolactam
ND
224
85.1
ug/L
05/20/21 09:44
05/21/21 21:33
20
Carbazole
ND
224
19.5
ug/L
05/20/21 09:44
05/21/21 21:33
20
4-Chloroaniline
ND
224
76.1
ug/L
05/20/21 09:44
05/21/21 21:33
20
Bis(2-chloroethoxy)methane
ND
224
15.5
ug/L
05/20/21 09:44
05/21/21 21:33
20
Bis(2-chloroethyl)ether
ND
224
16.6
ug/L
05/20/21 09:44
05/21/21 21:33
20
2-Chloronaphthalene
ND
224
11.6
ug/L
05/20/21 09:44
05/21/21 21:33
20
4-Chlorophenyl phenyl ether
ND
224
44.8
ug/L
05/20/21 09:44
05/21/21 21:33
20
Chrysene
ND
224
11.0
ug/L
05/20/21 09:44
05/21/21 21:33
20
Dibenz(a,h)anthracene
ND
224
26.2
ug/L
05/20/21 09:44
05/21/21 21:33
20
Dibenzofuran
ND
224
11.6
ug/L
05/20/21 09:44
05/21/21 21:33
20
Di-n-butyl phthalate
ND
224
60.5
ug/L
05/20/21 09:44
05/21/21 21:33
20
Di-n-octyl phthalate
ND
224
9.85
ug/L
05/20/21 09:44
05/21/21 21:33
20
3,3'-Dichlorobenzidine
ND
224
58.2
ug/L
05/20/21 09:44
05/21/21 21:33
20
Diethyl phthalate
ND
224
15.7
ug/L
05/20/21 09:44
05/21/21 21:33
20
Dimethyl phthalate
ND
224
13.4
ug/L
05/20/21 09:44
05/21/21 21:33
20
2,4-Dinitrotoluene
ND
224
42.6
ug/L
05/20/21 09:44
05/21/21 21:33
20
2,6-Dinitrotoluene
ND
224
42.6
ug/L
05/20/21 09:44
05/21/21 21:33
20
1,1'-Biphenyl
ND
224
8.96
ug/L
05/20/21 09:44
05/21/21 21:33
20
Bis(2-ethylhexyl) phthalate
ND
224
112
ug/L
05/20/21 09:44
05/21/21 21:33
20
Fluoranthene
ND
224
17.2
ug/L
05/20/21 09:44
05/21/21 21:33
20
Fluorene
ND
224
12.5
ug/L
05/20/21 09:44
05/21/21 21:33
20
Hexachlorobenzene
ND
224
5.60
ug/L
05/20/21 09:44
05/21/21 21:33
20
Hexachlorobutadiene
ND
224
80.6
ug/L
05/20/21 09:44
05/21/21 21:33
20
Hexachlorocyclopentadiene
ND
448
58.2
ug/L
05/20/21 09:44
05/21/21 21:33
20
Hexachloroethane
ND
224
94.1
ug/L
05/20/21 09:44
05/21/21 21:33
20
Indeno[1,2,3-cd]pyrene
ND
224
22.8
ug/L
05/20/21 09:44
05/21/21 21:33
20
Isophorone
ND
224
12.8
ug/L
05/20/21 09:44
05/21/21 21:33
20
Eurofins TestAmerica, Pensacola
Page 14 of 49 6/22/2021 (Rev. 1)

Client Sample Results
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Client Sample ID: EQ-1
Lab Sample
ID: 400-203460-2
Date Collected: 05/13/21 15:15
Matrix:
Water
Date Received: 05/15/21 08:58
Method: 8270E - Semivolatile Organic Compounds
(GC/MS) (Continued)
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Naphthalene
ND
224
14.1
ug/L
05/20/2109:44
05/21/2121:33
20
2-Methylnaphthalene
ND
224
12.1
ug/L
05/20/2109:44
05/21/2121:33
20
3-Nitroaniline
ND
224
40.3
ug/L
05/20/2109:44
05/21/2121:33
20
4-Nitroaniline
ND
224
55.5
ug/L
05/20/2109:44
05/21/2121:33
20
Nitrobenzene
ND
224
12.3
ug/L
05/20/2109:44
05/21/2121:33
20
n-Nitrosodiphenylamine(as
ND
224
10.5
ug/L
05/20/2109:44
05/21/2121:33
20
diphenylamine)
N-Nitrosodi-n-propylamine
ND
224
73.9
ug/L
05/20/2109:44
05/21/2121:33
20
Phenanthrene
ND
224
9.18
ug/L
05/20/2109:44
05/21/2121:33
20
Pyrene
ND
224
24.4
ug/L
05/20/2109:44
05/21/2121:33
20
2,2'-oxybis(1-chloropropane)
ND
224
18.1
ug/L
05/20/2109:44
05/21/2121:33
20
2-Nitroaniline
ND
224
49.3
ug/L
05/20/2109:44
05/21/2121:33
20
Benzo[g,h,i]perylene
ND
224
23.7
ug/L
05/20/2109:44
05/21/2121:33
20
Surrogate
%Recovery
Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol (Surr)
0
si-
15- 135
05120121 09:44
05121121 21:33
20
2-Fluorobiphenyl
11
S1-
34-120
05120121 09:44
0512112121:33
20
2-Fluorophenol (Surr)
3
S1-
10- 120
05120121 09:44
05121121 21:33
20
Nitrobenzene-d5 (Surr)
1
S1-
27- 120
05120121 09:44
05121121 21:33
20
Phenol-d5 (Surr)
8
S1-
10- 120
05120121 09:44
05121121 21:33
20
Terphenyl-d14 (Surr)
13
S1-
53- 125
05120121 09:44
05121121 21:33
20
Method: 8270E - Semivolatile Organic Compounds
(GC/MS) - DL
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Benzoic acid
46400
6720
1630
ug/L
05/20/21 09:44
06/18/21 21:13
200
Method: 8081B - Organochlorine
Pesticides
(GC)
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Aldrin
ND
0.102
0.00613
ug/L
05/17/21 09:06
05/18/21 16:43
5
alpha-BHC
ND
0.102
0.00736
ug/L
05/17/21 09:06
05/18/21 16:43
5
beta-BHC
ND
0.102
0.00613
ug/L
05/17/21 09:06
05/18/21 16:43
5
delta-BHC
ND
0.102
0.00429
ug/L
05/17/21 09:06
05/18/21 16:43
5
gamma-BHC (Lindane)
ND
0.255
0.0511
ug/L
05/17/21 09:06
05/18/21 16:43
5
cis -Chlordane
ND
0.102
0.00858
ug/L
05/17/21 09:06
05/18/21 16:43
5
trans -Chlordane
ND
0.102
0.00654
ug/L
05/17/21 09:06
05/18/21 16:43
5
4,4'-DDD
ND
0.102
0.00613
ug/L
05/17/21 09:06
05/18/21 16:43
5
4,4'-DDE
ND
0.102
0.00450
ug/L
05/17/21 09:06
05/18/21 16:43
5
4,4'-DDT
ND
0.102
0.00797
ug/L
05/17/21 09:06
05/18/21 16:43
5
Dieldrin
ND
0.102
0.00613
ug/L
05/17/21 09:06
05/18/21 16:43
5
Endosulfan I
ND
0.102
0.00613
ug/L
05/17/21 09:06
05/18/21 16:43
5
Endosulfan II
ND
0.102
0.0151
ug/L
05/17/21 09:06
05/18/21 16:43
5
Endosulfan sulfate
ND
0.102
0.00429
ug/L
05/17/21 09:06
05/18/21 16:43
5
Endrin
ND
0.102
0.00613
ug/L
05/17/21 09:06
05/18/21 16:43
5
Endrin aldehyde
ND
0.102
0.00572
ug/L
05/17/21 09:06
05/18/21 16:43
5
Endrin ketone
ND
0.102
0.00777
ug/L
05/17/21 09:06
05/18/21 16:43
5
Heptachlor
ND
0.102
0.00634
ug/L
05/17/21 09:06
05/18/21 16:43
5
Heptachlor epoxide
ND
0.102
0.00654
ug/L
05/17/21 09:06
05/18/21 16:43
5
Methoxychlor
ND
0.102
0.00838
ug/L
05/17/21 09:06
05/18/21 16:43
5
Toxaphene
ND
15.3
0.613
ug/L
05/17/21 09:06
05/18/21 16:43
5
Eurofins TestAmerica, Pensacola
Page 15 of 49 6/22/2021 (Rev. 1)

Client Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
F
Job ID: 400-203460-1
Client Sample ID: EQ-1 Lab Sample ID: 400-203460-2
Date Collected: 05/13/21 15:15 Matrix: Water
Date Received: 05/15/21 08:58
Surrogate %Recovery
Qualifier
DCB Decachlorobiphenyl
10
Tetrachloro-m-xylene
4
S1-
Method: 8151A - Herbicides (GC)
Analyte
Result
Qualifier
2,4,5-T
ND
2,4-D
ND
2,4-DB
ND
Dalapon
ND
Dicamba
ND
Dichlorprop
ND
Dinoseb
ND
MCPA
ND
Silvex (2,4,5-TP)
ND
Mecoprop
ND
Surrogate %Recovery
Qualifier
DCAA
98
Method: 6010D - Metals (ICP)
Analyte
Result
Qualifier
Silver
ND
Arsenic
ND
A+
Barium
0.0332
Cadmium
ND
Chromium
ND
Lead
ND
Selenium
ND
^+
Method: 7470A - Mercury (CVAA)
Analyte
Result
Qualifier
Mercury
0.153
J
General Chemistry
Analyte
Result
Qualifier
pH
7.29
HF
Temperature
20.0
HF
Analyte
Result
Qualifier
Ammonia (undistilled)
70.0
Biochemical Oxygen Demand
684
*+
Chemical Oxygen Demand
15800
Analyte
Result
Qualifier
Total Suspended Solids
2000
Limits
Prepared
Analyzed
Dil Fac
10 - 130
05117121 09:06
05118121 16:43
5
43 - 130
05117121 09:06
05118121 16:43
5
•
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
7.12
0.0712
ug/L
05/19/2108:17
05/20/2119:36
1
35.6
0.463
ug/L
05/19/2108:17
05/20/2119:36
1
35.6
0.569
ug/L
05/19/2108:17
05/20/2119:36
1
214
3.45
ug/L
05/19/2108:17
05/20/2119:36
1
10.7
0.121
ug/L
05/19/2108:17
05/20/2119:36
1
24.9
0.427
ug/L
05/19/2108:17
05/20/2119:36
1
3.56
0.292
ug/L
05/19/2108:17
05/20/2119:36
1
7120
71.2
ug/L
05/19/2108:17
05/20/2119:36
1
7.12
0.0324
ug/L
05/19/2108:17
05/20/2119:36
1
7120
71.2
ug/L
05/19/2108:17
05/20/2119:36
1
Limits
Prepared
Analyzed
Dil Fac
30 - 142
05119121 08:17
05120121 19:36
1
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
0.00500
0.00100
mg/L
05/17/2110:54
05/17/2123:12
1
0.0100
0.00300
mg/L
05/17/2110:54
05/17/2123:12
1
0.0100
0.00300
mg/L
05/17/2110:54
05/19/2117:55
1
0.00500
0.00100
mg/L
05/17/2110:54
05/17/2123:12
1
0.0100
0.00500
mg/L
05/17/2110:54
05/19/2117:55
1
0.0100
0.00200
mg/L
05/17/2110:54
05/17/2123:12
1
0.0200
0.00800
mg/L
05/17/2110:54
05/17/2123:12
1
RL MDL Unit
0.400 0.140 ug/L
NONE
NONE
Unit
Su
Degrees C
RL
MDL
Unit
1.00
0.480
mg/L
2.00
2.00
mg/L
4000
2560
mg/L
RL
RL
Unit
20.0
20.0
mg/L
D Prepared Analyzed Dil Fac
05/17/2109:40 05/17/2113:50 1
D Prepared
Analyzed
Dil Fac
05/17/21 08:40
1
05/17/21 08:40
1
D Prepared
Analyzed
Dil Fac
05/18/2114:26
20
05/15/21 10:36
1
05/16/2122:00
400
D Prepared
Analyzed
Dil Fac
05/17/21 12:08
1
Page 16 of 49
Eurofins TestAmerica, Pensacola
6/22/2021 (Rev. 1)

Definitions/Glossary
Client: Shield Engineering Inc Job ID: 400-203460-1
Project/Site: Celadon
Qualifiers
GC/MS VOA
Qualifier Qualifier Description
*+ LCS and/or LCSD is outside acceptance limits, high biased.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC/MS Semi VOA
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
S1- Surrogate recovery exceeds control limits, low biased.
GC Semi VOA
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
S1- Surrogate recovery exceeds control limits, low biased.
Metals
Qualifier Qualifier Description
A+ Continuing Calibration Verification (CCV) is outside acceptance limits, high biased.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
General Chemistry
Qualifier Qualifier Description
*+ LCS and/or LCSD is outside acceptance limits, high biased.
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
a Listed under the "Y column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRIES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
Eurofins TestAmerica, Pensacola
Page 17 of 49 6/22/2021 (Rev. 1)

Definitions/Glossary
Client: Shield Engineering Inc
Project/Site: Celadon
Glossary (Continued)
Abbreviation These commonly used abbreviations may or may not be present in this report.
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Job ID: 400-203460-1
Eurofins TestAmerica, Pensacola
Page 18 of 49 6/22/2021 (Rev. 1)

Surrogate Summary
Client: Shield Engineering Inc
Project/Site: Celadon
F
Job ID: 400-203460-1
Method: 8260D - Volatile Organic Compounds by GC/MS
Matrix: Water PreD TvDe: Total/NA
Lab Sample ID
400-203460-1
400-203460-1 MS
400-203460-1 MSD
400-203460-2
LCS 400-532736/1009
MB 400-532736/23
Surrogate Legend
Client Sample ID
W-1
W-1
W-1
EQ-1
Lab Control Sample
Method Blank
Percent Surrogate Recovery (Acceptance Limits)
BFB DBFM TOL DCA
(78-118) (81-121) (80-120) (67-134)
94
102
98
98
96
103
98
100
96
102
99
97
112
101
103
96
98
101
98
97
94
101
99
99
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
DCA= 1,2-Dichloroethane-d4 (Surr)
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Matrix: Water Prep Type: Total/NA
Lab Sample ID
400-203460-1
400-203460-2
400-203507-H-24-B MS
400-203507-H-24-C MSD
LCS 400-532580/2-A
MB 400-532580/1-A
Surrogate Legend
0
Percent Surrogate Recovery (Acceptance Limits)
TBP
FBP
2FP
NBZ
PHL
TPHL
Client Sample ID
(15-135)
(34-120)
(10-120)
(27-120)
(10-120)
(53-125)
W-1
121
61
22
46
54
41 S1-
EQ-1
0 S1-
11 S1-
3 S1-
1 S1-
8 S1-
13 S1-
Matrix Spike
89
81
45
97
78
100
Matrix Spike Duplicate
80
75
26
92
58
92
Lab Control Sample
97
89
43
108
82
112
Method Blank
59
86
35
89
73
114
TBP = 2,4,6-Tribromophenol (Surr)
FBP = 2-Fluorobiphenyl
2FP = 2-Fluorophenol (Surr)
NBZ = Nitrobenzene-d5 (Surr)
PHL = Phenol-d5 (Surr)
TPHL = Terphenyl-d14 (Surr)
Method: 8081 B - Organochlorine Pesticides (GC)
Matrix: Water Prep Type: Total/NA
Lab Sample ID
400-203460-1
400-203460-2
560-94533-E- 1 -A MS
560-94533-E-1-B MSD
MB 400-532015/1-A
Surrogate Legend
Client Sample ID
W-1
EQ-1
Matrix Spike
Matrix Spike Duplicate
Method Blank
DCBP = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Percent Surrogate Recovery (Acceptance Limits)
DCBP2 TCX2
(10-130) (43-130)
10
19 S1-
10
4 S1-
93
77
102
86
41
124
Eurofins TestAmerica, Pensacola
Page 19 of 49 6/22/2021 (Rev. 1)

Surrogate Summary
Client: Shield Engineering Inc
Project/Site: Celadon
Method: 8081 B - Organochlorine Pesticides (GC)
Matrix: Water
DCBP1
Lab Sample ID Client Sample ID (10-130)
LCS 400-532015/2-A Lab Control Sample 39
Surrogate Legend
DCBP = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8151A - Herbicides (GC)
Matrix: Water
DCPAA2
Lab Sample ID
Client Sample ID
(30-142)
400-203460-1
W-1
99
400-203460-2
EQ-1
98
LCS 400-532365/2-A
Lab Control Sample
87
LCSD 400-532365/3-A
Lab Control Sample Dup
89
MB 400-532365/1-A
Method Blank
85
Surrogate Legend
L DCPAA = DCAA
Job ID: 400-203460-1
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
TCX1
(43-130)
107
Pre
Percent Surrogate Recovery (Acceptance Limits)
Total/NA a
Eurofins TestAmerica, Pensacola
Page 20 of 49 6/22/2021 (Rev. 1)

QC Association Summary
Client: Shield Engineering Inc
Project/Site: Celadon
GC/MS VOA
Analysis Batch: 532736
Job ID: 400-203460-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
400-203460-1
W-1
Total/NA
Water
8260D
400-203460-2
EQ-1
Total/NA
Water
8260D
MB 400-532736/23
Method Blank
Total/NA
Water
8260D
LCS 400-532736/1009
Lab Control Sample
Total/NA
Water
8260D
400-203460-1 MS
W-1
Total/NA
Water
8260D
400-203460-1 MSD
W-1
Total/NA
Water
8260D
GC/MS Semi VOA
Prep Batch: 532580
Lab Sample ID
Client Sample ID
400-203460-1
W-1
400-203460-1 - DL
W-1
400-203460-2 - DL
EQ-1
400-203460-2
EQ-1
MB 400-532580/1-A
Method Blank
LCS 400-532580/2-A
Lab Control Sample
Analysis Batch: 532781
Lab Sample ID
Client Sample ID
400-203460-1
W-1
400-203460-2
EQ-1
Analysis Batch: 532788
Lab Sample ID
Client Sample ID
MB 400-532580/1-A
Method Blank
LCS 400-532580/2-A
Lab Control Sample
Analysis Batch: 536281
Prep Type
Matrix
Method
Total/NA
Water
3520C
Total/NA
Water
3520C
Total/NA
Water
3520C
Total/NA
Water
3520C
Total/NA
Water
3520C
Total/NA
Water
3520C
Prep Batch a
Prep Type
Matrix
Method
Prep Batch
Total/NA
Water
8270E
532580
Total/NA
Water
8270E
532580
Prep Type
Matrix
Method
Prep Batch
Total/NA
Water
8270E
532580
Total/NA
Water
8270E
532580
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203460-1 - DL
W-1
Total/NA
Water
8270E
532580
400-203460-2 - DL
EQ-1
Total/NA
Water
8270E
532580
GC Semi VOA
Prep Batch: 532015
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203460-1
W-1
Total/NA
Water
3520C
400-203460-2
EQ-1
Total/NA
Water
3520C
MB 400-532015/1-A
Method Blank
Total/NA
Water
3520C
LCS 400-532015/2-A
Lab Control Sample
Total/NA
Water
3520C
Analysis Batch: 532257
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203460-1
W-1
Total/NA
Water
8081 B
532015
400-203460-2
EQ-1
Total/NA
Water
8081 B
532015
M B 400-532015/1 -A
Method Blank
Total/NA
Water
8081B
532015
LCS 400-532015/2-A
Lab Control Sample
Total/NA
Water
8081 B
532015
Prep Batch: 532365
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203460-1
W-1
Total/NA
Water
8151A
Page 21 of 49
Eurofins TestAmerica, Pensacola
6/22/2021 (Rev. 1)

QC Association Summary
Client: Shield Engineering Inc
Project/Site: Celadon
GC Semi VOA (Continued)
Prep Batch: 532365 (Continued)
Lab Sample ID
Client Sample ID
400-203460-2
EQ-1
MB 400-532365/1-A
Method Blank
LCS 400-532365/2-A
Lab Control Sample
LCSD 400-532365/3-A
Lab Control Sample Dup
Analysis Batch: 532597
Lab Sample ID
Client Sample ID
400-203460-1
W-1
400-203460-2
EQ-1
MB 400-532365/1-A
Method Blank
LCS 400-532365/2-A
Lab Control Sample
LCSD 400-532365/3-A
Lab Control Sample Dup
Metals
Prep Batch: 531709
Lab Sample ID
Client Sample ID
400-203460-1
W-1
400-203460-2
EQ-1
MB 400-531709/14-A
Method Blank
LCS 400-531709/15-A
Lab Control Sample
Prep Batch: 532043
Lab Sample ID
Client Sample ID
400-203460-1
W-1
400-203460-2
EQ-1
MB 400-532043/1-A
Method Blank
LCS 400-532043/2-A
Lab Control Sample
Analysis Batch: 532149
Lab Sample ID
Client Sample ID
400-203460-1
W-1
400-203460-2
EQ-1
MB 400-531709/14-A
Method Blank
LCS 400-531709/15-A
Lab Control Sample
Analysis Batch: 532226
Lab Sample ID
Client Sample ID
400-203460-1
W-1
400-203460-2
EQ-1
MB 400-532043/1-A
Method Blank
LCS 400-532043/2-A
Lab Control Sample
Analysis Batch: 532562
Lab Sample ID
Client Sample ID
400-203460-1
W-1
400-203460-2
EQ-1
Job ID: 400-203460-1
Prep Type
Matrix
Method
Total/NA
Water
8151A
Total/NA
Water
8151A
Total/NA
Water
8151A
Total/NA
Water
8151A
Prep Type
Matrix
Method
Total/NA
Water
8151A
Total/NA
Water
8151A
Total/NA
Water
8151A
Total/NA
Water
8151A
Total/NA
Water
8151A
Prep Batch
Prep Batch
532365
532365
532365
532365
532365
Prep Type
Matrix
Method
Prep Batch
Total/NA
Water
7470A
Total/NA
Water
7470A
Total/NA
Water
7470A
Total/NA
Water
7470A
Prep Type
Matrix
Method
Prep Batch
Total/NA
Water
3010A
Total/NA
Water
3010A
Total/NA
Water
3010A
Total/NA
Water
3010A
Prep Type
Matrix
Method
Prep Batch
Total/NA
Water
7470A
531709
Total/NA
Water
7470A
531709
Total/NA
Water
7470A
531709
Total/NA
Water
7470A
531709
Prep Type
Matrix
Method
Prep Batch
Total/NA
Water
6010D
532043
Total/NA
Water
6010D
532043
Total/NA
Water
6010D
532043
Total/NA
Water
6010D
532043
Prep Type
Matrix
Method
Prep Batch
Total/NA
Water
6010D
532043
Total/NA
Water
6010D
532043
Eurofins TestAmerica, Pensacola
Page 22 of 49 6/22/2021 (Rev. 1)

QC Association Summary
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
General Chemistry
Analysis Batch: 531930
Lab Sample ID Client Sample ID
Prep Type
Matrix
Method Prep Batch
400-203460-1 W-1
Total/NA
Water
SM 5210B
400-203460-2 EQ-1
Total/NA
Water
SM 5210B
USB 400-531930/1 Method Blank
Total/NA
Water
SM 5210B
LCS 400-531930/2 Lab Control Sample
Total/NA
Water
SM 5210B
Analysis Batch: 532002
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203460-1
W-1
Total/NA
Water
SM 5220D
400-203460-2
EQ-1
Total/NA
Water
SM 5220D
MB 400-532002/4
Method Blank
Total/NA
Water
SM 5220D
LCS 400-532002/5
Lab Control Sample
Total/NA
Water
SM 5220D
MRL 400-532002/2
Lab Control Sample
Total/NA
Water
SM 5220D
Analysis Batch: 532071
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203460-1
W-1
Total/NA
Water
SM 2540D
400-203460-2
EQ-1
Total/NA
Water
SM 2540D
MB 400-532071/1
Method Blank
Total/NA
Water
SM 2540D
LCS 400-532071/2
Lab Control Sample
Total/NA
Water
SM 2540D
Analysis Batch: 532313
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203460-1
W-1
Total/NA
Water
350.1
400-203460-2
EQ-1
Total/NA
Water
350.1
MB 400-532313/47
Method Blank
Total/NA
Water
350.1
LCS 400-532313/48
Lab Control Sample
Total/NA
Water
350.1
MRL 400-532313/13
Lab Control Sample
Total/NA
Water
350.1
Analysis Batch: 532550
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203460-1
W-1
Total/NA
Water
9040C
400-203460-2
EQ-1
Total/NA
Water
9040C
LCS 400-532550/1
Lab Control Sample
Total/NA
Water
9040C
Eurofins TestAmerica, Pensacola
Page 23 of 49 6/22/2021 (Rev. 1)

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Method: 8260D - Volatile Organic
Compounds by GUMS
Lab Sample ID: MB 400-532736/23
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532736
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
Acetone
ND
25.0
10.0
ug/L
05/21/21 12:21
1
Benzene
ND
1.00
0.380
ug/L
05/21/21 12:21
1
Bromobenzene
ND
1.00
0.540
ug/L
05/21/21 12:21
1
Chlorobromomethane
ND
1.00
0.520
ug/L
05/21/21 12:21
1
Dichlorobromomethane
ND
1.00
0.500
ug/L
05/21/21 12:21
1
Bromoform
ND
5.00
0.710
ug/L
05/21/21 12:21
1
Bromomethane
ND
1.00
0.980
ug/L
05/21/21 12:21
1
2-Butanone (MEK)
ND
25.0
2.60
ug/L
05/21/21 12:21
1
n-Butylbenzene
ND
1.00
0.760
ug/L
05/21/21 12:21
1
sec-Butylbenzene
ND
1.00
0.700
ug/L
05/21/21 12:21
1
tert-Butylbenzene
ND
1.00
0.630
ug/L
05/21/21 12:21
1
Carbon disulfide
ND
1.00
0.500
ug/L
05/21/21 12:21
1
Carbon tetrachloride
ND
1.00
0.500
ug/L
05/21/21 12:21
1
Chlorobenzene
ND
1.00
0.500
ug/L
05/21/21 12:21
1
Chloroethane
ND
1.00
0.760
ug/L
05/21/21 12:21
1
Chloroform
ND
1.00
0.600
ug/L
05/21/21 12:21
1
Chloromethane
ND
1.00
0.830
ug/L
05/21/21 12:21
1
3-Chloro-1-propene
ND
5.00
1.00
ug/L
05/21/21 12:21
1
2-Chlorotoluene
ND
1.00
0.570
ug/L
05/21/21 12:21
1
4-Chlorotoluene
ND
1.00
0.560
ug/L
05/21/21 12:21
1
Chlorodibromomethane
ND
1.00
0.500
ug/L
05/21/21 12:21
1
1,2-Dibromo-3-Chloropropane
ND
5.00
1.50
ug/L
05/21/21 12:21
1
Ethylene Dibromide
ND
1.00
0.500
ug/L
05/21/21 12:21
1
Dibromomethane
ND
5.00
0.590
ug/L
05/21/21 12:21
1
1,2-Dichlorobenzene
ND
1.00
0.500
ug/L
05/21/21 12:21
1
1,3-Dichlorobenzene
ND
1.00
0.540
ug/L
05/21/21 12:21
1
1,4-Dichlorobenzene
ND
1.00
0.640
ug/L
05/21/21 12:21
1
trans- 1,4-Dichloro-2-butene
ND
5.00
1.00
ug/L
05/21/21 12:21
1
Dichlorodifluoromethane
ND
1.00
0.850
ug/L
05/21/21 12:21
1
1,1-Dichloroethane
ND
1.00
0.500
ug/L
05/21/21 12:21
1
1,2-Dichloroethane
ND
1.00
0.500
ug/L
05/21/21 12:21
1
cis-1,2-Dichloroethene
ND
1.00
0.500
ug/L
05/21/21 12:21
1
trans- 1,2-Dichloroethene
ND
1.00
0.500
ug/L
05/21/21 12:21
1
1,2-Dichloroethene, Total
ND
10.0
0.640
ug/L
05/21/21 12:21
1
1,1-Dichloroethene
ND
1.00
0.500
ug/L
05/21/21 12:21
1
1,2-Dichloropropane
ND
1.00
0.500
ug/L
05/21/21 12:21
1
1,3-Dichloropropane
ND
1.00
0.500
ug/L
05/21/21 12:21
1
2,2-Dichloropropane
ND
1.00
0.500
ug/L
05/21/21 12:21
1
1,1-Dichloropropene
ND
1.00
0.500
ug/L
05/21/21 12:21
1
cis-1,3-Dichloropropene
ND
5.00
0.500
ug/L
05/21/21 12:21
1
trans- 1,3-Dichloropropene
ND
5.00
0.500
ug/L
05/21/21 12:21
1
Ethylbenzene
ND
1.00
0.500
ug/L
05/21/21 12:21
1
Ethyl methacrylate
ND
1.00
0.600
ug/L
05/21/21 12:21
1
Hexachlorobutadiene
ND
5.00
0.900
ug/L
05/21/21 12:21
1
2-Hexanone
ND
25.0
3.10
ug/L
05/21/21 12:21
1
lodomethane
ND
1.00
0.900
ug/L
05/21/21 12:21
1
Isobutyl alcohol
ND
25.0
10.0
ug/L
05/21/21 12:21
1
Isopropylbenzene
ND
1.00
0.530
ug/L
05/21/21 12:21
1
Eurofins TestAmerica, Pensacola
Page 24 of 49 6/22/2021 (Rev. 1)

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Method: 8260D - Volatile Organic
Compounds by GUMS (Continued)
Lab Sample ID: MB 400-532736/23
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532736
MB
MB
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
4-Isopropyltoluene
ND
1.00
0.710
ug/L
05/21/21 12:21
1
Methylene Chloride
ND
5.00
3.00
ug/L
05/21/21 12:21
1
4-Methyl-2-pentanone (MIBK)
ND
25.0
1.80
ug/L
05/21/21 12:21
1
Methyl tert-butyl ether
ND
1.00
0.740
ug/L
05/21/21 12:21
1
Naphthalene
ND
1.00
1.00
ug/L
05/21/21 12:21
1
N-Propylbenzene
ND
1.00
0.690
ug/L
05/21/21 12:21
1
Styrene
ND
1.00
1.00
ug/L
05/21/21 12:21
1
1,1,1,2-Tetrachloroethane
ND
1.00
0.520
ug/L
05/21/21 12:21
1
1,1,2,2-Tetrachloroethane
ND
1.00
0.500
ug/L
05/21/21 12:21
1
Tetrachloroethene
ND
1.00
0.580
ug/L
05/21/21 12:21
1
Toluene
ND
1.00
0.410
ug/L
05/21/21 12:21
1
1,2,3-Trichlorobenzene
ND
1.00
0.700
ug/L
05/21/21 12:21
1
1,2,4-Trichlorobenzene
ND
1.00
0.820
ug/L
05/21/21 12:21
1
1,1,1-Trichloroethane
ND
1.00
0.500
ug/L
05/21/21 12:21
1
1,1,2-Trichloroethane
ND
5.00
0.500
ug/L
05/21/21 12:21
1
Trichloroethene
ND
1.00
0.500
ug/L
05/21/21 12:21
1
Trichlorofluoromethane
ND
1.00
0.520
ug/L
05/21/21 12:21
1
1,2,3-Trichloropropane
ND
5.00
0.840
ug/L
05/21/21 12:21
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
1.00
0.500
ug/L
05/21/21 12:21
1
1,2,4-Trimethylbenzene
ND
1.00
0.820
ug/L
05/21/21 12:21
1
1,3,5-Trimethylbenzene
ND
1.00
0.560
ug/L
05/21/21 12:21
1
Vinyl acetate
ND
25.0
2.00
ug/L
05/21/21 12:21
1
Vinyl chloride
ND
1.00
0.500
ug/L
05/21/21 12:21
1
o-Xylene
ND
5.00
0.600
ug/L
05/21/21 12:21
1
m-Xylene & p-Xylene
ND
5.00
1.60
ug/L
05/21/21 12:21
1
Xylenes, Total
ND
10.0
1.60
ug/L
05/21/21 12:21
1
Cyclohexane
ND
1.00
0.500
ug/L
05/21/21 12:21
1
Methyl acetate
ND
5.00
2.50
ug/L
05/21/21 12:21
1
Methylcyclohexane
ND
1.00
0.500
ug/L
05/21/21 12:21
1
Tetrahydrofuran
ND
5.00
1.50
ug/L
05/21/21 12:21
1
Hexane
ND
1.00
0.960
ug/L
05/21/21 12:21
1
Ethyl ether
ND
1.00
0.600
ug/L
05/21/21 12:21
1
n-Heptane
ND
1.00
0.700
ug/L
05/21/21 12:21
1
1,3-Dichloropropene, Total
ND
5.00
0.500
ug/L
05/21/21 12:21
1
Butadiene
ND
1.00
0.500
ug/L
05/21/21 12:21
1
Dichlorofluoromethane
ND
1.00
0.500
ug/L
05/21/21 12:21
1
2-Methyl-2-propanol
ND
10.0
4.90
ug/L
05/21/21 12:21
1
1,4-Dioxane
ND
400
100
ug/L
05/21/21 12:21
1
MB
MB
Surrogate %Recovery
Qualifier
Limits
Prepared Analyzed
Dil Fac
4-Bromofluorobenzene
94
78 - 118
05121121 12:21
1
Dibromofluoromethane
101
81- 121
05121121 12:21
1
Toluene-d8 (Surr)
99
80 - 120
05121121 12:21
1
1,2-Dichloroethane-d4 (Surr)
99
67- 134
05121121 12:21
1
Eurofins TestAmerica, Pensacola
Page 25 of 49 6/22/2021 (Rev. 1)

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Lab Sample ID: LCS 400-532736/1009
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532736
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Acetone
200
181.0
ug/L
91
43-160
Benzene
50.0
49.43
ug/L
99
70 -130
Bromobenzene
50.0
54.82
ug/L
110
70 -132
Chlorobromomethane
50.0
51.60
ug/L
103
70 -130
Dichlorobromomethane
50.0
50.83
ug/L
102
67 -133
Bromoform
50.0
55.25
ug/L
110
57 -140
Bromomethane
25.0
30.23
ug/L
121
10 -160
2-Butanone (MEK)
200
188.2
ug/L
94
61 _ 145
n-Butylbenzene
50.0
62.23
ug/L
124
67.130
sec-Butylbenzene
50.0
57.86
ug/L
116
66 -130
tert-Butylbenzene
50.0
55.91
ug/L
112
64 -139
Carbon disulfide
50.0
50.46
ug/L
101
61 -137
Carbon tetrachloride
50.0
52.22
ug/L
104
61 -137
Chlorobenzene
50.0
51.86
ug/L
104
70 -130
Chloroethane
25.0
24.17
ug/L
97
55 -141
Chloroform
50.0
49.45
ug/L
99
69 -130
Chloromethane
25.0
23.71
ug/L
95
58 -137
3-Chloro-1-propene
50.0
48.76
ug/L
98
65 -130
2-Chlorotoluene
50.0
54.41
ug/L
109
70 -130
4-Chlorotoluene
50.0
55.34
ug/L
111
70 -130
Chlorodibromomethane
50.0
51.99
ug/L
104
67 -135
1,2-Dibromo-3-Chloropropane
50.0
49.07
ug/L
98
54.135
Ethylene Dibromide
50.0
51.88
ug/L
104
70 -130
Dibromomethane
50.0
50.08
ug/L
100
70 -130
1,2-Dichlorobenzene
50.0
55.10
ug/L
110
67 -130
1,3-Dichlorobenzene
50.0
56.71
ug/L
113
70 -130
1,4-Dichlorobenzene
50.0
55.95
ug/L
112
70 -130
trans- 1,4-Dichloro-2-butene
50.0
48.49
ug/L
97
57-140
Dichlorodifluoromethane
25.0
24.01
ug/L
96
41 -146
1,1-Dichloroethane
50.0
46.30
ug/L
93
70-130
1,2-Dichloroethane
50.0
47.30
ug/L
95
69 -130
cis-1,2-Dichloroethene
50.0
48.23
ug/L
96
68 -130
trans- 1,2-Dichloroethene
50.0
48.65
ug/L
97
70-130
1,2-Dichloroethene, Total
100
96.88
ug/L
97
70 -130
1,1-Dichloroethene
50.0
48.51
ug/L
97
63-134
1,2-Dichloropropane
50.0
47.83
ug/L
96
70 -130
1,3-Dichloropropane
50.0
49.11
ug/L
98
70 -130
2,2-Dichloropropane
50.0
48.97
ug/L
98
52.135
1,1-Dichloropropene
50.0
50.07
ug/L
100
70-130
cis-1,3-Dichloropropene
50.0
50.68
ug/L
101
69 -132
trans- 1,3-Dichloropropene
50.0
50.31
ug/L
101
63-130
Ethylbenzene
50.0
52.94
ug/L
106
70 -130
Ethyl methacrylate
50.0
48.97
ug/L
98
68 -130
Hexachlorobutadiene
50.0
71.84 "+
ug/L
144
53 -140
2-Hexanone
200
175.4
ug/L
88
65 -137
lodomethane
50.0
50.08
ug/L
100
27 -159
Isobutyl alcohol
1250
1091
ug/L
87
52 -148
Isopropylbenzene
50.0
55.31
ug/L
111
70 -130
Eurofins TestAmerica, Pensacola
Page 26 of 49 6/22/2021 (Rev. 1)

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Method: 8260D - Volatile Organic Compounds
by GUMS (Continued)
Lab Sample ID: LCS 400-532736/1009
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532736
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
4-Isopropyltoluene
50.0
59.32
ug/L
119
65 -130
Methylene Chloride
50.0
48.47
ug/L
97
66 -135
4-Methyl-2-pentanone (MIBK)
200
171.8
ug/L
86
69-138
Methyl tert-butyl ether
50.0
47.78
ug/L
96
66 -130
Naphthalene
50.0
52.11
ug/L
104
47 -149
N-Propylbenzene
50.0
58.38
ug/L
117
70-130
Styrene
50.0
55.49
ug/L
111
70 -130
1,1,1,2-Tetrachloroethane
50.0
52.57
ug/L
105
67-131
1,1,2,2-Tetrachloroethane
50.0
49.47
ug/L
99
70-131
Tetrachloroethene
50.0
52.00
ug/L
104
65 -130
m
Toluene
50.0
49.99
ug/L
100
70 -130
1,2,3-Trichlorobenzene
50.0
57.03
ug/L
114
60-138
1,2,4-Trichlorobenzene
50.0
58.50
ug/L
117
60 -140
1,1,1-Trichloroethane
50.0
50.56
ug/L
101
68-130
1,1,2-Trichloroethane
50.0
48.32
ug/L
97
70-130
Trichloroethene
50.0
52.09
ug/L
104
70 -130
Trichlorofluoromethane
25.0
24.00
ug/L
96
65 -138
1,2,3-Trichloropropane
50.0
52.00
ug/L
104
70-130
1,1,2-Trichloro-1,2,2-trifluoroetha
50.0
48.36
ug/L
97
60-139
ne
1,2,4-Trimethylbenzene
50.0
57.08
ug/L
114
70 -130
1,3,5-Trimethylbenzene
50.0
56.57
ug/L
113
69-130
Vinyl acetate
50.0
52.44
ug/L
105
26 -160
Vinyl chloride
25.0
23.42
ug/L
94
59 -136
o-Xylene
50.0
53.46
ug/L
107
70 -130
m-Xylene & p-Xylene
50.0
54.23
ug/L
108
70 -130
Xylenes, Total
100
107.7
ug/L
108
70 -130
Cyclohexane
50.0
49.41
ug/L
99
70 -130
Methyl acetate
100
87.03
ug/L
87
45 -159
Methylcyclohexane
50.0
49.92
ug/L
100
70 -130
Tetrahydrofuran
100
88.83
ug/L
89
59 -145
Hexane
50.0
45.74
ug/L
91
69 -130
Ethyl ether
50.0
45.58
ug/L
91
64 -131
n-Heptane
50.0
46.21
ug/L
92
70 -130
1,3-Dichloropropene, Total
100
101.0
ug/L
101
70 -130
Butadiene
25.0
24.00
ug/L
96
60 -134
Dichlorofluoromethane
25.0
24.45
ug/L
98
62 -136
2-Methyl-2-propanol
500
444.1
ug/L
89
46 -143
1,4-Dioxane
1000
1011
ug/L
101
50-160
LCS LCS
Surrogate %Recovery Qualifier
Limits
4-Bromofluorobenzene 98
78 - 118
Dibromofluoromethane 101
81 - 121
Toluene-d8 (Surr) 98
80 - 120
1,2-Dichloroethane-d4 (Surr) 97
67- 134
Eurofins TestAmerica, Pensacola
Page 27 of 49 6/22/2021 (Rev. 1)

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Method: 8260D - Volatile
Organic Compounds
by GUMS (Continued)
Lab Sample ID: 400-203460-1 MS
Client Sample ID: W-1
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532736
Sample Sample
Spike
MS MS
%Rec.
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
Acetone
203
200
396.2
ug/L
97
43 -150
Benzene
ND
50.0
51.26
ug/L
103
56 -142
Bromobenzene
ND
50.0
54.24
ug/L
108
59 -136
Chlorobromomethane
ND
50.0
53.03
ug/L
106
64 -140
Dichlorobromomethane
ND
50.0
52.15
ug/L
104
59 -143
Bromoform
ND
50.0
55.69
ug/L
111
50 -140
Bromomethane
ND
50.0
48.97
ug/L
98
10 -150
2-Butanone (MEK)
9.74 J
200
208.0
ug/L
99
55 -150
n-Butylbenzene
ND
50.0
62.09
ug/L
124
41 -142
sec-Butylbenzene
ND
50.0
59.84
ug/L
120
50 -138
tert-Butylbenzene
ND
50.0
57.05
ug/L
114
54 -146
Carbon disulfide
15.1
50.0
67.83
ug/L
106
48 -150
Carbon tetrachloride
ND
50.0
53.68
ug/L
107
55 -145
Chlorobenzene
ND
50.0
53.87
ug/L
108
64 -130
Chloroethane
ND
50.0
52.30
ug/L
105
50 -150
Chloroform
ND
50.0
50.81
ug/L
102
60 -141
Chloromethane
ND
50.0
46.47
ug/L
93
49 -148
3-Chloro-1-propene
ND
50.0
50.21
ug/L
100
54 -144
2-Chlorotoluene
ND
50.0
55.80
ug/L
112
53 -134
4-Chlorotoluene
ND
50.0
56.10
ug/L
112
54 -133
Chlorodibromomethane
ND
50.0
54.14
ug/L
108
56 -143
1,2-Dibromo-3-Chloropropane
ND
50.0
54.60
ug/L
109
45-135
Ethylene Dibromide
ND
50.0
53.81
ug/L
108
64.132
Dibromomethane
ND
50.0
52.55
ug/L
105
63 -138
1,2-Dichlorobenzene
ND
50.0
56.51
ug/L
113
52 -137
1,3-Dichlorobenzene
ND
50.0
57.73
ug/L
115
54 -135
1,4-Dichlorobenzene
ND
50.0
56.65
ug/L
113
53-135
trans- 1,4-Dichloro-2-butene
ND
50.0
49.41
ug/L
99
43-147
Dichlorodifluoromethane
ND
50.0
48.21
ug/L
96
16-150
1,1-Dichloroethane
ND
50.0
48.35
ug/L
97
61-144
1,2-Dichloroethane
ND
50.0
49.94
ug/L
100
60-141
cis-1,2-Dichloroethene
ND
50.0
48.83
ug/L
98
59-143
trans- 1,2-Dichloroethene
ND
50.0
51.03
ug/L
102
61-143
1,2-Dichloroethene, Total
ND
100
99.87
ug/L
100
10-150
1,1-Dichloroethene
ND
50.0
50.49
ug/L
101
54-147
1,2-Dichloropropane
ND
50.0
48.93
ug/L
98
66-137
1,3-Dichloropropane
ND
50.0
50.36
ug/L
101
66-133
2,2-Dichloropropane
ND
50.0
49.57
ug/L
99
42.144
1,1-Dichloropropene
ND
50.0
52.24
ug/L
104
65-136
cis-1,3-Dichloropropene
ND
50.0
51.83
ug/L
104
57-140
trans- 1,3-Dichloropropene
ND
50.0
51.84
ug/L
104
53-133
Ethylbenzene
ND
50.0
54.99
ug/L
110
58 -131
Ethyl methacrylate
ND
50.0
50.59
ug/L
101
64 -130
Hexachlorobutadiene
ND "+
50.0
73.27
ug/L
147
31 -149
2-Hexanone
ND
200
184.5
ug/L
92
65 -140
lodomethane
ND
50.0
54.77
ug/L
110
20 -150
Isobutyl alcohol
ND
1250
1169
ug/L
94
41 -150
Isopropylbenzene
ND
50.0
57.83
ug/L
116
56 -133
Eurofins TestAmerica, Pensacola
Page 28 of 49 6/22/2021 (Rev. 1)

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Method: 8260D - Volatile Organic Compounds
by GUMS (Continued)
Lab Sample ID: 400-203460-1
MS
Client Sample ID: W-1
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532736
Sample
Sample
Spike
MS MS
%Rec.
Analyte
Result
Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
4-Isopropyltoluene
ND
50.0
61.30
ug/L
123
48-139
Methylene Chloride
ND
50.0
49.45
ug/L
99
60 -146
4-Methyl-2-pentanone (MIBK)
ND
200
185.1
ug/L
93
63-146
Methyl tert-butyl ether
ND
50.0
49.62
ug/L
99
59 -137
Naphthalene
ND
50.0
55.73
ug/L
111
25 -150
N-Propylbenzene
ND
50.0
59.09
ug/L
118
51 -138
Styrene
ND
50.0
56.78
ug/L
114
58 -131
1,1,1,2-Tetrachloroethane
ND
50.0
55.21
ug/L
110
59-137
1,1,2,2-Tetrachloroethane
ND
50.0
50.34
ug/L
101
66-135
Tetrachloroethene
ND
50.0
51.71
ug/L
103
52 -133
Toluene
3.71
50.0
55.60
ug/L
104
65 -130
1,2,3-Trichlorobenzene
ND
50.0
58.61
ug/L
117
43-145
1,2,4-Trichlorobenzene
ND
50.0
59.65
ug/L
119
39-148
1,1,1-Trichloroethane
ND
50.0
52.38
ug/L
105
57-142
1,1,2-Trichloroethane
ND
50.0
49.91
ug/L
100
66-131
Trichloroethene
ND
50.0
54.01
ug/L
108
64 -136
Trichlorofluoromethane
ND
50.0
53.33
ug/L
107
54 -150
1,2,3-Trichloropropane
ND
50.0
52.03
ug/L
104
65-133
1,1,2-Trichloro-1,2,2-trifluoroetha
ND
50.0
50.91
ug/L
102
55-150
ne
1,2,4-Trimethylbenzene
ND
50.0
57.38
ug/L
115
50-139
1,3,5-Trimethylbenzene
ND
50.0
57.07
ug/L
114
52 -135
Vinyl acetate
ND
100
108.0
ug/L
108
26 -150
Vinyl chloride
ND
50.0
46.74
ug/L
93
46 -150
o-Xylene
ND
50.0
55.44
ug/L
111
61 -130
m-Xylene & p-Xylene
ND
50.0
56.08
ug/L
112
57 -130
Xylenes, Total
ND
100
111.5
ug/L
112
59 -130
Cyclohexane
ND
50.0
51.32
ug/L
103
58 -141
Methyl acetate
ND
100
105.2
ug/L
105
21 -150
Methylcyclohexane
ND
50.0
51.46
ug/L
103
62 -141
Tetrahydrofuran
ND
100
89.90
ug/L
90
56-145
Hexane
ND
50.0
47.38
ug/L
95
60 -142
Ethyl ether
ND
50.0
47.19
ug/L
94
54 -143
n-Heptane
ND
50.0
46.70
ug/L
93
64 -142
1,3-Dichloropropene,Total
ND
100
103.7
ug/L
104
50-150
Butadiene
ND
50.0
47.21
ug/L
94
50 -148
Dichlorofluoromethane
ND
50.0
52.82
ug/L
106
53-150
2-Methyl-2-propanol
90.1
500
684.2
ug/L
119
31 -150
1,4-Dioxane
ND
1000
1098
ug/L
110
10-150
MS
MS
Surrogate
%Recovery
Qualifier
Limits
4-Bromofluorobenzene
96
78 - 118
Dibromofluoromethane
103
81 - 121
Toluene-d8 (Surr)
98
80 - 120
1,2-Dichloroethane-d4 (Surr)
100
67- 134
Eurofins TestAmerica, Pensacola
Page 29 of 49 6/22/2021 (Rev. 1)

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Method: 8260D - Volatile
Organic Compounds
by GUMS (Continued)
Lab Sample ID: 400-203460-1 MSD
Client Sample ID:
W-1
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532736
Sample Sample
Spike
MSD MSD
%Rec.
RPD
Analyte
Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
Acetone
203
200
389.7
ug/L
93
43-150
2
30
Benzene
ND
50.0
50.94
ug/L
102
56 -142
1
30
Bromobenzene
ND
50.0
53.63
ug/L
107
59 -136
1
30
Chlorobromomethane
ND
50.0
52.71
ug/L
105
64 -140
1
30
Dichlorobromomethane
ND
50.0
51.44
ug/L
103
59 -143
1
30
Bromoform
ND
50.0
54.20
ug/L
108
50 -140
3
30
Bromomethane
ND
50.0
49.86
ug/L
100
10 -150
2
50
2-Butanone (MEK)
9.74 J
200
207.7
ug/L
99
55 -150
0
30
n-Butylbenzene
ND
50.0
59.63
ug/L
119
41 -142
4
31
sec-Butylbenzene
ND
50.0
57.41
ug/L
115
50 -138
4
30
tert-Butylbenzene
ND
50.0
54.41
ug/L
109
54 -146
5
30
Carbon disulfide
15.1
50.0
67.05
ug/L
104
48 -150
1
30
Carbon tetrachloride
ND
50.0
53.29
ug/L
107
55 -145
1
30
Chlorobenzene
ND
50.0
52.50
ug/L
105
64 -130
3
30
Chloroethane
ND
50.0
49.13
ug/L
98
50 -150
6
30
Chloroform
ND
50.0
50.47
ug/L
101
60 -141
1
30
Chloromethane
ND
50.0
46.24
ug/L
92
49 -148
0
31
3-Chloro-1-propene
ND
50.0
51.90
ug/L
104
54 -144
3
30
2-Chlorotoluene
ND
50.0
53.52
ug/L
107
53 -134
4
30
4-Chlorotoluene
ND
50.0
53.61
ug/L
107
54 -133
5
30
Chlorodibromomethane
ND
50.0
52.82
ug/L
106
56 -143
2
30
1,2-Dibromo-3-Chloropropane
ND
50.0
51.92
ug/L
104
45-135
5
30
Ethylene Dibromide
ND
50.0
53.17
ug/L
106
64.132
1
30
Dibromomethane
ND
50.0
52.42
ug/L
105
63 -138
0
30
1,2-Dichlorobenzene
ND
50.0
53.83
ug/L
108
52 -137
5
30
1,3-Dichlorobenzene
ND
50.0
54.96
ug/L
110
54 -135
5
30
1,4-Dichlorobenzene
ND
50.0
54.77
ug/L
110
53-135
3
30
trans- 1,4-Dichloro-2-butene
ND
50.0
48.42
ug/L
97
43-147
2
36
Dichlorodifluoromethane
ND
50.0
47.27
ug/L
95
16-150
2
31
1,1-Dichloroethane
ND
50.0
47.92
ug/L
96
61-144
1
30
1,2-Dichloroethane
ND
50.0
49.33
ug/L
99
60-141
1
30
cis-1,2-Dichloroethene
ND
50.0
48.89
ug/L
98
59-143
0
30
trans- 1,2-Dichloroethene
ND
50.0
50.87
ug/L
102
61-143
0
30
1,2-Dichloroethene, Total
ND
100
99.76
ug/L
100
10-150
0
30
1,1-Dichloroethene
ND
50.0
50.95
ug/L
102
54-147
1
30
1,2-Dichloropropane
ND
50.0
48.84
ug/L
98
66-137
0
30
1,3-Dichloropropane
ND
50.0
49.87
ug/L
100
66-133
1
30
2,2-Dichloropropane
ND
50.0
49.31
ug/L
99
42.144
1
31
1,1-Dichloropropene
ND
50.0
51.32
ug/L
103
65-136
2
30
cis-1,3-Dichloropropene
ND
50.0
52.35
ug/L
105
57-140
1
30
trans- 1,3-Dichloropropene
ND
50.0
50.32
ug/L
101
53-133
3
30
Ethylbenzene
ND
50.0
53.75
ug/L
108
58 -131
2
30
Ethyl methacrylate
ND
50.0
49.95
ug/L
100
64 -130
1
30
Hexachlorobutadiene
ND "+
50.0
69.98
ug/L
140
31 -149
5
36
2-Hexanone
ND
200
185.6
ug/L
93
65 -140
1
30
lodomethane
ND
50.0
51.77
ug/L
104
20 -150
6
44
Isobutyl alcohol
ND
1250
1205
ug/L
96
41 -150
3
40
Isopropylbenzene
ND
50.0
55.45
ug/L
111
56 -133
4
30
Eurofins TestAmerica, Pensacola
Page 30 of 49 6/22/2021 (Rev. 1)

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Method: 8260D - Volatile Organic Compounds
by GUMS (Continued)
Lab Sample ID: 400-203460-1
MSD
Client Sample ID:
W-1
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532736
Sample
Sample
Spike
MSD MSD
%Rec.
RPD
Analyte
Result
Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits
RPD
Limit
4-Isopropyltoluene
ND
50.0
59.11
ug/L
118
48-139
4
30
Methylene Chloride
ND
50.0
49.91
ug/L
100
60 -146
1
32
4-Methyl-2-pentanone (MIBK)
ND
200
187.5
ug/L
94
63-146
1
30
Methyl tert-butyl ether
ND
50.0
49.37
ug/L
99
59 -137
1
30
Naphthalene
ND
50.0
53.26
ug/L
107
25 -150
5
30
N-Propylbenzene
ND
50.0
56.27
ug/L
113
51 -138
5
30
Styrene
ND
50.0
54.79
ug/L
110
58 -131
4
30
1,1,1,2-Tetrachloroethane
ND
50.0
53.55
ug/L
107
59-137
3
30
1,1,2,2-Tetrachloroethane
ND
50.0
50.19
ug/L
100
66-135
0
30
Tetrachloroethene
ND
50.0
49.93
ug/L
100
52 -133
4
30
Toluene
3.71
50.0
54.09
ug/L
101
65 -130
3
30
1,2,3-Trichlorobenzene
ND
50.0
55.74
ug/L
ill
43-145
5
30
1,2,4-Trichlorobenzene
ND
50.0
55.61
ug/L
111
39-148
7
30
1,1,1-Trichloroethane
ND
50.0
52.17
ug/L
104
57-142
0
30
1,1,2-Trichloroethane
ND
50.0
50.20
ug/L
100
66-131
1
30
Trichloroethene
ND
50.0
52.97
ug/L
106
64 -136
2
30
Trichlorofluoromethane
ND
50.0
50.59
ug/L
101
54 -150
5
30
1,2,3-Trichloropropane
ND
50.0
52.83
ug/L
106
65-133
2
30
1,1,2-Trichloro-1,2,2-trifluoroetha
ND
50.0
50.56
ug/L
101
55-150
1
30
ne
1,2,4-Trimethylbenzene
ND
50.0
54.66
ug/L
109
50-139
5
30
1,3,5-Trimethylbenzene
ND
50.0
54.37
ug/L
109
52 -135
5
30
Vinyl acetate
ND
100
101.1
ug/L
101
26 -150
7
33
Vinyl chloride
ND
50.0
46.68
ug/L
93
46 -150
0
30
o-Xylene
ND
50.0
53.41
ug/L
107
61 -130
4
30
m-Xylene & p-Xylene
ND
50.0
54.15
ug/L
108
57 -130
3
30
Xylenes, Total
ND
100
107.6
ug/L
108
59 -130
4
30
Cyclohexane
ND
50.0
51.02
ug/L
102
58 -141
1
30
Methyl acetate
ND
100
106.3
ug/L
106
21 -150
1
30
Methylcyclohexane
ND
50.0
51.20
ug/L
102
62 -141
1
30
Tetrahydrofuran
ND
100
95.13
ug/L
95
56-145
6
34
Hexane
ND
50.0
47.36
ug/L
95
60 -142
0
30
Ethyl ether
ND
50.0
48.57
ug/L
97
54 -143
3
31
n-Heptane
ND
50.0
46.23
ug/L
92
64 -142
1
30
1,3-Dichloropropene,Total
ND
100
102.7
ug/L
103
50-150
1
30
Butadiene
ND
50.0
47.34
ug/L
95
50 -148
0
30
Dichlorofluoromethane
ND
50.0
49.96
ug/L
100
53-150
6
30
2-Methyl-2-propanol
90.1
500
702.7
ug/L
123
31 -150
3
42
1,4-Dioxane
ND
1000
1082
ug/L
108
10-150
2
50
MSD
MSD
Surrogate
%Recovery
Qualifier
Limits
4-Bromofluorobenzene
96
78 - 118
Dibromofluoromethane
102
81 - 121
Toluene-d8 (Surr)
99
80 - 120
1,2-Dichloroethane-d4 (Surr)
97
67- 134
Eurofins TestAmerica, Pensacola
Page 31 of 49 6/22/2021 (Rev. 1)

QC Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Lab Sample ID: MB 400-532580/1-A
Matrix: Water
Analysis Batch: 532788
Analyte
Atrazine
4-Chloro-3-methylphenol
2-Chlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Dinitro-2-methyl phenol
2,4-Dinitrophenol
2-Methylphenol
3 & 4 Methylphenol
2-Nitrophenol
4-Nitrophenol
Pentachlorophenol
Phenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Acenaphthene
Acenaphthylene
Acetophenone
Anthracene
Benzaldehyde
Benzo[a]anthracene
Benzo[a]pyrene
Benzo[b]fluoranthene
Benzo[k]fluoranthene
4-Bromophenyl phenyl ether
Butyl benzyl phthalate
Caprolactam
Carbazole
4-Chloroaniline
Bis(2-chloroethoxy)methane
Bis(2-chloroethyl)ether
2-Chloronaphthalene
4-Chlorophenyl phenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
Di-n-butyl phthalate
Di-n-octyl phthalate
3,3'-Dichlorobenzidine
Diethyl phthalate
Dimethyl phthalate
2,4-Dinitrotoluene
2,6-Dinitrotoluene
1,1'-Biphenyl
Bis(2-ethylhexyl) phthalate
Fluoranthene
Fluorene
Hexachlorobenzene
MB MB
Result Qualifier
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Job ID: 400-203460-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch:532580
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
10.0
0.450
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
3.80
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
2.20
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
3.00
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
3.50
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
2.00
ug/L
05/20/2109:44
05/21/2117:31
1
30.0
3.40
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
1.80
ug/L
05/20/2109:44
05/21/2117:31
1
20.0
1.04
ug/L
05/20/2109:44
05/21/2117:31
1
m
10.0
0.650
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
2.10
ug/L
05/20/2109:44
05/21/2117:31
1
20.0
1.81
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
2.60
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
3.70
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
3.50
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.460
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.560
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.620
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.420
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
1.30
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.340
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.430
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.380
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.540
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.320
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.690
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
3.80
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.870
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
3.40
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.690
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.740
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.520
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
2.00
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.490
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
1.17
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.520
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
2.70
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.440
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
2.60
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.700
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.600
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
1.90
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
1.90
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.400
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
5.00
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.770
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.560
ug/L
05/20/2109:44
05/21/2117:31
1
10.0
0.250
ug/L
05/20/2109:44
05/21/2117:31
1
Eurofins TestAmerica, Pensacola
Page 32 of 49 6/22/2021 (Rev. 1)

QC Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: MB 400-532580/1-A
Matrix: Water
Analysis Batch: 532788
Analyte
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno[1,2,3-cd]pyrene
Isophorone
Naphthalene
2-Methyl naphtha lene
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
n-Nitrosodiphenylamine(as
diphenylamine)
N-N itrosod i-n-propylamine
Phenanthrene
Pyrene
2,2'-oxybis(1-chloropropane)
2-Nitroaniline
Benzo[g,h,i]perylene
Benzoic acid
Surrogate
2,4,6-Tribromophenol (Surr)
2-Fluorobiphenyl
2-Fluorophenol (Surr)
Nitrobenzene-d5 (Surr)
Phenol-d5 (Surr)
Terphenyl-d14 (Surr)
Job ID: 400-203460-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch:532580
MB MB
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
ND
10.0
3.60
ug/L
05/20/2109:44
05/21/2117:31 1
ND
20.0
2.60
ug/L
05/20/2109:44
05/21/2117:31 1
ND
10.0
4.20
ug/L
05/20/2109:44
05/21/2117:31 1
ND
10.0
1.02
ug/L
05/20/2109:44
05/21/2117:31 1
ND
10.0
0.570
ug/L
05/20/2109:44
05/21/2117:31 1
ND
10.0
0.630
ug/L
05/20/2109:44
05/21/2117:31 1
ND
10.0
0.540
ug/L
05/20/2109:44
05/21/2117:31 1
ND
10.0
1.80
ug/L
05/20/2109:44
05/21/2117:31 1
ND
10.0
2.48
ug/L
05/20/2109:44
05/21/2117:31 1
ND
10.0
0.550
ug/L
05/20/2109:44
05/21/2117:31 1
m
ND
10.0
0.470
ug/L
05/20/2109:44
05/21/2117:31 1
ND
10.0
3.30
ug/L
05/20/2109:44
05/21/2117:31 1
ND
10.0
0.410
ug/L
05/20/2109:44
05/21/2117:31 1
ND
10.0
1.09
ug/L
05/20/2109:44
05/21/2117:31 1
ND
10.0
0.810
ug/L
05/20/2109:44
05/21/2117:31 1
ND
10.0
2.20
ug/L
05/20/2109:44
05/21/2117:31 1
ND
10.0
1.06
ug/L
05/20/2109:44
05/21/2117:31 1
ND
30.0
7.30
ug/L
05/20/2109:44
05/21/2117:31 1
MB MB
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
59
15 - 135
05120121 09:44
05121121 17:31
1
86
34 - 120
05120121 09:44
05121121 17:31
1
35
10 - 120
05120121 09:44
05121121 17:31
1
89
27 - 120
05120121 09:44
05121121 17:31
1
73
10 - 120
05120121 09:44
05121121 17:31
1
114
53 - 125
05120121 09:44
05121121 17:31
1
Lab Sample ID: LCS 400-532580/2-A
Matrix: Water
Analysis Batch: 532788
Analyte
Spike
Added
LCS LCS
Result Qualifier
Client Sample ID
Unit D %Rec
4-Chloro-3-methylphenol
30.0
29.16
ug/L
97
2-Chlorophenol
30.0
23.21
ug/L
77
2,4-Dichlorophenol
30.0
27.94
ug/L
93
2,4-Dimethylphenol
30.0
25.18
ug/L
84
4,6-Dinitro-2-methylphenol
60.0
65.40
ug/L
109
2,4-Dinitrophenol
60.0
63.34
ug/L
106
2-Methylphenol
30.0
29.03
ug/L
97
3 & 4 Methylphenol
30.0
28.22
ug/L
94
2-Nitrophenol
30.0
24.38
ug/L
81
4-Nitrophenol
60.0
51.43
ug/L
86
Pentachlorophenol
60.0
52.01
ug/L
87
Phenol
30.0
22.52
ug/L
75
2,4,5-Trichlorophenol
30.0
25.60
ug/L
85
2,4,6-Trichlorophenol
30.0
25.84
ug/L
86
Acenaphthene
30.0
25.40
ug/L
85
Acenaphthylene
30.0
29.15
ug/L
97
Lab Control Sample
Prep Type: Total/NA
Prep Batch: 532580
%Rec.
Limits
39-140
34-120
39-128
44-120
10-150
10-150
39-123
38-121
28-136
10-150
15-141
33-120
38-147
36-139
54-126
45-132
Eurofins TestAmerica, Pensacola
Page 33 of 49 6/22/2021 (Rev. 1)

QC Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
Job ID: 400-203460-1
Method: 8270E - Semivolatile Organic Compounds (GUMS) (Continued)
Lab Sample ID: LCS 400-532580/2-A
Client
Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532788
Prep Batch: 532580
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Anthracene
30.0
29.54
ug/L
98
63 -120
Benzo[a]anthracene
30.0
30.37
ug/L
101
60 -120
Benzo[a]pyrene
30.0
27.09
ug/L
90
56 -126
Benzo[b]fluoranthene
30.0
28.52
ug/L
95
35 -150
Benzo[k]fluoranthene
30.0
29.37
ug/L
98
53 -132
4-Bromophenyl phenyl ether
30.0
30.74
ug/L
102
55 -122
Butyl benzyl phthalate
30.0
33.00
ug/L
110
46 -145
Carbazole
30.0
41.52
ug/L
138
57 -143
4-Chloroaniline
30.0
22.74
ug/L
76
30 -120
Bis(2-chloroethoxy)methane
30.0
27.48
ug/L
92
45 -120
Bis(2-chloroethyl)ether
30.0
25.43
ug/L
85
48 -120
2-Chloronaphthalene
30.0
26.53
ug/L
88
52 -120
4-Chlorophenyl phenyl ether
30.0
27.30
ug/L
91
58 -124
Chrysene
30.0
30.24
ug/L
101
61 -123
Dibenz(a,h)anthracene
30.0
28.33
ug/L
94
44 -150
Dibenzofuran
30.0
26.72
ug/L
89
58 -123
Di-n-butyl phthalate
30.0
31.43
ug/L
105
55 -131
Di-n-octyl phthalate
30.0
34.21
ug/L
114
50 -150
Diethyl phthalate
30.0
29.33
ug/L
98
44 -146
Dimethyl phthalate
30.0
27.58
ug/L
92
50 -131
2,4-Dinitrotoluene
30.0
26.68
ug/L
89
58-140
2,6-Dinitrotoluene
30.0
26.24
ug/L
87
57-130
Bis(2-ethylhexyl) phthalate
30.0
34.42
ug/L
115
48 -150
Fluoranthene
30.0
28.48
ug/L
95
58 -129
Fluorene
30.0
28.36
ug/L
95
54 -125
Hexachlorobenzene
30.0
32.07
ug/L
107
52 -131
Hexachlorobutadiene
30.0
26.80
ug/L
89
20 -120
Hexachlorocyclopentadiene
30.0
7.265 J
ug/L
24
10 -129
Hexachloroethane
30.0
27.13
ug/L
90
20 -120
Indeno[1,2,3-cd]pyrene
30.0
28.10
ug/L
94
44 -150
Isophorone
30.0
28.76
ug/L
96
49 -120
Naphthalene
30.0
27.74
ug/L
92
50 -120
2-Methylnaphthalene
30.0
28.52
ug/L
95
55 -120
3-Nitroaniline
30.0
28.28
ug/L
94
34.132
4-Nitroaniline
30.0
24.52
ug/L
82
41 _135
Nitrobenzene
30.0
28.14
ug/L
94
47 -120
n-Nitrosodiphenylamine(as
29.8
29.94
ug/L
101
56 -120
diphenylamine)
N-Nitrosodi-n-propylamine
30.0
29.40
ug/L
98
44 -120
Phenanthrene
30.0
28.73
ug/L
96
63 -120
Pyrene
30.0
31.44
ug/L
105
49 -135
2,2'-oxybis(1-chloropropane)
30.0
27.04
ug/L
90
30-125
2-Nitroaniline
30.0
27.95
ug/L
93
47 -150
Benzo[g,h,i]perylene
30.0
32.45
ug/L
108
40-150
Benzoic acid
125
111.1
ug/L
89
10 -150
LCS LCS
Surrogate %Recovery Qualifier
Limits
2,4,6-Tribromophenol (Surr) 97
15- 135
Eurofins TestAmerica, Pensacola
Page 34 of 49 6/22/2021 (Rev. 1)

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 400-532580/2-A
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532788
Prep Batch: 532580
LCS
LCS
Surrogate %Recovery
Qualifier
Limits
2-Fluorobiphenyl 89
34 - 120
2-Fluorophenol (Surr) 43
10 - 120
Nitrobenzene-d5 (Surr) 108
27- 120
Phenol-d5 (Surr) 82
10 - 120
Terphenyl-d 14 (Surr) 112
53 - 125
Method: 8081 B - Organochlorine Pesticides (GC)
Lab Sample ID: MB 400-532015/1-A
Client Sample ID: Method Blank ■I■I�
Matrix: Water
Prep Type: Total/NA 1
Analysis Batch: 532257
Prep Batch: 532015
MB MB
Analyte Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed Dil Fac
Aldrin
ND
0.0200
0.00120
ug/L
05/17/21 09:06
05/18/21 14:57 1
alpha-BHC
ND
0.0200
0.00144
ug/L
05/17/21 09:06
05/18/21 14:57 1
beta-BHC
ND
0.0200
0.00120
ug/L
05/17/21 09:06
05/18/21 14:57 1
delta-BHC
ND
0.0200
0.000840
ug/L
05/17/21 09:06
05/18/21 14:57 1
gamma-BHC (Lindane)
ND
0.0500
0.0100
ug/L
05/17/21 09:06
05/18/21 14:57 1
cis -Chlordane
ND
0.0200
0.00168
ug/L
05/17/21 09:06
05/18/21 14:57 1
trans -Chlordane
ND
0.0200
0.00128
ug/L
05/17/21 09:06
05/18/21 14:57 1
4,4'-DDD
ND
0.0200
0.00120
ug/L
05/17/21 09:06
05/18/21 14:57 1
4,4'-DDE
ND
0.0200
0.000880
ug/L
05/17/21 09:06
05/18/21 14:57 1
4,4'-DDT
ND
0.0200
0.00156
ug/L
05/17/21 09:06
05/18/21 14:57 1
Dieldrin
ND
0.0200
0.00120
ug/L
05/17/21 09:06
05/18/21 14:57 1
Endosulfan I
ND
0.0200
0.00120
ug/L
05/17/21 09:06
05/18/21 14:57 1
Endosulfan II
ND
0.0200
0.00296
ug/L
05/17/21 09:06
05/18/21 14:57 1
Endosulfan sulfate
ND
0.0200
0.000840
ug/L
05/17/21 09:06
05/18/21 14:57 1
Endrin
ND
0.0200
0.00120
ug/L
05/17/21 09:06
05/18/21 14:57 1
Endrin aldehyde
ND
0.0200
0.00112
ug/L
05/17/21 09:06
05/18/21 14:57 1
Endrin ketone
ND
0.0200
0.00152
ug/L
05/17/21 09:06
05/18/21 14:57 1
Heptachlor
ND
0.0200
0.00124
ug/L
05/17/21 09:06
05/18/21 14:57 1
Heptachlor epoxide
ND
0.0200
0.00128
ug/L
05/17/21 09:06
05/18/21 14:57 1
Methoxychlor
ND
0.0200
0.00164
ug/L
05/17/21 09:06
05/18/21 14:57 1
Toxaphene
ND
3.00
0.120
ug/L
05/17/21 09:06
05/18/21 14:57 1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
DCB Decachlorobiphenyl
41
10 - 130
05117121 09:06
05118121 14:57 1
Tetrachloro-m-xylene
124
43 - 130
05117121 09:06
05118121 14:57 1
Lab Sample ID: LCS 400-532015/2-A
Client Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532257
Prep Batch: 532015
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Aldrin
0.500
0.4225
ug/L
84
52 -150
alpha-BHC
0.500
0.4214
ug/L
84
50 -150
beta-BHC
0.500
0.3922
ug/L
78
58 -150
delta-BHC
0.500
0.4139
ug/L
83
42 -150
Eurofins TestAmerica, Pensacola
Page 35 of 49 6/22/2021 (Rev. 1)

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Method: 8081 B - Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: LCS 400-532015/2-A
Client
Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532257
Prep Batch: 532015
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
gamma-BHC (Lindane)
0.500
0.3959
ug/L
79
53 -150
cis -Chlordane
0.500
0.4236
ug/L
85
63 -150
trans -Chlordane
0.500
0.3903
ug/L
78
62 -150
4,4'-DDD
0.500
0.3750
ug/L
75
58 -150
4,4'-DDE
0.500
0.4095
ug/L
82
65 -150
4,4'-DDT
0.500
0.4725
ug/L
94
59 -150
Dieldrin
0.500
0.4266
ug/L
85
64 -150
Endosulfan 1
0.500
0.4288
ug/L
86
40 -127
Endosulfan 11
0.500
0.4314
ug/L
86
40 -135
Endosulfan sulfate
0.500
0.4140
ug/L
83
50 -150
m
Endrin
0.500
0.4289
ug/L
86
63 -150
Endrin aldehyde
0.500
0.3877
ug/L
78
40 -150
Endrin ketone
0.500
0.4179
ug/L
84
52 -150
Heptachlor
0.500
0.3822
ug/L
76
59 -150
Heptachlor epoxide
0.500
0.4339
ug/L
87
63 -150
Methoxychlor
0.500
0.4977
ug/L
100
57 -150
LCS LCS
Surrogate %Recovery Qualifier
Limits
DCB Decachlorobiphenyl 39
10- 130
Tetrachloro-m-xylene 107
43 - 130
Method: 8151A - Herbicides (GC)
Lab Sample ID: MB 400-532365/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532597
Prep Batch: 532365
MB MB
Analyte Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
2,4,5-T ND
1.60
0.0160
ug/L
05/19/2108:17
05/20/2116:48 1
2,4-D ND
8.00
0.104
ug/L
05/19/2108:17
05/20/2116:48 1
2,4-DB ND
8.00
0.128
ug/L
05/19/2108:17
05/20/2116:48 1
Dalapon ND
48.0
0.776
ug/L
05/19/2108:17
05/20/2116:48 1
Dicamba ND
2.40
0.0272
ug/L
05/19/2108:17
05/20/2116:48 1
Dichlorprop ND
5.60
0.0960
ug/L
05/19/2108:17
05/20/2116:48 1
Dinoseb ND
0.800
0.0656
ug/L
05/19/2108:17
05/20/2116:48 1
MCPA ND
1600
16.0
ug/L
05/19/2108:17
05/20/2116:48 1
Silvex (2,4,5-TP) ND
1.60
0.00728
ug/L
05/19/21 08:17
05/20/21 16:48 1
Mecoprop ND
1600
16.0
ug/L
05/19/2108:17
05/20/2116:48 1
MB MB
Surrogate %Recovery Qualifier
DCAA 85
Lab Sample ID: LCS 400-532365/2-A
Matrix: Water
Analysis Batch: 532597
Analyte
2,4,5-T
Limits
30-142
Prepared Analyzed Dil Fac
0511912108:17 0512012116:48 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 532365
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
10.0 7.774 ug/L 78 30 -124
Page 36 of 49
Eurofins TestAmerica, Pensacola
6/22/2021 (Rev. 1)

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Method: 8151A - Herbicides (GC) (Continued)
Lab Sample ID: LCS 400-532365/2-A
Client
Sample ID:
Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532597
Prep Batch: 532365
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
2,4-D
9.90
7.946 J
ug/L
80
27 -123
2,4-DB
10.1
10.33
ug/L
102
16 -150
Dalapon
10.1
5.320 J
ug/L
53
10 -150
Dicamba
9.82
6.492
ug/L
66
20 -124
Dichlorprop
9.93
8.907
ug/L
90
23 -131
Dinoseb
10.1
8.215
ug/L
81
20 -110
MCPA
991
798.0 J
ug/L
81
10 -150
Silvex (2,4,5-TP)
10.1
8.165
ug/L
81
25 -122
Mecoprop
984
577.6 J
ug/L
59
10 -146 m
'
LCS LCS
Surrogate %Recovery Qualifier
Limits
DCAA 87
30 - 142
Lab Sample ID: LCSD 400-532365/3-A
Client
Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532597
Prep Batch: 532365
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits RPD Limit
2,4,5-T
10.0
7.820
ug/L
78
30 -124 1 40
2,4-D
9.90
8.396
ug/L
85
27 -123 6 40
2,4-DB
10.1
10.73
ug/L
106
16 -150 4 40
Dalapon
10.1
4.815 J
ug/L
48
10 -150 10 40
Dicamba
9.82
7.344
ug/L
75
20 -124 12 40
Dichlorprop
9.93
10.00
ug/L
101
23 -131 12 40
Dinoseb
10.1
8.047
ug/L
80
20 -110 2 40
MCPA
991
831.3 J
ug/L
84
10 -150 4 40
Silvex (2,4,5-TP)
10.1
8.555
ug/L
85
25 -122 5 40
Mecoprop
984
606.8 J
ug/L
62
10 -146 5 40
LCSD LCSD
Surrogate %Recovery Qualifier
Limits
DCAA 89
30 - 142
Method: 6010D - Metals (ICP)
Lab Sample ID: MB 400-532043/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532226
Prep Batch: 532043
MB MB
Analyte Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Silver ND
0.00500
0.00100
mg/L
05/17/2110:28
05/17/2121:05 1
Arsenic ND
0.0100
0.00300
mg/L
05/17/2110:28
05/17/2121:05 1
Barium ND
0.0100
0.00300
mg/L
05/17/2110:28
05/17/2121:05 1
Cadmium ND
0.00500
0.00100
mg/L
05/17/2110:28
05/17/2121:05 1
Chromium ND A+
0.0100
0.00500
mg/L
05/17/2110:28
05/17/2121:05 1
Lead ND
0.0100
0.00200
mg/L
05/17/2110:28
05/17/2121:05 1
Selenium ND
0.0200
0.00800
mg/L
05/17/2110:28
05/17/2121:05 1
Eurofins TestAmerica, Pensacola
Page 37 of 49 6/22/2021 (Rev. 1)

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Method: 6010D - Metals (ICP) (Continued)
Lab Sample ID: LCS 400-532043/2-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532226
Prep Batch: 532043
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec Limits
Silver
0.500
0.5198
mg/L
104 80 -120
Arsenic
1.00
1.057
mg/L
106 80-120
Barium
1.00
1.093
mg/L
109 80-120
Cadmium
0.500
0.5026
mg/L
101 80-120
Chromium
1.00
1.154
^+
mg/L
115 80-120
Lead
1.00
1.012
mg/L
101 80 -120
Selenium
1.00
1.022
mg/L
102 80-120 F
Method: 7470A - Mercury (CVAA)
T
Lab Sample ID: MB 400-531709/14-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532149
Prep Batch: 531709
MB
MB
Analyte Result
Qualifier
RL
MDL Unit
D Prepared Analyzed Dil Fac
Mercury ND
0.200
0.0700 ug/L
05/17/2109:40 05/17/2113:18 1
Lab Sample ID: LCS 400-531709/15-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532149
Prep Batch: 531709
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec Limits
Mercury
1.01
0.9916
ug/L
98 80-120
Method: 350.1 - Nitrogen, Ammonia
Lab Sample ID: MB 400-532313/47
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532313
MB
MB
Analyte Result
Qualifier
RL
MDL Unit
D Prepared Analyzed Dil Fac
Ammonia (undistilled) ND
0.0500
0.0240 mg/L
05/18/21 14:16 1
Lab Sample ID: LCS 400-532313/48
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532313
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec Limits
Ammonia (undistilled)
2.00
1.905
mg/L
95 90-110
[Lab Sample ID: MRL 400-532313/13
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532313
Spike
MRL
MRL
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec Limits
Ammonia (undistilled)
0.0500
0.06200
mg/L
124 50-150
Eurofins TestAmerica, Pensacola
Page 38 of 49 6/22/2021 (Rev. 1)

QC Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
Method: SM 2540D - Solids, Total Suspended (TSS)
Lab Sample ID: MB 400-532071/1
Matrix: Water
Analysis Batch: 532071
MB MB
Analyte Result Qualifier RL
Total Suspended Solids ND 0.500
Lab Sample ID: LCS 400-532071/2
Matrix: Water
Analysis Batch: 532071
Spike
Analyte Added
Total Suspended Solids 265
Method: SM 5210B - BOD, 5-Day
Lab Sample ID: USB 400-531930/1
Matrix: Water
Analysis Batch: 531930
USB USB
Analyte Result Qualifier
Biochemical Oxygen Demand ND
Lab Sample ID: LCS 400-531930/2
Matrix: Water
Analysis Batch: 531930
Spike
Analyte Added
Biochemical Oxygen Demand 198
RL Unit
0.500 mg/L
F
Job ID: 400-203460-1
Client Sample ID: Method Blank
Prep Type: Total/NA
L
D Prepared Analyzed Dil Fac
05/17/21 12:08 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
LCS LCS %Rec.
Result Qualifier Unit D %Rec Limits
261.0 mg/L 98 82 -118
m
Client Sample ID: Method Blank
Prep Type: Total/NA
RL MDL Unit D Prepared Analyzed Dil Fac
2.00 2.00 mg/L 05/15/2117:14 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
LCS LCS
Result Qualifier Unit
247.5 '+ mg/L
%Rec.
D %Rec Limits
125 85-115
Method: SM 5220D - COD
Lab Sample ID: MB 400-532002/4
Matrix: Water
Analysis Batch: 532002
MB
Analyte Result
MB
Qualifier
RL MDL Unit
Client Sample ID: Method Blank
Prep Type: Total/NA
D Prepared Analyzed Dil Fac
Chemical Oxygen Demand ND
10.0 6.40 mg/L
05/16/21 22:00 1
Lab Sample ID: LCS 400-532002/5
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532002
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec Limits
Chemical Oxygen Demand
50.0
46.52
mg/L 93 90-1 00
Lab Sample ID: MRL 400-532002/2
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 532002
Spike
MRL MRL
%Rec.
Analyte
Added
Result Qualifier
Unit D %Rec Limits
Chemical Oxygen Demand
30.1
24.45
mg/L 81 50-150
Eurofins TestAmerica, Pensacola
Page 39 of 49 6/22/2021 (Rev. 1)

Lab Chronicle
Client: Shield Engineering Inc
Project/Site: Celadon
F
Job ID: 400-203460-1
Client Sample ID: W-1 Lab Sample ID: 400-203460-1
Date Collected: 05/13/21 11:45 Matrix: Water
Date Received: 05/15/21 08:58
Prep Type
Batch
Type
Batch
Method
Total/NA
Analysis
8260D
Total/NA
Prep
3520C
Total/NA
Analysis
8270E
Total/NA
Prep
3520C
Total/NA
Analysis
8270E
Total/NA
Prep
3520C
Total/NA
Analysis
8081 B
Total/NA
Prep
8151A
Total/NA
Analysis
8151A
Total/NA
Prep
3010A
Total/NA
Analysis
6010D
Total/NA
Prep
3010A
Total/NA
Analysis
6010D
Total/NA
Prep
7470A
Total/NA
Analysis
7470A
Total/NA
Analysis
350.1
Total/NA
Analysis
9040C
Total/NA
Analysis
SM 2540D
Total/NA
Analysis
SM 5210B
Total/NA
Analysis
SM 5220D
Dil
Run Factor
Initial
Amount
Final
Amount
Batch
Number
Prepared
or Analyzed
Analyst
Lab
1
5 mL
5 mL
532736
05/21/21 12:48
SAB
TAL PEN
866.6 mL
1 mL
532580
05/20/21 09:44
KWS
TAL PEN
5
532781
05/21/2121:11
SIB
TAL PEN
DL
866.6 mL
1 mL
532580
05/20/21 09:44
KWS
TAL PEN
DL 100
536281
06/18/2120:52
SIB
TAL PEN
969.4 mL
5 mL
532015
05/17/21 09:06
KWS
TAL PEN
1
532257
05/18/21 16:16
IDS
TAL PEN
102.8 mL
10 mL
532365
05/19/21 08:17
IAG
TAL PEN
1
532597
05/20/21 19:02
IDS
TAL PEN
50 mL
50 mL
532043
05/17/21 10:44
KWN
TAL PEN
1
532226
05/17/21 23:04
JTW
TAL PEN
50 mL
50 mL
532043
05/17/21 10:44
KWN
TAL PEN
1
532562
05/19/21 17:51
LDC
TAL PEN
40 mL
40 mL
531709
05/17/21 09:40
NET
TAL PEN
1
532149
05/17/21 13:48
NET
TAL PEN
2
10 mL
10 mL
532313
05/18/21 14:25
KJR
TAL PEN
1
532550
05/17/21 08:40
RLL
TAL PEN
1
50 mL
100 mL
532071
05/17/21 12:08
VB
TAL PEN
1
300 mL
300 mL
531930
DEK
TAL PEN
(Start)
05/15/2110:35
(End)
05/20/2113:22
10
2 mL
2 mL
532002
05/16/21 22:00
DN1
TAL PEN
Client Sample ID: EQ-1 Lab Sample ID: 400-203460-2
Date Collected: 05/13/21 15:15 Matrix: Water
Date Received: 05/15/21 08:58
Prep Type
Batch
Type
Batch
Method
Dil
Run Factor
Initial
Amount
Final
Amount
Batch
Number
Prepared
or Analyzed
Analyst
Lab
Total/NA
Analysis
8260D
1
5 mL
5 mL
532736
05/21/21 13:16
SAB
TAL PEN
Total/NA
Prep
3520C
893 mL
1 mL
532580
05/20/21 09:44
KWS
TAL PEN
Total/NA
Analysis
8270E
20
532781
05/21/2121:33
SIB
TAL PEN
Total/NA
Prep
3520C
DL
893 mL
1 mL
532580
05/20/21 09:44
KWS
TAL PEN
Total/NA
Analysis
8270E
DL 200
536281
06/18/2121:13
SIB
TAL PEN
Total/NA
Prep
3520C
978.6 mL
5 mL
532015
05/17/21 09:06
KWS
TAL PEN
Total/NA
Analysis
8081 B
5
532257
05/18/21 16:43
IDS
TAL PEN
Total/NA
Prep
8151A
56.2 mL
10 mL
532365
05/19/21 08:17
IAG
TAL PEN
Total/NA
Analysis
8151A
1
532597
05/20/21 19:36
IDS
TAL PEN
Total/NA
Prep
3010A
50 mL
50 mL
532043
05/17/21 10:54
KWN
TAL PEN
Total/NA
Analysis
6010D
1
532226
05/17/21 23:12
JTW
TAL PEN
Total/NA
Prep
3010A
50 mL
50 mL
532043
05/17/21 10:54
KWN
TAL PEN
Total/NA
Analysis
6010D
1
532562
05/19/21 17:55
LDC
TAL PEN
Total/NA
Prep
7470A
20 mL
40 mL
531709
05/17/21 09:40
NET
TAL PEN
Total/NA
Analysis
7470A
1
532149
05/17/21 13:50
NET
TAL PEN
Total/NA
Analysis
350.1
20
10 mL
10 mL
532313
05/18/21 14:26
KJR
TAL PEN
Eurofins TestAmerica,
Pensacola
Page 40 of 49
6/22/2021 (Rev. 1)

Lab Chronicle
Client: Shield Engineering Inc
Project/Site: Celadon
Client Sample ID: EQ-1
Date Collected: 05/13/21 15:15
Date Received: 05/15/21 08:58
F
Job ID: 400-203460-1
Lab Sample ID: 400-203460-2
Matrix: Water
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Analysis
9040C
1
532550
05/17/21 08:40
RLL TAL PEN
Total/NA Analysis
SM 2540D
1
25 mL
100 mL
532071
05/17/21 12:08
VB TAL PEN
Total/NA Analysis
SM 5210B
1
300 mL
300 mL
531930
DEK TAL PEN
(Start)
05/15/2110:36
(End)
05/20/2113:22
Total/NA Analysis
SM 5220D
400
2 mL
2 mL
532002
05/16/21 22:00
DN1 TAL PEN
Client Sample ID: Method Blank
Lab Sample ID: MB 400-531709/14-A C
Date Collected: N/A
Matrix: Water
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
m
Prep Type Type
Method
Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Prep
7470A
40 mL
40 mL
531 009
05/ 77/21 09:40
NET TAL PEN
Total/NA Analysis
7470A
1
532149
05/17/21 13:18
NET TAL PEN
Client Sample ID: Method Blank
Lab Sample
ID: MB 400-532002/4 C
Date Collected: N/A
Matrix: Water
Date Received: N/A
F
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Analysis
SM 5220D
1
2 mL
2 mL
532002
05/16/21 22:00
DN1 TAL PEN
Client Sample ID: Method Blank
Lab Sample ID: MB
400-532015/1-A
Date Collected: N/A
Matrix: Water
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Prep
3520C
10 00 mL
5 mL
532 115
05/ 77/21 09:06
KWS TAL PEN
Total/NA Analysis
8081 B
1
532257
05/18/21 14:57
IDS TAL PEN
Client Sample ID: Method Blank
Lab Sample ID: MB
400-532043/1-A
Date Collected: N/A
Matrix: Water
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Prep
3010A
50 mL
50 mL
532043
05/17/21 10:28
KWN TAL PEN
Total/NA Analysis
6010D
1
532226
05/17/21 21:05
JTW TAL PEN
Client Sample ID: Method Blank
Lab Sample
ID: MB 400-532071/1
Date Collected: N/A
Matrix: Water
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Analysis
SM 2540D
1
1000 mL
100 mL
532071
05/17/21 12:08
VB TAL PEN
Page 41 of 49
Eurofins TestAmerica, Pensacola
6/22/2021 (Rev. 1)

Lab Chronicle
Client: Shield Engineering Inc
Project/Site: Celadon
Client Sample ID: Method Blank
Date Collected: N/A
Date Received: N/A
F
Job ID: 400-203460-1
Lab Sample ID: MB 400-532313/47
Matrix: Water
F
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Analysis
350.1
1
10 mL
10 mL
532313
05/18/21 14:16
KJR TAL PEN
Client Sample ID: Method Blank
Lab Sample ID: MB
400-532365/1-A
Date Collected: N/A
Matrix: Water
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
C
Prep Type Type
Method
Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Prep
8151A
250 mL
10 mL
532365
05/19/21 08:17
IAG TAL PEN
Total/NA Analysis
8151A
1
532597
05/20/21 16:48
IDS TAL PEN
Client Sample ID: Method Blank
Lab Sample ID: MB
400-532580/1-A
Date Collected: N/A
Matrix: Water
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Prep
3520C
1000 mL
1 mL
532580
05/20/21 09:44
KWS TAL PEN
Total/NA Analysis
8270E
1
532788
05/21/2117:31
S113 TAL PEN
Client Sample ID: Method Blank
Lab Sample ID: MB 400-532736/23
Date Collected: N/A
Matrix: Water
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Analysis
8260D
1
5 mL
5 mL
532736
05/21/21 12:21
SAB TAL PEN
Client Sample ID: Method Blank
Lab Sample ID: USB 400-531930/1
Date Collected: N/A
Matrix: Water
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run
Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Analysis
SM 5210B
1
300 mL
300 mL
531930
DEK TAL PEN
(Start)
05/15/2117:14
(End)
05/20/2113:22
Client Sample ID: Lab Control Sample
Date Collected: N/A
Date Received: N/A
F Batch
Batch
Prep Type Type
Method Run
Total/NA Prep
7470A
Total/NA Analysis
7470A
Lab Sample ID: LCS 400-531709/15-A
Matrix: Water
Dil Initial Final Batch
Prepared
Factor Amount Amount Number
or Analyzed Analyst Lab
40 mL 40 mL 531709
05/17/21 09:40 NET TAL PEN
1 532149
05/17/21 13:20 NET TAL PEN
Eurofins TestAmerica, Pensacola
Page 42 of 49 6/22/2021 (Rev. 1)

Lab Chronicle
Client: Shield Engineering Inc
Project/Site: Celadon
Client Sample ID: Lab Control Sample
Date Collected: N/A
Date Received: N/A
F
Job ID: 400-203460-1
Lab Sample ID: LCS 400-531930/2
Matrix: Water
F Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis SM 5210B 1 1 mL 1 mL 531930 DEK TAL PEN
(Start) 05/15/2117:14
(End) 05/20/2113:22
Client Sample ID: Lab Control Sample
Date Collected: N/A
Date Received: N/A
Prep Type
Batch
Type
Batch
Method
Dil
Run Factor
Initial
Amount
Total/NA
Analysis
SM 5220D
1
2 mL
Client Sample ID: Lab Control Sample
Date Collected: N/A
Date Received: N/A
Batch
Batch
Prep Type Type
Method Run
Total/NA Prep
3520C
Total/NA Analysis
8081 B
Client Sample ID: Lab Control Sample
Date Collected: N/A
Date Received: N/A
Batch
Batch
Prep Type Type
Method Run
Total/NA Prep
3010A
Total/NA Analysis
6010D
Client Sample ID: Lab Control Sample
Date Collected: N/A
Date Received: N/A
Lab Sample ID: LCS 400-532002/5
Matrix: Water E:
Final Batch Prepared F
Amount Number or Analyzed Analyst Lab
2 mL 532002 05/16/21 22:00 DN1 TAL PEN
Lab Sample ID: LCS 400-53201512-A
Matrix: Water
Dil Initial Final Batch
Prepared
Factor Amount Amount Number
or Analyzed Analyst Lab
1000 mL 5 mL 532015
05/17/21 09:06 KWS TAL PEN
1 532257
05/18/21 15:23 IDS TAL PEN
L
Lab Sample ID: LCS 400-532043/2-A
Matrix: Water
Dil Initial Final Batch
Prepared
Factor Amount Amount Number
or Analyzed Analyst Lab
50 mL 50 mL 532043
05/17/21 10:28 KWN TAL PEN
1 532226
05/17/21 21:09 JTW TAL PEN
Lab Sample ID: LCS 400-532071/2
Matrix: Water
F Batch Batch Dil Initial Final Batch Prepared
Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab
Total/NA Analysis SM 2540D 1 100 mL 100 mL 532071 05/17/21 12:08 VB TAL PEN
Client Sample ID: Lab Control Sample
Date Collected: N/A
Date Received: N/A
F Batch Batch
Prep Type Type Method Run
Total/NA Analysis 350.1
Lab Sample ID: LCS 400-532313/48
Matrix: Water
Dil
Initial
Final
Batch
Prepared
Factor
Amount
Amount
Number
or Analyzed Analyst Lab
1
10 mL
10 mL
532313
05/18/21 14:17 KJR TAL PEN
Eurofins TestAmerica, Pensacola
Page 43 of 49 6/22/2021 (Rev. 1)

Lab Chronicle
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 400-532365/2-A
Date Collected: N/A
Matrix: Water
Date Received: N/A
F
Batch Batch
Dil Initial
Final
Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Prep 8151A
250 mL
10 mL
532365 05/19/21 08:17 IAG TAL PEN
Total/NA Analysis 8151A
1
532597 05/20/21 15:41 IDS TAL PEN
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 400-532550/1
Date Collected: N/A
Matrix: Water
Date Received: N/A
Batch Batch
Dil Initial
Final
Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Analysis 9040C
1
532550 05/17/21 08:40 RLL TAL PEN
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 400-532580/2-A
Date Collected: N/A
Matrix: Water m
Date Received: N/A
Batch Batch
Dil Initial
Final
Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Prep 3520C
1000 mL
1 mL
532580 05/20/21 09:44 KWS TAL PEN
Total/NA Analysis 8270E
1 0.4 mL
1.0 mL
532788 05/21/21 17:54 S113 TAL PEN
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 400-532736/1009
Date Collected: N/A
Matrix: Water
Date Received: N/A
Batch Batch
Dil Initial
Final
Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Analysis 8260D
1 5 mL
5 mL
532736 05/21/21 11:18 SAB TAL PEN
Client Sample ID: Lab Control Sample Dup
Lab Sample ID: LCSD 400-532365/3-A
Date Collected: N/A
Matrix: Water
Date Received: N/A
Batch Batch
Dil Initial
Final
Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Prep 8151A
250 mL
10 mL
532365 05/19/21 08:17 IAG TAL PEN
Total/NA Analysis 8151A
1
532597 05/20/21 16:14 IDS TAL PEN
Client Sample ID: Lab Control Sample
Lab Sample ID: MRL 400-532002/2
Date Collected: N/A
Matrix: Water
Date Received: N/A
F
Batch Batch
Dil Initial
Final
Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Analysis SM 5220D
1 2 mL
2 mL
532002 05/16/21 22:00 DN1 TAL PEN
Client Sample ID: Lab Control Sample
Lab Sample ID: MRL 400-532313/13
Date Collected: N/A
Matrix: Water
Date Received: N/A
Batch Batch
Dil Initial
Final
Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Analysis 350.1
1 10 mL
10 mL
532313 05/18/21 13:38 KJR TAL PEN
Eurofins TestAmerica, Pensacola
Page 44 of 49 6/22/2021 (Rev. 1)

Lab Chronicle
Client: Shield Engineering Inc
Job ID: 400-203460-1
Project/Site: Celadon
Client Sample ID: W-1
Lab Sample ID: 400-203460-1 MS
Date Collected: 05/13/21 11:45
Matrix: Water
Date Received: 05/15/21 08:58
Batch Batch
Dil
Initial
Final
Batch Prepared
Prep Type Type Method
Run Factor
Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Analysis 8260D
1
5 mL
5 mL
532736 05/21/21 13:43 SAB TAL PEN
Client Sample ID: W-1
Lab Sample ID: 400-203460-1 MSD
Date Collected: 05/13/21 11:45
Matrix: Water
Date Received: 05/15/21 08:58
Batch Batch
Dil
Initial
Final
Batch Prepared
C
Prep Type Type Method
Run Factor
Amount
Amount
Number or Analyzed Analyst Lab
Total/NA Analysis 8260D
1
5 mL
5 mL
532736 05/21/21 14:10 SAB TAL PEN
Laboratory References:
TAL PEN = Eurofins TestAmerica, Pensacola, 3355
McLemore Drive, Pensacola,
FL 32514, TEL [phone] m
Eurofins TestAmerica, Pensacola
Page 45 of 49 6/22/2021 (Rev. 1)

Method Summary
Client: Shield Engineering Inc
Project/Site: Celadon
Job ID: 400-203460-1
Method
Method Description
Protocol
Laboratory
8260D
Volatile Organic Compounds by GC/MS
SW846
TAL PEN
8270E
Semivolatile Organic Compounds (GC/MS)
SW846
TAL PEN
8081 B
Organochlorine Pesticides (GC)
SW846
TAL PEN
8151A
Herbicides (GC)
SW846
TAL PEN
6010D
Metals (ICP)
SW846
TAL PEN
7470A
Mercury (CVAA)
SW846
TAL PEN
350.1
Nitrogen, Ammonia
MCAWW
TAL PEN
9040C
pH
SW846
TAL PEN
SM 2540D
Solids, Total Suspended (TSS)
SM
TAL PEN
SM 5210B
BOD, 5-Day
SM
TAL PEN
SM 5220D
COD
SM
TAL PEN
3010A
Preparation, Total Metals
SW846
TAL PEN
3520C
Liquid -Liquid Extraction (Continuous)
SW846
TAL PEN
5030C
Purge and Trap
SW846
TAL PEN
7470A
Preparation, Mercury
SW846
TAL PEN
8151A
Extraction (Herbicides)
SW846
TAL PEN
Protocol References:
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL PEN = Eurofins TestAmerica, Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
Eurofins TestAmerica, Pensacola
Page 46 of 49 6/22/2021 (Rev. 1)

Accreditation/Certification Summary
Client: Shield Engineering Inc
Project/Site: Celadon
Laboratory: Eurofins TestAmerica, Pensacola
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Job ID: 400-203460-1
Authority Program Identification Number Expiration Date
North Carolina (WW/SW) State 314 12-31-21
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method
Matrix
Analyte
8260D
Water
1,2-Dichloroethene, Total
8260D
Water
1,3-Dichloropropene, Total
8260D
Water
Butadiene
8260D
Water
Hexane
8260D
Water
n-Heptane
8260D
Water
Tetrahydrofuran
9040C
Water
Temperature
Eurofins TestAmerica, Pensacola
Page 47 of 49 6/22/2021 (Rev. 1)

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Page 48 of 49
6/22/2021 (Rev. 1) 1

Login Sample Receipt Checklist
Client: Shield Engineering Inc Job Number: 400-203460-1
Login Number: 203460
List Number: 1
Creator: Conrady, Hank W
Question
List Source: Eurofins TestAmerica, Pensacola
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
N/A
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True 0.0°C IR-9
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Eurofins TestAmerica, Pensacola
Page 49 of 49 6/22/2021 (Rev. 1)

urofins
Environment Testing
America
ANALYTICAL REPORT
Eurofins TestAmerica, Pensacola
3355 McLemore Drive
Pensacola, FL 32514
Tel: [phone]
Laboratory Job ID: 400-203461-1
Client Project/Site: Celadon
r:
Shield Engineering Inc
4301 Taggart Creek Road
Charlotte, North Carolina 28208
Attn: Tom Witner
Authorized for release by.
512812021 1:29:28 PM
Ken Hayes, Project Manager II
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.

Client: Shield Engineering Inc
Project/Site: Celadon
Table of Contents
Laboratory Job ID: 400-203461-1
Cover Page ..............................................
1
Table of Contents .........................................
2
Case Narrative ...........................................
3 L
Detection Summary ........................................
5
Sample Summary .........................................
6
Client Sample Results ......................................
7
Definitions.........................................
14
Surrogate Summary .......................................
15 E:
QC Association ...........................................
19 F
QC Sample Results ........................................
24
Chronicle................................................
44
Method Summary .........................................
52
Certification Summary ......................................
53
Chain of Custody ..........................................
54
E:
Receipt Checklists .........................................
56
Eurofins TestAmerica, Pensacola
Page 2 of 56 5/28/2021

Case Narrative C
Client: Shield Engineering Inc Job ID: 400-203461-1
Project/Site: Celadon
Job ID: 400-203461-1
Laboratory: Eurofins TestAmerica, Pensacola
Narrative
Job Narrative
400-203461-1
Comments
No additional comments.
Receipt
The samples were received on 5/15/2021 10:31 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperatures of the 2 coolers at receipt time were 0.00 C and 0.00 C.
GC/MS VOA
Method 8260D: The continuing calibration verification (CCV) associated with batch 400-532492 recovered outside acceptance criteria, low
biased, for 1, 1 -Dichloroethene. A reporting limit (RL) standard was analyzed, and the target analyte was detected. Since the associated
samples were non -detect for this analyte, the data have been reported.
Method 8260D: Due to the TCLP extraction process, the following sample was diluted X5: S1-5 COMPOSITE (400-203461-6).
Method 8260D: The continuing calibration verification (CCV) associated with batch 400-532534 recovered above the upper control limit for
Isobutyl alcohol. The samples associated with this CCV were non -detects for the affected analytes; therefore, the data have been
reported.
Method 8260D: The matrix spike duplicate (MSD) recoveries for preparation batch 400-532586 and analytical batch 400-532534 were
outside control limits. Non -homogeneity is suspected because the associated laboratory control sample (LCS) recovery was within
acceptance limits.
Method 8260D: Surrogate recovery for the following samples were outside control limits: S1-5 COMPOSITE (400-203461-6),
(400-203461-1-6-J MS) and (400-203461-1-6-K MSD). Evidence of matrix interference is present.
Method 8260D: Internal standard responses were outside of acceptance limits for the following sample: S1-5 COMPOSITE
(400-203461-6), (400-203461-1-6-J MS) and (400-203461-1-6-K MSD). The sample shows evidence of matrix interference.
Method 8260D: The continuing calibration verification (CCV) associated with batch 400-532709 recovered outside acceptance criteria, low
biased, for Bromomethane and Carbon disulfide. A reporting limit (RL) standard was analyzed, and the target analyte was detected.
Since the associated samples were non -detect for this analyte, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC/MS Semi VOA
Method 8270E: The following analyte(s) recovered outside control limits for the LCSD associated with preparation batch 400-532298 and
analytical batch 400-532461: Bis(2-chloroethyl)ether. This is not indicative of a systematic control problem because these were random
marginal exceedances. Qualified results have been reported.
Method 8270E: The following sample was diluted due to the nature of the sample matrix: S1-5 COMPOSITE (400-203461-6). Elevated
reporting limits (RLs) are provided.
Method 8270E: The continuing calibration verification (CCV) associated with batch 400-532461 recovered outside acceptance criteria, low
biased, for Nitrobenzene, Isophorone, Caprolactam, Bis(2-chloroethoxy)methane and Dibenz(a,h)anthracene. A reporting limit (RL)
standard was analyzed, and the target analyte was detected. Since the associated samples were non -detect for this analyte, the data
have been reported.
Method 8270E: The continuing calibration verification (CCV) associated with batch 400-532802 recovered above the upper control limit for
Hexachlorobutadiene and Hexachlorobenzene. The samples associated with this CCV were non -detects for the affected analytes;
therefore, the data have been reported.
Method 8270E: The continuing calibration verification (CCV) associated with batch 400-532802 recovered outside acceptance criteria, low
Eurofins TestAmerica, Pensacola
Page 3 of 56 5/28/2021

Case Narrative
Client: Shield Engineering Inc
Project/Site: Celadon
Job ID: 400-203461-1 (Continued)
Laboratory: Eurofins TestAmerica, Pensacola (Continued)
Job ID: 400-203461-1
biased, for Pyridine, Nitrobenzene and 3 & 4 Methylphenol. A reporting limit (RL) standard was analyzed, and the target analyte was
detected. Since the associated samples were non -detect for this analyte, the data have been reported.
Method 8270E: The laboratory control sample duplicate (LCSD) for preparation batch 400-532706 and analytical batch 400-532781
recovered outside control limits for the following analyte: Pyridine. Pyridine has been identified as a poor performing analyte when
analyzed using this method; therefore, re-extraction/re-analysis was not performed. Batch precision also exceeded control limits for this
analyte. This result has been reported and qualified.
Method 8270E: The RPD of the laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for preparation batch
400-532706 and analytical batch 400-532781 recovered outside control limits for the following analytes: Pyridine.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
GC Semi VOA
Method 8081 B: The continuing calibration verification (CCV) associated with batch 400-532547 recovered above the upper control limit for
Chlordane (technical). The samples associated with this CCV were non -detects for the affected analytes; therefore, the data have been
reported.
Method 8151A: The following sample was diluted due to the nature of the sample matrix: S1-5 COMPOSITE (400-203461-6). Elevated
reporting limits (RLs) are provided.
Method 8081 B: The continuing calibration verification (CCV) associated with batch 400-532719 recovered outside acceptance criteria, low
biased, for Endrin aldehyde. A reporting limit (RL) standard was analyzed, and the target analyte was detected. Since the associated
samples were non -detect for this analyte, the data have been reported.
Method 8081 B: The following samples were diluted due to the nature of the sample matrix: S1-5 COMPOSITE (400-203461-6),
(400-203461-1-6-F MS) and (400-203461-1-6-G MSD). Elevated reporting limits (RLs) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
Method 7471 B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 400-532086 and analytical batch
400-532437 were outside control limits. Sample matrix interference and/or non -homogeneity are suspected because the associated
laboratory control sample (LCS) recovery was within acceptance limits.
Method 7471 B: The method blank for preparation batch 400-532377 and analytical batch 400-532437contained Hg above the method
detection limit. This target analyte concentration was less than the practical quantitation limit (PQL); therefore, re -extraction or re -analysis
of samples was not performed.
Method 6010D: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 400-532212 and analytical batch
400-532562 were outside control limits. Sample matrix interference and/or non -homogeneity are suspected because the associated
laboratory control sample (LCS) recovery was within acceptance limits.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Eurofins TestAmerica, Pensacola
Page 4 of 56 5/28/2021

Detection Summary
Client: Shield Engineering Inc
Project/Site: Celadon
F
Job ID: 400-203461-1
Client Sample ID: S1-5 COMPOSITE
Lab Sample ID: 400-203461-6
Analyte
Result Qualifier
RL
MDL
Unit
Dil Fac
D
Method
Prep Type
Acetone
503
198
103
ug/Kg
1
*
8260D
Total/NA
2-Butanone (MEK)
122 J
198
47.5
ug/Kg
1
*
8260D
Total/NA
Ethylbenzene
5.01 J
39.6
4.83
ug/Kg
1
*
8260D
Total/NA
4-Isopropyltoluene
8.26 J
39.6
7.91
ug/Kg
1
*
8260D
Total/NA
Toluene
155
39.6
7.91
ug/Kg
1
*
8260D
Total/NA
1,2,4-Trimethylbenzene
9.99 J
39.6
7.91
ug/Kg
1
*
8260D
Total/NA
2-Methyl-2-propanol
1670
79.1
63.3
ug/Kg
1
*
8260D
Total/NA
Bis(2-ethylhexyl) phthalate
16400 B
12800
1280
ug/Kg
5
*
8270E
Total/NA
Benzaldehyde
2360 J
12800
1280
ug/Kg
5
#
8270E
Total/NA
Barium
71.3
7.30
1.24
mg/Kg
1
6010D
Total/NA
Chromium
291
7.30
2.26
mg/Kg
1
6010D
Total/NA
Lead
14.4
7.30
1.61
mg/Kg
1
6010D
Total/NA
Hg
0.326
0.116
0.0696
mg/Kg
1
7471 B
Total/NA
This Detection Summary does not include radiochemical test results.
0
Eurofins TestAmerica, Pensacola
Page 5 of 56 5/28/2021

Sample Summary
Client: Shield Engineering Inc
Project/Site: Celadon
Job ID: 400-203461-1
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID
400-203461-6 S1-5 COMPOSITE Solid 05/13/21 14:05 05/15/21 10:31
Eurofins TestAmerica, Pensacola
Page 6 of 56 5/28/2021

Client Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
Job ID: 400-203461-1
Client Sample ID: S1-5 COMPOSITE Lab Sample ID: 400-203461-6
Date Collected: 05/13/21 14:05 Matrix: Solid
Date Received: 05/15/21 10:31 Percent Solids: 12.6
Method: 8260D - Volatile Organic Compounds by GC/MS
Analyte
Result
Qualifier
Acetone
503
Benzene
ND
Bromobenzene
ND
Chlorobromomethane
ND
Dichlorobromomethane
ND
Bromoform
ND
Bromomethane
ND
2-Butanone (MEK)
122
J
n-Butylbenzene
ND
sec- Butylbenzene
ND
tert-Butylbenzene
ND
Carbon disulfide
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chloroethane
ND
Chloroform
ND
Chloromethane
ND
3-Chloro-1-propene
ND
2-Chlorotoluene
ND
4-Chlorotoluene
ND
Chlorodibromomethane
ND
1,2-Dibromo-3-Chloropropane
ND
Ethylene Dibromide
ND
Dibromomethane
ND
1,2-Dichlorobenzene
ND
1,3-Dichlorobenzene
ND
1,4-Dichlorobenzene
ND
trans-1,4-Dichloro-2-butene
ND
Dichlorodifluoromethane
ND
1,1-Dichloroethane
ND
1,2-Dichloroethane
ND
cis-1,2-Dichloroethene
ND
trans- 1,2-Dichloroethene
ND
1,2-Dichloroethene, Total
ND
1,1-Dichloroethene
ND
1,2-Dichloropropane
ND
1,3-Dichloropropane
ND
2,2-Dichloropropane
ND
1,1-Dichloropropene
ND
cis-1,3-Dichloropropene
ND
trans- 1,3-Dichloropropene
ND
Ethylbenzene
5.01
J
Ethyl methacrylate
ND
Hexachlorobutadiene
ND
2-Hexanone
ND
lodomethane
ND
Isobutyl alcohol
ND
Isopropylbenzene
ND
4-Isopropyltoluene
8.26
J
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
198
103
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
5.30
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
10.3
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
19.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
19.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
19.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
40.2
20.1
ug/Kg
*
05/21/2108:15
05/21/2110:46
1
198
47.5
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
7.60
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
7.52
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
39.6
19.8
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
40.2
20.1
ug/Kg
05/21/2108:15
05/21/2110:46
1
39.6
13.5
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
4.11
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
19.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
19.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
7.91
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
7.91
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
19.8
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
39.6
7.75
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
39.6
19.8
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
39.6
26.1
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
7.91
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
19.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
5.62
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
7.52
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
39.6
19.8
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
39.6
19.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
40.2
10.5
ug/Kg
*
05/21/2108:15
05/21/2110:46
1
39.6
6.57
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
6.49
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
6.01
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
19.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
11.1
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
39.6
19.8
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
39.6
19.8
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
39.6
7.91
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
39.6
19.8
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
39.6
19.8
ug/Kg
#
05/20/21 08:15
05/20/21 14:36
1
39.6
9.49
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
19.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
4.83
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
7.91
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
19.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
198
39.6
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
40.2
27.3
ug/Kg
*
05/21/2108:15
05/21/2110:46
1
198
79.1
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
5.38
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
39.6
7.91
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
0
Eurofins TestAmerica, Pensacola
Page 7 of 56 5/28/2021

Client Sample Results
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Client Sample ID: S1-5 COMPOSITE
Lab Sample
ID: 400-203461-6
Date Collected: 05/13/21 14:05
Matrix:
Solid
Date Received: 05/15/21 10:31
Percent Solids:
12.6
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Methylene Chloride
ND
119
79.1
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
4-Methyl-2-pentanone (MIBK)
ND
198
39.6
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
�.
Methyl tert-butyl ether
ND
39.6
7.91
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
Naphthalene
ND
39.6
15.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
N-Propylbenzene
ND
39.6
7.12
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
Styrene
ND
39.6
7.91
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
1,1,1,2-Tetrachloroethane
ND
39.6
19.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
1,1,2,2-Tetrachloroethane
ND
39.6
19.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
Tetrachloroethene
ND
39.6
19.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
Toluene
155
39.6
7.91
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
1,2,3-Trichlorobenzene
ND
39.6
19.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
1,2,4-Trichlorobenzene
ND
39.6
15.8
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
1,1,1-Trichloroethane
ND
39.6
8.70
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
1,1,2-Trichloroethane
ND
39.6
19.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
Trichloroethene
ND
39.6
7.91
ug/Kg
i:�
05/20/21 08:15
05/20/21 14:36
1
Trichlorofluoromethane
ND
39.6
19.8
ug/Kg
i:�
05/20/21 08:15
05/20/21 14:36
1
1,2,3-Trichloropropane
ND
39.6
23.7
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
39.6
15.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
1,2,4-Trimethyl benzene
9.99 J
39.6
7.91
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
1,3,5-Trimethylbenzene
ND
39.6
6.57
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
Vinyl acetate
ND
198
72.0
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
Vinyl chloride
ND
39.6
19.8
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
o-Xylene
ND
39.6
7.91
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
m-Xylene & p-Xylene
ND
39.6
10.3
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
Xylenes, Total
ND
79.1
15.0
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
Cyclohexane
ND
39.6
7.44
ug/Kg
#
05/20/21 08:15
05/20/21 14:36
1
Methyl acetate
ND
39.6
36.4
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
Methylcyclohexane
ND
39.6
11.9
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
Tetrahydrofuran
ND
79.1
39.6
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
Hexane
ND
39.6
9.49
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
Ethyl ether
ND
39.6
7.91
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
n-Heptane
ND
39.6
19.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
1,3-Dichloropropene, Total
ND
39.6
19.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
Butadiene
ND
39.6
7.91
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
Dichlorofluoromethane
ND
39.6
19.8
ug/Kg
*
05/20/21 08:15
05/20/21 14:36
1
2-Methyl-2-propanol
1670
79.1
63.3
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
1,4-Dioxane
ND
3960
396
ug/Kg
05/20/21 08:15
05/20/21 14:36
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
4-Bromofluorobenzene
126
67- 130
05120121 08:15
05120121 14:36
1
4-Bromofluorobenzene
137 "3 S1+
67- 130
05121121 08:15
05121121 10:46
1
Dibromofluoromethane
93
77- 127
05120121 08:15
05120121 14:36
1
Dibromofluoromethane
93
77- 127
05121121 08:15
05121121 10:46
1
Toluene-d8 (Surr)
110
76 - 127
05120121 08:15
05120121 14:36
1
Toluene-d8 (Surr)
113
76 - 127
05121121 08:15
05121121 10:46
1
1,2-Dichloroethane-d4 (Surr)
101
78- 146
05120121 08:15
05120121 14:36
1
1,2-Dichloroethane-d4 (Surr)
102
78- 146
05121121 08:15
05121121 10:46
1
Eurofins TestAmerica, Pensacola
Page 8 of 56 5/28/2021

Client Sample Results
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Client Sample ID: S1-5 COMPOSITE
Lab Sample
ID: 400-203461-6
Date Collected: 05/13/21 14:05
Matrix:
Solid
Date Received: 05/15/21 10:31
Percent Solids:
12.6
Method: 8260D - Volatile Organic Compounds by GC/MS - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Benzene
ND
25.0
1.70
ug/L
05/20/21 03:56
5
Carbon tetrachloride
ND
25.0
2.50
ug/L
05/20/21 03:56
5
Chlorobenzene
ND
25.0
2.50
ug/L
05/20/21 03:56
5
Chloroform
ND
25.0
3.00
ug/L
05/20/21 03:56
5
1,4-Dichlorobenzene
ND
25.0
3.20
ug/L
05/20/21 03:56
5
1,2-Dichloroethane
ND
25.0
2.50
ug/L
05/20/21 03:56
5
1,1-Dichloroethene
ND
25.0
2.50
ug/L
05/20/21 03:56
5
2-Butanone (MEK)
ND
125
13.0
ug/L
05/20/21 03:56
5
Tetrachloroethene
ND
25.0
2.90
ug/L
05/20/21 03:56
5
Trichloroethene
ND
25.0
2.50
ug/L
05/20/21 03:56
5
Vinyl chloride
ND
25.0
2.50
ug/L
05/20/21 03:56
5
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
4-Bromofluorobenzene
94
78 - 118
05120121 03:56
5
Dibromofluoromethane
104
81- 121
05120121 03:56
5
Toluene-d8 (Surr)
101
80 - 120
05120121 03:56
5
Method: 8270E - Semivolatile Organic Compounds
(GC/MS)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
1,1'-Biphenyl
ND
12800
1280
ug/Kg
#
05/18/21 14:27
05/19/21 20:30
5
2,4,5-Trichlorophenol
ND
12800
1280
ug/Kg
#
05/18/21 14:27
05/19/21 20:30
5
2,4,6-Trichlorophenol
ND
12800
1280
ug/Kg
#
05/18/21 14:27
05/19/21 20:30
5
2,4-Dichlorophenol
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
2,4-Dimethylphenol
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
2,4-Dinitrophenol
ND
38500
11300
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
2,4-Dinitrotoluene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
2-Chlorophenol
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
2-Chloronaphthalene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
2-Methylnaphthalene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
2-Methylphenol
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
2-Nitroaniline
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
2-Nitrophenol
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
3 & 4 Methylphenol
ND
25700
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
3,3'-Dichlorobenzidine
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
3-Nitroaniline
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
4,6-Dinitro-2-methylphenol
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
4-Bromophenyl phenyl ether
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
4-Chloro-3-methylphenol
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
4-Chloroaniline
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
4-Chlorophenyl phenyl ether
ND
12800
1280
ug/Kg
3�,
05/18/21 14:27
05/19/21 20:30
5
4-Nitroaniline
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Acenaphthene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Acenaphthylene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Acetophenone
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Anthracene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Benzo[a]anthracene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Benzo[a]pyrene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Benzo[b]fluoranthene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Benzo[g,h,i]perylene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Benzo[k]fluoranthene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Eurofins TestAmerica, Pensacola
Page 9 of 56 5/28/2021

Client Sample Results
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Client Sample ID: S1-5 COMPOSITE
Lab Sample
ID: 400-203461-6
Date Collected: 05/13/21 14:05
Matrix:
Solid
Date Received: 05/15/21 10:31
Percent Solids:
12.6
Method: 8270E - Semivolatile Organic Compounds
(GC/MS) (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Bis(2-chloroethoxy)methane
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Bis(2-chloroethyl)ether
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Bis(2-ethylhexyl) phthalate
16400 B
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Chrysene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Dibenz(a,h)anthracene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Dibenzofuran
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Di-n-butyl phthalate
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Diethyl phthalate
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Dimethyl phthalate
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Di-n-octyl phthalate
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Fluoranthene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Fluorene
ND
12800
1280
ug/Kg
05/18/21 14:27
05/19/21 20:30
5
Hexachlorobenzene
ND
12800
3890
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Hexachlorobutadiene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Hexachlorocyclopentadiene
ND
12800
2570
ug/Kg
i:�
05/18/21 14:27
05/19/21 20:30
5
Hexachloroethane
ND
12800
3890
ug/Kg
i:�
05/18/21 14:27
05/19/21 20:30
5
Indeno[1,2,3-cd]pyrene
ND
12800
1280
ug/Kg
i:�
05/18/21 14:27
05/19/21 20:30
5
Isophorone
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Naphthalene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Nitrobenzene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
N-Nitrosodiphenylamine
ND
12800
1280
ug/Kg
05/18/21 14:27
05/19/21 20:30
5
N-Nitrosodi-n-propylamine
ND
12800
4280
ug/Kg
05/18/21 14:27
05/19/21 20:30
5
Pentachlorophenol
ND
25700
2570
ug/Kg
05/18/21 14:27
05/19/21 20:30
5
Phenanthrene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Phenol
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Pyrene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Butyl benzyl phthalate
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
bis (2-chloroisopropyl) ether
ND
12800
1280
ug/Kg
05/18/21 14:27
05/19/21 20:30
5
Carbazole
ND
12800
1280
ug/Kg
05/18/21 14:27
05/19/21 20:30
5
2,6-Dinitrotoluene
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
4-Nitrophenol
ND
12800
4280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Atrazine
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Benzaldehyde
2360 J
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Caprolactam
ND
12800
1280
ug/Kg
*
05/18/21 14:27
05/19/21 20:30
5
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol (Surr)
102
10- 150
05118121 14:27
05119121 20:30
5
2-Fluorobiphenyl (Surr)
50
27- 127
05118121 14:27
05119121 20:30
5
2-Fluorophenol (Surr)
43
25 - 128
05118121 14:27
05119121 20:30
5
Terphenyl-d14 (Surr)
65
24- 146
05118121 14:27
05119121 20:30
5
Phenol-d5 (Surr)
54
29 - 130
05118121 14:27
05119121 20:30
5
Nitrobenzene-d5 (Surr)
46
15 - 136
05118121 14:27
05119121 20:30
5
Method: 8270E - Semivolatile Organic Compounds
(GC/MS) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
2-Methylphenol
ND
13.9
2.09
ug/L
05/21/2107:30
05/21/2122:57
1
3 & 4 Methylphenol
ND
27.8
2.09
ug/L
05/21/21 07:30
05/21/21 22:57
1
2,4-Dinitrotoluene
ND
13.9
1.95
ug/L
05/21/2107:30
05/21/2122:57
1
Hexachloroethane
ND
13.9
3.34
ug/L
05/21/2107:30
05/21/2122:57
1
Hexachlorobutadiene
ND
13.9
2.37
ug/L
05/21/2107:30
05/21/2122:57
1
0
Eurofins TestAmerica, Pensacola
Page 10 of 56 5/28/2021

Client Sample Results
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Client Sample ID: S1-5 COMPOSITE
Lab Sample
ID: 400-203461-6
Date Collected: 05/13/21 14:05
Matrix:
Solid
Date Received: 05/15/21 10:31
Percent Solids:
12.6
Method: 8270E - Semivolatile Organic Compounds
(GC/MS) - TCLP (Continued)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Hexachlorobenzene
ND
13.9
1.67
ug/L
05/21/21 07:30
05/21/2122:57
1
Nitrobenzene
ND
13.9
2.23
ug/L
05/21/21 07:30
05/21/2122:57
1
Pentachlorophenol
ND
27.8
5.15
ug/L
05/21/21 07:30
05/21/2122:57
1
2,4,5-Trichlorophenol
ND
13.9
1.53
ug/L
05/21/21 07:30
05/21/2122:57
1
2,4,6-Trichlorophenol
ND
13.9
2.23
ug/L
05/21/21 07:30
05/21/2122:57
1
Pyridine
ND *- *1
13.9
6.12
ug/L
05/21/21 07:30
05/21/21 22:57
1
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol (Surr)
115
10- 150
05121121 07:30
05121121 22:57
1
2-Fluorobiphenyl
74
21- 114
05121121 07:30
05121121 22:57
1
2-Fluorophenol (Surr)
57
10 - 105
05121121 07:30
05121121 22:57
1
Nitrobenzene-d5 (Surr)
48
16 - 127
05121121 07:30
05121121 22:57
1
Phenol-d5 (Surr)
44
10- 129
05121121 07:30
05121121 22:57
1
Terphenyl-d14 (Surr)
95
13- 150
05121121 07:30
05121121 22:57
1
Method: 8081B - Organochlorine
Pesticides (GC)
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
4,4'-DDD
ND
133
14.9
ug/Kg
*
05/20/21 15:05
05/21/21 12:50
10
4,4'-DDE
ND
133
21.2
ug/Kg
*
05/20/21 15:05
05/21/21 12:50
10
4,4'-DDT
ND
133
60.3
ug/Kg
*
05/20/21 15:05
05/21/21 12:50
10
Aldrin
ND
133
47.8
ug/Kg
#
05/20/21 15:05
05/21/21 12:50
10
alpha-BHC
ND
133
18.8
ug/Kg
#
05/20/21 15:05
05/21/21 12:50
10
beta-BHC
ND
133
39.2
ug/Kg
#
05/20/21 15:05
05/21/21 12:50
10
Chlordane (technical)
ND
1330
196
ug/Kg
*
05/20/21 15:05
05/21/21 12:50
10
delta-BHC
ND
133
25.1
ug/Kg
*
05/20/21 15:05
05/21/21 12:50
10
Dieldrin
ND
133
28.2
ug/Kg
*
05/20/21 15:05
05/21/21 12:50
10
Endosulfan I
ND
133
16.5
ug/Kg
*
05/20/21 15:05
05/21/21 12:50
10
Endosulfan 11
ND
133
18.0
ug/Kg
*
05/20/21 15:05
05/21/21 12:50
10
Endosulfan sulfate
ND
133
16.5
ug/Kg
*
05/20/21 15:05
05/21/21 12:50
10
Endrin
ND
133
14.9
ug/Kg
*
05/20/21 15:05
05/21/21 12:50
10
Endrin aldehyde
ND
133
22.7
ug/Kg
*
05/20/21 15:05
05/21/21 12:50
10
gamma-BHC (Lindane)
ND
133
17.2
ug/Kg
*
05/20/21 15:05
05/21/21 12:50
10
Heptachlor
ND
133
18.8
ug/Kg
*
05/20/21 15:05
05/21/21 12:50
10
Heptachlor epoxide
ND
133
35.3
ug/Kg
*
05/20/21 15:05
05/21/21 12:50
10
Toxaphene
ND
7830
2270
ug/Kg
*
05/20/21 15:05
05/21/21 12:50
10
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
DCB Decachlorobiphenyl
37
26- 129
05120121 15:05
05121121 12:50
10
Tetrachloro-m-xylene
41
31- 122
05120121 15:05
05121121 12:50
10
Method: 8081B - Organochlorine
Pesticides (GC) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Chlordane (technical)
ND
25.0
2.60
ug/L
05/19/21 14:12
05/20/21 14:08
1
Endrin
ND
1.00
0.0600
ug/L
05/19/21 14:12
05/20/21 14:08
1
gamma-BHC (Lindane)
ND
2.50
0.500
ug/L
05/19/21 14:12
05/20/21 14:08
1
Heptachlor
ND
1.00
0.0620
ug/L
05/19/21 14:12
05/20/21 14:08
1
Heptachlor epoxide
ND
1.00
0.0640
ug/L
05/19/21 14:12
05/20/21 14:08
1
Methoxychlor
ND
1.00
0.0820
ug/L
05/19/21 14:12
05/20/21 14:08
1
Toxaphene
ND
150
6.00
ug/L
05/19/21 14:12
05/20/21 14:08
1
Eurofins TestAmerica, Pensacola
Page 11 of 56 5/28/2021

Client Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
Job ID: 400-203461-1
Client Sample ID: S1-5 COMPOSITE Lab Sample ID: 400-203461-6
Date Collected: 05/13/21 14:05 Matrix: Solid
Date Received: 05/15/21 10:31 Percent Solids: 12.6
Surrogate %Recovery Qualifier Limits
DCB Decachlorobiphenyl 66 10- 130
Tetrachloro-m-xylene 86 43 - 130
Method: 8151A - Herbicides (GC)
Analyte
2,4,5-T
2,4-D
2,4-DB
Dalapon
Dicamba
Dichlorprop
Dinoseb
MCPA
Silvex (2,4,5-TP)
Mecoprop
Prepared Analyzed Dil Fac
05119121 14:12 05120121 14:08 1
05119121 14:12 05120121 14:08 1
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
ND
3160
269
ug/Kg
05/19/2109:10
05/21/2111:23
10
ND
15800
869
ug/Kg
05/19/2109:10
05/21/2111:23
10
ND
1190
553
ug/Kg
05/19/2109:10
05/21/2111:23
10
ND
1580
790
ug/Kg
05/19/2109:10
05/21/2111:23
10
ND
4740
213
ug/Kg
05/19/2109:10
05/21/2111:23
10
ND
10300
261
ug/Kg
05/19/2109:10
05/21/2111:23
10
ND
15800
1340
ug/Kg
05/19/2109:10
05/21/2111:23
10
ND
3950000
68800
ug/Kg
05/19/2109:10
05/21/2111:23
10
ND
3160
1340
ug/Kg
05/19/2109:10
05/21/2111:23
10
ND
3950000
31600
ug/Kg
i:�
05/19/2109:10
05/21/2111:23
10
Surrogate %Recovery Qualifier
DCAA 68
Method: 8151A - Herbicides (GC) - TCLP
Analyte Result Qualifier
2,4-D ND
Silvex (2,4,5-TP) ND
Surrogate
2,4-Dichlorophenylacetic acid
Method: 6010D - Metals (ICP)
Analyte
Silver
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Limits
10-150
RL MDL Unit
100 1.30 ug/L
20.0 0.0910 ug/L
%Recovery Qualifier Limits
81 30-142
Prepared Analyzed Dil Fac
05119121 09:10 05121121 11:23 10
D Prepared Analyzed Dil Fac
05/19/2108:17 05/20/2118:29 1
05/19/2108:17 05/20/2118:29 1
Prepared Analyzed Dil Fac
0511912108:17 0512012118:29 1
Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
ND
3.65
2.41
mg/Kg
05/18/2109:24
05/19/2112:28
1
ND
7.30
4.16
mg/Kg
05/18/2109:24
05/19/2112:28
1
71.3
7.30
1.24
mg/Kg
05/18/2109:24
05/19/2112:28
1
ND
3.65
0.642
mg/Kg
05/18/2109:24
05/19/2112:28
1
291
7.30
2.26
mg/Kg
05/18/2109:24
05/19/2112:28
1
14.4
7.30
1.61
mg/Kg
05/18/2109:24
05/19/2112:28
1
ND
14.6
6.35
mg/Kg
05/18/2109:24
05/19/2112:28
1
Method: 6010D - Metals (ICP) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Silver
ND
0.0250
0.0100
mg/L
05/26/2115:07
05/27/2113:50
1
Arsenic
ND
0.0500
0.0200
mg/L
05/19/2111:11
05/20/2122:48
1
Barium
ND
5.00
1.05
mg/L
05/19/2111:11
05/20/2122:48
1
Cadmium
ND
0.0250
0.00500
mg/L
05/19/2111:11
05/20/2122:48
1
Chromium
ND
0.0500
0.0100
mg/L
05/19/2111:11
05/20/2122:48
1
Lead
ND
0.0500
0.0100
mg/L
05/19/2111:11
05/20/2122:48
1
Selenium
ND
0.100
0.0200
mg/L
05/19/2111:11
05/20/2122:48
1
Method: 7470A - Mercury (CVAA) - TCLP
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Mercury
ND
1.60
0.560
ug/L
05/19/2108:19
05/19/2117:26
1
Eurofins TestAmerica, Pensacola
Page 12 of 56 5/28/2021

Client Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
F
Job ID: 400-203461-1
Client Sample ID: S1-5 COMPOSITE Lab Sample ID: 400-203461-6
Date Collected: 05/13/21 14:05 Matrix: Solid
Date Received: 05/15/21 10:31 Percent Solids: 12.6
Method: 7471 B - Mercury (CVAA)
Analyte
Result Qualifier
Hg
0.326
General Chemistry
Analyte
Result Qualifier
Percent Solids
12.6
Percent Moisture
87.4
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
0.116
0.0696
mg/Kg
i:� 05/17/21 11:37
05/19/21 11:30
1
•
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
0.01
0.01
%
05/18/2111:12
1
0.01
0.01
%
05/18/2111:12
1
F
Eurofins TestAmerica, Pensacola
Page 13 of 56 5/28/2021

Definitions/Glossary
Client: Shield Engineering Inc Job ID: 400-203461-1
Project/Site: Celadon
Qualifiers
GC/MS VOA
Qualifier Qualifier Description
*3 ISTD response or retention time outside acceptable limits.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
S1+ Surrogate recovery exceeds control limits, high biased.
GC/MS Semi VOA
Qualifier Qualifier Description
LCS and/or LCSD is outside acceptance limits, low biased.
*1 LCS/LCSD RPD exceeds control limits.
B Compound was found in the blank and sample.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
GC Semi VOA
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report.
tt Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Lever'
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRIES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins TestAmerica, Pensacola
Page 14 of 56 5/28/2021

Surrogate Summary
Client: Shield Engineering Inc
Project/Site: Celadon
F
Job ID: 400-203461-1
Method: 8260D - Volatile Organic Compounds by GC/MS
Matrix: Solid
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
BFB DBFM
TOL
Lab Sample ID Client Sample ID (78-118) (81-121)
(80-120)
400-203395-A-1 MS Matrix Spike 98 100
99
400-203395-A-1 MSD Matrix Spike Duplicate 99 100
101
LCS 400-532492/1002 Lab Control Sample 96 101
100
Surrogate Legend
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
Method: 8260D - Volatile Organic Compounds by GC/MS
Matrix: Solid
Prep Type: Total/NA
Lab Sample ID
Client Sample ID
400-203461-6
S1-5 COMPOSITE
400-203461-6
S1-5 COMPOSITE
400-203461-6 MS
S1-5 COMPOSITE
400-203461-6 MSD
400-203476-A-1-B MS
400-203476-A-1-C MSD
LCS 400-532586/1-A
LCS 400-532734/1-A
MB 400-532586/2-A
MB 400-532734/2-A
Surrogate Legend
S1-5 COMPOSITE
Matrix Spike
Matrix Spike Duplicate
Lab Control Sample
Lab Control Sample
Method Blank
Method Blank
Percent Surrogate Recovery (Acceptance Limits)
BFB
DBFM
TOL
DCA
(67-130)
(77-127)
(76-127)
(78-146)
126
93
110
101
137*3
93
113
102
S1+
139 S1+
95
110
108
"3
139 S1+
95
108
100
"3
105
95
104
109
108
95
104
105
100
95
102
109
103
97
101
107
99
94
100
107
101
96
100
110
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
DCA= 1,2-Dichloroethane-d4 (Surr)
Method: 8260D - Volatile Organic Compounds by GC/MS
Matrix: Solid Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
Lab Sample ID Client Sample ID
400-203461-6 S1-5 COMPOSITE
LB 400-532125/1-A Method Blank
Surrogate Legend
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
BFB
DBFM
TOL
(78-118)
(81-121)
(80-120)
94
104
101
99
99
103
0
Eurofins TestAmerica, Pensacola
Page 15 of 56 5/28/2021

Surrogate Summary
Client: Shield Engineering Inc Job ID: 400-203461-1
Project/Site: Celadon
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Matrix: Solid Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
TBP
FBP
2FP
TPHL
PHL
NBZ
Lab Sample ID
Client Sample ID
(10-150)
(27-127)
(25-128)
(24-146)
(29-130)
(15-136)
400-203461-6
S1-5 COMPOSITE
102
50
43
65
54
46
LCS 400-532298/2-A
Lab Control Sample
83
66
63
85
68
67
LCSD 400-532298/3-A
Lab Control Sample Dup
78
64
56
83
65
63
MB 400-532298/1-A
Method Blank
78
69
74
97
76
63
Surrogate Legend
TBP = 2,4,6-Tribromophenol (Surr)
FBP = 2-Fluorobiphenyl (Surr)
2FP = 2-Fluorophenol (Surr)
TPHL = Terphenyl-d14 (Surr)
PHL = Phenol-d5 (Surr)
NBZ = Nitrobenzene-d5 (Surr)
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Matrix: Solid Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
TBP FBP 2FP TPHL PHL NBZ
Lab Sample ID Client Sample ID (10-150) (21-114) (10-105) (13-150) (10-129) (16-127) E:
LCS 400-532706/2-A Lab Control Sample 70 61 49 82 42 68
LCSD 400-532706/3-A Lab Control Sample Dup 66 60 55 85 54 67
Surrogate Legend
TBP = 2,4,6-Tribromophenol (Surr)
FBP = 2-Fluorobiphenyl
2FP = 2-Fluorophenol (Surr)
TPHL = Terphenyl-d14 (Surr)
PHL = Phenol-d5 (Surr)
NBZ = Nitrobenzene-d5 (Surr)
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Matrix: Solid Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
TBP
FBP 2FP
NBZ
PHL
TPHL
Lab Sample ID Client Sample ID
(10-150)
(21-114) (10-105)
(16-127)
(10-129)
(13-150)
400-203461-6 S1-5 COMPOSITE
115
74 57
48
44
95
LB 400-532045/1-G Method Blank
100
69 55
44
43
84
Surrogate Legend
TBP = 2,4,6-Tribromophenol (Surr)
FBP = 2-Fluorobiphenyl
2FP = 2-Fluorophenol (Surr)
NBZ = Nitrobenzene-d5 (Surr)
PHL = Phenol-d5 (Surr)
TPHL = Terphenyl-d14 (Surr)
Eurofins TestAmerica, Pensacola
Page 16 of 56 5/28/2021

Surrogate Summary
Client: Shield Engineering Inc Job ID: 400-203461-1
Project/Site: Celadon
Method: 8081 B - Organochlorine Pesticides (GC)
Matrix: Solid Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
DCBP1
TCX1
Lab Sample ID Client Sample ID
(26-129)
(31-122)
400-203461-6 S1-5 COMPOSITE
37
41
400-203461-6 MS S1-5 COMPOSITE
39
47
400-203461-6 MSD S1-5 COMPOSITE
59
57
LCS 400-532668/2-A Lab Control Sample
78
72
MB 400-532668/1-A Method Blank
74
80
Surrogate Legend
DCBP = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8081 B - Organochlorine Pesticides (GC)
Matrix: Solid
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
DCBP1
TCX1
Lab Sample ID Client Sample ID
(10-130)
(43-130)
LCS 400-532474/3-A Lab Control Sample
80
98
LCSD 400-532474/4-A Lab Control Sample Dup
55
106
Surrogate Legend
DCBP = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8081 B - Organochlorine Pesticides (GC)
Matrix: Solid
Prep Type: TCLP
Percent Surrogate Recovery (Acceptance Limits)
DCBP1
TCX1
Lab Sample ID Client Sample ID
(10-130)
(43-130)
400-203461-6 S1-5 COMPOSITE
66
86
LB 400-532045/1-F Method Blank
48
77
Surrogate Legend
DCBP = DCB Decachlorobiphenyl
TCX = Tetrachloro-m-xylene
Method: 8151A - Herbicides (GC)
Matrix: Solid
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
DCPAA2
Lab Sample ID Client Sample ID
(10-150)
400-203461-6 S1-5 COMPOSITE
68
LCS 400-532379/2-A Lab Control Sample
67
LCSD 400-532379/3-A Lab Control Sample Dup
67
MB 400-532379/1-A Method Blank
59
Surrogate Legend
DCPAA = DCAA
Eurofins TestAmerica, Pensacola
Page 17 of 56 5/28/2021

Surrogate Summary
Client: Shield Engineering Inc
Project/Site: Celadon
Method: 8151A - Herbicides (GC)
Matrix: Solid
Lab Sample ID Client Sample ID
LCS 400-532365/2-A Lab Control Sample
LCSD 400-532365/3-A Lab Control Sample Dup
Surrogate Legend
DCPAA = 2,4-Dichlorophenylacetic acid
F
Job ID: 400-203461-1
Prep Type: Total/NA
Percent Surrogate Recovery (Acceptance Limits)
DCPAA2
(30-142)
87
89
Method: 8151A - Herbicides (GC)
Matrix: Solid
DCPAA2
Lab Sample ID Client Sample ID
(30-142)
400-203461-6 S1-5 COMPOSITE
81
LB 400-532045/1-B Method Blank
91
Surrogate Legend
L DCPAA = 2,4-Dichlorophenylacetic acid
:TCLP
Percent Surrogate Recovery (Acceptance Limits)
Eurofins TestAmerica, Pensacola
Page 18 of 56 5/28/2021

QC Association Summary
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
GC/MS VOA
Leach Batch: 532125
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
TCLP
Solid
1311
LB 400-532125/1-A
Method Blank
TCLP
Solid
1311
Analysis Batch: 532492
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
TCLP
Solid
8260D
532125
LB 400-532125/1-A
Method Blank
TCLP
Solid
8260D
532125
LCS 400-532492/1002
Lab Control Sample
Total/NA
Solid
8260D
Analysis Batch: 532534
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
Total/NA
Solid
8260D
532586
MB 400-532586/2-A
Method Blank
Total/NA
Solid
8260D
532586
LCS 400-532586/1-A
Lab Control Sample
Total/NA
Solid
8260D
532586
Prep Batch: 532586
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
Total/NA
Solid
5035
MB 400-532586/2-A
Method Blank
Total/NA
Solid
5035
LCS 400-532586/1-A
Lab Control Sample
Total/NA
Solid
5035
Analysis Batch: 532709
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
Total/NA
Solid
8260D
532734
MB 400-532734/2-A
Method Blank
Total/NA
Solid
8260D
532734
LCS 400-532734/1-A
Lab Control Sample
Total/NA
Solid
8260D
532734
400-203461-6 MS
S1-5 COMPOSITE
Total/NA
Solid
8260D
532734
400-203461-6 MSD
S1-5 COMPOSITE
Total/NA
Solid
8260D
532734
Prep Batch: 532734
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
400-203461-6
S1-5 COMPOSITE
Total/NA
Solid
5035
MB 400-532734/2-A
Method Blank
Total/NA
Solid
5035
LCS 400-532734/1-A
Lab Control Sample
Total/NA
Solid
5035
400-203461-6 MS
S1-5 COMPOSITE
Total/NA
Solid
5035
400-203461-6 MSD
S1-5 COMPOSITE
Total/NA
Solid
5035
GC/MS Semi VOA
Leach Batch: 532045
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
400-203461-6
S1-5 COMPOSITE
TCLP
Solid
1311
LB 400-532045/1-G
Method Blank
TCLP
Solid
1311
Prep Batch: 532298
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
400-203461-6
S1-5 COMPOSITE
Total/NA
Solid
3546
MB 400-532298/1-A
Method Blank
Total/NA
Solid
3546
LCS 400-532298/2-A
Lab Control Sample
Total/NA
Solid
3546
LCSD 400-532298/3-A
Lab Control Sample Dup
Total/NA
Solid
3546
Eurofins TestAmerica, Pensacola
Page 19 of 56 5/28/2021

QC Association Summary
Client: Shield Engineering Inc
Project/Site: Celadon
GC/MS Semi VOA
Analysis Batch: 532461
Lab Sample ID
400-203461-6
MB 400-532298/1-A
LCS 400-532298/2-A
LCSD 400-532298/3-A
Prep Batch: 532706
Lab Sample ID
400-203461-6
LB 400-532045/1-G
LCS 400-532706/2-A
LCSD 400-532706/3-A
Analysis Batch: 532781
Lab Sample ID
LCS 400-532706/2-A
LCSD 400-532706/3-A
Job ID: 400-203461-1
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
S1-5 COMPOSITE
Total/NA
Solid
8270E
532298
Method Blank
Total/NA
Solid
8270E
532298
Lab Control Sample
Total/NA
Solid
8270E
532298
Lab Control Sample Dup
Total/NA
Solid
8270E
532298
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
S1-5 COMPOSITE
TCLP
Solid
3510C
532045
Method Blank
TCLP
Solid
3510C
532045
Lab Control Sample
Total/NA
Solid
3510C
Lab Control Sample Dup
Total/NA
Solid
3510C
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
Lab Control Sample
Total/NA
Solid
8270E
532706
Lab Control Sample Dup
Total/NA
Solid
8270E
532706
Analysis Batch: 532802
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
400-203461-6 S1-5 COMPOSITE TCLP Solid 8270E 532706
LB 400-532045/1-G Method Blank TCLP Solid 8270E 532706
GC Semi VOA
Leach Batch: 532045
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
400-203461-6
S1-5 COMPOSITE
TCLP
Solid
1311
LB 400-532045/1-B
Method Blank
TCLP
Solid
1311
LB 400-532045/1-F
Method Blank
TCLP
Solid
1311
Prep Batch: 532365
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
400-203461-6
S1-5 COMPOSITE
TCLP
Solid
8151A
LB 400-532045/1-B
Method Blank
TCLP
Solid
8151A
LCS 400-532365/2-A
Lab Control Sample
Total/NA
Solid
8151A
LCSD 400-532365/3-A
Lab Control Sample Dup
Total/NA
Solid
8151A
Prep Batch: 532379
Prep Batch
532045
532045
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
400-203461-6
S1-5 COMPOSITE
Total/NA
Solid
8151A
MB 400-532379/1-A
Method Blank
Total/NA
Solid
8151A
LCS 400-532379/2-A
Lab Control Sample
Total/NA
Solid
8151A
LCSD 400-532379/3-A
Lab Control Sample Dup
Total/NA
Solid
8151A
Prep Batch: 532474
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
400-203461-6
S1-5 COMPOSITE
TCLP
Solid
H-20C 532045
LB 400-532045/1-F
Method Blank
TCLP
Solid
3520C 532045
LCS 400-532474/3-A
Lab Control Sample
Total/NA
Solid
3520C
LCSD 400-532474/4-A
Lab Control Sample Dup
Total/NA
Solid
3520C
Eurofins TestAmerica, Pensacola
Page 20 of 56 5/28/2021

QC Association Summary
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
GC Semi VOA
Analysis Batch: 532547
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
TCLP
Solid
8081B
532474
LB 400-532045/1 -F
Method Blank
TCLP
Solid
8081B
532474
LCS 400-532474/3-A
Lab Control Sample
Total/NA
Solid
8081B
532474
LCSD 400-532474/4-A
Lab Control Sample Dup
Total/NA
Solid
8081B
532474
Analysis Batch: 532597
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
TCLP
Solid
8151A
532365
LB 400-532045/1-B
Method Blank
TCLP
Solid
8151A
532365
MB 400-532379/1-A
Method Blank
Total/NA
Solid
8151A
532379
LCS 400-532365/2-A
Lab Control Sample
Total/NA
Solid
8151A
532365
LCS 400-532379/2-A
Lab Control Sample
Total/NA
Solid
8151A
532379
LCSD 400-532365/3-A
Lab Control Sample Dup
Total/NA
Solid
8151A
532365
LCSD 400-532379/3-A
Lab Control Sample Dup
Total/NA
Solid
8151A
532379
Prep Batch: 532668
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
Total/NA
Solid
3546
MB 400-532668/1-A
Method Blank
Total/NA
Solid
3546
LCS 400-532668/2-A
Lab Control Sample
Total/NA
Solid
3546
400-203461-6 MS
S1-5 COMPOSITE
Total/NA
Solid
3546
400-203461-6 MSD
S1-5 COMPOSITE
Total/NA
Solid
3546
Analysis Batch: 532712
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
Total/NA
Solid
8151A
532379
Analysis Batch: 532719
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
Total/NA
Solid
8081E
532668
M B 400-532668/1 -A
Method Blank
Total/NA
Solid
8081E
532668
LCS 400-532668/2-A
Lab Control Sample
Total/NA
Solid
8081B
532668
400-203461-6 MS
S1-5 COMPOSITE
Total/NA
Solid
8081B
532668
400-203461-6 MSD
S1-5 COMPOSITE
Total/NA
Solid
8081B
532668
Metals
Leach Batch: 532045
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
400-203461-6
S1-5 COMPOSITE
TCLP
Solid
1311
LB 400-532045/1-C
Method Blank
TCLP
Solid
1311
LB 400-532045/1-D
Method Blank
TCLP
Solid
1311
LB 400-532045/1-1
Method Blank
TCLP
Solid
1311
Prep Batch: 532086
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
400-203461-6
S1-5 COMPOSITE
Total/NA
Solid
74716
MB400-532086/14-A
Method Blank
Total/NA
Solid
7471E
LCS 400-532086/15-A
Lab Control Sample
Total/NA
Solid
7471 B
Eurofins TestAmerica, Pensacola
Page 21 of 56 5/28/2021

QC Association Summary
Client: Shield Engineering Inc
Project/Site: Celadon
Metals
Prep Batch: 532212
Job ID: 400-203461-1
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
Total/NA
Solid
3050B
MB 400-532212/1-A
Method Blank
Total/NA
Solid
3050B
LCS 400-532212/2-A
Lab Control Sample
Total/NA
Solid
3050B
Prep Batch: 532366
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
TCLP
Solid
7470A
532045
LB 400-532045/1-C
Method Blank
TCLP
Solid
7470A
532045
LCS 400-532366/15-A
Lab Control Sample
Total/NA
Solid
7470A
Prep Batch: 532421
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
TCLP
Solid
3010A
532045
LB 400-532045/1-D
Method Blank
TCLP
Solid
3010A
532045
LCS 400-532421/2-A
Lab Control Sample
Total/NA
Solid
3010A
Analysis Batch: 532437
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
Total/NA
Solid
7471B
532086
MB400-532086/14-A
Method Blank
Total/NA
Solid
7471B
532086
LCS 400-532086/15-A
Lab Control Sample
Total/NA
Solid
7471B
532086
Analysis Batch: 532562
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
Total/NA
Solid
6010D
532212
MB 400-532212/1-A
Method Blank
Total/NA
Solid
6010D
532212
LCS 400-532212/2-A
Lab Control Sample
Total/NA
Solid
6010D
532212
Analysis Batch: 532563
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
TCLP
Solid
7470A
532366
LB 400-532045/1-C
Method Blank
TCLP
Solid
7470A
532366
LCS 400-532366/15-A
Lab Control Sample
Total/NA
Solid
7470A
532366
Analysis Batch: 532716
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
TCLP
Solid
6010D
532421
LB 400-532045/1-D
Method Blank
TCLP
Solid
6010D
532421
LCS 400-532421/2-A
Lab Control Sample
Total/NA
Solid
6010D
532421
Prep Batch: 533359
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
TCLP
Solid
3010A
532045
LB 400-532045/1-1
Method Blank
TCLP
Solid
3010A
532045
LCS 400-533359/2-A
Lab Control Sample
Total/NA
Solid
3010A
Analysis Batch: 533622
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
400-203461-6
S1-5 COMPOSITE
TCLP
Solid
6010D
533359
LB 400-532045/1-1
Method Blank
TCLP
Solid
6010D
533359
LCS 400-533359/2-A
Lab Control Sample
Total/NA
Solid
6010D
533359
Eurofins TestAmerica, Pensacola
Page 22 of 56 5/28/2021

Client: Shield Engineering Inc
Project/Site: Celadon
General Chemistry
Analysis Batch: 532214
Lab Sample ID Client Sample ID
400-203461-6 S1-5 COMPOSITE
QC Association Summary
Prep Type Matrix
Total/NA Solid
F
Job ID: 400-203461-1
Method Prep Batch
Moisture L
0
Page 23 of 56
Eurofins TestAmerica, Pensacola
5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
Method: 8260D - Volatile Organic Compounds by GC/MS
Lab Sample ID: LCS 400-532492/1002
Matrix: Solid
Analysis Batch: 532492
Analyte
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
LCS LCS
Surrogate %Recovery Qualifier
4-Bromofluorobenzene 96
Dibromofluoromethane 101
Toluene-d8 (Surr) 100
Lab Sample ID: MB 400-532586/2-A
Matrix: Solid
Analysis Batch: 532534
Job ID: 400-203461-1
Spike
Added
LCS LCS
Result Qualifier
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
%Rec. C
Unit D %Rec Limits
50.0
48.82
ug/L
98
70 -130
200
188.8
ug/L
94
61-145
50.0
48.62
ug/L
97
61 -137
50.0
50.73
ug/L
101
70 -130
50.0
47.67
ug/L
95
69 -130
50.0
52.53
ug/L
105
70 -130
50.0
46.61
ug/L
93
69 -130
50.0
35.72
ug/L
71
63-134
50.0
43.59
ug/L
87
65 -130 m
50.0
48.01
ug/L
96
70 -130
50.0
47.10
ug/L
94
59 -136
Limits
78 - 118
81- 121
80 - 120
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 532586
Analyte
MB MB
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
Acetone
ND
25.0
13.0
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Benzene
ND
5.00
0.670
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Bromobenzene
ND
5.00
1.30
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Chlorobromomethane
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Dichlorobromomethane
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Bromoform
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
2-Butanone (MEK)
ND
25.0
6.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
n-Butylbenzene
ND
5.00
0.960
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
sec-Butylbenzene
ND
5.00
0.950
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
tert-Butylbenzene
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Carbon tetrachloride
ND
5.00
1.70
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Chlorobenzene
ND
5.00
0.520
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Chloroethane
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Chloroform
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Chloromethane
ND
5.00
1.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
3-Chloro-1-propene
ND
5.00
1.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
2-Chlorotoluene
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
4-Chlorotoluene
ND
5.00
0.980
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Chlorodibromomethane
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,2-Dibromo-3-Chloropropane
ND
5.00
3.30
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Ethylene Dibromide
ND
5.00
1.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Dibromomethane
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,2-Dichlorobenzene
ND
5.00
0.710
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,3-Dichlorobenzene
ND
5.00
0.950
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,4-Dichlorobenzene
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
trans- 1,4-Dichloro-2-butene
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Page 24 of 56
Eurofins TestAmerica, Pensacola
5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
Job ID: 400-203461-1
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Lab Sample ID: MB 400-532586/2-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532534
Prep Batch: 532586
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
1,1-Dichloroethane
ND
5.00
0.830
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,2-Dichloroethane
ND
5.00
0.820
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
cis-1,2-Dichloroethene
ND
5.00
0.760
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
trans- 1,2-Dichloroethene
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,2-Dichloroethene, Total
ND
5.00
1.40
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,1-Dichloroethene
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,2-Dichloropropane
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,3-Dichloropropane
ND
5.00
1.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
2,2-Dichloropropane
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,1-Dichloropropene
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
cis-1,3-Dichloropropene
ND
5.00
1.20
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
trans- 1,3-Dichloropropene
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Ethylbenzene
ND
5.00
0.610
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Ethyl methacrylate
ND
5.00
1.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Hexachlorobutadiene
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
2-Hexanone
ND
25.0
5.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Isobutyl alcohol
ND
25.0
10.0
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Isopropylbenzene
ND
5.00
0.680
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
4-Isopropyltoluene
ND
5.00
1.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Methylene Chloride
ND
15.0
10.0
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
4-Methyl-2-pentanone (MIBK)
ND
25.0
5.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Methyl tert-butyl ether
ND
5.00
1.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Naphthalene
ND
5.00
2.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
N-Propylbenzene
ND
5.00
0.900
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Styrene
ND
5.00
1.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,1,1,2-Tetrachloroethane
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,1,2,2-Tetrachloroethane
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Tetrachloroethene
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Toluene
ND
5.00
1.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,2,3-Trichlorobenzene
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,2,4-Trichlorobenzene
ND
5.00
2.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,1,1-Trichloroethane
ND
5.00
1.10
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,1,2-Trichloroethane
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Trichloroethene
ND
5.00
1.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Trichlorofluoromethane
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,2,3-Trichloropropane
ND
5.00
3.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,1,2-Trichloro-1,2,2-trifluoroethane
ND
5.00
2.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,2,4-Trimethylbenzene
ND
5.00
1.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
1,3,5-Trimethylbenzene
ND
5.00
0.830
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Vinyl acetate
ND
25.0
9.10
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Vinyl chloride
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
o-Xylene
ND
5.00
1.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
m-Xylene & p-Xylene
ND
5.00
1.30
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Xylenes, Total
ND
10.0
1.90
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Cyclohexane
ND
5.00
0.940
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Methyl acetate
ND
5.00
4.60
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Methylcyclohexane
ND
5.00
1.50
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Tetrahydrofuran
ND
10.0
5.00
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Hexane
ND
5.00
1.20
ug/Kg
05/20/21 08:15
05/20/21 11:02
1
Eurofins TestAmerica, Pensacola
Page 25 of 56 5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Lab Sample ID: MB 400-532586/2-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532534
Prep Batch: 532586
MB
MB
Analyte
Result
Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Ethyl ether
ND
5.00
1.00
ug/Kg
05/20/21 08:15
05/20/21 11:02 1
n-Heptane
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02 1
1,3-Dichloropropene, Total
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02 1
Butadiene
ND
5.00
1.00
ug/Kg
05/20/21 08:15
05/20/21 11:02 1
Dichlorofluoromethane
ND
5.00
2.50
ug/Kg
05/20/21 08:15
05/20/21 11:02 1
2-Methyl-2-propanol
ND
10.0
8.00
ug/Kg
05/20/21 08:15
05/20/21 11:02 1
1,4-Dioxane
ND
500
50.0
ug/Kg
05/20/21 08:15
05/20/21 11:02 1
MB
MB
Surrogate %Recovery
Qualifier
Limits
Prepared
Analyzed Dil Fac
4-Bromofluorobenzene
99
67- 130
05120121 08:15
05120121 11:02 1
Dibromofluoromethane
94
77- 127
05120121 08:15
05120121 11:02 1
Toluene-d8 (Surr)
100
76 - 127
05120121 08:15
05120121 11:02 1
1,2-Dichloroethane-d4 (Surr)
107
78- 146
05120121 08:15
05120121 11:02 1
Lab Sample ID: LCS 400-532586/1-A
Matrix: Solid
Analysis Batch: 532534
Analyte
Spike
Added
LCS LCS
Result Qualifier
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 532586
%Rec.
Unit D %Rec Limits
Acetone
200
214.3
ug/Kg
107
48-160
Benzene
50.0
43.04
ug/Kg
86
65-130
Bromobenzene
50.0
44.16
ug/Kg
88
65 -130
Chlorobromomethane
50.0
42.05
ug/Kg
84
65 -130
Dichlorobromomethane
50.0
43.52
ug/Kg
87
61 -130
Bromoform
50.0
46.80
ug/Kg
94
52 -136
2-Butanone (MEK)
200
198.8
ug/Kg
99
55 -130
n-Butylbenzene
50.0
52.21
ug/Kg
104
66 -130
sec- Butylbenzene
50.0
49.29
ug/Kg
99
67 -130
tert-Butylbenzene
50.0
49.54
ug/Kg
99
67 -130
Carbon tetrachloride
50.0
46.79
ug/Kg
94
60 -130
Chlorobenzene
50.0
44.71
ug/Kg
89
70 -130
Chloroethane
50.0
51.84
ug/Kg
104
55 -134
Chloroform
50.0
42.24
ug/Kg
84
62 -130
Chloromethane
50.0
54.15
ug/Kg
108
49 -136
3-Chloro-1-propene
50.0
41.42
ug/Kg
83
57 -130
2-Chlorotoluene
50.0
47.06
ug/Kg
94
67 -130
4-Chlorotoluene
50.0
48.12
ug/Kg
96
66 -130
Chlorodibromomethane
50.0
45.60
ug/Kg
91
58 -132
1,2-Dibromo-3-Chloropropane
50.0
49.40
ug/Kg
99
49-130
Ethylene Dibromide
50.0
43.70
ug/Kg
87
67 -130
Dibromomethane
50.0
42.16
ug/Kg
84
65 -130
1,2-Dichlorobenzene
50.0
42.39
ug/Kg
85
64 -130
1,3-Dichlorobenzene
50.0
43.45
ug/Kg
87
66 -130
1,4-Dichlorobenzene
50.0
41.68
ug/Kg
83
65 -130
trans- 1,4-Dichloro-2-butene
50.0
57.02
ug/Kg
114
45-137
1,1-Dichloroethane
50.0
44.99
ug/Kg
90
59-130
1,2-Dichloroethane
50.0
45.35
ug/Kg
91
62 -130
cis-1,2-Dichloroethene
50.0
48.98
ug/Kg
98
53 -135
Eurofins TestAmerica, Pensacola
Page 26 of 56 5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
Method: 8260D - Volatile Organic Compounds by GC/MS (Continued)
Lab Sample ID: LCS 400-532586/1-A
Matrix: Solid
Analysis Batch: 532534
Analyte
trans-1,2-Dichloroethene
1,2-Dichloroethene, Total
1,1-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachlorobutadiene
2-Hexanone
Isobutyl alcohol
Isopropylbenzene
4-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthalene
N-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,1,2-Trichloro-1,2,2-trifluoroetha
ne
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
o-Xylene
m-Xylene & p-Xylene
Xylenes, Total
Cyclohexane
Methyl acetate
Methylcyclohexane
Tetrahydrofuran
Hexane
Ethyl ether
n-Heptane
Client Sample ID
Spike
Added
LCS LCS
Result Qualifier
Unit
D %Rec
50.0
37.49
ug/Kg
75
100
86.47
ug/Kg
86
50.0
41.01
ug/Kg
82
50.0
49.14
ug/Kg
98
50.0
43.17
ug/Kg
86
50.0
48.85
ug/Kg
98
50.0
45.51
ug/Kg
91
50.0
44.41
ug/Kg
89
50.0
47.18
ug/Kg
94
50.0
46.63
ug/Kg
93
50.0
49.24
ug/Kg
98
50.0
44.38
ug/Kg
89
200
224.0
ug/Kg
112
1250
1642
ug/Kg
131
50.0
48.84
ug/Kg
98
50.0
50.50
ug/Kg
101
50.0
37.18
ug/Kg
74
200
213.3
ug/Kg
107
50.0
38.89
ug/Kg
78
50.0
51.12
ug/Kg
102
50.0
49.72
ug/Kg
99
50.0
46.10
ug/Kg
92
50.0
45.72
ug/Kg
91
50.0
43.92
ug/Kg
88
50.0
39.40
ug/Kg
79
50.0
43.96
ug/Kg
88
50.0
43.39
ug/Kg
87
50.0
43.09
ug/Kg
86
50.0
43.61
ug/Kg
87
50.0
44.77
ug/Kg
90
50.0
43.23
ug/Kg
86
50.0
46.22
ug/Kg
92
50.0
40.92
ug/Kg
82
50.0
40.31
ug/Kg
81
Job ID: 400-203461-1
Lab Control Sample
Prep Type: Total/NA
Prep Batch: 532586
%Rec.
Limits
58-134
70-130
55-137
64-130
67-130
51 -132
65-130
61 -130
60-130
70-130
62-130
62-133
57-131
44-136
70-130
68-130
57-132
58-130
63-130
45-144
67-130
68-130
65-130
60-131
67-130
70-130
58-135
56-138
63-130
65-130
65-130
61 -136
60-130
47-143
50.0
48.17
ug/Kg
96
66 -130
50.0
48.74
ug/Kg
97
67 -130
100
94.35
ug/Kg
94
24 -160
50.0
59.09
ug/Kg
118
52 -132
50.0
47.50
ug/Kg
95
70-130
50.0
47.61
ug/Kg
95
70 -130
100
95.11
ug/Kg
95
70-130
50.0
42.58
ug/Kg
85
61-130
100
101.0
ug/Kg
101
49-139
50.0
44.26
ug/Kg
89
64 -130
100
106.0
ug/Kg
106
52-132
50.0
47.34
ug/Kg
95
57 -132
50.0
44.23
ug/Kg
88
58 -130
50.0
52.70
ug/Kg
105
61-130
Page 27 of 56
Eurofins TestAmerica, Pensacola
5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
Job ID: 400-203461-1
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Lab Sample ID: LCS 400-532586/1-A
Client Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532534
Prep Batch: 532586
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
1,3-Dichloropropene, Total
100
91.59
ug/Kg
92
60 -140
Butadiene
50.0
52.59
ug/Kg
105
52 -132
Dichlorofluoromethane
50.0
55.42
ug/Kg
111
57 -134
2-Methyl-2-propanol
500
532.9
ug/Kg
107
33 -130
1,4-Dioxane
1000
1082
ug/Kg
108
41-148
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
Toluene-d8 (Surr)
1,2-Dichloroethane-d4 (Surr)
LCS LCS
%Recovery Qualifier
Limits
100
67-130
95
77-127
102
76-127
109
78-146
Lab Sample ID: MB 400-532734/2-A
Matrix: Solid
Analysis Batch: 532709
Analyte
Bromomethane
Carbon disulfide
Dichlorodifluoromethane
lodomethane
MB MB
Result Qualifier
RL
MDL
Unit
ND
5.00
2.50
ug/Kg
ND
5.00
2.50
ug/Kg
ND
5.00
1.30
ug/Kg
ND
5.00
3.40
ug/Kg
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 532734
D Prepared
Analyzed Dil Fac
05/21 /21 08:15
05/21 /21 10:21 1
05/21 /21 08:15
05/21 /21 10:21 1
05/21 /21 08:15
05/21 /21 10:21 1
05/21 /21 08:15
05/21 /21 10:21 1
MB MB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
4-Bromofluorobenzene
101
67- 130
05121121 08:15
05121121 10:21 1
Dibromofluoromethane
96
77- 127
05121121 08:15
05121121 10:21 1
Toluene-d8 (Surr)
100
76 - 127
05121121 08:15
05121121 10:21 1
1,2-Dichloroethane-d4 (Surr)
110
78- 146
05121121 08:15
05121121 10:21 1
Lab Sample ID: LCS 400-532734/1-A
Client
Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532709
Prep Batch: 532734
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Bromomethane
50.0
35.98
ug/Kg
72
12 -160
Carbon disulfide
50.0
33.13
ug/Kg
66
46 -141
Dichlorodifluoromethane
50.0
35.92
ug/Kg
72
34 -143
lodomethane
50.0
34.67
ug/Kg
69
12 -160
LCS
LCS
Surrogate
%Recovery
Qualifier
Limits
4-Bromofluorobenzene
103
67 - 130
Dibromofluoromethane
97
77 - 127
Toluene-d8 (Surr)
101
76 - 127
1,2-Dichloroethane-d4 (Surr)
107
78- 146
Eurofins TestAmerica, Pensacola
Page 28 of 56 5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Lab Sample ID: 400-203461-6 MS
Matrix: Solid
Analysis Batch: 532709
Analyte
Bromomethane
Carbon disulfide
Dichlorodifluoromethane
lodomethane
Surrogate
Sample Sample
Result Qualifier
ND
ND
ND
ND
MS MS
%Recovery Qualifier
4-Bromofluorobenzene 139 S1+ *3
Dibromofluoromethane 95
Toluene-d8 (Surr) 110
1,2-Dichloroethane-d4 (Surr) 108
Lab Sample ID: 400-203461-6 MSD
Matrix: Solid
Analysis Batch: 532709
Analyte
Sample
Result
Sample
Qualifier
Bromomethane
ND
Carbon disulfide
ND
Dichlorodifluoromethane
ND
lodomethane
ND
MSD
MSD
Surrogate
%Recovery
Qualifier
4-Bromofluorobenzene
139
S1+ *3
Dibromofluoromethane
95
Toluene-d8 (Surr)
108
1,2-Dichloroethane-d4 (Surr)
100
Lab Sample ID: LB 400-532125/1-A
Matrix: Solid
Analysis Batch: 532492
Analyte
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
Surrogate
4-Bromofluorobenzene
Dibromofluoromethane
LB
Result
LB
Qualifier
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
LB
LB
%Recovery
Qualifier
99
99
Spike
Added
MS
Result
MS
Qualifier
Unit
402
359.7
ug/Kg
402
203.4
ug/Kg
402
228.3
ug/Kg
402
157.0
ug/Kg
Limits
67-130
77-127
76-127
78-146
Spike
MSD
MSD
Added
Result
Qualifier
Unit
400
243.9
ug/Kg
400
183.4
ug/Kg
400
219.3
ug/Kg
400
168.4
ug/Kg
Limits
67-130
77-127
76-127
78- 146
F
Job ID: 400-203461-1
Client Sample ID: S1-5 COMPOSITE
Prep Type: Total/NA
Prep Batch: 532734
%Rec.
D
%Rec
Limits
3:�
89
10-150
51
29-141
57
21 -146
#
39
10-150
F
F
Client Sample
ED
ID: S1-5 COMPOSITE
Prep Type: Total/NA
Prep Batch: 532734
%Rec. RPD
D
%Rec
Limits RPD Limit
F—
61
10-150 38 47
3:�
46
29-141 10 39
3:�
55
21-146 4 46
42
10-150 7 52
Client Sample ID: Method Blank
Prep Type: TCLP
RL
MDL
Unit
D Prepared Analyzed
Dil Fac
5.00
0.340
ug/L
05/19/2120:03
1
25.0
2.60
ug/L
05/19/2120:03
1
5.00
0.500
ug/L
05/19/2120:03
1
5.00
0.500
ug/L
05/19/2120:03
1
5.00
0.600
ug/L
05/19/2120:03
1
5.00
0.640
ug/L
05/19/2120:03
1
5.00
0.500
ug/L
05/19/2120:03
1
5.00
0.500
ug/L
05/19/2120:03
1
5.00
0.580
ug/L
05/19/2120:03
1
5.00
0.500
ug/L
05/19/2120:03
1
5.00
0.500
ug/L
05/19/2120:03
1
Limits
Prepared Analyzed
Dil Fac
78 - 118
05119121 20: 03
1
81- 121
05119121 20:03
1
Eurofins TestAmerica, Pensacola
Page 29 of 56 5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Method: 8260D - Volatile Organic Compounds by GUMS (Continued)
Lab Sample ID: LB 400-532125/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type:
TCLP
Analysis Batch: 532492
LB LB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed
Dil Fac
Toluene-d8 (Surr)
103
80 - 120
05119121 20:03
1
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Lab Sample ID: MB 400-532298/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532461
Prep Batch: 532298
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed
Dil Fac
1,1'-Biphenyl
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
2,4-Dichlorophenol
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
2,4-Dimethylphenol
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
2,4-Dinitrophenol
ND
990
290
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
2,4-Dinitrotoluene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
2-Chlorophenol
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
2,4,5-Trichlorophenol
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
2-Chloronaphthalene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
2,4,6-Trichlorophenol
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
2-Methylnaphthalene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
2-Methylphenol
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
2-Nitroaniline
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
2-Nitrophenol
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
3 & 4 Methylphenol
ND
660
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
3,3'-Dichlorobenzidine
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
3-Nitroaniline
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
4,6-Dinitro-2-methylphenol
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
4-Bromophenyl phenyl ether
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
4-Chloro-3-methylphenol
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
4-Chloroaniline
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
4-Chlorophenyl phenyl ether
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
4-Nitroaniline
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Acenaphthene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Acenaphthylene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Acetophenone
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Anthracene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Benzo[a]anthracene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Benzo[a]pyrene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Benzo[b]fluoranthene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Benzo[g,h,i]perylene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Benzo[k]fluoranthene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Bis(2-chloroethoxy)methane
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Bis(2-chloroethyl)ether
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Bis(2-ethylhexyl) phthalate
51.28 J
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Chrysene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Dibenz(a,h)anthracene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Dibenzofuran
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Di-n-butyl phthalate
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Diethyl phthalate
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Dimethyl phthalate
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Eurofins TestAmerica, Pensacola
Page 30 of 56 5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
(Continued)
Lab Sample ID: MB 400-532298/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532461
Prep Batch: 532298
MB
MB
Analyte Result
Qualifier RL
MDL
Unit
D
Prepared
Analyzed
Dil Fac
Di-n-octyl phthalate
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Fluoranthene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Fluorene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Hexachlorobenzene
ND
330
100
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Hexachlorobutadiene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Hexachlorocyclopentadiene
ND
330
66.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Hexachloroethane
ND
330
100
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Indeno[1,2,3-cd]pyrene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Isophorone
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Naphthalene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
m
Nitrobenzene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
N-Nitrosodiphenylamine
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
N-Nitrosodi-n-propylamine
ND
330
110
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Pentachlorophenol
ND
660
66.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Phenanthrene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Phenol
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Pyrene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Butyl benzyl phthalate
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
bis (2-chloroisopropyl) ether
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Carbazole
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
2,6-Dinitrotoluene
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
4-Nitrophenol
ND
330
110
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Atrazine
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Benzaldehyde
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
Caprolactam
ND
330
33.0
ug/Kg
05/18/21 14:27
05/19/21 19:05
1
MB
MB
Surrogate %Recovery
Qualifier Limits
Prepared
Analyzed
Dil Fac
2,4,6-Tribromophenol (Surr)
78
10- 150
05118121 14:27
05119121 19:05
1
2-Fluorobiphenyl (Surr)
69
27- 127
05118121 14:27
05119121 19:05
1
2-Fluorophenol (Surr)
74
25 - 128
05118121 14:27
05119121 19:05
1
Terphenyl-d14 (Surr)
97
24- 146
05118121 14:27
05119121 19:05
1
Phenol-d5 (Surr)
76
29 - 130
05118121 14:27
05119121 19:05
1
Nitrobenzene-d5 (Surr)
63
15 - 136
05118121 14:27
05119121 19:05
1
Lab Sample ID: LCS 400-532298/2-A
Client Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532461
Prep Batch: 532298
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
1,1'-Biphenyl
2000
1310
ug/Kg
66
56-120
2,4-Dichlorophenol
2000
1475
ug/Kg
74
56 -120
2,4-Dimethylphenol
2000
1484
ug/Kg
74
54 -120
2,4-Dinitrophenol
4000
4283
ug/Kg
107
10 -138
2,4-Dinitrotoluene
2000
1513
ug/Kg
76
59-133
2-Chlorophenol
2000
1477
ug/Kg
74
52 -120
2,4,5-Trichlorophenol
2000
1542
ug/Kg
77
53 -133
2-Chloronaphthalene
2000
1261
ug/Kg
63
55 -120
2,4,6-Trichlorophenol
2000
1446
ug/Kg
72
51 -125
Eurofins TestAmerica, Pensacola
Page 31 of 56 5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
Job ID: 400-203461-1
Method: 8270E - Semivolatile Organic Compounds (GUMS) (Continued)
Lab Sample ID: LCS 400-532298/2-A
Client
Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532461
Prep Batch: 532298
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
2-Methyl naphtha lene
2000
1388
ug/Kg
69
40 -120
2-Methylphenol
2000
1593
ug/Kg
80
51 -123
2-Nitroaniline
2000
1365
ug/Kg
68
55 -129
2-Nitrophenol
2000
1581
ug/Kg
79
53 -120
3 & 4 Methylphenol
2000
1495
ug/Kg
75
47 -123
3,3'-Dichlorobenzidine
2670
2158
ug/Kg
81
42 -120
3-Nitroaniline
2000
1243
ug/Kg
62
45 -120
4,6-Dinitro-2-methylphenol
4000
3967
ug/Kg
99
35 -135
4-Bromophenyl phenyl ether
2000
1599
ug/Kg
80
51 -120
4-Chloro-3-methylphenol
2000
1629
ug/Kg
81
57 -124
4-Chloroaniline
2000
1286
ug/Kg
64
34 -120
4-Chlorophenyl phenyl ether
2000
1445
ug/Kg
72
56 -120
4-Nitroaniline
2000
1084
ug/Kg
54
52 -126
Acenaphthene
2000
1421
ug/Kg
71
50-120
Acenaphthylene
2000
1482
ug/Kg
74
50-120
Acetophenone
2000
1222
ug/Kg
61
52-120
Anthracene
2000
1702
ug/Kg
85
52-120
Benzo[a]anthracene
2000
1676
ug/Kg
84
55 -120
Benzo[a]pyrene
2000
1786
ug/Kg
89
54-120
Benzo[k]fluoranthene
2000
1737
ug/Kg
87
55 -120
Benzo[g,h,i]perylene
2000
1795
ug/Kg
90
45-120
Benzo[k]fluoranthene
2000
1837
ug/Kg
92
52 -120
Bis(2-chloroethoxy)methane
2000
1121
ug/Kg
56
52 -120
Bis(2-chloroethyl)ether
2000
1169
ug/Kg
58
50 -120
Bis(2-ethylhexyl) phthalate
2000
1919
ug/Kg
96
58 -158
Chrysene
2000
1742
ug/Kg
87
54-120
Dibenz(a,h)anthracene
2000
1682
ug/Kg
84
49-120
Dibenzofuran
2000
1391
ug/Kg
70
58 -120
Di-n-butyl phthalate
2000
1873
ug/Kg
94
64 -122
Diethyl phthalate
2000
1812
ug/Kg
91
56 -128
Dimethyl phthalate
2000
1508
ug/Kg
75
58 -120
Di-n-octyl phthalate
2000
1951
ug/Kg
98
57 -137
Fluoranthene
2000
1593
ug/Kg
80
49 -120
Fluorene
2000
1615
ug/Kg
81
47-120
Hexachlorobenzene
2000
1801
ug/Kg
90
49-127
Hexachlorobutadiene
2000
1375
ug/Kg
69
43 -120
Hexachlorocyclopentadiene
2000
1202
ug/Kg
60
10 -140
Hexachloroethane
2000
1303
ug/Kg
65
45-120
Indeno[1,2,3-cd]pyrene
2000
1646
ug/Kg
82
47-120
Isophorone
2000
1201
ug/Kg
60
50-120
Naphthalene
2000
1344
ug/Kg
67
41 -120
Nitrobenzene
2000
1110
ug/Kg
55
50-120
N-Nitrosodiphenylamine
1980
1502
ug/Kg
76
54 -120
N-Nitrosodi-n-propylamine
2000
1336
ug/Kg
67
48-120
Pentachlorophenol
4000
3221
ug/Kg
81
32-131
Phenanthrene
2000
1713
ug/Kg
86
50-120
Phenol
2000
1435
ug/Kg
72
51-120
Pyrene
2000
1608
ug/Kg
80
54-120
Butyl benzyl phthalate
2000
1839
ug/Kg
92
58 -126
Eurofins TestAmerica, Pensacola
Page 32 of 56 5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 400-532298/2-A
Client
Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532461
Prep Batch: 532298
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
bis (2-chloroisopropyl) ether
2000
1091
ug/Kg
55
34 -120
Carbazole
2000
1787
ug/Kg
89
61 -132
2,6-Dinitrotoluene
2000
1469
ug/Kg
73
57-123
4-Nitrophenol
4000
3820
ug/Kg
96
38 -133
Atrazine
2000
1754
ug/Kg
88
44 -120
Benzaldehyde
2000
1067
ug/Kg
53
20-120
Caprolactam
2000
1213
ug/Kg
61
53 -127
LCS LCS
Surrogate %Recovery Qualifier
Limits
2,4,6-Tribromophenol (Surr) 83
10- 150
2-Fluorobiphenyl (Surr) 66
27- 127
2-Fluorophenol (Surr) 63
25 - 128
Terphenyl-d14 (Surr) 85
24 - 146
Phenol-d5 (Surr) 68
29 - 130
Nitrobenzene-d5 (Surr) 67
15 - 136
Lab Sample ID: LCSD 400-532298/3-A
Client Sample
ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532461
Prep Batch: 532298
Spike
LCSD
LCSD
%Rec.
RPD
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
RPD
Limit
1,1'-Biphenyl
2000
1224
ug/Kg
61
56-120
7
30
2,4-Dichlorophenol
2000
1401
ug/Kg
70
56 -120
5
30
2,4-Dimethylphenol
2000
1402
ug/Kg
70
54 -120
6
30
2,4-Dinitrophenol
4000
4003
ug/Kg
100
10 -138
7
30
2,4-Dinitrotoluene
2000
1492
ug/Kg
75
59-133
1
30
2-Chlorophenol
2000
1377
ug/Kg
69
52-120
7
30
2,4,5-Trichlorophenol
2000
1514
ug/Kg
76
53 -133
2
30
2-Chloronaphthalene
2000
1210
ug/Kg
60
55 -120
4
30
2,4,6-Trichlorophenol
2000
1399
ug/Kg
70
51 -125
3
30
2-Methyl naphtha lene
2000
1292
ug/Kg
65
40 -120
7
30
2-Methylphenol
2000
1424
ug/Kg
71
51 -123
11
30
2-Nitroaniline
2000
1348
ug/Kg
67
55 -129
1
30
2-Nitrophenol
2000
1491
ug/Kg
75
53 -120
6
30
3 & 4 Methylphenol
2000
1390
ug/Kg
69
47 -123
7
30
3,3'-Dichlorobenzidine
2670
1939
ug/Kg
73
42 -120
11
30
3-Nitroaniline
2000
1235
ug/Kg
62
45 -120
1
30
4,6-Dinitro-2-methyl phenol
4000
3715
ug/Kg
93
35 -135
7
30
4-Bromophenyl phenyl ether
2000
1536
ug/Kg
77
51 -120
4
30
4-Chloro-3-methylphenol
2000
1596
ug/Kg
80
57 -124
2
30
4-Chloroaniline
2000
1257
ug/Kg
63
34 -120
2
30
4-Chlorophenyl phenyl ether
2000
1397
ug/Kg
70
56 -120
3
30
4-Nitroaniline
2000
1099
ug/Kg
55
52 -126
1
30
Acenaphthene
2000
1345
ug/Kg
67
50-120
6
30
Acenaphthylene
2000
1399
ug/Kg
70
50-120
6
30
Acetophenone
2000
1163
ug/Kg
58
52-120
5
30
Anthracene
2000
1675
ug/Kg
84
52-120
2
30
Benzo[a]anthracene
2000
1632
ug/Kg
82
55 -120
3
30
Eurofins TestAmerica, Pensacola
Page 33 of 56 5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Method: 8270E - Semivolatile Organic Compounds (GUMS) (Continued)
Lab Sample ID: LCSD 400-532298/3-A
Client Sample
ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532461
Prep Batch: 532298
Spike
LCSD
LCSD
%Rec.
RPD
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
RPD
Limit
Benzo[a]pyrene
2000
1760
ug/Kg
88
54-120
1
30
Benzo[b]fluoranthene
2000
1716
ug/Kg
86
55 -120
1
30
Benzo[g,h,i]perylene
2000
1622
ug/Kg
81
45-120
10
30
Benzo[k]fluoranthene
2000
1798
ug/Kg
90
52 -120
2
30
Bis(2-chloroethoxy)methane
2000
1071
ug/Kg
54
52 -120
5
30
Bis(2-chloroethyl)ether
2000
988.7
"- ug/Kg
49
50 -120
17
30
Bis(2-ethylhexyl) phthalate
2000
1818
ug/Kg
91
58 -158
5
30
Chrysene
2000
1684
ug/Kg
84
54-120
3
30
Dibenz(a,h)anthracene
2000
1566
ug/Kg
78
49-120
7
30
Dibenzofuran
2000
1317
ug/Kg
66
58 -120
5
30
Di-n-butyl phthalate
2000
1772
ug/Kg
89
64 -122
6
30
Diethyl phthalate
2000
1738
ug/Kg
87
56 -128
4
30
Dimethyl phthalate
2000
1442
ug/Kg
72
58 -120
5
30
Di-n-octyl phthalate
2000
1864
ug/Kg
93
57 -137
5
30
Fluoranthene
2000
1516
ug/Kg
76
49 -120
5
30
Fluorene
2000
1549
ug/Kg
77
47-120
4
30
Hexachlorobenzene
2000
1748
ug/Kg
87
49-127
3
30
Hexachlorobutadiene
2000
1307
ug/Kg
65
43 -120
5
30
Hexachlorocyclopentadiene
2000
1194
ug/Kg
60
10 -140
1
30
Hexachloroethane
2000
1244
ug/Kg
62
45 -120
5
30
Indeno[1,2,3-cd]pyrene
2000
1514
ug/Kg
76
47-120
8
30
Isophorone
2000
1128
ug/Kg
56
50-120
6
30
Naphthalene
2000
1267
ug/Kg
63
41 -120
6
30
Nitrobenzene
2000
1026
ug/Kg
51
50-120
8
30
N-Nitrosodiphenylamine
1980
1472
ug/Kg
74
54 -120
2
30
N-Nitrosodi-n-propylamine
2000
1294
ug/Kg
65
48-120
3
30
Pentachlorophenol
4000
3063
ug/Kg
77
32-131
5
30
Phenanthrene
2000
1667
ug/Kg
83
50-120
3
30
Phenol
2000
1280
ug/Kg
64
51-120
11
30
Pyrene
2000
1580
ug/Kg
79
54-120
2
30
Butyl benzyl phthalate
2000
1783
ug/Kg
89
58 -126
3
30
bis (2-chloroisopropyl) ether
2000
1010
ug/Kg
51
34 -120
8
30
Carbazole
2000
1741
ug/Kg
87
61 -132
3
30
2,6-Dinitrotoluene
2000
1414
ug/Kg
71
57-123
4
30
4-Nitrophenol
4000
3753
ug/Kg
94
38-133
2
30
Atrazine
2000
1717
ug/Kg
86
44 -120
2
30
Benzaldehyde
2000
902.6
ug/Kg
45
20-120
17
30
Caprolactam
2000
1203
ug/Kg
60
53 -127
1
30
LCSD LCSD
Surrogate
%Recovery Qualifier
Limits
2,4,6-Tribromophenol (Surr)
78
10- 150
2-Fluorobiphenyl (Surr)
64
27 - 127
2-Fluorophenol (Surr)
56
25 - 128
Terphenyl-d14 (Surr)
83
24 -146
Phenol-d5 (Surr)
65
29 -130
Nitrobenzene-d5 (Surr)
63
15 -136
Eurofins TestAmerica, Pensacola
Page 34 of 56 5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 400-532706/2-A
Client
Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532781
Prep Batch: 532706
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits
2,4-Dinitrotoluene
120
80.44
ug/L
67
35-136
2,4,5-Trichlorophenol
120
84.35
ug/L
70
30 -144
2,4,6-Trichlorophenol
120
78.07
ug/L
65
27 -147
2-Methylphenol
120
78.95
ug/L
66
34 -124
Pyridine
240
50.84
ug/L
21
10 - 82
3 & 4 Methylphenol
120
77.24
ug/L
64
32 -122
Hexachlorobenzene
120
99.50
ug/L
83
10 -150
Hexachlorobutadiene
120
67.66
ug/L
56
10 -150
Hexachloroethane
120
65.56
ug/L
55
10 -127
m
Nitrobenzene
120
68.11
ug/L
57
29 -120
Pentachlorophenol
240
135.0
ug/L
56
19 -150
LCS LCS
Surrogate
%Recovery Qualifier
Limits
2,4,6-Tribromophenol (Surr)
70
10- 150
2-Fluorobiphenyl
61
21- 114
E:
2-Fluorophenol (Surr)
49
10 - 105
Terphenyl-d 14 (Surr)
82
13 - 150
Phenol-d5 (Surr)
42
10 - 129
Nitrobenzene-d5 (Surr)
68
16 - 127
Lab Sample ID: LCSD 400-532706/3-A
Client Sample
ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532781
Prep Batch: 532706
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier Unit
D %Rec
Limits RPD Limit
2,4-Dinitrotoluene
120
78.03
ug/L
65
35-136 3 40
2,4,5-Trichlorophenol
120
79.18
ug/L
66
30 -144 6 40
2,4,6-Trichlorophenol
120
74.96
ug/L
62
27 -147 4 40
2-Methylphenol
120
80.73
ug/L
67
34 -124 2 40
Pyridine
240
ND
'-*1 ug/L
0.09
10-82 198 40
3 & 4 Methylphenol
120
81.11
ug/L
68
32 -122 5 40
Hexachlorobenzene
120
97.27
ug/L
81
10 -150 2 40
Hexachlorobutadiene
120
67.46
ug/L
56
10 -150 0 40
Hexachloroethane
120
67.19
ug/L
56
10 -127 2 40
Nitrobenzene
120
65.31
ug/L
54
29 -120 4 40
Pentachlorophenol
240
120.9
ug/L
50
19 -150 11 40
LCSD LCSD
Surrogate
%Recovery Qualifier
Limits
2,4,6-Tribromophenol (Surr)
66
10- 150
2-Fluorobiphenyl
60
21 - 114
2-Fluorophenol (Surr)
55
10 - 105
Terphenyl-d14 (Surr)
85
13- 150
Phenol-d5 (Surr)
54
10- 129
Nitrobenzene-d5 (Surr)
67
16 - 127
Eurofins TestAmerica, Pensacola
Page 35 of 56 5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LB 400-532045/1-G
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 532802
Prep Batch: 532706
LB LB
Analyte Result Qualifier
RL
MDL
Unit
D
Prepared
Analyzed Dil Fac
2,4-Dinitrotoluene
ND
14.5
2.03
ug/L
05/21/21 07:30
05/21/21 19:30 1
2,4,5-Trichlorophenol
ND
14.5
1.60
ug/L
05/21/21 07:30
05/21/21 19:30 1
2,4,6-Trichlorophenol
ND
14.5
2.32
ug/L
05/21/21 07:30
05/21/21 19:30 1
2-Methylphenol
ND
14.5
2.18
ug/L
05/21/21 07:30
05/21/21 19:30 1
Pyridine
ND
14.5
6.38
ug/L
05/21/21 07:30
05/21/21 19:30 1
3 & 4 Methylphenol
ND
29.0
2.18
ug/L
05/21/21 07:30
05/21/21 19:30 1
Hexachlorobenzene
ND
14.5
1.74
ug/L
05/21/21 07:30
05/21/21 19:30 1
Hexachlorobutadiene
ND
14.5
2.47
ug/L
05/21/21 07:30
05/21/21 19:30 1
Hexachloroethane
ND
14.5
3.48
ug/L
05/21/21 07:30
05/21/21 19:30 1 m
Nitrobenzene
ND
14.5
2.32
ug/L
05/21/21 07:30
05/21/21 19:30 1
Pentachlorophenol
ND
29.0
5.37
ug/L
05/21/21 07:30
05/21/21 19:30 1
LB LB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
2,4,6-Tribromophenol (Surr)
100
10- 150
05121121 07:30
05121121 19:30 1
2-Fluorobiphenyl
69
21- 114
05121121 07:30
05121121 19:30 1
2-Fluorophenol (Surr)
55
10 - 105
05121121 07:30
05121121 19:30 1
Terphenyl-d14 (Surr)
84
13- 150
05121121 07:30
05121121 19:30 1
Phenol-d5 (Surr)
43
10 - 129
05121121 07:30
05121121 19:30 1
Nitrobenzene-d5 (Surr)
44
16 - 127
05121121 07:30
05121121 19:30 1
Method: 8081 B - Organochlorine
Pesticides (GC)
Lab Sample ID: LCS 400-532474/3-A
Client Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532547
Prep Batch: 532474
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Methoxychlor
2.00
1.643
ug/L
82
36 -161
Endrin
2.00
1.733
ug/L
87
36 -173
gamma-BHC (Lindane)
2.00
1.961
ug/L
98
29 -160
Heptachlor
2.00
1.689
ug/L
84
31 -172
Heptachlor epoxide
2.00
2.076
ug/L
104
38 -156
LCS
LCS
Surrogate %Recovery
Qualifier
Limits
DCB Decachlorobiphenyl 80
10- 130
Tetrachloro-m-xylene 98
43 - 130
Lab Sample ID: LCSD 400-532474/4-A
Client Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532547
Prep Batch: 532474
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits RPD Limit
Methoxychlor
2.00
1.505
ug/L
75
36 -161 9 40
Endrin
2.00
1.624
ug/L
81
36 -173 7 40
gamma-BHC (Lindane)
2.00
1.934
ug/L
97
29 -160 1 40
Heptachlor
2.00
1.540
ug/L
77
31 -172 9 40
Heptachlor epoxide
2.00
2.035
ug/L
102
38 -156 2 40
Eurofins TestAmerica, Pensacola
Page 36 of 56 5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Method: 8081 B - Organochlorine
Pesticides (GC) (Continued)
Lab Sample ID: LCSD 400-532474/4-A
Client Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532547
Prep Batch: 532474
LCSD
LCSD
C
Surrogate %Recovery
Qualifier
Limits
DCB Decachlorobiphenyl 55
10- 130
Tetrachloro-m-xylene 106
43 - 130
Lab Sample ID: MB 400-532668/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532719
Prep Batch: 532668
MB MB
Analyte Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
4,4'-DDD
ND
1.70
0.190
ug/Kg
05/20/21 15:04
05/21/21 11:53 1 m
4,4'-DDE
ND
1.70
0.270
ug/Kg
05/20/21 15:04
05/21/21 11:53 1
4,4'-DDT
ND
1.70
0.770
ug/Kg
05/20/21 15:04
05/21/21 11:53 1
Aldrin
ND
1.70
0.610
ug/Kg
05/20/21 15:04
05/21/21 11:53 1
alpha-BHC
ND
1.70
0.240
ug/Kg
05/20/21 15:04
05/21/21 11:53 1
beta-BHC
ND
1.70
0.500
ug/Kg
05/20/21 15:04
05/21/21 11:53 1
Chlordane (technical)
ND
17.0
2.50
ug/Kg
05/20/21 15:04
05/21/21 11:53 1
delta-BHC
ND
1.70
0.320
ug/Kg
05/20/21 15:04
05/21/21 11:53 1
Dieldrin
ND
1.70
0.360
ug/Kg
05/20/21 15:04
05/21/21 11:53 1
Endosulfan I
ND
1.70
0.210
ug/Kg
05/20/21 15:04
05/21/21 11:53 1
Endosulfan 11
ND
1.70
0.230
ug/Kg
05/20/21 15:04
05/21/21 11:53 1
Endosulfan sulfate
ND
1.70
0.210
ug/Kg
05/20/21 15:04
05/21/21 11:53 1
Endrin
ND
1.70
0.190
ug/Kg
05/20/21 15:04
05/21/21 11:53 1
Endrin aldehyde
ND
1.70
0.290
ug/Kg
05/20/21 15:04
05/21/21 11:53 1
gamma-BHC (Lindane)
ND
1.70
0.220
ug/Kg
05/20/21 15:04
05/21/21 11:53 1
Heptachlor
ND
1.70
0.240
ug/Kg
05/20/21 15:04
05/21/21 11:53 1
Heptachlor epoxide
ND
1.70
0.450
ug/Kg
05/20/21 15:04
05/21/21 11:53 1
Toxaphene
ND
100
29.0
ug/Kg
05/20/21 15:04
05/21/21 11:53 1
MB MB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
DCB Decachlorobiphenyl
74
26-
129
05120121 15:04
05121121 11:53 1
Tetrachloro-m-xylene
80
31-
122
05120121 15:04
05121121 11:53 1
Lab Sample ID: LCS 400-532668/2-A
Client
Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532719
Prep Batch: 532668
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
4,4'-DDD
33.3
15.57
ug/Kg
47
46 -150
4,4'-DDE
33.3
32.38
ug/Kg
97
49 -148
4,4'-DDT
33.3
26.57
ug/Kg
80
44 -150
Aldrin
33.3
32.32
ug/Kg
97
47 -137
alpha-BHC
33.3
27.82
ug/Kg
83
50 -148
beta-BHC
33.3
30.57
ug/Kg
92
46 -133
delta-BHC
33.3
30.18
ug/Kg
91
10 -150
Dieldrin
33.3
30.74
ug/Kg
92
41 -150
Endosulfan 1
33.3
30.16
ug/Kg
90
50 -141
Endosulfan II
33.3
25.76
ug/Kg
77
47 -148
Endosulfan sulfate
33.3
25.82
ug/Kg
77
50 -145
Endrin
33.3
26.66
ug/Kg
80
45 -150
Eurofins TestAmerica, Pensacola
Page 37 of 56 5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
Method: 8081 B - Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: LCS 400-532668/2-A
Client Sample ID
Matrix: Solid
Analysis Batch: 532719
Spike
LCS LCS
Analyte
Added
Result Qualifier
Unit
D %Rec
Endrin aldehyde
33.3
19.72
ug/Kg
59
gamma-BHC (Lindane)
33.3
27.01
ug/Kg
81
Heptachlor
33.3
24.51
ug/Kg
74
Heptachlor epoxide
33.3
31.09
ug/Kg
93
LCS
LCS
Surrogate
%Recovery
Qualifier
Limits
DCB Decachlorobiphenyl
78
26 - 129
Tetrachloro-m-xylene
72
31 - 122
Lab Sample ID: 400-203461-6 MS
Matrix: Solid
Analysis Batch: 532719
Sample
Sample
Spike
MS
MS
Analyte
Result
Qualifier
Added
Result
Qualifier
Unit
4,4'-DDD
ND
262
145.3
ug/Kg
4,4'-DDE
ND
262
162.5
ug/Kg
4,4'-DDT
ND
262
333.9
ug/Kg
Aldrin
ND
262
173.1
ug/Kg
alpha-BHC
ND
262
183.3
ug/Kg
beta-BHC
ND
262
172.9
ug/Kg
delta-BHC
ND
262
165.5
ug/Kg
Dieldrin
ND
262
169.2
ug/Kg
Endosulfan I
ND
262
215.1
ug/Kg
Endosulfan II
ND
262
138.5
ug/Kg
Endosulfan sulfate
ND
262
129.7
J
ug/Kg
Endrin
ND
262
131.0
J
ug/Kg
Endrin aldehyde
ND
262
94.69
J
ug/Kg
gamma-BHC (Lindane)
ND
262
176.5
ug/Kg
Heptachlor
ND
262
147.8
ug/Kg
Heptachlor epoxide
ND
262
175.8
ug/Kg
MS
MS
Surrogate
%Recovery
Qualifier
Limits
DCB Decachlorobiphenyl
39
26- 129
Tetrachloro-m-xylene
47
31- 122
Lab Sample ID: 400-203461-6 MSD
Matrix: Solid
Analysis Batch: 532719
Sample
Sample
Spike
MSD
MSD
Analyte
Result
Qualifier
Added
Result
Qualifier
Unit
4,4'-DDD
ND
261
181.1
ug/Kg
4,4'-DDE
ND
261
200.0
ug/Kg
4,4'-DDT
ND
261
348.8
ug/Kg
Aldrin
ND
261
217.7
ug/Kg
alpha-BHC
ND
261
215.3
ug/Kg
beta-BHC
ND
261
203.6
ug/Kg
delta-BHC
ND
261
193.0
ug/Kg
Dieldrin
ND
261
203.9
ug/Kg
Job ID: 400-203461-1
Lab Control Sample
Prep Type: Total/NA
Prep Batch: 532668
%Rec.
Limits
10-150
50-148
46-150
49-148
Client Sample ID: S1-5 COMPOSITE
Prep Type: Total/NA
Prep Batch: 532668
%Rec.
D %Rec Limits
# 55 13-146
62 23-143
127 10-160
66 10-154
70 15-152
66 10-160
63 10-160
65 10-160
82 10-160
# 53 10-160
# 49 27-143
# 50 20-156
# 36 14-160
# 67 26-142
# 56 10-160
67 10-160
Client Sample ID: S1-5 COMPOSITE
Prep Type: Total/NA
Prep Batch: 532668
%Rec. RPD
D
%Rec
Limits RPD Limit
69
13-146 22 50
77
23-143 21 50
134
10-160 4 50
83
10-154 23 50
83
15-152 16 50
78
10-160 16 50
74
10-160 15 50
78
10-160 19 50
Eurofins TestAmerica, Pensacola
Page 38 of 56 5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Method: 8081 B - Organochlorine Pesticides (GC) (Continued)
Lab Sample ID: 400-203461-6 MSD
Client Sample ID: S1-5 COMPOSITE
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532719
Prep Batch: 532668
Sample Sample
Spike
MSD MSD
%Rec. RPD
Analyte Result Qualifier
Added
Result Qualifier
Unit
D %Rec
Limits RPD Limit
Endosulfan I ND
261
257.0
ug/Kg
# 98
10 -160 18 50
Endosulfan II ND
261
160.0
ug/Kg
61
10 -160 14 50
Endosulfan sulfate ND
261
153.3
ug/Kg
59
27 -143 17 50
Endrin ND
261
161.6
ug/Kg
62
20-156 21 50
Endrin aldehyde ND
261
103.4 J
ug/Kg
40
14 -160 9 50
gamma-BHC (Lindane) ND
261
209.6
ug/Kg
80
26 -142 17 50
Heptachlor ND
261
185.9
ug/Kg
# 71
10 -160 23 50
Heptachlor epoxide ND
261
208.1
ug/Kg
80
10 -160 17 50
MSD MSD
ED
Surrogate %Recovery Qualifier
Limits
DCB Decachlorobiphenyl 59
26 - 129
Tetrachloro-m-xylene 57
31 - 122
Lab Sample ID: LB 400-532045/1-F
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 532547
Prep Batch: 532474
LB LB
Analyte Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Chlordane (technical) ND
25.0
2.60
ug/L
05/19/21 14:12
05/20/21 13:40 1
Methoxychlor ND
1.00
0.0820
ug/L
05/19/21 14:12
05/20/21 13:40 1
Endrin ND
1.00
0.0600
ug/L
05/19/21 14:12
05/20/21 13:40 1
gamma-BHC (Lindane) ND
2.50
0.500
ug/L
05/19/21 14:12
05/20/21 13:40 1
Heptachlor ND
1.00
0.0620
ug/L
05/19/21 14:12
05/20/21 13:40 1
Heptachlor epoxide ND
1.00
0.0640
ug/L
05/19/21 14:12
05/20/21 13:40 1
Toxaphene ND
150
6.00
ug/L
05/19/21 14:12
05/20/21 13:40 1
LB LB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
DCB Decachlorobiphenyl 48
10- 130
05119121 14:12
05120121 13:40 1
Tetrachloro-m-xylene 77
43 - 130
05119121 14:12
05120121 13:40 1
Method: 8151A - Herbicides (GC)
Lab Sample ID: LCS 400-532365/2-A
Client
Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532597
Prep Batch: 532365
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
2,4-D
9.90
7.946 J
ug/L
80
27 -123
Silvex (2,4,5-TP)
10.1
8.165
ug/L
81
25 -122
LCS LCS
Surrogate %Recovery Qualifier
Limits
2,4-Dichlorophenylacetic acid 87
30- 142
Eurofins TestAmerica, Pensacola
Page 39 of 56 5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Method: 8151A - Herbicides (GC) (Continued)
Lab Sample ID: LCSD 400-532365/3-A
Client Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532597
Prep Batch: 532365
Spike
LCSD
LCSD
%Rec. RPD
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits RPD Limit
2,4-D
9.90
8.396
ug/L
85
27 -123 6 40
Silvex (2,4,5-TP)
10.1
8.555
ug/L
85
25 -122 5 40
LCSD LCSD
Surrogate
%Recovery Qualifier
Limits
2,4-Dichlorophenylacetic acid
89
30 - 142
Lab Sample ID: MB 400-532379/1-A
Client Sample ID: Method Blank C
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532597
Prep Batch: 532379
m
MB MB
Analyte
Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
2,4,5-T
ND
40.0
3.40
ug/Kg
05/19/2109:10
05/20/2120:10 1
2,4-D
ND
200
11.0
ug/Kg
05/19/2109:10
05/20/2120:10 1
2,4-DB
ND
15.0
7.00
ug/Kg
05/19/2109:10
05/20/2120:10 1
Dalapon
ND
20.0
10.0
ug/Kg
05/19/2109:10
05/20/2120:10 1
Dicamba
ND
60.0
2.70
ug/Kg
05/19/2109:10
05/20/2120:10 1
Dichlorprop
ND
130
3.30
ug/Kg
05/19/2109:10
05/20/2120:10 1
Dinoseb
ND
200
17.0
ug/Kg
05/19/2109:10
05/20/2120:10 1
MCPA
ND
50000
870
ug/Kg
05/19/2109:10
05/20/2120:10 1
Silvex (2,4,5-TP)
ND
40.0
17.0
ug/Kg
05/19/21 09:10
05/20/21 20:10 1
Mecoprop
ND
50000
400
ug/Kg
05/19/2109:10
05/20/2120:10 1
MB MB
Surrogate
%Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
DCAA
59
10
- 150
05119121 09:10
05120121 20:10 1
Lab Sample ID: LCS 400-532379/2-A
Client
Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532597
Prep Batch: 532379
Spike
LCS
LCS
%Rec.
Analyte
Added
Result
Qualifier
Unit
D %Rec
Limits
2,4,5-T
83.6
48.79
ug/Kg
58
40 -120
2,4-D
82.5
55.64
J
ug/Kg
67
34 -120
2,4-DB
84.1
64.59
ug/Kg
77
16 -120
Dalapon
84.3
35.28
ug/Kg
42
10 -120
Dicamba
81.8
41.85
J
ug/Kg
51
10 -141
Dichlorprop
82.7
70.58
J
ug/Kg
85
28 -120
Dinoseb
84.2
36.51
J
ug/Kg
43
10-120
MCPA
8260
5479
J
ug/Kg
66
10 -120
Silvex (2,4,5-TP)
83.9
51.99
ug/Kg
62
34 -120
Mecoprop
8200
4019
J
ug/Kg
49
10-120
LCS LCS
Surrogate
%Recovery Qualifier
Limits
DCAA
67
10 - 150
Eurofins TestAmerica, Pensacola
Page 40 of 56 5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Method: 8151A - Herbicides (GC) (Continued)
Lab Sample ID: LCSD 400-532379/3-A
Client
Sample ID: Lab Control Sample Dup
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532597
Prep Batch: 532379
Spike
LCSD LCSD
%Rec. RPD
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits RPD Limit
2,4,5-T
83.6
53.15
ug/Kg
64
40 -120 9 40
2,4-D
82.5
56.26 J
ug/Kg
68
34 -120 1 40
2,4-DB
84.1
70.23
ug/Kg
84
16 -120 8 40
Dalapon
84.3
27.65
ug/Kg
33
10 -120 24 40
Dicamba
81.8
47.12 J
ug/Kg
58
10 -141 12 40
Dichlorprop
82.7
72.95 J
ug/Kg
88
28 -120 3 40
Dinoseb
84.2
36.16 J
ug/Kg
43
10 -120 1 40
MCPA
8260
5698 J
ug/Kg
69
10 -120 4 40
Silvex (2,4,5-TP)
83.9
56.10
ug/Kg
67
34 -120 8 40 m
Mecoprop
8200
4190 J
ug/Kg
51
10-120 4 40
LCSD
LCSD
Surrogate %Recovery
Qualifier
Limits
DCAA 67
10 - 150
Lab Sample ID: LB 400-532045/1-B
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 532597
Prep Batch: 532365
LB LB
Analyte Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
2,4-D
ND
100
1.30
ug/L
05/19/2108:17
05/20/2117:21 1
Silvex (2,4,5-TP)
ND
20.0
0.0910
ug/L
05/19/21 08:17
05/20/21 17:21 1
LB LB
Surrogate %Recovery Qualifier
Limits
Prepared
Analyzed Dil Fac
2,4-Dichlorophenylacetic acid
91
30-
142
05119121 08:17
05120121 17:21 1
Method: 6010D - Metals (ICP)
Lab Sample ID: MB 400-532212/1-A
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532562
Prep Batch: 532212
MB MB
Analyte Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Silver
ND
0.500
0.330
mg/Kg
05/18/2109:24
05/19/2111:43 1
Arsenic
ND
1.00
0.570
mg/Kg
05/18/2109:24
05/19/2111:43 1
Barium
ND
1.00
0.170
mg/Kg
05/18/2109:24
05/19/2111:43 1
Cadmium
ND
0.500
0.0880
mg/Kg
05/18/2109:24
05/19/2111:43 1
Chromium
ND
1.00
0.310
mg/Kg
05/18/2109:24
05/19/2111:43 1
Lead
ND
1.00
0.220
mg/Kg
05/18/2109:24
05/19/2111:43 1
Selenium
ND
2.00
0.870
mg/Kg
05/18/2109:24
05/19/2111:43 1
Lab Sample ID: LCS 400-532212/2-A
Client Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532562
Prep Batch: 532212
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Silver
49.9
48.05
mg/Kg
96
80 -120
Arsenic
99.9
94.83
mg/Kg
95
80 -120
Barium
99.9
100.7
mg/Kg
101
80-120
Eurofins TestAmerica, Pensacola
Page 41 of 56 5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Method: 6010D - Metals (ICP) (Continued)
Lab Sample ID: LCS 400-532212/2-A
Client Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532562
Prep Batch: 532212
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Cadmium
49.9
51.64
mg/Kg
103
80 -120
Chromium
99.9
99.82
mg/Kg
100
80 -120
Lead
99.9
97.50
mg/Kg
98
80 -120
Selenium
99.9
96.13
mg/Kg
96
80 -120
Lab Sample ID: LCS 400-532421/2-A
Client Sample ID:
Lab Control Sample C
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 532716
Prep Batch: 532421
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits m
Arsenic
1.00
1.035
mg/L
103
80 -120
Barium
3.00
3.149
mg/L
105
80-120
Cadmium
0.500
0.5248
mg/L
105
80 -120
Chromium
1.00
1.065
mg/L
107
80 -120
Lead
1.00
1.055
mg/L
105
80 -120
Selenium
1.00
1.056
mg/L
106
80 -120
Lab Sample ID: LCS 400-533359/2-A
Client Sample ID:
Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch: 533622
Prep Batch: 533359
Spike
LCS LCS
%Rec.
Analyte
Added
Result Qualifier
Unit
D %Rec
Limits
Silver
0.500
0.5087
mg/L
102
80 -120
Lab Sample ID: LB 400-532045/1-D
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 532716
Prep Batch: 532421
LB LB
Analyte Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Arsenic
ND
0.0500
0.0200
mg/L
05/19/2111:11
05/20/2122:04 1
Barium
ND
5.00
1.05
mg/L
05/19/2111:11
05/20/2122:04 1
Cadmium
ND
0.0250
0.00500
mg/L
05/19/2111:11
05/20/2122:04 1
Chromium
ND
0.0500
0.0100
mg/L
05/19/2111:11
05/20/2122:04 1
Lead
ND
0.0500
0.0100
mg/L
05/19/2111:11
05/20/2122:04 1
Selenium
ND
0.100
0.0200
mg/L
05/19/2111:11
05/20/2122:04 1
Lab Sample ID: LB 400-532045/1-1
Client Sample ID: Method Blank
Matrix: Solid
Prep Type: TCLP
Analysis Batch: 533622
Prep Batch: 533359
LB LB
Analyte Result Qualifier
RL
MDL
Unit
D Prepared
Analyzed Dil Fac
Silver
ND
0.0250
0.0100
mg/L
05/26/2115:07
05/27/2112:36 1
Eurofins TestAmerica, Pensacola
Page 42 of 56 5/28/2021

QC Sample Results
Client: Shield Engineering Inc
Project/Site: Celadon
Method: 7470A - Mercury (CVAA)
Lab Sample ID: LCS 400-532366/15-A
Matrix: Solid
Analysis Batch: 532563
Analyte
Mercury
Lab Sample ID: LB 400-532045/1-C
Matrix: Solid
Analysis Batch: 532563
LB LB
Analyte Result Qualifier
Mercury ND
Method: 7471 B - Mercury (CVAA)
Lab Sample ID: MB 400-532086/14-A
Matrix: Solid
Analysis Batch: 532437
MB MB
Analyte Result Qualifier
Hg ND
Lab Sample ID: LCS 400-532086/15-A
Matrix: Solid
Analysis Batch: 532437
Analyte
Hg
F
Job ID: 400-203461-1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 532366
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
1.01 1.012 ug/L 101 80-120
Client Sample ID: Method Blank
Prep Type: TCLP
Prep Batch: 532366
RL MDL Unit D Prepared Analyzed Dil Fac
1.60 0.560 ug/L 05/19/2108:19 05/19/2117:11 1
In
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 532086
RL MDL Unit D Prepared Analyzed Dil Fac
0.0133 0.00798 mg/Kg 05/17/2111:37 05/19/2111:02 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 532086
Spike LCS LCS %Rec.
Added Result Qualifier Unit D %Rec Limits
0.0669 0.06195 mg/Kg 93 80 - 220
Page 43 of 56
Eurofins TestAmerica, Pensacola
5/28/2021

Lab Chronicle
Client: Shield Engineering Inc
Project/Site: Celadon
F
Job ID: 400-203461-1
Client Sample ID: S1-5 COMPOSITE
Lab Sample ID: 400-203461-6
Date Collected:
05/13/21 14:05
Matrix: Solid
Date Received: 05/15/21 10:31
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type
Type
Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
TCLP
Leach
1311
25.05 g
500 mL
532125
05/17/21 14:10
BAW
TAL PEN
TCLP
Analysis
8260D
5
5 mL
5 mL
532492
05/20/21 03:56
WPD
TAL PEN
TCLP
Leach
1311
100.05 g
2000 mL
532045
05/17/21 10:07
BAW
TAL PEN
TCLP
Prep
3510C
179.6 mL
1 mL
532706
05/21/21 07:30
HMW
TAL PEN
TCLP
Analysis
8270E
1
532802
05/21/2122:57
SIB
TAL PEN
TCLP
Leach
1311
100.05 g
2000 mL
532045
05/17/21 10:07
BAW
TAL PEN
TCLP
Prep
3520C
20 mL
5 mL
532474
05/19/21 14:12
KWS
TAL PEN
TCLP
Analysis
8081 B
1
532547
05/20/21 14:08
IDS
TAL PEN
TCLP
Leach
1311
100.05 g
2000 mL
532045
05/17/21 10:07
BAW
TAL PEN
TCLP
Prep
8151A
20 mL
10 mL
532365
05/19/21 08:17
IAG
TAL PEN
TCLP
Analysis
8151A
1
532597
05/20/21 18:29
IDS
TAL PEN
TCLP
Leach
1311
100.05 g
2000 mL
532045
05/17/21 10:07
BAW
TAL PEN
TCLP
Prep
3010A
10 mL
50 mL
532421
05/19/21 11:11
KW
TAL PEN
TCLP
Analysis
6010D
1
532716
05/20/21 22:48
JTW
TAL PEN
TCLP
Leach
1311
100.05 g
2000 mL
532045
05/17/21 10:07
BAW
TAL PEN
TCLP
Prep
3010A
10 mL
50 mL
533359
05/26/21 15:07
KW
TAL PEN
TCLP
Analysis
6010D
1
533622
05/27/21 13:50
JTW
TAL PEN
TCLP
Leach
1311
100.05 g
2000 mL
532045
05/17/21 10:07
BAW
TAL PEN
TCLP
Prep
7470A
5 mL
40 mL
532366
05/19/21 08:19
NET
TAL PEN
TCLP
Analysis
7470A
1
532563
05/19/21 17:26
NET
TAL PEN
Total/NA
Analysis
Moisture
1
532214
05/18/21 11:12
BKW
TAL PEN
Client Sample ID: S1-5 COMPOSITE
Lab
Sample ID: 400-203461-6
Date Collected:
05/13/21 14:05
Matrix: Solid
Date Received: 05/15/21 10:31
Percent
Solids:
12.6
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type
Type
Method Run
Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA
Prep
5035
5.00 g
5.00 g
532586
05/20/21 08:15
BEP
TAL PEN
Total/NA
Analysis
8260D
1
5 mL
5 mL
532534
05/20/21 14:36
BEP
TAL PEN
Total/NA
Prep
5035
4.92 g
5.00 g
532734
05/21/21 08:15
BEP
TAL PEN
Total/NA
Analysis
8260D
1
5 mL
5 mL
532709
05/21/21 10:46
BEP
TAL PEN
Total/NA
Prep
3546
15.24 g
1 mL
532298
05/18/21 14:27
BKL
TAL PEN
Total/NA
Analysis
8270E
5
532461
05/19/2120:30
SIB
TAL PEN
Total/NA
Prep
3546
15.15 g
5 mL
532668
05/20/21 15:05
BKL
TAL PEN
Total/NA
Analysis
8081B
10
532719
05/21/2112:50
IDS
TAL PEN
Total/NA
Prep
8151A
30.03 g
10 mL
532379
05/19/21 09:10
KWS
TAL PEN
Total/NA
Analysis
8151A
10
532712
05/21/21 11:23
IDS
TAL PEN
Total/NA
Prep
3050B
.5420 g
50 mL
532212
05/18/21 09:24
NET
TAL PEN
Total/NA
Analysis
6010D
1
532562
05/19/21 12:28
LDC
TAL PEN
Total/NA
Prep
7471 B
.5454 g
40 mL
532086
05/17/21 11:37
NET
TAL PEN
Total/NA
Analysis
7471B
1
532437
05/19/2111:30
NET
TAL PEN
Li
Page 44 of 56
Eurofins TestAmerica, Pensacola
5/28/2021

Lab Chronicle
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Client Sample ID: Method Blank
Lab Sample ID: LB
400-532045/1-B
Date Collected: N/A
Matrix: Solid
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
TCLP Leach
1311
2000 mL
2000 mL
532045
05/17/21 10:07
BAW TAL PEN
TCLP Prep
8151A
20 mL
10 mL
532365
05/19/21 08:17
IAG TAL PEN
TCLP Analysis
8151A
1
532597
05/20/21 17:21
DS TAL PEN
Client Sample ID: Method Blank
Lab Sample ID: LB
400-532045/1-C
Date Collected: N/A
Matrix: Solid
E:
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
F
Prep Type Type
Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
TCLP Leach
1311
2000 mL
2000 mL
532045
05/17/21 10:07
BAW TAL PEN
TCLP Prep
7470A
5 mL
40 mL
532366
05/19/21 08:19
NET TAL PEN
TCLP Analysis
7470A
1
532563
05/19/21 17:11
NET TAL PEN
Client Sample ID: Method Blank
Lab Sample ID: LB
400-532045/1-D
Date Collected: N/A
Matrix: Solid
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
TCLP Leach
1311
2000 mL
2000 mL
532045
05/17/21 10:07
BAW TAL PEN
TCLP Prep
3010A
10 mL
50 mL
532421
05/19/21 11:11
KW TAL PEN
TCLP Analysis
6010D
1
532716
05/20/21 22:04
JTW TAL PEN
Client Sample ID: Method Blank
Lab Sample ID: LB
400-532045/1-F
Date Collected: N/A
Matrix: Solid
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
TCLP Leach
1311
2000 mL
2000 mL
532045
05/17/21 10:07
BAW TAL PEN
TCLP Prep
3520C
20 mL
5 mL
532474
05/19/21 14:12
KWS TAL PEN
TCLP Analysis
8081 B
1
532547
05/20/21 13:40
IDS TAL PEN
Client Sample ID: Method Blank
Lab Sample ID: LB
400-532045/1-G
Date Collected: N/A
Matrix: Solid
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
TCLP Leach
1311
2000 mL
2000 mL
532045
05/17/21 10:07
BAW TAL PEN
TCLP Prep
3510C
172.4 mL
1 mL
532706
05/21/21 07:30
HMW TAL PEN
TCLP Analysis
8270E
1
532802
05/21/21 19:30
S16 TAL PEN
Eurofins TestAmerica, Pensacola
Page 45 of 56 5/28/2021

Lab Chronicle
Client: Shield Engineering Inc
Project/Site: Celadon
Client Sample ID: Method Blank
Date Collected: N/A
Date Received: N/A
F
Job ID: 400-203461-1
Lab Sample ID: LB 400-532045/1-1
Matrix: Solid
F
Batch
Batch
Dil Initial
Final
Batch
Prepared
Prep Type
Type
Method
Run Factor Amount
Amount
Number
or Analyzed
Analyst
Lab
TCLP
Leach
1311
2000 mL
2000 mL
532045
05/17/21 10:07
BAW
TAL PEN
TCLP
Prep
3010A
10 mL
50 mL
533359
05/26/21 15:07
KW
TAL PEN
TCLP
Analysis
6010D
1
533622
05/27/21 12:36
JTW
TAL PEN
Client Sample ID: Method Blank
Date Collected: N/A
Date Received: N/A
Batch
Batch
Dil Initial
Prep Type Type
Method
Run Factor Amount
TCLP Leach
1311
500 mL
TCLP Analysis
8260D
1 5 mL
Client Sample ID: Method Blank
Date Collected: N/A
Date Received: N/A
Batch
Batch
Prep Type Type
Method
Total/NA Prep
7471 B
Total/NA Analysis
7471 B
Client Sample ID: Method Blank
Date Collected: N/A
Date Received: N/A
Batch
Batch
Prep Type Type
Method
Total/NA Prep
3050B
Total/NA Analysis
6010D
Client Sample ID: Method Blank
Date Collected: N/A
Date Received: N/A
Batch
Batch
Prep Type Type
Method
Total/NA Prep
3546
Total/NA Analysis
8270E
Client Sample ID: Method Blank
Date Collected: N/A
Date Received: N/A
Batch
Batch
Prep Type Type
Method
Total/NA Prep
8151A
Total/NA Analysis
8151A
Lab Sample ID: LB 400-532125/1-A
Matrix: Solid
E:
Final
Batch
Prepared
F
Amount
Number
or Analyzed
Analyst Lab
500 mL
532125
05/17/21 14:10
BAW TAL PEN
5 mL
532492
05/19/21 20:03
WPD TAL PEN T
Lab Sample ID: MB 400-532086/14-A W
Matrix: Solid
Dil Initial Final Batch Prepared F
Run Factor Amount Amount Number or Analyzed Analyst Lab
.6012 g 40 mL 532086 05/17/21 11:37 NET TAL PEN
1 532437 05/19/21 11:02 NET TAL PEN L
F
Lab Sample ID: MB 400-532212/1-A (
Matrix: Solid
Dil Initial Final Batch
Prepared
Run Factor Amount Amount Number
or Analyzed
Analyst Lab
.5000 g 50 mL 532212
05/18/21 09:24
NET TAL PEN
1 532562
05/19/21 11:43
LDC TAL PEN
Lab Sample ID: MB 400-532298/1-A
Matrix: Solid
Dil Initial Final Batch
Prepared
Run Factor Amount Amount Number
or Analyzed Analyst Lab
15 g 1 mL 532298
05/18/21 14:27 BKL TAL PEN
1 532461
05/19/2119:05 S1B TAL PEN
Lab Sample ID: MB 400-532379/1-A
Matrix: Solid
Dil Initial Final Batch
Prepared
Run Factor Amount Amount Number
or Analyzed Analyst Lab
30 g 10 mL 532379
05/19/21 09:10 KWS TAL PEN
1 532597
05/20/21 20:10 IDS TAL PEN
Page 46 of 56
Eurofins TestAmerica, Pensacola
5/28/2021

Lab Chronicle
Client: Shield Engineering Inc
Project/Site: Celadon
Client Sample ID: Method Blank
Date Collected: N/A
Date Received: N/A
F
Job ID: 400-203461-1
Lab Sample ID: MB 400-532586/2-A
Matrix: Solid
F
Batch
Batch
Dil Initial
Final
Batch
Prepared
Prep Type Type
Method
Run Factor Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Prep
5035
5.00 g
5.00 g
532586
05/20/21 08:15 BEP TAL PEN
Total/NA Analysis
8260D
1 5 mL
5 mL
532534
05/20/21 11:02 BEP TAL PEN
Client Sample ID: Method Blank
Date Collected: N/A
Date Received: N/A
Batch
Batch
Prep Type Type
Method
Total/NA Prep
3546
Total/NA Analysis
8081 B
Client Sample ID: Method Blank
Date Collected: N/A
Date Received: N/A
Batch
Batch
Prep Type Type
Method
Total/NA Prep
5035
Total/NA Analysis
8260D
Dil Initial
Run Factor Amount
15g
I
Lab Sample ID: MB 400-532668/1-A
Matrix: Solid
F
Final Batch Prepared
Amount Number or Analyzed Analyst Lab
5 mL 532668 05/20/21 15:04 BKL TAL PEN
532719 05/21/21 11:53 IDS TAL PEN
Lab Sample ID: MB 400-532734/2-A
m
Matrix: Solid
Dil Initial
Final
Batch
Prepared
Run Factor Amount
Amount
Number
or Analyzed
Analyst Lab
5.00 g
5.00 g
532734
05/21/21 08:15
BEP TAL PEN
1 5 mL
5 mL
532709
05/21/21 10:21
BEP TAL PEN
L
Client Sample ID: Lab Control Sample
Date Collected: N/A
Date Received: N/A
Lab Sample ID: LCS 400-532086/15-A
Matrix: Solid
Batch
Batch
Dil
Initial
Final Batch
Prepared
Prep Type Type
Method Run
Factor
Amount
Amount Number
or Analyzed
Analyst Lab
Total/NA Prep
7471 B
.6024 g
40 mL 532086
05/17/21 11:37
NET TAL PEN
Total/NA Analysis
7471B
1
532437
05/19/2111:03
NET TAL PEN
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS
400-532212/2-A
Date Collected: N/A
Matrix: Solid
Date Received: N/A
F Batch
Batch
Dil
Initial
Final Batch
Prepared
Prep Type Type
Method Run
Factor
Amount
Amount Number
or Analyzed
Analyst Lab
Total/NA Prep
3050B
.5006 g
50 mL 532212
05/18/21 09:24
NET TAL PEN
Total/NA Analysis
6010D
1
532562
05/19/21 11:47
LDC TAL PEN
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS
400-532298/2-A
Date Collected: N/A
Matrix: Solid
Date Received: N/A
Batch
Batch
Dil
Initial
Final Batch
Prepared
Prep Type Type
Method Run
Factor
Amount
Amount Number
or Analyzed
Analyst Lab
Total/NA Prep
3546
15 g
1 mL 532298
05/18/21 14:27
BKL TAL PEN
Total/NA Analysis
8270E
1
532461
05/19/2119:26
S113 TAL PEN
Eurofins TestAmerica, Pensacola
Page 47 of 56 5/28/2021

Lab Chronicle
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 400-532365/2-A
Date Collected: N/A
Matrix: Solid
Date Received: N/A
F Batch Batch
Dil Initial
Final Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Prep 8151A
250 mL
10 mL 532365 05/19/21 08:17 IAG TAL PEN
Total/NA Analysis 8151A
1
532597 05/20/21 15:41 IDS TAL PEN
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 400-532366/15-A
Date Collected: N/A
Matrix: Solid
Date Received: N/A
Batch Batch
Dil Initial
Final Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Prep 7470A
40 mL
40 mL 532366 05/19/21 08:19 NET TAL PEN
Total/NA Analysis 7470A
1
532563 05/19/21 17:13 NET TAL PEN
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 400-532379/2-A
m
Date Collected: N/A
Matrix: Solid
Date Received: N/A
Batch Batch
Dil Initial
Final Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Prep 8151A
30 g
10 mL 532379 05/19/21 09:10 KWS TAL PEN
Total/NA Analysis 8151A
1
532597 05/20/21 20:43 IDS TAL PEN
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 400-532421/2-A
Date Collected: N/A
Matrix: Solid
Date Received: N/A
Batch Batch
Dil Initial
Final Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Prep 3010A
50 mL
50 mL 532421 05/19/21 11:11 KW TAL PEN
Total/NA Analysis 6010D
1
532716 05/20/21 22:08 JTW TAL PEN
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 400-532474/3-A
Date Collected: N/A
Matrix: Solid
Date Received: N/A
F Batch Batch
Dil Initial
Final Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Prep 3520C
250 mL
5 mL 532474 05/19/21 14:12 KWS TAL PEN
Total/NA Analysis 8081 B
1
532547 05/20/21 11:18 IDS TAL PEN
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 400-532492/1002
Date Collected: N/A
Matrix: Solid
Date Received: N/A
Batch Batch
Dil Initial
Final Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Analysis 8260D
1 5 mL
5 mL 532492 05/19/21 16:32 WPD TAL PEN
Page 48 of 56
Eurofins TestAmerica, Pensacola
5/28/2021

Lab Chronicle
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 400-532586/1-A
Date Collected: N/A
Matrix: Solid
Date Received: N/A
F Batch Batch
Dil Initial
Final Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Prep 5035
5.00 g
5.00 g 532586 05/20/21 08:15 BEP TAL PEN
Total/NA Analysis 8260D
1 5 mL
5 mL 532534 05/20/21 10:12 BEP TAL PEN
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 400-532668/2-A
Date Collected: N/A
Matrix: Solid
Date Received: N/A
Batch Batch
Dil Initial
Final Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Prep 3546
15 g
5 mL 532668 05/20/21 15:04 BKL TAL PEN
Total/NA Analysis 8081B
1
532719 05/21/2112:22 IDS TAL PEN
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 400-532706/2-A
m
Date Collected: N/A
Matrix: Solid
Date Received: N/A
Batch Batch
Dil Initial
Final Batch Prepared
Prep Type Type Method Run
Factor Amount
Amount Number or Analyzed Analyst Lab
Total/NA Prep 3510C
250 mL
1 mL 532706 05/21/21 07:30 HMW TAL PEN
Total/NA Analysis 8270E
1
532781 05/21/2122:36 S113 TAL PEN
L
Client Sample ID: Lab Control Sample
Lab Sample ID: LCS 400-532734/1-A
Date Collected: N/A
Matrix: Solid
Date Received: N/A
Batch
Batch
Prep Type Type
Method Run
Total/NA Prep
5035
Total/NA Analysis
8260D
Client Sample ID: Lab Control Sample
Date Collected: N/A
Date Received: N/A
Dil Initial
Final
Batch
Prepared
Factor Amount
Amount
Number
or Analyzed Analyst Lab
5.00 g
5.00 g
532734
05/21/21 08:15 BEP TAL PEN
1 5 mL
5 mL
532709
05/21/21 09:31 BEP TAL PEN
Lab Sample ID: LCS 400-533359/2-A
Matrix: Solid
F Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Prep
3010A
50 mL
50 mL
533359
05/26/21 15:07
KW TAL PEN
Total/NA Analysis
6010D
1
533622
05/27/21 13:24
JTW TAL PEN
Client Sample ID: Lab Control Sample Dup
Lab Sample ID: LCSD
400-532298/3-A
Date Collected: N/A
Matrix: Solid
Date Received: N/A
Batch
Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type
Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst Lab
Total/NA Prep
3546
15 g
1 mL
532298
05/18/21 14:27
BKL TAL PEN
Total/NA Analysis
8270E
1
532461
05/19/2119:48
S113 TAL PEN
Page 49 of 56
Eurofins TestAmerica, Pensacola
5/28/2021

Lab Chronicle
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Client Sample ID: Lab Control Sample Dup
Lab Sample ID: LCSD 400-532365/3-A
Date Collected: N/A
Matrix: Solid
Date Received: N/A
F
Batch Batch Dil Initial
Final Batch
Prepared
Prep Type Type Method Run Factor Amount
Amount Number
or Analyzed Analyst Lab
Total/NA Prep 8151A 250 mL
10 mL 532365
05/19/21 08:17 IAG TAL PEN
Total/NA Analysis 8151A 1
532597
05/20/21 16:14 DS TAL PEN
Client Sample ID: Lab Control Sample Dup
Date Collected: N/A
Date Received: N/A
Batch
Batch
Prep Type Type
Method Run
Total/NA Prep
8151A
Total/NA Analysis
8151A
Client Sample ID: Lab Control Sample Dup
Date Collected: N/A
Date Received: N/A
Batch
Batch
Prep Type Type
Method Run
Total/NA Prep
3520C
Total/NA Analysis
8081 B
Dil Initial
Factor Amount
30 g
1
Dil Initial
Factor Amount
250 mL
Client Sample ID: Lab Control Sample Dup
Date Collected: N/A
Date Received: N/A
f
Lab Sample ID: LCSD 400-532379/3-A
Matrix: Solid
F
Final Batch Prepared
Amount Number or Analyzed Analyst Lab
10 mL 532379 05/19/21 09:10 KWS TAL PEN
532597 05/20/21 21:17 DS TAL PEN
Lab Sample ID: LCSD 400-532474/4-A
Matrix: Solid
Final Batch
Prepared
Amount Number
or Analyzed Analyst Lab
5 mL 532474
05/19/21 14:12 KWS TAL PEN
532547
05/20/21 11:47 DS TAL PEN
Lab Sample ID: LCSD 400-532706/3-A
Matrix: Solid
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Prep 3510C
250 mL
1 mL
532 006
05/ 11/21 07:30 HMW TAL PEN
Total/NA Analysis 8270E
1
532781
05/21/2122:57 S1B TAL PEN
Client Sample ID: S1-5 COMPOSITE
Lab Sample ID: 400-203461-6 MS
Date Collected: 05/13/21 14:05
Matrix: Solid
Date Received: 05/15/21 10:31
Percent Solids: 12.6
F Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Prep 5035
4.92 g
5.00 g
532734
05/21/21 08:15 BEP TAL PEN
Total/NA Analysis 8260D
1
5 mL
5 mL
532709
05/21/21 14:16 BEP TAL PEN
Total/NA Prep 3546
15.09 g
5 mL
532668
05/20/21 15:05 BKL TAL PEN
Total/NA Analysis 8081B
10
532719
05/21/2113:19 DS TAL PEN
Client Sample ID: S1-5 COMPOSITE
Lab Sample ID: 400-203461-6 MSD
Date Collected: 05/13/21 14:05
Matrix: Solid
Date Received: 05/15/21 10:31
Percent Solids: 12.6
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type Type Method Run
Factor
Amount
Amount
Number
or Analyzed Analyst Lab
Total/NA Prep 5035
4.95 g
5.00 g
532734
05/21/21 08:15 BEP TAL PEN
Total/NA Analysis 8260D
1
5 mL
5 mL
532709
05/21/21 14:41 BEP TAL PEN
Total/NA Prep 3546
15.16 g
5 mL
532668
05/20/21 15:05 BKL TAL PEN
LTotal/NA Analysis 8081 B
10
532719
05/21/21 13:47 DS TAL PEN
Page 50 of 56
Eurofins TestAmerica, Pensacola
5/28/2021

Lab Chronicle
Client: Shield Engineering Inc Job ID: 400-203461-1
Project/Site: Celadon
Laboratory References:
TAL PEN = Eurofins TestAmerica, Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
Eurofins TestAmerica, Pensacola
Page 51 of 56 5/28/2021

Method Summary
Client: Shield Engineering Inc
Project/Site: Celadon
Job ID: 400-203461-1
Method
Method Description
Protocol
Laboratory
8260D
Volatile Organic Compounds by GC/MS
SW846
TAL PEN
8270E
Semivolatile Organic Compounds (GC/MS)
SW846
TAL PEN
8081 B
Organochlorine Pesticides (GC)
SW846
TAL PEN
8151A
Herbicides (GC)
SW846
TAL PEN
6010D
Metals (ICP)
SW846
TAL PEN
7470A
Mercury (CVAA)
SW846
TAL PEN
7471 B
Mercury (CVAA)
SW846
TAL PEN
Moisture
Percent Moisture
EPA
TAL PEN
1311
TCLP Extraction
SW846
TAL PEN
1311
TCLP Zero Headspace Extraction
SW846
TAL PEN
3010A
Preparation, Total Metals
SW846
TAL PEN
3050B
Preparation, Metals
SW846
TAL PEN
3510C
Liquid -Liquid Extraction (Separatory Funnel)
SW846
TAL PEN
3520C
Liquid -Liquid Extraction (Continuous)
SW846
TAL PEN
3546
Microwave Extraction
SW846
TAL PEN
5030C
Purge and Trap
SW846
TAL PEN
5035
Closed System Purge and Trap
SW846
TAL PEN
7470A
Preparation, Mercury
SW846
TAL PEN
7471 B
Preparation, Mercury
SW846
TAL PEN
8151A
Extraction (Herbicides)
SW846
TAL PEN
Protocol References:
EPA= US Environmental Protection Agency
SW846
= "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods",
Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL PEN = Eurofins TestAmerica, Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
Eurofins TestAmerica, Pensacola
Page 52 of 56 5/28/2021

Accreditation/Certification Summary
Client: Shield Engineering Inc
Job ID: 400-203461-1
Project/Site: Celadon
Laboratory: Eurofins TestAmerica, Pensacola
Unless otherwise noted, all analytes for this laboratory were covered under each
accreditation/certification below.
Authority Program
Identification Number
Expiration Date
North Carolina (WW/SW) State
314
12-31-21
The following analytes are included in this report, but the laboratory is not certified by the governing authority.
This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix
Analyte
7470A 7470A Solid
Mercury
8260D 5035 Solid
1,2-Dichloroethene, Total
8260D 5035 Solid
1,3-Dichloropropene, Total
8260D 5035 Solid
Butadiene
8260D 5035 Solid
Hexane
8260D 5035 Solid
n-Heptane
8260D 5035 Solid
Tetrahydrofuran
Moisture Solid
Percent Moisture
Moisture Solid
Percent Solids
Eurofins TestAmerica, Pensacola
Page 53 of 56 5/28/2021

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Page 54 of 56 5/28/2021

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Page 55 of 56
5/28/2021

Login Sample Receipt Checklist
Client: Shield Engineering Inc Job Number: 400-203461-1
Login Number: 203461
List Number: 1
Creator: Conrady, Hank W
Question
List Source: Eurofins TestAmerica, Pensacola
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
N/A
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True 0.0°C 0.0°C IR-9
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Eurofins TestAmerica, Pensacola
Page 56 of 56 5/28/2021