WQ0009267_Monitoring - 06-2023_20230728

Monitoring Report Submittal
Permit Number#*
Name of Facility:*
Month:* June
Report Information
Type *
GW-59
WQ0009267
City of Jacksonville WWTF
Confirmation Email Address: *
Name of Submitter: *
Signature:
Date of submittal:
Initial Review
Year:* 2023
Upload Document*
WQ0009267 June 2023 GW-59 MW Report, VOCs 22.53MB
Attached.pdf
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
[e-mail]
Amy Palaschak
7/28/2023
This will be filled in automatically
Reviewer: Wanda.Gerald

Is the project number correct?* WQ0009267
Is the monitoring report accepted?* Yes No
Regional Office* Wilmington
Reviewer: _anonymous
Review Date: 8/8/2023

GW-59A COMPLIANCE REPORT FORM Permit #_WQ0009267
(Submit one each monitoring period with GW-59 forms.)
I
Enter date monitoring results were due. (7/31/2023) Will this monitoring report (GW-59 and GW-59A) be
YES NO
submitted after the established due date?
2
Was any required information missing on the GW-59 report forms?
YES NO
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s)and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES NO
identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance.
4
Are any monitored constituents equal to or above the established standards?
YES NO
If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells
individually with constituent(s) and concentration(s) exceeding standards in the space provided below:
MW 3 — VOCs — Toluene 19.5 ug/L, p-Isopropyltoluene 65.7 ug/L
MW 10 — TDS 604.5 mg/L
5
For the constituents identified in question 4 above, have standards been exceeded previously for the same
YES NO
constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space
provided below, each well with constituent(s) exceeding standards, concentrations) reported, and sample
collection date for each occurrence (for the last two years).
MW3—12/2020 (Toluene 25.0 ug/L, p-Isopropyltoluene 24.2 ug/L), 12/2022 (Toluene 10.6 ug/L,
p-Isopropyltoluene 18.8 ug/L), 312023 (Toluene 13.7 ug/L, p-Isopropyltoluene 21.5 ug/L, Chloromethane
0.73 ug/L)
MW10 — all TDS — 6/2021 (657 mg/L), 912021 (675 mg/L), 12/2021 (633 mg/L), 3/2022 (607.5 mg/L), 6/2022
(577 mg/L), 9/2022 (560.5 mg/L), 12/2022 (660 mg/L), 3/2023 (618.5 mg/L)
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES NO
If the answer is "YES', a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE
IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact
the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this groundwater
YES NO
quality problem?
If the answer to question 7 is "YES', describe those actions in the space provided below. If the answer to
question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the
impact the waste disposal system is having at the review and compliance boundaries surrounding this facility.
Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties.
MW10 — high background TDS — noted in current permit
MW3 — Tom Tharrington (NC DEQ, DWR) was contacted on Thursday July 27, 2023 regarding the VOC
presence in MW3. VOCs will be sampled again in September 2023 with the quarterly set.
g
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form
with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report (Compliance Report GW-59A) is true and complete to the best of my knowledge
07/27/2023
Signat e of Permittee(or Authorized Agent) Date
GW-59A 12/8/2003

SUL3MI I rUKNI UN 7tLLUyy riArr-m UINL1
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Please Print Clearly or Type
Facility Name: City of Jacksonville Land Treatment System
Permit Name (if different):
Facility Address: 716 Firetower Road
Jacksonville NC 28540 County Onslow
Contact Person: Amy Palaschak Telephone#: [phone]
Well Location/Site Name MW-1 No. of wells to be sampled: 1. 17
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
PERMIT Number: Expiration Date: 7/31/2029
Non -Discharge WQ0009267 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): MWA Date sample collected: 6/28/2023
Well Depth: 16.6 ft. Well Diameter: 2 in.
Depth to Water Level 82546: 4.9 ft. below measuring point Screened Interval: 3 ft. to 13 ft.
Measuring Point is 3.2 ft. above land surface Relative M.P. Elevation: 1.7 ft.
Volume of water pumped/bailed before sampling: 5.62 gallons
Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
FIELD ANALYSES:
pH 00400: 5.2 units
Spec. Cond. 00094:
Odor 00085:
Appearance
D I 1 zed 6/28/2023 Laboratory Name: 1. Jacksonville 2. Environmental Chemists
ate same e ana y
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
issolved Solids:Total 70300 127
mg/L
Al - Aluminum oilo5
mg/L
pH (Lab) 00403 5.16
units
Ba - Barium 01007
ug/L
TOC 00680 14.5
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 45
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
Sulfate 00945 15
mg/L
Hg - Mercury 71900
ug/L
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
Total Ammonia oo6lo <0.2
mg/L
Mg - Magnesium 00927
mg/L
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
For Remediation Systems Only (Attach Lab Reports):
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please orint or type
GW-59 Rev.8/2013
Temp. 000lo: 23.3 oC
uMhos
Certification No. 1. 128 2. 94
Pb - Lead 01051 ug/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ® Yes (1) ❑ No (0)
VOC 7873 method # SM 6200C
method #
method #
method #
Influent I otal VUGs: mgiL trrluent I utdl vUUo.
(or Authorized Agent)
If WELL
WAS
DRY at
time of
sampling,
check
here:❑
mg/L VOC Removal%
methods of analysis by a
7/27/2023
(Date)

RI IRMIT FORM ON YFI LOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT 8, NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
M '
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address: 716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
c'tv'
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-2
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-2
Date sample collected: 6/28/2023
FIELD ANALYSES:
WAS
Well Depth: 17.0 ft.
Well Diameter: 2 in.
pH 00400: 5.3 units Temp. 000lo: 26.7 °C
DRY at
time of
Depth to Water Level 82546: 4.8 ft. below measuring point Screened Interval: 3 ft. to
13 ft. Spec. Cond. 00094: µMhos
sampling,
Measuring Point is 2.4 ft. above land surface
Relative M.P. Elevation: 2.4 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 5.86
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 6/28/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615 0.04
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 2 /100mL
Nitrate (NO3) as N 00620 0.03
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 242 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 5.3 units
Ba - Barium 01007
ug/L
TOC 00680 13 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 115 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 10 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095 µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia oo610 <0.2 mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625 mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Apent) Name and Title - Please print or type
GW-59 Rev.8/2013
(or Authorized Aoent)
(Date)
7/27/2023

Sl1RMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31 /2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address: 716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-3
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-3
Date sample collected: 6/27/2023
FIELD ANALYSES:
WAS
Well Depth: 17.0 ft.
Well Diameter: 2 in.
pH 00400: 4.9 units Temp. 000lo: 28.3 °C
DRY at
time of
Depth to Water Level 82546: 3.8 ft. below measuring point Screened Interval: 3 ft. to
13 ft. Spec. Cond. 00094: µMhos
sampling,
Measuring Point is 3.2 ft. above land surface
Relative M.P. Elevation: 0.6 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 6.34
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 6/27/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL
Nitrate (NO3) as N 00620 0.06
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus. Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 59.5 mg/L
Al - Aluminum oilo5
mg/L
pH (Lab) 00403 4.9 units
Ba - Barium 01007
ug/L
TOC 00680 2.1 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 10 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095 µMhos
K - Potassium 00937
mg/L
VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625 mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please print or tvoe
GW-59 Rev.8/2013
(or Authorized Agent)
(Date)
7/27/2023

SUBMIT FORM ON YELLOW PAPER ONLY
•
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
• •
•
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address: 716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 25540 County Onslow
X Spray Field Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-4
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-4
Date sample collected: 6/27/2023
FIELD ANALYSES:
WAS
Well Depth: 16.0 ft.
Well Diameter: 2 in.
pH 00400: 4.8 units Temp. 000lo: 26.6 °C
DRY at
Depth to Water Level 82546: 3.2 ft. below measuring point Screened Interval: 5.8 ft. to
14 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.68 ft. above land surface
Relative M.P. Elevation: 0.52 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 6.14
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 6/27/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 166.5 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 4.77 units
Ba - Barium 01007
ug/L
TOC 00680 1.6 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 63 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 39 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095 µMhos
K - Potassium 00937
mg/L
VOC 7873 method # SM 6200C
Total Ammonia oo6lo <0.2 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3 as N: Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625 mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aoent) Name and Title - Please print or type
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 25540 County Onslow
°ay
X Spray Field Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-5
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-5
Date sample collected: 6/26/2023
FIELD ANALYSES:
WAS
Well Depth: 18.1 ft.
Well Diameter: 2 in.
pH 00400: 5.1 units Temp. 000lo: 27.8 °C
DRY at
Depth to Water Level 82546: 5.8 ft. below measuring point
Screened Interval: 5 ft. to
15 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.57 ft. above land surface
Relative M.P. Elevation: 3.23 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
5.90
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 6/26/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 40.5
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 5.13
units
Ba - Barium 01007
ug/L
TOC oo68o 1.5
mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 7
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 0.21
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aoent) Name and Title - Please print or tvoe
GW-59 Rev.8/2013
(or Authorized Aoent)
(Date)
7/27/2023

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address: 716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
t� 1:
X Spray Field Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-6
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-6
Date sample collected: 6/27/2023
FIELD ANALYSES:
WAS
Well Depth: 16.8 ft.
Well Diameter: 2 in.
pH 00400: 5.7 units Temp. 000lo: 21.4 °C
DRY at
Depth to Water Level s2546: 3 ft. below measuring point Screened Interval: 3.5 ft. to
14 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.65 ft. above land surface
Relative M.P. Elevation: 0.35 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 6.62
gallons
Appearance
here: El
Samples for metals were collected unfiltered: X YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 6/27/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615 0.09
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P oo665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids. -Total 70300 247 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 5.72 units
Ba - Barium 01007
ug/L
TOC om8o 6.1 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 47 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 19 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095 µMhos
K - Potassium 00937
mg/L
VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; N1­13as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625 mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please print or twe
GW-59 Rev.8/2013
(or Authorized Aqent)
(Date)
7/27/2023

SUBMIT FORM ON YELLOW PAPER ONLY
•
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
• •
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: _ 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address: 716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 23540 County Onslow
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-7
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-7
Date sample collected: 6/26/2023
FIELD ANALYSES:
WAS
Well Depth: 15.0 ft.
Well Diameter: 2 in.
pH 00400: 4.1 units Temp. 000lc 22.7 °C
DRY at
Depth to Water Level 82546: 2.8 ft. below measuring point
Screened Interval: 2.5 ft. to
13 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: -0.2 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 5.86
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 6/26/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L
Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids.Total 70300 247 mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 4.09 units
Ba - Barium 01007
ug/L
TOC 00680 7.6 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 72 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 63 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095 µMhos
K - Potassium 00937
mg/L
VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625 mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please print or Noe gnatur of Per i ee (or Authorized Agent)
GW-59 Rev.8/2013
(Date)
7/27/2023

SUBMIT FORM ON YELLOW PAPER ONLY
•
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
•
•
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address: 716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallerycity)
Jacksonville NC 2'`j40 County Onslow
X Spray Field Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-8
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-8
Date sample collected: 6/26/2023
FIELD ANALYSES:
WAS
Well Depth: 12.1 ft.
Well Diameter: 2 in.
pH 0040o: 5.2 units Temp. 000lo: 23.2 °C
DRY at
Depth to Water Level 82546: 6.7 ft. below measuring point
Screened Interval: 3 ft. to
9 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: 3.7 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 2.59
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 6/26/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL
Nitrate (NO3) as N 00620 0.13
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids.Total 70300 221 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 5.19 units
Ba - Barium 01007
ug/L
TOC 00680 3.1 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 7 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 95 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095 µMhos
K - Potassium 00937
mg/L
VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625 mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aaent) Name and Title - Please print or Noe
GW-59 Rev.8/2013
of Perkiftee (or Authorized Aaent)
(Date)
7/27/2023

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
• • •
•
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, INC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 23.` 40 County Onslow
I
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-9
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-9
Date sample collected: 6/26/2023
FIELD ANALYSES:
WAS
Well Depth: 14.0 ft.
Well Diameter: 2 in.
pH 00400: 3.77 units Temp. 000lo: 23.6 °C
DRY at
Depth to Water Level 82546: 7.1 ft. below measuring point
Screened Interval: 7 ft. to
11 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.55 ft. above land surface
Relative M.P. Elevation: 4.55 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
3.31
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 6/26/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 256
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 3.77
units
Ba - Barium 01007
ug/L
TOC oo68o 2.3
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 9
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 97
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese o1o55
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aoent) Name and Title - Please print or Noe
GW-59 Rev.8/2013
(or Authorized Aoent)
(uate)
7/27/2023

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, INC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address: 716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
c°y
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-10
No. of wells to be sampled: 17
ElWater Source Heat Pump ElOther:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-10
Date sample collected: 6/26/2023
FIELD ANALYSES:
WAS
Well Depth: 30.1 ft.
Well Diameter: 2 in.
pH 00400: 6.3 units Temp. 000lo 26.7 eC
DRY at
Depth to Water Level 82546: 7.4 ft. below measuring point Screened Interval: 17 ft. to
27 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.9 ft. above land surface
Relative M.P. Elevation: 4.5 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 10.90
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 6/26/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1 /100mL
Nitrate (NO3) as N 00620 0.03
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 604.5 mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 6.32 units
Ba - Barium 01007
ug/L
TOC 00680 2.1 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 21 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 149 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095 µMhos
K - Potassium 00937
mg/L
VOC 7873 method # SM 6200C
Total Ammonia oo6lo 0.33 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625 mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.8/2013
(or Authorized Aoent)
( uate)
7/27/2023

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
•
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address: 716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 22,540 County Onslow
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-11
No. of wells to be sampled: 17
❑ Water Source Heat Pump ElOther:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MWA 1
Date sample collected: 6/28/2023
FIELD ANALYSES:
WAS
Well Depth: 22.2 ft.
Well Diameter: 2 in.
pH 00400: 4.8 units Temp. 000lc 26.5 °C
DRY at
Depth to Water Level 82546: 13 ft. below measuring point Screened Interval: 5 ft. to
20 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.25 ft. above land surface
Relative M.P. Elevation: 10.35 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 4.61
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 6/28/2023
Laboratory Name. 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 <1 /100mL
Nitrate (NO3) as N 00620 0.42
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P oo665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 31 mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 4.83 units
Ba - Barium 01007
ug/L
TOC 00680 <0.5 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 80 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095 µMhos
K - Potassium 00937
mg/L
VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen: NH3 as N: Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625 mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please print or Noe
GW-59 Rev.8/2013
Authorized Agent)
(Date)
7/27/2023

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
Jacksonville NC
28540 County Onslow
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-12
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-12
Date sample collected: 6/27/2023
FIELD ANALYSES:
WAS
Well Depth: 18.3 ft.
Well Diameter: 2 in.
pH 0040o: 5.5 units Temp. 000lo: 22.2 °C
DRY at
Depth to Water Level 82546: 5.1 ft. below measuring point
Screened Interval: 5 ft. to
15 ft. Spec. Cond. 00094: ItMhos
time of
sampling,
Measuring Point is 3.04 ft. above land surface
Relative M.P. Elevation: 2.06 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
6.34
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 6/27/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 0.09
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 148.5
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 5.53
units
Ba - Barium 01007
ug/L
TOC 00680 27
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 13
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 9
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia oo6lo <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%

SUBMIT FORM ON YELLOW PAPER ONLY
• .
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-13
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-13
Date sample collected: 6/26/2023
FIELD ANALYSES:
WAS
Well Depth: 23.2 ft.
Well Diameter: 2 in.
pH 00400: 4.7 units Temp. 000lc 29.7 °C
DRY at
Depth to Water Level 62546: 14 ft. below measuring point Screened Interval: 10.5 ft. to
23.2 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.75 ft. above land surface
Relative M.P. Elevation: 11.25 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
4.42
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 6/26/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 60.5
mg/L
Al - Aluminum 01105
mg/L
pH (Lab) 00403 4.7
units
Ba - Barium 01007
ug/L
TOC 00680 1.3
mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 27
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.8/2013
(or Authorized Aoent)
(Date)
7/27/2023

SUBMIT FORM ON YELLOW PAPER ONLY
• .
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• •
•
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print
Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville Land Treatment System
Non -Discharge W00009267 UIC
Permit Name (if different):
NPDES Other
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 28540 County Onslow
1'
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-14
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-14
Date sample collected: 6/26/2023
FIELD ANALYSES:
WAS
Well Depth: 17.9 ft.
Well Diameter: 2 in.
pH 00400: 4.8 units Temp. 000lo: 28.2 °C
DRY at
Depth to Water Level 82546: 12 ft. below measuring point Screened Interval: 5 ft. to
15 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 11.8 ft. above land surface
Relative M.P. Elevation: -0.3 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
3.07
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 6/26/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.03
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 53.5
mg/L
AI - Aluminum 01105
mg/L
pH (Lab) 00403 4.84
units
Ba - Barium 01007
ug/L
TOC 00680 12.1
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 15
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia 00610 0.75
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aoent) Name and Title - Please print or Noe
GW-59
Rev. 8/2013

SUBMIT FORM ON YELLOW PAPFR nNl Y
GROUNDWATER QUALITY MONITORING:
• •
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
•
•
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 26540 County Onslow
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-15
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-15
Date sample collected: 6/28/2023
FIELD ANALYSES:
WAS
Well Depth: 15 ft.
Well Diameter: 2 in.
pH 0040o: 4.7 units Temp. 000lo: 24.4 °C
DRY at
Depth to Water Level 82546: 3.8 ft. below measuring point
Screened Interval: 5 ft. to
15
ft. Spec. Cond. 00094: µMhos
time of
Measuring Point is 2.9 ft. above land surface
Relative M.P. Elevation: 0.9 ft.
Odor 00085:
sampling,
Volume of water pumped/bailed before sampling:
5.38
gallons
Appearance
check
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES El NO
LABORATORY INFORMATION
Date sample analyzed: 6/28/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L
Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 1.36
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 107
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 4.71
units
Ba - Barium 01007
ug/L
TOC omm 1.2
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 46
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ® Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 7873 method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 0105s
9
uglL
,method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aoent) Name and Title - Please print or tvoe
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
•
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
Permit Name (if different):
NPDES Other
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC-,,r,ao County Onslow
'!"l
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-16
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-16
Date sample collected: 6/28/2023
FIELD ANALYSES:
WAS
Well Depth: 25 ft.
Well Diameter: 2 in.
pH 00400: 4.9 units Temp. 000lo: 20.8 oC
DRY at
Depth to Water Level 82546: 10 ft. below measuring point
Screened Interval: 15 ft. to
20 ft. Spec. Cond. 00094 µMhos
time of
sampling,
Measuring Point is 2.4 ft. above land surface
Relative M.P. Elevation: 7.8 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling:
7.10
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 6/28/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 0.58
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 116.5
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 4.94
units
Ba - Barium 01007
ug/L
TOC om8o 1.7
mg/L
Ca - Calcium oo916
mg/L
Chloride o0940 38
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate o0945 9
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia oo6lo <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aoent) Name and Title - Please print or tvoe
GW-59 Rev.8/2013
Authorized Aoent)
(Date)
7/27/2023

SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print
Clearly or Type
PERMIT Number: Expiration Date: 7/31/2029
Facility Name: City of Jacksonville
Land Treatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Jacksonville NC 2854C' County Onslow
X Spray Field ❑ Remediation:
Contact Person: Amy Palaschak
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW-17
No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-17
Date sample collected: 6/28/2023
FIELD ANALYSES:
WAS
Well Depth: 25 ft.
Well Diameter: 2 in.
pH 0040o: 4.9 units Temp. 000lo 19.7 °C
DRY at
Depth to Water Level 82546: 7.2 ft. below measuring point
Screened Interval: 15 ft. to
20 ft. Spec. Cond. 00094: µMhos
time of
sampling,check
Measuring Point is 1.9 ft. above land surface
Relative M.P. Elevation: 5.3 ft.
Odor 00085:
Volume of water pumped/bailed before sampling:
8.54
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: X
YES
❑ NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 6/28/2023
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665 <0.2
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids -.Total 70300 102
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403 4.86
units
Ba - Barium 01007
ug/L
TOC 00680 0.8
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 33
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 11
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ® Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia oo6lo <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn -Manganese oloss
ug/L ,method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Wally Hansen - Public Services Director
Permittee (or Authorized Aqent) Name and Title - Please print or tvoe
GW-59 Rev.8/2013

F"0507
6eZnviroehem:1.
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab;'Fax
inf6a environmentalchemists.corn
City of Jacksonville Date of Report: Jul 20, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-13296
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-33099 Site: MW-5 6/26/2023 11:42 AM Water Cv
Test Method Results Date Analyzed
Sulfate
EPA 300.0, Rev. 2.1, 1993
<5 mg/L
06/29/2023
Total Organic Carbon (TOC)
SM 6310 B-2014
1.5 mg/L
06/29/2023
Chloride
SM4500 CI E-2011
7 mg/L
06/29/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
1, 1, 1 -Trichloroethane
SW 846 Method 826oD/5030B
<0.5 pg/L
06/29/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0 5 pg/L
06/29/2023
1,1,2-Trichloroethane
SW 846 Method 82SOD15030B
<0,5 pg/L
06/29/2023
1,1-Dichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,1-D ichloroethene
SW 846 Method 82600/50306
<0.5 pg/L
06/29/2023
1,1-Dichloropropene
SW 846 Method 8260DIS03DB
<0.5 pg/L
06/29/2023
1,2, 3-Trichlorobenzene
SW 846 Method 826OD150308
<0.5 pg/L
06/29/2023
1,2,3-Trichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,2,4-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/29/2023
1,2,4-Trimethylbenzene
SW 846 Method 82BOD16030B
<0.5 pg/L
06/29/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
<0,5 pg/L
06/29/2023
1,2-Dibromoethane
SW 846 Method 826OD150308
<0.5 pg/L
06/29/2023
1,2-Dichlorobenzene
SW 846 Method 826013/503013
<0.5 pg/L
06/29/2023
1,2-Dichloroethane
SW 846 Method 8260DIS030B
<0,5 pg/L
06/29/2023
1,2-Dichloropropane
SW 846 Method 8260D/50308
<0.5 pg/L
06/29/2023
1,3,5-Trimethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1, 3-Dichlorobenzene
SW 846 Method 8260DIS030B
<0.5 pg/L
06/29/2023
1,3-Dichloropropane
SW 846 Method 82s0D15030B
<0.5 pg/L
06/29/2023
1,4-Dichlorobenzene
SW 846 Method 826OD15030B
<0,5 pg/L
06/29/2023
2,2-Dichloropropane
SW 846 Method 826OD150308
<0.5 pg/L
06/29/2023
2-Chlorotoluene
SW 846 Method 826013/50308
<0.5 pg/L
06/29/2023
4-Chlorotoluene
SW 846 Method MOD15030B
<0.5 pg/L
06/29/2023
Report tt:: 2023-13296 Page 1 of 1 B

envirochem
�M
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, Nc_ 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab,, Fax
into a envtronmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Jul 20, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-13296
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D150308
<0.5 pg/L
06/29/2023
Bromobenzene
SW 848 Method 8260D15030B
<0.5 pg/L
06/29/2023
Bromochloromethane
SW 846 Method 82SOD15030B
<0.5 pg/L
06/29/2023
Bromodichloromethane
SW 846 Method 82BOD16030B
<0.5 pg/L
06/29/2023
Bromoform
SW 846 Method 826OD/5030B
<0.5 pg/L
06/29/2023
Bromomethane
SW 846 Method 8260D15D30B
<0.5 pg/L
06/29/2023
Carbon tetrachloride
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
Chlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Chloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Chloroform
SW 846 Method 8260015030E
<0.5 pg/L
06/29/2023
Chloromethane
SW 846 Method 82601)/5030B
<0.5 pg/L
06/29/2023
cis- 1,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
cis-1, 3-Dichloropropene
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
Dibromochloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
Dibromomethane
SW W Method 8260DIS030B
<0.5 pg/L
05/29/2023
Dichlorodifluoromethane
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
Ethylbenzene
SW 848 Method 8260D/5030B
<0.5 pg/L
06/29/2023
Hexachlorobutadiene
SW B46 Method 8260D/5030B
<0.5 pg/L
06/29/2023
Isopropylbenzene
SW 848 Method 8MD/50308
<0.5 pg/L
06/29/2023
M+P Xylene
SW 846 Method 826OD/5030B
<1.0 pg/L
06/29/2023
Methylene chloride
SW 8" Method 8260D15030B
<0.5 pg/L
06/29/2023
Naphthalene
SW 846 Method 8260D!5030B
<0.5 pg/L
06/29/2023
n-Butylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
n-Propylbenzene
SW 846 Method 8260DISO30B
<0.5 pg/L
06/29/2023
ortho-Xylene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
p-Isopropyltoluene
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
sec -Butyl benzene
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
Styrene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
tert-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/29/2023
Tetrachloroethene
SW 848 method 82ND150 OB
<0.5 pg/L
06/29/2023
Report #- 2023-13296
Pape 2 of 18

M
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 @ 910.347.5843 Lab/Fax
info a environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Jul 20, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-13296
Project ID: Monitoring Wells
Toluene
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
Trans-1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
Trans- 1,3-dichloropropene
SW 646 Method 826OD15030B
<0.5 µg/L
06/29/2023
Tnchloroethene
SW 846 Method 8260D/5030B
<0.5 µg/L
06/29/2023
Tnchlorofluoromethane
SW 846 Method 826OD15030B
<Q.5 ug/L
06/29/2023
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 µg/L
06/29/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA353.2, Rev 20. 1993
< 0.02 mg/L
06/28/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev 2.0, 1993
< 0.02 mg/L
06/28/2023
Nitrate Nitrogen
subtraction Method
<0.02 mg/L
07/14/2023
Report # 2023-13296 Page 3 of 18

F"0007
,Znviroch7em]
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392,4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab Fax
255 A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab,,, Fax
info a environmentalchemists.com
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-13296
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-33100 Site: MW-8
6/26/2023
9A5 AM Water CV
Test
Method
Results Date Analyzed
Sulfate
EPA 3000 Rev 21, 1993
95 mg/L
06/29/2023
Total Organic Carbon (TOG)
SM 5310 B-2014
3.1 mg/L
06/29/2023
Chloride
SM4500 CI E-2011
7 mg/L
06/29/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 82BOD15030B
<0.5 µg/L
06/29/2023
1. 1, 1 -Trichloroethane
SW 848 Method 8260D 5a30B
<0.5 µg/L
06/29/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 µg/L
06/29/2023
1,1,2-Trichloroethane
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
1,1-Dichloroethane
SW B46 Method 826GD1503GB
<0.5 µg/L
06/29/2023
1,1-Dichloroethene
SW 046 Method 8260D'50308
<0.5 µg/L
06/29/2023
1,1-Dichloropropene
SW 846 Method 8260D15030B
<0.5 µg/L
06/29/2023
1, 2, 3-Trichlorobenzene
SW s48 Method 826OD15030B
<0.5 µg/L
06/29/2023
1,2,3-Trichloropropane
SW a46 Method 82600r503013
<0.5 µg/L
06/29/2023
1,2,4-Trichlorobenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260D'5030B
<0.5 µg/L
06/29/2023
1 2-Dibromo-3-Chloropropane
SW 646 Method 8260&5030B
<0.5 µg/L
06/29/2023
1,2-Dlbromoethane
SW 646 Method 8260M50306
<0.5 µg/L
06/29/2023
1,2-Dichlorobenzene
SW 846 Method 8260D'5030e
<0.5 µg/L
06/29/2023
1,2-Dichloroethane
SW 846 Method 8260D50308
<0.5 µg/L
06/29/2023
1,2-Dichloropropane
SW B46 Method 8260D,,5030B
<0.5 µg/L
06/29/2023
1,3,5-Trimethylbenzene
SW 846 Method 8260D 50306
<0.5 µg/L
06/29/2023
1,3-Dichlorobenzene
SW 846 Method 8260015030B
<0.5 µg/L
06/29/2023
1, 3-Dichloropropane
SW 846 Method 826ODM30B
<0.5 µg/L
06/29/2023
1,4-Dichlorobenzene
SW 846 Method 8260DIS030B
<0.5 µg/L
06/29/2023
2,2-Dichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
2-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
4-Chlorotoluene
SW 846 Method 8260D50808
<0.5 µg/L
06/29/2023
Report It 2023-13296 Page 4 of 18

Cnvirochelm
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/ Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab,/ Fax
info a,environmentalchemists.com
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-13296
Project ID: Monitoring Wells
Benzene
SW 846 Method 826OD15030B
<0.5 lag/L
06/29/2023
Bromobenzene
SW 845 Method 826OD15030B
<0.5 lag/L
06/29/2023
Bromochloromethane
SW 846 Method 82BOD/5030B
<0.5 pg/L
06/29/2023
Bromodichloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
Bromoform
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Bromomethane
SW 84B Method 826DD15030B
<0.5 pg/L
06/29/2023
Carbon tetrachloride
SW 846 Method 826OD15030B
<0.5 lag/L
06/29/2023
Chlorobenzene
sw 846 Method 826OD15030B
<0.5 lag/L
06/29/2023
Chloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Chloroform
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Chloromethane
SW 846 Method MOD15030B
<0.5 pg/L
06/29/2023
cis-1, 2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
cis- 1,3-Dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Dibromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Dibromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Dtchlorodifluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Ethylbenzene
SW 846 Method 8260016030E
<0.5 pg/L
06/29/2023
Hexachlorobutadiene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
lsopropylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
M+P Xylene
SW 846 Method 826OD15030B
<1.0 pg/L
06/29/2023
Methylene chloride
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Naphthalene
SW 946 Method 826OD15030B
<0.5 pg/L
06/29/2023
n-Butylbenzene
SW a46 Method 82SOD15030B
<0.5 pg/L
06/29/2023
n-Propylbenzene
SW 846 Method 82BOD15030B
<0.5 pg/L
06/29/2023
ortho-Xylene
SW a46 Method 826OD/5030B
<0.5 pg/L
06/29/2023
p-Isopropyltoluene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
sec-Butylbenzene
SW 846 Method 8260015030E
<0.5 pg/L
06/29/2023
Styrene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
tert-Butylbenzene
SW 848 Method 826OD150308
<0.5 pg/L
06/29/2023
Tetrachloroethene
sw 8" Memod MM/50M
<0.5 pg1L
06/29/2023
Report It 2023-13296 Page 5 of 18

Environmental Chemists, Inc.
enviroehem
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
inf6a environmentalchemists.com
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO M
Jacksonville NC
28541
Customer ID: 08110015
Attention-
Report #: 2023-13296
Project ID: Monitoring Wells
Toluene
SW 846 Method 82600150308
<0.5 pg/L
06/29/2023
Trans-1 ,2-Dichloroethene
SW 646 Method 826OD15030B
<0.5 pg/L
06/29/2023
Trans-1,3-dichloropropene
SW 646 Method 826OD150308
<0.5 pg/L
06/29/2023
Trichloroethene
SW 846 Method 82600/5030B
<0.5 pg/L
06/29/2023
Trichlorofluoromethane
SW W Method 826ODr5030B
<0.5 pg/L
06/29/2023
Vinyl chloride
SW 846 Method BMD15030B
<0.5 ug/L
06/29/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2, Rev 2.0, 1993 < 0.02 mg/L 06/28/2023
Nitrate+Nitnte-Nitrogen EPA 353.2. Rev 2 0, 1993 0.13 mg/L 06/28/2023
Nitrate Nitrogen Subtraction Method 0.13 mg/L 07/14/2023
Report* 2023-13298 Page 6 of 18

6Znviroche]m
F""07
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392,0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab; Fax
ANALYTICAL & CONSULTING CHEMISTS info a environmentalchemists.com
City of Jacksonville Date of Report: Jul 20, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-13296
Project ID: Monitoring Wells
Lab ID Sample ID:
23-33101 Site: MW-9
Test
Sulfate
Total Organic Carbon (TOC)
Chloride
1, 1, 1,2-Tetrachloroethane
1, 1, 1 -Trichloroethane
1, 1,2,2-Tetrach loroethane
1,1,2-Trichloroethane
1, 1 -Dich loroethane
1,1-Dichloroethene
1,1-Dichloropropene
1, 2, 3-Trichlorobenzene
1,2, 3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1, 3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Collect Date/Time Matrix
6/26/2023 10:10 AM Water
Method
EPA 300.0, Rev 2 1, 1993
SM 5310 B-2014
SM4500 Cl E-2011
SW 846 Method 8260D150308
SW 846 Method 8260D/5030B
SW 846 Method MOD15030B
SW 848 Method 826OD15030B
SW 846 Method 82600/5030B
SW 846 Method 8260D/5030B
SW 846 Method 826OD150308
SW 846 Method 8280D/5030B
SW 846 Method 826OD15030B
SW 846 Method 826aD/5030B
SW 848 Method 8260D/5030B
SW 846 Method 826aD/5030B
SW 846 Method 8260DIS0306
SW 846 Method 826OD15030B
SW 846 Method 826OD15030B
SW 846 Method 826OD150303
SW 846 Method 826OD15030B
SW 846 Method MOD15030B
SW 846 Method 826OD15030B
SW 846 Method 826OD16030B
SW 846 Method 826OD15030B
SW 846 Method 8260015030E
SW 846 Method 826OD15030B
Results
Sampled by
CV
Date Analyzed
97 mg/L
06/29/2023
2.3 mg/L
06/29/2023
9 mg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
Report*: 2023-13296 Page 7 of 18

77
Environmental Chemists,
Inc.
envirochem
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392,4424
Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington
Highway, Jacksonville, NC 28540 • 910.347.5843 Lab,' Fax
ANALYTICAL & CONSULTING CHEMISTS
info(a environmentalchemists.com
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO M
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report M 2023-13296
Project ID: Monitoring Wells
Benzene
SW 846 Method 82601)/50308
<0.5 pg/L
06/29/2023
Bromobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Bromochloromethane
SW 646 Method 828oD15030B
<0.5 pg/L
06/29/2023
Bromodichloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
06/29/2023
Bromomethane
SW 846 Method 826OD150308
<0.5 pg/L
06/29/2023
Carbon tetrachloride
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/29/2023
Chloroethane
SW 80 Method 8260D/5030B
<0.5 pg/L
06/29/2023
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
06/29/2023
Chloromethane
SW 846 Method BMD1503DB
<0.5 lag/L
06/29/2023
cis-12-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/29/2023
cis-1,3-Dichloropropene
SW B46 Method 8260DI5030B
<0.5 pg/L
06/29/2023
Dibromochloromethane
SW 846 Method 8260D/5030B
<Q.5 pg/L
06/29/2023
Dibromomethane
SW B48 Method 826OD15030B
<0.5 pg/L
06/29/2023
Dichlorodifluoromethane
SW 848 Method 8260D/5030B
<0.5 pg/L
06/29/2023
Ethylbenzene
SW 80 Method 8260D/5030B
<0.5 pg/L
06/29/2023
Hexachlorobutadiene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Isopropylbenzene
SW B46 Method B26OD15030B
<0.5 pg/L
06/29/2023
M+P Xylene
SW 846 Method 826OD15030B
<1.0 pg/L
06/29/2023
Methylene chloride
SW 848 Method 826OD15030B
<0.5 pg/L
06/29/2023
Naphthalene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
n-Butylbenzene
SW 848 Method 8260DI5030B
<0.5 pg/L
06/29/2023
n-Propylbenzene
SW B46 Method 826OD/5030B
<0.5 pg/L
06/29/2023
ortho-Xylene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
p-Isopropyltoluene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
sec-Butylbenzene
SW 846 Method 826OD150308
<0.5 pg/L
06/29/2023
Styrene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
tert-Butylbenzene
SW 646 Method 826OD15030B
<0.5 pg/L
06/29/2023
Tetrachloroethene
SW 840 Method 629DW50"
<0.5 pg/L
08/29/2023
Report* 2023-13296
Page 8 of 18

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infofh environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Jul 20, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-13296
Project ID: Monitoring Wells
Toluene
SW 8" Method 626ODr5030B
<0.5 pg/L
06/29/2023
Trans- 1,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
Trans- 1,3-dichioropropene
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
Trichioroethene
SW 846 Method 8280015030E
<0,5 pg/L
06/29/2023
Trichlorofluoromethane
SW 846 Method 82601)15030B
<0.5 pg/L
06/29/2023
Vinyl chloride
SW 846 Method 8260D1503013
<0.5 pg/L
06/29/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev 2.0, 1993
< 0.02 mg/L
06/28/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2. Rev 2 0, 1993
< 0.02 mg/L
06/28/2023
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
07/14/2023
Report # 2023-13296 Page 9 of 18

[en7v_oeh7]ir
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab,, Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab?, Fax
info(u environmentalchemists.com
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-13296
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect DatelTime Matrix Sampled by
23-33102 Site: MW-10
6/26/2023
10:29 AM Water Cv
Test
Method
Results Date Analyzed
Sulfate
EPA 300.0, Rev. 2.1, 1993
149 mg/L
06/29/2023
Total Organic Carbon (TOG)
SM 5310 6-2014
2.1 mg/L
06/29/2023
Chloride
SM45M CI E-2011
21 mg1L
06/29/2023
1.1,1,2-Tetrachloroethane
SW 848 Method 82BOD15030B
<0.5pg/L
06/29/2023
1,1,1-Tiichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,1,2-Trcchloroethane
SW 846 Method 826OD15030B
<0,5 pg/L
06/29/2023
1,1-Dichloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
06/29/2023
1. 1 -Dichloroethene
SW 846 Method 826oD/5030B
<0.5 pg/L
06/29/2023
1, 1 -Dich loropropene
SW 846 Method 82600/5030B
<0.5 pg/L
06/29/2023
1,2,3-Trichlorobenzene
SW 846 Method 8260D/50306
<0.5 pg/L
06/29/2023
1,2, 3-Trichloropropane
SW 846 Method 82601)150308
<0.5 pg/L
06/29/2023
1, 2,4-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/29/2023
1,2,4-Trimethylbenzene
SW 646 Method 826OD150308
<0.5 pg/L
06/29/2023
1,2-Dibromo-3-Chloropropane
SW 046 Method 8260D/5030B
<0.5 pg/L
06/29/2023
1,2-Dibromoethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,2-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/29/2023
1, 2-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
06/29/2023
1,2-Dichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,3,5-Trimethylbenzene
SW 846 Method 026OD150308
<0.5 pg/L
06/29/2023
1, 3-Dichlorobenzene
SW 646 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,3-Dichloropropane
SW 848 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/29/2023
2,2-Dichloropropane
SW 848Method 82600/5030B
<0.5 pg/L
06/29/2023
2-Chlorotoluene
SW 846 Method MOD15030B
<0.5 pg/L
06/29/2023
4-Chlorotoluene
SW 846 Method 82BOD15030B
<0.5 pg/L
06/29/2023
Report #: 2023-13296 Page 10 of 18

[en7virroche]m
ANALYTICAL 8 CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/ Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/ Fax
info rcenvironmen talchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Jul 20, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-13296
Project ID: Monitoring Wells
Benzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Bromobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Bromochloromethane
Sw 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Bromodichloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
Bromoform
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
Bromomethane
SW 846 Method 826OD150308
<0_5 pg/L
06/29/2023
Carbon tetrachloride
SW 846 Method 8260M6030B
<0.5 pg/L
06/29/2023
Chlorobenzene
SW 845 Method 826OD15030B
<0.5 pg/L
06/29/2023
Chloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Chloroform
SW 846 Method 826OD15030B
<0.5 pg/L
06/2912023
Chloromethane
SW 846 Method 8260015030E
<0.5 pg/L
06/29/2023
cis-1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
cis- 1,3-Dichloropropene
SW a46 Method 8260D15030B
<0.5 pg/L
06/29/2023
Dibromochloromethane
SW 846 Method B26OD150308
<0.5 pg/L
06/29/2023
Dibromomethane
sw 646 Method 826OD15030B
<0.5 pg/L
06/29/2023
Dichlorodifluoromethane
SW 846 Method 8260015030E
<0.5 pg/L
06/29/2023
Ethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Hexachlorobutadiene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
lsopropylbenzene
SW 846 Method B26DD15030B
<0.5 pg/L
06/29/2023
M+P Xylene
SW 846 Method 826OD150308
<1.0 pg/L
06/29/2023
Methylene chloride
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Naphthalene
SW 846 Method 826OD150308
<0.5 pg/L
06/29/2023
n-Butylbenzene
SW 846 Method 8260D15030B
<Q.5 pg/L
06/29/2023
n-Propylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
ortho-Xylene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
p-Isopropyltoluene
SW 846 Method 8260015030E
<0.5 pg/L
06/29/2023
sec-Butylbenzene
sw 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Styrene
SW 846 Method 826OD150308
<0.5 pg/L
06/29/2023
tert-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Tetrachloroethene
SW 840 MOMM 82M IM03
<0.5 pg/L
06/29/2023
Report tk 2023-13296
Page 11 of 1e

F7�
je:nviroc:hem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info a environmentalchemists.com
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-13296
Project ID: Monitoring Wells
Toluene
SW s46 Method 826OD15030B
<0,5 pg/L
06/29/2023
Trans-1,2-Dichloroethene
SW 846 Method MOD/5030B
<0.5 pg/L
06/29/2023
Trans- 1,3-dichloropropene
SW 846 Method 82GOD15030B
<Q.5 pg/L
06/29/2023
Trichloroethene
SW B46 Method 826OD15030B
<0.5 pg/L
06/29/2023
Trichlorofluoromethane
SW 946 Method 826OD15030B
<0.5 pg/L
06/29/2023
Vinyl chloride
SW 846 Method 826OD/5030B
<0.5 Wg/L
06/29/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 06/28/2023
Nitrate+ Nitrite-N itrogen EPA 353.2, Rev. 2.0. 1993 0.03 mg/L 06/28/2023
Nitrate Nitrogen Subtraction Method 0.03 mg/L 07/14/2023
Report #: � 2023-13296 Page 12 of 18

F"017— Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS inf6a emironmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC 28541
Attention:
Date of Report: Jul 20, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-13296
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-33103 Site: MW-13
6/26/2023
12:49 PM Water CV
Test
Method
Results Date Analyzed
Sulfate
EPA 300 0 Rev 2 1 1993
<5 mg/L
06/29/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
1.3 mg/L
06/29/2023
Chloride
SM4500 Q E-2011
27 mg/L
06/29/2023
1, 1, 1,2-Tetrachloroethane
SW a46 Method 8260Dr5o3nB
<0.5 pg/L
06/29/2023
1,1,1-Trichloroethane
SW 846 Method 8260D;5030B
<0.5 pg/L
06/29/2023
1,1,2,2-Tetrachloroethane
SW846Method 8260D/5030B
<0.5pg/L
06/29/2023
1,1,2-Trichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,1-Dichloroethane
SW 846 Method 8280D15030B
<0.5 pg/L
06/29/2023
1,1-Dichloroethene
SW 846 Method 826OD150308
<0.5 pg/L
06/29/2023
1, 1 -Dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,2, 3-Trichlorobenzene
SW 846 Method 8260D150308
<0.5 pg/L
06/29/2023
1,2,3-Trichloropropane
SW 846 Method 826OD15030B
<0_5 pg/L
06/29/2023
1,2,4-Trichlorobenzene
SW 646 Method 82BOD15030B
<0.5 pg/L
06/29/2023
1,2,4-Trimethylbenzene
SW 846 Method MOD15030B
<0.5 pg/L
06/29/2023
1,2-Dibromo-3-Chloropropane
SW 84_ Method 8260D15030B
<0.5 pg/L
06/29/2023
1,2-Dibromoethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,2-Dichlorobenzene
SW 846 Method 8280D150308
<0.5 pg/L
06/29/2023
1,2-Dichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,2-Dichloropropane
SW 846 Method 826OD150308
<0.5 pg/L
06/29/2023
1,3,5-Trimethylbenzene
SW 846 Method 82BOD15030B
<0.5 pg/L
06/29/2023
1,3-Dichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
1, 3-Dichloropropane
SW 846 Method B26ODY5030B
<0.5 pg/L
06/29/2023
1,4-Dichlorobenzene
SW 846 Method 626OD15030B
<0.5 pg/L
06/29/2023
2,2-Dichloropropane
SW 846 Method 8260015030B
<0.5 pg/L
06/29/2023
2-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
4-Chlorotoluene
SW 846 Method 8260o15030B
<0.5 pg/L
06/29/2023
Report #:: 2023-13296
Page 13 of 18

ro"07 q1 Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
L to 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255 A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoialenvironmentalchemists.com
City of Jacksonville Date of Report: Jul 20, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-13296
Project ID: Monitoring Wells
Benzene
SW 846 Method 82600150308
<0.5 µg/L
06/29/2023
Bromobenzene
SW 846 Method 8269D15030B
<0.5 µg/L
06/29/2023
Bromochloromethane
SW Safi Method 82BOD15030B
<0.5 µg/L
06/29/2023
Bromodichloromethane
SW 846 Method 8260D15030B
<0.5 µg/L
06/29/2023
Bromoform
SW Safi Method 8260D15030B
<0.5 µg/L
06/29/2023
Bromomethane
SW 846 Method 8260131503013
<0.5 pg/L
06/29/2023
Carbon tetrachloride
SW B46 Method 826OD15030B
<0.5 µg/L
06/29/2023
Chlorobenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
Chloroethane
SW 846 Method 82601)15030B
<0.5 pg/L
06/29/2023
Chloroform
SW 646 Method 826OD15030B
<0.5 µg/L
06/29/2023
Chloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
cis-1,2-Dichloroethene
SW S46 Method 826OD150308
<0.5 pg/L
06/29/2023
cis- 1,3-Dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Dlbromochloromethane
SW 646 Method 82BODIM30B
<0.5 µg/L
06/29/2023
Dibromomethane
SW Safi Method 826OD15030B
<0.5 pg/L
06/29/2023
Dichlorodifluoromethane
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
Ethylbenzene
SW 846 Method 8260D15030B
<0.5 µg/L
06/29/2023
Hexachlorobutadiene
SW Safi Method MOD15030B
<0.5 µg/L
06/29/2023
Isopropylbenzene
SW B46 Method 8260131503013
<fl.5 µg/L
06/29/2023
M+P Xylene
SW 846 Method 826OD15030B
<1.0 µg/L
06/29/2023
Methylene chloride
SW 846 Method 82601)15030B
<0.5 µg/L
06/29/2023
Naphthalene
SW 648 Method 826OD15030B
<0.5 pg/L
06/29/2023
n-Butylbenzene
SW Safi Method 826OD15030B
<0.5 µg/L
06/29/2023
n-Propylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
ortho-Xylene
SW 846 Method 826OD/5030B
<0.5 µg/L
06/29/2023
p-Isopropyltoluene
SW Safi Method 826ODM30B
<0.5 µg/L
06/29/2023
sec -Butyl benzene
SW 946 Method 826OD15030B
<0.5 µg/L
06/29/2023
Styrene
SW 646 Method 82600/5030B
<0.5 pg/L
06/29/2023
tert-Butylbenzene
SW 646 Method 826OD15030B
<0.5 µg/L
06/29/2023
Tetrachloroethene
sW lute Memod as M,,5=8
<0.5 pg/L
06/29/2023
Report 9- 2023-13296
Page 14 of 18

- -71
ANALYTICAL & CONSULTING CHEMISTS
FFOPO'.
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Jul 20, 2023
Customer PO M
Customer ID: 08110015
Report M 2023-13296
Project ID: Monitoring Wells
Toluene
SW 848 Method 826OW503013
<0.5 pg/L
06/29/2023
Trans-1.2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Trans-1,3-dichloropropene
SW 846 Method 8260D/50306
<0.5 pg/L
06/29/2023
Trichloroethene
SW 846 Method 8260D15030B
<0.5 Ng/L
06/29/2023
Tnchlorofluoro methane
SW 646 Method 826OD15030B
<0 5 ug/L
06/29/2023
Vinyl chloride
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev 2 0, 1993
< 0.02 mg/L
06/28/2023
Nitrate+Nitrite-Nitrogen
EPA353.2, Rev 20,1993
< 0.02 mg/L
06/28/2023
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
07/14/2023
Report # 2023-13296 Page 15 of 18

[en7viroche]m
ANALYTICAL & CONSULTING CHEMISTS
City of Jacksonville
Post Office Box 128
Jacksonville
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab e 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
info i environmentalchemists.com
Date of Report: Jul 20, 2023
Customer PO M
NC 28541 Customer ID: 08110015
Report #: 2023-13296
Project ID: Monitoring Wells
Lab 1D Sample ID:
23-33104 Site: MW-14
Test
Sulfate
Total Organic Carbon (TOC)
Chloride
1, 1, 1,2-Tetrachloroethane
1,1,1-Trish loroethane
1,1,2,2-Tetrachloroethane
1,1, 2-Trichloroetha ne
1,1-Dichloroethane
1,1-Dichloroethene
1, 1 -Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1, 2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1, 3, 5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Collect Date/Time Matrix
6/26/2023 12:38 PM Water
Method
EPA 300.0, Rev, 2.1, 1993
SM 5310 B-2014
SM4500 CI E-2011
SW 846 Method MOD15030B
SW 846 Method 8260D15030B
SW 846 Method 8260D15030B
SW 846 Method 8260D/5030B
SW 946 Method 0260016030B
SW 846 Method 8260D15030B
SW 846 Method 82SOD15030B
SW 846 Method 8260D15030B
SW 846 Method 8260D150308
SW 846 Method 82BOD16030B
SW 846 Method 8260D15030B
SW 846 Method 6260D15030B
SW 846 Method 8280D/50308
SW 848 Method 826OD15030B
SW 846 Method 82BOD15030B
SW B46 Method 8260D15030B
SW 946 Method 8260015030E
SW 846 Method 8260D15030B
SW 848 Method 826OD/50308
SW 846 Method 8280D/5030B
SW 846 Method 82BOD/5030B
SW 846 Method 8260D15030B
SW 848 Method 0260DI6030B
Results
Sampled by
CV
Date Analyzed
<5 mg/L
06/29/2023
12.1 mg/L
06/29/2023
15 mg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
<0.5 pg/L
06/29/2023
Reportk. 2023-13298 Page 16 of 18

71 Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab,, Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info Cenvironmentalchemists.com
City of Jacksonville Date of Report: Jul 20, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-13296
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
Bromobenzene
SW 846 Method 82BOD/5030B
<0.5 pg/L
06/29/2023
Bromochloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
Bromodichloromethane
SW 846 Method 826OD150306
<0.5 pg/L
06/29/2023
Bromoform
SW 846 Method 8260DIS030B
<0.5 pg/L
06/29/2023
Bromomethane
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
Carbon tetrachloride
SW 846 Method 826OD15030B
<0.5 pglL
06/29/2023
Chlorobenzene
SW 846 Method 8260DI5030B
<0.5 pg/L
06/29/2023
Chloroethane
SW 848 Method 8260D15030B
<0.5 pg/L
06/29/2023
Chloroform
SW 848 Method 8260D15030B
<0 5 pg/L
06/29/2023
Chloromethane
SW 846 Method 8260D150308
<0.5 pg/L
06/29/2023
cis- 1,2-Dichloroethene
SW 846 Method 82601)50a0B
<0.5 pg/L
06/29/2023
cis-1, 3-Dichloropropene
SW 846 Method 8260Dr50306
<0.5 pg/L
06/29/2023
Dibromochloromethane
SW 846 Method 8260Dr50306
<0.5 pg/L
06/29/2023
Dibromomethane
SW 846 Method 8260D,50308
<0.5 pglL
06/29/2023
Dichlorodifluoromethane
SW 848 Method 8260D5030B
<0.5 pg/L
06/29/2023
Ethylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
Hexachlorobutadiene
SW 846 Method 8260D150306
<0.5 pg/L
06/29/2023
Isopropylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
M+P Xylene
SW 848 Method 8260D�5030B
<1.0 pg/L
06/29/2023
Methylene chloride
SW 846 Method 8260D�50306
<0.5 pg/L
06/29/2023
Naphthalene
SW 846 Method 8260D50306
<0.5 pg/L
06/29/2023
n-Butylbenzene
SW B46 Method 8260D5030B
<0.5 pg/L
06/29/2023
n-Propylbenzene
sw 840 Method 8260D�5030B
<0.5 pg/L
06/29/2023
ortho-Xylene
SW 846 Method 8260DI5D30B
<0.5 pg/L
06/29/2023
p-Isopropyltoluene
SW 846 Method 8260D5030B
<0.5 pg/L
06/29/2023
sec-Butylbenzene
SW 846 Method 8260D5030B
<0.5 pg/L
06/29/2023
Styrene
SW 846 Method 82BOD.!50308
<0.5 pg/L
06/29/2023
tert-Butylbenzene
SW 846 Method 825OD15D306
<0.5 pg/L
06/29/2023
Tetrachloroethene
SW 80 Mellnd e2801360308
<0.5 pg/L
06/29/2023
Report #- 2023-13296
Page 17 of 18

EK
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347,5843 Lab/Fax
info'a environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Jul 20, 2023
Customer PO M
Customer ID: 08110015
Report M 2023-13296
Project ID: Monitoring Wells
Toluene
SW M6 Method 8260DIS0308
<0.5 pg/L
06/29/2023
Trans- l ,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Trans- 1,3-dichloropropene
SW 846 Method 826OD150308
<0.5 pg/L
06/29/2023
Tdchloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Tdchlorofluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Vinyl chloride
SW 846 Method 8260DIS030B
<0.5 pg/L
06/29/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353 2. Rev. 2.0. 1993
<0.02mg/L
06/28/2023
Nitrate+Nitrite-Nitrogen
EPA 353 2. Rev. 2.0.1993
0.03mg/L
06/28/2023
Nitrate Nitrogen
Suatraofim Method
0.03 mg/L
07/14/2023
Comment:
Reviewed by:
Report#. 2023-13296 Page 18 of 18

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill W,
Wilmington, NC 284C
Sample Receipt Checklist 910-392.022
ci;ent�.l �(;{�p�1lJ� (�l� , �.}
Date: eport Number: 2Q?3- �� a
Re0 i;Pz Of ca:' P, . : nir. 1
i W
❑
YES
p
NO
ere cuSLody seals present on the cooler?
N/A
If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C
How tem t
gra;u p �e taken:
Corrected te mperature upon receipt
❑ =emp:3 �-L B a-t1- ® —
Against
IR Gun ID: Thomas Traceable S/N 210886869 r =C: 0.
I IR Gun Correction Factor `C: 0.0
YES
YES
❑
❑
NO
NO
3. if temperature of cooler exceeded 6`C, was Project M r, ?
g /QA notified.
12
YES
❑
NO
4. Were proper custody
Y procedures (relinquished/received} followed?
YES
S. Were sample ID s listed on the COC?
p
YES
❑
NO
6. Were samples ID's listed on sample containers?
YES
❑
❑
NO
7. Were collection date and time listed on the COC?
�i
YES
❑
NO
8. Were tests to be performed listed on the COC?
�$
YES
❑
NO
9. Did samples arrive in proper containers for each test?
L�
YES
❑
NO
10. Did samples arrive in good condition for each test?
l
YES
❑
NO
11. Was adequate sample volume available?'
YES
❑
NO
NO
12. Were samples received within proper holding time for requested tests?
❑
YES
❑
13. Were acid preserved samples received at a pH of <2?
❑
YES
❑
NO
14. Were cyanide samples received at a pH >12?
❑
YES
❑
NO
15. Were sulfide samples received at a pH >9?
❑
YES
❑
NO
NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L?
❑
YES
❑
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 f'n/L?
18. Were orthophosphate samples filtered in the field
within 15 minutes?
* TOC/Voiati!es are pH checked at time of analysis and recorded on the benchsheet.
** Bacter;a samp:es are checked for Ch'or:ne at t-me of analysis and recorded on the benchshe-,
bample Preservation: (Must be completed for any sampie(s} incorrect)
Sample(s) Y preserved or with headspacej
were by adding (c;rc:e one}: H�S0, HNO received incorrectly preserved and were adjusted accordingly
3 HG NaOH
.Time of preservat'on; If more than one preservative is needed, notate in comments below
Vote trot fy custo-ne-sen/ce i^
-^ed aie'y fo-l-co-•ect'y p-ese-ve- sa.np e; Qbta'r a new sample or
notify the state:ab if directea to ar•alyzed by the customer Who was notifed, date and time:
Volatiles Sample(s)
were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
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envirochen�71
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab, Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab!Fax
[e-mail]
City of Jacksonville Date of Report: Jul 20, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-13297
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-33105 Site: MW-3 6/27/2023 11:35 AM Water CV
Test Method Results Date Analyzed
Sulfate
EPA 300 0 Rev 2 1 1993
<5 mg/L
06/29/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
2.1 mg/L
06/29/2023
Chloride
SM4500 CI E-2011
10 mg/L
06/29/2023
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
06/29/2023
1, 1, 1 -Trichloroethane
SW 846 Method 826ODY5030B
<0.5 pg/L
06/29/2023
1,1,2 2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,1, 2-Trichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,1-Dichloroethane
SW 046 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,1-Dichloroethene
SW 846 Method 82600150308
<0.5 pg/L
06/29/2023
1,1-Dichloropropene
SW 846 Method 826OD150308
<0.5 pg/L
06/29/2023
1,2,3-Trichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
06/29/2023
1,2,3-Trichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
06/29/2023
1,2,4-Trichlorobenzene
SW 848 Method 8260D15030B
<0.5 pg/L
06/29/2023
1,2,4-Trimethylbenzene
SW 846 Method 8269D/5030B
<0.5 pg/L
06/29/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
06/29/2023
1,2-Dlbromoethane
SW 846 Method 82BOD150308
<0.5 pg/L
06/29/2023
1,2-Dichlorobenzene
SW WMethod 626OD150308
<0.5 pg/L
06/29/2023
1,2-Dichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,2-Dichloropropane
SW 846 Method 8260D50306
<0.5 pg/L
06/29/2023
1,3,5-Trimethylbenzene
SW 846 Method 8260D50308
<0.5 pg/L
06/29/2023
1,3-Dichlorobenzene
SW 846 Method 8260D5030B
<0.5 pg/L
06/29/2023
1,3-Dichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,4-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
06/29/2023
2-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
4-Chlorotoluene
SW 846 Method 8260131503013
<0.5 lag/L
06/29/2023
Report #' 2023-13297 Page 1 of 15

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab Fax
ANALYTICAL & CONSULTING CHEMISTS info;a-enviroil mentalchemists.com
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-13297
Project ID: Monitoring Wells
Benzene
SW 8a6 Method 826OD15030B
<0.5 µg/L
06/29/2023
Bromobenzene
SW 848 Method 82BOD15030B
<0.5 µg/L
06/29/2023
Bromochloromethane
SW 80 Method 826OD15030B
<0.5 µg/L
06/29/2023
Bromodichloromethane
SW 846 Method 8260D150308
<0.5 µg/L
06/29/2023
Bromoform
SW 846 Method 826OD/5030B
<0.5 µg/L
06/29/2023
Bromomethane
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
Carbon tetrachloride
SW 80 Method 826OD/5030B
<0.5 µg/L
06/29/2023
Chlorobenzene
SW sa6 Method 826OD/5030B
<0.5 µg/L
06/29/2023
Chloroethane
SW sas Method 826OD15030B
<0.5 µg/L
06/29/2023
Chloroform
SW 846 Method 826OD/5030B
<0.5 µg/L
06/29/2023
Chloromethane
SW eas Method 826OD/5030B
<0.5 µg/L
06/29/2023
cis-1 2-Dichloroethene
SW Bab method 826OD/5030B
<0.5 µg/L
06/29/2023
cis-1,3-Dichloropropene
SW 846 Method 82BOD16030B
<0.5 µg/L
06/29/2023
Dibromochloromethane
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
Dibromomethane
SW 846 Method 82601)150306
<0.5 µg/L
06/29/2023
Dichlorodifluoromethane
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
Ethylbenzene
SW 846 Method 826OD/5030B
<0.5 µg/L
06/29/2023
Hexachlorobutadiene
SW 846 Method B26OD15030B
<0.5 µg/L
06/29/2023
tsopropylbenzene
SW 846 Method 8260015030B
<0.5 µg/L
06/29/2023
M+P Xylene
SW 846 Method 82600/5030B
<1.0 µg/L
06/29/2023
Methylene chloride
SW 8a6 Method 8260015030E
<0.5 µg/L
06/29/2023
Naphthalene
SW 846 Method 826OD/5030B
<0.5 µg/L
06/29/2023
n-Butylbenzene
SW 80 Method 826OD15030B
<0.5 µg/L
06/29/2023
n-Propylbenzene
SW 846 Method 8260015030E
<0.5 pg/L
06/29/2023
ortho-Xylene
SW 846 Method MOD15030B
<0.5 pq/L
06/29/2023
p-Isopropyltoluene
SW 846 Method 826OD15030B
65.7 µg/L
06/29/2023
sec-Butylbenzene
SW 846 Method 82600/5030B
<0.5 µg/L
06/29/2023
Styrene
SW sa6 Method 826OD1503013
<0.5 fag/L
06/29/2023
tert Butylbenzene
SW 846 Method 826OD150308
<0.5 pg/L
06/29/2023
Tetrachloroethene
SW Sae Memos ezeoo>g M
<0.5 pgA
06/29/2023
Report # 2023 13297
Page 2 of 15

Environmental Chemists, Inc.
1 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Jul 20, 2023
Customer PO #:
Customer ID: 08110015
Report M 2023-13297
Project ID: Monitoring Wells
Toluene
SW 946 Method 8260D/50308
19.5 pg/L
06/29/2023
Trans- 1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Trans- 1,3-dichloropropene
SW 846 Method 826GD15030B
<0.5 pg/L
06/29/2023
Tnchloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Trichlorofluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Vinyl chloride
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353 2, Rev 2.0, 1993
< 0.02 mg/L
06/28/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev 2 0, 1993
0.06 mg/L
06/28/2023
Nitrate Nitrogen
Subtraction Method
0.06 mg/L
07/14/2023
Report # 2023-13297 Page 3 of 15

envirochen�7,
L'
ANALYTICAL 8 CONSULTING CHEMISTS
City of Jacksonville
Post Office Box 128
Jacksonville NC 28541
Attention:
Lab ID Sample ID:
23-33106 Site: MW-4
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/ Fax
inf6a environmentalchemists.com
Date of Report: Jul 20, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-13297
Project ID: Monitoring Wells
Collect Date/Time Matrix Sampled by
6/27/2023 11:17 AM Water CV
Test
Method
Results
Date Analyzed
Sulfate
EPA 3000. Rev 2 1, 1993
39 mg/L
06/29/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
1.6 mg/L
06/29/2023
Chloride
SM4500 CI E-2011
63 mg/L
06/29/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 826oD/50308
<0.5 pg/L
06/29/2023
1,1,1-Trichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,1,2,2-Tetrachloroethane
SW B46 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,1,2-Trichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1, 1 -Dich loroethane
SW 846 Method 8260D15036B
<0.5 pg/L
06/29/2023
1,1-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,1-Dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,2, 3-Trichlorobenzene
SW 846 Method 826OD150308
<0.5 pg/L
06/29/2023
1,2,3-Trichloropropane
SW 846 Method 8260D/50308
<0.5 pg/L
06/29/2023
1,2,4-Trichlorobenzene
SW B46Method 8260D160306
<0.5 pg/L
06/29/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260D,503013
<0.5 pg/L
06/29/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260Dt50306
<0.5 pg/L
06/29/2023
1,2-Dibromoethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,2-Dichlorobenzene
SW 646 Method 8260Dt5030B
<0.5 pg/L
06/29/2023
1,2-Dichloroethane
SW 846 Method 8260D,50306
<0.5 pg/L
06/29/2023
1,2-Dichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
1,3,5-Trimethylbenzene
SW 848 Method 8260D/5030B
<0.5 pg/L
06/29/2023
1,3-Dichlorobenzene
SW 846 Method 82600,5030B
<0.5 pg/L
06/29/2023
1, 3-Dichloropropane
SW 846 Method 8260D,,5030B
<0.5 pg/L
06/29/2023
1,4-Dichlorobenzene
SW 846 Method 82501);50306
<0.5 pg/L
06/29/2023
2,2-Dichloropropane
SW 846Method 8260D15030B
<0.5 pg/L
06/29/2023
2-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
4-Chlorotoluene
SW 846 Method 826OD150308
<0.5 pg/L
06/29/2023
Report # 2023-13297 Page 4 of 15

Environmental Chemists, Inc.
envirochem
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-13297
Project ID: Monitoring Wells
Benzene
SW 646 Method B26OD150308
<0 5 µg/L
06/29/2023
Bromobenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
Bromochloromethane
SW 846 Method 8260D15030B
<0 5 µg/L
06/29/2023
Bromodichloromethane
SW 846 Method 826OD15030B
<0 5 µg/L
06/29/2023
Bromoform
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
Bromomethane
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
Carbon tetrachloride
SW 848 Method 826OD15030B
<0.5 µg/L
06/29/2023
Chlorobenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
Chloroethane
SW 646 Method 826OD15030B
<0.5 µg/L
06/29/2023
Chloroform
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
Chloromethane
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
cis-1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
cis-1,3-Dichloropropene
SW 846 Method MOD15030B
<0.5 µg/L
06/29/2023
Dibromochloromethane
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
Dibromomethane
SW 846 Method 8260D15030B
<0.5 µg/L
06/29/2023
Dichlorodifluoromethane
SW 846 Method 8260DIS030B
<0.5 µg/L
06/29/2023
Ethylbenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
Hexachlorobutadiene
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
Isopropylbenzene
SW 846 Method 8260D/5030B
<0.5 µg/L
06/29/2023
M+P Xylene
SW 846 Method 826OD15030B
<1.0 µg/L
06/29/2023
Methylene chloride
SW 846 Method 828OD15030B
<0.5 µg/L
06/29/2023
Naphthalene
SW 846 Method 8260D15030B
<0.5 µg/L
06/29/2023
n-Butylbenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 µg/L
06/29/2023
ortho-Xylene
SW 846 Method MOD15030B
<0.5 µg/L
06/29/2023
p-Isopropyltoluene
SW 646 Method 8260D/5030B
<0.5 µg/L
06/29/2023
sec-Butylbenzene
SW 846 Method 82600/5030B
<0.5 pg/L
06/29/2023
Styrene
SW 846 Method 8260D/5030B
<0.5 µg/L
06/29/2023
tert-Butylbenzene
SW 846 Method 8260D/50308
<0.5 µg/L
06/29/2023
Tetrachloroethene
SW 846 Method BMD150308
<0.5 pg/L
06/29/2023
Report V 2023-13297
Page 5 of 15

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Jul 20, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-13297
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260Df5030B
<0,5 pg/L
06/29/2023
Trans- 1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Trans- 1,3-dichloropropene
SW 846 Method 826OD15030B
<0.5 Ng/L
06/29/2023
Trichloroethene
SW 80 Method 826OD15030B
<0.5 ug/L
06/29/2023
Trichlorofluoromethane
SW 846 Method 826OD15030B
<0.5 Ng/L
06/29/2023
Vinyl chloride
SW 846 Method 826OD/5030B
<0.5 ug/L
06/29/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2, Rev. 2 0, 1993
< 0.02 mg/L
06/28/2023
Nitrate+ Nitrite-N itrogen
EPA 353.2, Rev. 2.0, 1993
< 0.02 mg/L
06/29/2023
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
07/14/2023
Report # 2023-13297 Pape 6 of 15

6en::viroehem]
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255 A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info:a,environ mentalchemists.com
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-13297
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-33107 Site: MW-6
6/27/2023
10:19 AM Water CV
Test
Method
Results
Date Analyzed
Sulfate
EPA 3DO 0, Rev 2 1, 1993
19 mg/L
06/29/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
6.1 mg/L
06/29/2023
Chloride
SM4500 CI E-2011
47 mg/L
06/29/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 8260D,5030B
<0.5 µg/L
06/29/2023
1, 1, 1 -Trichloroethane
SW 846 Method 8260DIS030B
<0.5 µg/L
06/29/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 826OD1503013
<0.5 µg/L
06/29/2023
1,1,2-Trichloroethane
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
1, 1 -Dichloroethane
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
1,1-Dichloroethene
SW 846 Method 826OD1503OB
<0.5 µg/L
06/29/2023
1,1-Dichloropropene
SW 848 Method B26OD15030B
<0.5 µg/L
06/29/2023
1,2,3-Trichlorobenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
1,2,3-Trichloropropane
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
1,2,4-Trichlorobenzene
SW a48 Method 8260D15030B
<0.5 µg/L
06/29/2023
1,2,4-Trimethylbenzene
SW 846 Method 826013,,503013
<0.5 µg/L
06/29/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 826OD,5030B
<0.5 µg/L
06/29/2023
1,2-Dibromoethane
SW 846 Method 82BOD15030B
<0.5 µg/L
06/29/2023
1,2-Dichlorobenzene
SW 846 Method 8260015030E
<0.5 µg/L
06/29/2023
1,2-Dichloroethane
SW 80 Method 826OD15D30B
<0.5 µg/L
06/29/2023
1,2-Dichloropropane
SW 846 Method 826OD15030B
<0.5 µq/L
06/29/2023
1, 3,5-Trimethylbenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
1, 3-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/29/2023
1, 3-Dichloropropane
SW 846 Method 82WD15030B
<0.5 µg/L
06/29/2023
1,4-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 Ng/L
06/29/2023
2,2-Dichloropropane
SW 646 Method 8260D5030B
<0.5 µg/L
06/29/2023
2-Chlorotoluene
SW 646 Method 826OD15030B
<0.5 µg/L
06/29/2023
4-Chlorotoluene
SW $46 Method 826OD15030B
<0.5 µg/L
06/29/2023
Report C 2023-13297 Page 7 of 15

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab,"Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info,a environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Jul 20, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-13297
Project ID: Monitoring Wells
Benzene
SW 846 Method 826OD/5030B
<0.5 pg/L
06/29/2023
Bromobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Bromochloromethane
SW 846 Method 8280D/5030B
<0.5 pg/L
06/29/2023
Bromodichloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Bromoform
SW 846 Method 826013/50308
<0.5 pg/L
06/29/2023
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
06/29/2023
Carbon tetrachloride
sw 846 Method 826CD/5030B
<0.5 pg/L
06/29/2023
Chlorobenzene
SW B46 Method 82BOD/5030B
<0.5 pg/L
06/29/2023
Chloroethane
SW B46 Method 826OD/5030B
<0.5 pg/L
06/29/2023
Chloroform
SW 84e Method 826OD/5030B
<0.5 pg/L
06/29/2023
Chloromethane
SW sae Method 826OD/5030B
<0.5 pg/L
06/29/2023
cis- 1,2-Dichloroethene
SW 846 Method 826OD/5030B
<0.5 pg/L
06/29/2023
cis- 1,3-Dichloropropene
SW 846 Method 82BOD/5030B
<0.5 pg/L
06/29/2023
Dibromochloromethane
SW 846 Method 826OD/5030B
<0.5 pg/L
06/29/2023
Dibromomethane
SW 846 Method 826OD/5030B
<0.5 pg/L
06/29/2023
Dichlorodifluoromethane
SW B46 Method 826013150308
<0.5 pg/L
06/29/2023
Ethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Hexachlorobutadiene
SW 848 Method 826OD15030B
<0.5 pg/L
06/29/2023
Isopropylbenzene
SW 846 Method 82BOD/5030B
<0.5 pg/L
06/29/2023
M+P Xylene
SW B46 Method 826OD15030B
<1.0 pg/L
06/29/2023
Methylene chloride
SW 846 Method 826OD15030B
<0.5 pg/L
06/29/2023
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/29/2023
n-Butylbenzene
SW 846 Method 82BOD15030B
<0.5 pg/L
06/29/2023
n-Propylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
06/29/2023
ortho-Xylene
SW 846 Method 826OD/5030B
<0.5 pg/L
06/29/2023
p-Isopropyltoluene
SW 846 Method 826OD/5030B
<0.5 pg/L
06/29/2023
sec-Butylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
06/29/2023
Styrene
SW 846 Method 82BOD/5030B
<0.5 pg/L
06/29/2023
tert-Butylbenzene
SW 846 Method 626OD/5030B
<0.5 pg/L
06/29/2023
Tetmchioroethene
SW 8" Method 82WU50308
<0.5 pg/L
06/29/2023
Report $t 2023-13297
Page 8 of 15

6e�nvirochem]
ANALYTICAL 8 CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab; Fax
info(a�environmentalchemists.com
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer 1D: 08110015
Attention:
Report #: 2023-13297
Project ID: Monitoring Wells
Toluene
SW 84B Method 8280D/50308
<0.5 pg/L
06/29/2023
Trans-1 ,2-Dichloroethene
SW 846 Method 8280D15030B
<0.5 Wg/L
06/29/2023
Trans-1 ,3-dichloropropene
SW 846 Method 828013/50308
<0.5 ug/L
06/29/2023
Trichloroethene
SW 848 Method 8280D15030B
<0.5 ug/L
06/29/2023
Tdchlorofluoromethane
SW 846 Method 826013/50308
<0.5 ug/L
06/29/2023
Vinyl chloride
SW 846 Method 8280D/5030B
<0.5 ug/L
06/29/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2, Rev 2 0, 1993 0.09 mg/L 06/28/2023
Nitrate+Nitrite-Nitrogen EPA 353.2 Rev 2 0, 1993 0.05 mg/L 06/29/2023
Nitrate Nitrogen Subtraction Method <0.02 mg/L 07/14/2023
teport # 2023-13297
Page 9 of 15

Environmental Chemists, Inc.
envirochem
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab,, Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info -a envtronmentalchemists.com
City of Jacksonville Date of Report: Jul 20, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-13297
Project ID: Monitoring Wells
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
23-33108 Site: MW-7 6/27/2023 10:22 AM Water CV
Test Method Results Date Analyzed
Sulfate
EPA 300.0, Rev. 2.1, 1993
63 mg/L
06/29/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
7.6 mg/L
06/29/2023
Chloride
SM4500 ci E-2011
72 mg/L
06/29/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,1,1-Trichooroethane
SW B46 Method 826oDr5030B
<0 5 pg/L
06/30/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260DI50306
<0.5 pg/L
06/30/2023
1,1,2-Trichloroethane
SW 848 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,1-Dichloroethane
SW 846 Method 82BOD15030B
<0.5 pg/L
06/30/2023
1, 1 -Dichloroethene
SW 846 Method 826OD15030B
<0,5 pg/L
06/30/2023
1,1-Dichloropropene
SW 846 Method 826=6030B
<0.5 pg/L
06/30/2023
1,2,3-Trichlorobenzene
SW 846 Method 8260Df503oB
<0.5 pg/L
06/30/2023
1,2,3-Thchloropropane
SW 646 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,2,4-Trichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,2, 4-Trimethylbenzene
SW 846 Method 826ODY5030B
<0.5 pg/L
06/30/2023
1,2-Dibromo-3-Chloropropane
SW B46 Method 826OU50308
<0,5 pg/L
06/30/2023
1,2-Dibromoethane
SW 846 Method 82601)150308
<0.5 pg/L
06/30/2023
1,2-Dichlorobenzene
SW 846 Method 8260D'5030B
<0.5 pg/L
06/30/2023
1,2-Dichloroethane
SW 846 Method 8260D'5030B
<0.5 pg/L
06/30/2023
1,2-Dichloropropane
SW 846 Method 8260D150308
<0.5 pg/L
06/30/2023
1, 3,5-Trimethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,3-Dichlorobenzene
SW 846 Method 8260DIS030B
<0.5 pg/L
06/30/2023
1,3-Dichloropropane
SW 846 Method 82e0D,5030B
<0.5 pg/L
06/30/2023
1,4-Dichlorobenzene
SW 846 Method 82600f5030B
<0.5 pg/L
06/30/2023
2,2-Dichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
06/30/2023
2-Chlorotoluene
SW 846 Method 826aD!5030B
<0.5 pg/L
06/30/2023
4-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Report it: 2023 13297 Page 10 of 15

Environmental Chemists, Inc.
!Fenvirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info rrenvironmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Jul 20, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-13297
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D15030B
<0.5 µg/L
06/30/2023
Bromobenzene
SW 846 Method 82BOD15030B
<0.5 µg/L
06/30/2023
Bromochloromethane
SW 848 Method 826OD15030B
<0.5 i]g/L
06/30/2023
Bromodichloromethane
SW 846 Method 8280D1503DB
<0.5 µg/L
06/30/2023
Bromoform
SW m6 Method 82600/5030B
<0.5 µg/L
06/30/2023
Bromomethane
sw m6 Method 826OD15030B
<0.5 µg/L
06/30/2023
Carbon tetrachloride
SW 848 Method 828OD15030B
<0.5 µg/L
06/30/2023
Chlorobenzene
sw 846 Method 826DD15030B
<0.5 µg/L
06/30/2023
Chloroethane
SW m6 Method 826OD15030B
<0.5 µg/L
06/30/2023
Chloroform
sw 846 Method 8260D/50308
<0.5 µg/L
06/30/2023
Chloromethane
SW 646 Method 8260D15D30B
<0.5 µg/L
06/30/2023
cis- 1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
cis- 1,3-Dlchloropropene
SW 846 Method 8260DI5030B
<0.5 µg/L
06/30/2023
Dibromochloromethane
SW 846 Method 8260DIW308
<0.5 µg/L
06/30/2023
Dibromomethane
SW 846 Method 8260D15030B
<0.5 µg/L
06/30/2023
Dichlorodifluoromethane
SW 848 Method 8260D15030B
<0.5 µg/L
06/30/2023
Ethylbenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
Hexachlorobutadiene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
Isopropylbenzene
sw 84e Method 8280D15030B
<0.5 µg/L
06/30/2023
M+P Xylene
SW 846 Method 826OD150305
<1.0 µg/L
06/30/2023
Methylene chloride
SW B46 Method 826DD15030B
<0.5 µg/L
06/30/2023
Naphthalene
5W 846 Method 8260D15030B
<0.5 µg/L
06/30/2023
n-Butylbenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
n-Propylbenzene
SW 846 Method 82600/503013
<0.5 µg/L
06/30/2023
ortho-Xylene
SW 846 Method 82600/5030B
<0.5 pg/L
06/30/2023
p-Isopropyltoluene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
sec-Butylbenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
Styrene
sw e46 Method 826DD15030B
<0.5 µg/L
06/30/2023
tert-Butylbenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
Tetrachloroethene
SW M6 McUwod 826ot316030B
<0.5 Pg/L
06/30/2023
Report #: 2023-13297
Page 11 of 15

Environmental Chemists,
Inc.
enviroehe,1�7
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
M
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
infoa environmentalchemists.com
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention,
Report #: 2023-13297
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260D/5030B <0.5 pg/L
06/30/2023
Trans- 1,2-Dichloroethene
SW 646 Method 826OD15030B <0,5 pg/L
06/30/2023
Trans- 1,3-dichloropropene
SW 845 Method 8260D/5030B <0.5 pg/L
06/30/2023
Trichloroethene
SW 846 Method 8260D/5030B <0.5 pg/L
06/30/2023
Trichlorofluoromethane
SW 846 Method 8260D/5030B <0.5 pg/L
06/30/2023
Vinyl chloride
SW 846 Method 8260D/5030B <0.5 pg/L
06/30/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353 2 Rev 2.0, 1903 < 0.02 mg/L
06/28/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev 2 0, 1993 < 0.02 mg/L
06/29/2023
Nitrate Nitrogen
Subtraction Method <0.02 mg/L
07/14/2023
Report # 2023-13297 Page 12 of 15

Environmental Chemists, Inc.
envirochem
ANALYTICAL 8 CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(« environmentalchemists.com
City of Jacksonville Date of Report: Jul 20, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-13297
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-33109 Site: MW-12 6/27/2023 10:02 AM Water CV
Test Method Results Date Analyzed
Sulfate
EPA 300.0, Rev 2.1, 1993
9 mg/L
06/29/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
27.0 mg/L
06/29/2023
Chloride
SM4500 CI E-2011
13 mg/L
06/29/2023
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0,5 pg/L
06/30/2023
1, 1,1 -Trichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,1,2,2-Tetrachloroethane
SW sae Method 826OD15030B
<0,5 pg/L
06/30/2023
1,1,2-Trichloroethane
SW 846 Method 826oD15030B
<0.5 pg/L
06/30/2023
1,1-Dichloroethane
SW 846 Method 8280D 5030E
<0.5 pg/L
06/30/2023
1,1-Dichloroethene
SW 646 Method 826OD15030B
<0,5 pg/L
06/30/2023
1,1-Dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,2,3-Trichlorobenzene
SW 846 Method 826OD150308
<0.5 pg/L
06/30/2023
1,2, 3-Trichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,2,4-Trichlorobenzene
SW 646 Method 826oD15030B
<0.5 pg/L
06/30/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260D,5030B
<0.5 pg/L
06/30/2023
1,2-Dibromo-3-Chloropropane
SW a46 Method 8280D,5030B
<0.5 pg/L
06/30/2023
1, 2-Dibromoethane
SW 8" Method 826OD15030B
<0_5 pg/L
06/30/2023
1,2-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,2-Dichloroethane
SW 848 Method 8260D150308
<0.5 pg/L
06/30/2023
1,2-Dichloropropane
SW 846 Method 8260D,50308
<0.5 pg/L
06/30/2023
1,3,5-Trimethylbenzene
SW 846 Method 62BOD150300
<0.5 pg/L
06/30/2023
1,3-Dichlorobenzene
SW 8" Method 826OD15030B
<0.5 pg/L
06/30/2023
1,3-Dichloropropane
SW B48Method 826OD15030B
<0.5 pg/L
06/30/2023
1,4-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
2,2-Dichloropropane
SW 846 Method 8280D15030B
<0.5 pg/L
06/30/2023
2-Chlorotoluene
SW 846 Method 8260D5030B
<0.5 pg/L
06/30/2023
4-Chlorotoluene
SW 848 Method 826OD15030B
<0.5 pg/L
06/30/2023
Report p 2023-13297 Page 13 of 15

Cen7virochlem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab,, Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab; Fax
infoia environmentalchemismcom
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-13297
Project ID: Monitoring Wells
Benzene
SW 646 Method 826OD15030B
<0.5 µg/L
06/30/2023
Bromobenzene
sw 846 Method 82WD15030B
<0.5 µg/L
06/30/2023
Bromochloromethane
SW 646 Method 826001503DB
<0.5 µg/L
06/30/2023
Bromodichloromethane
SW W Method 8260D15030B
<0.5 µg/L
06/30/2023
Bromoform
SW 846 Method 82WD15030B
<0.5 µg/L
06/30/2023
Bromomethane
SW 848 Method 826013/503013
<0.5 µg/L
06/30/2023
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0,5 µg/L
06/30/2023
Chlorobenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
Chloroethane
SW 646 Method 8260D/50308
<0.5 µg/L
06/30/2023
Chloroform
SW 846 Method eMD15030B
<Q.5 µg/L
06/30/2023
Chloromethane
SW B46 Method 8280D�50308
<0.5 µg/L
06/30/2023
cis-1,2-Dichloroethene
SW 846 Method 82600,50306
<0.5 µg/L
06/30/2023
cis-1 ,3-Dichloropropene
SW 846 Method 826CD,50306
<0.5 µg/L
06/30/2023
Dibromochloromethane
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
Dibromomethane
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
Dichlorodifluoromethane
sw 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
Ethylbenzene
SW 848 Method 82601)r50306
<0.5 µg/L
06/30/2023
Hexachlorobutadiene
SW 848 Method 8260D5030B
<0.5 µg/L
06/30/2023
Isopropylbenzene
SW 846 Method 82BOD15030B
<0.5 µg/L
06/30/2023
M+P Xylene
SW 846 Method 826OD15030B
<1.0 µg/L
06/30/2023
Methylene chloride
SW 846 Method 82WO15030B
<0.5 µg/L
06/30/2023
Naphthalene
SW 846 Method 82600/5030B
<0.5 µg/L
06/30/2023
n-Butylbenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
n-Propylbenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
ortho-Xylene
SW B48 Method 82600.5030E
<0.5 µg/L
06/30/2023
p-Isopropyltoluene
SW 846 Method 82600f5030B
<0.5 µg/L
06/30/2023
sec-Butylbenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
Styrene
SW 848 Method 8260D15030B
<0.5 pg/L
06/30/2023
tert-Butylbenzene
SW 848 Method 8260D/5030s
<0.5 µg/L
06/30/2023
Tetrachloroethene
sw 80 Method 8268016OWB
<0.5 µg/L
06/30/2023
Report#' 2023-13297
Page 14 of 15

Environmental Chemists, Inc.
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252,473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention-
Report #: 2023-13297
Project ID: Monitoring Wells
Toluene
sw 848 Method 82BOD15030B
<0.5 Ng/L
06/30/2023
Trans-1 ,2-Dichloroethene
SW W Method 826OD15030B
<0.5 Ng/L
06/30/2023
Trans-1,3-dichloropropene
SW 846 Method 826OD15030B
<0.5 ug/L
06/30/2023
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/30/2023
Trichlorofluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Vinyl chloride
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2, Rev 2A 1993 0.09 mg/L 06/28/2023
N itrate+ N itrite-N itrogen EPA 363 2, Rev 2 0, 1993 0.06 mg/L 06/29/2023
Nitrate Nitrogen Subtraction Method <0.02 mg/L 07/14/2023
Comment:
Reviewed by:
Report P 2023-13297 Page 15 of 15

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill W,
Wilmington, NC 284{
Sample Receipt Checklist 910 392 022
Clien M C(Cjrj U �-- Q,
Date: eport Number:
RC01L,P` of slrnp!�.
❑ vES ❑ Iti 0
❑ YES ❑ NO
Origina! temperature upon
How temperature taken:
IR Gun, 10: Thomas Traceabl
ECHEFvS pmdc '.
N/A
receipt
i. �Vv,custody seals present on the cooler? C�.. Li
7 1 _..--
u34,uuy sears were present, were they inta
;C Corrected temoerati,rR i in.
❑ Tempera_.` B'an
M Against Bottle;
broken?
n rece
YES
c -J/ iv c,LU0006bJ c: O
IR Gun Correction Facto .Q
❑ NO
YES
O NO
�3. IF temperature of cooVC. exceeded C, was Project Mgr./QA notified?
4.
[$� YES
❑ NO
Were proper custody procedures (relinquished/received) followed?
YES
5. Were sample ID's listed on the COC?
YES
❑ NO
❑
6. Were samples ID's listed on sample containers?
YES
NO
❑
7. Were collection date and time listed on the COC?
�l YES
NO
❑
8. Were tests to be performed listed on the COC?
YES
NO
❑
9. Did samples arrive in proper containers for each test?
YES
NO
❑
10. Did samples arrive in good condition for each test?
YES
NO
❑
11, Was adequate sample volume available?'
YES
NO
❑ NO
12. Were samples received within proper holding time for requested tests?
13. Were acid preserved
❑ YES
❑ NO
samples received at a pH of <2?
14. Were cyanide samples
❑ YES
❑
❑ NO
received at a pH >12?
15. Were sulfide samples received at a pH >9?
YES
❑ YES
❑ NO
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <05 m/i % X'
❑ YES
❑ NO
17, Were Sulfide/Cyanide received at a chlorine residual of <0.5 M/L?
18. Were orthophosphate samples filtered in the field within 1S minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of ana,ysls and recorded on the benchshr,
Sample Preservation: (Must be completed for any samples) incorrect)
Samples) y preserved or with headspace)
by add'ng (circle one): H250,
were received incorrectly preserved and were adjusted accordingly
HNO3 HCI NaOH
Vote: tio_ fy Cllit
Time preservation: If more than one preservative is needed, notate in comments below
C7'n2' serr Ce : -nrrled r �
a.e y for �ncorrect•y preserved ,a np'es. Obta'r a new sample or
not ry the state lab if d'rected to a-a.yzed by the customer. Wrio was notified, date and time:
Volables Sampfe(s)
were received with headspace
COMMENTS:
DOC. 5.002 Rev 2
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envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab;' Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/ Fax
info a1environmen talchemists.com
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-13417
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-33408 Site: MW-1
6/28/2023
10:29 AM Water NB
Test
Method
Results Date Analyzed
Sulfate
EPA 300.0, Rev. 2.1, 1993
15 mg/L
06/29/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
14.5 mg/L
06/29/2023
Chloride
SW600 CI E-2011
45 mg/L
06/30/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 82e0D/5030B
<0.5 µg/L
06/30/2023
1, 1, 1 -Trichloroethane
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260015030B
<0.5 µg/L
06/30/2023
1,1,2-Trichloroethane
SW 846 Method 826OD16030B
<0.5 µg/L
06/30/2023
1,1-Dichloroethane
SW 846 Method 8260D15030B
<0.5 µg/L
06/30/2023
1,1-Dichloroethene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
1, 1 -Dich loropropene
SW 846 Method 826OD16030B
<0.5 pg/L
06/30/2023
1,2,3-Trichlorobenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
1,2,3-Trichloropropane
SW 946 Method 826OD150308
<0.5 µg/L
06/30/2023
1,2,4-Trlchlorobenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
1,2,4-Trimethylbenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 82s0D15030B
<0.5 µg/L
06/30/2023
1,2-Dibromoethane
SW 846 Method 8260015030E
<0.5 pg/L
06/30/2023
1,2-Dichlorobenzene
SW 646 Method 826OD15030B
<0.5 µg/L
06/30/2023
1,2-Dichloroethane
SW W Method 8260D/5030B
<0.5 µg/L
06/30/2023
1,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 µg/L
06/30/2023
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 µg/L
06/30/2023
1, 3-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
1, 3-Dichloropropane
SW 846 Method B26OD15030B
<0.5 µg/L
06/30/2023
1,4-Dichlorobenzene
SW 846 Method 8260131503013
<0.5 µg/L
06/30/2023
2,2-Dichloropropane
SW 846 Method 8260D15030B
<0.5 µg/L
06/30/2023
2-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 µg1L
06/30/2023
4-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
Report #- 2023-13417
Page 1 of 18

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 LabJFax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab! Fax
info—, environmentalchemists.com
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer 1D: 08110015
Attention:
Report #: 2023-13417
Project ID: Monitoring Wells
Benzene
SW 846 Method 8280D/5030B
<0.5 pg/L
06/30/2023
Bromobenzene
SW B46 Method 826OD15030B
<0.5 pg/L
06/30/2023
Bromochloromethane
SW 848 Method 8260D/5030B
<0.5 pg/L
06/30/2023
Bromodichloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Bromoform
SW 846 Method 8260150306
<0.5 pg/L
06/30/2023
Bromomethane
SW 846 Method 8260D15030B
<0.5 pg/L
06/30/2023
Carbon tetrachloride
SW 846 Method 826OD150308
<0.5 pg/L
06/30/2023
Chlorobenzene
SW 846 Method 8280015030B
<0.5 pg/L
06/30/2023
Chloroethane
SW 845 Method 8260D/5030B
<0.5 pg/L
06/30/2023
Chloroform
SW 846 Method 826oD/5030B
<0.5 pg/L
06/30/2023
Chloromethane
SW 846 Method 82BOD15030B
<0.5 pg/L
06/30/2023
cis-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/30/2023
cis-1, 3-Dichloropropene
SW 846 Method 82601)/5030B
<0.5 pg/L
06/30/2023
Dibromochloromethane
SW a48 Method 8260D'5030B
<0.5 pg/L
06/30/2023
Dtbromomethane
SW 846 Method 8260D5030B
<0.5 pg/L
06/30/2023
Dichlorodifluoromethane
SW 846 Method 8260D,5030B
<0.5 pg/L
06/30/2023
Ethylbenzene
SW 846 Method 8260D.,50305
<0.5 pg/L
06/30/2023
Hexachlorobutadiene
SW 846 Method 8260Di5030B
<0.5 pg/L
06/30/2023
lsopropylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
06/30/2023
Methylene chloride
SW 846 Method 826DD15030B
<0.5 pg/L
06/30/2023
Naphthalene
SW 846 Method 8260D/50308
<0.5 pg/L
06/30/2023
n-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
n-Propylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/30/2023
p-Isopropyltoluene
SW 80 Method 82600/503013
<0.5 pg/L
06/30/2023
sec-Butylbenzene
SW 846 Method 82600150308
<0.5 pg/L
06/30/2023
Styrene
SW 80 Method 8260D16030B
<0.5 pg/L
06/30/2023
tert-Butylbenzene
SW 846 Method 8260Dt5030B
<0.5 pg/L
06/30/2023
Tetrachloroethene
SVV 846 metmd 82WD,'50108
<0.5 pg/L
06/30/2023
Report #- 2023-1341 r
Page 2 of 18

Environmental Chemists,
Inc.
,,,•nvirochem6602
Windmill Way, Wilmington, NC 28405 . 910,392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
mfoi:i environmentalchemists.com
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-13417
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260DI50308 <0.5 pg/L
06/30/2023
Trans- 1,2-Dichloroethene
SW 846 Method 8260DIS0308 <0.5 pg/L
06/30/2023
Trans-1,3-dichloropropene
SW 846 Method 826OD150303 <0.5 pg/L
06/30/2023
Tdchloroethene
SW 846 Method 826013r503013 <0.5 pg/L
06/30/2023
Trichlorofluoromethane
SW 846 Method 8260131503013 <0.5 pg/L
06/30/2023
Vinyl chloride
SW 846 Method 828oD15030B <0.5 pg/L
06/30/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2 0. 1993 < 0.02 mg/L
06/28/2023
Nitrate+Nitrite-Nitrogen
EPA353.2, Rev 2.0. 1993 < 0.02 mg/L
06/29/2023
Nitrate Nitrogen
Subtraction Method <0.02 mg/L
07/14/2023
Report # 2023-13417 Page 3 of 18

Zen7viroehe]m
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347,5843 Lab/ Fax
infoi,r environmentalchemists.com
City of Jacksonville Date of Report: Jul 20, 2023
Post Office Box 128 Customer PO M
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-13417
Project ID: Monitoring Wells
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
23-33409 Site: MW-2 6/28/2023 11:33 AM Water NB
Test Method Results Date Analyzed
Sulfate
EPA 300.0, Rev. 2.1, 1993
10 mg/L
06/29/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
13.0 mg/L
06/29/2023
Chloride
SM4500 C1 E-2011
115 mg/L
06/30/2023
1,1,1,2-Tetrachloroethane
SW 848 Method 8260D/5030B
<0.5 pg/L
06/30/2023
1, 1, 1 -Trichloroethane
SW 846 Method MOD15030B
<0.5 pg/L
06/30/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 626ODY5030B
<0.5 pg/L
06/30/2023
1,1,2-Trichloroethane
SW 846 Method 826OD150308
<0.5 pg/L
06/30/2023
1,1-D ich loroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,1-Dichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
06/30/2023
1,1-Dichloropropene
SW 848 Method 826OD150308
<0.5 pg/L
06/30/2023
1, 2, 3-Trich lorobenzene
sW 846 Method B26OD150308
<0.5 pg/L
06/30/2023
1,2,3-Trichloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,2,4-Trichlorobenzene
SW 846 Method 82BOD15030B
<0.5 pg/L
06/30/2023
1,2,4-Trimethylbenzene
SW 846 Method 82600150308
<0.5 pg/L
06/30/2023
1,2-Dlbromo-3-Chloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,2-Dibromoethane
SW 846 Method 8260D150308
<0.5 pg/L
06/30/2023
1,2-Dichlorobenzene
SW W Method 826013/50308
<0.5 pg/L
06/30/2023
1, 2-Dichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,2-Dichloropropane
SW 846 Method 826oD150308
<0.5 pg/L
06/30/2023
1, 3, 5-Trimethylbenzene
SW 646 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,3-Dichlorobenzene
SW 840 Method 82601)150306
<0.5 pg/L
06/30/2023
1,3-Dichloropropane
SW W Method 826OD15030B
<0.5 pg/L
06/30/2023
1,4-Dichlorobenzene
SW W Method 8260D/5030B
<0.5 pg/L
06/30/2023
2,2-Dichloropropane
SW 846 Method 8260015030E
<0.5 pg/L
06/30/2023
2-Chlorotoluene
SW 8" Method 826OD15030B
<0.5 pg/L
06/30/2023
4-Chlorotoluene
SW B46 Method 826OD15030B
<0.5 pg/L
06/30/2023
Report p 2023-1341' Page 4 of 18

Environmental Chemists, Inc.
envirochem
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Labr'Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab,, Fax
[e-mail]
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO M
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report M 2023-13417
Project ID: Monitoring Wells
Benzene
SW 848 Method 8260D/5030B
<0.5 pg/L
06/30/2023
Bromobenzene
SW 846 Method 8260015030E
<0.5 pg/L
06/30/2023
Bromochloromethane
SW 846 Method 8260DIS0308
<0.5 pg/L
06/30/2023
Bromodichloromethane
SW 846 Method 82BOD150308
<0.5 pg/L
06/30/2023
Bromoform
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Bromomethane
SW 846 Method 826OD/5030B
<0.5 pg/L
06/30/2023
Carbon tetrachloride
SW 846 Method 826OD/5030B
<0.5 pg/L
06/30/2023
Chlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
06/30/2023
Chloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Chloroform
SW 846 Method 8260D15030B
<0.5 pg/L
06/30/2023
Chloromethane
SW Me Method 826OD15030B
<0.5 pg/L
06/30/2023
cis- 1,2-Dichloroethene
SW 846 Method 8260D+5030B
<0.5 pg/L
06/30/2023
cis-1,3-Dichloropropene
SW846Method 826OD/5030B
<0.5 pg/L
06/30/2023
Dibromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Dibromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Dichlorodifluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Ethylbenzene
SW 846 Method 82600/5030B
<0.5 pg/L
06/30/2023
Hexachlorobutadiene
SW 846 Method 826OD150308
<0.5 pg/L
06/30/2023
Isopropylbenzene
SW 846 Method BMD15030B
<0.5 pg/L
06/30/2023
M+P Xylene
SW 846 Method 826OD15030B
<1.0 pg/L
06/30/2023
Methylene chloride
SW 848 Method 825OD15030B
<0.5 pg/L
06/30/2023
Naphthalene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
n-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
n-Propylbenzene
SW 846 Method 826OD150308
<0.5 pg/L
06/30/2023
ortho-Xylene
SW 846 Method 826OD/5030B
<0.5 pg/L
06/30/2023
p-Isopropyltoluene
SW 846 Method 82BOD15030B
<0.5 pg/L
06/30/2023
sec-Butylbenzene
SW B45 Method 82BOD15030B
<0.5 pg/L
06/30/2023
Styrene
SW 846 Method 826DD15030B
<0.5 pg/L
06/30/2023
tert-Butylbenzene
SW 846 Method 8280D/5030B
<0.5 pg/L
06/30/2023
Tetrachioroethene
SW 840 McVW 8260DPMOS
<0.5 pg/L
06/30/2023
Report # 2023-13417
Page 5 of i8

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Jul 20, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-13417
Project ID: Monitoring Wells
Toluene
SW 846 Method 8260D/50308
<0.5 µg/L
06/30/2023
Trans- 1,2-Dichloroethene
SW 646 Method 826OD15030B
<Q.5 µg/L
06/30/2023
Trans- 1,3-dichloropropene
SW 846 Method 8260D/5030B
<0.5 µg/L
06/30/2023
Trichloroethene
SW 848 Method 826OD150308
<0.5 µg/L
06/30/2023
Trichlorofluoro methane
SW 846 Method 8260D/5030B
<0.5 µg/L
06/30/2023
Vinyl chloride
SW 846 Method 8260M50306
<0.5 µg/L
06/30/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 3532, Rev 2 0 1993
0.04 mg/L
06/28/2023
Nitrate+Nitrite-Nitrogen
EPA 353 2, Rev 2 0 1993
0.07 mg/L
06/29/2023
Nitrate Nitrogen
SubtraOnn Method
0.03 mg/L
07/14/2023
Report ft 2023.13417 Page 6 of 18

F00,07 "I Environmental Chemists, Inc.
envirochem A 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax
'.0 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
City of Jacksonville
Post Office Box 128
Jacksonville NC 28541
Attention:
Date of Report: Jul 20, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-13417
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect DateITime Matrix Sampled by
23-33410 Site: MW-11
6/28/2023
10:18 AM Water NB
Test
Method
Results
Date Analyzed
Sulfate
EPA 300 0, Rev 2 1, 1993
<5 mg/L
06/29/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
<0.5 mg/L
06/29/2023
Chloride
SM4500 C1 E-2011
80 mg/L
06/30/2023
1.1,1,2-Tetrachloroethane
sw 846 Method 82e0D,5030B
<0.5 µg/L
06/30/2023
1, 1, 1 -Trichloroethane
SW 846 Method 8260D/5030B
<0.5 µg/L
06/30/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 µg/L
06/30/2023
1,1,2-Trichloroethane
SW 846 Method 8260D15030B
<0.5 µg/L
06/30/2023
1,1-Dichloroethane
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
1,1-Dichloroethene
SW 846 Method 8260D1503013
<0.5 µg/L
06/30/2023
1,1-Dichloropropene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
1,2,3-Trichlorobenzene
SW 846 Method 02600150306
<0.5 µg/L
06/30/2023
1,2,3-Trichioropropane
SW 846 Method 82BOD15030B
<0.5 µg/L
06/30/2023
1,2,4-Trichlorobenzene
SW 846 Method 8280D15030B
<0.5 pg/L
06/30/2023
1,2,4-Trimethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,2-Dibromo-3-Chloropropane
SW 848 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,2-Dibromoethane
SW 848 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,2-Dichlorobenzene
SW 846 Method 8260D15030B
<0.5 µg/L
06/30/2023
1,2-Dichloroethane
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
1,2-Dichloropropane
SW 846 Method 826OD/5030B
<0.5 µg/L
06/30/2023
1,3,5-Trimethylbenzene
sw 846 Method 8260D/50308
<0.5 µg/L
06/30/2023
1, 3-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
1, 3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 µg/L
06/30/2023
1,4-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
2, 2-Dichloropropane
SW 846 Method 826oD/5030B
<0.5 µg/L
06/30/2023
2-Chlorotoluene
SW M Method 826OD15030B
<0.5 µg/L
06/30/2023
4-Chlorotoluene
sw W Method 9280D/50308
<0.5 pg/L
06/30/2023
Report P: 2023-13417
Page 7 of 18

F"W�' -- -77
envirochem
ANALYTICAL & CONSULTING CHEMISTS
City of Jacksonville
Post Office Box 128
Jacksonville NC 28541
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab, Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab, Fax
info a environmentalchemists.com
Date of Report: Jul 20, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-13417
Project ID: Monitoring Wells
Benzene
SW a46 Method 82600150308
<0.5 pg/L
06/30/2023
Bromobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
06/30/2023
Bromochloromethane
SW 846 Method 8260DI5030B
<0.5 pg/L
06/30/2023
Bromodichloromethane
SW Me Method 8260D15030B
<0.5 pg/L
06/30/2023
Bromoform
SW 846 Method 8260D15030B
<0.5 pg/L
06/30/2023
Bromomethane
SW 846 Method 8260015030B
<0.5 pg/L
06/30/2023
Carbon tetrachloride
SW 80 Method 8260DIS030B
<0.5 pg/L
06/30/2023
Chlorobenzene
SW 846 Method 82s0D15030B
<0.5 pg/L
06/30/2023
Chloroethane
SW B48 Method 8MD150308
<0.5 pg/L
06/30/2023
Chloroform
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Chloromethane
sw 846 Method 828oDr5030B
<0.5 pg/L
06/30/2023
cis- 1.2-Dlchloroethene
SW B46 Method 826OD15030B
<0.5 pg/L
06/30/2023
cis-1,3-Dichloropropene
SW 845 Method 82e0D15030B
<0.5 pg/L
06/30/2023
Dibromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Dibromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Dichlorodifluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Ethylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
06/30/2023
Hexachlorobutadiene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Isopropylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
M+P Xylene
SW 646 Method 826OD15030B
<1.0 pg/L
06/30/2023
Methylene chloride
SW 846 Method 8260D150306
<0.5 pg/L
06/30/2023
Naphthalene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
n-Butylbenzene
SW 846 Method 82BOD15030B
<0.5 pg/L
06/30/2023
n-Propylbenzene
SW W Method 8260015030E
<0.5 pg/L
06/30/2023
ortho-Xylene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
p4sopropyltoluene
SW 848 Method 826OD15030B
<0.5 pg/L
06/30/2023
sec-Butylbenzene
SW 846 Method 82BOD15030B
<0.5 pg/L
06/30/2023
Styrene
SW 846 Method 8260D/50306
<0.5 pg/L
06/30/2023
tert-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Tetrachloroethene
s^t so Method 8260ot0308
<0.5 pg/L
06/30/2023
Report it 2023-13417
Page 8 of 18

F"P� -- 71 Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab;'Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab!Fax
ANALYTICAL & CONSULTING CHEMISTS info&nvironmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Jul 20, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-13417
Project ID: Monitoring Wells
Toluene
SW 846 Method 826OD15030B
<0,5 pg/L
06/30/2023
Trans- 1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pglL
06/30/2023
Trans- 1,3-dichloropropene
SW 646 Method 826OD15030B
<0.5 pg/L
06/30/2023
Tdchloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
06/30/2023
Trichlorofluoromethane
SW 846 Method 8260D15030B
<0.5 pg/L
06/30/2023
Vinyl chloride
SW 846 Method 8260D15030B
<0.5 pg/L
06/30/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
< 0.02 mg/L
06/28/2023
Nitrate+ N itrite-Nitrogen
EPA 353.2, Rev. 2.0. 1993
0.42 mg/L
06/29/2023
Nitrate Nitrogen
Subtraction Method
0.42 mg/L
07/14/2023
Report tk 2023.13417 Page 9 of 18

Environmental Chemists, Inc.
envirochem
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab;' Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab; Fax
info,a envtronmentalchemists.com
City of Jacksonville Date of Report: Jul 20, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-13417
Project ID: Monitoring Wells
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
23-33411 Site: MW-15 6/28/2023 11:12 AM Water NB
Test Method Results Date Analyzed
Sulfate
EPA 300.0, Rev. 2.1. 1993
<5 mg/L
06/29/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
1.2 mg/L
06/29/2023
Chloride
SM4500 CI E-2011
46 mg/L
06/30/2023
1.1,1,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1, 1, 1-Trichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 826OD150308
<0.5 pg/L
06/30/2023
1,1,2-T6chloroethane
SW 846 Method 8260D 5030E
<0.5 pg/L
06/30/2023
1,1-Dichloroethane
SW 846 Method 8260D 5030E
<0.5 pg/L
06/30/2023
1, 1 -Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,1-Dichloropropene
SW 846 Method 8260D15030B
<0.5 pg/L
06/30/2023
1,2,3-Trichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
06/30/2023
1, 2, 3-Tiichooropropane
sw 846 Method 8260D15030B
<0.5 pg/L
06/30/2023
1,2,4-Trichlorobenzene
SW 846 Method 626OD15030B
<0.5 pg/L
06/30/2023
1,2.4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/30/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method BMD15030B
<0.5 pg/L
06/30/2023
1, 2-Dibromoethane
SW 846 Method 8260D15030B
<0.5 pg/L
06/30/2023
1,2-Dichlorobenzene
SW 846 Method 8260015030B
<0.5 pg/L
06/30/2023
1,2-Dichloroethane
SW 846 Method MOD15030B
<0.5 pg/L
06/30/2023
1,2-Dichloropropane
SW 846 Method 826OD15030B
<0_5 pg/L
06/30/2023
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/30/2023
1. 3-Dichlorobenzene
SW 846 Method 82BOD15030B
<0.5 pg/L
06/30/2023
1,3-Dichloropropane
SW 846 Method 82600/5030B
<0.5 pg/L
06/30/2023
1,4-Dichlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
06/30/2023
2,2-Dichloropropane
SW 846 Method 8280D/5030B
<0.5 pg/L
06/30/2023
2-Chlorotoluene
SW 848 Method 8260D/5030B
<0.5 pg/L
06/30/2023
4-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Report # 2023-13417 Page 10 of 18

[en7virochem]
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392,4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab;"Fax
[e-mail]
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-13417
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260015D308
<0.5 µg/L
06/30/2023
Bromobenzene
SW 848 Method 8260D15030B
<0.5 pg/L
06/30/2023
Bromochloromethane
SW B46 Method 8260D15030B
<0.5 pg/L
06/30/2023
Bromodichloromethane
SW 846 Method 826OD1503013
<0.5 µg/L
06/30/2023
Bromoform
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
Bromomethane
SW 846 Method 82BOD/5030B
<0.5 µg/L
06/30/2023
Carbon tetrachloride
SW 846 Method 82BOD15030B
<0.5 tag/L
06/30/2023
Chlorobenzene
SW 646 Method 826ODM30B
<0.5 µg/L
06/30/2023
Chloroethane
SW 646 Method 82BOD150308
<0.5 µg/L
06/30/2023
Chloroform
SW 846 Method B26OD15030B
<0.5 pg/L
06/30/2023
Chloromethane
SW M6 Method 826OD15030B
<0.5 lag/L
06/30/2023
cis- 1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
cis-1, 3-Dichloropropene
SW B46 Method 826OD150308
<0.5 µg/L
06/30/2023
Dibromochloromethane
SW 846 Method 8260015030E
<0.5 pg/L
06/30/2023
Dibromomethane
SW 846 Method 82SOD15030B
<0.5 pg/L
06/30/2023
Dichlorodifluoromethane
SW W Method 8260DIS0308
<0.5 µg/L
06/30/2023
Ethylbenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
Hexachlorobutadiene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
Isopropylbenzene
SW 846 Method 828OD15030B
<0.5 µg/L
06/30/2023
M+P Xylene
SW 846 Method 826OD15030B
<1.0 Ng/L
06/30/2023
Methylene chloride
SW 846 Method 8260D15030B
<0.5 µg/L
06/30/2023
Naphthalene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
n-Butylbenzene
SW 848 Method 8260015030E
<0.5 pg/L
06/30/2023
n-Propylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
ortho-Xylene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
p-Isopropyltoluene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
sec-Butylbenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
Styrene
SW 846 Method 8MD15030B
<0.5 µg/L
06/30/2023
tert-Butylbenzene
SW 846 Method B260D15030B
<0.5 pg/L
06/30/2023
Tetrachloroethene
SWMeMethod 82BDD/SMOB
<0.5 µg/L
06/30/2023
Report d 2023-13417
Page 11 of 18

renvirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-13417
Project ID: Monitoring Wells
Toluene
SW 846 Method 826OD160308
<0.5 pg/L
06/30/2023
Trans-1,2-Dichloroethene
SW 846 Method 8260D/50308
<0.5 pg/L
06/30/2023
Trans-1,3-dichloropropene
SW 846 Method 8260D150308
<0.5 pg/L
06/30/2023
Trichloroethene
SW 846 Method 82600/60308
<0.5 pg/L
06/30/2023
Trichlorofluoromethane
SW 846 Method 8260D/50308
<0.5 pg/L
06/30/2023
Vinyl chloride
SW 846 Method 8260D150308
<0.5 pg/L
06/30/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen EPA 353.2. Rev. 2 0, 1993 < 0.02 mg/L 06/28/2023
Nitrate+Nitrite-Nitrogen EPA 353.2. Rev, 2 0,1993 1.36 mg/L 06/29/2023
Nitrate Nitrogen Subtraction Method 1, 36 mg/L 07/14/2023
Report 9 2023-13417 Page 12 of 18

Environmental Chemists,
Inc.
envirochem6602
Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/flax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
ANALYTICAL 8 CONSULTING CHEMISTS
[e-mail]
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention:
Report #: 2023-13417
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
23-33412 Site: MW-16
6/28/2023
9:22 AM Water NB
Test
Method
Results Date Analyzed
Sulfate
EPA 300.0, Rev 2 1, 1993
9 mg/L
06/29/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
1.7 mg/L
06/29/2023
Chloride
SM4501) ci E-2011
38 mg/L
06/30/2023
1,1,1, 2-Tetrach loroethane
SW 846 Method 8260015030E
<0.5 µg/L
06/30/2023
1,1,1-Tiichloroethane
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
1,1,2,2-Tetrachloroethane
SW Safi Method 8260D150308
<0.5 µg/L
06/30/2023
1,1 2-Trichooroethane
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
1,1-Dichloroethane
SW U6 Method 8280D/5030B
<0.5 µg/L
06/30/2023
1, 1 -Dichloroethene
SW 846 Method 82BOD15030B
<0.5 µg/L
06/30/2023
1, 1 -Dichloropropene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
1,2,3-Trichlorobenzene
SW 846 Method 82601)/5030B
<0.5 µg/L
06/30/2023
1,2,3-Trichooropropane
SW 8" Method 8MD1503013
<0.5 µg/L
06/30/2023
1,2,4-Trichlorobenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
1,2,4-Trimethylbenzene
SW 846 Method 8260D150013
<0.5 µg/L
06/30/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 826oD/5030B
<0.5 µg/L
06/30/2023
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 µg/L
06/30/2023
1,2-Dichlorobenzene
SW 046 Method 8MD15030B
<0.5 µg/L
06/30/2023
1,2-Dichloroethane
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
1,2-Dichloropropane
SW 846 Method 8260015030E
<0.5 µg/L
06/30/2023
1,3,5-Trimethylbenzene
SW 846 Method M0015030B
<0.5 µg/L
06/30/2023
1,3-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 µg/L
06/30/2023
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 µg/L
06/30/2023
1,4-Dichlorobenzene
SW 848 Method 82SOD15030B
<0.5 µg/L
06/30/2023
2,2-Dichloropropane
SW 846 Method 82601)/50308
<0.5 µg/L
06/30/2023
2-Chlorotoluene
SW 846 Method 82WD/5030B
<0.5 µg/L
06/30/2023
4-Chlorotoluene
SW 846 Method 8250DI5030B
<0.5 µg/L
06/30/2023
Report # 2023-13417 Page 13 of 18

[en7-och7]iirr
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910 392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab,,` Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab;'Fax
[e-mail]
City of Jacksonville Date of Report: Jul 20, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-13417
Project ID: Monitoring Wells
Benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/30/2023
Bromobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
06/30/2023
Bromodichloromethane
SW W Method 826OD15030B
<0.5 pg/L
06/30/2023
Bromoform
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Bromomethane
SW 846 Method 826OD150308
<0.5 pg/L
06/30/2023
Carbon tetrachloride
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Chlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Chloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
06/30/2023
Chloroform
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Chloromethane
SW 846 Method 626OD150308
<0.5 pg/L
06/30/2023
cis-1,2-Dichloroethene
SW Me Method 8280D150308
<0.5 pg/L
06/30/2023
cis-1,3-Dichloropropene
SW 646 Method 826GD15030B
<0.5 pg/L
06/30/2023
Dibromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Dibromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Dichlorodifluoromethane
SW 846 Method 826OD1503DB
<0.5 pg/L
06/30/2023
Ethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/30/2023
Hexachlorobutadiene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Isopropylbenzene
SW 846 Method 82SOD15030B
<0.5 pg/L
06/30/2023
M+P Xylene
SW 846 Method 826oD/5030B
<1.0 pg/L
06/30/2023
Methylene chloride
SW B46 Method 826oD/5030B
<0.5 pg/L
06/30/2023
Naphthalene
SW B46 Method MOD15030B
<0.5 pg/L
06/30/2023
n-Butylbenzene
SW 846 Method 826OD150308
<0.5 pg/L
06/30/2023
n-Propylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
ortho-Xylene
sw 846 Method 826oD/5030B
<0.5 pg/L
06/30/2023
p-Isopropyltoluene
SW 848 Method 8260D/5030B
<0.5 µg/L
06/30/2023
sec-Butylbenzene
SW 846 Method 82BOD15030B
<0.5 pg/L
06/30/2023
Styrene
SW 646 Method 826OD15030B
<0.5 pg/L
06/30/2023
tert-Butylbenzene
SW 646 Method 826OD15030B
<0.5 pg/L
06/30/2023
Tetrachloroethene
SW 846 Method 82BOD150M
<0.5 pg/L
06/3012023
Report P. 2023-13417
Page 14 of 18

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info a environmcntalchcmists.com
City of Jacksonville
Date of Report: Jul 20, 2023
Post Office Box 128
Customer PO M
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report M 2023-13417
Project ID: Monitoring Wells
Toluene
sw 848 Method 8280D/5030B
<0.5 pg/L
06/30/2023
Trans-1 ,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/30/2023
Trans- 1,3-dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Trichloroethene
SW 846 Method 82WD15030B
<0 5 pg/L
06/30/2023
Tdchlorofluoromethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Vinyl chloride
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 3532, Rev 20, 1993 < 0_02 mg/L 06/28/2023
Nitrate+Nitrite-Nitrogen EPA 353 2, Rev 2 0, 1993 0.58 mg/L 06/29/2023
Nitrate Nitrogen Subtraction Method 0.58 mg/L 07/14/2023
Report #:: 2023-13417 Page 15 of 18

F-01,W176nvirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910,392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252,473.5702 Lab / Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab i Fax
info�a environmentalchemists.com
City of Jacksonville Date of Report: Jul 20, 2023
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Report #: 2023-13417
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
23-33413 Site: MW-17 6/28/2023 8:58 AM Water NB
Test
Method
Results Date Analyzed
Sulfate
EPA 300.0. Rev. 2.1, 1993
11 mg/L
06/29/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
0.8 mg/L
06/29/2023
Chloride
SM4500 CI E-2011
33 mg/L
06/30/2023
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
06/30/2023
1,1,1-Trichioroethane
SW 846 Method 8260D/50306
<0.5 pg/L
06/30/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,1,2-Trichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,1-Dichloroethane
SW 8a6 Method 8260D/5030B
<0.5 pg/L
06/30/2023
1,1-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,1-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/30/2023
1,2,3-Trichlorobenzene
SW 846 Method 828oD/5030B
<0.5 pg/L
06/30/2023
1,2, 3-Trichloropropane
SW 848 Method 826OD/50306
<0.5 pg/L
06/30/2023
1,2,4-Trichlorobenzene
SW 846 Method 8260D/503013
<0.5 pg/L
06/30/2023
1,2,4-Trimethylbenzene
SW sae Method 8260D/5030B
<0.5 pg/L
06/30/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,2-Dibromoethane
SW W Method 8280D/5030B
<0.5 pg/L
06/30/2023
1,2-Dichlorobenzene
SW a46 Method 8260D/5030B
<0.5 pg/L
06/30/2023
1,2-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
06/30/2023
1,2-Dichloropropane
SW 848 Method 8260D/5030B
<0.5 pg/L
06/30/2023
1,3,5-Trimethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,3-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
06/30/2023
1,4-Dichlorobenzene
SW 846 Method 8260D16030B
<0.5 pg/L
06/30/2023
2,2-Dichloropropane
SW "S Method 82BOD15030B
<0.5 pg/L
06/30/2023
2-Chlorotoluene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
4-Chlorotoluene
SW sae Method 82GOD15030B
<0.5 pg/L
06/30/2023
Report # 2023-134 1 7 Page 16 of 18

ro"'W07 _747 Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 . 910,392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255 A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS inf6a environmentalchemists.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention:
28541
Date of Report: Jul 20, 2023
Customer PO #:
Customer ID: 08110015
Report #: 2023-13417
Project ID: Monitoring Wells
Benzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/30/2023
Bromochloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Bromodichloromethane
SW 846 Method 8260015030E
<0.5 pg/L
06/30/2023
Bromoform
SW 846 Method 826OD150308
<0.5 pg/L
06/30/2023
Bromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Carbon tetrachloride
sw 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Chlorobenzene
SW 846 Method 820OD/5030B
<0.5 pg/L
06/30/2023
Chloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
06/30/2023
Chloromethane
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
cis-1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
cis-1,3-Dichloropropene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Dibromochloromethane
SW 846 Method 82e013/503013
<0.5 pg/L
06/30/2023
Dibromomethane
SW 646 Method 82ND1503013
<0.5 pg/L
06/30/2023
Dichlorodifluoromethane
SW 846 Method 82BOD15030B
<0.5 pg/L
06/30/2023
Ethylbenzene
SW 64s Method 8260D/50308
<0.5 pg/L
06/30/2023
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
06/30/2023
Isopropylbenzene
SW 846 Method 626OD15030B
<0.5 pg/L
06/30/2023
M+P Xylene
SW 846 Method 826OD15030B
<1.0 pg/L
06/30/2023
Methylene chloride
SW 846 Method 8260D15030B
<0.5 pg/L
06/30/2023
Naphthalene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
n-Butylbenzene
SW 848 Method 8260D/5030B
<0.5 pg/L
06/30/2023
n-Propylbenzene
SW 846 Method 826oD/5030B
<0.5 pg/L
06/30/2023
ortho-Xylene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
p-Isopropyltoluene
SW 846 Method 8260D/50306
<0.5 pg/L
06/30/2023
sec -Butyl benzene
SW 846 Method 8260D15030B
<0.5 pg/L
06/30/2023
Styrene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
tert-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
06/30/2023
Tetrachloroethene
sw sae ^mad 82000t osee
<0.5 pg/L
06/3012023
Report it- 2023-13417
Page 17 of 18

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoo environmentalchemists.com
City of Jacksonville
Date of Report: Jul 20, 2023
Past Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:
Report #: 2023-13417
Project ID: Monitoring Wells
Toluene
SW 846 Method 82BOD15030B
<0.5 pg/L
06/30/2023
Trans-1 ,2-Dichloroethene
SW 846 Method 626OD15030B
<0.5 pg/L
06/30/2023
Trans- 1,3-dichloropropene
SW B46 Method 8260D1503DB
<0.5 pg/L
06/30/2023
Trichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
06/30/2023
Tdchlorofluoromethane
SW 846 Method 8260D150308
<0.5 pg/L
06/30/2023
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
06/30/2023
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA363.2, Rev. 20. 1993
< 0.02 mg/L
06/28/2023
Nitrate+Nitrite-Nitrogen
EPA 3532, Rev. 20 1993
< 0.02 mg/L
06/29/2023
Nitrate Nitrogen
Subtrac don Method
<0.02 mg/L
07/14/2023
Comment:
Reviewed by:
Report #' 2023-13417 Page 18 of 18

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
Clien l
Date:
6602 Windmill W
Wilmington, NC 284(
910.392.02 i
eportNumber: _ 20 �ql
I -r 1Ill- t
❑ ❑ ieo N/H 1. Were custody seals present on the cooler? ❑ YES ❑ NO N/A it cost d J
Original
temperature
upon
receipt.
o y sea s were present, were they intact/unbroken?
-C
,
1 Howtemperature— Corrected temperature noon
- receipt _
taken' El Bia�l-®
1R Gun ID:
Thomas Traceable
Against Born : -
S/N 210886869
YES
❑
NO
IR Gun Correction Factor'C. 0.0
YES
❑
NO
3. If temperature of cooler exceeded 6-C, was Project Mgr./QA notified?
4. Were proper custod
ron
YES
El
NO
5. Were sample ID's listed therCOes r�linquished/received} fol;o�ved?
�]
YES
YES
❑
❑
NO
6. Were samples ID's listed on sample containers?
YES
❑
NO
7. Were collection date and time listed on the COC?
YES
O
NO
8. Were tests to be performed listed on the COC?
�$
YES
❑
NO
NO
9. Did samples arrive in proper containers for each test?
d
YES
❑
10. Did samples arrive in good condition for each test?
YES
❑
NO
11. Was adequate sample volume available?'
YES
❑
NO
NO
12. Were samples received within proper holding time for requested tests?
YES
❑
13. Were acid preserved samples received at a pH of <2?
❑
YES
❑
NO
14. Were cyanide samples received at a pH >12?
YES
❑
NO
15. Were sulfide samples received at a pH >9?
YES
❑
NO
NO
16. Were NH3/TKN/Phenol rece.ved at a chlorine residual of <0 3 m/`; Tf
17. Were Sulfide/Cyanide
❑
YES
❑
NO
received at a chlorine residual of <0.5 m/E?
18. Were orthophosphate samples filtered in the field
with,-n 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchs•-
Sample Preservation: (Must be completed for any sample(s) incorrect)
Samples) Y preserved or with headspace)
were rece`ved incorrectly preserved and were adjusted accord,ng'y
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Vote: NotTy tustome sz i'cz imr~�zd' « a,elyfor ircorrect'.y p,eserved sa-np es Qbta'r a new samp'e or not'fY the state tab if directed to analyzed by the customer. Who way notifed, date and t me:
Volatiles Sampfe(s)——.--_.�_
were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
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