NC0048879_Pretreatment_Annual_Report_Amended_20230807

CARY
. ' A
-LIVE INSPIRED'" --
August 7, 2023
Mr. Michael Montebello
Division of Water Resources
Water Quality Permitting Section - NPDES
1617 Mail Service Center
Raleigh, NC 27699-1617
Electronic email submittal
Re: Pretreatment Annual Report 2022 - Amendment
Dear Mr. Montebello:
Enclosed is the Town of Cary Amended Pretreatment Annual Report (PAR) for calendar year
(CY) 2022. During a Pretreatment Program audit, it was discovered that a daily permit limit was
exceeded at FujiFilm Diosynth Biotechnologies USA, one of Cary's permitted Significant
Industrial Users (SIU), which resulted in a technical review criterion (TRC) — significant non-
compliance (SNC) for the second six month compliance judgement period. A notice of violation,
civil penalty, and a public notice was issued for the SNC. Please find enclosed amended sheets
for the 2022 PAR. Information will be included in the 2023 PAR narrative section detailing the
discovered SNC and enclosed amendment.
Please feel free to contact me at 919-469-4095 if there are any questions regarding this
amendment.
Sincerely,
Donald Smith
Wastewater Collection System Manager
Cc: Jamie Revels, P.E., Utilities Director
Enclosures: 2022 Amended Pretreatment Performance Summary Form
2022 Amended Significant Non -Compliance Report Form- Western Wake WRF
2022 Amended Industrial Data Summary Form (WWRWRF)
919.469.4000 1 carync.gov
PO Box 8005 Cary, NC 27512

THIS PAGE REPLACED WITH REVISION
Mr, Michael Montebello
Division of Water Resources
Water Quality Permitting Section - NPDES
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: Pretreatment Annual Report 2022
Dear Mr. Montebello:
UTILITIES DEPARTMENT
February 21, 2023
Certified Mail
Enclosed is the Town of Cary Pretreatment Annual Report for calendar year (CY) 2022. All information
contained herein reflects the proceedings of the Town of Cary Industrial Pretreatment Program.
Please feel free to contact me at 919-469-4095 if there are any questions regarding the Town of Cary 2022
Pretreatment Annual Report.
Sincerely,
Donald Smith RECEIVED
Wastewater Collection System Manager
Cc: Jamie Revels, P.E., Utilities Director FEB 2 7 2023
Enclosures: 2022 Pretreatment Annual Report Narrative NCDEQ/DWR/NPDES
Western Wake WRF Allocation Table
North Cary WRF Allocation Table
North Cary WRF Pharmaceutical Organics Allocation Table
2022 Pretreatment Program Information Sheets
Historical SNC Report
2022 Pretreatment Performance Summary Form
2022 Significant Non -Compliance Report Form- North Cary WRF
2022 Significant Non -Compliance Report Form- Western Wake WRF
(3) 2022 Industrial Data Summary Form
(3) Copy of Notice of Violation
TOWN Of CARY
400 fames Jackson Avenue • Cary, NC 27513 • PO Box 8005 • Cary, NC 27512-8005
te1919-469-4090 • fax [phone] • �v-%Nw.to%amofcary.org

Town of Cary
2022 PAR Narrative
2022 Pretreatment Annual Report (PAR) - Town of Cary
Applies to Significant Industrial Users contributing wastewater to the Town of Cary in CY 2022. On
January 6, 2015 SILT flow from both FujiFilm Diosynth Biotechnologies USA, Inc (FujiFilm) and
Biogen began discharging to the Western Wake Regional Water Reclamation Facility (WRF)
(NPDES Permit # NCO088846). On August 16, 2016 CIU flow from Catalent Pharma Solutions,
LLC (Catalent) began discharging to the North Cary WRF (NPDES Permit # NC0048879). All three
industrial permits are still active.
Number of Water Reclamation Facilities: 3 - North and South Cary WRFs and the Western Wake
Regional WRF.
The Western Wake Regional WRF was commissioned on July 28, 2014 and is a shared reclamation
facility among the Western Wake Partners who consist of the Town of Cary, Town of Morrisville,
and Town of Apex. Cary is responsible for the management, operation, and maintenance of the
facility. Cary provides sewer service to the Town of Morrisville through an agreement in 2005 where
Cary acquired ownership of the water and wastewater utilities and is the Control Authority for said
service area. An updated inter -local sewer service agreement between the Town of Apex and Town
of Cary was agreed upon for the Western Wake Regional WRF on January 19, 2016. Cary remains
the Lead Agency for the WRF, and both entities maintain pretreatment programs for their respective
portions of ownership in the WRF. Information is shared between the agencies with regards to Head
Works Analysis and Allocation Tables.
2022 Industrial Data Summary Forms (IDSFs) are enclosed for each of the two SIUs. Averages were
calculated for 6- month periods using detection limits (DL) for those with all values <DL in the 6-
month period, and zero values for <DL where there were some measurable quantities sampled in the
6-month period. Wastewater disposal to Cary from the regulated pipes at both Biogen and FujiFilm
occurred daily in 2022. There was no wastewater disposal to Cary from the CIU (Catalent) in all of
2022.
NARRATIVE OF 2022 ANNUAL PRETREATMENT PROGRAM ACTIVITIES
GENERAL PROGRAM INFORMATION SECTION
General Information for the Town of Cary Pretreatment Program for
Calendar Year (CY) 2022 with supporting historical information
North Cary WRF HWA & AT — Submitted and received March 26, 2019 and was approved with
corrections June 24, 2019. Corrections included updating stream standards based on total metals
allocated to this WRF. For arsenic the stream standard was updated based on Human
Health/Water Supply standard. PERCS chose to approve the use of 0 mg/L, for uncontrollable
silver concentration as sampling data showed <1 mg/L. The next 14WA is due March 31, 2024.
(Current NPDES Permit expires February 28, 2023)
North Cary WRF Pharmaceutical Organic Headworks Analysis (POHA) — Submitted and
received along with updated HWA and AT March 26, 2019 and was approved June 24, 2019.
South Cary WRF HWA & AT — Submitted and received May 13, 2019 and was approved with
corrections August 6, 2019. Corrections included updating the dissolved metals calculator and
Page I of 6

Town of Cary
2022 PAR Narrative
updating stream standards based on total metals allocated to this WRF. For arsenic the stream
standard was updated based on Human Health/Water Supply standard. PERCS chose to use
NPDES loading for total nitrogen as it is more conservative than design criteria loading. PERCS
also chose to use mercury literature removal rate and approved the HWA with negative mercury
allocation since there are no SNs discharging to the South Cary WRF and 95% of effluent data
was below the detection limit. PERCS chose to approve the use of 0 mg/L for uncontrollable
silver concentration as data showed <1 mg/L. No SIU or CNs contributed wastewater flow to
South Cary WRF in 2022.
• Western Wake Regional WRF HWA and AT— Submitted and received by PERCS on January 14,
2021 and is still under review. (HWA due date April 1, 2021, current NPDES permit expired July
31, 2021 and no draft permit received yet.) An updated AT was submitted along with the SIU
permit modification for FujiFilm Diosynth Biotechnologies USA, Inc on January 14, 2021 with
modification approved February 10, 2021. Another SILT permit modification for FujiFilm
Diosynth Biotechnologies USA, Inc (updating reporting requirements with no effect on the AT)
was submitted January 4, 2022 and is currently under review by PERCS. There were no SIU/CIU
contributions to the W WRWRF from the Town of Apex in 2022, see Town of Apex PAR.
• North Cary WRF LTMP —Submitted for revision and received August 27, 2019 and approved
November 19, 2019.
• South Cary WRF LTMP —Submitted for revision and received January 19, 2017 and approved
April 18, 2017.
• Western Wake Regional WRF LTMP- Submitted for revision and received January 19, 2017 and
approved April 18, 2017.
• SUO —On October 28, 2011 the PERCS Unit received a proposed modified SUO to reflect then
recent changes to the NC Pretreatment Rules. On November 8, 2011 the Town received approval
from PERCS for said modification. On December 15, 2011 the modified SUO was approved by
the Cary Town Council. The Town received approval from PERCS on April 12, 2012 for the
modified SUO.
• A modified ERP was submitted on November 18, 2019 to reflect addition of an ERP for Dental
Users and approved March 17, 2020. The program information sheets received from NCDEQ
indicate that the updated ERP was received February 24, 2020.
• Since the EPA rule for Dental Dischargers went into effect in 2017, 20 new users and 97 existing
users have been identified and One Time Compliance Reports received. Reporting compliance is
100% for both new and existing users, with reports received from all existing users prior to the
October 12, 2020 deadline.
• IWS for Cary, Morrisville, and South Eastern RTP is conducted on an ongoing basis per
plumbing permit review and approval. Cary also issues IW Ss for facilities where more
information is necessary for determining IU or SIU status. An IWS report for 2014-2019 was
submitted and received March 29, 2019 and was approved April 5, 2019. The next IWS report is
due April 1, 2024. The Town of Apex maintains IWS information for the portion of Apex that
flows to the Western Wake Regional WRF.
• In 2022 there were no SNs or CNs contributing wastewater flow to the South Cary WRF.
• A Pretreatment Compliance Inspection was performed on August 25, 2021 and an inspection
report was received dated December 6, 2021. The inspection report indicated a requirement to
update the SIU Permit for FujiFilm Biotechnologies USA Inc to clarify reporting requirements. A
modified permit was submitted on January 4, 2021 and is currently under review. A pretreatment
Page 2 of 6

Town of Cary
2022 PAR Narrative
program audit was conducted on July 28, 2017 and an audit report was received dated August 24,
2017.
• A Mercury Minimization Plan (MMP) was developed in accordance with NPDES permits, is on
file as per NPDES requirements, and is part of on -going operational activities.
• A copy of the current North Cary, South Cary, and Western Wake WRF Program Information
sheets are included with this 2022 PAR.
• Included is the Historical SNC Report for Cary that lists Catalent as SNC for missed sampling in
the first half of 2017, which is correct. Catalent has not had any additional permit or SNC
violations to date.
Town of Cary SIU Permitting Activities
The first 2 SIUs listed below in the SIU Information Section began discharging to the new
Western Wake Regional WRF on January 6, 2015 and are located within Cary's sewer service
area. One CIU was issued an IUP to discharge to the North Cary WRF on August 16, 2016.
There were no SIU or CIU contributions to the South Cary Water Reclamation Facilities in CY
2022.
1. Total number of enforcement actions taken against SIUs during period: 3
2. Number of Civil or Criminal Penalties against SIUs: 3
3. Total amount of fines levied against SIUs: $744.00
4. Number of SIUs in SNC this period: 0
No Compliance Schedules were in effect during this period.
SIU INFORMATION SECTION
BIOGEN. TOC-051
5000 Davis Drive
Research Triangle Park, NC
A.) Permit Issuance:
• A Permit Application was received on August 29, 2013 in anticipation of wastewater
discharges commencing to the Western Wake Regional WRF.
• SIU discharge permit was submitted to PERCS and received September 26, 2014,
and approved October 22, 2014. Permit was issued to begin on January 6, 2015
(Discharges from this service area began flowing to Western Wake Regional WRF on
January 6, 2015) and expired June 30, 2019.
• A Permit Renewal Application was received March 25, 2019 that included requests
for increased loading allocation.
• SIU Permit was submitted to PERCS and received May 20, 2019, and approved June
14, 2019.
• Permit was renewed with the changes requested by permittee on July 1, 2019 and
expires June 30, 2024. Permit Renewal fees were paid October 10, 2019.
B.) Enforcement Actions:
Page 3 of 6

Town of Cary
2022 PAR Narrative
On September 17, 2022 a Notice of Violation was issued for Industrial User Permit
(IUP) TOC-051 Part II 6 which specifies a duty to mitigate to prevent adverse
impacts on the Publicly Owned Treatment Works (POTW). Biogen's RTP bio-
utilities manager identified a propylene glycol leak to the biowaste system, it was
estimated that approximately 8,000 gallons of 28% propylene glycol was discharged.
A sample of the 28% glycol solution was collected on Monday, September 19 from
Biogen's glycol system. The sample was analyzed and contained a concentration of
340,000 milligrams per liter of BOD. The calculated daily load of BOD discharged
during the time of the glycol discharge was 164,107 pounds, based on an estimated
flow of 57,874 gallons during the ten-hour discharge event. The BOD daily
maximum discharge limit of 3,021 pounds was likely exceeded and exceeds the
Technical Review Criteria (TRC) threshold which is defined as 20 percent above the
permitted limit. A Tier I civil penalty of $300 was issued and paid on November 17,
2022. Monitoring occurred at the Western Wake Regional Water Reclamation
Facility and no facility pass through, upset, or permit limit violation was identified
with the accidental glycol release.
2. FUJIFILM DIOSYNTH BIOTECHNOLOGY. TOC-052
6501 George Watts Hill Drive
Research Triangle Park, NC
A.) Permit Issuance:
• A Permit Application was received on July 11, 2014 in anticipation of wastewater
discharges commencing to the Western Wake Regional WRF.
• SIU discharge permit was submitted to PERCS and received September 26, 2014,
and approved October 22, 2014. Permit was issued on January 6, 2015 (Discharges
from this service area began flowing to Western Wake Regional WRF on January 6,
2015.) and expired June 30, 2019.
• A Permit Renewal Application was received March 27, 2019.
• SIU Permit was submitted to PERCS and received May 31, 2019, and approved June
14, 2019.
• Permit was renewed with no changes on July 1, 2019 and expires June 30, 2024.
Permit Renewal fees were paid December 2, 2019.
• A Permit Application for modification was received September 2, 2020 that included
requests for increased loading allocation.
• SIU Permit was submitted to PERCS and received January 14, 2021, and approved
February 10, 2021. The modification effective date was February 15, 2021.
• Per request in the Pretreatment Compliance Inspection report dated December 6,
2021, a permit modification was issued to clarify reporting requirements, submitted
on January 4, 2022 and is currently under review.
B.) Enforcement Actions:
• On May 27, 2022 a Notice of Violation was issued for missed sampling of Ethanol
for the month of April, per FDBU industrial user permit (IUP) TOC-052 - Part I F.
requires ethanol to be collected by grab sample once per month with a required
Page 4 of 6

Town of Cary
2022 PAR Narrative
detection level of 5.0 milligrams per liter. An Ethanol sample was collected in May
which will constitute as a makeup sample for the missed April sample. A civil
penalty of $144 was issued and paid on June 30, 2022.
On August 30, 2022 a Notice of Violation was issued for a chloride limit exceedance,
Meritech Labs reported the chloride value was 1,490 mg/l (1940 lbs/day). This value
exceeds the permitted daily maximum value of 1300 Ibs/day, it also exceeds the
Technical Review Criteria (TRC) threshold which is defined as 20 percent above the
permitted limit. A Tier I civil penalty of $300 was issued and paid on December 8,
2022.
Noted Discrepancies for minor pH excursions were issued on March 6, 2022 and
March 31, 2022 for pH monitoring within the pH neutralization system. A violation
was not identified at the permitted monitoring location, a proactive noted discrepancy
was issued in order to help maintain compliance at permitted discharge pipe. The
longest duration of these events was 40 minutes. The highest recorded pH of these
events was 12.0 and the system remained compliant on the low end. The permitted
pH allowable range is 5.0 to 11.0. Follow up actions included additional staff training
and additional notification requirements prior to buffer disposal. A Notice of Concern
letter was sent on March 23, 2022 that required a pH grab sample to be taken and
analyzed from the sampling monitoring point -Pipe 03 anytime a pH excursion occurs
in the pH neutralization system.
Noted Discrepancies for minor pH excursions were issued on July 11, 2022 and July
20, 2022 for pH monitoring within the pH neutralization system. A violation was not
identified at the permitted monitoring location, a proactive noted discrepancy was
issued in order to help maintain compliance at permitted discharge pipe. The longest
duration of theses events was 7 minutes, the highest recorded pH of these events was
11.1 and the lowest was 3.9. The permitted pH allowable range is 5.0 to 11.0, follow
up actions included additional staff training and additional notification requirements.
C.) Additional Information:
• On April 6, 2020 an Authorization to Construct was issued for a new waste
neutralization building and upgrades to the neutralization system. On October 15,
2020 the final pretreatment inspections were completed and final system testing
occurred in January 2022. New pH neutralization system became full time
operational in September 2022.
• On July 28, 2020 an Authorization to Construct was issued for a manufacturing site
expansion to include two building additions and one warehouse. On June 17, 2021
the final pretreatment inspections were completed and the buildings were placed
online in early January, 2022.
3. CATALENT PHARMA SOLUTIONS, LLC.
160 N. Pharma Dr
Morrisville, NC
A.) Permit Issuance:
• A permit application was received on December 18, 2014 for fit -up of existing lab
space into a manufacturing suite that falls under 40 CFR Part 439 Subpart D. This
location discharges to the North Cary WRF.
Page 5 of 6

Town of Cary
2022 PAR Narrative
• An Authorization to Construct was issued March 9, 2015 for pretreatment
components that include flow monitoring, temperature and pH monitoring,
inside/outside process waste tanks, and a sampling pit. Construction inspections were
conducted October 13, 2015, March 14, 2016 and May 13, 2016.
• CIU Discharge Permit was submitted to PERCS and received August 15, 2016, and
approved August 26, 2016. The Permit was issued on August 16, 2016 and expired
December 31, 2018. Permit modifications were submitted to PERCS and received
February 20, 2017, and approved March 20, 2017.
• A Permit Renewal Application was received from Catalent on June 27, 2018.
• CIU Permit was submitted to PERCS and received December 7, 2018, and approved
December 21, 2018.
• Permit was renewed with no changes January 1, 2019 and expires December 31,
2023.
B.) Enforcement Actions:
• No enforcement actions were necessary in CY 2022. There was no wastewater
disposal to Cary in CY 2022.
Page 6 of 6

Workbook Name : HWA 2021.xlsx, Worksheet Name: AT
Allocation Table
Headworks last appmved 07 9r78
Allocation Table updated'. 01 14/21
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Allocation Table
Heatlworks last approved 07/29/16
Allocation Table updated 01]14/21
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Workbook Name : HWA 2021.xisx, Worksheet Name: AT
Allocation Table
Headwarks last approved: 0712 1
Allocation Table updated. 01/14/21
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Workbook Name : HWA 2021.xlsx, Worksheet Name: AT
Headworks last approved'. ]/29/16
Allocation Table updated'. 01 1
Town of Cary - Allocation Table
Western Wake Regional Watrer Reclamation Facility
Caryproxata Flow(MGD)=> 1
Cary Average Flow (MGD)=> .33
Cary Uncontrollable Flow (MGD)=> .1
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Handwerker last approved. 07/29/16
Allocation Table updated. 01/14/21
Town of Cary - Allocation Table
Western Wake Regional Watrer Reclamate
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Cary Average Flow (MOD) _>
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Workbook Name : HWA 2021.xlsx, Worksheet Name: AT
Headworks last approved
Allocation Table updated: 114121
Town of Cary - Allocation Table
Western Wake Regional Watrer Reclamatic
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Workbook Name : HWA 2021.xlsx, Worksheet Name: AT
Heatlworks laid approved'. 0]129116
Allocation Taale updated'. 01114/21
Town of Apex - Allocation Table
Western Wake Regional Watrer Reclamation Facility
Apex ProRata Flow (MGDJ=> 1
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Headre rks last approved 07/29/1
Allocation Table updated:1 0 14 21
Town of Apex - Allocation Table
Western Wake Regional Watrer Reclannatic
Apex ProRan Flow (MGD)=> 6.1200
Apex Avenge Flow (MGD)=> 2.
Apex Dabber. MeN: Flaw(PAGE, .fib
Apex %overall MARL (Ibr/day)=> 34.0%
UP
C^....
5
6
6
,6
Workbook Name: HWA 2021.xisx, Worksheet Name: AT
a s..—
sra
���
ss1
rrr1111
�11��
ssrr
arrr—
s1
A... MAHL (.J...) _>
P...... UL.=.U..^. ^.P=..^..^...•..^<.^...C.....rnnvn.n66922 fi086 6985 11.778fi520B 0196924 0.829 3.6296 193%
(-A) 00354 W28 1W26 0060 L....^07853 00621 00222 0577 01331
I..Ai..„....,., I^ ... ..(MAIL)(^J... 54233 16364 34965
<. ., (.J...0.0000 0.000 0.0000 0.000000 0.0000 0.0000 MAIL—(,,J...) 5233 1636A
A.— .(MAIL)100% 100% 100% 100% 100% 493%
P..MAI IL WW%
99% 87% 96% 89% 5 P...... MAI IL(.J..y)-> 09841 091 02498 OW2896 01213 05338 a1068 00232

10
Workbook Name : HWA 2021.x1sx, Worksheet Name: AT
HeaMorks last approved 071 16
Allocation Table updated-. 01/14/21
Town of Apex - Allocation Table
Western Wake Regional Watrer Reclamatio
Apex PmRala Flow (Moo)=> 6.1200
Apex Average Flaw(MOD)=> 2.66
Apex Uncontrollable Flow, (MOD)=> 2.86
Apex %overall MAHL (Ibs/day) _>
----------
lkan—®—�—
all
Ap.> MAI IL 6.4...)-> 11,7994 2 30&8 421.09 E15562
U.........— C..,,..... ...... lmv7L)-> 01972 6371 746
U....�—..�. L.. (.. J..,)-> 4.3740 1413.37 165. K)
L..A.,„—.—I..,,,,,,(MA IL) (I. J..,)-> 74245 131731 25559
I—P....--.. L,.,,„.. (,.J..r)-> 0.0000 0.60 0.00
MAIL—, (�.J...1 _> 74246 131731 255.59 A,..„. —(MAIL).., ....�..�. (%)-> 100% 100% 100% MAI IL ...��.,........(%)-> 63% 46% 61%
5 11--, MAUL 0 61 9245 248] 8300

Allocation Table
3adworks last approved: 06/24/19
Ilocation Table updated: 06/24/19
Permits last modified: 1/Ol/19
Party=
NPDEW-
IUP
Count
2
3
4
5
6
7
8
9
10
> Town of Cary - North Cary WRF
> NC-0048879
FLOW
Industry Type Renewal Modificatior Date Permit Limits
STRY NA Permit Pipe of Effective Effective Permit
number number Industry Date Date Expires MGD gal/day
Catalent Ph
TOC-053
CIU
12/30/19
0.0140
14,000
Column Totals =>
0.0140
14,000
Basis=>
MAHL from HWA (lbs/day) => NPDES Permitted
Jncontrollable Loading (lbs/day) =>
)le for Industry (MAIL) (lbs/day) =>
al Permitted to Industry (lbs/day) =>
MAIL left (lbs/day) =>
✓. Ind. (MAIL) still available (%) =>
'ercent MAHL still available (%) =>
5 Percent MAHL (lbs/day) =>
NPDES

CBOD
Permit Limits
TSS
Permit Limits
Ammonia
Permit Limits
Arsenic
Permit Limits
Cadmium
Permit Limits
Conc. Load
mg/I lbs/day
Conc. Load
mg/l Ibs/day
Conc. Load
mg/I Ibs/day
Conc. Load
mg/I Ibs/day
Conc. Load
mg/I lbs/day
0
0
0
1
0.0000
0.0000
Criteria
Criteria
Criteria
Stream Std
Stream Std
25020
35528
4503.60
1.0978
0.1830
14993
19124
2206.38
0.1467
0.0293
10027
16405
2297.22
0.9511
0.1536
0
0
0.00
0.0000
0.0000
10027
16405
2297.22
0.9511
0.1536
100.0%
100.0%
100.0%
100.07/.
100.0%
40.1 %
46.2 °/a
51.0 %
86.6 %
84.0 %
12511 1 17761 1 225.181 1 0.05491 1 0.0091

Chromium
Permit Limits
Copper
Permit Limits
Cyanide
Permit Limits
Lead
Permit Limits
Mercury
Permit Limits
Cone. Load
mg/I Ibs/day
Cone. Load
mg/I Ibs/day
Cone. Load
mg/l Ibs/day
Cone. Load
mg/l Ibs/day
Cone Load
mg/I Ibs/day
0.000189
0.00002
0.0000
0.0000
0.0000
0.0000
0.000022
Stream Std
Stream Stoll
Stream Std
Stream Std
Stream Std
3.6900
12.1917
0.9739
1.2386
0.054073
0.1467
2.6406
0.1467
0.2934
0.007570
3.5433
9.5511
0.8272
0.9452
0.046503
0.0000
0.0000
0.0000
0.0000
0.000022
3.5433
9.5511
0.8272
0.9452
0.046481
100.0%
100.0%
100.0%
100.0%
100.0%
96.00
78.3 %
84.9 %
76.3 %
86.0 %
0.1845

Molybdenum
Permit Limits
Nickel
Permit Limits
Selenium
Permit Limits
Silver
Permit Limits
Zinc
Permit Limits
Cone. Load
mg/I Ibs/day
Cone. Load
mg/I Ibs/day
Cone. Load
mg/I Ibs/day
Conc. Load
mg/I Ibs/day
Cone. Load
mg/I Ibs/day
0.0000
0.0000
0.0000
0.0000
0.0000
Ceiling
Stream Std
Stream Std
Stream Std
Mon. Avg.
3.7104
8.2764
0.6038
0.0145
60.673-1
0.1467
0.2934
0.1467
0.0000
10.7972
3.5637
7.9830
0.4571
0.0145
49.8765
0.0000
0.0000
0.0000
0.0000
0.0000
3.5637
7.9830
0.4571
0.0145
49.8765
100.0%
100.0%
100.0%
100.0%
100.0%
96.0 %
96.5 %
75.7 %
100.0 %
82.2 %
0.18551 1 0.41381 1 0.03021 1 0.00071 1 3.0337

TN (TKN basis)
Permit Limits
Total Phos.
Permit Limits
Fluoride
Permit Limits
Cone. Load
mg/1 Ibs/day
Cone. Load
mg/1 Ibs/day
Cone. Load
mg/1 Ibs/day
0.00
0.00
0.0000
Criteria
Criteria
Stream Sttl
7005.6000
900.72
113.21T
3116.1555
394.33
29.3401
3889.44
506.39
93.8754
0.00
0.00
0.0000
3889.44
506.39
83.8754
100.0%
100.0%
100.0%
55.5 %
56.2 %
74.1 %
45.03601 1 5.6608
RECEIVED
FEB 2 7 2023
NC,DEO/DWR/NPDES

Pharmaceutical Allocation Table
norw- orLary
IUP
Count
1
3
4
5
6
7
8
9
10
Workbook Name: POHWA_2019.xlsx
Worksheet Name: Linked PAT
Printed: 2/15/2023, 7:29 AM
Page 1 of 1
INDUSIRY NAMES
... ... ..
Catalcnl Pharma Solutions
FLOW
Permit Limit
MGD gal/day
1 0 01401 14,000
Benzene (c)
Industry Result
Cone. Load
mg/I Ibs/day
Chlorobenzene
Industry Result
Cone Load
mg/I Ibs/day
Chloroform (c)
Industry Result
Con,. Load
mg/1 Ibs/day
Methylene Chloride (c)
Industry Result
Cone. Load
mg/I Ibs/day
3.0 0,3503
Toluene
Industry Result
Cone. Load
mg/1 Ibs/day
Xylenes
Industry Result
Cone. Load
mg/I Ibs/day
1,2-Dichloroethane
Industry Result
Cone. Load
mg/l Ibs/day
Column Totals =>1
0 01401
14,000
0.3503
Basis
MAIIL from OHWA (Ibs/day) _>
"Total Loading from Industry (Ibs/day) >
Allowable loading left (Ibs/day) _>
Percent MAHL still available (o) ->
5 Percent MAHL (Ibs/dav) _>
Filename: Pharmaceutical OHWA
Revision Date. September, 2001
Fresh Fresh Fresh
Human Health Screen Screen Human Health Screen
Human
Health

Pretreatment Program Info Database
printed on: 1 /19/2023
for Program Name Cary
WWTP Name Western Wake Regional
Program Approval Date 08110/1984
Pretreatment Status Full
Region RRO
County Wake
NPDES Number
Stream Information IWC % at 7Q10 7.39
7Q10 Flow cfs / mgd 349 / 225.45
1,010 Flow cis / mgd 282.39 / 182.51
Stream Classification WS-V
Basin Number CPF 03-06-07
Receiving Stream Name CAPE FEAR RIVER
NC0088846
NPDES Effective Date 11/01/2016
Last PAR Rec 02/21/2022
PAR Due Date03/01/2023
mercury
NPDES Expire Date 07/31/2021
Current Fiscal 08/25/2021
1631
required d
YearPCl Done
es
POTW is Primary WWTP TRUE
Last Audit on 07/28/2017
Audit Year Next 21/22
Design Flow mgd 18.0000 % Design
mgd is SIU permitted F3.75
Permitted SIU flow (mgd) [Pt_SIU) .675
WWTP SIU's Program SIUs 3
WWrP CIU's 0 Program CIUs�
HWA LTMP
IWS SUO
ERP
date Inactive Date Next Due
04/01/2024
Date Received by DWR
01/14/2021 01/19/2017
03/29/2019 02/13/2012
11/18/2019
Date Approved
04/18/2017
04/05/2019 04/12/2012
03/17/2020
Adopt Date Required
Date Adopted
12/15/2011
Info in this Box from Pt Contacts
Date Date Date
PT_Pro Attended Attended Attended
Formal Name g. Prime Phonel ext Fax HWA Wksp IUP Wks❑ PAR Wkso
Mr. Donald Smith jPrm
[phone]
[phone] 11
3/15/2001 1 9/27/2011
1/30/2001
[e-mail]
I
Wastewater Collections Program
jP0 Box 8005
k7512
Mr. Jamie Revels, P.E.
1
[phone]
[e-mail]
I
Utilities Director
1P.0. Box 8005 IP7512
Mr. Donald Johnson
jPrim
919-414-8092
[e-mail]
Utility Pretreatment 1400 James Jackson Avenue
7513
DWR Central Office Contact JPretreatment Staff
DWR Regional Contact heng Zhang

Pretreatment Program Info Database
printed on: 1 /19/2023
for Program Name Cary
WWTP Name North Cary
Program Approval Date 08110/1984
Pretreatment Status Full
Region RRO
County Wake
NPDES Number NC0048879
NPDES Effective Date 01/01/2019
Last PAR Rec 02/21/2022
PAR Due Date03/01/2023
mercury
NPDES Expire Date 02/28/2023
Current Fiscal 08/25/2021
1631
required
Year PCI Done
POTW is Primary WWfP FALSE
Last Audit on 07/28/2017
Audit Year Next 21/22
es
Design Flow mgd 12.0000 % Design mgd is SIU permitted
FO.12
Permitted SIU flow (mgd) [Pt—SIU) .014
VWVrP SIU's
1 Program SIUs
WWTP CIU's
1 Program CIUsR
HWA 4 LTMP
JWS SUO
ERP
date Inactive Date Next Due
03/31/2024
04/01/2024
Date Received by DWR
03/26/2019 08/27/2019
03/29/2019 02/13/2012
11/18/2019
Date Approved
06/24/2019 11/19/2019
04/05/2019 04/12/2012
03/17/2020
Adopt Date Required
Date Adopted
12/15/2011
Info in this Box from Pt Contacts
Date Date Date
PT_Pro Attended Attended Attended
Formal Name p,Prime Phonel ext Fax HWA Wka. II IO1A&- oeo rnm�..
Mr. Donald Smith
Prim
[phone]
[phone]
3/15/2001
1 9/27/2011 1/30/2001
[e-mail]
Wastewater Collections Program jP0
Box 8005 IF7512
Mr. Jamie Revels, P.E. 1 11(919)
469-4303
[e-mail]
IUtilities Director 1P.O.
Box 8005
7512
Mr. Donald Johnson jPrim
919-414-8092
[e-mail]
Utility Pretreatment 1400
James Jackson Avenue JR7513
DWR Central Office Contact JPretreatment Staff
DWR Regional Contact heng Zhang
RECEIVED
FEB 2 7 2023
NCDEQ/DWR/NPDES

Pretreatment Program Info Database
printed on: 1/19/2023
for Program Name Cary
WWTP Name South Cary
Program Approval Date 08110/1984
Pretreatment Status Full
Region RRO
County Wake
NPDES Number
NPDES Effective Date NC0065102
12/01/2018
Last PAR Rec 02/21/2022
PAR Due Date03/01/2023
mercury
NPDES Expire Date 04/30/2023
Current Fiscal 08/25/2021
1631
required
Year PCI Done
POTW is Primary WWTP FALSE
Last Audit on 07/28/2017
Audit Year Next 21/22
es
Design Flow mgd 12.8000 % Design
mgd is SIU permitted
0.00
Permitted SIU flow (mgd) [Pt_SIU)
WWTP SIU's
W
WTPCIU'S
Program SIUs
---� LT-.�
HWA 1 M--P
IWS * SUO
ERP
ProgramClUsR
date Inactive Date Next Due
01/01/2999
04/01/2024
Date Received by DWR
05/13/2019 01/19/2017
03/29/2019 02/13/2012
11/18/2019
Date Approved
08/06/2019 04/18/2017
04/05/2019 04/12/2012
03/17/2020
Adopt Date Required
Date Adopted
12/15/2011
Info in this Box from Pt Contacts
Date Date Date
PT_Pro Attended Attended Attended
Formal Name o.Pnme Phonel ext Fax HWA Wksm II IP VM�r PCP IAAren
Mr. Donald Smith
Prim
[phone]
1
1(919) 469-4304
3/15/2001 1 9/27/2011
1/30/2001
[e-mail]
I Wastewater Collections Program 1PO
Box 8005
IP7512
Mr. Jamie Revels, P.E.
1 11(919)
469-4303
[e-mail]
I Utilities Director 1P.O.
Box 8005
7512
Mr. Donald Johnson
jPrim
919-414-8092
[e-mail]
Utility Pretreatment 1400
James Jackson Avenue 7513
DWR Central Office Contact JPretreatment Staff
DWR Regional Contact Fheng Zhang

„VMCREPORT
atalent Pharma Solutions, LLC
IUP# TOC-053
IUP Status: Active
2016 2017 2016 2019 2020 2021 2022
let half 12nd half 1st half 12nd half 1st half 12nd half tat half 12nd half tat half 12nd half tat half 12nd half tat half 12nd half
PreviousNames:
Pipe # 01
Reporting
XI
SIU WON D..Pt,.,,
Phamamuticals
An W in a semi-annual period indicates snc for the period for the respective parameter.
INTED ON: 1/19/2023 This information is compiled from many sources, and has not been verified. PAGE 17

Chapter 9, PAR Guidance
Pretreatment Performance Summary (PPS)
1. Pretreatment Town Name: Town of Cary
2. "Primary" NPDES Number NC00 88846
or Non -Discharge Permit # if applicable =>
3.
PAR begin Date, please enter 01/01/yy
3. _>
1/1/2022
4.
PAR end Date, please enter 12/31/yy
4. _>
12/31/2022
5.
Total number of SIUs, includes CIUs
5. =>
3
6.
Number of CIUs
6. =>
1
7.
Number of SIUs with no IUP, or with an expired IUP
7. =>
0
8.
Number of SIUs not inspected by POTW
8. =>
0
9.
Number of SIUs not sampled by POTW
9. =>
0
10.
Number of SIUs in SNC due to IUP Limit violations
10. =>
1
11.
Number of SIUs in SNC due to Reporting violations
11. =>
0
12.
Number of SIUs in SNC due to violation of a compliance schedule, CO, AO or similar
12. =>
0
13.
Number of CIUs in SNC
13. =>
0
14.
Number of SIUs included in public notice
14. =>
1
15
Total number of SIUs on a compliance schedule, CO, AO or similar
15. =>
0
16.
Number of NOVs, NNCs or similar assesed to SIUs
16. =>
3
17.
Number of Civil Penalties assessed to SIUs
17. =>
3
18.
Number of Criminal Penalties assessed to SIUs
18. =>
0
19.
Total Amount of Civil Penalties Collected 19. =>
$
744.00
20.
Number of IUs from which penalties collected
20. =>
2
Votes:
AO Administrative Order IUP Industrial User Pretreatment Permit POTW
CIU Categorical Industrial User NNC Notice of Non -Compliance SIU
Publicly Owned Treatment Works
Significant Industrial User
CO Consent Order NOV Notice of Violation SNC
Significant
Non -Compliance
IU Industrial User PAR Pretreatment Annual Report
revised 1 /2018: PAR PPS 2018

THIS PAGE REPLACED WITH
REVISION
Chapter 9, PAR Guidance
Pretreatment Performance Summary (PPS)
I.
2.
Pretreatment Town Name: Town of Cary
"Primary" NPDES Number NC00 88846
or Non -Discharge Permit # if applicable =>
3.
PAR begin Date, please enter 01/01/yy
3. =>
1/1/2022
4.
PAR end Date, please enter 12/31/yy
4. =>
12/31/2022
5.
Total number of SIUs, includes CIUs
5. =>
3
6.
Number of CIUs
6. =>
1
7.
Number of SIUs with no IUP, or with an expired IUP
7. =>
0
8.
Number of SIUs not inspected by POTW
8. =>
0
9.
Number of SIUs not sampled by POTW
9. =>
0
10.
Number of SIUs in SNC due to IUP Limit violations
10. =>
0
]I.
Number of SIUs in SNC due to Reporting violations
11. =>
0
12.
Number of SIUs in SNC due to violation of a compliance schedule, CO, AO or similar
12. =>
0
13.
Number of CIUs in SNC
13. =>
0
14.
Number of SIUs included in public notice
14. =>
0
15
Total number of SIUs on a compliance schedule, CO, AO or similar
15. =>
0
16.
Number of NOVs, NNCs or similar assesed to SIUs
16. =>
3
17.
Number of Civil Penalties assessed to SIUs
17. ->
3
18.
Number of Criminal Penalties assessed to SIUs
18. =>
0
19.
Total Amount of Civil Penalties Collected 19. =>
$
744.00
20.
Number of IUs from which penalties collected
20. =>
2
Votes:
AO A., ,..--.:0,.- IUP I.,d - ,, U-1 P..--.- P.rm„ POTW
CIU C. _- - I . .r, .. U-r NNC Noy -r N-Cor.c-- SIU
P, .- 0-.., T,,..,., - W.
S e^ r ­L.o. - ,n U,.,
CO Co 1-1 0-1 NOV N., -.,r V ..,..,. SNC
S., ...- N.-C.I.I.....
U I ..,. U.- PAR R.u.--A..- R.P,.r
,- 1/2018 PAR PPS 2018

Pretreatment Annual Report (PAR)
Significant Non -Compliance Report (SNCR)
W WTP = Wastewater Treatment Plant, use separate form for each W WTP.
SIU = Significant Industrial User
SNC = Significant Non -Compliance
PAR covers this calendar year => 2022
Control Authority=Program=Town Name => Town of Cary
W WTP Name => North Cary WRF
NPDES # _> NCO048879
A SNCR Form must be submitted with every PAR, ulease write "None "if you had No SIUs in SNC durinv enlendar vear
IUP
#
Pipe
#
Industry Name
Parameter
or "Reporting"
SNC? ( Yes / No )
for each 6-month period.
Jan. - June
July - Dec.
TOC-053
I
Catalent Pharma Solutions, LLC
None
No
No
rAaacn a copy or me Division's 'S Us in SNU Histoncal Report" for your POTW's SIUs behind this page.
Is the database correct ? Notify the Division of any errors ! Database indicates SNC history for previous years.
EVERY SNC MUST be explained in the Narrative, How was, is, or will it be resolved?
REPEAT SNCs are serious matters that MUST be explained in the Narrative.
Fe.m , .. PAR,SNCR.2001
D.- R.. ... 1 /4/2001

Pretreatment Annual Report (PAR)
Significant Non -Compliance Report (SNCR)
WWTP = Wastewater Treatment Plant, use separate form for each WWTP.
SIU = Significant Industrial User
SNC = Significant Non -Compliance
PAR covers this calendar year => 2022
Control Authority--Program--Town Name => Town of
WWTP Name => Western Wake Regional
NPDES # => NCO088846
A SNCR Form must be submitted with every PAR, please write "None " if you had No SIUs in SNC during calendar year
1 UP
#
Pipe
#
Industry Name
Parameter
or "Reporting"
SNC? ( Yes / No)
for each 6-month period.
Jan. - June
July - Dec.
TOC-051
9
Biogen
None
None
None
TOC-052
3
FujiFilm Diosynth Biotechnologies USA In
Mecury
None
Yes
Attach a copy of the Division's "SIUs in SNC Historical Report" for your POTW's SIUs behind this page.
Is the database correct ? Notify the Division of any errors ! Database indicates SNC history for previous years.
EVERY SNC MUST be explained in the Narrative, How was, is, or will it be resolved?
REPEAT SNCs are serious matters that MUST be explained in the Narrative.
Form name: PAR,SNCR,2001
Date Revised: 1I4I2001

THIS PAGE REPLACED WITH REVISION
Pretreatment Annual Report (PAR)
Significant Non -Compliance Report SNCR
WWTP = Wastewater Treatment Plant, use separate form for each WWTP.
SIU = Significant Industrial User
SNC = Significant Non -Compliance
A SNCR Form must be submitted with every P�
f U P P� P e Industry Name
TOC-051 9 Qiocen
3 IFuiiFilm Di
PAR covers this calendar year => 2022
Control Authority=Program=Town Name => Town of Cary
WWTP Name => Western Wake Regional
NPDES # => NC00RRS46
lease write "None " if you had No SIUs in SNC
USA
Parameter
or " Renortim
Nonc
Nonc
luring calendar year
SNC? (Yes/No)
ror each 6-month perl0d.
Jan. - June July - Dec.
Nonc None
None I None
Attach a copy of the Division's "SIUs in SNC Historical Report" for your POTW's SIUs behind this page .
Is the database correct ? Notify the Division of any errors ! Database indicates SNC history for previous years.
EVERY SNC MUST be explained in the Narrative, How was, is, or will it be resolved?
REPEAT SNCs are serious matters that MUST be explained in the Narrative.
F.- ­.,: PAR.5NCR,2001
0- R-, 114/2001

Pretreatment Annual Report (PAR) Control Authority, Town of "Cary Industry
Town Name=> Cary Name Biogen
Industrial Data Summary Form (IDSF) Use separate forms for each industry/pipe t WTP Name=> Western Wake Regional IUP # TOC-051
Enter BDL values as < (value) NPDES # _> NC0088846 Pipe # 09
1 st 6 months, dates => to
2nd 6 months, dates => to
Total # of samples =>
* Maximum (mg/1) _>
* or Maximum (lb/d) _>
* or _ Average (mg/1) _>
* or Average Loading (lb/d) _>
% violations,(chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) _> o
% violations,(chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) _>
Total # of samples =>
* Maximum (mg/1) _>
* or Maximum (lb/d) _>
* or _ Average (mg/l) _>
* or Average Loading (lb/d) _> _
% violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) _> o
% violations,(chronic SNC is >= 660;.) _>
% TRC violations, (SNC is >= 33 %) _>
Total # of samples =>
* Maximum (mg/1) _>
* or Maximum (lb/d) _>
* or Average (mg/1) _>
* or Average Loading (lb/d) _>
% violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) _> o
% violations,(chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) _>
Flow, mgd
BOD
TSS
Ammonia
Ist 6 months
2nd 6 months
1st 6 months
2nd 6 months
Ist 6 months
2nd 6 months
1st 6 months
2nd 6 months
181
184
13
13
13
13
13
13
0.24
0.34
1000
1200
150
120
150
110
1187.8
1384.8
122.6
151.5
159.9
114.8
0.12
0.15
615.1
664.
70.1
54.
45.
.2
565.1
.8
0.9
71.1
46.5
38.7
0%
0%
O%
0%
0
0°/n
0%
0%
0%
0%
0%
0%
00
0%
O%
0%
N/A
N/A
0%
0%
0%
0%
0%
0%
N/A
N/A
0%
0%
0%
0%
0%
0%
Arsenic
Cadmium
Chromium
ICOD
1st 6 months
2nd 6 months
1st 6 months
2nd 6 months
1st 6 months
2nd 6 months
1st 6 months
2nd 6 months
2
2
2
2
2
2
N/A
N/A
<0.0038
<0.0032
<0.0003
<0.00025
0.0028
<0.0025
N/A
N/A
<0.0040
<0.0032
<0.0002
<0.0003
0.0029
<0.0026
N/A
N/A
< .0024
70.0021
70.0002
<0.0002
0.0014
70.0013
N/A
9/A
< .0024
< .0021
70.0002
<0.0002
0.0014
70.0013
7/A
N/A
N/A
N/A
N A
N A
N/A
N/A
N A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N A
N A
N/A
N A
N A
N A
N/A
N/A
INIA
N/A
N/A
N/A
N/A
N/A
Copper
Cyanide
Lead
Mercury
1 at 6 months
2nd 6 months
1 st 6 months
2nd 6 months
1 st 6 months
12nd 6 months
I st 6 months
2nd 6 months
2
2
2
2
2
2
2
2
0.0515
0.0546
0.019
0.011
<0.0015
<0.0033
0.0000172
0.0000296
0.0413
0.0564
0.01995
0.0109
<0.0016
<0.0033
0.0000138
0.0000306
0.0360
0.0383
0.0095
0.0055
<0.0013
<0.0022
0.0000096
0.0000218
0.0314
0.0391
0.0099
0.0055
<0.0012
<0.0022
0.0000080
0.0000223
N/A
N/A
0%
0%
N/A
N/A
0%
0%
N/A
N/A
00/
0%
N/A
N/A
0%
0%
N/A
N/A
N/A
NIA
N/A
N/A
INIA
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
BDL -> B.,.- D--..,, L. m., m,/. ->
PIOTW ... IUP-> I,. ,.,.,�.� U.. P.. " ..... ., ..
. . m ele -> p
.. ..w.. P�.... �,,.�.... .w ..e.. w... �. ��. SNCN..-C.mp, .,,.. mg.-> m �1.,..,....... p..
A., �. Q.. • 6-m „ & ,. BDL �1/2BDL TRC -> T. R.,, „, C., W WTP-> . ple
Cn.pu.: PARG-a.... F,i...m,: PAG�LQSF. .R.C�a,,.o"A. R1.1"B,p.°., 12,13,14 B--IDSF F.,-, C.p,..,- ... .... PAR N„ms.....- ... ... . IUP,.p.-P.s.

Pretreatment Annual Report (PAR)
Industrial Data Summary Form (IDSF)
Use separate forms for each industry/pipe
Enter BDL values as < (value)
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) =>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
% violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) _>
% violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 °/a) =>
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) =>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
• violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) _> o
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 °/a) =>
Total # of samples =>
* Maximum (mg/I) =>
* or Maximum (Ib/d) =>
* or Average (mgA) =>
* or Average Loading (lb/d) =>
• violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) _> o
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) =>
Industry Name Biogen
IUP # TOC-051
Pipe # 09
CBOD
Fluoride
TKN
JTN
1st 6 months
2nd 6 months
I st 6 months
12nd6mcinths
1st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
980
970
712
775
180
160
180
161
1014.3
984.4
0.126
70.498
239.8
273.1
239.8
273.1
550.4
538.5
0.06
< .275
87.4
77.0
87.7
77.7
504.8
659.4
0.063
-N
<0.251
82.9
102.6
83.2
102.8
N/A
N/A
TA-
N/A
N/A
-NTA-
0%
0%
N/A
N/A
N/A
N/A
N/A
N/A
=0=
121
N/A
N/A
1NA
N/A
N/A
N/A
0.
O%
N/A
N/A
N/A
I N/A
N/A
N/A
Molybdenum
Chloride
Ethanol
JTP
lst 6 months
2nd 6 months
1st 6 months
12nd 6 months
1st 6 months
12nd 6 months
1st 6 months
2nd 6 months
70.003
70.0060
2100
I100
731
2.80
]00
85.0
<0.0020
70.0060
1868.5
20 1.4
0.25
3.95
1 .
71.
< .0019
<0.0043
987.7
652.2
0.04
1.I1
25.9
25.3
<0. 17
< .0043
10.4
866.1
0.04
1.45
25.7
27.5
N/A
N/A
0%
0%
N/A
N/A
0%
0%
N/A
N/A
0%
0%
N/A
N/A
0%
0%
N/A
1 N/A
121
0%
1N/A
N A
0%
0%
N A
N/A
0%
0%
N A
N A
0%
0%
Nickel
Selenium
Silver
Zinc
1 st 6 months
2nd 6 months
1 st 6 months
12nd 6 months
1st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
0.002
<0.005
<0.0031
<0. OS
<0. Ol
70.0005
0.05
0.12
. 025
70.0052
70.003
70,005
<0. 4
70.0005
0.049
0.119
0.0012
<0.003
70.002
70.003 55
70.0003
70.000 777
0.0332
0.0743
0. 012
70.003
<0.0 26
70. 38
<0.0003
70.0 3
0.0325
0.0745
N A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N A
N/A
IN/A
N/A
N A
BDL -> B...- D.- L. a/, > m,�i a.. m....
IUP -> I..--.i U... P.-L ld/d -> ....d. Pill lly
R..., dw .a. _ ,. < <,,,.. SNC -> S a. .,, N..-C.m ..... mad -> , 110 a... P.. d.y
&,BDL, 1/2BDL. TRC ->T. iR,,, „.C. WWTP->
C..a..•: PAR G.,...d. F......,.: PA112�_AQSE,...,R„4a,.d„n "Ap ,S, J-1aWB. P.a.. 12, 13. 14 Bi- IDSF F.- Clip, - -.,. y,.. PAR N,,.. d....d..., 1.1 ,.,. IUP a, a.- P.a.

Pretreatment Annual Report (PAR)
Industrial Data Summary Form (IDSF)
Use separate forms for each industry/pipe
Total # of samples =>
* Maximum =>
* or Minimum =>
% violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) _> o
% violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) _>
Total # of samples =>
* Maximum (mg/1) _>
* or Maximum (lb/d) _>
* or _ Average (mg/1) _>
* or Average Loading (Ib/d) _>
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) _>
• violations, (chronic SNC is >= 66%) _> r
% TRC violations, (SNC is >= 33 %) _>
Total # of samples =>
* Maximum (mg/1) _>
* or Maximum (lb/d) _>
* or _ Average (mg/1) _>
* or Average Loading (lb/d) _> _
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) _> o
• violations, (chronic SNC is >= 66%) _> r
% TRC violations, (SNC is >= 33 %) _>
Industry Name Bingen
lUP # TOC-051
Pipe # 09
bUL -> tS n.., U.-., .. L.-, ../� ->
FOTW m,,.. ,,.,.. ., o,,..r ..,... IUP-> I. ,,.....� U. , P.. m, �,..m....
A., ..w.. P�.... �.,�..,. .w .. .g. w... �,. �.. SNC ->Ss N.C.-
�Q.. .6 .&�, BDL eI/2BDL. TRC ->T. WWTP
Ch.,...: PAR G.a.... F—.,.m.: PP0.�A@SE..M,R..:.m,.a,G...9.q,9.%.1.99AB...... 12,13,14 B,.,,. IDSF F..m. C.,, ,e.,PAR N„mo......,,. r—..—IUP,.o.-Pa.

Pretreatment Annual Report (PAR) Industry Name
Industrial Data Summary Form (IDSF) luP #
Use separate forms for each industry/pipe Pipe #
Enter BDL values as < (value)
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) =>
* or Average (mgfl) _>
* or Average Loading (lb/d) =>
• violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
• violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) =>
* or Average (mg/I) =>
* or Average Loading (lb/d) =>
• violations, (chronic SNC is>= 66%) =>
% TRC violations, (SNC is >= 33 %) _>
% violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC
Total # of samples =>
* Maximum (mg/1) _>
* or Maximum (lb/d) =>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is>= 33 %) =>
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) =>
MUM=
SEEM=
mum=
EEOMMZO�
�TW m,,...°... .. ,..,, °°° °, .,,.,. BDL -> B—w D.. .�.. L.— .,g6 -> .. m, ,..m. ,
IUP->I°°°.,.... U..' P..m,. .1.->°°„° ,°, .>
.°_.. R.....°°,°... .w ...g. w.... � SNC -> S.,. °. °.m°. -> M...— g.
A„s >.. �. Q.. . 6 . & .. BDL a1/2BDL, TRC -> T. . R... w C. WWTP->
Cn.°...: PAR & ..°.. F... ,,.,..: PPk72Af�5F,...�R..Gi..m..n d.; dd.9.9. ]..1294B. °.°.. 12, 13. 14 B—, IDSF F.— C.a, — -- >°,.. PAR N„m........,..°.. IUP °.°., � P.s. ..

Pretreatment Annual Report (PAR) Control Authority, 'Town of Cary Industry
Industrial Data Summary Form (IDSF)
Town Name => Cary Name Catalent Pharma Solutions, LLC Use separate forms For each industry/pipe W WTP Name => NCW RF ( North Cary) IUP # TOC-053
Enter BDL values as < (value) NPDES # => NC0048879 Pipe # 01
1 st 6 months, dates => to 6/3072022
2nd 6 months, dates => to
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d)=>
* or Average (mgA) =>
* or Average Loading (lb/d) =>
% violations,(chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) => o
% violations,(chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) => s
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) =>
* or _ Average (mg/1) =>
* or Average Loading (lb/d) =>
% violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) => o
% violations,(chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) =>
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) =>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
% violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) _> o
% violations,(chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) =>
Flow, mgd
BOD
TSS
Ammonia
1st 6 months
2nd 6 months
1st 6 months
2nd 6 months
1st 6 months
2nd 6 months
1st 6 months
2nd 6 months
0/7ergo
� 0/n .7
tl 0/.
tl 7 ,.q,
0/.7„q.
0/. nr
0 9e
0/U .
5 77
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.007
0
0
0
0
0
0
0
0
0.0
.00
0.00
0.0
.00
0.00
0.00
0. 0
0
0
0
0
0
0
0
0%
0%
0°/u
0°/g
07
0°/g
0%
0%
0%
0%
0%
0°/g
0%
0%
0%
0%
N/A
N/A
0%
0°/q
0%
0%
0%
0%
N/A
N/A
0%
0%
0%
0%
0%
0%
Arsenic
Cadmium
Chromium
COD
1st 6 months
2nd 6 months
1st 6 months
2nd 6 months
Ist 6 months
2nd 6 months
1st 6 months
2nd 6 months
0/� e,q.
0/- „q.
0/�
0/� „q.
0/7 „q.
0/7 g.
N/A
N/A
0.00
0.00
0.00
0.00°
0.00�
0.00
N/A
N/A
0
0
0
0
0
0
N/A
N/A
.00
0.00
0.
0.00
0.10
0.00
N/A
N/A
0
0
0
0
0
0
N/A
N A
N A
N/A
N/A
N/A
N A
N A
N/A
N/A
N/A
IN/
N/A
N/A
N/A
N/A
N/A
/A
N/A
N/A
N A
N A
I N/A
I N/A
N/A
N/A
I N/A
N/A
N/A
N/A
N/A
N/A
opper
Cyanide
Lead
Mercury
1st 6 months
2nd 6 months
1st 6 months
2nd 6 months
1st 6 months
12nd 6 months
1st 6 months
2nd 6 months
D/n e,q.
0/n ar9e
0/.
0/n e,ge
D/n n,ge
D/n n,q.
t]/n erg•
D/n urg•
0.00
0.000
0.00e
0.00°
0.00�
0.00�
0.00tl
0.000
0
0
0
0
0
0
0
0
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0
0
0
0
0
0
0
0
N/A
N/A
0%
0%
N/A
N/A
0°/.
0%
N/A
N/A
0°/g
0%
N/A
N/A
0%
0%
N/A
N/A
N/A
N/A
N/A
INIA
INIA
N/A
N/A
I N/A
N/A
N/A
N/A
I N/A
N/A
N/A
POTW „�:, ..,...., »„:, ... m .n.�. UUL -> B-- U..,...,. L m., male -> m� g , , P.
IUP-> I.,.....1.1 U..' P.,m. ....,
AV '-, P�...., .. e..... r ,q.. w.,..... SNC ->S.g..--N..-C..,w,.- ..g.->Pm����.. g, .., P„ ,
6-m P & . BDL o1/2BDL, TRC-> T. . R... w C., WWTP
C..P,.,. PAR G....- F... ,,.-.; PPI�AQBFi,.,,.R..G. ,>�,; /d„�,g. ]„da94B. P.q.. 12,1114 B-- IDSF F.,-, C.,, .,. ...,,, ,.- PAR N„m.11 ..P. ,.. r..... . IUP P.P P,q. .r

Pretreatment Annual Report (PAR)
Industrial Data Summary Form (IDSF)
Use separate forms for each industry/pipe
Enter BDL values as < (value)
Total # of samples =>
* Maximum (mg/I) _>
* or Maximum (lb/d) _>
* or _ Average (mgA) _>
* or Average Loading (lb/d) _>
%violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) _> o
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC
Total # of samples =>
* Maximum (mg/1) _>
* or Maximum (lb/d) _>
* or Average (mgA) _>
* or Average Loading (lb/d) _>
% violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is>= 33 %) _> o
% violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) _>
Total # of samples =>
* Maximum (mg/1) _>
* or Maximum (lb/d) _>
* or Average (mg/1) _>
* or Average Loading (lb/d) _>
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is>= 33 %) _>
Industry Name Catalent Pharma Solutions, LLC
IUP # TOC-053
Pipe # Ol
CBOD
Fluoride
TN
1st 6 months
2nd 6 months
1st 6 months
2nd 6 months
2nd 6 months
Ist 6 months
2nd 6 months
.r°.
,r°.
g•0
O.00U
O.00e
.00
0.00tl
MTKN
0.00
0.00e
0.00e
0
0
0
0
0
00.00
0. 0
0.00
0.00
0.00
0.00
.00
0
00
0
0
0
0
N/A
N/A
N/A
N/A
N/A
N A
0%
0%
N/A
N A
N/A
N/A
N A
N A
0%
0%
N/A
N/A
N/A
N/A
N/A
N/A
0%
0%
N A
N/A
N/A
N A
N/A
N/A
0%
0%
Molybdenum
Chloride
Ethanol
JTP
1st 6 months
2nd 6 months
1st 6 months
12nd 6 months
Ist 6 months
12nd6months
1st 6 months
2nd 6 months
ar9.
ergs
ar9e,7
.7.
° erg •
°
0.00
0.00�
0.00a
0.00tl
0.00tl
0.00
.00
0.00
0
0
0
0
0
0
0
0.00
0.00
0. 0
0.00
0.00
0.00
0.00
0.00
0
0
0
0
0
0
N/A
N/A
0%
O%
N/A
N/A
77
0%
N/A
N A
O%
O%
N A
N A
0%
O%
N/A
N/A
0%
0%
N/A
NIA
ju%
0%
N/A
N A
0%
0%
N A
I N/A
0%
0%
Selenium
Silver
Zinc
2nd 6 months
I st 6 months
2nd 6 months
1st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
tl e7.
vr�e
ergs
OO7.
OOOo
O.00e
0.^Oe
O.00tl
O.000
rN/A
0
0
0
0
00.00
0.00
0.00
.00
0.00
.00
0.00
0
0
0
0
0
0
0
N A
N/A
N/A
N A
N A
N/A
N/A
N A
N A
/A
N/AN
A
N A
N/A
N A
N/A
N/A
N/A
N A
N A
N/A
N/A
N A
N/A
N/A
N/A
N/A
N A
N/A
..... ....r .. �..,. ^,,........ BDL -> B..._ D........ L.—
POTW
IUP-> I.....r�.1 U..r P.r ..I. ->
A .r ..w.. P.... ........w . .°. SNC -> S° .r.. a.. N.—C., m°. ->vm,V gee ... P., ..,.
Q.. 6-ms w. & . BDL o1/26DL. TRC -> T. R... „. C.. WWTP ->
Cn.P.er: PAR G.­..e F......,.: .1..1,994B. ,.°.. 12, 13. 14 B—, IDSF F...,. C.ar ... ,,.^ ­>.— PAR N.,..er e........r .a.. IUP o.o. - P.°. .,

Pretreatment Annual Report (PAR)
Industrial Data Summary Form (IDSF)
Use separate forms for each industry/pipe
Total # of samples =>
* Maximum =>
or Minimum =>
*
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) _> o
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) _>
Total # of samples =>
* Maximum (mg/1) _>
* or Maximum (lb/d) _>
* or _ Average (mg/1) _>
* or Average Loading (lb/d) _>
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) _> o
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) _>
Total # of samples =>
* Maximum (mg/1)=>
* or Maximum (lb/d) _>
* or _ Average (mg/1) _>
* or Average Loading (lb/d) _>
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) _>
• violations, (chronic SNC is >= 66%) _> -
% TRC violations, (SNC is >= 33 %) _>
Industry Name Catalent Pharma Solutions, LLC
IUP # TOC-053
Pipe # 01
111
111
11
11
----
1
1 1
1 11
1 11
------
1 11
1 11
------
111
111
------
POTW mom.. .,..., „�.... .,,... ..->u..1.-I" L, m., ms/.->m� e.m. n.. �....
.,.. ..T P�.... w.,. w....,. . UP I..,..".. U..' P., m" �-/.->,,.��,. o. ,
A .g. SNC->S�e. .��.., N..-C.- .—->,.���.. ,
�. Q,. . 6-m . & . BDL , 1/2BDL, TRC -> T. R.,. „. C..WWTP-> w � s. • a=
Cn.ou.: PAR G-...- F.... --- :PF bFbSE,.,,.R..L,"n...»„G:ad..�.9.-1-VqWB.p..-12.13.14B.—IDSF F.—Ceay..,a,,..->a,..PAR N,.-..,..--1.1--IUPp,p.-P.a. _.,.

Pretreatment Annual Report (PAR) Industry Name
Industrial Data Summary Form (IDSF) IUP #
Use separate forms for each industry/pipe Pipe #
Enter BDL values as < (value)
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (Ib/d) =>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
• violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
• violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) =>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
• violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) =>
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) _>
* or Average (mg/1) =>
* or Average Loading (Ib/d) =>
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is>= 33 %) =>
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) =>
EMMEM
MEC=
HERE=
®'
®'
=CM=EE3=MCC=1Ma=MCC=EE3=
BDL -> B,— D....... . L — -gh -> m, ..m. .,
ROTW IUP->1„... -.. U..'P-m„ d.- ..
....aw.. R..,..,,a..... .w .. ,g. w... , . SNC -> S' 1 -- N..-Co ..,.. .,sd -> M'o— g. , . p.
A,. M1 Q.. . 6-m d & BDL .1/2BDL. TRC -> T. R. „. C., WWTP-> d.,
C-P..r: PARG—..d.F.....m-: PP(�44SFi,.,,.,R.,f, n,..&::/d�.9.Ad.1.AQ4B.ns.. 12,13.14 B.—IDSF F.—C.o,-,.—>—PAR N,.md......,.. 1.1.. IUPP.P.-Pa. .r

Pretreatment Annual Report (PAR)
Industrial Data Summary Form (IDSF)
Use separate forms for each industry/pipe
Enter BDL values as < (value)
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) =>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
% violations,(chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
% violations,(chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) =>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
% violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
% violations,(chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) =>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
% violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
% violations,(chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
Control Authority, Town of Cary
Town Name => Cary
WWTP Name => Western Wake Regional
NPDES # => NCO088846
1st 6 months, dates => to 30 2022
2nd 6 months, dates => 7 to 12 31 2022
Industry
Name FujiFilm Diosynth Biotech
IUP # TOC-052
Pipe # 03
Flow, mgd
BOD
TSS
Ammonia
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
110.7
1 st 6 months
2nd 6 months
181
184
13
13
13
13
13
13
0.22
0.29
498
495
65
46
17.3
247.8
574.2
30.8
44.3
10.8
22.5
0.08
0.12
213.5
195.0
22.5
26.0
4.4
5.7
145.5
192.7
14.4
25.5
3.2
5.9
a
0%
0%
0%
0%
0%
0%
0%
0%
0
0%
0%
0%
0%
0%
0%
0%
0%
t
N/A
N/A
0%
0%
N/A
N/A
0%
0%
N/A
N/A
0%
0%
N/A
N/A
0%
0%
Arsenic
Cadmium
Chromium
COD
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
2
2
2
2
2
2
N/A
N/A
<0.001
<0.001
<0.0003
<0.0003
<0.003
0.0030
N/A
N/A
<0.0006
<0.0011
<0.0002
<0.0003
<0.0016
0.0030
N/A
N/A
0.001
<0.001
<0.0002
<0.0002
<0.0018
0.0015
N/A
N/A
<0.006
<0.0011
<0.0001
<0.0002
<0.0011
0.0015
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
o
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
t
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
2
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
Copper
Cyanide
Lead
Mercury
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
2
2
2
2
2
2
3
2
0.029
0.0410
<0.003
<0.003
<0.0025
0.0006
0.0000257
0.0003840
0.0154
0.0356
<0.0016
<0.0028
<0.0016
0.0006
0.0000165
0.0004314
0.0266
0.0364
<0.0025
<0.0025
<0.0018
0.0003
0.0000158
0.0001969
0.0864
0.0198
<0.0016
<0.0026
<0.0011
0.0003
0.0000101
0.0002206
21
N/A
N/A
0%
0%
N/A
N/A
0%
0%
o
N/A
N/A
0%
0%
N/A
N/A
0%
50%
L
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
BDL => Below Detection Limit mg/I => mi I I i grams per liter
POTW must enter at least one of these IUP=> Industrial User Permit Ib/d => pounds per day
four rows, Please indicate how averages were calculated SNC => Significant Non -Compliance mgd => million gallons per day
Avg period could be month, Qtr, or 6-month & if BDL , 1/2BDL, or zero values used. TRC => Technical Review Criteria WWTP=> wastewater treatment plant
Chapter: PAR Guidance File name: PlFde�i§ 6�edaj§ts�cti9SB, pages 12, 13, 14 Blank IDSF Form, Copy and use in your PAR Number each set for each IUP pipe- Page of

Pretreatment Annual Report (PAR)
Industrial Data Summary Form (IDSF)
Use separate forms for each industry/pipe
Enter BDL values as < (value)
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) =>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
• violations, (chronic SNC is >= 66%) => ,,
% TRC violations, (SNC is >= 33 %) => o
• violations, (chronic SNC is >= 66%) => t
% TRC violations, (SNC is >= 33 %) =>
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) =>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
• violations, (chronic SNC is >= 66%) => ,
% TRC violations, (SNC is >= 33 %) => o
• violations, (chronic SNC is >= 66%) => L
% TRC violations, (SNC is >= 33 %) =>
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) =>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
• violations, (chronic SNC is >= 66%) => ,
% TRC violations, (SNC is >= 33 %) => o
• violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
Industry Name FujiFilm Diosynth Biotechnologies USA, Inc
IUP # TOC-052
Pipe # 03
CBOD
Fluoride
TKN
TN
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
13
3
2
2
399
472
0.76
1.00
41.4
67.0
41.7
67
403.6
488.3
0.49
0.99
41.9
51.2
42.2
51.2
188.9
158.7
0.38
0.50
11.6
18.8
11.9
19.2
147.7
160.6
0.24
0.50
8.9
17.3
9.1
17.8
N/A
N/A
N/A
N/A
N/A
N/A
0%
0%
N/A
N/A
N/A
N/A
N/A
N/A
0%
0%
N/A
N/A
N/A
N/A
N/A
N/A
0%
0%
N/A
N/A
N/A
N/A
N/A
N/A
0%
0%
Nickel
Selenium
Silver
Zinc
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
1<0.0005
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
0.0015
0.0023
<0.0025
<0.0025
<0.0005
0.0370
0.0430
0.0010
0.0023
<0.0016
<0.0028
<0.0003
<0.0006
0.0237
0.2573
0.0008
0.0012
<0.0015
<0.0015
<0.0004
<0.0004
0.0265
0.0330
0.0005
0.0011
<0.0010
<0.0017
<0.0002
<0.0004
0.0170
0.1500
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
Molybdenum
lChloride
Ethanol
TP
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
1685
7
7
27
7
<0.0025
0.003
1490
2.58
4.62
19.7
20.5
<0.0016
0.0030
449.4
1940.0
80.21
4.83
13.6
26.7
<0.0018
0.002
203.9
390.2
0.94
0.66
6.2
6.2
<0.0011
0.0015
142.0
438.6
13.91
0.69
4.2
6.3
N/A
N/A
0%
0%
N/A
N/A
0%
0%
N/A
N/A
0%
0%
N/A
N/A
0%
0%
N/A
N/A
N/A
N/A
N/A
N/A
0%
0%
N/A
N/A
N/A
N/A
N/A
N/A
0%
0%
BDL => Below Detection Limit mg/I => mi I I i grams per liter
POTW must enter at least one of these IUP=> Industrial User Permit Ib/d => pounds per day
four rows, Please indicate how averages were calculated SNC => Significant Non -Compliance mgd => million gallons per day
Avg period could be month, Otr, or 6-month & if BDL , 1/2BDL, or zero values used. TRC => Technical Review Criteria WWTP => wastewater treatment plant
Chapter: PAR Guidance File name: PlFde�i§ 6�edaj§ts�cti9SB, pages 12, 13, 14 Blank IDSF Form, Copy and use in your PAR Number each set for each IUP pipe- Page of

Pretreatment Annual Report (PAR)
Industrial Data Summary Form (IDSF)
Use separate forms for each industry/pipe
Enter BDL values as < (value)
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) =>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) =>
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) =>
Total # of samples =>
* Maximum =>
* or Minimum =>
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) =>
• violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) =>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) =>
• violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
Industry Name FujiFilm Diosynth Biotechnologies USA, Inc
IUP # TOC-052
Pipe # 03
BDL => Below Detection Limit mg/I => mi I I i grams per liter
POTW must enter at least one of these IUP => Industrial User Permit Ib/d => pounds per day
four rows, Please i ndi cate how averages were calculated SNC => Significant Non -Compliance mgd => million gallons per day
Avg period could be month, Qtr, or 6-month & if BDL , 1/2BDL, or zero values used. TRC => Technical Review Criteria WWTP=> wastewater treatment plant
Chapter: PAR Guidance File name: PlFde�i§ 6�edaj§ts�cti9SB, pages 12, 13, 14 Blank IDSF Form, Copy and use in your PAR Number each set for each IUP pipe- Page of

Pretreatment Annual Report (PAR)
Industrial Data Summary Form (IDSF)
Use separate forms for each industry/pipe
Enter BDL values as < (value)
THIS PAGE
REPLACEDo,W �,, .
* Maximum (mg/1) _>
RVISIONorMaximum (Ib/d)=>
or Average (mg/1) _>
* or Average Loading (]bid) _>
% violations,(chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) ->
% violations,(chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) =>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
% violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
% violations,(chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 °/v) =>
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (Ibld) =>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
% violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is - 33 %) =>
% violations,(chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
Control Authority, Town of Cary
Town Name => Cary
W WTP Name => Western Wake Regional
NPDES # => NCO088846
1st 6 months, dates -> to
2nd 6 months, dates => to31/2022
Industry
Name FujiFilm Diosynth Biotech
IUP # TOC-052
Pipe # 03
Flow, mgd
BOD
TSS
Ammonia
I st 6 months
2nd 6 mon1498
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
1st 6 months
110.7
2nd 6 months
181
184
13
13
13
13
13
13
0.22
0.29
495
65
46
17.3
0.08
0,12
247.8
213.5
574.2
195.0
30.8
22.5
44.3
26.0
10.8
4.4
22.5
5.7
0%
T°/v
145.5
0/v
192.7
0%
14.4
0%
25.5
0%
3.2
0%
5,9
0%
n
A
0%
NIA
0%
NIA
0%
0°/v
0%
0%
0%
NIA
0%
N/A
0%
0%
0%
0%
N/A
N/A
0%
0%
N/A
N/A
0%
0%
Arsenic
Cadmium
Chromium
COD
ist 6 months
2nd 6 months
1st 6 months
2nd 6 months
1st 6 months
2nd 6 months
1st 6 months
po
2nd 6 months
2
<0.001
2
<0.001
2
<0.0003
2
<0.0003
2
<0.003
2
0.0030
N/A
N/A
N/A
NIA
<0.0006
<0.0011
<0.0002
<0,0003
<0,0016
0.0030
N/A
N/A
0.001
<aool
<0.0002
<0.0002
<0. 018
0.0 15
N/A
N/A
-
<0.006
N/A
N/A
NIA
70.0011
N/A
NIA
NIA
70.0001
NIA
N/A
N/A
<Q,Q 02
N/A
NIA
NIA
<0. 011
N/A
N/A
N/A
0.0015
NIA
N/A
N/A
IN/A.
N/A
N/A
NIA
N/A
NIA
N/A
N/A
N/A
NIA
N/A
NIA
N/A
NIA
N/A
N/A
Copper
Cyanide
Lead
Mercury
1 st 6 months
2nd 6 months
1st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
1 it 6 months
2nd 6 months
2
2
2
2
2
2
3
2
0.029
0.0410
<0.003
<0.003
<0.0025
0.0006
0.0000257
0,0003840
0.0154
0.0356
<0.0016
<0.0028
<0.0016
0.0006
0.0000165
0.0004314
0.0266
0.0364
<0.0025
<0.0025
<0.0018
0.0003
0.0000158
0.0001969
0.0864
N/A
0,0198
N/A
<0.0016
0%
<0.0026
0%
<0.0011
N/A
0.0003
N/A
0.0000101
0%
0.0002206
0%
o
N/A
N/A
0%
0%
N/A
N/A
0%
0%
N/A
N/A
N/A
N/A
NIA
NIA
❑ni _- ❑
NIA
NIA
N/A
N/A
N/A
N/A
NIA
N/A
NIA
N/A
' Porw mux .near m +Wahl one o "vim -1 LJe .1- L-1 m9�i -> m„ii grams Par „Ler
f lfi... 1UP-> User P-IL
[`I,/�
pountls per eay
Tour rqw s. ,.....n -'. m.- a�arflg Ps were [: a,c 1.1.4 SNC -> So-f.-L Nen-Comp-n
mgtl -7 m�,i�an ga,i pas per tlay
tl q b nL,, Q111 qr 6-mq.,. & 11 BDL , 112BDL TRC -> T - h - - R„„, aw C,.,.,.a WWTP-> ...... ar LraaLm anL pi0nl
Ch a P, er: PAR G-tl-- F„a „ama: PALF;d_,( i,.n��f a,ja, -p,C; A", - A J-10-94B. P„ - 12. 13, 14 B,-n fDSF Farm Copy ane ,,.„,,, ya.,r PAR IV„�., L,,,r a„�� ,aL rqr �a�n I U P Pin. - P.

Pretreatment Annual Report (PAR)
Industrial Data Summary Form (IDSF)
Use separate fortes for each industry/pipe
Enter BDL values as < (value)
THIS PAGE
REPLACE aXW=f,
* or Maximum (lb/d) =>
Rt V I S I Q Average (mg) =>
ge Loading (Eb/d) _>
% violations, (chronic SNC is >- 66%) =>
% TRC violations, (SNC is >= 33 %) ->
• violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >- 33 %) =>
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) _>
* ar Average (mg/1) =>
* or Average Loading (lb/d) =>
violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
Total # of samples =>
* Maximum (mg/1) ->
* or Maximum (lb/d) =>
° or Average (mg/1) =>
* or Average Loading (lb/d) =>
% violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >- 33 %) =>
% violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is - 33 %) =>
Industry Name FujiFilm Diosynth Biotechnologies USA, Inc
]UP # TOC-052
Pipe # 03
CBOD
Fluoride
TKN
TN
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
I st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
i399
472
0.76
1.00
41.4
67.0
41.7
67
403.6
488.3
0.49
57
41.9
S I.2
42.2
51.2
188.9
158.7
0.38
0.50
11.6
t8.8
11.9
19.2
147.7
160.6
0.24
0.50
8.9
17.3
9.1
17.8
N/A
N/A
N A
N/A
N/A
NIA
%
0%
o
NIA
N/A
N/A
N/A
N/A
N/A
0%
097
NIA
N/A
NIA
N A
N/A
N/A
/0
0%
NIA
N/A
N/A
N/A
NIA
1 NIA
0%
0%
Nickel
Selenium
Silver
Zinc
Ist 6 months
2nd 6 months
Ist 6 months
2nd 6 months
1st 6 months
2nd 6 months
1st 6 months
2nd 6 months
0.0015
.0023
<0.0025
0- 0025
70.0005
<0.00 5
0.0370
0.0430
6.0010
0.0023
<0.0016
<0.0028
70003
<0.0006
0.0237
0.2573
0.0008
.0012
70015
<0.0015
<0.0004
7.0004
0.0265
0.0330
0.0005
0.0011
<0.0010
<0.0017
<0.0002
<0.0004
0.0170
0.1500
r
N/A
N/A
N/A
N/A
N/A
NIA
N/A
N/A
o
NIA
NIA
N/A
N/A
N/A
NIA
N/A
N/A
N/A
NIA
N A
NIA
NIA
N A
NIA
NIA
N/A
NIA
N A
N/A
N A
N/A
I N/A
NIA
Molybdenum
Chloride
Ethanol
TP
I st 6 months
2nd 6 months
1st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
1 st 6 months
2nd 6 months
<0.0025
0.003
685
1490
2.58
4.62
19.7
20.5
<0.0016
0.0030
449.4
1946.0
80.21
4.83
13.6
26.7
<0. 018
0.002
203.9
39 .2
0.94
0.66
6.2
<0.0011
0,0015
142.0
438.6
1TO-i
0.6
4.2
E6.3�]
N/A
N A
0%
0°1°
NIA
NIA
0%
0.
N/A
N/A
o/
0%
N/A
N/A
0%
0°0
i
N/A
N/A
N/A
N/A
N/A
NIA
0%
0%
N/A
NIA
N/A
N/A
N/A
N/A
0%
0%
BDL -> B.- D.-- L -., nal -> m ngrams per
PQTV51 .n�e� .nr.r .a i.egr o.,. or lease up-> lnn�eir� ei Ue,,.1r Perm„ initl -> pn„nas p.r a.,y iLef
�r rows, Pl ae se �ntl�cnre new ey erege were cei c..i ar atl SNC -> V �gniricenc l en-Cem A-nce mgn -7 m�n�on gallons par nay
A.,9 c..n , Q,,, 6-.n n,n & r BDL 1/2BDL, s.a. TRC -> Tecn-ei RI-1- Cr, er,. WWTP-> ..Em.n, pi .nl
Cn P-i PAR G- -- F i. nem.: PA�9 t{�Sf . b,F2e�a m.p� �d .n 9a �.�749AB r.,12, 13. 14 B�.- IDSF F- Copy -a - PAR N,.-, a.- see ror .ern IUp p'p. - Pe°. .,

Pretreatment Annual Report (PAR)
Industrial Data Summary Form (IDSF)
Use separate forms for each industry/pipe
Enter BDL values as < (value)
THIS PAGE
3
REPLACEDMWa,,TTJ)T>
* or Maximum (lb/d) =>
REISIOAverage (mgll)
or A crag, Loading (lb/d) =>
% violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
% violations, (chronic SNC is >= 66%) —>
% TRC violations, (SNC is >= 33 %) =>
Total # of samples =>
* Maximum =>
or Minimum =>
% violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
% violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
Total # of samples =>
* Maximum (mg/1) _>
* or Maximum (lbld) =>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
% violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
% violations, (chronic SNC is >— 66%) =>
% TRC violations, (SNC is >= 33 %) =>
Industry Name FujiFilm Diosynth Biotechnologies USA, Inc
IUP # TOC-052
Pipe # 03
��
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PQTW m s. P�.P . _ nUi , Ls.i.- U.—I.— L,-,, m911 -> M. g-1 Per
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f nur raw 5. PI.... . SNC -> 5,9n�Ar.. n[ Nan-C.-,—... TOd -> —11'0. R-111 per d.y
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Pretreatment Annual Report (PAR)
Industrial Data Summary Form (IDSF) Industry Name
IUP #
Use separate forms for each industry/pipe Pipe #
Enter BDL values as < (value)
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) =>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
• violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
• violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
Total # of samples =>
* Maximum (mg/1) =>
* or Maximum (lb/d) _>
* or Average (mg/1) =>
* or Average Loading (lb/d) =>
• violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
• violations, (chronic SNC is >= 66%) =>
% TRC violations, (SNC is >= 33 %) =>
Total # of samples =>
* Maximum (mg/1) _>
* or Maximum (Ib/d) =>
* or Average (mg/1) _>
* or Average Loading (Ib/d) =>
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) =>
• violations, (chronic SNC is >= 66%) _>
% TRC violations, (SNC is >= 33 %) =>
,.
MEM=
..
L.
R7TW .,.,. ..,... .. �..., ..,......,. BDL -> B—... D., 1.. m�, mg/' -> m, s .m, p..
... ..w.. R.... ,....... _ . .w.. . IUP-> I .... ...,,1 U.., P.,,.., �./.-> �.....
ASNC ->Ss. N..-C.m .... mg.->��... �. .,,.... ...
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A ff••�1
4R
September 28, 2022
Ms. Christine Vannais
Chief Operating Officer
FujiFilm Diosynth Biotechnologies USA, Inc.
101 J. Morris Commons Lane
Morrisville, NC 27560
TOWN OF CARY
NOTICE OF VIOLATION
TIER I — CIVIL PENALTY
CERTIFIED MAIL
Re: Chloride Permit Limit Exceedance — Civil Penalty Assessment
Dear Ms. Vannais,
On August 30, 2022, Don Johnson, Utility Pretreatment Program Supervisor, received a text
message at 10:00 PM from Mr. Brad Shelton that FujiFilm Diosynth Biotechnologies USA,
Incorporated (FDBU) received wastewater data indicating that a chloride permit limit
exceedance occurred on July 19, 2022. On August 31, 2022, Cary pretreatment staff received
FDBU industrial wastewater discharge report that included a self -monitoring wastewater
chloride concentration result of 1,490 mg/L.
FDBU Industrial User Permit (IUP) TOC-052 - Part I F specifies a chloride daily maximum
discharge limit of 1,300 lb/day. The reported daily concentration of 1,490 mg/L and an
industrial wastewater discharge of 156,116 gallons, equals a discharge of 1,940 pounds of
chloride and exceeds the daily chloride permit limit. Please note that it also exceeds the
Technical Review Criteria (TRC) threshold which is defined as values above 20 percent the
permitted limit. Please see the code of federal reregister (CFR), 40 CFR Part
430.8(f)(2)(viii)(B) for further information on TRC.
As a result of the limits exceedance violation and in accordance with Cary's enforcement
response plan, FDBU is hereby issued a Notice of Violation with a Tier I civil penalty of three
hundred dollars ($300.00).
According to the Cary sewer user ordinance, section 36-188, a user who receives notice of an
assessment of a civil penalty under section 36-179(b); or a user who receives notice of the
issuance of an administrative order under section 36-179(a)(4) shall have the right, upon filing
written demand, to a hearing before a hearing officer designated by the director. The written
demand for a hearing shall be filed with the director within 30 days of receipt of this notice.
Unless such written demand is filed within the time specified herein, the contested action shall
be final.
TOWN Of CARY
400 James Jackson Avenue • Cary, NC 27513 • PO Box 8005 • Cary, NC 27512-8005
tel 919A69-4090 • fax [phone] • www.townofcary.org

Notice of Violation and Assessment of Civil Penalty September 28 2022
Unless a written demand for a hearing is fled in accordance with Cary's sewer use ordinance,
please submit your civil penalty payment to:
Town of Cary Finance Department
P.O. Box 8049
Cary NC 27512-8049
Additional or continued noncompliance may result in increased enforcement action. Please
contact Don Johnson, Utility Pretreatment Program Supervisor at [phone] if there are
any questions.
Sincerely,
amie Revel4PE
Utilities Director
Cc: Donald Smith, Wastewater Collections Program Manager
Don Johnson, Utility Pretreatment Program Supervisor
Enclosure: Town of Cary Enforcement Response Plan

TDrN LF Cp�Y
+# MTO a AFT +41
Ober: CBRYAN Type: C Drag: I
Date: 12/060 01 Recelpt no: 290725
Descrlptim Awnt
C 0uantlAfION $300 00
BAXTERB Sf1TOONN�p p�
MAYµMINA, T 275a
r data I
POS
RISC PAY
t3001
1300.
Total
payment
Trans date: 12/08/22
T1me: 14:27:22
- + MN1J'G11 ruin fR ia;y K.
1.17' 11•

UTILITIES DEPARTMENT
June 8, 2022
Ms. Christine Vannais
Chief Operating Officer
FujiFilm Diosynth Biotechnologies USA, Inc.
101 J. Morris Commons Lane
Morrisville, NC 27560
NOTICE OF VIOLATION
ELECTRONIC SUBMITTAL
Re: Compliance Violation for Missed Sampling- Ethanol
Dear Ms. Vannais,
On May 27, 2022, the Town of Cary Utilities Department, Pretreatment Division staff became
aware through a phone call from Mr. Brad Shelton that FujiFilm Diosynth Biotechnologies USA,
Incorporated (FDBU) had neglected to collect the required monthly ethanol sample for April
2022. The missed ethanol sample was identified when the April 2022 monthly wastewater report
was being assembled on May 27. A written follow up of the missed sample was submitted by
Mr. Shelton that included corrective actions that will be taken to prevent missing this sample
again in the future. An ethanol sample was collected in May which will constitute as a makeup
sample for the missed April sample.
FDBU industrial user permit (IUP) TOC-052 - Part I F. requires ethanol to be collected by grab
sample once per month with a required detection level of 5.0 milligrams per liter. Please note
that it is the responsibility of the permittee to ensure that all requirements specified in the IUP
are met.
As a result of the missed sampling violation and in accordance with Cary's Enforcement Response
Plan, FDBU is hereby issued a Notice of Violation with a Tier 1 civil penalty of one hundred forty-
four dollars ($144.00), which is the cost of the missed sampling plus 20%.
Unless a written demand for a hearing is filed in accordance with Cary's sewer use ordinance,
failure to pay the one hundred forty-four dollar ($144.00) civil penalty in full by thirty (30) days
from receipt of this letter will result in Cary undertaking collection efforts.
TOWN 4?1 CARY
400 James Jackson Avenue • Cary, NC 27513 • PO Box 8005 • Cary, NC 27512-8005
tel[phone] • fax [phone] • w .townofcary.org

Ms. Christine Vannais, June 8. 2022 Pa e 2
Please submit your civil penalty payment to:
Town of Cary Finance Department
P.O. Box 8049
Cary NC 27512-8049
Additional or continued noncompliance may result in increased enforcement and civil penalties.
Please contact Don Johnson, Utility Pretreatment Program Supervisor at 919-414-8052 if there
are any questions.
Sincerely,
ie Rev /sP..
Utilities Director
Cc: Donald Smith, Wastewater Collections Program Manager
Don Johnson, Utility Pretreatment Program Supervisor

November 14, 2022
Mr. Peter Self
Associate Director, EHSS
Biogen
5000 Davis Drive
RTP, NC 27709
Subject: Propylene Glycol Discharge
Dear Mr. Self,
TOWN OF CARY
0tto
NOTICE OF VIOLATION
Certified Mail
On September 17, 2022, the Town of Cary Utilities Department, Pretreatment Division
received phone and email notifications from Ms. Hanna Gamache (Biogen EHS)
regarding an accidental propylene glycol discharge. Ms. Gamache also called and
notified the on -shift operator at the Western Wake Regional Water Reclamation Facility
(WWRWRF) in accordance with Biogen's Spill Control and Countermeasures Plan.
During the time frame of 10:00 AM on September 16, 2022, until 8:00 AM on September
17, 2022, Biogen's RTP bio-utilities manager identified a propylene glycol leak to the
biowaste system. Biogen submitted their 5-day follow-up report on September 20, 2022,
which detailed the investigation and corrective actions taken. It was estimated that
approximately 8,000 gallons of 28% propylene glycol was discharged. No sampling from
the permit -regulated sampling point (Pipe 09) occurred during the time of the propylene
glycol discharge.
Industrial User Permit (IUP) TOC-051 Part II 6 specifies a duty to mitigate to prevent
adverse impacts on the Publicly Owned treatment Works (POTW) and specifically states:
Duty to Mitigate - Prevention of Adverse Impact
The permittee shall take all reasonable sti
violation of this permit which has a reason
health, the POTW, the waters receiving the
!ps to minimize or prevent any discharge in
able likelihood of adversely affecting human
POTW's discharge, or the environment.
Industrial User Permit (IUP) TOC-051 Part I Section F specifies a Biochemical Oxygen
Demand (BOD) daily max mass limit of 3021.0 pounds per day. A sample of the 28%
glycol solution was collected on Monday, September 19 from Biogen's glycol system.
TOWN Ot CARY
400 James Jackson Avenue • Cary, NC 27513 • PO Box 8005 • Cary, NC 27512-8005
tel [phone] • fax [phone] • w .townofcary.org

The sample was analyzed and contained a concentration of 340,000 milligrams per liter
of BOO. The calculated daily load of BOO discharged during the time of the glycol
discharge was 164,107 pounds, based on an estimated flow of 57,874 gallons during the
ten-hour discharge event. The BOO daily maximum discharge limit of 3,021 pounds was
likely exceeded and exceeds the Technical Review Criteria (TRC) threshold which is
defined as 20 percent above the permitted limit. Please see 40 CFR Part
430.8(f)(2)(viii)(B) for further information.
As a result of the duty to mitigate violation, the following actions are required:
• Review and revise procedures for the Building Management System (BMS) to help
identify slower and longer duration propylene glycol leaks for earlier detection and
warning.
Provide awareness training to operations and maintenance staff for early notification to
appropriate industrial user permit management staff of any propylene glycol, high
strength, or hazardous discharges to the biowaste system and sanitary sewer system
that may require spill notification or mitigation efforts.
As a result of the duty to mitigate violation and in accordance with the Town of Cary's
Enforcement Response Plan, the Town hereby issues Biogen a Notice of Violation with
a Tier I civil penalty of three hundred dollars ($300.00).
According to the Cary sewer user ordinance, section 36-188, a user who receives notice
of an assessment of a civil penalty under section 36-179(b); or a user who receives
notice of the issuance of an administrative order under section 36-179(a)(4) shall have
the right, upon filing written demand, to a hearing before a hearing officer designated by
the director. The written demand for a hearing shall be filed with the director within 30
days of receipt of this notice. Unless such written demand is filed within the time
specified herein, the contested action shall be final.
Unless a written demand for a hearing is filed in accordance with Cary's sewer use
ordinance, please submit your civil penalty payment to:
Town of Cary Finance Department
P.O. Box 8049
Cary NC 27512-8049 �+
Additional or continued noncompl ce
penalties. Please contact Dqn Jo� ltitityt?
319-4564 if there are any quiksti is y
Sincerely,
mie Revels,
! MN 1 19'. 1
Utilities Director
Vlt in increased enforcement and civil
Program Supervisor at 919-
Cc: Donald Smith, Wastewater Collections Program Manager
Don Johnson,'Utility Pretreatment Program Supervisor

Don E. Johnson - Pretreatment
PO BOX 8005
TOWN OF CARV UTILITIES DEPARTMENT
CARV NO 27512-8005
CERTIFIED MAIL
IIY�II111111111111111111=
9407 1118 9876 5830 8003 13
NC Division of Water Resources
NPDES Permitting Section
1617 MAIL SERVICE CTR
RALEIGH NC 27699-1617
I�I�IIiP���Ihrhl��I��hlwhldl��m��IIh��Inl�����Pt�r
$6.85 US POSTAGE
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Feb 21 2023
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062SO012913542