WQ0034775_Comprehensive Site Assessment_20230731

Initial Review
Reviewer
nathaniel.thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other Comprehensive Site Assessment
Permit Number (IR) *
W00034775
Applicant/Permittee
Bakelite LLC
Email Notifications
Does this need review by the hydrogeologist? *
Yes No
Regional Office
Wilmington
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Anton Heitger
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Comprehensive Site Assessment
Phone Number*
16033897946
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https:Hedocs.deq.nc.gov/Forms/NonDischarge Monitori ng_Report
Permit Type:*
Wastewater Irrigation High -Rate Infiltration
Other Wastewater Reclaimed Water
Closed -Loop Recycle Residuals
Single -Family Residence Wastewater Other
Irrigation
Permit Number:*
WQ0034775
Has Current Existing permit number
Applicant/Permittee Address*
333 Neils Eddy Road, Riegelwood, NC 28459-9570
Facility Name*
Bakelite Synthetics - Riegelwood CLRS
Please provide comments/notes
on your current submittal below.
On behalf of Bakelite Synthetics, please find the Comprehensive Site Assessment (CSA) as required by Condition 1.1 of the July 2021 Closed -Loop
Recycle System Permit WQ0034775 for the Bakelite Acme Facility in Riegelwood (Acme), North Carolina,
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Bakelite Comprehensive Site Assessment —July 2023.pdf 19.54MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 7/31/2023

E H S Support
July 28, 2023
North Carolina Department of Environmental Quality
Division of Water Resources, Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Delivered via email — [e-mail]
Subject: Submittal of Comprehensive Site Assessment for the Bakelite Acme Facility in Acme, North
Carolina — Closed -Loop Recycle System Permit WQ0034775
To Whom it May Concern,
On behalf of Bakelite Synthetics, ("Bakelite"), EHS Support, LLC is providing the North Carolina
Department of Environmental Quality (NCDEQ) the enclosed Comprehensive Site Assessment (CSA) as
required by Condition 1.1 of the July 2021 Closed -Loop Recycle System Permit WQ0034775 for the
Bakelite Acme Facility in Acme, North Carolina. This CSA was developed in accordance with 15A NCAC
02L .0106(g) as required by the Condition 1.1.
Should you have any questions or require additional information, please feel free to contact me at
603-389-7946 or by email at [e-mail].
Sincerely,
Anton Heitger
Project Manager
Enclosure
Cc: Emily Thompson, Bakelite
Ronald Bazinet, Bakelite
Rusty Field, ONE Environmental Group, LLC
Anton Heitger • Northwood, NH 03261
603-389-7946 • [e-mail] • www.ehs-support.com

Comprehensive Site
Assessment
Bakelite Acme
Acme, NC
Prepared for:
Bakelite Synthetics
Prepared by:
E H S %;- Support
July 2023

Comprehensive Site Assessment — Bakelite Acme
Table of Contents
Table of Contents
1 Introduction..........................................................................................................................1
1.1 Purpose and Objectives......................................................................................................1
1.2 Site Background..................................................................................................................2
1.3 CLRS Pond Closure..............................................................................................................2
1.4 Report Organization............................................................................................................3
2 Assessment Activities.............................................................................................................4
2.1 Historical Report and Data Review.....................................................................................4
2.2 Baseline Groundwater Sampling Event..............................................................................4
2.3 Data Gap Assessment.........................................................................................................4
2.4 Groundwater Monitoring Well Installation........................................................................5
2.5 Geochemical Evaluation.....................................................................................................5
2.6 Compliance Boundary Demonstration...............................................................................5
3 Hydrogeological Framework...................................................................................................6
3.1 Groundwater Monitoring...................................................................................................6
3.1.1 COPCs.....................................................................................................................6
3.2 Groundwater Flow..............................................................................................................7
4 Geochemical Evaluation.........................................................................................................9
4.1 Groundwater Geochemistry...............................................................................................9
4.2 Disturbance to Soil During Lined Pond Closure................................................................10
4.3 Groundwater Concentration Trends.................................................................................10
4.3.1 Ammonia and Nitrate..........................................................................................11
4.3.2 Formaldehyde......................................................................................................12
4.3.3 TDS.......................................................................................................................12
4.3.4 Sulfate..................................................................................................................12
5 Compliance Boundary Demonstration..................................................................................14
5.1 Approach...........................................................................................................................14
5.2 Calibration.........................................................................................................................15
5.3 Plume Extent.....................................................................................................................16
6 Summary and Conclusions....................................................................................................17
6.1 Summary...........................................................................................................................17
6.2 Conclusions.......................................................................................................................17
7 References...........................................................................................................................18
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Table of Contents
List of Embedded Tables
Table 4-1 Summary of Groundwater Concentration Trends in WWMW-1 through WWMW-3
Table 5-1 Summary of Compliance Boundary BIOSCREEN and BIOCHLOR modeling
List of Attached Tables
Table 1 Summary of Groundwater Field Parameters
Table 2 Summary of Groundwater Sampling Results
List of Embedded Figure
Figure 3-1 Groundwater elevations measured in 2016 for the 2018 Remedial Investigation (Shield
Engineering, Inc., 2018).
Figure 3-2 Groundwater elevations for WWMW-1 through WWMW-3
Figure 4-1 Sulfate concentrations at WWMW-1 over time with precipitation
List of Attached Figures
Figure 1 Topographic Location Map
Figure 2 Facility Configuration
Figure 3 Current Site Conditions
Figure 4 Potentiometric Surface Map —July 2022
Figure 5 Potentiometric Surface Map —August 2022
Figure 6 Potentiometric Surface Map — November 2022
Figure 7 Potentiometric Surface Map — March 2023
Figure 8 Cross plots of redox parameters WWMW-1 through WWMW-3 (July 2022 through
March 2023)
Figure 9 Cross plots of historical data for COPCs with increases at WWMW-1 and WWMW-2
compared to upgradient well data from 2016
Figure 10 WWMW-1 Oxidation Model Results
Figure 11 Time Series Plots of Concentrations at WWMW-1
Figure 12 Time Series Plots of Concentrations at WWMW-2
Figure 13 Time Series Plots of Concentrations at WWMW-3
Figure 14 BIOSCREEN calibration model input and output (TDS example)
Figure 15 BIOSCREEN plume extent model input and output (ammonia example)
List of Appendice,
Appendix A WWMW-3 Boring Log and NCDEQ Well Construction Record
Appendix B Groundwater Sampling Field Sheets
Appendix C Laboratory Reports (2019 to 2023)
Appendix D Groundwater elevation data for WWMW-1 through WWMW-3 (Since RI)
Appendix E BIOSCREEN and BIOCHLOR Input Parameters and Model Outputs
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Comprehensive Site Assessment —Bakelite Acme
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Acronyms
Acronyms
CAP
Corrective Action Plan
C
Celsius
CSA
Comprehensive Site Assessment
CLRS
Closed Loop Recycle System
COPC
constituents of potential concern
DWQ
Division of Water Quality
Fe(II)
ferrous iron
Fe(III)
ferric iron
Oz
oxygen
NOa-
nitrate
NH4+
ammonium
Mn(II)
dissolved manganese
Mn(IV)
manganese cation
S042-
sulfate
mg/L
milligrams per liter
N
nitrogen
NOAA
National Oceanic and Atmospheric Administration
NCDEQ
North Carolina Department of Environmental Quality
PCE
tetrachloroethene
P.E.
professional engineer
RI
Remedial Investigation
SO4
Total Sulfate
TDS
total dissolved solids
TCE
trichloroethene
USEPA
United States Environmental Protection Agency
VOC
volatile organic compound
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Comprehensive Site Assessment — Bakelite Acme
Certification by Qualified Professional Engineer
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ONE Environmental Group of Carolina, PLLC (ONE) herein provides a certification for the comprehensive
site assessment at the referenced facility. The area of assessment was a former lined pond that was
regulated under North Carolina Department of Environmental Quality (NCDEQ) Closed -Loop Recycle
System Permit ("Permit") No. WQ0034775. A revised Permit was issued on July 29, 2021, following a
change of ownership request. The lined pond was removed from service in July 2011, closed in
November 2019, and restoration activities were observed by ONE (EHS Support, 2020).
The Permit issued in July 2021, included a condition (Condition 1.1) which required this comprehensive
site assessment. Section I — Schedules of the Permit stated that "Work that is within the scope of the
practice of geology and engineering, which involves site assessment, the interpretation of subsurface
geologic conditions, preparation of conceptual corrective action plans or any work requiring detailed
technical knowledge of site conditions shall be performed by persons, firms or professional corporations
who are duly licensed to offer geological or engineering services. " The certification by a P.E. meets this
requirement.
Printed Name ❑ acensed Professional Engineer
Signature
State of North Carolina
Professional Engineer
License No. 040609
Date 7f
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Comprehensive Site Assessment — Bakelite Acme
Introduction
i Introduction
kl
EHS Support LLC ("EHS Support") on behalf of Bakelite Synthetics ("Bakelite") has prepared this
Comprehensive Site Assessment (CSA) required by the July 2021 Closed Loop Recycle System (CLRS)
Permit (WQ0034775) for the Acme Facility located at 333 Neils Eddy Road in Acme (Riegelwood), North
Carolina ("Facility") (Figure 1). As part of the CLRS Permit, this CSA is to be completed within 2 years
following the issuance of the final permit. This CSA includes the items identified in 15A NCAC 02L
.0106(g) and "I" Schedules of the CLRS Permit. This CSA was developed by EHS Support in concert with
ONE Environmental of Carolina, PLLC ("ONE") as necessary to provide the Professional Engineer (P.E.)
certification of the CSA as required by Section I — Schedules of the Permit.
The area of interest for this CSA is the former CLRS lined pond that was taken out of service in 2011 and
obtained final closure in November 2019 (EHS Support, 2020). This area is herein referred to as the
"Site" and is provided on the topographic location map (Figure 1) which provides the outline and
location of the Bakelite Acme Facility and the Site. The Site is also shown on Figure 2 to present the
location in relation to the Bakelite Acme Facility. The current site conditions are presented as Figure 3.
1.1 Purpose and Objectives
On July 29, 2021, the North Carolina Department of Environmental Quality (NCDEQ) issued a revised
CLRS Permit WQ0034775 based on change of ownership of the Facility to Bakelite. Several existing
conditions to the Permit were removed because the lined pond was closed, and the following two new
conditions were added to the Permit:
• Condition 1.1— Within 24 months of Permit issuance, the Permittee shall submit a CSA
addressing the cause, significance, and extent of groundwater contamination in accordance with
15 A NCAC 02L.0106(g).
Condition 1.2 — Upon approval of the CSA, the Permittee may be required to prepare and submit
a Corrective Action Plan (CAP) for restoration of groundwater quality in accordance with 15 A
NCAC 02L.0106(h).
The following objectives were identified for this CSA in accordance with 15A NCAC 02L .0106 Corrective
Action (paragraphs "d" and "g") to satisfy condition 1.1 of the permit:
1. Review historical reports and data for soil, sediment, sediment porewater, surface water, and
groundwater data collected for the Acme, North Carolina Facility, and associated Wright
Chemical Superfund Site to determine the source and cause of contamination.
2. Identify hazards to the public health and safety, and receptors and significant exposure
pathways.
3. Determine the current groundwater conditions surrounding the CLRS.
4. Identify potential data gaps to characterize the horizontal and vertical extent of soil and
groundwater contaminants and significant factors affecting contaminant transport.
5. Identify geological and hydrogeological features influencing the movement, chemical, and
physical character of the contaminants.
6. Demonstrate that natural attenuation is occurring at the Site and that groundwater
contaminants will not exceed the Permit standards at a compliance boundary.
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Comprehensive Site Assessment — Bakelite Acme
Introduction
1.2 Site Background
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The Acme Facility (owned and operated by Bakelite) is an active facility specializing primarily in the
production of formaldehyde, aqua ammonia, and hexamine. The Site is the former CLRS lined pond area
in the northwest corner of the Facility that was associated with the CLRS (Figure 2 and Figure 3). The
Acme Facility is within the footprint of a United States Environmental Protection Agency (USEPA) led
Superfund Site (Wright Chemical Corporation Superfund Site) (Figure 2). The former lined pond was
regulated under the NCDEQ Division of Water Quality (DWQ) CLRS Permit number WQ0034775, issued
to Momentive (d.b.a. Hexion) on November 30, 2010 (NCDENR, 2010). The current Permit issued in July
2021 was updated based on the change in ownership and the closure of the lined pond.
Water (including stormwater first flush) previously generated from plant operations was discharged to
the former lined pond as a historical practice. As allowed by the Permit, Bakelite operates three cooling
towers (CT-3, CT-5, and CT-6) to support the manufacturing process, with the lined pond historically
being both the source of the cooling tower make-up water and the discharge location of the cooling
tower blowdown. Over time, the lined pond accumulated sludge, as indicated in the sludge surveys
conducted in April 2009 and February 2010 (Arcadis, 2012).
In 2010, Hexion installed two groundwater monitoring wells per NCDEQ DWQ CLRS Permit number
WQ0034775CLRP. The locations of these monitoring wells are shown on Figure 2 and Figure 3. The
monitoring wells, located northwest (WWMW-1) and southwest (WWMW-2), are sampled triennially
(three times per year) and analyzed for pH, total dissolved solids (TDS), total sulfate (as SO4), total
ammonia nitrogen (as N), total nitrate nitrogen (as N), volatile organic compounds (VOCs), total organic
carbon (TOC), and methanal (formaldehyde) whole water. Groundwater monitoring has continued at
the two monitoring wells after the lined pond was taken out of service. As part of this CSA, a third
monitoring well (WWMW-3) was installed southeast of the former lined pond on July 7, 2022 (Figure 2
and Figure 3). This monitoring well was added to the triennial monitoring program and groundwater
samples from all three wells were analyzed for the Permit required parameters and three additional CSA
parameters (sulfide, dissolved iron, and dissolved manganese).
1.3 CLRS Pond Closure
The CLRS lined pond was placed into service in the early 1990s (J.M. Waller Associates, Inc., 2012) in
support of the prior owner's operations. Hexion (formerly d.b.a. Momentive Specialty Chemicals, Inc.
["Momentive"]) acquired this Site in 2006 and continued to operate the lined pond in a similar manner
to the prior operations. Hexion took the lined pond out of service and initiated pre -characterization
activities in July 2011. Initial cleaning of the lined pond started on July 26, 2011, and finished by the end
of October 2011. After the sludge removal was complete the liner was inspected, and it was determined
the liner was not repairable and the lined pond remained out of service since 2011.
Final closure activities for the former lined pond were implemented by Hexion in 2019. The final closure
activities consisted of liner removal, localized over -excavation beneath the liner, berm removal, and
regrading to support positive drainage and placement of a vegetative layer, and were completed in
November 2019. Following final closure, a three-year groundwater compliance monitoring program was
implemented to assess the ongoing attenuation of Site -related constituents of potential concern
(COPCs) in groundwater (EHS Support, 2020). Additional details of the lined pond closure are presented
in the Lined Pond Closure Completion Report (EHS Support, 2020).
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Comprehensive Site Assessment — Bakelite Acme
Introduction
1.4 Report Organization
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As required by the Permit, this CSA was prepared to describe and include the items listed in 15A NCAC
02L .0106(g) and "I" Schedules of the draft CLRS Permit (Section 1.1). The CSA includes a summary of
assessment activities and sampling results, a tabulated summary of field and laboratory data. The CSA
also includes scaled figures showing sample locations, potentiometric surface maps, geochemical
analyses, and example model parameters.
Following this introductory section, the CSA consists of the following sections:
• Section 2 — Assessment Activities: Summarizes the assessment activities conducted to meet the
requirements of the CSA.
• Section 3 — Hydrogeological Framework: Summarizes the groundwater contaminants and
hydrogeology of the Site.
• Section 4 — Geochemical Evaluation: Provides a summary of geochemical evaluation conducted
as part of the CSA using data collected and Remedial Investigation (RI) data.
• Section 5 — Compliance Boundary Demonstration: Summarizes the application of BIOSCREEN
and BIOCHLOR models to demonstrate that that groundwater contaminants will not exceed the
Permit standards at the compliance boundary.
• Section 6 — Summary and Conclusions: Summarizes the assessment and evaluations completed
as part of the CSA and conclusions following the findings of the CSA.
• Section 7 — References: Provides a list of reference materials used in the preparation of the CSA.
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Assessment Activities
2 Assessment Activities
The following activities were conducted to prepare the CSA in accordance with 15A NCAC 02L .0106
Corrective Action (paragraphs "d" and "g"):
• Historical report and data review for soil, sediment, sediment porewater, surface water, and
groundwater data collected for the Acme, North Carolina Facility, and associated Wright
Chemical Superfund Site for source, hazards to the public health and safety, and receptors and
significant exposure pathways.
• A baseline groundwater monitoring event to determine the current groundwater conditions
surrounding the Site and compare groundwater sampling methods.
• Data gap assessment to identify potential data gaps in the characterization of the horizontal and
vertical extent of soil and groundwater contaminants.
• Demonstration that groundwater contaminants will not exceed the permit standards at the
compliance boundary (Mill Creek).
• Geochemical evaluation to assess the concentrations and source of constituents of potential
concern (COPC) in groundwater.
2.1 Historical Report and Data Review
A comprehensive review of historical reports and data for the Acme Facility and Wright Chemical
Superfund Site surrounding the former lined pond was conducted to identify potential data gaps in the
Site characterization. Historical soil, groundwater, pore water, and surface water investigation findings
were reviewed for historical concentrations of Site COPCs. In addition, historical laboratory results for
the two groundwater monitoring wells (WWMW-1 and WWMW-2) were reviewed to evaluate COPC
trends and permit standard exceedances.
2.2 Baseline Groundwater Sampling Event
Following the historical report and data review for potential data gaps and historical concentrations of
COPCs, a baseline groundwater sampling event was conducted to determine the current groundwater
concentrations. Two monitoring wells (WWMW-1 and WWMW-2) were redeveloped to remove any
potential sediment or solids from the well casing and sampled approximately 24 hours later using low -
flow groundwater sampling techniques. The groundwater samples were analyzed for the constituents
required by the 2021 Permit and compared to the typical triennial sampling results which were collected
approximately one day following low -flow sampling. The triennial samples are collected by bailing three
well volumes, allowing the well to recharge, and returning the following day to collect a sample from
each well with a bailer. The results for both low -flow sampling and the triennial samples collected by
bailer appeared to correlate in both wells sampled and it was determined the sampling method did not
influence concentrations of COPCs.
2.3 Data Gap Assessment
The historical data review and the baseline groundwater sampling data supported the completion of a
data gap assessment to identify where additional sampling or analyses may be required to refine the
Site conceptual model. The data gap assessment concluded that the Site -related COPCs above Permit
groundwater standards at WWMW-1 and WWMW-2 are most likely derived from upgradient
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Comprehensive Site Assessment —Bakelite Acme
Assessment Activities
groundwater; therefore, one new monitoring well south-southeast of the former lined pond was
recommended to investigate an upgradient source of COPCs.
2.4 Groundwater Monitoring Well Installation
Based on the data gap assessment identifying that the Site did not have an appropriately located
monitoring well upgradient of the former lined pond area, a recommendation of the data gap
assessment was to install a monitoring well (WWMW-3) southeast of the former lined pond area (Figure
2 and Figure 3). Specifically, the well was proposed to be installed upgradient of the former lined pond
area in the southeast corner just outside of the former berm.
Groundwater monitoring well WWMW-3 was subsequently installed in July 2022 to help define the
horizontal extent of COPCs in Site groundwater and facilitate the generation of localized potentiometric
surface in this area. The boring log including well construction details and the NCDEQ division of water
resources well construction record are provided as Appendix A.
The groundwater monitoring well was developed at least 24 hours after installation and groundwater
samples were collected as part of the triennial sampling conducted in accordance with the Permit. The
groundwater samples were analyzed for the permitted constituents along with natural attenuation
parameters (sulfide, dissolved iron, and dissolved manganese as recommended in the data gap
assessment).
2.5 Geochemical Evaluation
The geochemical evaluation provided in the data gap assessment was updated for the CSA following the
installation of WWMW-3 and an additional year of monitoring to update the findings and conclusions. Ir
addition, the installation of WWMW-3 facilitated the development of groundwater contour maps
(Figure 4 through Figure 7) to determine the localized flow direction of shallow groundwater at the Site.
The geochemical evaluation is provided as Section 4.
2.6 Compliance Boundary Demonstration
The compliance boundary demonstration leverages predictive calculations and modeling using
BIOSCREEN and BIOCHLOR, Domenico based models. These models were produced to show
groundwater contaminants will not exceed the CLRS Permit standards Mat the compliance boundary
through natural site conditions, facility design, and operational controls as identified in 15A NCAC 02L
.0106(d)(1). The input parameters, assumptions, and summary of this compliance boundary
demonstration are provided in Section 5.
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Hydrogeological Framework
3 Hydrogeological Framework
This section provides a summary of groundwater monitoring, Site COPCs, and hydrogeology of the Site.
3.1 Groundwater Monitoring
Three wells WWMW-1, WWMW-2, and WWMW-3 are monitored triennially by Wood Environment &
Infrastructure Solutions, Inc. (now WSP USA Environment & Infrastructure Inc.) of Wilmington, NC.
Groundwater sampling is typically completed over two days. The depth to groundwater and purging of
three well volumes with a bailer and collection of water quality parameters (temperature, pH, and
specific conductivity) are completed on the first day of each sampling event. The following day, a set of
water quality parameters is collected from each well at the time of sampling for the permitted
constituents:
• TOC
• Formaldehyde Whole Water
• Ammonia as N
• Total Nitrate (as N)
• pH
• Total Phosphorus
• TDS
• Total Sulfate
• VOCS
In addition to the permitted constituents, the last three sampling events (July 2022 through March
2023) included the following constituents for the geochemical evaluation:
• Dissolved iron
• Dissolved manganese
• Sulfide
Field parameters including depth to water prior to purging, and water quality parameters collected at
the time of sampling are provided on Table 1. The field sampling sheets are provided as Appendix B.
3.1.1 COPCs
Based on the evaluation of groundwater monitoring results to Permit standards, the Site COPCs with
their respective Permit standard are:
• Ammonia — 1.5 milligrams per liter (mg/L)
• Formaldehyde — 0.6 mg/L
• Nitrate (as N) — 10 mg/L
• Sulfate — 250 mg/L
• TDS — 500 mg/L at 180 degrees Celsius (C)
These COPCs were evaluated for this CSA as the Site groundwater contaminants in Section 4 and Section
5. Periodic detections of VOCs were observed (Table 2) in all three wells from April 2011 to March 2023
and reported in the triennial submittals of the Compliance Monitoring Form (GW-59). However, these
were not evaluated for this CSA because the detections were sporadic and may be from an upgradient
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Comprehensive Site Assessment — Bakelite Acme
Hydrogeological Framework
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groundwater source or potential lab contamination. Groundwater sample results are summarized in
Table 2 and laboratory reports are provided in Appendix C.
3.2 Groundwater Flow
The potentiometric surface map and groundwater elevations collected in 2016 and presented in the
2018 RI (Shield Engineering, Inc., 2018) indicated that groundwater beneath the former manufacturing
area flows from the southeast to the northwest toward WWMW-1 and WWMW-2 (Figure 3-1). The 10-
foot elevation contour has a notable northward bend around WWMW-1 immediately north of the
former lined pond. The cause of the bend in the potentiometric surface was identified as a data gap as
part of the data gap assessment, as it was uncertain if this condition was due to preferential infiltration
from the former lined pond causing groundwater mounding in the vicinity of WWMW-2, or due to
another cause.
In July 2022, a new well (WWMW-3) was installed southeast of WWMW-2 to better understand
constraints on groundwater flow and to obtain a sample upgradient of the former lined pond to identify
if the feature or its removal in 2019 affected groundwater quality. Groundwater elevation data from the
new WWMW-3 monitoring well indicate groundwater where the former lined pond was located flows
consistently from east to west toward WWMW-2 (Figure 4 through Figure 7). Consequently, WWMW-2
provides a point directly downgradient of the former lined pond and can be used to identify water
quality impacts attributed to the former lined pond or its removal.
a
Figure 3-1: Groundwater Elevations Measured in 2016 for the 2018 RI (Shield Engineering, Inc., 2018).
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Comprehensive Site Assessment —Bakelite Acme
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Hydrogeological Framework
To better understand upgradient influences on groundwater quality, WWMW-1 and WWMW-3 are
compared to concentration data for upgradient groundwater wells provided in the 2018 RI report and
are further discussed in Section 4.
Available water level data indicate groundwater elevations in WWMW-1 and WWMW-2 initially
declined following removal of lined pond, supporting the idea that the former pond was a source of
recharge. Water levels in WWMW-1, WWMW-2, and WWMW-3 show a recent increasing elevation
trend, suggesting the groundwater system is re -equilibrating as groundwater from upgradient moves
through the system (Figure 3-2). This supports the idea that infiltration to groundwater through the
former lined pond is no longer occurring following closure of the pond and re -grading to redirect surface
runoff away from the Site. Groundwater elevations from the RI to March 2023 are included in Appendix
D.
V
16
1/1/2016 6/14/2017 11/26/2018 5/9/2020 10/21/2021
Date
Figure 3-2: Groundwater elevations for WWMW-1 through WWMW-3 (note, the dashed line
represents the time between 2016 RI groundwater measurement and July 2019 measurement)
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Geochemical Evaluation
4 Geochemical Evaluation
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This section provides the details of the geochemical evaluation following the data gap assessment and
one year of groundwater monitoring following the installation of WWMW-3. The geochemical
assessment provides a primary line of evidence for the source of COPCs at WWMW-1 and WWMW-2.
4.1 Groundwater Geochemistry
In addition to the standard analytes, samples were analyzed for sulfide, and field filtered (0.45 micron)
dissolved iron and dissolved manganese to assess redox conditions as part of the geochemical
evaluation. The results were evaluated in the context of the redox ladder, which refers to the order of
preferential electron acceptor utilization in waters, which follows the sequence — Oz > NO3 > Mn(IV) >
Fe(III) > S042- in progressively more reducing conditions (McMahon and Chapelle, 2008). Given the
sequential nature of electron acceptor utilization, increased concentrations of the end products
(ammonium [NH4'], dissolved manganese [Mn(II)], ferrous iron [Fe(II)], sulfide), and depleted electron
acceptors (02, NO3, S042-) through water quality sampling can be used to identify redox conditions.
The redox assessment results are summarized on Figure 8:
• Samples from upgradient well WWMW-1 are highly reduced and sulfate/sulfide controls redox.
• Samples from downgradient well WWMW-2 are oxic; sulfide is not detected; iron is very low;
ammonia is low; and nitrate is elevated. The presence of manganese (a slightly more reducing
indicator) suggests this water was once more reduced and is transforming to more oxidizing
conditions or is a disequilibrium mixture between oxidized and reduced waters.
• Groundwater in WWMW-3 is reduced, but low to non -detect sulfide suggests fewer reducing
conditions than at WWMW-1.
• In summary, natural attenuation of COPCs is occurring due to a combination of geochemical
reactions and mixing with infiltrated precipitation.
Figure 8 indicates a correlation between sulfate and sulfide in WWMW-1: elevated sulfate corresponds
to lower sulfide and vice versa. Given that pH values are circum-neutral at WWMW-1 (Table 2), sulfide
oxidation at this location is not likely as this process generates substantial acidity. This observation
suggests that sulfate is transforming to sulfide at this location. Sulfide precipitation in groundwater at
WWMW-1 is consistent with the field sampling logs, which indicate that a black color is present in
samples (commonly a result of microcrystalline iron sulfide minerals precipitating) and an odor that is
noted on the sampling logs suggesting hydrogen sulfide is present (Appendix B).
Constituent cross plots indicate WWMW-1 is distinct in composition from WWMW-2 and WWMW-3,
and the composition of samples from WWMW-1 can be explained by mixture of waters from upgradient
wells MW-4 or MW-28 (Figure 9). WWMW-3 and downgradient well WWMW-2, and WWMW-2 appear
to mixtures from background groundwater upgradient of the facility (represented by the 2016 sample
reported in the RI from KMW-2) and WWMW-1.
The pH data in combination with the redox conditions at WWMW-1 through WWMW-3 support this
mixing model. Notably, the pH in downgradient well WWMW-2 is distinctly acidic compared to
upgradient wells WWMW-1 and WWMW-3. A geochemical model using a simplified WWMW-1
composition illustrates a potential cause of the pH change in the downgradient direction (Figure 10).
Complete oxidation of the sulfide measured in the WWMW-1 sample can conceivably result in a pH shift
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Comprehensive Site Assessment — Bakelite Acme
Geochemical Evaluation
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to acidic conditions of over 3.5 pH units. Analytical results at WWMW-2 compared to the upgradient
wells further support this oxidation model. Specifically, sulfide is absent at WWMW-2, ammonia is
depleted, and nitrate is elevated (indicating ammonia oxidation). The cause of the oxidation is
potentially infiltration of oxidized precipitation into the area where the former lined pond was removed.
4.2 Disturbance to Soil During Lined Pond Closure
During closure activities, four composite soil samples were collected from four quadrants of the base of
the lined pond and four composite samples were collected from the four berms. Soil samples were
collected from the 0 to 6-inch interval and were biased toward areas of potential impact, as determined
by visual inspection and field screening using an organic vapor monitor and a formaldehyde monitor.
The results of the composite soil sampling showed no exceedances of protection of groundwater
standards for any of the COPCs (EHS Support, 2020). Detections of total Kjeldahl nitrogen, ammonia
nitrogen, nitrate, and nitrogen were noted but only one detection of nitrite at a low concentration (J
flagged by the laboratory for a lower concentration than the reporting limit). These results were
consistent with no increases in these constituents in groundwater following soil removal activities.
Furthermore, the absence of composite soil exceedances indicates an upgradient source for the
nitrogen constituents that persistently exceed permit standards in WWMW-1 and WWMW-2.
Formaldehyde and molybdenum were the only COPCs present in the berm and soil composite samples
that exceeded their respective protection of groundwater standards (EHS Support, 2020). As there are
no soil standards for the protection of groundwater for sulfate or TDS, and TDS cannot be directly
measured in soil, soil composite sampling cannot be used to determine if berm soils used to fill the lined
pond or in the soils that were left in -place were a source for these constituents to groundwater.
In summary, composite sampling indicates that soil at the former lined pond is not the source of
nitrogen compounds to groundwater at the Site.
4.3 Groundwater Concentration Trends
The cause of increases in groundwater sulfate, formaldehyde, and TDS in 2020 following removal of the
former lined pond were identified as a data gap. Hypotheses for the increasing trends include:
• Changes in precipitation infiltration at the former lined pond led to decreased dilution.
Changes in upgradient water quality.
Soil disturbed during the lined pond closure construction temporarily led to elevated
groundwater concentrations.
Geochemical changes in samples during transit to the laboratory.
Time series concentration data through March 2023, coupled with the revised understanding of
groundwater flow directions described in Section 3.2, provide a basis for understanding the cause of the
concentration increases (Figure 11 through Figure 13). The time series charts indicate that the
concentration increases have generally decreased for most monitored parameters and have stabilized
and returned to pre -closure conditions. A summary of the concentration trends is provided in Table 4-1
for the period of operation, after the lined pond was cleaned and after final closure activities.
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Geochemical Evaluation
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Table 4-1 Summary of Groundwater Concentration Trends in WWMW-1 through WWMW-3
WWMW-1
WWMW-2
WWMW-3
Operational
Out of
Post-
Operational
Out of
Post-
Post-
COPC
Period
Service
Closure
Period
Service
Closure
Installation
(2010-
(2011-
(2019--
(2010-2011)
(2011-
(2019--
(July 2022 -
2011)
2019)
March
2019)
March
March
2023)
2023)
2023)
Decreasing
Decreasing
Decreasing
Slightly
Ammonia-
Above
trend
trend
Above
Decreasing
trend
decreasing
trend above
Nitrogen
standard
above
above
standard
above
trend above
standard
standard
standard
standard
standard
Below
Points
Late
Below
Remained
Standard,
Below
above and
increasing
Below
Formaldehyde
below
except one
below
trend
standard
standard
Standard
standard
point in
standard —
below
time
no trend
standard
Elevated
but
Decreasing
Below
Below
Above
Above
Below
Nitrate
remained
trend above
standard
standard
Standard
Standard
Standard
below
standard
standard
Stable
Increasing
Below
above and
Increasing
Above
Decreasing
trend
Below
Sulfate
above
trend below
Standard
below
standard
above
Standard
standard
standard
standard
standard
DecreasingIncreasing
Decreasing
Increasing
trend to
Above
trend
trend
Above
trend
Below
TDS
stable
standard
above
above
standard
above
Standard
below
standard
standard
standard
standard
Notes:
COPC = constituent of potential concern
TDS = total dissolved solids
Observations and interpretations of the trend graphs (Figure 11 through Figure 13) are discussed in
Sections 4.3.1 through 4.3.4.
4.3.1 Ammonia and Nitrate
Ammonia is above the Permit standard in all three wells. Time series data for WWMW-1 and WWMW-2
indicate that concentrations remained stable throughout closure activities (Figure 11 and Figure 12).
Ammonia concentrations are highest in well WWMW-1 (located upgradient of the former lined pond)
and lowest in well WWMW-2 (located downgradient of the former lined pond). Nitrate is below the
Permit standard in WWMW-1 and WWMW-3 but the groundwater concentrations at downgradient well
WWMW-2 are above the standard.
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These observations are interpreted to indicate that ammonia in wells WWMW-1 through WWMW-3 are
from an upgradient source. The lower concentrations of ammonia at downgradient well WWMW-2
suggest that dilution from infiltration of precipitation where the former lined pond was located
contributes to lower ammonia concentrations at WWMW-2. In addition, oxidation of ammonia to
nitrate is supported by elevated nitrate above the Permit standard at downgradient well WWMW-2.
4.3.2 Formaldehyde
Concentrations of formaldehyde in WWMW-1 had increased above the Permit standard briefly following
removal of the former lined pond and have since returned to values below the Permit standard and
returned to pre -removal levels. A brief increase in formaldehyde was observed in WWMW-2 following
removal of the former lined pond, but concentrations have remained below the Permit standard and
subsequently returned to pre -removal levels. Formaldehyde was below the Permit standard for all
samples collected from WWMW-3. Formaldehyde concentrations briefly spiked following soil
disturbance during removal of the lined pond but are now below the Permit standard in all three wells.
4.3.3 TDS
Concentrations of TDS in WWMW-1 had increased above the Permit standard briefly following removal
of the former lined pond and have since declined to pre -removal levels but still above the Permit
standard. A brief increase in TDS was observed in WWMW-2 following removal of the former lined
pond, but concentrations have remained near (above and below) the Permit standard. TDS was below
the Permit standard for all samples collected from WWMW-3.
4.3.4 SulfotF
Concentrations of sulfate in downgradient well WWMW-2 had increased above the Permit standard
following removal of the former lined pond, and quickly decreased to below the standard in WWMW-2
by 2022. Between July 2022 and March 2023, sulfate was below the Permit standard in WWMW-3.
Sulfate hovered above and below the Permit standard in WWMW-1 prior to pond removal, and
increased following removal of the lined pond and has since persisted above the Permit standard
although fluctuates seasonally.
Elevated sulfate in downgradient well WWMW-2 in 2020 and 2021 was a temporary condition that
occurred due to disturbance caused during removal of the former lined pond. Concentrations returned
to below the Permit standard indicating that sulfate attenuates between the upgradient and
downgradient points likely due to dilution by precipitation infiltration. The source of the sulfate is likely
sulfide from a location upgradient of WWMW-1 and WWMW-3 that is oxidized to sulfate by infiltration
of oxic precipitation.
An increase in sulfate at WWMW-1 followed removal of the former lined pond. As indicated in Figure 4-
1, times of elevated sulfate in WWMW-1 correspond to periods of elevated precipitation (90 day rolling
average) following removal of the former lined pond in 2019. It is not clear if the precipitation
infiltration is mobilizing sulfate from soil disturbed during removal of the former lined pond, or if
oxidation of sulfide in groundwater from an upgradient source is occurring as a result of precipitation
infiltration. Precipitation data presented on Figure 4-1 was reported by the National Oceanic and
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Atmospheric Administration (NOAA) station located at Wilmington International Airport in Wilmington,
North Carolina.
1800
1600
1400
-- 1200
E 1000
v
0 800
'^ 600
400
200
0
Sulfate Sulfate Std Precipitation
Figure 4-1: Sulfate concentrations at WWMW-1 over time with precipitation
0.5
v
0.4
c
c
0.3 .2
.Q
0.2 u
a)
0.1
F
a
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Comprehensive Site Assessment — Bakelite Acme
Compliance Boundary Demonstration
5 Compliance Boundary Demonstration
kl
This section provides the details regarding the compliance boundary demonstration using Domenico
based BIOSCREEN and BIOCHLOR models. The compliance boundary used for these models was the
closest portion of Mill Creek in the direction of groundwater flow which may potentially discharge to
surface water (Figure 7).
5.1 Approach
BIOSCREEN (USEPA, 1997) and BIOCHLOR (USEPA, 2002) are screening models that simulate
remediation through natural attenuation of dissolved components and were used to model the extent
of the plume. The software was developed by Groundwater Services, Inc and the United States Air Force
and uses the Domenico analytical solute transport model to simulate one -dimension advection, three -
dimension dispersion, linear adsorption, and biotransformation. In addition, BIOCHLOR, can simulate the
sequential degradation of one compound into another. The models were run for compounds exceeding
their corresponding standard in the March 2023 sampling event: sulfate, ammonia nitrogen, nitrate, and
TDS. As stated in Section 4.3, oxidation of ammonia to nitrate is supported by elevated nitrate above the
Permit standard at downgradient well WWMW-2. For this model, nitrate was assumed to be the only
degradation product of ammonia oxidation.
Although BIOCHLOR is primarily programmed to model the reductive dechlorination of chlorinated
ethenes and ethanes, it can also be used to model any compound that degrades via sequential first
order decay kinetics by entering the yield constants for the specified reaction. In the model, ammonia
was modeled as tetrachloroethene (PCE) and nitrate as the first daughter product, trichloroethene
(TCE). The previously calculated half-life of 0.06 years for ammonia was used for ammonia degradation
and the model was then calibrated to field data by adjusting the biodegradation half-life of nitrate until
the model matched the concentrations measured at WWMW-2. The model -derived half-life for nitrate
was found to be 0.02 years (7 days).
The starting input parameters are organized into different screen boxes in BIOSCREEN and are
summarized as follows:
Hydrogeology. Seepage velocity, Vs, was entered directly into the model as this parameter was
provided in the RI Report (Shield Engineering, Inc., 2018). Seepage velocities between 11 and
210 feet per year were reported and the highest velocity of 210 feet per year was selected for
the model. Hydraulic conductivity, K, and hydraulic gradient, i, are not required if seepage
velocity is provided as an input. However, porosity, n, is required for adsorption and mass
calculations. For this parameter, the default value of 0.25 was accepted.
Dispersion. As dispersivity is difficult to measure in the field, dispersivity was estimated in the
calibration step described below. Longitudinal dispersivity, alpha x; transverse dispersivity,
alpha y; and vertical dispersivity, alpha z were all calculated by the models using an estimated
plume length.
Adsorption. The models use a retardation factor, R, to calculate how sorption of contaminants
to organic material in the solid aquifer matrix decreases advection of the contaminants through
the plume. However, all dissolved contaminants considered in the model were ionic
components. Thus, adsorption was assumed to be negligible, and R was set to 1 for all modeled
contaminants. If R is entered, no other sorption parameters are needed in the models.
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• Biodegradation. BIOSCREEN calculates plume length using three distinct methods: no
degradation, first -order decay kinetics and instantaneous reaction kinetics. BIOCHLOR uses only
the first two approaches. Degradation of TDS was assumed to be negligible and thus transport
of this COPC was modeled with no degradation. The biodegrading rates for the other
compounds were estimated in the calibration step, described in Section 5.2 below. The yield
(required for BIOCHLOR only) is the the ratio of the daughter product molecular weight to the
parent compound molecular weight which was calculated to be 3.6 for the oxidation of
ammonia into nitrate.
• Modeled Area Length and Width. The model area length was adjusted to include the entire
plume. As only the centerline output is used for this model, the plume width was not required.
• Simulation Time. The time of the simulation was adjusted as needed for each specific model.
• Source Data. The default value of 10 feet for the source thickness in the saturated zone was
used. Site data from the second quarterly sampling event was used for both calibrating plume
properties and predicting plume extents. The source width was calibrated in the following step.
Due to uncertainties in the source of the contaminants, the soluble mass of the source was
assumed to be infinite as a conservative approach.
• Field Data for Comparison. WWMW-1 and WWMW-2 were used to define the centerline of the
plume to leverage field data in the model. Concentrations reported at these monitoring points
during the March 2023 sampling event were used. To obtain distances for the compliance point
(Mill Creek), a transect was determined parallel to groundwater flow using the groundwater
contours (Figure 7) near each well. The distance between the contour lines was taken as the
distance between WWMW-1 and WWMW-2 (90 feet). The distance from WWMW-2 to Mill
Creek was 65 feet (in the direction of groundwater flow).
• Output. Only the Centerline output was used for this model.
5.2 CaiiDrazion
The BIOSCREEN and BIOCHLOR calibration input and output for each contaminant are provided in
Appendix E and an example is provided on Figure 14. The TDS data for WWMW-1 and WWMW-2 was
used to calibrate the model for plume length and source zone width, assuming negligible degradation of
TDS along the length of the plume ("No Degradation" kinetics). It is important to note that for the
model, WWMW-1 was modeled as the "source" as it was the most upgradient well with the highest
concentration of each contaminant. However, this does not imply that WWMW-1 is the ultimate source
of contaminants at the Site.
Total plume length and source zone width were determined through an iterative process. The time was
set to 1 year for the calibration step as the seepage velocity indicated that contaminants would travel
the 90 feet between the two wells in this time. The other model parameters were used are exactly as
described in Section 5.1. An initial approximation for plume length was estimated by plotting TDS at
each well as a function of distance downgradient from WWMW-1 and extending the regression to
determine the distance at which this linear approximation predicts the plume will end. BIOSCREEN was
then run to determine the predicted length of the plume (here assumed to be the distance along the
center line at which modeled concentration falls below 1% of initial concentration). This modeled value
for the plume was then taken as the plume length and the model re -run. This step is consistent with the
methodology described in the BIOSCREEN User's Manual (USEPA, 1996). The source zone width was
then adjusted so that the concentration 90 feet downgradient matched those measured for WWMW-2.
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Compliance Boundary Demonstration
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From this process, the final plume length and source zone width were estimated to be 360 feet and 19
feet, respectively.
BIOSCREEN's no degradation kinetics overpredicted the concentrations of sulfate and ammonia
observed at WWMW-2, supporting the fact that degradation of these compounds occurs, in addition to
dispersion of the plume as it moves downgradient. The biodegradation rates for degrading compounds
(sulfate, ammonia) were then calibrated to field data by adjusting the biodegradation half-life until the
model matched the concentrations measured at WWMW-2. The model -derived half-life for sulfate was
found to be 0.55 years (200 days). The half-life for ammonia was found to be 0.06 years (22 days).
As nitrate is assumed to be produced by the oxidation of ammonia, BIOCHLOR was used to model the
production of nitrate as ammonia is degraded.
5.3 Plume Extent
The BIOSCREEN and BIOCHLOR plume extent model input and output for each contaminant are provided
in Appendix E and an example is provided on Figure 15. The model results are summarized in Table 5-1.
The calibrated models were used to determine the concentration of each contaminant reaching the
compliance point (receptor) 155 feet downgradient of WWMW-1 along the centerline of the plume. The
simulation time was extended until concentration at the compliance point no longer increased to
determine the maximum concentration expected at the compliance point. This occurred at simulation
times longer than 4 years.
Concentrations of TDS, sulfate, ammonia, and nitrate at the receptor were found to be 334 mg/L, 146
mg/L, 0.7 mg/L, and 1.0 mg/L respectively, all lower than the corresponding Permit standards. In
summary, the modeled plume extent of these COPCs are below corresponding Permit Standards at the
compliance boundary.
Table 5-1
Parameter
TDS
Sulfate
Ammonia
Nitrogen
Nitrate
Summary of Compliance Boundary BIOSCREEN and BIOCHLOR modeling
WWMW-1 WWMW-2 Permit Time to Peak Peak
Concentration Concentration Standard (days) Half-life Concentration Concentration at Receptor
(mg/L) I (mg/L) (mg/L) I (Years) (mg/L)
1,310 534 500 — 4 334
1,020 264 , 250 1 26 4 146
490 8.8 1.5 237 4 0.7
0.04 12.6 10 7 4
Notes:
mg/L = milligrams per liter
— = infinite
1.0
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Comprehensive Site Assessment —Bakelite Acme
k14h..4--01-q
Summary and Conclusions
6 Summary and Conclusions
This section provides a summary of the findings of the CSA and conclusions.
6.1 Summary
The geochemistry evaluation combined with the revised understanding of groundwater flow suggest
that constituent contributions are not likely sourced from the area where the former lined pond was
located and are potentially from an upgradient source. Oxidation reactions occur in groundwater as it
flows beneath the area where the former lined pond was located by infiltration of precipitation. Sulfide
is oxidized to sulfate which lowers the pH, and ammonia is oxidized to nitrate. The ammonia and sulfide
that lead to the nitrate and pH exceedances at downgradient well WWMW-2 are present in upgradient
wells WWMW-1 and WWMW-3, suggesting a source other than the former lined pond for these
constituents.
Acquisition of additional time series data indicates that concentration increases observed in 2019-2020
at WWMW-1 and WWMW-2 were a brief event that has returned to prior conditions for most
constituents. The brief spike in concentrations is attributed to ground disturbance and modification of
the hydrological system during construction activities related to closure of the former lined pond.
BIOSCREEN and BIOCHLOR models incorporating the most recent concentrations of groundwater
contaminants forecast that it will take approximately four years to reach peak concentrations. However,
at these peak concentrations, the groundwater at the compliance point (closest portion of Mill Creek to
WWMW-2) will not exceed the Permit standards and therefore do not require corrective action.
6.2 Conclusions
Natural attenuation at the Site is occurring and is evident from the trend evaluations described in
Section 4.3 and the BIOSCREEN and BIOCHLOR models described in Section 5. As modeled, the Site
COPCs will be below Permit standards at the compliance boundary (Mill Creek). In November 2019, the
Pond closure returned the Site to natural conditions (pre-CLRS) which allows infiltration of oxic
stormwater. Ground disturbance during construction temporarily caused an increase in some reported
COPCs. As noted in the Closure Report the source of the CURS constituents was removed and the
residual COPCs in soil will continue to naturally attenuate (EHS Support, 2020).
This Site is within the footprint of the Wright Chemical Corporation Superfund Site where several COPCs
were detected at much higher concentrations in upgradient and sidegradient groundwater. This
upgradient/sidegradient source of COPCs will continue to flux into the former CURS pond area until they
are attenuated before reaching Mill Creek. As WWMW-2 is now the most downgradient well, future
monitoring will continue to report COPCs from the upgradient sources.
Since the source of most of the Site impacts is from upgradient / sidegradient groundwater
contamination managed by the USEPA Region 4 superfund program, we recommend cessation of the
triennial sampling for the CLRS Permit. Three years of data since the closure of the pond support natural
attenuation is occurring as evidenced by the compliance boundary demonstration (Section 5).
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Comprehensive Site Assessment —Bakelite Acme
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References
7 References
Arcadis. 2012. Lined Pond Removal Action Completion Report, Momentive Specialty Chemicals Plant,
Riegelwood, North Carolina. March.
EHS Support. 2020. Lined Pond Closure Report. Hexion Acme, 333 Neils Eddy Rd., Acme North Carolina.
Prepared for Hexion, Inc. January.
J.M. Waller Associates, Inc. 2012. Final Pre -Remedial Investigation Report, Wright Chemical Corporation
Site, Riegelwood, Columbus County, North Carolina, NCD024766719. October.
McMahon, P.B., Chapelle, F.H. (2008). Redox Processes and Water Quality of Selected Principal Aquifers,
Ground Water, vol. 46(2), 259-271.
Shield Engineering, Inc. 2018. Final Remedial Investigation Report, Wright Chemical Site. EPA
ID#NCD024766719, Riegelwood, North Carolina. April.
USEPA. 1996. BIOSCREEN, Natural Attenuation Decision Support System - User's Manual, Version 1.3
(PDF). Publication No. EPA/600/R-96/087. August 1996
USEPA. 1997. BIOSCREEN Natural Attenuation Decision Support System, Version 1.4, by Newell, C. J.,
McLeod, R. K. and Gonzales, J. R., July 1997.
USEPA. 2002. BIOCHLOR Natural Attenuation Decision Support System, Version 2.2, by Aziz, C.E., Newell,
C. J., and Gonzales, J. R., March 2002.
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Table 1
Summary of Groundwater Field Parameters
Comprehensive Site Assessment
Bakelite Acme Facility - Acme, NC
Well ID
SAMPLE
TIME
DATE
DTW
TEMPERATURE
(degrees C)
pH (SU)
0.1 SU
Stabilization
Criteria
SPEC. COND.
(uhmos/cm)
5%
Stabilization
Criteria
DISSOLVED
OXYGEN
mg/L
ORP mV
APPEARANCE
SAMPLE
READING
(YES/NO)
Gallons
Purged
Notes
WWMW-01
1200
11/19/2014
9.86
17.13
8.27
7341
0.67
-397.00
YELLOW/CLOUDY/ODOR
YES
6
Sulfur odor while purging WWMW-01
WWMW-01
1030
3/24/2015
8.87
12.87
8.84
5318
1.23
-364.50
CLOUDY
YES
5
Sulfur odor while purging WWMW-01
WWMW-01
1430
7/23/2015
9.59
23.64
7.73
4818
0.30
-388.10
GRAY STAINING
YES
6.5
Sulfur odor while purging WWMW-01
WWMW-01
1020
11/12/2015
8.87
20.78
8.18
4858
3.25
-366.10
GRAY STAINING
YES
8
Sulfur odor while purging WWMW-01
WWMW-01
1430
11/24/2015
9.32
19.03
7.76
5787
0.90
-370.70
GRAY STAINING
YES
6
Sulfur odor while purging WWMW-01
WWMW-01
1100
3/8/2016
9.47
15.58
8.09
4441
1.30
-441.90
GRAY STAINING
YES
6
Sulfur odor while purging WWMW-01
WWMW-01
1030
7/19/2016
9.15
24.12
7.62
4690
2.82
-168.00
GRAY/CLOUDY
YES
6
Sulfur odor while purging WWMW-01
WWMW-01
1015
11/16/2016
9.72
20.14
7.96
4964
0.07
-349.70
GRAY/CLOUDY
YES
7
Sulfur odor while purging WWMW-01
WWMW-01
1015
3/9/2017
9.89
18.20
8.42
746.0
CLOUDY
YES
5
WWMW-01
930
7/6/2017
9.37
28.00
7.78
5200
CLOUDY
YES
5
WWMW-01
940
7/13/2017
9.60
25.30
7.81
4000
CLOUDY
YES
5
Resampled due to lab error in shipping.
WWMW-01
945
11/2/2017
7.68
22.03
8.80
4066
CLOUDY
YES
5.5
WWMW-01
1020
3/20/2018
9.89
18.60
7.78
4475
BLACK/CLOUDY
YES
5
WWMW-01
930
7/19/2018
9.55
29.10
7.88
4549
CLOUDY
YES
5
WWMW-01
1000
11/8/2018
8.87
21.60
7.89
6870
CLOUDY/ODOR
YES
5
WWMW-01
1020
3/13/2019
9.44
14.60
7.95
4800
CLOUDY/ODOR
YES
5
WWMW-01
945
7/24/2019
9.46
23.90
11.97
3370
CLOUDY/ODOR
YES
5
WWMW-01
900
11/6/2019
10.07
21.24
7.70
3801
CLOUDY
YES
4
WWMW-01
945
3/10/2020
9.72
16.60
7.72
4279
BLACK/ODOR
YES
4.5
WWMW-01
930
7/16/2020
9.80
26.10
7.27
4191
1
IBLACKJODOR
YES
4
WWMW-01
915
11/24/2020
9.64
18.70
6.17
2340
BLACK/ODOR
YES
4
WWMW-01
1015
3/17/2021
10.00
13.80
7.54
4080
BLACK/ODOR
YES
4
WWMW-01
1000
7/8/2021
10.13
22.80
7.42
6130
BLACK/ODOR
YES
4
WWMW-01
940
11/10/2021
10.54
21.20
7.47
721
BLACK/ODOR
YES
4.5
pH reading is from 3rd purge volume
WWMW-01
1015
3/9/2022
10.85
16.27
7.59
3995
BLACK/ODOR
YES
5
WWMW-01
945
7/13/2022
10.78
27.10
7.09
3852
--
--
BLACK/ODOR
YES
5
WWMW-01
930
11/2/2022
10.7
19.87
7.44
3536
--
--
BLACK/ODOR
YES
5
WWMW-01
920
3/8/2023
10.27
15.9
6.95
2646
BLACK/ODOR
YES
5
WWMW-02
1130
11/18/2014
7.92
18.02
6.34
720.0
3.35
17.90
CLEAR
YES
3.5
WWMW-02
1000
3/24/2015
6.33
13.51
5.62
370.0
7.33
100.90
CLEAR
YES
4.5
WWMW-02
1015
7/23/2015
7.08
24.43
5.74
575.0
1.74
138.50
CLEAR
YES
4
WWMW-02
945
11/12/2015
4.58
20.34
5.97
449.0
11.55
60.20
CLEAR
YES
5
WWMW-02
1400
11/24/2015
5.93
17.58
7.51
514.0
3A4
-24.60
CLEAR
YES
5
WWMW-02
1030
3/8/2016
5.93
15.06
6.65
267.0
7.31
9.00
CLEAR
YES
4.5
WWMW-02
1000
7/19/2016
6.51
25.30
6.69
449.0
3.71
66.00
CLEAR
YES
4.5
WWMW-02
930
11/16/2016
6.71
20.01
6.24
375.0
3.20
38.80
CLEAR
YES
4
WWMW-02
1000
3/9/2017
7.46
19.00
7.03
619.0
CLOUDY
YES
4
WWMW-02
910
7/6/2017
6.35
29.40
5.85
416.5
CLOUDY
YES
5
WWMW-02
920
7/13/2017
6.63
25.80
5.70
376.0
CLOUDY
YES
5
Resampled due to lab error in shipping.
WWMW-02
930
11/2/2017
6.55
21.94
7.26
419.0
CLOUDY
YES
5
WWMW-02
1000
3/20/2018
6.95
20.40
5.64
324.0
CLEAR
YES
5
WWMW-02
945
7/19/2018
6.84
27.50
6.07
326.6
CLOUDY
YES
4
WWMW-02
1015
11/8/2018
6.75
21.00
6.07
449.8
CLOUDY
YES
4
WWMW-02
925
3/13/2019
5.53
25.00
8.26
469.0
CLOUDY
YES
4
specific conductivity reading is from 3rd purge volume
WWMW-02
925
7/24/2019
6.75
25.00
8.26
800.0
CLOUDY
YES
4
specific conductivity reading is from 3rd purge volume
WWMW-02
930
11/6/2019
7.73
23.71
5.91
626.0
CLOUDY
YES
4
WWMW-02
930
3/10/2020
6.97
16.20
6.15
794.0
CLOUDY
YES
4
WWMW-02
900
7/16/2020
6.61
27.30
5.25
1256
CLEAR
YES
4
WWMW-02
900
11/24/2020
5.33
20.00
4.88
988.0
CLOUDY
YES
4
WWMW-02
1000
3/17/2021
6.43
13.20
4.73
1564
CLEAR
YES
3.5
WWMW-02
930
7/8/2021
7.50
24.30
5.58
549.0
CLEAR
YES
4.5
Purged dry
WWMW-02
920
11/10/2021
8.76
21.20
5.56
721.0
CLEAR
YES
3.5
Purged dry.
WWMW-02
955
3/9/2022
8.30
16.65
5.92
716.0
CLOUDY
YES
4.5
WWMW-02
1000
7/12/2022
8.82
27.20
6.21
1235
CLOUDY
YES
4.5
WWMW-02
945
11/2/2022
8.35
20.91
5.89
1147
CLOUDY
YES
4
WWMW-02
930
3/8/2023
7.35
13.7
6.39
596.0
CLOUDY
YES
5
WWMW-03
1015
7/12/2022
6.58
27.90
6.72
1812
CLOUDY/ODOR
YES
1
Purged dry after one reading.
WWMW-03
1000
11/2/2022
6.58
20.62
7.00
1569
--
--
CLOUDY
YES
2.5
WWMW-03
945
3/8/2023
6.1
23.6
6.85
1078
BLACK/CLOUDY
YES
3.5
Notes:
C = celsius
DTW = depth to water
mg/L = milligrams per liter
mV = millivolts
ORP =oxidation reduction potential
Spec Cond. = specific conductivity
SU = standard units
uhmos/cm = micromhos per centimeter
--= parameter not measured
%= percent
EHS W. Support
Page 1 of 1

.bk2
Summary of Groundwater 5amPlin Besul[s
Comprehensive Site Assessment
Bakelite Acme Facility - Acme, NC
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ism
IMF
Notes:
0=above a Permit Groundwater Standard
Bold=above. Permit Grwndwater5tand.Mor VOCdnat d
mgf—illigams Per liter
-dard un
NB=Not Detected s
ug/l =m cmgrams Per liter
VOC=wlatile organic compound
—= analyeai or no Permit Boundwater standaN
<=less Man reporting limit
EHS CO"- Support
Page 1 of 3

Summary of G—dwatet Sampling Results
Comprehensive Site Assessment
Bakelite Acme Facility- Acme, NC
®®®®®®®®®®®®®®®®®®®®®®®®®®®®®®®®®®®
®®®®®®®®®®®®®®®®®®®®®®®®®®®®®®®®®®®
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�e�ee��eee���eee�eeeeeeeeeeee��®�m��m�
�e�e���eee����eeeeeeeeeeeeeeeeeeeee�
e�e�e�eeee��eeeeeeeeeeeeeeeeeeeeee�
��a�a�aaaa��aaaaaaaaaaaaa�����������
�e�e�e�e�ee��eeeeeeeee�e�eeeeeeeeeeeee
Notes:
0 = above a Permit Gmoed.A, Raedard
Bold = above a Permit Groundwater Standard or VOC detected
mg/L = milligrams per liter
..- —dard oe
NB = Not Detected s
ug/l= icrograms per liter
-C =volatile organic compound
-= analyzedorno P,'kgrooedwarerstaedard
<=less than reporting limit
EHS Supporf
Page 2 of 3

Table 2
Summary of Groundwater Sampling Results
Comprehensive Site Assessment
Bakelite Acme Facility - Acme, NC
®®®
®®®
®�m�m
m��mm
®moo
��aaa
NONA
Notes:
0 =above a Permit Groundwater Standard
Bold =above a Permit Groundwater Standard or VOC detected
CSA = comprehensive site assessment
mg/L = milligams per liter
.. = standard units
ND- D..aed
ug/L = micrograms per liter
VOC = volatile organic compound
—= not analyzed or no Permit gmundwater standard
<=less than reporting limit
EHS V"- Support
Page 3 of 3

Comprehensive Site Assessment — Bakelite Acme
k7
Figures
EHS Support LLC

y
LEGEND z
U
U
Property Boundary U
C
Site (Former Lined Pond Area)
z
Y, s
e �
m
v
0 500 1,000 2,000
Service Layer Credits: USGS The National Map: National Boundaries Dataset, 3DEP Elevation Program, Geographic Names Information System, Scale in Feet I
C
v
x
Bakelite Synthetics s
EHS Support 333 Neils Eddy Road Topographic Location Map Figure 1 o"
Acme, NC. c
s

wwMw— 2 5
MILL CREEK
5�
1 —
wwmw— 3
LIVINGSTON CREEK
4.8 I
SCRUB
SCRUB ��—
�\`�
wwmw--7 MINIMUM 50' SETBACK
FROM TREATMENT/STORAGE UNIT
�I APPROXIMATE LOCATION
OF WATER WELL
SCRUB
\
o O WATER \\\ \\ \ J
TANK \ \ O/ ��/ / `
/ \ '
FIRE
K RAP
BLDG \-----------------4— --
o
C I ` ``' UB STA J G PIPE SUPPORTS
SCRUB
PACKAGING G AR
�/ / / /
D HEXAMINE WASTE` TK Ac NITS ' WHSE /
Q P WAREHOUSE
Ap REGEN TANK (LINE TANK ' o
(4) TKS O V PIPE SUPPORTS %
M I
/ WAST TE O END TANK
Op
R TANK / /'^> r PIPE PPORTS u
\ 3 ,000 GAL
\\ \ / / / / // / PIPE _U\PPDRY
O \
PRODUCTS
` \ HEXAMINE OPE SUPPORTS p
° I �
WAREHOUSE 35 \
q@ O
� O
® SCR BA LITE \ �j O \
S NTHETI
BOILER •SP /IAL
sc i/ / \\` UNIT 1. _ PR(CC TS
SC L
wo1\ O <
\ WE 24.7
SCRUB
(/ o
/ po
Cam) O \\
\ a
\\ \\ ® BROKEN /
\ N VEMENT/
`\� \ SCRUB SCRUB
O
D �
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�\ --- —30 \ k\
DUCK POND 11�
30
ENTEGRIS WHSE
HEXAMINE �,i
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00 O)E SUPPORTS
MONOFILL
70
`\emsIGN
I � o
0
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--- Q p O ICI
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o
0 4-
ADMIN
O \cq<F BLDG
35
p O
FLAGPOLE \ /LIGHT
W.
O C�
SC
\ SCRUB
� s\
SCRUB
SCR
_Vr
35
\\ SC
RUB
NOTES:
-WELL LOCATIONS ARE APPROXIMATE.
LEGEND:
wwMw-1
Q�
LINED POND MONITORING WELL
13�
EXISTING MONITORING WELL LOCATION
PROPERTY LINE
Q
APPROXIMATE FORMER LINED POND
PERIMETER
STRUCTURE
STREAM/WATER BODY
VEGETATION
MAJOR CONTOUR LINE
------------
MINOR CONTOUR LINE
x
FENCE
\ J \
O�SCO�L�\
4 \ \ \ \\ \ \ \ \ \
J 30
i
SCRUB
\ n r
OBSCURE
r40
l /
' SCRUB
OAK -BARK
KELITE
THETICS , ,
/OBSCUR
i
Sm
MAINTENANCE / 35
BLDG H
SCRUB
/
fn
PTIC TAN
AC UNITS FUE EPOT
REA
GRAPHIC SCALE - IN FEET
W/ LIGHT4p
i
NQ
0 100 200
—�/--\,
E H S
Support"
. •W/LIGHT�� /�
/
/ —J
IGH /
o �
b/
i
40 GN /
3S \'
SIG
0
BAKELITE SYNTHETICS MAIN ENTRANCE
333 NEILS EDDY ROAD
cR " ACME, N.C. 28456-9570
�� DODO � DODO
/5�
sc UB
REFERENCE: MACTEC drawing Figure 1 Site Map

Legend
WE
4.8 i
SCRUB
n
I
LL CREEK
Monitoring Well
/ `�-�' Approximate Ground Surface
Contours
Property Boundary
F Former Lined Pond
/O
I/O
/ SYSTEM
BUILDING
i
/ WWMW-02 \ I
�o
�'50*
20
/ 7)
III y,,-
• )iScale'ln Feet
50
•
X,
O
90
Current Site Conditions
Bakelite Synthetics
Acme, NC
E H S gol Support FIGURE 3

1
Legend
wwMw-01 $ Monitoring Well
i.(13.)—� 2 — Groundwater Flow Direction
Groundwater Contours (1 ft
1/0 intervals)
/ I SYSTEM _ Approximate Ground Surface
Contours
BUILDING —C— Property Boundary
OFormer Lined Pond
wV1►MW-02
/ (7.92)
�
\ \gyp
---��
{ \ \ WWMW- 3
(11.54);
Scale In Feet
Potentiometric Surface
July 2022
Bakelite Synthetics
Acme, NC
EHS Support FIGURE 4

\
1
I
I
I
I
1
1
a
1
(13 43)— —
1/O
SYSTEM
BUILDING
\ \\\ \?O
WWMW- 3
401
c�0 Legend
$ Monitoring Well
Groundwater Flow Direction
20
Groundwater Contours (1 ft
intervals)
_ Approximate Ground Surface
Contours
O�r Property Boundary
= Former Lined Pond
/0
0
V /
Potentiometric Surface
/ I August 2022
Bakelite Synthetics
Acme, NC
20 0 40 \�
Scale In Feet EHS 0 Support FIGURE 5

i ir
WWMW-01
(13.38)- —
i 1/O
II I t I SYSTEM
BUILDING
1 / / WW 1 -02
l I
Legend
$ Monitoring Well
2 — Groundwater Flow Direction
_ Groundwater Contours (1 ft
% intervals)
_ Approximate Ground Surface
Contours
O \
\ \ —Cr Property Boundary
\ O Former Lined Pond
\
\
�-,.j/'\
I �A
Scale In Feet
' I \
Potentiometric Surface
November 2022
Bakelite Synthetics
Acme, NC
EHS Support FIGURE 6

j �r
WWMW-01
ii (13.81)
i 1/O
II I t I SYSTEM
BUILDING
I
winrMw-02
I \ \ I I I
L� v/ � l I
Legend
$ Monitoring Well
2 — Groundwater Flow Direction
_ Groundwater Contours (1 ft
% intervals)
_ Approximate Ground Surface
Contours
O \
\ \ —Cr Property Boundary
\ O Former Lined Pond
?O /
WVHMW 031
(12. �)
/P\,
/ \ \_
/ \ \-------- J� / 401 20 0 40
Scale In Feet
Potentiometric Surface
March 2023
Bakelite Synthetics
Acme, NC
EHS �� SUppOYt FIGURE 7

60
50
40
a�
30
cr-
z
20
10
0
C�0
�N
�x
0
dJ
a—+
(B
L
r0
� Q
E
O
:D U
Comparatively Reducing
:Y1� [1111i [.�11�IIT11�1.Y1=Gild=c].�11E SIi11t �.�1'
1.1
1
.9
.8
_ .7
rn
E
v .6
Z3
5 .5
.4
.3
.2
.1
0
0 0
NH+ in fluid (mg/1)
Redox Ladder: 02 > NO3- > Mn(IV) > Fe(III) > So42-
❑ Comparatively Reducing
❑ ❑
A
1 2 3 4
Fe++ in fluid (mg/1)
1000
900
800
700
rn
E 600
cr-
❑ E 500
Iv
0
U)
400
300
200
100
5 6 0
<-O
In
Comparatively Reducing
AA
1 1 10
HS- in fluid (mgll) (as S--)
❑ WWMW-01
❑ WWMW-01
❑ WWMW-01
0 WWMW-02
0 WWMW-02
0 WWMW-02
A WWMW-03
❑ WWMW-03
WWMW-03
M
N
O
N
N
G
li
J
J
V)
Ln
2
w
✓= Indicator met
0
X = Indicator not met
Q
EHS ��i Support
Bakelite Synthetics Acme Plant
Acme, North Carolina
Cross plots of redox parameters WWMW-1 through WWMW-3 (July
2022 through March 2023)
Figure 8

1800 MW 04
1600
1400
1200
1000
E
600
i51
4_
-• X MW-29 Mixing vectors between
background groundwateror
precipitation and upgradient
groundwater
® I I I I I I
0 1
KMW-2
(upgradient)
2 3 4 5 6
Formaldehyde (mg/1)
2018 Remedial Investigation
(Sampled 3/2016)
❑ MW-04
0 MW-05
0 MW-05 DUP
A MW-06
0 MW-07
MW-08
M W-28
g M W-29
MW-ACE
■ WWMW-01
WWMW-02
r WWMW-02 DUP
KMW-02
Compliance Monitoring
(3/2016 to 11/2019 )
❑ WWMW-01
0 WWMW-02
Compliance Monitoring
(3/2020to 3/2023)
❑ WWMW-01
0 WWMW-02
A WWMW-03
H Below Reporting Limit
7 8
1400
11101114
1000
no
E
C
4J
0 800
z
0
a 600
400
200
0`
0
_ Mixing vectors between
background groundwater or
precipitation and upgradient
,r * MW-28
groundwr
w �
_
R ''
❑• a
ro
❑
�'C7
o
4�
❑
❑
}
�00------ -----------�
0
❑■
n
1800
1600
1400
1200
_-1000
0o
E
800
600
400
200
0�
0
500 1000 1500 2000 2500 3000
Total Dissolved Solids (mg/1)
I
■❑
Mixing vectors between
background groundwater or
precipitation and upgradient * -
groundwater m
❑x c
m
❑❑ ❑ ` ❑
c
.k
❑' ro
❑
r-� '
,�E I b o
va
---------------► MW-28
❑■
500 1000 1500 2000 2500 3000
Dissolved solids (mg/1)
2018 Remedial Investigation
(Sampled 3/2016)
© M W-04
0 M W-05
0 MW-05 DUP
A MW-06
Q M W-07
d M W-08
M W-28
g M W-29
MW-ACE
■ WWMW-01
WWMW-02
WWMW-02 DUP
V KMW-02
Compliance Monitoring
(3/2016 to 11/2019 )
El WWMW-01
0 WWMW-02
Compliance Monitoring
(3/2020to 3/2023)
El WWMW-01
0 WWMW-02
Q WWMW-03
F I Below Reporting Limit
2018 Remedial Investigation
(Sampled 3/2016)
❑ MW-04
0 MW-05
0 MW-05 DUP
IL MW-06
17 MW-07
MW-08
MW-28
g MW-29
MW-ACE
■ WWMW-01
WWMW-02
WWMW-02 DUP
KMW-02
Compliance Monitoring
(3/2016 to 11/2019
❑ WWMW-01
0 WWMW-02
Compliance Monitoring
(3/2020to 3/2023)
❑ WWMW-01
O WWMW-02
WWMW-03
<--- Below Reporting Limit
EHS V Support
Bakelite Synthetics Acme Plant
Acme, North Carolina
Cross plots of historical data for COPCs with increases at WWMW-1
and WWMW-2 compared to upgradient well data from 2016
Figure 9

7.5
fi_5
fi
5.5
2
CL
5
4.5
4
3.5
3 0 .1 .2 .3 .4 .5 .6 .7 .8 .9 1
Rxn progress
Input Parameter
Input Value
pH
7.09
Sulfide
22.5 mg/I
Eh (redox)
-0.48 V
Sodium
500 mg/I
Chloride
500 mg/I (charge balance)
1e20
H-
11
1e-20
1e-40
E
U)
a)
cI 1 e-60
m
CL
U)
m
0 1e-80
co
1e-100
1e-120
so-
1e-140 I I
0 .1 .2 .3 .4 .5 .6 .7 .8 .9 1
Rxn progress
Geochemists' Workbench Model: React oxygen with simplified WWMW-1
solution (based on 7/13/2022 sample) to observe pH change resulting from
sulfide oxidation. Sodium and chloride are added to mimic the approximately
1000 mg/I total dissolved solids in the sample. The initial sample is set at reducing
conditions to allow the measured sulfide to exist.
Result: Transition from sulfide to sulfate is accompanied by a sharp pH drop.
EHS V Support
Bakelite Synthetics Acme Plant
Acme, North Carolina
WWMW-1 Oxidation Model Results
Figure 10

2000
Sulfate
1600
1200
800
400
A
V_
0
�_A A
-1.4
V
• �°\�°,y��°\�°,y1�°\�°,y��°\�°,y0ti�'\�°,yOti�'\�°,y'yti�'\�°,y'L�'\�°•y'b "'\3
—Sulfate —Sulfate Std
12
Nitrate -Nitrogen
10
8
6
4
2
AA
MA
O.S.—
ti°may °p ti°p ti°!' °, ti°tip ti°tip ti°p ti°p ti°�° ti°�~ ti°�� ti°'p
\�ti\ \�ti\ \�ti\ \,�°\ \gyp\ \,Sp\ \,,gyp\ \�o,\ \10,\ \�o,\ \,�o,\
b\� 4", 4"
3 3 . . . 4 3 3 3 3 3 3
—Nitrate Nitrogen —Nitrogen Std
3000
Total Dissolved Solids (TDS)
2500
2000
1500
1000
500
0
oti� o''ti oti°` oy� oti� o''�' o''� oti° otiti oti�" oti�
b\,ti\'L\'Lti\'Lti\Y \'L°\'L\'Y\1.,6\ti�\'L,6\tip'\'1•,6\tip\L
—Total Dissolved Solids (TDS) —TDS Std
2,5ao
Ammonia -Nitrogen
2,000
1,500
1,000
500
0
°,5'1. °ti3 °,yb °yh °tip °tit °tip \�°tip °.y0 °,ti1 °.y'L oy'6
b\'~,,\3�\�, \3ti\�,y\'�ti 140" "\+ ,�\'1°\ "\+ "\3°'4111 '411\�4P 1.101
—Ammonia Nitrogen
—Ammonia Std 1.5 mg/L
-Linear (Ammonia Nitrogen)
9
Formaldehyde
8
7
6
5
4
3
2
1
0
b\\°y\'�ti\�°y\'�ti\�°y\'�ti\�°~\�ti\�° \�°\~° \'�°\V°y\'�°\tip\ry°ry\��\��'
� 3 3 3 3 3 3
—Formaldehyde — Formaldehyde Std
12
p H
11
10
9
8
7
6
5
4
°'y1' °'y'� °'1b °tih °y0 °y'1 °y0 °tip °.10 °.ti'y °.ti'L °.ti'6
\� 5\6,\� \S,\ti,5\�i,\� 5\'i'°\� \\ry '\'b°\ry'.\o'\� h\1°�\ti,y\-,C" ,6\-iC' ,6\ic",
_pH mph Min mph Max
EH5 Support Bakelite Synthetics Acme Plant Time Series Plots of Concentrations g
Acme, North Carolina
at WWMW-1 Figure 11

1800
Sulfate
1600
1400
1200
1000
800
600
400
200
0
1\y0yby\V 41 y\'P y\YOy� POyro O\�Oy1 O\"Oyu O\"Oy�i ��\O�O
b\ b\b \b b\3 5\h ,b\+ "' '.'0 "0 6\v
-Sulfate -Sulfate Std
80.0
70.0
Nitrate -Nitrogen
60.0
50.0
40.0
30.0
20.0
100
V.
0.0
oyy oyti oy� ayb oy�' oy�O oy� oy� oy�' otia otiy otiti
0y
-Nitrate Nitrogen -Nitrate Std -Linear (Nitrate Nitrogen)
1000
Total Dissolved Solids TDS
900
800
700
600
500
400
300
200
100
0
O,y Oy'L Oyu Oyb Oyu Oyu 01^ O,� OAS 01O oy'4 O•y'L Ory3
b\y\Y41y\L41y\Y41y\L4"y\L410\L,5\30\1 410\L,41O\L b\tip'\L3\tip'\L b\tip\L 5\tip'\Y
-Total Dissolved Solids (TDS) -TDS Std
400.0
76
Ammonia -Nitrogen
350.0
300.0
250.0
200.0
150.0
100.0
50.0
0.0
Oyy OyL OyS OSb Oyy Oyro OyA Dy'b Oyu Oy0 O�y O� , Oyy
bXy 3 3O
-Ammonia Nitrogen -Ammonia Std 1.5 mg/L
-Linear (Ammonia Nitrogen)
0
0.8A
Formaldehyde
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0
O�y Oyu O�� O,b O�y OyO O,� &11 O,CI
\'L'\'L,�\"�y\'L (L 5\3�,�\'�O\y,�\4\'L 'sp �\35\50\L
-Formaldehyde -Formaldehyde Std
10.00
pH
9.00
8.00
7.00
6.00
5.00
4.00
0 �\TOy'yy\T O\�OyrO o '�\ \ry0y1'y0I\V 'b\ O\V ��\ryOti ��KT �W, ��\,
Ob\ti\Vy'�y\Kp �4
'y\ ''0'S\ +�\ y\ y\ -,\
-pH -ph Min mph Max
EFis Su pCt Bakelite Synthetics Acme Plant Time Series Plots of Concentrations g
Acme, North Carolina
at WWMW-2 Fi ure 12

300
250
Sulfate
200
150
100
50
0
\�Otiti \�Otiti \�Otiti \�Otiti ti0�� `�Oti3
—Sulfate —Sulfate Std
12.00
Nitrate -Nitrogen
10.00
&.00
6.00
4.00
2.00
0.00
Off~ 00ry O�ry
03�
O�� O��
—Nitrate Nitrogen
Nitrate Std —Linear
(Nitrate Nitrogen)
600
Total Dissolved Solids (TDS)
500
400
300
200
100
0
ti
-Total Dissolved Solids (TDS) -TDS Std
400
350
Ammonia -Nitrogen
300
250
200
150
100
50
0
y\y�4 R\ti�L
-Ammonia Nitrogen -Ammonia Std 1.5 mg/L
-Linear (Ammonia Nitrogen)
D.7
Q.6
Formaldehyde
0.5
0.4
0.3
0.2
0.1
0
—Formaldehyde—Formaldehyde Std
9
8
7
pH
6
5
4
—pH —ph Min
—ph Max
EH5 Support Bakelite Synthetics Acme Plant Time Series Plots of Concentrations g
Acme, North Carolina
at WWMW-3 Figure 13

Input Parameters
BIOSCREEN Natural Attenuation Decision Support System
Air Force Center for Environmental Exceffence Version 1.4
t. HYDROGEOLOGY
Seepage Velocity*
Vs
210.0
(ft/yr)
or
- l or =_
Hydraulic Conductivity
K
1.0E-D3
(crn/sec)
Hydraulic Gradient
i
0.047
(11M)
Poros ilY
n
025
{
... ....................
2_ DISPERSION
Longitudinal Dispersivir
alpha
15.2
(ft)
Transverse DisperswW
alphay
i_5
{if)
Vertical DispersMty*
alpha
00
(ft)
or
= or
Estimated Plume Length
Lp
®(ft)
3. ADSORPTION
Retardation Factor"
R
1 ol( J
or
or
Soil Bulk Density
rho
1.7 (kg/l)
Partition Coefficient
Koc
14.3 (L/kg)
FractionOrganir-Carbon
foc
1.OE3 {)
......................„,,,,,,,,,,,,,,,„,,,,,,,,,,,,,,,„,,,,,,,,,,,,,,,„,,,,,,,,,,,
4. BIODEGRADATION
1st Order Decay Coeff'
lambda
6.9E-7 (per yr)
or
Solute Half -Life
1-half
-_ or
(year)
or or instantaneous Reaction Model
Delta Oxygen`
DO
1.65 (rng/L)
Delta Nitrate
NO3
0.7 (mg/L)
Observed Ferrous Iron*
Fe2+
16 6 (nrg/L)
Delta Sulfate*
SO4
22.4 (mg/L)
Observed Methane*
CH4
0.6 (nVIL)
5. GENERAL
Modeled Area Length*
Modeled Area Width`
Simulation Time*
450 (ft) } L
200 (ft) W
(yr) �
i Input Instructions:
115
1. Enter value dfrectfv ---- or
=_
2_ Calculate by filling in grey
p_02
cells below_ (To restore
formulas, hit button below)
Vanable
Data used directly in model_
1
Value calculated b model
y
Don't enter anv data)_
6. SOURCE DATA
Source Thickness in Set.Zone* 10 100 Vertical Piano Source_ Look at Plume Cross -Section
Source Zones- and Input Concentrations & Widths
Width* fl Conc. m 1L _ for Zones 11 2, and 3
a a
a a
19 1310 o e o ra ra ra ® ra
1 1
1 1
Source Halflife (see Help}:
(yr) View of Plume Looking Down
Inst. React. 1st Order.
................................
Mass{KgJ Observed Centerline Concentrations at Monitoring Wolfs
In FIELD DATA FORtC It No Data Leave Blank or Enter "U"
In Source e NAPL, Soil
OMPARISON
Concentration (mg/Q 1310.0 1 .0 534-0 .0 1 .0 1 .0 1 .0 .0 -0 0
Dist_ from Source (fl) 0 1 45 1 90 1 135 1 180 60
B. CHOOSE TYPE OF OUTPUT TO SEE:
RUN
CENTERLINE
View Output
RUN ARRAY
View Output
Model Output
DISSOLVED HYDROCARBON CONCENTRATION ALONG PLUME CENTERLINE (mglL at Lill)
Dislanee from Source (ff)
TYPE OF MODEL
0
45
90
135
180
225
270
315
360 405
450
No Degradation
1310.000
748.708
530.490
390.103
266.727
157 971
77.037
29.858
B.978 2.061
0.357
1st Order Decay
1310.000
748 708
530.490
390.103
266.727
157.971
77.037
29.858
t3.978 2.061
0.357
Inst. Reaction
1310.000
742.427
521.768
379.810
255.054
145.082
63.242
15.535
0.000 0.000
0.000
Field Data from Site
1310.000
534.000
1st
Order Decay
-P--Instantaneous Reaction
-E-No Degradation
.:
Field Data from Site
1400.000
12 00.000
01000.000
0.000
00.000
U400.000
200.000
0.000
Nelda Recalculate This 0
Sheet
Paste Example Dataset Calculate
Restore Formulas for Vs, Animation
❑ispersivities, R, lambda, other
50 100 150 200 250 300
Distance From Source (ft)
Time:
1 Years
350 400 450 500
Return to Recalculate This
EHS V Support
Bakelite Synthetics Acme Plant
Acme, North Carolina
BIOSCEEN calibration model input and output (TDS example)
Figure 14

Model Output
Input Parameters
BIOCHLOR Natural Attenuation Decision Support System
Version 2.2
Exce1200D
TYPE OF CHLORINATED SOLVENT:
Bakelite I Data Input Instructions:
Ammonia -Nitrate March 23 115 1 Enter value directiv....or
Run Name ^ or 2. Calculate by filling in gray
J0.02 cells. Press Enter then C1
4 Cyr) t L (To restore formulas• hit "Restore Formulas" button }
1. ADVECTION J Modeled Area Width' 200 (ft) W Variable- Data used directly in model
Seepage Velocity* W; 210 0 ("CModeled Area Length* 516 (ft) Test if Natural Attenuation
or :Zone 1 Length* 516 (ft) Biotransformatior Screening Protocol
Hydraulic Conductivity K 1.0E-03 (crtdsec) _Zane 2 Length' 0 (ft) Zone 2= 7 is Occurring
Hydraulic Gradient I (flIR) IL -Zone 1 Vertical Plane Source Determine Source Well
Effective Poros tv n 025 () ti SOURCE DATA TYPE Continuous
22.. DISPERSION 5 2 Gal
lax Source Options Single Planar
{ t}
Localion and Input Solvent Concentrations
(Npha y)1 {Alpha x}* 0.1 {-} Source Thickness in Sat. Zone 10 (ft}
(Alpha a)1 (Alpha x)' E-D2 (-} Y1
•••••••••••••••••••••••••••••••••••••••......•• J
3. ADSORPTION C Width` (ft) 19
Retardation Factor- R �*
or Conc. (mg/L)' C1 (lfyr)
Soil Bulk Dens ty, rho 1.7 (kg1L) PCE 496.E D
FractionOrganicCa bon, foc 1 OE-3 I-} TCE 04 0 View of Plume Looking Down
Partition Coefficient Koo 71 DGE 0
PCE E14
(Lfkg) 1.10 {-) VC 0 Observed Centerline Conc. at Monitoring Wells
TCE (Ukg) 1.10 {-} ETH
DCE (Lfkg) 1.10 {-)
VC (Ukg) 1.10 (-} 7. FIELD DATA FOR COMPARISON
ETH (Ukg) 1.1 (-) PCE Conc. (mglL) 4200 0 8.8 .0 .0 .0 .0 .0 .0 0 ❑
Common R (used in model)' = 1. 0 TCE Conic - (mg/L) 04 0 126 0 0 0 0 0 0 0 0
4. BIOTRANSFORMATION -1st Order Decay Coefficient' IDCE Conc. (mg/i .0 A .0 .0 .0 .0 .0 .0 A -0 ❑
Zone 7- (1lyr) half-life (vrs) Yield VC Conc. (mgi D-D 0 D 0 D 0 .0 .0 .0 -0 D
PCE TCE 11.550 F 0.06 3.60 ETH Conc. (mq/L)
TGE DCE 34.650 F 0.02 1.00 _far FnDm .ti_urce {ft) 0 50 9D 155 26D 250 300 350 46D 450 500
DCE VC 0.000 F 1.00 :Date Data Collected 2023
......... . ... ......... ......... ......... ......... ......... ......... ...... ...... ...... ...... ...... ....
ETH 0 oDa E 1 00 8 CHOOSE TYPE OF OUTPUT TO SEE
Zone � (lryr) halt -life (yrs) Restore
P(.:E TCE l0000
F Help Formulas RESET
TCE DCE F HE RUN CENTERLINE RUN ARRAY
L` E VC F SEE OUTPUT Example Unpratect
ETH F -
Ethenes
Ethanes I
5. GENERAL
Simulation Time'
Notes:
Although BIOCHLOR was programmed to model the degradation of
ammonia into nitrate, input and figures will still show the chlorinated
ethene labels. In these examples, ammonia was modeled as
tetrachloroethene (PCE) and nitrate was modeled as tricholoroethene (TICE).
Bakelite Synthetics Acme Plant
EHS �1 Support Acme, North Carolina
DISSOLVED CHLORINATED SOLVENT CONCENTRATIONS ALONG PLUME CENTERLINE (ni at Z=0
PCE
No Degradatior
Biotransformatior
Distance from Source ft
0
52
103
155
206
258
310
1 361
1 413
1 464
1 516
490.000
267.279
185.213
141.85-'
114.852
9E436
83.076
1 72926
1 64.907
1 58.315
1 52306
999.9998
E22122.435
4.669
0.568
0.073
0.010
0.001
1 0.000
1 0.000
1 0.000
1 0.000
Monitoring Well Locations (ft)
......... .........
0 50 90 155 200 250 300 350 400 450 500
................
Field Data from Site 490 000 0 000 8 800 0 000 0 000 0 000 0 000 1 0 000 1 0 000 1 0 000 1 0 000
-No Degradation/Production -Sequential 1st Order Decay .. Field Data from Site
100000D
" t 100.000
to
� 1 Q 000
O
0.100
b
=0 0010
U
0 001
0
Prepare Animation
100 200 300 400
Distance From Source {ft.)
516
500 600
See PCE
See TCE
See DCE
See VC
See ETH
Time:
4.0 Years Return to
To All To Array
Unpratect
Loki Sheet Input
DISSOLVED CHLORINATED SOLVENT CONCENTRATIONS ALONG PLUME CENTERLINE (mg/L) atZ=O
Distance from Source (ft)
TCE
No Degradation
Biotransformatior
0
52
103
155
206
258
310
361
413
464
510
0.040
0.022
0.015
0.012
0.D09
0.008
0.007
0.D06
0.005
0.0D5
0.004
0-0404
670:29
8.277
1.02a
0.131
0.018
0.a02
0.000
0-000
0.000
0.000
Monitorina Well Locations
........ ......... ...................
Feld Data from Site
-No Degradation/Production -Sequential 1st Order Decay o Field Data from Site
100.000
0.001 +
0
100 200 300 400
Distance From Source (ft.)
516
500 600
See PCE
See TCE
See DCE
See VC
See ETH
Time:
4-0 Years t Return o
Prepare Animation unprotect ReTo All To Array
Lo� Sheet Input
BIOCHLOR plume extent model input and output (ammonia/nitrate example) Figure 15

Comprehensive Site Assessment —Bakelite Acme
Appendix A WWMW-3 Boring Log and NCDEQ Well Construction
Record
EHS Support LLC

WELL CONSTRUCTION RECORD (GW-1)
1. Well Contractor Information:
John C. Schappell
Well Contractor Name
2332-A
NC Well Contractor Certification Number
M&W Drilling, LLC
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc)
3. Well Use (check well use):
Water Supply Well:
Geothermal (Heating/Cooling Supply)
Industrial/Commercial
Non -Water Supply Well:
Aquifer Recharge
Aquifer Storage and Recovery
Aquifer Test
Experimental Technology
Geothermal (Closed Loop)
Geothermal (Heating/Cooling
4. Date Well(s) Completed: 7/6/22
5a. Well Location:
Bakelite Synthetics
DMunicipal/Public
DResidential Water Supply (single)
DResidential Water Supply (shared)
0 Groundwater Remediation
EISalinity Barrier
DStormwater Drainage
DSubsidence Control
E] Tracer
DOther (explain under #21 Remarks
Well maWWMW-3
Facility/Owner Name Facility ID# (ifapplicable)
333 Neils Eddy Road, Riegelwood, NC 28456
Physical Address, City, and Zip
Columbus
County
Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(ifwell field, one lat/long is sufficient)
34019'36.73" N 78012'04.68"
6. Is(are) the well(s)Ex Permanent or DTemporary
14. WATER ZONES
FROM
TO
DESCRIPTION
ft.
ft.
ft.
ft.
15. OUTER CASING (for multi -cased wells) OR LINER (if a licable
FROM
TO
DIAMETER
THICKNESS
MATERIAL
ft.
ft.
in.
16. INNER CASING OR TUBING (geothermal closed -loop)
FROM
TO
DIAMETER
THICKNESS
MATERIAL
+4 1 ft.
5 ft.
2 h"
SCh 40
PVC
ft.
ft.
in.
17. SCREEN
FROM
TO
DIAMETER
SLOT SIZE
THICKNESS
MATERIAL
5 &
12 f -
2 in•
0.010
SCh 40
PVC
ft.
ft.
in.
18. GROUT
FROM
TO
MATERIAL
EMPLACEMENT METHOD & AMOUNT
0 ft.
1 ft.
Portland Cement
Pour
1 ft.
3 ft.
Bentonite Chips
Pour
ft.
ft.
19.SAND/GRAVEL PACK ifa licable
FROM
TO
MATERIAL
EMPLACEMENT METHOD
3 ft
12 ft
#2 Medium Sand
Pour
ft.
I ft.
20. DRILLING LOG attach additional sheets if necessary)
FROM
TO
DESCRIPTION color, hardness, soillrock type, grain size, etc.
0 ft.
1 ft.
Light brown -tan sand
1 ft
2 75 ft.
Brown sand
2.75 ft.
4.25 ft,
Blackish brown fine sand
4.25 ft
7 5 ft.
Blackish dark gray sand
7.5 ft-
15 ft•
Dark gray silt
ft.
ft.
ft.
ft.
21. REMARKS
22. V.n-W 7/26
Signature of Certified Well Cm tr ctor Date
7. Is this a repair to an existing well: E]Yes or !DNo
If this is a repair•, fill out known well construction information and explain the nature of the
repair under fi21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed -Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: 15 (ft.)
For multiple wells list all depths if different (example- 3@200' and 2@100')
10. Static water level below top of casing: (ft.)
If water level is above casing, use
11. Borehole diameter: 2
12. Well construction method: Direct Push
(i.e. auger, rotary, cable, direct push, etc.)
By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy ofthi.s record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Underground Injection Control Program,
FOR WATER SUPPLY WELLS ONLY: 1636 Mail Service Center, Raleigh, NC 27699-1636
13a. Yield (gpm) Method of test: 24c. For Water Supply & Iniection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
13b. Disinfection type: Amount: completion of well construction to the county health department of the county
where constructed.
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016

EHS %7 Support'
Boring ID: WWMW-3
C
Refer to Figure
U)
Project / Site: Bakelite Synthetics Acme Facility
Location / Address: 333 Neils Eddy Rd, Acme, INC
Date Started: 7/6/2022
Date Finished: 7/7/2022
Ground Surface Elevation (NAVD88): 14.02
Top of Casing Elevation (NAVD88): 18.12
INC State Plane Easting: 2240736.922 Northing: 211736.651
Total Depth: 15
Drilling Method: Hand auger / Direct Push
Borehole Diameter: 3.25-inch (in)
Rig Type: Geoprobe 7822DT
Casing Diameter / Type: 3.25-in DP Tooling
Client: Bakelite Synthetics
Drilling Company: MW Drilling
Sampler / Type: 1.25-in dia. Acetate Liner
(AL)
Project Number: REM C03536
Drilled by: Jason Bowelman
Logged by: S. Kloubec
EHS Support PM: A. Heitger
o
Q �,
o
Lithologic
a a)
'
Q
Q°
E
— �`
a
o w
w o
Description
0
o
Notes
WZ
JU
of
U)
0
14
13
0
1
��•`
:•:
Topsoil
Light brown -tan SAND (SP), moist, loose, poorly graded, fine
grained
0
0
- --
Hand cleared to 3 ft bgs; lithology logged and
PID readings collected from hand auger
cuttings
Brown SAND (SP), moist, loose, poorly graded, some
clay/silt, fine grained, trace gravel
- --
12
2
0
- --
36
- --
11
3
0
- --
::
Poor recovery from 3 to 10 ft bgs in initial
::
Blackish brown fine SAND (SP), moist, loose, poorly graded,
with silt
boring, offset boring and monitoring well —10
10
4
0
ft northeast
Blackish -dark gray SAND (SP), wet, loose to medium loose,
medium grained, with silt
9
5
0
Well Construction Details:
8
6
0
Stick-up protective casing with 2x2 ft pad
Grout 0 to 1 feet
Bentonite plug 1 to 3 ft bgs
7
7
0
::
Filter sand 3 to 12 ft bgs
Screened 5 to 12 ft bgs
33
Dark gray SILT (ML), moist, dense, with some fine sand,
6
8
trace clay
0
5
9
0
4
10
0
3
11
0
2
12
0
60
--------
1
13
0
--------
--------
Backfill from 12 to 15 ft bgs
0
14
0
----
-1
15
End of Boring at 15 ft bgs; WWMW-3 installed
- - ---
Notes: Boring: WWMW-3
Soil classification based on the Unified Soil Depth to water in borehole during drilling (ft bgs): 4.25
Classification System (USCS). Soil color Page: 1 of 1
classification based on Munsell Soil Color Charts. Depth to water in borehole after drilling (ft bTOC): 6.50 EHS Lr SU
61 pigt

Comprehensive Site Assessment —Bakelite Acme
L14h.4--ol-q
Appendix B Groundwater Sampling Field Sheets
EHS Support LLC

TRI-ANNUAL CLRS SAMPLING EVENT
BAKELITE ACME, NORTH CAROLINA
FIELD DATA RECORD
GROUND -WATER SAMPLING
WWM W-01
6228230003 Mar-23
WELL ID
PROJ. NUMBER DATE
WWM W-01
None
SAMPLE ID
QC SAMPLES I of �
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH TO 10.27
WATER
MEASURED
FT TOC WELL DEPTH
NA
CASING STICKUP NA WELL Pvc
FT TOC (FROM GROUND) FT MATERIAL
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL 2
FT(TOC DIAMETER IN
GENERAL INFORMATION
WEATHER: Sunny
AIR TEMP ff): 60oF
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS:
5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
935
945
955
920
MILITARY TIME
3/7/2023
3/7/2023
3/7/2023
3/8/2023
DATE
20.4
20.1
18.7
15.9
TEMPERATURE de reesC
pH Standard Units (SU)
6.88
6.90
6.92
6.95
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
2547
3104
3038
2646
5% Stabilization Criteria
BLACKIODOR
BLACKIODOR
BLACKIODOR
BLACKIODOR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration, sulfide, Dissolved Iron, Dissolved Manganese
NOTES:
Created by: WBM 3/20/2023

TRI-ANNUAL CLRS SAMPLING EVENT
" \'
BAKELITE ACME, NORTH CAROLINA
FIELD DATA RECORD
GROUND -WATER SAMPLING
W WM W-02
6228230003
Mar-23
WELL ID
PROJ. NUMBER DATE
WWM W-02
None
SAMPLE ID
QC SAMPLES
I of �
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH TO
WATER 735
MEASURED
FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL 2
FT(TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: Sunny
AIR TEMP ff): 60oF
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS:
5.0 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1010
1020
1030
930
MILITARY TIME
3/7/2023
3/7/2023
3/7/2023
3/8/2022
DATE
20.8
20.3
20.1
13.7
TEMPERATURE de reesC
pH Standard Units (SU)
5.65
5.41
5.33
6.39
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
791
596
306
596
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOD, Formaldehyde (8315), Phosphorus, 8260 low concentration, Dissolved Iron, Dissolved Manganese, SuRide
NOTES:
Created by: WBM 3/20/2023

TRI-ANNUAL CLRS SAMPLING EVENT
"
BAKELITE ACME, NORTH CAROLINA
I
FIELD DATA RECORD
GROUND -WATER SAMPLING
W W M W-03
6228230003
Mar-23
WELL ID
PROJ. NUMBER DATE
WWMW-03
None
SAMPLE ID
QC SAMPLES
t OF i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 6.10
MEASURED FT TOC WELL DEPTH
15
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF 5 bgs
SCREEN
BOTTOM OF
SCREEN
12 bgs
TUBING INTAKE SET NA WELL 2
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: Sunny
AIR TEMP ("F): 60°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS:
3.5 gallon purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1040
1050
1100
945
MILITARY TIME
3/7/2023
3/7/2023
3/7/2023
3/8/2022
DATE
TEMPERATURE de reesC
21.2
20.2
19.9
23.6
pH Standard Units (SU)
6.85
6.88
6.89
6.85
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
1434
1417
1426
1078
5% Stabilization Criteria
BLACK
BLACK
BLACK
BLACK/CLDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration, Sulfide, Dissolved Iron, Dissolved Manganese
NOTES:
Created by: WBM 3/20/2023

TRI-ANNUAL CLRS SAMPLING EVENT
"
BAKELITE ACME, NORTH CAROLINA
I
FIELD DATA RECORD
GROUND -WATER SAMPLING
W W M W-01
6228220017.00
Nov-22
WELL ID
PROJ. NUMBER DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 10.7
MEASURED
FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN I
TUBING INTAKE SET NA WELL 2
I I FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: Partly Cloudy
AIR TEMP ("F): 77°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1030
1040
1050
930
MILITARY TIME
11 /1 /2022
11 /1 /2022
11 /1 /2022
11 /2/2022
DATE
TEMPERATURE de reesC
21.33
21.20
21.27
19.87
pH Standard Units (SU)
7.30
7.36
7.38
7.44
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
3091
3130
3219
3536
5% Stabilization Criteria
BLACKIODOR
BLACKIODOR
BLACKIODOR
BLACKIODOR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration, sulfide, Dissolved Iron, Dissolved Manganese
NOTES:
Created by: WBM 7/14/2099

TRI-ANNUAL CLRS SAMPLING EVENT
"
BAKELITE ACME, NORTH CAROLINA
I
FIELD DATA RECORD
GROUND -WATER SAMPLING
W W M W-02
6228220017.00
Nov-22
WELL ID
PROJ. NUMBER DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 8.35
MEASURED FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN I
TUBING INTAKE SET NA WELL 2
I I FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: Partly Cloudy
AIR TEMP ("F): 77°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4.0 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1100
1110
1120
945
MILITARY TIME
11 /1 /2022
11 /1 /2022
11 /1 /2022
11 /2/2022
DATE
TEMPERATURE de reesC
22.83
22.94
22.92
20.91
pH Standard Units (SU)
5.61
5.68
5.93
5.89
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
1180
1127
1149
1147
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration, Dissolved Iron, Dissolved Manganese, Sulfide
NOTES:
Created by: WBM 7/14/2099

TRI-ANNUAL CLRS SAMPLING EVENT
"
BAKELITE ACME, NORTH CAROLINA
I
FIELD DATA RECORD
GROUND -WATER SAMPLING
W W M W-03
6228220017.00
Nov-22
WELL ID
PROJ. NUMBER DATE
WWMW-03
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 6.58
MEASURED FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN I
TUBING INTAKE SET NA WELL 2
I I FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: Partly Cloudy
AIR TEMP ("F): 77°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 2.5 gallon purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1130
1140
1000
MILITARY TIME
11/1/2022
11/1/2022
11/2/2022
DATE
TEMPERATURE de reesC
22.58
22.65
20.62
pH Standard Units (SU)
6.94
7.03
7.00
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
1773
1787
1569
5% Stabilization Criteria
CLOUDY
CLOUDY/BLACK
CLOUDY
APPEARANCE
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration, Sulfide, Dissolved Iron, Dissolved Manganese
NOTES: PURGED DRY AFTER TWO READINGS
Created by: WBM 7/14/2099

TRI-ANNUAL CLRS SAMPLING EVENT
BAKELITE ACME, NORTH CAROLINA
woo •
FIELD DATA RECORD
GROUND -WATER SAMPLING
WWMW-01
6228220017.00
J u 1-22
WELL ID
PROJ. NUMBER
DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
t OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 10.78
MEASURED
FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN I
TUBING INTAKE SET NA WELL
I I FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: Partly Cloudy
AIR TEMP ("F): 90°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1010
1020
1030
945
MILITARY TIME
7/12/2022
7/12/2022
7/12/2022
7/13/2022
DATE
TEMPERATURE de reesC
24.80
24.30
24.00
27.10
pH Standard Units (SU)
7.20
7.16
7.18
7.09
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
3437.0
3476.0
3549.0
3852.0
5% Stabilization Criteria
BLACKIODOR
BLACKIODOR
BLACKIODOR
BLACKIODOR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration, sulfide, Dissolved Iron, Dissolved Manganese
NOTES:
Created by: WBM 7/14/2022

TRI-ANNUAL CLRS SAMPLING EVENT
BAKELITE ACME, NORTH CAROLINA
wood.
FIELD DATA RECORD
GROUND -WATER SAMPLING
WWMW-02
6228220017.00
J u 1-22
WELL ID
PROJ. NUMBER
DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
t OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 8.82
MEASURED FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN I
TUBING INTAKE SET NA WELL
I I FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: Partly Cloudy
AIR TEMP ("F): 90°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4.5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1040
1050
1100
1000
MILITARY TIME
7/12/2022
7/12/2022
7/12/2022
7/13/2022
DATE
TEMPERATURE de reesC
27.00
25.10
24.50
27.20
pH Standard Units (SU)
6.13
6.05
6.09
6.21
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
968.0
1286.0
1309.0
1235.0
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration, Dissolved Iron, Dissolved Manganese, Sulfide
NOTES:
Created by: WBM 7/14/2022

TRI-ANNUAL CLRS SAMPLING EVENT
ACME, NORTH CAROLINA
wood.
FIELD DATA RECORD
GROUND -WATER SAMPLING
WWMW-03
6228220017.00
J u 1-22
WELL ID
PROJ. NUMBER DATE
WWMW-03
None
SAMPLE ID
QC SAMPLES
1 OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 6.58 MEASURED FT TOC WELL DEPTH
CASING STICKUP WELL
NA FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA BOTTOM OF NA
SCREEN SCREEN I
TUBING INTAKE SET NA WELL
I I FT TOC DIAMETER
2
IN
GENERAL INFORMATION WEATHER: Partly Cloudy
AIR TEMP ("F): 90°F
SAMPLES COLLECTED BY: WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 1
gallon purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1110
1015
MILITARY TIME
7/12/2022
7/13/2022
DATE
TEMPERATURE de reesC
27.40
27.90
pH Standard Units (SU)
6.75
6.72
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
1928.0
1812.0
5% Stabilization Criteria
BLACKIODOR
CLOUDY/ODOR
APPEARANCE
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration, Sulfide, Dissolved Iron, Dissolved Manganese
NOTES: PURGED DRY AFTER ONE READING
Created by: WBM 7/14/2022

TRI-ANNUAL CLRS SAMPLING EVENT
BAKELITE ACME, NORTH CAROLINA
woo •
FIELD DATA RECORD
GROUND -WATER SAMPLING
W W M W-01
6228220017.00
Mar-22
WELL ID
PROJ. NUMBER
DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
i OF i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 10.85
MEASURED FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN I
TUBING INTAKE SET NA WELL
I I FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: Partly Cloudy
AIR TEMP ("F): 60°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1040
1050
1100
1015
MILITARY TIME
3/8/2022
3/8/2022
3/8/2022
3/9/2022
DATE
TEMPERATURE de reesC
16.40
15.87
16.01
16.27
pH Standard Units (SU)
7.59
7.59
7.60
7.59
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
4165.0
4208.0
4137.0
3995.0
5% Stabilization Criteria
BLACKIODOR
BLACKIODOR
BLACKIODOR
BLACKIODOR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 3/13/2022

TRI-ANNUAL CLRS SAMPLING EVENT
BAKELITE ACME, NORTH CAROLINA
wood.
FIELD DATA RECORD
GROUND -WATER SAMPLING
W W M W-02
6228220017.00
Mar-22
WELL ID
PROJ. NUMBER
DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
i OF i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 8.30
MEASURED
FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN I
TUBING INTAKE SET NA WELL
I I FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: Partly Cloudy
AIR TEMP ("F): 60°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4.5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1010
1020
1030
955
MILITARY TIME
3/8/2022
3/8/2022
3/8/2022
3/9/2022
DATE
TEMPERATURE de reesC
17.71
17.11
17.14
16.65
pH Standard Units (SU)
6.18
5.97
6.22
5.92
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
1005.0
723.0
865.0
716.0
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 3/13/2022

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
woo •
FIELD DATA RECORD
GROUND -WATER SAMPLING
W W M W-01
6228210006
Nov-21
WELL ID
PROJ. NUMBER
DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
t OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 10.54
MEASURED FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN I
TUBING INTAKE SET NA WELL
I I FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: Partly Cloudy
AIR TEMP ("F): 60°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4.5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1000
1005
1010
940
MILITARY TIME
11/9/2021
11/9/2021
11/9/2021
11/10/2021
DATE
TEMPERATURE de reesC
20.60
20.20
20.30
21.20
pH Standard Units (SU)
7.41
7.44
7.47
5.56
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
4920.0
5990.0
4997.0
721.0
5% Stabilization Criteria
BLACKIODOR
BLACKIODOR
BLACKIODOR
BLACKIODOR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM1112112021

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
wood.
FIELD DATA RECORD
GROUND -WATER SAMPLING
W W M W-02
6228210006
Nov-21
WELL ID
PROJ. NUMBER
DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
t OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 8.76
MEASURED
FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN I
TUBING INTAKE SET NA WELL
I I FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: Partly Cloudy
AIR TEMP ("F): 60°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 3.5 gallons purged -purged dry
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
935
940
945
920
MILITARY TIME
11/9/2021
11/9/2021
11/9/2021
11/10/2021
DATE
TEMPERATURE de reesC
22.20
23.30
23.30
21.20
pH Standard Units (SU)
5.45
5.62
5.97
5.56
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
792.0
700.0
821.0
721.0
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLEAR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 1112112021

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
woo •
FIELD DATA RECORD
GROUND -WATER SAMPLING
WWMW-01
6228210006
J u 1-21
WELL ID
PROJ. NUMBER
DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
t OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 10.13
MEASURED FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: Sun
AIR TEMP ("F): 85°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS:
4.0 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
950
1000
1010
1000
MILITARY TIME
7/7/2021
7/7/2021
7/7/2021
7/8/2021
DATE
TEMPERATURE de reesC
22.10
22.80
22.90
22.80
pH Standard Units (SU)
7.31
7.34
7.38
7.42
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
1723.0
6040.0
6250.0
6130.0
5% Stabilization Criteria
BLACKIODOR
BLACKIODOR
BLACKIODOR
BLACKIODOR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 7/20/2021

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
wood.
FIELD DATA RECORD
GROUND -WATER SAMPLING
WWMW-02
6228210006
J u 1-21
WELL ID
PROJ. NUMBER
DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
t OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 7.50
MEASURED
FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: Sun
AIR TEMP ("F): 85°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS:
4.5 gallons purged -purged dry
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
920
930
940
930
MILITARY TIME
7/7/2021
7/7/2021
7/7/2021
7/8/2021
DATE
TEMPERATURE de reesC
24.00
23.20
23.00
24.30
pH Standard Units (SU)
5.38
5.03
5.34
5.58
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
1163.0
1188.0
1184.0
549.0
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLEAR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 7/20/2021

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
woo •
FIELD DATA RECORD
GROUND -WATER SAMPLING
W W M W-01
6228210006
Mar-21
WELL ID
PROJ. NUMBER
DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
i OF i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 1
FT TOC WELL DEPTH MEASURED NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: Sun
AIR TEMP ("F): 65°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4.0 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1040
1050
1100
1015
MILITARY TIME
3/16/2021
3/16/2021
3/16/2021
3/17/2021
DATE
TEMPERATURE de reesC
12.90
12.90
13.10
13.80
pH Standard Units (SU)
7.13
7.37
7.42
7.54
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
3313.0
4010.0
4098.0
4080.0
5% Stabilization Criteria
BLACKIODOR
BLACKIODOR
BLACKIODOR
BLACKIODOR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 3/20/2021

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
wood.
FIELD DATA RECORD
GROUND -WATER SAMPLING
W W M W-02
6228210006
Mar-21
WELL ID
PROJ. NUMBER
DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
i OF i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 6.43
MEASURED FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: Sun
AIR TEMP ("F): 65°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS:
3.5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1000
1010
1020
1000
MILITARY TIME
7/7/2021
7/7/2021
7/7/2021
7/8/2021
DATE
TEMPERATURE de reesC
14.21
14.30
14.50
13.20
pH Standard Units (SU)
4.34
4.52
4.49
4.73
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
1557.0
1491.0
1509.0
1564.0
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLEAR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 3/20/2021

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
woo •
FIELD DATA RECORD
GROUND -WATER SAMPLING
W W M W-01
6480200031
Nov-20
WELL ID
PROJ. NUMBER
DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
t OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 9.64
MEASURED
FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: Sun
AIR TEMP ("F): 65°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4.0 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1005
1010
1015
915
MILITARY TIME
11/23/2020
11/23/2020
11/23/2020
11/24/2020
DATE
TEMPERATURE de reesC
20.40
20.40
20.30
18.70
pH Standard Units (SU)
6.79
7.18
7.16
6.17
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
2791.0
4390.0
4400.0
2340.0
5% Stabilization Criteria
BLACKIODOR
BLACKIODOR
BLACKIODOR
BLACKIODOR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 1112512020

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
wood.
FIELD DATA RECORD
GROUND -WATER SAMPLING
W W M W-02
6480200031
Nov-20
WELL ID
PROJ. NUMBER
DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
t OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 5.33
MEASURED FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: Sun
AIR TEMP ("F): 65°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
945
950
955
900
MILITARY TIME
11/23/2020
11/23/2020
11/23/2020
11/24/2020
DATE
TEMPERATURE de reesC
20.70
20.80
21.20
20.00
pH Standard Units (SU)
4.25
4.08
4.27
4.88
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
855.0
719.0
771.0
988.0
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 1112512020

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
woo •
FIELD DATA RECORD
GROUND -WATER SAMPLING
WWMW-01
6480200031
J u 1-20
WELL ID
PROJ. NUMBER
DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
t OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 9.8
MEASURED FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: Sun
AIR TEMP ("F): 90°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4.0 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
945
950
955
930
MILITARY TIME
7/15/2020
7/15/2020
7/15/2020
7/16/2020
DATE
TEMPERATURE de reesC
24.30
23.60
23.50
26.10
pH Standard Units (SU)
7.20
7.28
7.31
7.27
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
3515.0
4433.0
4819.0
4191.0
5% Stabilization Criteria
BLACKIODOR
BLACKIODOR
BLACKIODOR
BLACKIODOR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 7/25/2020

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
wood.
FIELD DATA RECORD
GROUND -WATER SAMPLING
WWMW-02
6480200031
J u 1-20
WELL ID
PROJ. NUMBER
DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
t OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 6.61
MEASURED FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: Sun
AIR TEMP ("F): 65°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
915
925
935
900
MILITARY TIME
7/15/2020
7/15/2020
7/15/2020
7/16/2020
DATE
TEMPERATURE de reesC
25.10
24.70
24.40
27.30
pH Standard Units (SU)
4.73
4.66
4.65
5.25
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
1176.0
1261.0
1266.0
1256.0
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLEAR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 7/25/2020

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
woo •
FIELD DATA RECORD
GROUND -WATER SAMPLING
W W M W-01
6480200031
Mar-20
WELL ID
PROJ. NUMBER
DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
t OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 9.72
MEASURED
FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: Sun
AIR TEMP ("F): 60°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS:
4.5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1050
1100
1110
945
MILITARY TIME
3/9/2020
3/9/2020
3/9/2020
3/10/2020
DATE
TEMPERATURE de reesC
16.00
16.40
15.90
16.60
pH Standard Units (SU)
7.66
7.66
7.70
7.72
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
3588.0
4514.0
5540.0
4279.0
5% Stabilization Criteria
BLACKIODOR
BLACKIODOR
BLACKIODOR
BLACKIODOR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 3/15/2020

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
wood.
FIELD DATA RECORD
GROUND -WATER SAMPLING
W W M W-02
6480200031
Mar-20
WELL ID
PROJ. NUMBER
DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
t OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 6.97
MEASURED
FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: Sun
AIR TEMP ("F): 60°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS:
4 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1020
1030
1040
930
MILITARY TIME
3/9/2020
3/9/2020
3/9/2020
3/10/2020
DATE
TEMPERATURE de reesC
17.20
17.10
17.90
16.20
pH Standard Units (SU)
6.93
6.12
6.04
6.15
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
573.0
573.0
589.0
794.0
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 3/15/2020

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
woo •
FIELD DATA RECORD
GROUND -WATER SAMPLING
W W M W-01
6480199024
Nov-19
WELL ID
PROJ. NUMBER
DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
t OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 10.07
MEASURED FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: Sun
AIR TEMP ("F): 60°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4.0 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
930
935
940
900
MILITARY TIME
11 /5/2019
11 /5/2019
11 /5/2019
11 /6/2019
DATE
TEMPERATURE de reesC
22.37
22.64
22.67
21.24
pH Standard Units (SU)
7.58
7.65
7.67
7.70
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
3451.0
3660.0
3853.0
3801.0
5% Stabilization Criteria
BLACKIODOR
BLACKIODOR
BLACKIODOR
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 1111712019

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
wood.
FIELD DATA RECORD
GROUND -WATER SAMPLING
W W M W-02
6480199024
Nov-19
WELL ID
PROJ. NUMBER
DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
t OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 7.73
MEASURED
FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: Sun
AIR TEMP ("F): 60°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
950
955
1000
930
MILITARY TIME
11 /5/2019
11 /5/2019
11 /5/2019
11 /6/2019
DATE
TEMPERATURE de reesC
23.15
23.50
23.42
23.71
pH Standard Units (SU)
5.90
5.66
5.66
5.91
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
640.0
532.0
549.0
626.0
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 1111712019

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
woo •
FIELD DATA RECORD
GROUND -WATER SAMPLING
WWMW-01
6480199024
JUI-19
WELL ID
PROJ. NUMBER
DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
i OF i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 9.46
MEASURED
FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: PC
AIR TEMP ("F): 78°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 5.0 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1015
1025
1035
945
MILITARY TIME
7/23/2019
7/23/2019
7/23/2019
7/24/2019
DATE
TEMPERATURE de reesC
28.10
28.00
26.70
23.90
pH Standard Units (SU)
13.20
13.45
13.60
11.97
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
3658.0
3879.0
3889.0
3370.0
5% Stabilization Criteria
BLACKIODOR
BLACKIODOR
BLACKIODOR
CLOUDY/ODOR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 7/24/2019

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
wood.
FIELD DATA RECORD
GROUND -WATER SAMPLING
WWMW-02
6480199024
J U I-19
WELL ID
PROJ. NUMBER
DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
i OF i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 6.75
MEASURED
FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: PC
AIR TEMP ("F): 78°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
940
950
1000
925
MILITARY TIME
7/23/2019
7/23/2019
7/23/2019
7/24/2019
DATE
TEMPERATURE de reesC
29.50
28.10
29.60
25.00
pH Standard Units (SU)
5.49
6.07
6.47
8.26
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
679.0
787.0
800.0
8.2
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 7/24/2019

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
woo •
FIELD DATA RECORD
GROUND -WATER SAMPLING
WWMW-01
6480199024
Mar-19
WELL ID
PROJ. NUMBER
DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
i OF i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 9.44
MEASURED
FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: SUN
AIR TEMP ("F): 50°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 5.0 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1100
1110
1120
1020
MILITARY TIME
3/12/2019
3/12/2019
3/12/2019
3/13/2019
DATE
TEMPERATURE de reesC
15.20
15.60
15.10
14.60
pH Standard Units (SU)
7.95
8.03
7.95
7.95
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
4660.0
5070.0
4980.0
4800.0
5% Stabilization Criteria
BLACKIODOR
BLACKIODOR
CLOUDY/ODOR
CLOUDY/ODOR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 3/13/2019

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
wood.
FIELD DATA RECORD
GROUND -WATER SAMPLING
WWMW-02
6480199024
Mar-19
WELL ID
PROJ. NUMBER
DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
i OF i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 5.53
MEASURED FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: SUN
AIR TEMP ("F): 50oF
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1030
1040
1050
925
MILITARY TIME
3/12/2019
3/12/2019
3/12/2019
3/13/2019
DATE
TEMPERATURE de reesC
16.00
15.80
15.30
25.00
pH Standard Units (SU)
4.59
4.21
4.44
8.26
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
466.0
453.0
469.0
8.2
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 3/13/2019

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
woo •
FIELD DATA RECORD
GROUND -WATER SAMPLING
WWMW-01
6480188032
Nov-18
WELL ID
PROJ. NUMBER
DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
t OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 8.87
MEASURED FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: SUN
AIR TEMP ("F): 70oF
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 5.0 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1010
1015
1020
1000
MILITARY TIME
11 /7/2018
11 /7/2018
11 /7/2018
11 /8/2018
DATE
TEMPERATURE de reesC
23.30
22.40
21.80
21.60
pH Standard Units (SU)
7.94
7.90
7.93
7.89
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
6237.0
5487.0
6102.0
6870.0
5% Stabilization Criteria
BLACKIODOR
BLACKIODOR
CLOUDY/ODOR
CLOUDY/ODOR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 1111012018

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
wood.
FIELD DATA RECORD
GROUND -WATER SAMPLING
WWMW-02
6480188032
Nov-18
WELL ID
PROJ. NUMBER
DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
t OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 6.75
MEASURED FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: SUN
AIR TEMP ("F): 50oF
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1030
1040
1050
1015
MILITARY TIME
11 /7/2018
11 /7/2018
11 /7/2018
11 /8/2018
DATE
TEMPERATURE de reesC
24.10
23.60
23.20
21.00
pH Standard Units (SU)
6.62
5.68
5.58
6.07
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
374.9
262.2
311.2
449.8
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 1111012018

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
woo •
FIELD DATA RECORD
GROUND -WATER SAMPLING
WWMW-01
6480188032
JUI-18
WELL ID
PROJ. NUMBER
DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
t OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 9.55
MEASURED
FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: PC
AIR TEMP ("F): 80°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 5.0 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
950
1000
1010
930
MILITARY TIME
7/18/2018
7/18/2018
7/18/2018
7/19/2018
DATE
TEMPERATURE de reesC
25.10
24.30
24.20
29.10
pH Standard Units (SU)
7.94
7.91
7.97
7.88
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
4234.0
4359.0
4648.0
4549.0
5% Stabilization Criteria
BLACKIODOR
BLACKIODOR
CLOUDY/ODOR
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 7/20/2018

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
wood.
FIELD DATA RECORD
GROUND -WATER SAMPLING
WWMW-02
6480188032
JUI-18
WELL ID
PROJ. NUMBER
DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
t OF t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 6.84
MEASURED FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: PC
AIR TEMP ("F): 80oF
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1020
1030
1040
945
MILITARY TIME
7/18/2018
7/18/2018
7/18/2018
7/19/2018
DATE
TEMPERATURE de reesC
25.30
24.50
24.00
27.50
pH Standard Units (SU)
6.64
6.07
5.71
6.07
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
291.1
256.9
266.9
326.6
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 7/20/2018

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
woo •
FIELD DATA RECORD
GROUND -WATER SAMPLING
WWMW-01
6480188032
Mar-18
WELL ID
PROJ. NUMBER
DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
i OF i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 9.89
MEASURED
FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: PC
AIR TEMP ("F): 60oF
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 5.0 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1105
1110
1115
1020
MILITARY TIME
3/19/2018
3/19/2018
3/19/2018
3/20/2018
DATE
TEMPERATURE de reesC
14.80
15.10
15.20
18.60
pH Standard Units (SU)
7.78
7.87
7.87
7.78
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
3610.0
3987.0
4147.0
4475.0
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
BLACKICLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 3/20/2018

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
wood.
FIELD DATA RECORD
GROUND -WATER SAMPLING
WWMW-02
6480188032
Mar-18
WELL ID
PROJ. NUMBER
DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
i OF i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 6.95
MEASURED
FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL
FT TOC DIAMETER
2
IN
GENERAL INFORMATION
WEATHER: PC
AIR TEMP ("F): 80oF
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1045
1050
1055
1000
MILITARY TIME
3/19/2018
3/19/2018
3/19/2018
3/20/2018
DATE
TEMPERATURE de reesC
16.80
16.20
16.10
20.40
pH Standard Units (SU)
6.12
5.67
5.57
5.64
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
317.0
273.0
289.0
324.0
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLEAR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 3/20/2018

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
'.
FIELD DATA RECORD
amec
foster
GROUND -WATER SAMPLING
wheeler
W W M W-01
6550170001
Nov-17
WELL ID
PROJ. NUMBER DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
1 of t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
7.68
MEASURED
NA
CASING STICKUP WELL
NA
PVC
WATER
FT TOC WELL DEPTH
FT TOC (FROM GROUND) FT MATERIAL
TOP OF NA
BOTTOM OF
NA
TUBING INTAKE SET NA WELL 2
SCREEN
SCREEN
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: SUN
AIR TEMP ("F): 65°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 5.5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1005
1015
1025
945
MILITARY TIME
11 /1 /2017
11 /1 /2017
11 /1 /2017
11 /2/2017
DATE
21.94
22.03
21.91
22.03
TEMPERATURE de reesC
pH Standard Units (SU)
8.08
8.73
8.83
8.80
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
4750.0
4556.0
4466.0
4066.0
5% Stabilization Criteria
BLACKICLOUDY
CLOUDY
CLOUDY
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 11/03/2017

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
®'
FIELD DATA RECORD
aMec
foster
GROUND -WATER SAMPLING
wheeler
W W M W-02
6550170001
Nov-17
WELL ID
PROJ. NUMBER DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
1 of t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
6.55
MEASURED
NA
CASING STICKUP WELL
NA
PVC
WATER
FT TOC WELL DEPTH
FT TOC (FROM GROUND) FT MATERIAL
TOP OF NA
BOTTOM OF
NA
TUBING INTAKE SET NA WELL 2
SCREEN
SCREEN
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: SUN
AIR TEMP ("F): 65°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
935
945
955
930
MILITARY TIME
11 /1 /2017
11 /1 /2017
11 /1 /2017
11 /2/2017
DATE
21.88
21.92
21.93
21.94
TEMPERATURE de reesC
pH Standard Units (SU)
8.12
7.28
6.91
7.26
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
324.0
346.0
361.0
419.0
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 11/03/2017

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
®-V
FIELD DATA RECORD
aMeC
foster
GROUND -WATER SAMPLING
wheeler
WWMW-01
6550170001
J u 1-17
WELL ID
PROJ. NUMBER DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
1 of t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
9.37
MEASURED
NA
CASING STICKUP WELL
NA
PVC
WATER
FT TOC WELL DEPTH
FT TOC (FROM GROUND) FT MATERIAL
TOP OF NA
BOTTOM OF
NA
TUBING INTAKE SET NA WELL 2
SCREEN
SCREEN
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: SUN
AIR TEMP ("F): 90oF
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS:
5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1000
1005
1010
930
MILITARY TIME
7/5/2017
7/5/2017
7/5/2017
7/6/2017
DATE
26.30
25.60
25.20
28.00
TEMPERATURE de reesC
pH Standard Units (SU)
7.87
7.92
8.03
7.78
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
4879.0
5290.0
5730.0
5200.0
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 7/13/2017

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
FIELD DATA RECORD
amec
foster
GROUND -WATER SAMPLING
wheeler
WWMW-02
6550170001
J u 1-17
WELL ID
PROJ. NUMBER DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
1 of t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
6.35
MEASURED
NA
CASING STICKUP WELL
NA
PVC
WATER
FT TOC WELL DEPTH
FT TOC (FROM GROUND) FT MATERIAL
TOP OF NA
BOTTOM OF
NA
TUBING INTAKE SET NA WELL 2
SCREEN
SCREEN
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: SUN
AIR TEMP ("F): 90°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS:
5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
940
945
950
910
MILITARY TIME
7/5/2017
7/5/2017
7/5/2017
7/6/2017
DATE
25.90
25.60
24.10
29.40
TEMPERATURE de reesC
pH Standard Units (SU)
5.52
5.39
5.70
5.85
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
360.5
308.4
345.9
416.5
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 7/13/2017

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
'
FIELD DATA RECORD
amec
GROUND -WATER SAMPLING
foster
wheeler
WWMW-01
6550170001
J u 1-17
WELL ID
PROJ. NUMBER DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
1 of t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 9.6
MEASURED FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL 2
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: SUN
AIR TEMP ("F): 90oF
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
950
955
1000
940
MILITARY TIME
7/12/2017
7/12/2017
7/12/2017
7/13/2017
DATE
TEMPERATURE de reesC
24.80
23.40
23.40
25.30
pH Standard Units (SU)
7.71
7.46
7.92
7.81
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
5000.0
5000.0
5000.0
4000.0
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES: RESAMPLED DUE TO LAB ERROR
IN SHIPPING
Created by: WBM 7/13/2017

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
®�
FIELD DATA RECORD
amec
foster
GROUND -WATER SAMPLING
wheeler
WWMW-02
6550170001
Jul-17
WELL ID
PROJ. NUMBER DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
1 of t
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
6.63
MEASURED
NA
CASING STICKUP WELL
NA
PVC
WATER
FT TOC WELL DEPTH
FT TOC (FROM GROUND) FT MATERIAL
TOP OF NA
BOTTOM OF
NA
TUBING INTAKE SET NA WELL 2
SCREEN
SCREEN
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: SUN
AIR TEMP ("F): 90°F
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
930
935
940
920
MILITARY TIME
7/12/2017
7/12/2017
7/12/2017
7/13/2017
DATE
24.70
23.50
22.90
25.80
TEMPERATURE de reesC
pH Standard Units (SU)
5.92
5.57
5.57
5.70
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
341.0
380.0
383.0
376.0
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
RESAMPLED DUE TO LAB ERROR IN SHIPPING
Created by: WBM 7/13/2017

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
FIELD DATA RECORD
amec
foster
GROUND -WATER SAMPLING
wheeler
W W M W-01
6550170001
Mar-17
WELL ID
PROJ. NUMBER DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
9.89
MEASURED
NA
CASING STICKUP WELL
NA
PVC
WATER
FT TOC WELL DEPTH
FT TOC (FROM GROUND) FT MATERIAL
TOP OF NA
BOTTOM OF
NA
TUBING INTAKE SET NA WELL 2
SCREEN
SCREEN
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: PC
AIR TEMP ("F): 70oF
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS:
5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1315
1330
1345
1015
MILITARY TIME
3/8/2017
3/8/2017
3/8/2017
3/9/2017
DATE
20.70
19.30
19.10
18.20
TEMPERATURE de reesC
pH Standard Units (SU)
8.29
8.37
8.43
8.42
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
710.0
720.0
963.0
746.0
5% Stabilization Criteria
BLACKIODOR
BLACKIODOR
BLACKIODOR
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 3/30/2017

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
FIELD DATA RECORD
amec
foster
GROUND -WATER SAMPLING
wheeler
W W M W-02
6550170001
Mar-17
WELL ID
PROJ. NUMBER DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
7.46
MEASURED
NA
CASING STICKUP WELL
NA
PVC
WATER
FT TOC WELL DEPTH
FT TOC (FROM GROUND) FT MATERIAL
TOP OF NA
BOTTOM OF
NA
TUBING INTAKE SET NA WELL 2
SCREEN
SCREEN
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: PC
AIR TEMP ("F): 70oF
SAMPLES COLLECTED BY:
WBM
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS:
4 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1230
1245
1300
1000
MILITARY TIME
3/8/2017
3/8/2017
3/8/2017
3/9/2017
DATE
18.90
18.70
20.20
19.00
TEMPERATURE de reesC
pH Standard Units (SU)
6.67
6.44
6.16
7.03
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
593.0
626.0
651.0
619.0
5% Stabilization Criteria
CLOUDY
CLOUDY
CLOUDY
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
Created by: WBM 3/30/2017

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
®�
FIELD DATA RECORD
amec
GROUND -WATER SAMPLING
foster
wheeler
WWMW-01
6550160005
Nov-16
WELL ID
PROJ. NUMBER DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 9.72
MEASURED
FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN
TUBING INTAKE SET NA WELL 2
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: SUN
AIR TEMP ("F): 65°F
SAMPLES COLLECTED BY:
JJB
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 7 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1215
1225
1230
1015
MILITARY TIME
11 /15/2016
11 /15/2016
11 /15/2016
11 /16/2016
DATE
TEMPERATURE de reesC
21.10
21.24
21.15
20.14
pH Standard Units (SU)
7.85
7.93
7.99
7.96
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
5279.0
5867.0
5594.0
4964.0
5% Stabilization Criteria
0.25
0.40
0.22
0.07
DISSOLVED OXYGEN /L
-250.10
-372.40
-387.90
-349.70
ORP My
GRAY/CLOUDY
GRAY/CLOUDY
GRAY/CLOUDY
GRAY/CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
sulfer odor while purging WWMW-01

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
®�
FIELD DATA RECORD
amec
GROUND -WATER SAMPLING
foster
wheeler
W W M W-02
6550170001
Nov-16
WELL ID
PROJ. NUMBER DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 6.71
MEASURED
FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL 2
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: sun
AIR TEMP ("F): 65°F
SAMPLES COLLECTED BY:
JJB
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1150
1155
1200
930
MILITARY TIME
11 / 15/2016
11 /15/2016
11 /15/2016
11 /16/2016
DATE
TEMPERATURE de reesC
21.16
21.56
21.61
20.01
pH Standard Units (SU)
6.22
5.92
5.96
6.24
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
320.0
339.0
369.0
375.0
5% Stabilization Criteria
1.91
1.48
1.29
3.20
DISSOLVED OXYGEN /L
56.80
56.70
57.30
38.80
ORP My
CLOUDY
CLOUDY
CLEAR
CLEAR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
�.
FIELD DATA RECORD
amec
GROUND -WATER SAMPLING
foster
wheeler
WWMW-01
6550160005
Jul-16
WELL ID
PROJ. NUMBER DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 9.15
MEASURED FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN
TUBING INTAKE SET NA WELL 2
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: SUN
AIR TEMP ("F): 90oF
SAMPLES COLLECTED BY:
JJB
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 6 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1515
1520
1525
1030
MILITARY TIME
7/18/2016
7/18/2016
7/18/2016
7/19/2016
DATE
TEMPERATURE de reesC
23.60
23.38
23.28
24.12
pH Standard Units (SU)
7.45
7.90
8.02
7.62
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
5186.0
5228.0
5275.0
4690.0
5% Stabilization Criteria
0.93
0.71
0.66
2.82
DISSOLVED OXYGEN /L
20.50
-139.30
-224.00
-168.00
ORP My
GRAY/CLEAR
GRAY/CLEAR
GRAY/CLEAR
GRAY/CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
sulfer odor while purging WWMW-01

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
'
FIELD DATA RECORD
amec
GROUND -WATER SAMPLING
foster
wheeler
WWMW-02
6550170001
J U I-16
WELL ID
PROJ. NUMBER DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 6.51
MEASURED FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL 2
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: sun
AIR TEMP ("F): 90°F
SAMPLES COLLECTED BY:
JJB
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4.5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1440
1445
1450
1000
MILITARY TIME
7/18/2016
7/18/2016
7/18/2016
7/19/2016
DATE
TEMPERATURE de reesC
25.44
23.59
22.84
25.30
pH Standard Units (SU)
7.13
6.35
6.04
6.69
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
412.0
474.0
507.0
449.0
5% Stabilization Criteria
1.82
1.73
1.44
3.71
DISSOLVED OXYGEN /L
219.50
211.20
187.30
66.00
ORP My
CLOUDY
CLOUDY
CLEAR
CLEAR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
FIELD DATA RECORD
amec
GROUND -WATER SAMPLING
foster
wheeler
WWMW-01
6550160005
Mar-16
WELL ID
PROJ. NUMBER DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 9.47
MEASURED
FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL 2
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: SUN
AIR TEMP ("F): 55°F
SAMPLES COLLECTED BY:
JJB
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS:
6 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1455
1500
1505
1100
MILITARY TIME
3/7/2016
3/7/2016
3/7/2016
3/8/2016
DATE
TEMPERATURE de reesC
15.42
15.08
15.11
15.58
pH Standard Units (SU)
7.63
7.97
7.98
8.09
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
4440.0
4484.0
4609.0
4441.0
5% Stabilization Criteria
1.21
1.30
1.53
1.30
DISSOLVED OXYGEN /L
-314.10
-420.50
-422.10
-441.90
ORP My
GRAY STAINING
GRAY STAINING
GRAY STAINING
GRAY STAINING
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
sulfer odor while purging WWMW-01

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
FIELD DATA RECORD
amec
GROUND -WATER SAMPLING
foster
wheeler
W W M W-02
6550170001
Mar-16
WELL ID
PROJ. NUMBER DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 5.93
MEASURED
FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL 2
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: sun
AIR TEMP ("F): 55°F
SAMPLES COLLECTED BY:
JJB
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS:
4.5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1430
1435
1440
1030
MILITARY TIME
3/7/2016
3/7/2016
3/7/2016
3/8/2016
DATE
TEMPERATURE de reesC
15.66
15.79
15.92
15.06
pH Standard Units (SU)
6.65
6.05
5.91
6.65
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
232.0
235.0
262.0
267.0
5% Stabilization Criteria
4.21
3.37
2.78
7.31
DISSOLVED OXYGEN /L
13.00
22.20
14.60
9.00
ORP My
HAZY
CLOUDY
CLEAR
CLEAR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
'.
FIELD DATA RECORD
amec
GROUND -WATER SAMPLING
foster
wheeler
WWMW-01
6550150008
Nov-15
WELL ID
PROJ. NUMBER DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 8.87
MEASURED FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN
TUBING INTAKE SET NA WELL 2
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: SUN
AIR TEMP ("F): 65°F
SAMPLES COLLECTED BY:
JJB
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 8 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1320
1330
1340
1020
MILITARY TIME
11/11/2015
11/11/2015
11/11/2015
11/12/2015
DATE
TEMPERATURE de reesC
21.60
21.56
21.73
20.78
pH Standard Units (SU)
8.07
8.07
8.08
8.18
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
5185.0
5574.0
5917.0
4858.0
5% Stabilization Criteria
1.96
2.95
1.59
3.25
DISSOLVED OXYGEN /L
-365.10
-461.10
-414.60
-366.10
ORP My
GRAY STAINING
GRAY STAINING
GRAY STAINING
GRAY STAINING
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
sulfer odor while purging WWMW-01

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
FIELD DATA RECORD
amec
GROUND -WATER SAMPLING
foster
wheeler
W W M W-02
6550150008
Nov-15
WELL ID
PROJ. NUMBER DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 4.58
MEASURED FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL 2
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: sun
AIR TEMP ("F): 65°F
SAMPLES COLLECTED BY:
JJB
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1250
1300
1310
945
MILITARY TIME
11/11/2015
11/11/2015
11/11/2015
11/12/2015
DATE
TEMPERATURE de reesC
20.48
20.98
21.29
20.34
pH Standard Units (SU)
4.60
4.90
5.65
5.97
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
282.0
319.0
403.0
449.0
5% Stabilization Criteria
5.94
3.49
5.36
11.55
DISSOLVED OXYGEN /L
70.80
106.10
114.40
60.20
ORP My
CLOUDY
CLOUDY
CLOUDY
CLEAR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
®-V
FIELD DATA RECORD
aMeC
GROUND -WATER SAMPLING
foster
wheeler
WWMW-01
6550150008
Nov-15
WELL ID
PROJ. NUMBER DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 9.32
MEASURED
FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN
TUBING INTAKE SET NA WELL 2
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: SUN
AIR TEMP ("F): 40oF
SAMPLES COLLECTED BY:
JJB
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 6 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1055
1100
1105
1430
MILITARY TIME
11/23/2015
11/23/2015
11/23/2015
11/24/2015
DATE
TEMPERATURE de reesC
18.48
18.52
19.00
19.03
pH Standard Units (SU)
7.59
7.79
7.83
7.76
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
5219.0
5506.0
5665.0
5787.0
5% Stabilization Criteria
0.80
0.56
0.45
0.90
DISSOLVED OXYGEN /L
-331.70
-354.00
-364.10
-370.70
ORP My
GRAY STAINING
GRAY STAINING
GRAY STAINING
GRAY STAINING
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
sulfer odor while purging WWMW-01

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
®-
FIELD DATA RECORD
aMec
GROUND -WATER SAMPLING
foster
wheeler
W W M W-02
6550150008
Nov-15
WELL ID
PROJ. NUMBER DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 5.93
MEASURED
FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL 2
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: sun
AIR TEMP ("F): 40oF
SAMPLES COLLECTED BY:
JJB
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1035
1040
1045
1400
MILITARY TIME
11/23/2015
11/23/2015
11/23/2015
11/24/2015
DATE
TEMPERATURE de reesC
17.96
18.30
19.49
17.58
pH Standard Units (SU)
6.24
5.98
5.92
7.51
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
356.0
394.0
454.0
514.0
5% Stabilization Criteria
2.42
2.61
2.19
3.44
DISSOLVED OXYGEN /L
128.00
136.10
142.70
-24.60
ORP My
CLOUDY
CLEAR
CLEAR
CLEAR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
FIELD DATA RECORD
amec
GROUND -WATER SAMPLING
foster
wheeler
WWMW-01
6550150008
J u 1-15
WELL ID
PROJ. NUMBER DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 959
MEASURED
FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN
TUBING INTAKE SET NA WELL 2
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: SUN
AIR TEMP ("F): 95°F
SAMPLES COLLECTED BY:
JJB
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 6.5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1225
1235
1245
1430
MILITARY TIME
7/22/2015
7/22/2015
7/22/2015
7/23/2015
DATE
TEMPERATURE de reesC
22.90
22.54
22.78
23.64
pH Standard Units (SU)
7.79
7.78
7.76
7.73
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
4774.0
4869.0
4821.0
4818.0
5% Stabilization Criteria
0.15
0.39
0.27
0.30
DISSOLVED OXYGEN /L
-365.20
-382.00
-393.80
-388.10
ORP My
GRAY STAINING
GRAY STAINING
GRAY STAINING
GRAY STAINING
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
sulfer odor while purging WWMW-01

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
''
FIELD DATA RECORD
amec
GROUND -WATER SAMPLING
foster
wheeler
WWMW-02
6550150008
J u 1-15
WELL ID
PROJ. NUMBER DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 7.08
MEASURED FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL 2
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: sun
AIR TEMP ("F): 95°F
SAMPLES COLLECTED BY:
JJB
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1150
1200
1205
1015
MILITARY TIME
7/22/2015
7/22/2015
7/22/2015
7/23/2015
DATE
TEMPERATURE de reesC
23.64
22.22
21.99
24.43
pH Standard Units (SU)
5.79
5.67
5.82
5.74
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
523.0
562.0
620.0
575.0
5% Stabilization Criteria
1.73
1.59
4.45
1.74
DISSOLVED OXYGEN /L
135.30
131.80
128.10
138.50
ORP My
CLEAR
CLEAR
CLEAR
CLEAR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
®-
FIELD DATA RECORD
aMec
GROUND -WATER SAMPLING
foster
wheeler
WWMW-01
6550150008
Mar-15
WELL ID
PROJ. NUMBER DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 8.87
MEASURED FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN I
NA
TUBING INTAKE SET NA WELL 2
I I FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: CLOUDY
AIR TEMP ("F): 55°F
SAMPLES COLLECTED BY:
JJB
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1130
1030
MILITARY TIME
3/23/2015
3/23/2015
3/23/2015
3/24/2015
DATE
TEMPERATURE de reesC
13.50
13.41
13.26
12.87
pH Standard Units (SU)
7.44
8.07
8.31
8.84
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
5424.0
5519.0
5673.0
5318.0
5% Stabilization Criteria
0.60
0.35
0.64
1.23
DISSOLVED OXYGEN /L
-210.30
-335.90
-338.40
-364.50
ORP My
CLOUDY
BROWN
BROWN
CLOUDY
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
sulfer odor
while purging WWMW-01

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
'.
FIELD DATA RECORD
amec
GROUND -WATER SAMPLING
foster
wheeler
W W M W-02
6550150008
Mar-15
WELL ID
PROJ. NUMBER DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH TO 6.33
WATER
MEASURED
FT (TO C) WELL DEPTH
NA
CASING STICKUP NA WELL
FT (TOC) (FROM GROUND) FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL 2
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: sun
AIR TEMP ("F): 95°F
SAMPLES COLLECTED BY:
JJB
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 4.5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1130
1000
MILITARY TIME
3/23/2015
3/23/2015
3/23/2015
3/24/2015
DATE
TEMPERATURE de reesC
14.01
13.97
14.20
13.51
pH Standard Units (SU)
4.35
3.95
4.12
5.62
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
401.0
345.0
375.0
370.0
5% Stabilization Criteria
2.35
2.25
2.18
7.33
DISSOLVED OXYGEN mg/L
82.30
98.80
89.00
100.90
ORP My
CLOUDY/ORANGE
CLEAR
CLEAR
CLEAR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING (YES/NO)
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
FIELD DATA RECORD
amec
GROUND -WATER SAMPLING
foster
wheeler
W W M W-02
6550150008
Nov-14
WELL ID
PROJ. NUMBER DATE
WWMW-02
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 7.92
MEASURED
FT TOC WELL DEPTH
NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF
SCREEN
NA
TUBING INTAKE SET NA WELL 2
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: sun
AIR TEMP ("F): 40oF
SAMPLES COLLECTED BY:
JJB
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 3.5 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1245
1130
MILITARY TIME
11 / 18/2014
11 /18/2014
11 /18/2014
11 /18/2014
DATE
TEMPERATURE de reesC
20.04
19.58
20.14
18.02
pH Standard Units (SU)
6.18
6.08
6.15
6.34
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
667.0
706.0
735.0
720.00
5% Stabilization Criteria
1.66
1.82
2.26
3.35
DISSOLVED OXYGEN /L
20.80
27.10
22.00
17.90
ORP My
CLOUDY
CLEAR
CLEAR
CLEAR
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:

TRI-ANNUAL CLRS SAMPLING EVENT
HEXION ACME, NORTH CAROLINA
'
FIELD DATA RECORD
amec
GROUND -WATER SAMPLING
foster
wheeler
WWMW-01
6550150008
Nov-14
WELL ID
PROJ. NUMBER DATE
WWMW-01
None
SAMPLE ID
QC SAMPLES
I of i
WATER LEVEL / WELL DATA
PROTECTIVE
DEPTH
WATER 9.86
MEASURED
FT TOC WELL DEPTH NA
CASING STICKUP WELL
FT TOC (FROM GROUND) NA FT MATERIAL
PVC
TOP OF NA
SCREEN
BOTTOM OF NA
SCREEN
TUBING INTAKE SET NA WELL 2
FT TOC DIAMETER
IN
GENERAL INFORMATION
WEATHER: SUN
AIR TEMP ("F): 40oF
SAMPLES COLLECTED BY:
JJB
COMMENTS, FIELD CALIBRATIONS, INSTRUMENT PROBLEMS: 6 gallons purged
PURGE DATA
PURGE TIME ELAPSED
1 volume
2 volume
3 volume
Sample
1245
1200
MILITARY TIME
11 / 18/2014
11 /18/2014
11 /18/2014
11 /19/2014
DATE
TEMPERATURE de reesC
18.32
19.31
18.82
17.13
pH Standard Units (SU)
8.14
8.17
8.14
8.27
0.1 SU Stabilization Criteria
SPEC. COND. (uhmos/cm)
8240.0
8252.0
8162.0
7341.0
5% Stabilization Criteria
0.18
0.44
0.53
0.67
DISSOLVED OXYGEN /L
-341.60
-386.00
-390.80
-397.00
ORP My
DARKSTAINING
DARKSTAINING
DARK STAINING
YEuowiCLouDYi000R
APPEARANCE
NO
NO
NO
YES
SAMPLE READING YES/NO
PURGE METHOD: Bailer/YSI
ANALYSIS METHOD: TDS, Total Sulfate, Ammonia Nitrogen, Nitrate Nitrogen, TOC, Formaldehyde (8315), Phosphorus, 8260 low concentration
NOTES:
sulfer odor while purging WWMW-01

Comprehensive Site Assessment —Bakelite Acme
C14h.4--ol-q
Appendix C Laboratory Reports (2019 to 2023)
EHS Support LLC

envirochem
ANALYTICAL & CONSULTING CHEMISTS
EHS Support, LLC
4885 McKnight Road, Suite 188
Pittsburgh PA 15237
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Mar 21, 2022
Customer PO #:
Customer ID: 19090024
Report #: 2022-04138
Project ID: Bakelite
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-09873 Site: WWMW-1 3/7/2022 3:00 PM Water client
Test Method Results Date Analyzed
Sulfate EPA 300.0, Rev. 2.1,1993 838 mg/L 03/10/2022
Total Dissolved Solids (TDS) SM 2540 C-2015 1450 mg/L 03/08/2022
pH SM 4500 H B-2011 7.4 units 03/14/2022
Result estimated. Analyzed out of 15 minutes hold time.
Ammonia Nitrogen
SM 4500 NH3 C-2011
624 mg/L
03/09/2022
Total Phosphorus
SM 4500 P (F-H)-2011
0.48 mg/L
03/14/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
77.5 mg/L
03/11 /2022
Formaldehyde
SW846 8315A
<500 pg/L
03/09/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.07 mg/L
03/08/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0,1993
0.17 mg/L
03/10/2022
Nitrate Nitrogen
Subtraction Method
0.10 mg/L
03/18/2022
Report #:: 2022-04138 Page 1 of 3

[envirrochem
ANALYTICAL & CONSULTING CHEMISTS
EHS Support, LLC
4885 McKnight Road, Suite 188
Pittsburgh PA 15237
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info Cenvironmentalchemists.com
Date of Report: Mar 21, 2022
Customer PO #:
Customer ID: 19090024
Report #: 2022-04138
Project ID: Bakelite
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-09874 Site: WWMW-2 3/7/2022 2:20 PM Water client
Test Method Results Date Analyzed
Sulfate EPA 300.0, Rev. 2.1,1993 213 mg/L 03/10/2022
Total Dissolved Solids (TDS) SM 2540 C-2015 555 mg/L 03/08/2022
pH SM 4500 H B-2011 6.0 units 03/14/2022
Result estimated. Analyzed out of 15 minutes hold time.
Ammonia Nitrogen SM 4500 NH3 C-2011
22.7 mg/L
03/09/2022
Total Phosphorus SM 4500 P (F-H)-2011
0.06 mg/L
03/17/2022
Total Organic Carbon (TOC) SM 5310 B-2014
5.4 mg/L
03/11/2022
Formaldehyde SW846 8315A
<50 pg/L
03/09/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 0.09 mg/L 03/08/2022
Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0,1993 26.4 mg/L 03/11/2022
Nitrate Nitrogen Subtraction Method 26.3 mg/L 03/18/2022
Report #:: 2022-04138 Page 2 of 3

[en7virocheml
ANALYTICAL & CONSULTING CHEMISTS
EHS Support, LLC
4885 McKnight Road, Suite 188
Pittsburgh PA 15237
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Mar 21, 2022
Customer PO M
Customer ID: 19090024
Report #: 2022-04138
Project ID: Bakelite
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-09875 Site: DUP01 3/7/2022 Water client
Test Method Results Date Analyzed
Sulfate EPA 300.0, Rev. 2.1,1993 894 mg/L 03/10/2022
Total Dissolved Solids (TDS) SM 2540 C-2015 1400 mg/L 03/08/2022
pH SM 4500 H B-2011 7.4 units 03/14/2022
Result estimated. Analyzed out of 15 minutes hold time.
Ammonia Nitrogen
SM 4500 NH3 C-2011
680 mg/L
03/09/2022
Total Phosphorus
SM 4500 P (F-H)-2011
2.46 mg/L
03/14/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
68.2 mg/L
03/14/2022
Formaldehyde
Sw846 8315A
<500 pg/L
03/09/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.14 mg/L
03/08/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.31 mg/L
03/10/2022
Nitrate Nitrogen
Subtraction Method
0.17 mg/L
03/18/2022
Comment:
►n , ...n.�
N). � r, , 11 ,
Reviewed by:
Report #:: 2022-04138 Page 3 of 3

Analytical Environmental Services, Inc
Date: 16-Mar-22
Client:
Environmental Chemists, Inc.
Client Sample ID:
#9873
Project Name:
2022-4138
Collection Date:
3/7/2022 3:00:00 PM
Lab ID:
2203A26-001
Matrix:
Aqueous
Analyses xepornng Dilution
Y Result Limit Qual Units BatchID Factor Date Analyzed Analyst
Formaldehyde by SW8315A
Formaldehyde
Qualifier: • Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
BRL 500 tig/L 332238 1 03/09/202218:17 TO
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit
22 — 04
� Page 4 of 10

Analytical Environmental Services, Inc
Date: 16-Mar-22
Client:
Environmental Chemists, Inc.
Client Sample ID:
#9874
Project Name:
2022-4138
Collection Date:
3/7/2022 2:20:00 PM
Lab ID:
2203A26-002
Matrix:
Aqueous
Analyses Result nepurcmg Dilution
Qua] Units BatchID Date Analyzed Analyst
Limit Factor
Formaldehyde by SW8315A
Formaldehyde BRL 50 ug/L 332238 1 03/09/202218:28 TO
Qualifiers: • Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
1 Estimated value detected below Reporting Limit
Page 5 of 10

Analytical Environmental Services, Inc
Date: 16-Mar-22
Client:
Environmental Chemists, Inc.
Client Sample ID:
#9875 (DUP)
Project Name:
2022-4138
Collection Date:
3/7/2022 2:20:00 PM
Lab ID:
2203A26-003
Matrix:
Aqueous
Analyses xeporang Dilution
Y Result Limit Qua] Units BatchlD Factor Date Analyzed Analyst
Formaldehyde by SW8315A
Formaldehyde BRL 500 ug/L 332238 1 03/09/202218:39 TO
Qualifiers: • Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysts exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantitation range)
S spike Recovery outside limits due to matrix
Nair See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit
Page 6 of 10

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
Sample Receipt Checklist 910.392.0223
Client: [—�
`
Date:
ReportNumber: _ 2022- q (3(0�-
Receipt of sample:
❑ YES ❑ NO
ECHEM Pickup ❑ Client Delivery UPS ❑ Fe
❑ Other El❑ N/A
❑ YES ❑ NO
1. Were custody seals present on the cooler?
❑ N/A
Original temperature upon
2. If custody seals were present, were they intact/unbroken?
receipt. °C
.0
How temperature taken: ❑ Temperature BlaCorrected temperature upon receipt °C
nk
Against Bottles
IR Gun ID: Thomas Traceable S/N: 210835468 IR Gun Correction Factor °C:
❑ YES ❑ NO
0.0
3. If temperature of cooler exceeded 6°C,
YES ❑ NO
YES
was Project Mgr./QA notified?
4. Were proper custody procedures (relinquished/received)
El NO
followed?
5. Were sample ID's listed on the COC?
YES ❑ NO
YES ❑
6. Were samples ID's listed on sample containers?
NO
YES ❑
7. Were collection date and time listed on the COC?
NO
YES ❑
8. Were tests to be performed listed on the COC?
NO
YES ❑ f;Ci
9. Did samples arrive in proper containers for each test?
i FYJ rrs lu NO
10. Did samples arrive in good condition for each test?
YES ❑ NO
11 �A/?s adequate sample volume availab!e?'
YES ❑ NO
12. Were samples received within proper holding time for requested tests?
❑ YES ❑
13. Were acid preserved samples received at a pH of <2?
NO
YES ❑
14. Were cyanide samples received at a pH >12?
NO
YES ❑
15. Were sulfide samples received at a pH >9?
NO
❑ YES ❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L?
❑ YES ❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
**
Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
(Must be completed for any sample(s) incorrectly y preserved
by adding (circle one):
or with headspace)
were received incorrectly preserved and were adjusted accordingly
H2504 HNO3
Time of preservation:
HCI NaOH
If more than one preservative is needed, notate in comments below
,Vote: Notify customer service immediately for incorrectly
preserved samples. Obtain a new sample or
notify the state lab if directed to ana''yzed by the customer. who was notified, date and time:
Volatiles Sample(s)
were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

0 M
<
tD
fD
CL 0
N W 9
72
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8
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G)
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n
n
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rnGrabe
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(P or G)
Chlorine
0
mg/L
CD
pH of bottle
fD
LAB ID
NUMBER
NONE
HCL
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H2SO4
m
N
HNO3
M
CD
NAOH
D
N
THIO
a
W
FILTERED
Z
OTHER
a
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Environmental Chemists, Inc.
71O c>,,t s,-�rt,,)wn Road, eta -4e(,, NC_ ') }2-� - 252. 72._5 02 E - 'F x
2';'-.,-A Wilmington Highway , Jacksonville, NC 285,40 - 910 47 581"! Lab,/Fax
ANALYTICAL & CONSULTINGCHEMISTS
Test
Method
Results
Date Analyzed
Sulfate
EPA 300,0
120 rng/L
07/26/2019
Total Dissolved Solids (T[
2548 C
376 mg/L
07/2/019
Ammonia Nitrogen
Sid4500NH3 C
468 mg/L
08/01/2019
Total Phosphorus
SM 4500 P F
2.0 mg/L
07/31/2019
Total Organic Carbon T
Sty 5318 B
60. mg/L
07/26/2019
1;11,2-Ttr l ro tha to
SIN 846 meth 82C-OB;50 0B
< /L
07/29/201
1, 1, 1 -Trichloroethane
SW 846 method 8260W5030
<2 leg/L
07/29/2019
1, 1,2,2-Tetrachloroethane
Sri 846 method 8260B/5030B
< leg/L
07/29/2019
1 ;1 ,2- i rinhloro th n
SW 846 method 260BI5636B
<g/L
7 t291201
1,1-Dichloroethane
SW 846 method 8260B/5030B
<2 /L
07/29/2019
1,1-1 lohloro th n
SW 846 mp�th 8260B,5030B
<:9- g/L
07/29/2019
1,1-Diohloroprop ne
SW 846 method 200Bt5030
<2 /L
07/29/2019
1,2,3-Tri hlorob nz n
V 846 method 828 B/5030
<2 g/L
07/29/2019
1,2,3-Trichloropropane
SW 846 method 826OB/5030B
<2 Ig/L
07/29/2019
1,2, - T richlorobenzene
SW 846 method 8260B15030B
<2 /L
07/29/ 019
1,2,4-Trim th lb nzen
SVV 846 method 82668t5030B
<2 pg/L
07/291 0 1
1,2-Dibromo-3-Chloropropane
SW 846 method 8260815030E
<2 p /L
07/29/2019
12- ibromo th n
SW 846 method 826OB15030B
<2 gig/L
07/29/2019
1,2-Dichlorobenzene
SW 846 method 8260B,15030B
<2 pg/L
07/ 9/ 019
1, -1 iohloro th n
SW 846 method 8260BA5030B
<2 Ig1L
07/29/2019
1,2-Dichloropropane
SW 846 method 8260B/5030B
<2 p /L
07/29/2019
1, 3,5-Trimethylbenzene
:SW 846 method 8260B/5030B
<2 /L
07/29/201
1,3-Dichlorobenzene
SW 8A8 method 820Be 030B
<2 g/L
07/29/2019
1,3-Dichloropropane
SW 846 method 8260B/5030B
< /L
07/29/2019
1,4-Dichlorobenzene
SW 846 method 8260B; 030B
<2 idg/L
07/29/201
2,2-Dichloropropane
SW 846 method 8260B/5030B
<2 /L
07/29/2019
Burt f#:: 201 -12031
Page ; of 6

A Y` €1CAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602) 'Winc mfl f a,, Wilmington, NC 28W, * 910.392, 223 Lab - 910,392 '424 Fax
710 Bowsertown Road, Mant c> NC 279;4 o 2-52.4 3 ~ [22 Lab/Fax
2-5A ; fli inn -ton t-sighw v ,act o , iile, NC 25540
its[ ei, r- it nnient ici miste.cornn
Wood -AMEC
Date of Report: Aug 07, 2019
5710 Oleander Drive , Suite 110
Customer 1992
Wilmington 28405
Customer ; 11719
Attention: Bey Moore
Report: 2 19-12 21
Project . Hexion CLRS
2-Chlorotoluene
SW 846 method 8260B/5034B
<2 pg/L
07/29/2019
4-Chlorotoluene
SW 846 method 8260B/50308
<2 g/L
07/29/2019
Benzene
SW 846 method 826OB/5030B
<2 pg/L
7/29/2019
Bromobenzene
SW 846 method 826OB/5030B
<2 pg/L
07/29/2019
rom lorom th � to
Sof 846 method 82 OB/50 08
<2 pg/L7/2
/ 1
Bromodichloromethane
SW 846 method 82 OB15030
<2 g/L
07/29/2019
Bromoform
SW 846 method 8260BI5030B
<2 pg/L
07/29/2019
Bromomethane
SW 846 method 8260B/5030
<2 gg/L
07/29/2019
Carbon tetrachloride
SW 846 method 260B15030
<2 g/L
07/29/2019
Chlorobenzene
SW 846 method 826OB/5030B
<2 g/L
7/L9/2919
Chloroethane
SW 846 method 8260B/5030B
<2 gtL
07/29/2019
Chloroform
SW 846 method 8260B/5030B
<2 g/L
19
07/29/2019
Chloromethane
SW 846 method 8260B/ 030
<2 g/L
07/29/2019
cis- 1,2-Dichloroethene
SW 846 method 826OB15030B
<2 pg/L
07/29/2019
19
cis- 1,3-Dichl r prop rt
SW 846 method 8260B/5030
<2 fag/L
07/29/2019
Dibromochloromethane
SW 846 method 82605030B
<2 g/L
07/29/2019
Dibromomethane
SW 846 method 8260B/5030
<2 g/L
07/29/2019
Dichlorodifluoromethane
SW 846 method 826OB/5030B
<2 pg/L
07/29/2019
Elthylbenzene
SW 846 method 826OB/5030B
<2 g/L
07/29/2019
Hexachlorobutadiene
SW 846 method 8260B/5030B
<2 g/L
07/29/2019
1 sopropylb zen
SW 846 method 260 /5030B
<2 /L
07/29/2019
M+P Xylene
SW 846 method 826OB/5030B
< rL
07/29/2019
Methylene chloride
SW 846 method 82606/5030B
<2 /L
7/29/2019
Naphthalene
SW 846 method 826OB/5030B
<2 g/L
07/29/2019
n-Butylbenzene
SW 846 method 826OB/5030B
<2 p /L
7/29/2019
n-Propylbenzene
SW 846 method 8260B/5030B
<2 g/L
07/29/2019
ortho-Xylene
SW 846 method 8260B15030B
<2 pg/L
07/29/2019
p-lsopropyltoluene
SW 846 method 8256B15030B
<2 pg/L
r /2912t 19
sec-Butylbenzene
SW 846 method 826OB/5030B
<2 leg/L
07/29/2019
Styrene
SW 846 method 8260B/5030B
<2 g/L
07/29/2019
Report .. 2019-12031
Page 2 of 6

Environmental Chemists, Inc.
02 x` n7_m.l1'v'Va fir, W'niingt0n, NC ? 05 -- 910. 9-1 223 I_ab o 910392 4424 Fax
7101 Boxvsertown Road Nbnteo, NC 2795 152.473q702 1 b/ Fax
25 2 Wilmington lllighwa,%, Jacksonville, NC 2 540 * 910,347,5843 Lab's Fax
ANALYTICAL & CONSULTING CHEMISTS
Wood -AMEC
Date of Report, Aug 97, 219
5710 Oleander Drive , Suite 110
Customer 919932
Wilmington NC 28405
Customer ID, 11719
Attention: Ben Moon
Report #: 219-2931
Project ID: Hexion CLRS
tert-Butylbenzene
Svc 846 method 826OB/5830B
<2 fag/L
07/29/2019
Tetrachloroethene
W 846 method 8260B/5030
<2 pg/L
07/29/2019
Toluene
SW 846 method 826O /5030B
<2 g/L
7/29/2 19
Trans-12-Dichloroethene
SW 846 method 82 4&15038B
<2 p /L
7129/2019
Trans- 1, 3-ichloropropene
SW 846 method 8260B/5 3 B
<2 pg/L
7/29/2 19
Trichloroethene
SW 846 method 8260B/550308
<2 g/L
7/29,2019
Trichlorofluoromethane
SIN 846 method 8250815030E
<2 pg/L
07/29/2019
Vinyl chloride
SW 846 method 26 1 030
2 g/L
7/29/2 19
Formaldehyde
W846 8315A
< 9 g/L
7/2 /201
Nitrateitr
Nitrite itrogEPA
11113.2
< 0.02 g/L
07/2 /2 19
Nitrate+ ltrit-Nitrog
EPA 353,2
< 0,02 t g1L
1 12919
Nitrate Nitrogen
Subtraction Whod
<9. 2 m /L
8/07/2 19
Report :: 201 -f 2031 'age 3 of 6

Wood -AMEC Oleander Drive, Suite 116
Wilmington 28405
Attention_ Ben Moore
Lab ID Sample
19-3955 Site; � -2
MM
Environmental Chemists, Inc.
6602 W: c�cn i. tN:; �� d n n ton, C 28405 e 910.39�.0223 Lab a 9' ?. 392. 424 Fax
:..> _ ,
Ifs BowseltoWn Road, , Nlanteo, NC 279 A f, 1. 1 i32 a tax
Results Date Analyzed
Sulfate
EPA 300.E
84 mg/L
7/26/2 19
Ammonia Nitrogen
EPA 35*0.1
56.1 mg/L
07/30/20,119
Total Dissolved Solids (
2540 C
251 rig/L
7/24/ 0 9
Total Phosphorus
SM 4506 P r
9.25 g/
07/31/2019
Total Organic Carbon (7 )
Say 5316 B
5.4 g/
7/25/2019
1,1,12-T tr chior th
SW 846 method 8260B/5030
< .5 idg/L
07/29/2019
1, 1, 1 -Trichloroethane
SW 846 method 826O 1 30
< .5 pg/
07/29/2019
1,12,2-T tr o loro th
U 846 method 8266 t6 3G
< .5 g1i
07/29/2019
1,12-Triohloro th
Sol 846 method 8260515630E
< .5 /
07/29/2019
M-Dichloroethane
Sol 846 method 8260Bt5030B
<t .5 pg/L
07/29/2019
M-Dichloroethene
SW84 method 8 6 B/503 B
< ,5 g/
07/29/2019
11a iohloroprop
W 846 method 826O 15 3
<9.5 leg/ .
07/29/2019
12,3- rl hloro n
SW 846 method 826 B/5030
< .5 /
07/29/2019
1, ,3-Trichloroprop n
SW 846 method 826O tso3 B
<9,5 g/L
07/29/2019
1,2,4-Trichlorobenzene
Ski 846 method 82 O 1503
<6.5 p /L
07/29/2019
1,2,4-Trimethylbenzene
SW 846 method 8266 150308
<9.5 /L
07/29/2019
1,2-Dibrom -3® hloroprop e
SIN 846 method 8266 ,5030
< .5 g?
07/29/2019
1 r'7-Dibromoethane
SW 846 method 82 5 15630
< /Is
07/29/201
12- iichlorobenz n
Sid 846 method826OB15030
<6,5 /L
7/29/201
1,2-Dichloroethane
SW 846 method 8260B/5030B
<6,5 pg/L
07/29/2019
1,2-Dichloropropane
SIN 846 method 8260B,5030B
<M g/I_
07/29/2019
1,3,5-Trimethylbenzene
SW 846 method 8 60B/5030
< .5 /
07/29/2019
1,3-Dichlorobenzene
SW 846 Method 260 15030
< .5 /
07/29/2019
1,3-Dichloroproparte
SW 846 method 8266 T5030B
< ,5 /
07/29/2019
1,4-Dichlorobenzene
SW 846 mete 8260B15030B
< .5 g/L
07/29/2019
2,2-Dichloroproparte
SW 846 method 26€i t5o36S
<9, pg/L
07,129/2019
Report #:: 2 19-t 2531 Page 4 of 6

Wood -AMEC
Date of Report: Aug 071, 291
5710 Oleander Drive, Suite 110
Customer 6480199024
Wilmington NC 28405
Customer : 11070019
Attention: Ben Moore
Report . 219-1231
Project : Hexion CLRS
2- hlorot luen
SW 846 method 8260B15030B
<g/L
7/29/ 19
4-Chlorotoluene
SW 846 method 826OB/5030B
<0 /L
07/29/2019
Benzene
SW 846 method 826OB/5030B
< . /L
07/29/2019
Bromobenzene
SW 846 method 826OB/5030B
< ,5 /L
07/29/2019
Bromochloromethane
SW 846 method 826OB15030B
< ,5 pg/L
07/29/2019
Bromodichloromethane
SW 846 method 8260B/5030Bs
< ,5 /L
07/29/2019
r omo orm
SW 846 method 826OB/5030B
<0 5 /L
07/29/2019
Bromomethane
SW 846 method 8260B/5030B
< ,5 g/L
07/29/2019
Carbon tetrachloride
SW 846 method 8280B150308
< . pg/L
07/29/2019
Chlorobenzene
SW 846 method 8260815030E
< , 5 pg/ L
0 7 /29/2019
Chloroethane
SW 846 method 82608,5030E
<9,5 l /L
07/29/2019
Chloroform
SW846method 8260 /s030B
< ,5 g/L
7/29/201
Chloromethane
SW 846 method 8260B/5030B
< ,5 /L
07/29/2019
i -1,2- l hloro th n
SW 846 method 8260B/5030B
< ,5 /L
07/29/2019
ds-1,3-Dichloropropene
SW 846 method 826OB15030B
< _5 /L
07/29/2019
Dibromochloromethane
Sri 846 method 8260815030E
< _5 /L
7/2 /2 19
Dibromomethane
SW 846 method 8260B15030B
< ,5 /L
07/29/2019
Dichlorodifluoromethane
SW 846 method 8260B/5030B
< ,5 /L
07/29/2019
Ethylbenzene
SW 846 method 82608/5030B
< ,5 /L
07/29/2019
Hexachlorobutadiene
SW 846 method 8264B/5030B
< ,5 pg L
07/29/2019
Isopropylbenzene
SW 846 method 8260B15030B
< ,5 g/L
07/29/2019
M+P XyleneSW
846 method 8260Bi5030B
<1 , g/L
7129/2 19
Methylene chloride
SW 846 method 8260B,5030B
< ,5 g/L
07/29/2019
Naphthalene
5W 846 method 826OB/5030B
< . pg/L
07/29/2019
n-Butylbenzene
5W 846 method 826OB/5030B
< .5 jig/L
07/29/2019
n-Propylbenzene
SW 846 method 82608/5030B
< ,5 g/L
7/29/2019
ortho-Xylene
SW 846 method 8260B/5030B
< ,5 pg/L
07/29/2019
p-lsopropyltoluene
SW 8546 method 3260B/5030B
< ,5 /
07/29/2019
sec-Butylbenzene
SW 846 method 8260B/50308
< _5 /L
l 7/29/2919
Styrene
SW 846 method 8260B/5030B
< ,5 pg/L
7/2912 19
Report #:: 2019_1203'
Page 5 of 6

Wood -AMEC
Date ofReport- Aug 07, 2019
5719 Oleander Drive , Suite 119
Customer PO #: 51992
Wilmington NC 28405
Customer ID: 11079919
Attention, Ben Moore
Report , 2 19-12031
Project s Hexion CLRS
tert-Butyl enzet e
SW 846 method 826OB/5030B
< ,5 pg/L
07/ 9/2019
Tetrachloroethene
SW 646 method 3266B/5030B
< , /L
07/29.1 019
Toluene
SW 846 method 826OB/5030B
<9. pg/L
7/29/2 19
Trans- 1, - ichlor eth ne
SW 646 method 8260B,5030B
<9.5 g/L
07/29/2019
Trans- 1,3-di h loropropene
SW 846 method 8260 /50 0B
<9,5 fag/L
7/ 9/2 19
Tri hloro th ne
SW 846 method 826c6/5030B
< .5 p /L
07/29/20,119
Trichlorofluoromethane
SW 646 method 826OB15030B
< , /L
7/29/2 19
Vinyl chloride
SW 346 mete 826 Br 030B
< .5 pg/L
7/29/2 19
Formaldehyde
SW846 8 1 A
<5 g/L
07/2 /2 19
Nitrate itr
Goo,t #:: 201 - f 2031 Page 6 4i 6

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
600? '=nd mi11 ' y V ^ ington, IBC 28405 '- 9101. 92,0223 Lab 11 910392.4424 Fax
710 11c wse.tows= Road, N an4eo, NC 27954 0 252. 3,5702 Fabj x
2 5-A5-A Wilmington Fligh ay, jacksonville, NC 28 40 0 10347,"5843 _,abl!'�ax
Zn envi€onmentc C._ e 1nstti.,'o-m
Wood-f ec QC - 201-12031
LCS
Value
result
% recovery
Limits �
ParameterTrue
Yi2g,1L
mg/L
Ammonia
5.0
4.9
98
90-110
Ammonia
5.0
4,9
98
90-110
NO2
0.60
0,59
98
90-1 10
NO3 & NO2
1.00
0,96
96
90-110
Sulfate
50.0
48.8
98
90-110
TDS
600
595
99
90-110
TO
10.0
10.5
105
90-11 0
TP
1.60
1.50
94
90-110
MS/MSD
�
71,
True Value
Recovery
%
Limits %
Lin its
Parameter
Recovery
mug//"
mg'L
Df rence
Recovery
Dlf erence
Ammonia
1. i
1.07
97
NIA
80- 120
<20
Ammonia
100
1091106
109/106
80-120
<20
NO2
0.50
0.51
102
N/A
80-120
<20
NO3 & NO2
0.50
0.52
104
N/A
80-120
<20
Sulfate
10.0
10.0/10.0
100/100
0
80-120
<20
TDS
N/A
N/A
N/A
N/A
80-120
<20
TOC
10.0
10.0
100
N/A
N/A
<20
`I'P
1.00
0.97
97
NIA
80/120
< 20

ANALYTICAL & CONSUL-TING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way NC 28405 m 9"I0., 92.022 > Lab 0 910.392 424 ='--ax
710 Illovvserto n Road, !,Ianteo, NC 27`35- � 2-,2. L , 5" 02 I-aL;`Fax
255-A Wily .ng,on I w r jackso ill ,NC 285 0 * 910 3;7,584- La ,' Fax
=fin€o(q,'envi. onnnenta ciieInIsts,cC,:.
Results
Parameter
%Dff�t� c�
Limns
l; g1L
Ammonia
<0.2
<0.2
0
< 10
Ammonia
N/A
N/A
Nth
N/A
NO2
<0.02
<0M
0
< 10
NO3 & NO2
<0.02
<0.02
0
< 20
Sulfate
<15
<15
0
< 10
TDS
272
279
3
< 10
TOC
2.7
17
0
<10
TP
1,47
1,4
1
<10
BLANK
Results
Limit
Parameter
mg1L
m
Ammonia
<0.1
0A
Ammonia
<0,05
0.05
NO2
<0.01
0,01
NO3 & NO2
<0.01
0,0 1
Sulfate
<2.5
15
TDS
<2.5
2.5
TC
<0.25
025
TP
<0.02
0.02

J
_.dparo $ C; m 33omuld-13
Blaulk
i ak/
Result z
R....e. eij;
Resum
�v
q
ethane
<15
r
x
r
a
e
j�
iY
�'
z
a°f
6
ypp s
28
�___._....._.
..._.......
_.._.13
Vi:.a p (,'1 i.o..
"c
e maw; "3
92
—134
..so`.?
21)
97
18.97
919
_v .".;6 — 14
�
_r.'
,:.'
e
18,72
93s6
5,19 3
Methviene chloride
MS
20
61
9&1
RAI141
_
ti an 1 y:_)ic1,15,or ie he n e
` .a .%
20
2135
102
5...3
1 1 i eh 1r e _ha__e
M5
20
SM.2MS7
03
6. 14 1
� fix,,._`,.__,_.
1 64
_.��_.�.
.r
:8.2
_.. ._1)
-Cis-1
20
1911
1_
_15
s ,
101 A h_o ro a,_a n,
An"
20
2031
6 130
I, 1 - 1) c iln_> r y[3e
A.r
2
> ",
8.
r 6 1:
.e_`�.zen.+c
<i<15
20
1%77
y
"a
Ifich .,F„(<y.,_>enc,
20
1 19S2
sx.1
., =. 138
L i bruznn mt,_a ne

ABOR "l
Blankg
e
E
Res
713-143
-
€s
im 5
_1 a�
u
9
trans-
s
z
3
It a_1 c;_
10
1%94
9%7
W , 13
153- _c
<15
2 ,,
9.1
w _ 147
2
ESE. 1.)t. t=. .. ec,
„ ,.
,,.
9 Y,
r gg
1.1. ' e _. aa,___o ro ,ca__....
91
A
61A 131
AA -Al xlee
r40
910
13
A.. 9_
20
S
>„ 3 0
>. 3.
B ronn, 6mi �
i <45
20
-
14 1,
_ W _
[�--. iss z f _�q ._
LrG i. t.7ii>�: �s,>=.€ ,e„ _+.r
` �a. c,... �
�., �-
� � Nf',
G
Y�
..X s�� o-
1MIi
ry „�
1..1, >wc _osow__an
IS
2
z a
_. 11v
<01
20
2M49
_ 0 _
2 — 1-
2-Chuh
W5
20
2M36
102
. Ts 147
1 h 1: _.,a w _, :
<03
20
2016
0.:
1 i,

` m R� .0 (T
x2
x„
Lip
a
terpButliberizene
< 19
20
201
03
63M 12
..�.e..
t. l"'�Ji�':.� _,_,_ .�_ .xa.-.. .-„-
,_e.
2,,
.a. .,e. te,
,_
yam®
ro2' E _-
x�a �t
1.,2"_.� ., a1z ..x ✓ -`'v i .. �'CY xs.s... a,
) 5
2
21 xt
107
ram,. 39
2219
f

ANALYTICAL ENWRONMENTAL SERVICES,INC.
AES
August 01, 2019
Jay Baker
Environmental Chemists, Inc.
6602 Windmill Way
Wilmington NC 28405
RE: 30884 - 30885
Dear Jay Baker: Order No: 1907N 18
Analytical Environmental Services, Inc. received 2 samples on 7/25/2019 10:26:00 AM
for the analyses presented in following report.
No problems were encountered during the analyses. Additionally, all results for the associated
Quality Control samples were within EPA and/or AES established limits. Any discrepancies associated with the
analyses contained herein will be noted and submitted in the form of a project Case Narrative.
AES's accreditations are as follows:
-NELAP/State of Florida Laboratory ID E87582 for analysis of Non -Potable Water, Solid & Chemical
Materials, Air & Emissions Volatile Organics, and Drinking Water Microbiology & Metals, effective
07/01 / 19-06i`30/20.
State of Georgia, Department of Natural Resources ID 4800 for analysis of Drinking Water Metals, effective
07/01/19-06/30/20 and Total Coliforms/ E. coli_ effective 04/25117-04124120.
-AIHA-LAP, LLC Laboratory ITS: 100671 for Industrial Hygiene samples (Metals and PCM Asbestos),
Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct
Examination, effective until 11/01/19,
These results relate only to the items tested as received. This report may only be reproduced in full.
If you have any questions regarding these test results, please feel free to call.
Sincerely,
Mirzeta Kararic
Project Manager
»`_ i 1#3c,> " iv .'�dari€a, G rgia 0 4 el; i0� 4 , 17 Faw 70,457,e 188 T.11 Fr.,, 800,972,4889

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCOENR: DWO CERTIFICATION 0 94 NCDHHS: DLS CERTIFICATION # 3TT29
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
I CIO
Wffl �W �jZ41 0
PROJECT NA:M::E:
AD-RESS:
D
CONTACT NAME:
'M
iREPORT
W9161;MM
TO: _4
I
PHONEIFAX:
MIIIIIIIIIII
Sampled By: SAMPLE PE: I x Irdl E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
e W PRESERVATION
� 0
C0 1 W
E
0 iL
z
ANALYSIS REQUESTED
L)ate,f
EL
E
Time Temp
0
9
W
0
1y I
A
C P
I G J_G
C P G
G
I -A
C P
G G
CIO
C p_
G G
C P
_G G
C P
G JG
C I P
C P
G G
C P
G G
Transfer
getirished By:
4132togime
I Received By:
-11-Cl DaterriMe
2.
or- -
VW
Temperature when Received: Accepted- Rejected: Resample Requested:---
Delivered By: —Received Ely:-- -Date: Time:
Comments: TURNAROUND:
Page 2 of 7

Analytical Environmental Services, Inc
Date: 11-Aug-19
Client:
Environmental Chemists, Inc.
Client Sample ID:
i# 30884
Project Nance:
30884 - 30885
Collection hate:
7/24/2019 9.45.00 A
Lab ID:
1907N'18-001
Matrix:
Aqueous
Reporting Dilution
Analyses Result Qual Units BatchID Date Analyzed Analyst
Limit Factor
Formaldehyde by SW8315A
Formaldehyde BRL 50 ug1L 282494 1 07/26/201915:01 HL
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
Greater than Result value
E Estimated {value above quantitation range}
S Spike Recovery outside limits due to matrix
Nair See case narrative
NC Not confirmed
I Less than Result value
T Estimated value detected below Reporting Limit

Analytical Environmental Services, In
Date: I-Aug-19
'Bent:
Environmental Chemists, Inc.
Client Sample ID:
# 30885
Tolect Name:
30884 - 30885
Collection hate:
7%24f2019 9:25:00 AM
,ab ID;
1907N18-002
Matrix:
Aqueous
Reporting Dilution
Analyses Result Qual Units Bat£hID Date Analyzed Analyst
Limit Factor
Formaldehyde by SW8315A
Formaldehyde
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Amlyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
BRL 5o ig/L 282494 1 07/26/201915:15 RL
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
NC Not confirmed
< Less than Result value
T Estimated value detected below Reporting Limit

(SIANALVnCAL
ENVIRONMMAL
AFES SERvIeFs, jNc- SAMPLE/COOLER RECEIPT CHECKLIST
1. Client Name: Environmental Chemists, Inc. AES Work Order Number: 1907N18
2. Carrier: Fed Exo UPSF—U] USPS❑ clientE] Courier❑ Othei_
Yes No N/A Details
3.
4.
S.
6.
7.
8,
9.
10.
11,
12.
Comments
Shipping container/cooler received in good condition?
(1)
damaged 0 leaking D othei-E]
Custody seals present on shipping container?
V)
Custody seals intact on shipping container?
I
•
Temperature blanks present?
I
Cooler temperature(s) within limits of 0-61C? [See item 13 and 14 for
temperature recordings.]
G
0
. 0
Cooling initiated for recently collected samples ice
present ❑
Chain of Custody (CDC) present?
C-)
0
Chain of Custody signed, dated, and timed when relinquished and received?
•
Sampler name and/or signature on COC?
•-7'N—
VV
V- J
Were all samples received within holding time?
-7"
TAT marked on the COC?
If no TAT indicated proceeded with standard TAT per Terms & Conditions.
13. Cooler 1 Temperature 0.4 Oc Cooler 2 Temperature 0C Cooler 3 Temperature Oc Cooler 4 Temperature 0C
14, Cooler 5 Temperature_ OC Cooler 6 Temperature 0C Cooler 7 Temperature Oc Cooler 8 Temperature Oc
15. Comments:
I certify that I have completed sections 1-15 (dated initials). MJ 7/25/19
Yes No N/A Details Comments
Were sample containers intact upon receipt?
0
0
Custody seals present on sample containers?
0
9
0
Custody seals intact on sample containers?
•
Do sample container labels match the COC?
0
0
0
incomplete info 0 illegible ❑
no label 0 other El
Are analyses requested indicated on the COC?
•0
0
Were all of the samples listed on the COC received?
-,,N
%j
0
❑
samples received but not listed on CDCsamples listed on CDC not received El
Was the sample collection date/time noted?
0
0
0
Did we receive sufficient sample volume for indicated analyses?
Were samples received in appropriate containers?
Were VOA samples received without headspace (< 1/4" bubble)?
I
Were trip blanks submitted?
listed on COC E] not listed on COC ❑
27. Comments:
This section only applies to samples where pH can be I certify that I have completed sections 16-27 (dated initials). BC 7/25/19
checked at Sample Receipt. Yes No N/A Details Comments
28.
29.
30.
ave containers needing chemical preservation been checked? * 01
ontainers meet preservation guidelines? •
", 1 0
/as pH adjusted at Sample Receipt? %-./
Note: Certain analyses require chemical preservation but must be checked in the laboratory and not upon Sample Receipt such as Coliforms, VOCs and Oil & Grease/TPH.
I certify that I have completed sections 28-30 (dated initials). BC 7/25/19
Checklist 6.9.17 Rev 2
Page 5 of 7

Analytical Environmental Services, Inc
Date: 1-Aug-19
Client: Environmental Chemists, Inc,
Project Name: 30884 - 30885 Dates Report
Lab Order: 1907N18
Lab Sample ID Client Sample ID Collection Date Matrix Test Name TCLP Date Prep Date Analysis Date
1907N18-001A # 30884 7/24/2019 9:45:OOAM Aqueous Formaldehyde by SW8315A 7/26/2019 8:30:OOAM 07/26/2019
1907N18-002A # 30885 7/24/2019 9:25:OOAM Aqueous Formaldehyde by SW8315A 7/26/2019 8:30:OOAM 0712612019

Analytical Environmental Services, Inc Date: I -Aug- 19
Client: Environmental Chemists, Inc. ANALYTICAL QC SUMMARY REPORT
Project Name: 30884 - 30885
Workorder: 1907N18 BatchID: 282494
Sample ID: MB-282494
Client ID:
Units: ug/L
Prep Date: 07/26/2019
Run No: 403383
SampleType: MBLK
TestCode: Formaldehyde by SW8315A
BatchID: 282494
Analysis Date: 07/26/2019
Seq No: 9059533
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qua]
Formaldehyde BRL 50
Sample ID: LCS-282494 Client ID: Units: ug/L Prep Date: 07/26/2019 Run No: 403383
SampleType: LCS TestCode: Formaldehyde by SW8315A BatchID: 282494 Analysis Date: 07/26/2019 Seq No: 9059534
Analyte Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Limit Qual
Formaldehyde 805.5 50 1000 80.5 70 130
Sample ID: 1907L92-002CMS
Client ID:
Units: ug/L
Prep Date: 07/26/2019
Run No: 403383
SampleType: MS
TestCode: Formaldehyde by SW8315A
BatchID: 282494
Analysis Date: 07/26/2019
Seq No: 9059536
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
I ligh Limit RPD Ref Val %RPD
RPD Limit Qual
Formaldehyde 741.7 50 1000 4435 69.7 50.1 139
Sample ID: 1907L92-002CMSD Client ID: Units: ug/l, Prep Date: 07/26/2019 Run No: 403383
SampleType: NTSD TestCode: Formaldehyde by SW8315A BatchID: 282494 Analysis Date: 07/26/2019 Seq No: 9059537
Analyte Result RPT Limit SPK value SPK Ref Val %REC Low Limit High Limit RPD Ref Val %RPD RPD Lumt Qual
Formaldehyde 817.4
Qualifiers: I Greater than Result value
BRL Below reporting limit
J Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
50 1000 44.35 77.3 50.1 139 741,7 9,70 161
I Less than Result value
E Estimated (value above quantutation range)
N Analyte not NELAC certified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix
Page 7 of 7

Analytical & Consulting Chernists
Client:
ADDRESS:
J
Transfer
C 6602 Windmill Way , NC 205
ENVIRONMENTAL CHEMISTS, IN OFFICE: 910-392-0223 FAXWilmington910-392-442844
NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 infoOenvironmentatchemists.com
COLLECTION AND CHAIN OF CUSTODY
PROJECT NAME: REPORT NO:
CONTACT NAME: PO NO: 1p �4`6,
REPORT TO: PHONE/FAX:
COPY TO: email: P
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Collection
W
PRESERVATION
0
.2 2
z
0
0
ANALYSIS REQUESTED
a
Time
Temp
E
E 0 E
0 0 M
z
0
z
0
0
777
C P
G"
"16
`fix
C P
77 =
G'
777
1 �171
IL&I 'j,
C P
C
'i:`,'�`)
U 5
G
C
G
G
�Klli
C P
1. 1 /1,11 0,1,111111-
Received
Datefrime
2.
Temperature when Received : '.—Accepted:-. I _____ --.Rejected: ---.---..------Resample Requested:
Delivered. % ...... . . ... Date- 1, 1
Received By:'
Titpe:
Comments:
- — ----- TURNAROUND: .....

<
ENVIRONMENTAL CHEMISTS,
6602 Windmill Wagton, NC 28405
INC
OFFICE: 910-392-0y 223WilminFAX 910-392-4424
Analytical & Consulting Chemists
NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client:
PROJECT NAME: C_A,,,AX1"­'','
REPORT NO:
ADDRESS:
CONTACT NAME:
PO NO:
'S\)
REPORT TO:
PHONE/FAX:""""1i(,,,'
U
COPY TO:
small: .. ...C
Sampled B
AMPLE TYPE: I o Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SIL = Sludge, Other:
Collection
2
PRESERVATION
Sample Identification
a0.8
'00 2WCr
S 8 8
2
W
ANALYSIS REQUESTED
Date
Time
Temp
E 0 C
0 0 U z
0
z
x
0
z
x
0
4
z
x
0
C P
17T
A
L
)q)
PIG 1.1 (9
C P
G
C
V,
G
G
C
tad
G
fx
C
Lid-
Transfer
Relinquished By: Date/Time
Received By: Date/rime
"T:7
2.
Temperature when Received:
Accepted: _Rejected:
Resample Requested:
Delivered By:
Received Time: Date:
''ND:"
Comments: -- -, ----
- --------
3,
TURNAROu

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Wood -AMEC
Date of Report: Jul 31, 2020
5710 Oleander Drive , Suite 110
Customer PO #: 6480200031
Wilmington NC 28405
Customer ID: 11070019
Attention: Ben Moore
Report #: 2020-11837
Project ID: Hexion CLRS
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
20-29771 Site: WWMW-01
7/16/2020
9:30 AM Water Ben Moore
Test
Method
Results
Date Analyzed
Sulfate
EPA 300.0
1470 mg/L
07/20/2020
Ammonia Nitrogen
EPA 350.1
916 mg/L
07/28/2020
Total Dissolved Solids (TDS)
SM 2540 c
1090 mg/L
07/16/2020
Total Phosphorus
SM 4500 P F
1.79 mg/L
07/22/2020
Total Organic Carbon (TOC)
SM 5310 B
49.1 mg/L
07/21/2020
1, 1, 1,2-Tetrachloroethane
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
1, 1,1-Trichloroethane
SW 846 method 82606/5030B
<0.5 pg/L
07/21/2020
1,1,2,2-Tetrachloroethane
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
1,1,2-Trichloroethane
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
1,1-Dichloroethane
SW 846 method 82BOB/5030B
<0.5 pg/L
07/21/2020
1,1-Dichloroethene
SW 846 method 826013/5030B
<0.5 pg/L
07/21/2020
1, 1 -Dichloropropene
SW 846 method 826013/5030B
<0.5 pg/L
07/21/2020
1,2,3-Trichlorobenzene
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
1,2,3-Trichloropropane
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
1,2,4-Trichlorobenzene
SW 846 method 82606/5030B
<0.5 pg/L
07/21/2020
1,2,4-Trimethylbenzene
SW 846 method 82608/503013
<0.5 pg/L
07/21/2020
1,2-Dibromo-3-Chloropropane
SW 846 method 82606/5030B
<0.5 pg/L
07/21/2020
1,2-Dibromoethane
SW 846 method 8260B15030B
<0.5 pg/L
07/21/2020
1,2-Dichlorobenzene
SW 846 method 8260B15030B
<0.5 ug/L
07/21/2020
1,2-Dichloroethane
SW 846 method 826013/50308
<0.5 ug/L
07/21/2020
1,2-Dichloropropane
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
1,3,5-Trimethylbenzene
SW 846 method 826013/50308
<0.5 Ng/L
07/21/2020
1,3-Dichlorobenzene
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
1,3-Dichloropropane
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
1,4-Dichlorobenzene
SW 846 method 82606/50306
<0.5 pg/L
07/21/2020
2,2-Dichloropropane
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
Reoort 9" 2020-11837
Page 1 of 6

Environmental Chemists, Inc.
envirochem
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 + 910.347.5843 Lab/Fax
[e-mail]
Wood -AMEC
5710 Oleander Drive, Suite 110
Wilmington NC 28405
Attention: Ben Moore
Date of Report: Jul 31, 2020
Customer PO #: 6480200031
Customer ID: 11070019
Report #: 2020-11837
Project ID: Hexion CLRS
2-Chlorotoluene
SW 846 method 82608/50306
<0.5 pg/L
07/21/2020
4-Chlorotoluene
SW 846 method 82606/503013
<0.5 pg/L
07/21/2020
Benzene
SW 846 method 82608/50306
<0.5 pg/L
07/21/2020
Bromobenzene
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
Bromochloromethane
SW 846 method 826OB15030B
<0.5 pg/L
07/21/2020
Bromodichloromethane
SW 846 method 82608/503013
<0.5 pg/L
07/21/2020
Bromoform
SW 846 method 8260B15030B
<0.5 pg/L
07/21/2020
Bromomethane
SW 846 method 82606/503013
<0.5 pg/L
07/21/2020
Carbon tetrachloride
SW 846 method 82608/50308
<0.5 pg/L
07/21/2020
Chlorobenzene
SW 846 method 82608/50306
<0.5 pg/L
07/21/2020
Chloroethane
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
Chloroform
SW 846 method 82606/503013
<0.5 pg/L
07/21/2020
Chloromethane
SW 846 method 82606/503013
<0.5 pg/L
07/21/2020
cis-1,2-Dichloroethene
SW 846 method 82608/50308
<0.5 pg/L
07/21/2020
cis-1,3-Dichloropropene
SW 846 method 82608/50306
<0.5 pg/L
07/21/2020
Dibromochloromethane
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
Dibromomethane
SW 846 method 8260B15030B
<0.5 pg/L
07/21/2020
Dichlorodifluoromethane
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
Ethylbenzene
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
Hexachlorobutadiene
SW 846 method 82608/50308
<0.5 pg/L
07/21/2020
Isopropylbenzene
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
M+P Xylene
SW 846 method 826013/50308
<1.0 pg/L
07/21/2020
Methylene chloride
SW 846 method 826013/50306
<0.5 pg/L
07/21/2020
Naphthalene
SW 846 method 82606/50306
1.10 pg/L
07/21/2020
n-Butylbenzene
SW 846 method 82606/503013
<0.5 pg/L
07/21/2020
n-Propylbenzene
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
ortho-Xylene
SW 846 method 826013/50308
<0.5 pg/L
07/21/2020
p-Isopropyltoluene
SW 846 method 826013/50306
<0.5 pg/L
07/21/2020
sec-Butylbenzene
SW 846 method 82606/503013
<0.5 pg/L
07/21/2020
Styrene
SW 846 method 8260B15030B
<0.5 pg/L
07/21/2020
Report #:: 2020-11837
Page 2 of 6

[en7virrochem)
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
[e-mail]
Wood -AMEC
Date of Report: Jul 31, 2020
5710 Oleander Drive, Suite 110
Customer PO #: 6480200031
Wilmington NC 28405
Customer ID: 11070019
Attention: Ben Moore
Report #: 2020-11837
Project ID: Hexion CLRS
tert-Butylbenzene
SW 846 method 82606/503013
<0.5 pg/L
07/21/2020
Tetrachloroethene
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
Toluene
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
Trans-1,2-Dichloroethene
SW 846 method 82608/503013
<0.5 pg/L
07/21/2020
Trans-1,3-dichloropropene
SW 846 method 82606/503013
<0.5 pg/L
07/21/2020
Trichloroethene
SW 846 method 828013/503013
<0.5 pg/L
07/21/2020
Trichlorofluoromethane
SW 846 method 82606/503013
<0.5 pg/L
07/21/2020
Vinyl chloride
SW 846 method 82608/50308
<0.5 pg/L
07/21/2020
Formaldehyde
SW846 8315A
450.0 pg/L
07/18/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 07/16/2020
Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 07/26/2020
Nitrate Nitrogen Subtraction Method <0.02 mg/L 07/29/2020
Total Nitrogen (Calc)
Total Kieldahl Nitrogen (TKN) EPA 351.2 775 mg/L 07/30/2020
Report #:: 2020-11837 Page 3 of 6

Environmental Chemists, Inc.
envirochem
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
[e-mail]
Wood -AMEC Date of Report: Jul 31, 2020
5710 Oleander Drive, Suite 110 Customer PO #: 6480200031
Wilmington NC 28405 Customer ID: 11070019
Attention: Ben Moore Report #: 2020-11837
Project ID: Hexion CLRS
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
20-29772 Site: WWMW-02 7/16/2020 9:00 AM Water Ben Moore
Test Method Results Date Analyzed
Sulfate
EPA 300.0
357 mg/L
07/22/2020
Ammonia Nitrogen
EPA 350.1
48.0 mg/L
07/22/2020
Total Dissolved Solids (TDS)
SM 2540 c
758 mg/L
07/16/2020
Total Phosphorus
SM 4500 P F
0.05 mg/L
07/22/2020
Total Organic Carbon (TOC)
SM 5310 B
6.4 mg/L
07/21/2020
1, 1, 1,2-Tetrachloroethane
SW 846 method 826013/50306
<0.5 pg/L
07/21/2020
1, 1, 1 -Trichloroethane
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
1,1,2,2-Tetrachloroethane
SW 846 method 826013/50306
<0.5 pg/L
07/21/2020
1,1,2-Trichloroethane
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
1,1-Dichloroethane
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
1,1-Dichloroethene
SW 846 method 82606/50306
<0.5 pg/L
07/21/2020
1, 1 -Dichloropropene
SW 846 method 82606/503013
<0.5 pg/L
07/21/2020
1,2,3-Trichlorobenzene
SW 846 method 82608/503013
<0.5 pg/L
07/21/2020
1,2,3-Trichloropropane
SW 846 method 826013/50308
<0.5 pg/L
07/21/2020
1,2,4-Trichlorobenzene
SW 846 method 82608/50306
<0.5 pg/L
07/21/2020
1,2,4-Trimethylbenzene
SW 846 method 82606/503013
<0.5 pg/L
07/21/2020
1,2-Dibromo-3-Chloropropane
SW 846 method 826013/50306
<0.5 pg/L
07/21/2020
1,2-Dibromoethane
SW 846 method 826013/50306
<0.5 pg/L
07/21/2020
1,2-Dichlorobenzene
SW 846 method 826013/50306
<0.5 pg/L
07/21/2020
1,2-Dichloroethane
SW 846 method 82606/50306
<0.5 pg/L
07/21/2020
1,2-Dichloropropane
SW 846 method 82606/503013
<0.5 pg/L
07/21/2020
1,3,5-Trimethylbenzene
SW 846 method 82608/503013
<0.5 pg/L
07/21/2020
1,3-Dichlorobenzene
SW 846 method 82608/50306
<0.5 pg/L
07/21/2020
1,3-Dichloropropane
SW 846 method 82606/503013
<0.5 pg/L
07/21/2020
1,4-Dichlorobenzene
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
2,2-Dichloropropane
SW 846 method 82606/503013
<0.5 pg/L
07/21/2020
Reoort #:: 2020-11837 Page 4 of 6

Cnviroche]m
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 e 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Wood -AMEC
5710 Oleander Drive , Suite 110
Wilmington NC 28405
Attention: Ben Moore
Date of Report: Jul 31, 2020
Customer PO #: 6480200031
Customer ID: 11070019
Report #: 2020-11837
Project ID: Hexion CLRS
2-Chlorotoluene
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
4-Chlorotoluene
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
Benzene
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
Bromobenzene
SW 846 method 82608/503013
<0.5 pg/L
07/21/2020
Bromochloromethane
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
Bromodichloromethane
SW 846 method 826013/50308
<0.5 pg/L
07/21/2020
Bromoform
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
Bromomethane
SW 846 method 8260B15030B
<0.5 pg/L
07/21/2020
Carbon tetrachloride
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
Chlorobenzene
SW 846 method 82606/5030B
<0.5 pg/L
07/21/2020
Chloroethane
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
Chloroform
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
Chloromethane
SW 846 method 82608/5030B
<0.5 pg/L
07/21/2020
cis-1,2-Dichloroethene
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
cis-1,3-Dichloropropene
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
Dibromochloromethane
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
Dibromomethane
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
Dichlorodifluoromethane
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
Ethylbenzene
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
Hexachlorobutadiene
SW 846 method 82608/50306
<0.5 pg/L
07/21/2020
Isopropylbenzene
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
M+P Xylene
SW 846 method 826013/5030B
<1.0 pg/L
07/21/2020
Methylene chloride
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
Naphthalene
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
n-Butylbenzene
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
n-Propylbenzene
SW 846 method 82608/503013
<0.5 pg/L
07/21/2020
ortho-Xylene
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
p-Isopropyltoluene
SW 846 method 82606/5030B
<0.5 pg/L
07/21/2020
sec-Butylbenzene
SW 846 method 826013/50308
<0.5 pg/L
07/21/2020
Styrene
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
Report #:: 2020-11837
Page 5 of 6

[en7virochem
ANALYTICAL & CONSULTING CHEMISTS
Wood -AMEC
5710 Oleander Drive , Suite 110
Wilmington NC 28405
Attention: Ben Moore
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report:
Jul 31, 2020
Customer PO #:
6480200031
Customer ID:
11070019
Report #:
2020-11837
Project ID: Hexion CLRS
tert-Butylbenzene
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
Tetrachloroethene
SW 846 method 826013/50306
<0.5 pg/L
07/21/2020
Toluene
SW 846 method 826013/503013
<0.5 ug/L
07/21/2020
Trans- 1,2-Dichloroethene
SW 846 method 8260B/5030B
<0.5 pg/L
07/21/2020
Trans- 1, 3-d ich loropropene
SW 846 method 826013/50306
<0.5 pg/L
07/21/2020
Trichloroethene
SW 846 method 826013/503013
<0.5 ug/L
07/21/2020
Trichlorofluoromethane
SW 846 method 82608/503013
<0.5 pg/L
07/21/2020
Vinyl chloride
SW 846 method 826013/503013
<0.5 pg/L
07/21/2020
Formaldehyde
SW846 8315A
<250 pg/L
07/18/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 07/16/2020
Nitrate+Nitrite-Nitrogen EPA353.2 67.8mg/L 07/27/2020
Nitrate Nitrogen Subtraction Method 67.8 mg/L 07/29/2020
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN) EPA 351.2 19.1 mg/L 07/30/2020
Comment:
Reviewed by:
Report #:: 2020-11837 Page 6 of 6

00 00 1
C
virochem
ANALYTICAL & CONSULTING CHEMISTS
LCS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
info[ environmentalchemists.com
Wood-Amec QC - 2020-11837
Parameter
True Value
mg1L
Result
mg1L
% Recovery
Limits
ro
Ammonia
5.0
4.9
98
90-110
Ammonia
5.0
5.0
100
90-110
NO2
0.60
0.55
92
90-1 10
NO3 & NO2
1.00
0.97
97
90-110
Sulfate
50.0
48.2
96
90-110
TDS
600
581
97
90-110
TOC
10.0
10.2
102
90-110
TKN
4.0
4.0
100
90-110
TP
1.60
1.63
102
90-110
MS/MSD
Parameter
True Value
mg1L
Recovery
mg1L
00
Recovery
%
Difference
Limits %
Recovery
Limits
Difference
Ammonia
5.0
5.115.1
102/ 102
0
80-120
<20
Ammonia
5.0
5.015.1
100/102
2
80-120
<20
NO2
0.50
0.48/0.49
96198
2
80-120
<20
NO3 & NO2
0.50
N/A
N/A
N/A
80-120
<20
Sulfate
10.0
10.9/10.9
109/109
0
80-120
<20
TDS
N/A
N/A
N/A
N/A
80-120
<20
TOC
10.0
10.1
101
N/A
N/A
<20
TKN
4.0
4.2/4.2
1
0
N/A
<20
TP
1.60
1.64/ 1.47
102/92
10
80/ 120
<20

F7 W7
Ln virochel
ANALYTICAL & CONSULTING CHEMISTS
DUPLICATE SAMPLES
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Parameter
Results1L
g
% Difference
Limits %
Ammonia
NIA
N/A
N/A
< 10
Ammonia
N/A
N/A
N/A
NIA
NO2
N/A
N/A
N/A
<10
NO3 & NO2
0.22
0.22
0
< 20
Sulfate
5
5
0
<10
TDS
378
358
5
<10
TOC
2.0
2.0
0
<10
TKN
N/A
N/A
N/A
<10
TP
N/A
N/A
N/A
<10
BLANK
Parameter
Results
mg/L
Limit
mg1L
Ammonia
<0.1
0.1
Ammonia
<0.1
0.1
NO2
<0.01
0.01
NO3 & NO2
<0.01
0.01
Sulfate
<2.5
2.5
TDS
<2.5
2.5
TOC
<0.25
0.25
TKN
<0.25
0.25
TP
<0.02
0.02

LABORATORY CONTROL SAMPLE #1
Report#2020-1 1837 Page I of 3
Compounds
Spike Com
p p
Method
Blank
Result
Spike
Added
Blank Spike
QC Limits
(Mandatory)
Recovery Range
Result
Recovery
Dichlorodifluoromethane
<0.5
10
9.04
90.4
33.3 - 150
Chloromethane
<0.5
10
9.75
97.5
61.2 -128
Vinyl chloride
<0.5
10
9.81
98.1
54.3 -134
Bromomethane
<0.5
10
11.17
112
64.6 -143
Chloroethane
<0.5
10
10.65
107
55.8 -153
Trichlorofluoromethane
<0.5
10
9.9
99
52.9 - 153
1, 1 -Dichloroethene
<0.5
10
9.97
99.7
59.1 - 145
Methylene chloride
<0.5
10
9.98
99.8
52.0 -141
trans-l.2-Dichloroethene
<0.5
10
10.08
101
58.3 - 145
1, 1 -Dichloroethane
<0.5
10
9.77
97.7
66.1 -140
2,2-Dichloropropane
I <0.5
10
9.59
95.9
59.9 -137
cis-1,2-Dichloroethene
<0.5
10
9.91
99.1
57.4 -139
Bromochloromethane
<0.5
10
9.67
96.7
63.5 - 130
Chloroform
<0.5
10
10.18
102
54.2 -153
1, 1, 1 -Trichloroethane
<0.5
10
9.92
99.2
60.6 - 130
Carbon tetrachloride
<0.5
10
9.87
98.7
51.7 - 147
1, 1 -Dichloropropene
<0.5
10
9.94
99.4
53.6 -134
Benzene
<0.5
10
9.96
99.6
63.3 - 133
1.2-Dichloroethane
<0.5
10
10.17
102
62.6 -150
Trichloroethene
<0.5
10
10.2
102
73.1 -138
1,2-Dichloropropane
<0.5
10
77
97.7
61.8 -138
Dibromomethane
<0.5
10
10.14
101
56.4 - 136

LABORATORY CONTROL SAMPLE #1
Report#2020-11837 Page 2 of
Spike Compounds
Method
Blank
Result
Spike
Added
Blank Spike
QC Limits
(Mandatory)
% Recovery Range
Result
Recovery
Bromodichloromethane
<0.5
10
10.1
101
74.3 - 143
cis-1,3-Dichloropropene
<0.5
10
10.18
102
63.9 -135
Toluene
<0.5
10
9.99
99.9
62.3 -143
trans-1,3-Dichloropropene
<0.5
10
9.76
97.6
71.3 - 143
1,1,2-Trichloroethane
<0.5
10
9.76
97.6
57.7 - 147
Tetrachloroethene
<0.5
10
9.83
98.3
58.1 - 139
1,3-Dichloropropene
<0.5
10
9.97
99.7
61.5 - 147
Dibromochloromethane
<0.5
10
10.02
100
69.5 -147
1,2-Dibromoethane
<0.5
10
9.97
99.7
69.2 -133
Chlorobenzene
<0.5
10
9.85
98.5
76.5 -117
Ethylbenzene
<0.5
10
9.88
1 98.8
62.9 -143
1, 1, 1,2-Tetrachloroethane
<0.5
10
9.76
97.6
69.4 -137
M+P Xylene
<1
20
19.75
98.8
62.5 - 134
O-Xylene
<0.5
10
9.9
99
62.3 -140
Styrene
<0.5
10
9.89
98.9
66.8 -131
Bromoforin
<0.5
10
9.8
98
61.6 - 141
IsopropyIbenzene
<0.5
10
9.79
97.9
68.1 -130
Bromobenzene
<0.5
10
10.76
108
64.9 -125
1,1,2,2-Tetrachloroethane
<0.5
10
9.83
98.3
65.7 - 146
n-Propylbenzene
<0.5
10
10.71
107
54.2 -149
1,2,3-Trichloropropane
<0.5
10
10.93
109
68.5 - 145
2-Chlorotoluene
<0.5
10
10.79
108
56.8 -147
1,3,5-Trimethylbenzene
<0.5
10
10.8
108
63.8 - 137

LABORATORY CONTROL SAMPLE #1
Report#2020-1 1837 Page 3 of
Spike Compounds
Method
Blank
Result
Spike
Added
Blank Spike
QC Limits
(Mandatory)
Recovery Range
Result
Recovery
4-Chlorotoluene
<0.5
10
10.69
107
62.6 -145
tert-Butylbenzene
<0.5
10
10.55
106
63.0 - 128
1,2,4-Trimethylbenzene
<0.5
10
10.68
107
63.8 -138
sec-Butylbenzene
<0.5
10
10.59
106
71.0 - 143
I,')-Dichlorobenzene
<0.5
10
10.63
106
70.5 - 127
4-Isopropyltoluene
<0.5
10
10.64
106
58.9 -132
1,4-Dichlorobenzene
<0.5
10
10.73
107
78.8 -122
n-Butylbenzene
<0.5
10
10.34
103
55.5 - 136
1,2-Dichlorobenzene
<0.5
10
10.75
108
78.6 -121
1,2-Dibromo-3-chloropropane
<0.5
10
10.64
106
65.5 -139
1,2,4-Trichlorobenzene
<0.5
10
10.67
107
60.5 - 137
Hexachlorobutadiene
<0.5
10
10.74
107
37.0 -131
Naphthalene
<0.5
10
11.04
110
54.9 -138
1,2,3-Trichlorobenzene
<0.5
10
10.94
109
62.5 -13

ANALYTICAL_ ENVIRONMENTAL SERVICES, INC.
AES
July 23, 2020
Jay Baker
Environmental Chemists, Inc.
6602 Windmill Way
Wilmington NC 28405
RE: 2020-11837
Dear Jay Baker: Order No: 2007I69
Analytical Environmental Services, Inc. received 2 samples on 7/17/2020 12:44:00 PM
for the analyses presented in following report.
No problems were encountered during the analyses. Additionally, all results for the associated
Quality Control samples were within EPA and/or AES established limits. Any discrepancies associated with the
analyses contained herein will be noted and submitted in the form of a project Case Narrative.
AES's accreditations are as follows:
-NELAP/State of Florida Laboratory ID E87582 for analysis of Non -Potable Water, Solid & Chemical
Materials, Air & Emissions Volatile Organics, and Drinking Water Microbiology & Metals, effective
07/01 /20-06/30/21.
State of Georgia, Department of Natural Resources ID 9800 for analysis of Drinking Water Metals, effective
through 06/30/20 and Total Colifornis/ E. coli, effective 04/20/20-04/24/23.
-AIHA-LAP, LLC Laboratory ID: 100671 for Industrial Hygiene samples (Metals and PCM Asbestos),
Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct
Examination, effective until 11/01/21.
These results relate only to the items tested as received. This report may only be reproduced in full.
If you have any questions regarding these test results, please feel free to call.
Sincerely,
�efV ranc
Mirzeta Kararic
Project Manager
?I t} f'r;• iclrnt6.tl l�ri•.v �at�.cnla, \.ir, r i.i illi (1 1'rl: 1 rCl.l^i. 1 % F as. 111-457.8 186 • ToI1 f'rcc:800.9 2.4 889
t I.111 tcl.i iTitl

Environmental Chemist
66002 Windmill Way, Wilmington, NC 28405
Phone: [phone] Fax: [phone]
[e-mail]
REQUEST FOR SUBCONTRACTED SERVICES
Report # Sample # Date Time Matrix Analysis Requested Preservation
Comments
Z01i(all
2020-11837
20-29771
7/16/2020
9:30
Water
Formaldehyde
Cool,4-c
2020-11837
20-29772
7/16/2020
9:00
Water
Formaldehyde
Cool, VC
Prepared by:
For Shipment By:
Relinquished B
Date/Time:
Received By: 0 -)
Date/Time: j Z ic
Thursday, July 16, 2020 Page I of 1

Analytical Environmental Services, Inc Date: 23-Jul-20
Client: Environmental Chemists, Inc.
Project: 2020-11837 Case Narrative
Lab ID: 2007169
Formaldehyde Analysis by Method 8315:
Due to sample matrix, sample 2007169-002 required dilution during analysis resulting in elevated reporting limits.

Analytical Environmental Services, Inc
Date: 23-Jul-20
Client:
Environmental Chemists, Inc.
Client Sample ID:
20-29771
Project Name:
2020-11837
Collection Date:
7/ 16/2020 9:30:00 AM
Lab ID:
2007169-001
Matrix:
Aqueous
Analyses Result Reporting Qual Units BatchID Dilution Date Analyzed Analyst
Limit Factor
Formaldehyde by SW8315A
Formaldehyde 450 250 ug/L 300127 1 07/18/2020 02 59 HL
Qualifiers: •
Value exceeds maximum contaminant level
BRL Below reporting limn
H
Holding times for preparation or analysis exceeded
N
Analyte not NELAC certified
B
Analyte detected in the associated method blank
>
Greater than Result ,slue
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
F Analyzed in the lab which is a deviation from the method
c Less than Result value
J Estimated value detected below Reporting Limn

Analytical Environmental Services, Inc
Date: 23-Jul-20
Client:
Environmental Chemists, Inc.
Client Sample ID:
20-29772
Project Name:
2020-11837
Collection Date:
7/16/2020 9:00:00 AM
Lab ID:
2007169-002
Matrix:
Aqueous
Reporting Dilution
Analyses Result Qual Units BatchlD Date Analyzed Analyst
Limit Factor
Formaldehyde by SW8315A
Formaldehyde
Qualifiers: '
Value exceeds maximum contaminant level
BRL
Belowreporting limit
H
Holding times for preparation or analysis exceeded
N
Analyte not NELAC certified
B
Analyte detected in the associated method blank
>
Greater than Result %slue
BRL 250 uyL 300127 1 07/18/2020 03 12 HL
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
F Anal) zed in the lab which is a deviation from the method
Less than Result value
1 Estimated value detected below Reporting Limit

�i IANALvfICAI,
zS ENVIRONMENTAL
AES SERVICES, INC.
1. client Name: Environmental Chemists, Inc.
SAMPLE/COOLER RECEIPT CHECKLIST
2. Carrier: FedEx ❑ UPS[k] USPS❑ Client❑ Courier❑ Othei
Yes No N/A
3.
4.
5.
6.
7.
8.
9.
10.
11.
12.
AES Work Order Number: 2007169
n-+,a�
Clear Save as
Shipping container/cooler received in good condition?
•n
i ndamaged
❑ leaking ❑ other❑
Custody seals present on shipping container?
•
Custody seals intact on shipping container?
•
Temperature blanks present?
U•
Cooler temperature(s) within limits of 0-6°C? [See item 13 and 14 for
temperature recordings.]
O
O
O
Cooling initiated for recently collected samples / ice
present ❑
Chain of Custody (CDC) present?
•
Chain of Custody signed, dated, and timed when relinquished and received?
•
o
in
Sampler name and/or signature on COC?
•
Were all samples received within holding time?
•
TAT marked on the COC?
•
If no TAT indicated, proceeded with standard TAT per Terms & Conditions.
13. Cooler 1 Temperature 0.8 0C Cooler 2 Temperature
14. Cooler 5 Temperature 0C Cooler 6 Temperature
15. Comments:
16.
17.
18.
19.
20.
21.
22.
23.
24.
25.
26.
0C Cooler 3 Temperature 0C Cooler 4 Temperature 0C
0C Cooler 7 Temperature 0C Cooler 8 Temperature 0C
certify that I have completed sections 1-15 (dated initials). LM 7/17/20
Vne Nn rd/A n..a..:�-
Were sample containers intact upon receipt?
•
Custody seals present on sample containers?
•
Custody seals intact on sample containers?
F
sample container labels match the COC?
OOincomplete
info illegible
illeDo ❑
no label ❑ other ❑
Are analyses requested indicated on the COC?
•
Were all of the samples listed on the CDC received?
O
©
O
samples received but not listed on CDC ❑
samples listed on CDC not received ❑
Was the sample collection date/time noted?
•
Did we receive sufficient sample volume for indicated analyses?
Were samples received in appropriate containers?
•
Were VOA samples received without headspace (< 1/4" bubble)?
VO
Were trip blanks submitted?
listed on CDC ❑ not listed on COC ❑
27. Comments:
This section only applies to samples where pH can be
I certify that I have completed sections 16-27 (dated initials). LM 7/17/20
checked at Sample Receipt. Yes No N/A Details rnmmantc
28.
29.
In
-------------
Have containers needing chemical preservation been checked? U 1•
Containers meet preservation guidelines? •
Was pH adjusted at Sample Receipt? •
- Note: Lertain analyses require chemical preservation but must be checked in the laboratory and not upon Sample Receipt such as Coliforms, VOCs and Oil & Grease/TPH.
I certify that I have completed sections 28-30 (dated initials). LM 7/17/20
Checklist 6.9.17 Rev 2
Locked

Analytical Environmental Services, Inc
Date: 23-Jul-20
Client: Environmental Chemists, Inc.
Project Name: 2020-11837 Dates Report
Lab Order: 2007169
Lab Sample ID
Client Sample ID
Collection Date
Matrix
Test Name
TCLP Date Prep Date
Analysis Date
2007169-001A
20-29771
7/16/2020 9:30:OOAM
Aqueous
Formaldehyde by SW8315A
7/17/2020 12:37:24PM
07/18/2020
2007169-002A
20-29772
7/16/2020 9:00:OOAM
Aqueous
Formaldehyde by SW8315A
7/17/2020 12:37:24PM
07/18/2020
D- 7 ni n

Analytical Environmental Services, Inc
Client: Environmental Chemists, Inc.
Project Name: 2020-11837
workorder: 2007169
Date: 23-Jul-20
ANALYTICAL QC SUMMARY REPORT
BatchlD: 300127
Sample ID: MB-300127
Client ID:
Units: ug/L
Prep Date: 07/17/2020
Run No: 430457
SampleType: NIBLK
TestCode: Formaldehyde by SW8315A
BatchlD: 300127
Analysis Date: 07/18/2020
Seq No: 9764317
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val °oRPD
RPD Limit Qual
Formaldehyde BRL 50
Sample ID: LCS-300127
Client ID:
Units: ug/L
Prep Date: 07/17/2020
Run No: 430457
SampleType: LCS
TestCode: Formaldehyde by SW8315A
BatchlD: 300127
Analysis Date: 07/18/2020
Seq No: 9764318
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val °/oRPD
RPD Limit Qual
Formaldehyde 1078 50 1000 108 70 130
Sample ID: 20071439-OOIAMS
Client ID:
Units: ug/L
Prep Date: 07/17/2020
Run No: 430457
SampleType: MS
TestCode: Formaldehyde by SW8315A
BatchlD: 300127
Analysis Date: 07/18/2020
Seq No: 9764320
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val °!oRPD
RPD Limit Qual
Formaldehyde 1203 50 1000 83.97 112 50.1 139
Sample ID: 20071-139-00IANISD
Client ID:
Units: ug/L
Prep Date: 07/17/2020
Run No: 430457
SampleType: MSD
TestCode: Formaldehyde by SW8315A
BatchlD: 300127
Analysis Date: 07/18/2020
Seq No: 9764321
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Formaldehyde 1213 50 1000 83,97 113 50.1 139 1203 0.817 16.2
Qualitters: > Greater than Result value
BRL Below reporting limn
1 Estimated value detected below Reporting Limn
Rpt Lim Reporting Limn
t Less than Result value
E Estimated (value above quanwation range)
N Analyte not NELAC certified
S Spike Recovery outside limns due to matrix
B Analyte detected in the associated method blank
1-1 Holding times for preparation or analysts exceeded
R RPD outside limits due to matrix
o- -- o c n

End of Report
0-n ofO

.._ �.,
An.lW,4 A Cmsldhnq Chennsts
Client: aw
ADDRESS: . �)o
Sampled Bv:
ENVIRONMENTAL CHEMISTS, INC
NCDENW DWO CERTIFICATION 0 94 NCDHHS: DLS CERTIFICATION • 37M
COLLECTION AND CHAIN OF CUSTODY
PROJECT NAME:
CONTACT NAME.
REPORT TO:
COPY TO:
CAYDI C TVDc. \
6602 Windmill Way Wilmington, N(. 29405
OFFICE: 910-392-0223 FAX 910-M-4424
Info0environmentalchemist s.com
REPORT NO• O
PO NO: 6
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PHONEIFAX: IIo
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[en7virroche]m
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
[e-mail]
Wood -AMEC Date of Report: Jul 26, 2021
5710 Oleander Drive, Suite 110 Customer PO #:
Wilmington NC 28405 Customer ID: 11070019
Attention: Ben Moore Report #: 2021-11259
Project ID: Hexion CLRS
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-28013 Site: WWMW-1 7/8/2021 10:00 AM Water Client
Test Method Results Date Analyzed
Sulfate
EPA 300.0
315 mg/L
07/15/2021
Total Dissolved Solids (TDS)
SM 2540 C
2520 mg/L
07/08/2021
Ammonia Nitrogen
SM 4500 NH3 C-2011
890 mg/L
07/16/2021
Total Phosphorus
SM 4500 P F
1.69 mg/L
07/14/2021
Total Organic Carbon (TOC)
SM 5310 B
105 mg/L
07/12/2021
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
1, 1, 1 -Trichloroethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
1,1,2-Trichloroethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
1,1-Dichloroethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
1,1-Dichloroethene
SW 846 Method 8260D15030B
< 0.50 pg/L
7/14/2021
1,1-Dichloropropene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
1,2,3-Trichlorobenzene
SW 846 Method 8260D/50308
< 0.50 pg/L
7/14/2021
1,2,3-Trichloropropane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
1,2,4-Trichlorobenzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
1,2-Dibromoethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
1,2-Dichlorobenzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
1,2-Dichloroethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
1,2-Dichloropropane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
1,3-Dichloropropane
SW 846 Method 8260D/50308
< 0.50 pg/L
7/14/2021
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
2,2-Dichloropropane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Report #:: 2021-11259 Page 1 of 6

F""O' -- Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Wood -AMEC Date of Report: Jul 26, 2021
5710 Oleander Drive, Suite 110 Customer PO #:
Wilmington NC 28405 Customer ID: 11070019
Attention: Ben Moore Report #: 2021-11259
Project ID: Hexion CLRS
2-Chlorotoluene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
4-Chlorotoluene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Benzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Bromobenzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Bromochloromethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Bromodichloromethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Bromoform
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Bromomethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Carbon tetrachloride
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Chlorobenzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Chloroethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Chloroform
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Chloromethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
cis-1,2-Dichloroethene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
cis- 1,3-Dichloropropene
SW 846 Method 8260D/50308
< 0.50 pg/L
7/14/2021
Dibromochloromethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Dibromomethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Dichlorodifluoromethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Ethylbenzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Hexachlorobutadiene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Isopropylbenzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
M+P Xylene
SW 846 Method 8260D/5030B
< 1.00 pg/L
7/14/2021
Methylene chloride
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Naphthalene
SW 846 Method 8260D/5030B
1.52 pg/L
7/14/2021
n-Butylbenzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
n-Propylbenzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
ortho-Xylene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
p-Isopropyltoluene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
sec-B utyl benzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Styrene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Report #:: 2021-11259
Page 2 of 6

envirochem
rM,
ANALYTICAL & CONSULTING CHEMISTS
Wood -AMEC
5710 Oleander Drive, Suite 110
Wilmington NC 28405
Attention: Ben Moore
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Jul 26, 2021
Customer PO #:
Customer ID: 11070019
Report #: 2021-11259
Project ID: Hexion CLRS
tert-Butyl benzene
SW 846 Method 8260D/5030B
< 0.50 Ng/L
7/14/2021
Tetrachloroethene
SW 846 Method 8260D/5030B
< 0.50 ug/L
7/14/2021
Toluene
SW 646 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Trans- 1,2-Dichloroethene
SW 846 Method 8260D/5030B
< 0.50 Ng/L
7/14/2021
Trans-1,3-dichloropropene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Trichloroethene
SW 846 Method 8260D/5030B
< 0.50 ug/L
7/14/2021
Trichlorofluoromethane
SW 846 Method 8260D/5030B
< 0.50 ug/L
7/14/2021
Vinyl chloride
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Formaldehyde
SW846 8315A
660.0 ug/L
07/09/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.09 mg/L
07/09/2021
Nitrate+Nitrite-Nitrogen
EPA353.2, Rev. 2.0,1993
0.03mg/L
07/12/2021
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
07/19/2021
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
874 mg/L
07/14/2021
Total Nitrogen
Total Nitrogen
843 mg/L
07/19/2021
Report #:: 2021-11259 Page 3 of 6

envirochem
sr�
ANALYTICAL & CONSULTING CHEMISTS
Wood -AMEC
5710 Oleander Drive, Suite 110
Wilmington NC 28405
Attention: Ben Moore
Lab ID Sample ID:
21-28014 Site: WWMW-2
Test
Sulfate
Ammonia Nitrogen
Total Dissolved Solids (TDS)
Total Phosphorus
Total Organic Carbon (TOC)
1, 1, 1,2-Tetrachloroethane
1, 1, 1 -Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1, 1 -Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Jul 26, 2021
Customer PO #:
Customer ID: 11070019
Report #: 2021-11259
Project ID: Hexion CLRS
Collect Date/Time Matrix
7/8/2021 9:30 AM Water
Method
EPA 300.0
EPA 350.1
SM 2540 C
SM 4500 P F
SM 5310 B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D15030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D15030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
Results
Sampled by
Client
Date Analyzed
1680 mg/L
07/15/2021
54.1 mg/L
07/13/2021
623 mg/L
07/08/2021
< 0.04 mg/L
07/14/2021
6.2 mg/L
07/12/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
< 0.50 pg/L
7/14/2021
Report M., 2021-11259 Page 4 of 6

Environmental Chemists, Inc.
CD.
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
[e-mail]
Wood -AMEC
5710 Oleander Drive, Suite 110
Wilmington NC 28405
Attention: Ben Moore
Date of Report: Jul 26, 2021
Customer PO #:
Customer ID: 11070019
Report #: 2021-11259
Project ID: Hexion CLRS
2-Chlorotoluene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
4-Chlorotoluene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Benzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Bromobenzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Bromochloromethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Bromodichloromethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Bromoform
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Bromomethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Carbon tetrachloride
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Chlorobenzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Chloroethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Chloroform
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Chloromethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
cis- 1,2-Dichloroethene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
cis-1,3-Dichloropropene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Dibromochloromethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Dibromomethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Dichlorodifluoromethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Ethylbenzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Hexachlorobutadiene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
lsopropyl benzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
M+P Xylene
SW 846 Method 8260D/5030B
< 1.00 pg/L
7/14/2021
Methylene chloride
SW 846 Method 8260D/6030B
< 0.50 pg/L
7/14/2021
Naphthalene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
n-Butylbenzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
n-Propylbenzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
ortho-Xylene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
p-Isopropyltoluene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
sec-B utyl benzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Styrene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Report #.: 2021-11259
Page 5 of 6

SM,
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
[e-mail]
Wood -AMEC
Date of Report: Jul 26, 2021
5710 Oleander Drive , Suite 110
Customer PO M
Wilmington NC 28405
Customer ID: 11070019
Attention: Ben Moore
Report M 2021-11259
Project ID: Hexion CLRS
tert-Butyl benzene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Tetrachloroethene
SW 846 Method 8260D/50308
< 0.50 pg/L
7/14/2021
Toluene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Trans-1,2-Dichloroethene
SW 846 Method 8260D/50306
< 0.50 pg/L
7/14/2021
Trans- 1,3-dichloropropene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Trichloroethene
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Trichlorofluoromethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Vinyl chloride
SW 846 Method 8260D/5030B
< 0.50 pg/L
7/14/2021
Formaldehyde
SW846 8315A
71.0 pg/L
07/09/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.14 mg/L
07/09/2021
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0,1993
66.5 mg/L
07/12/2021
Nitrate Nitrogen
Subtraction Method
66.4 mg/L
07/19/2021
Total Nitrogen (Calc)
Total Nitrogen
Total Nitrogen
127 mg/L
07/19/2021
Recalculated 7-26-21
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
21-28014A Site: WWMW-2
7/8/2021
9:30 AM Water Client
Test
Method
Results
Date Analyzed
Total Kjeldahl Nitrogen (TKN)
SM 4500 Norg B-2011
60.4 mg/L
07/22/2021
Comment:
Reviewed by:
Report #. 2G—
Page 6 of 6

[en7viroehem]
ANALYTICAL & CONSULTING CHEMISTS
LCS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
Wood-Amec QC - 2021-11259
Parameter
True Value
mg1L
Result
m91L
% Recovery
Limits
%
Ammonia
5.0
5.0
100
90-110
Ammonia
5.0
5.3
106
90-110
NO2
0.60
0.56
93
90-110
NO3 & NO2
1.00
1.06
106
90-110
Sulfate
50.0
47.5
95
90-110
TDS
600
612
102
90-110
TOC
10.0
10.5
105
90-110
TKN
0.50
0.55
110
90- 110
TKN
4.0
4.0
100
90-110
TP
1.60
1.64
102
90-110
MS/MSD
Parameter
True Value
mg/L
Recovery
mg/L
%
Recovery
%
Difference
Limits %
Recovery
Limits %
Difference
Ammonia
5.0
5.015.0
100/ 100
0
80-120
< 20
Ammonia
10.0
11.0/9.3
110/93
17
80-120
<20
NO2
0.50
0.50/0.49
100/98
2
80-120
<20
NO3 & NO2
0.50
0.53/0.54
106/108
2
80-120
<20
Sulfate
10.0
11.6/11.6
116/116
0
80-120
<20
TDS
75.0
82.0
109
N/A
80-120
<20
TOC
10.0
11.0
110
N/A
N/A
<20
TKN
10.0
10.4
104
N/A
N/A
<20
TKN
4.0
4.0/4.1
100/ 102
2
N/A
< 20
TP
2.50
2.30/2.38
92/95
3 1
80-120
<20

Environmental Chemists, Inc.
envirochem
ANALYTICAL & CONSULTING CHEMISTS
DUPLICATE SAMPLES
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
Parameter
Results,L
g
% Difference
Limits %
Ammonia
N/A
N/A
N/A
< 10
Ammonia
NIA
N/A
N/A
N/A
NO2
N/A
N/A
NIA
< 10
NO3 & NO2
NIA
N/A
N/A
< 20
Sulfate
48.0
48.0
0
<10
TDS
406
401
1
<10
TOC
6.2
6.0
3
<10
TKN
N/A
N/A
N/A
<10
TKN
N/A
N/A
N/A
<10
TP
N/A
N/A
N/A
<10
BLANK
Parameter
Results
M91L
Limit
M91L
Ammonia
<0.1
0.1
Ammonia
0.055
0.05
NO2
<0.01
0.01
NO3 & NO2
<0.01
0.01
Sulfate
<2.5
2.5
TDS
<2.5
2.5
TOC
<0.25
0.25
TKN
<0.25
0.25
TKN
<0.25
0.25
TP
<0.02
0.02

Analytical Environmental Services, Inc
Date: 15-Jul-21
Client:
Environmental Chemists, Inc.
Client Sample ID:
21-28013
Project Name:
2021-11259
Collection Date:
7/8/2021 10:00:00 AM
Lab ID:
2107893-001
Matrix:
Aqueous
Reporting Dilution
Analyses Result Qual Units BatchlD Date Analyzed Analyst
Limit Factor
Formaldehyde by SW8315A
Formaldehyde 660 50 ug/L 318632 1 07/09/202118:51 RF
Qualifien: • Value exceeds maximum contaminant level
BRL Below reporting limn
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Nair See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporung Limn
Page 4 of 9

Analytical Environmental Services, Inc
Date: 15-Jul-21
Client:
Environmental Chemists, Inc.
Client Sample ID:
21-28014
Project Name:
2021-11259
Collection Date:
7/8/2021 9:30:00 AM
Lab ID:
2107893-002
Matrix:
Aqueous
Reporting Dilution
Analyses Result Limit Qual Units BatchID Factor Date Analyzed Analyst
Formaldehyde by SW8315A
Formaldehyde 71 50 ug/L 318632 1 07/09/202119:19 RF
Qualifien: • Value exceeds maximum contaminant level E Estimated (value above quantiti tion range)
BRL Below reporting limit S Spike Recovery outside limits due to matrix
H Holding times for preparation or analysts exceeded Narr See case narrative
N Analyte not NELAC certified F Analyzed in the lab which is a deviation from the method
B Analyte detected in the associated method blank < Less than Result value
> Greater than Result value J Estimated value detected below Reporting Limn
Page 5 of 9

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: Wb — 'C I Date: � �% Report Number: — j �j
Receipt of sample:
ECHEM Pickup ❑ Client Delivery
UPS ❑ FedEx ❑ Other ❑
❑ YES
❑
NO
N/A
11. Were custody seals present on the cooler?
❑ YES
10
NO
X N/A
2. If custody seals were present, were they intact/unbroken?
temperature upon receipt °C Corrected temperature upon receipt
1Original
How temperature taken:
❑ Temperature Blank EFT Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES
I ❑
NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
10
NO
4. Were proper custody procedures (relinquished/received) followed?
14 YES
10
NO
5. Were sample ID's listed on the COC?
14 YES
10
NO
6. Were samples ID's listed on sample containers?
YES
I ❑
NO
7. Were collection date and time listed on the COC?
YES
ID
NO
8. Were tests to be performed listed on the COC?
YES
ID
NO
9. Did samples arrive in proper containers for each test?
YES
ID
NO 110. Did samples arrive in good condition for each test?
YES
10
NO 111. Was adequate sample volume availableT
YES
I ❑
NO 112. Were samples received within proper holding time for requested tests?
YES
ID
NO 113. Were acid preserved samples received at a pH of <2?
❑ YES
I ❑
NO 114. Were cyanide samples received at a pH >12?
❑ YES
10
NO 115. Were sulfide samples received at a pH >9?
YES
10
NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑
NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
ID
NO 118. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
°C

C ,
Analytical & Consulting Chemists
Client: W'00 r
ADDRESS:,,_ 1�
Sampled By:
I —
Sample Identification
wVa'mU�"
ENVIRONMENTAL CHEMISTS, 6602WindmillWa Wilmington, 5 I
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION ISTS I N Cj OFFICE: 910-392- 2231 FAX [phone]
# 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
PROJECT NAME: a
REPORT NO: oZI—
CONTACT NAME: �U PO NO: REPORT TO: { L-'/FAX:
C' COPY TPHON
O: t'f D.S
email: SAMPLE TYPE• I
Collection
o
- Influent,
E = Effluent,
W =Well,
ST = Stream,
SO =Soil, SL =Sludge, Other:
T
O '�°
f`
�,
C
W
PRESERVATION
Date Time Temp
N
a
E
E
o 0
' a
o
o a
J
o rn
c E
"
O
a
`o
m m
D
S Z
w
_
z J o p
o
zp o it W
ANALYSIS REQUESTED
a
z°
= i
z � w �
LL o
P
W
80/.3
NOTICE - DECHLORINATION: Samples for
Transfer
2.
V>L
Mw
0180�
I C P
G
C P
G �—
C P
G G
C P
G G
la, TKN, Cyanide, Phenol and Bacteria must be dechlorinated (0.5 ppm or
Relin�tiiehed-By., Date/Time
• c•11Ncrawre wnen Received °C:
Delivered By: Accepted:�
Comments: Received By:
5 Ui
<a•
G tQ PI < a • <0
F;. z ZAct,
in the field at the time of collection. See reverse for Instructions
Received By: Date/Time
cted: Resam a equested:
Date: $ 21 Time: /07
TUR AROUND:

Environmental Chemists, Incl,
sty,
A ALYTIC. L & CONSULTINGCHEMISTS
6602 Windmill v'Va . lil ingto , `tiC 28405 * 910,392,0223 Lab - 910392.4424 Fax
7l0 c wsnh ern Road, Manteo, NC 27 54 - 2 2. 73 5 { 2 1-ab / Pax
255-AWilrnington Highway, ackson:rilie, NC 23541 * 910.3 7.58 3 Lab/Fax
infc>r;en,i®cnm ntalchemists,c m
nood -AMEC
Date ofReport: Mar 2, 22
5710 Oleander Drive, Suite 110
Customer PO #:
Wilmington NC 28405
Customer ; 11701
Attention: Ben Moore
Report ; 2020-04002
Project l; Hexion CLRS
Lab ID Sample ID:
Collect Date/Time MWINply
2009761 Sites NMVWI
3/1 /2
Water Ben Moore
Test
MeBod
Resultsate Analyzed
Sulfate
EPA NO-0
779 rig/L
3/12/2 2
Ammonia Nitrogen
EPA 3511
783 /L
/23/2 2
Total Dissolved Bonds i ` ;
SM240C
11 /L
3/ i /2 2
Toth Hosphows
S 450 P r
2,12 m/L
3/2/22
Total Organic Carbon
SM 59 a
mg/L03/11/2020
1,1,12-T tr for th n
V 846 method 82608/5030B
<2 ply/L
3/17/2 2
9; 1 -Trichloroethane
SW 846 method 8265 15030B
<2 /L
3/17r2 2
1,1,22mT tr l r t
W 546 method 826OB15030B
< /L03/17/2020
, 12-Trichloroethane
SW546method 8zsc t503B
<2 ;
3/17t2 2
1 . 1 -Dich loroethane
SW 846 method 8260B,5030B
<2 /L03/17/2020
1,1-Dichloroethene
SW 846 method 826O /5 0
<2 ply/L
3/17/ 2
1,1® i l l r pr p n
W 846 method 8260B/5 30
<2 lag/L
/17/2 2
12,3-Tr4c E ro n n
W B46method 260B/5030
< /L03/17/2020
1,2,3-Trichloropropane
SW 646 method 626OB/5630
<2 /L
3/1712 20
1,2,4-Trichlorobenzene
Sof 846 method 826r5 34B
<2 1L
3/17/2 2
1,2,4- raih1 t
846 method 826 /5030
<2 p /L
3/1 12 2
12- Di rom - ® nl r pr p rt
SW 346 method 8260 /5030
<2 ply/L
03/17/2020
1 2-Dibrornoethane
SW 846 method 826 B!5030B
<2 /L
03/1 /2 2
1,2m i l l r n
W 6-46method 826ti /5030
<2 p/L
3117/2 2
12-1 , loro t%
e; 3-46 € eth d 826O /56'3
<2 p /L
3/ 17/2 2
1 ,2- ichl r pr p n
Sim 346 method 8260W5030B
<2 /L
3/1 i /2 2
t3,5-Trimethylbenzene
SW 846 method 8260 s5d3
<2 /L
3/17/ 2
1,3-Dichlorobenzene
SW 846 meshed 826OB15030
< /L03/17/2020
1,3-Dichicgopropane
SW 846 method 826OB/5030B
<2p° tL
OV7/2 2
1,4-Dichlorobenzene
SW 346method 8266 15030
<2 g/L
3/17F2 2
2,2-Dichloropropane
SW 46 method d 92 0 ,`5030
<2 leg/L
3/17/2 20
Report , 2520-42 Page 146

ANALYTICAL & CONSULTINGHEWST
Environmental Chemists, Inc.
66;1�2 Windmill way, ,NV lm`tt�n, NC 2 405 a 910.392,0223 Lab a 91 0.32 442=i Fax
710 Bowsertown Road, Man_co, NC 27 54 a 252,473,5702 Lab Fax
255-Al/Vilmington Highway, Jacksonville, NC" 28540 * 91 17,58 3 Lab/Fax
tf b(( e,n .,iro til ntalc emi,,tu.c o ,
Wood -AMEC
Date ofReport: tsar 24, 2320
713 Oleander Drive, Suite 110Customer
Wilmington NC 28405
Customer e 11070019
Aftentioni Ben Moon
Report s 2020-04002
Project a Hexion CLRS
2-Chlorotoluene
SW 845 method 26O /5 30
<2 /L
3117/202
4-Chlorotoluene
SW 846 method 8260B15030B
<2 p /L
3/1 7 /2 2
Benzene
SW 846 method 826OB15 335
<2 p /L
3/17/2 2
Bromobenzene
SW 846 method 826OB15030B
<2 /L
3,117/2 2
Bromochloromethane
SW 846 method 8260B150388
e2 /L
3/17/2 2
Bromodichloromethane
SW 846 methmethoo 82608/5 30B
<2 ply/L
3/17/2 2
Bromogform
SW 846 method 826O /5 30
<2 /L
3/17/2 2
Bromomethane
SW 64e. method 8260 /5030B
<2 /L03/17/2020
Carbon tetrachloride
SW 846 melt 82 B/5020
<2 ply/L
3/17/2020
Chlorobenzene
SW 646 method 826OB/5030B
<2 lag/L
03/17/2 2
Chloroethane
SW 846 me hod 82601V50308
<2 ply/L
3/17/2 2
Chlorofol,m
SW 846 method 8260Bi 0i353
<2 pg/L
3/ 7/2 2
Chlor mt ri
SW 346 method 8260B15030B
<2 /L
l 3/1 7 /2 2
i A 2-Dichloroethene
SW 846 method 826OB/5030B
<2 p /L03/17/2020
cis- i0® i hlor prop n
SW 846 method 826 B15038B
<2 w /L
3/17/2 2
Dibromochloromethane
Sof 846 method 8260B15030B
<2 p /L
3/17/2 2
Dibromomethane
SW 846 method 8260B/5030B
<2 p /L
3/17/2 2
Dichlorodifluoromethane
W 846 method 8260B/5030B
<2 /L03/17/2020
Ethylbenzene
SW 846 method 8260B/5030B
<2 p /L03/17/2020
Hexachlorobutadiene
SW 846 method 8260B/5030B
<2 /L
03/17/2020
Isopropylbenzene
SW 846 method 826OB15030B
<2 w /L
33/17/2 2
M+P Xylene
SW 846me' hod 8260B/5030B
<4 ply/L
0 /17/2 2
Methylene chloride
SW 846 method 82BOB1503 B
<2 /03/17/2020
Naphthalene
SW 846 method 826OB15030B
<2 g/L
3/17/2 2
rt-Butylbenzene
SW 846 method 8260B/5030B
<2 pgiL
3/1712 2
n-Propylbenzene
SW 846 method 8263B15330B
<2 /1.
03/17/2020
ortho-Xylene
SW 846 method 826OB15030B
<2 g/L
3/17/2 2
r abn 3..
=i sc.1p c,py1LtaS LaeI e
;lei _ A mo-thr €;7ROBI5i 1OR
- _
ar it
sv �.s sc..
W111 "7P)020
cf.�r , :.—
c t tyl nzen
SW 846 method 8260B,5030B
<2 ply/L
3/17/2 2
Styrene
SW 846 method 8260B15030B
<2 /L
03f 17/2 2
Report : 2020-040 2
Page 2 of

Environmental Chemists, Inc.
6602 Windmill'Are v, M:, gton NC 2840 o c i).- 9 02' .3 Lab � 903 2 Fax
710 o s -to n Road, , anteo, NC 27954 s 252.47 3.570 ! a 1 Flix
255A W,lmsng'-Ic.n I-iirwi%1acksc,nvillc, — 28��G a 903_. ,5847, Lab , Fax
ANALYTICAL & CONSULTING CHEMISTS
Wood -AMEC
Date of Report, Mar 24, 21020
5710 Oleander Drive, Suite 110
Customer PO #:
Wilmington NC 28405
Customer ; 1171
Attention-, Berg Moore
Report2020-04002
Project : Hexion CLRS
tert-Buttylbenzene
SW 846 method 826OB15030B
< /L
3/17/2 2
Tetrachloroethene
SW 846 method 626 1 Q36
< /L
31 17/2 2
Toluene
SW 846 method 82608,'50308
<2 ply/L
3117/2 2
Trans-12-Dichloroethene
SW 846 method 826OB/50308<2
/L
03/17/2020
Trans- 1, - ich loropropene
SVV846 method 826 Br o30
2 /L
/17,2 20
ii hl r th
l 646 method 8260!603
2 /L
3/17/202
Trichlorofluoromethane
5W W method 264 / 03v
<2 g/L
3/1712 2
Vinyl chloride
SW 846 method 8260B15030B
<2 leg/L
3117/2 2
Formaldehyde
S 2646 9-315A
120,0 g/L
03/13/2020
Nitrate Nitres (Cale)
Nitrite Nitrogen
EPA 35',2
0,02 mg/
3/10/2 2
Nitrate+ irit ®ltr g
EPA35.2
0,32 g/
3/1 /2 2
Nitrate Nitrogen
Subtraction teat
_3 rig/
3/23/ 20
e ort #: 2620-043 2 Page 3 v§ 6

Environmental Chemists, Inc.
66A2 Windmill Wav, Wilniin ;ton , NC 28405 - 910 392,022,; Lab e 9 ), ,92 4424 Fax
{10 Bowsertown Road, Manteo, NC ?795' e 25 2, 73.5702 _a",,` =ax
25-5-A Wilmington Highway, Jacksonville, NC 2 540 - 910,347,5843 Lab/Fa
ANALYTICAL CONSULTING CHEWSTS
Test
Method
Resuft
Date Analyzed
Sulfate
EPA 305.0
1 06 g/L
3/12/2 20
Ammonia Nitrogen
EPA 358,1
34,3 tag/L
3/ 3/2 2(
Total Dissolved Solids {'ADS)
SM 25440 C
362 g/L
3/1/2 20
Total Phosphorus
SM 46 G P r
0,3 g/L
3/2 /2 2
Total Organic Carbon (T )
SM 5310 B
5,2 rig/L
3/11/202
i ,1 ; 1,2-Tetrachloroethane
SW 846 methw2608/50 0B
< _pg/L03/12/2020
1 1 , 1 -Trichloroethane
SAW 846 method 828 /5030
< ,5 pg/L
3/12/2 2
1 ,1 ,22-- ` tr hlor th
SW 846 method 826OB/ 030
< ,5 pg/L
03/ 12/2 2
1, 1,2-Trichloroethane
Sty 846 method 28O t5030B
< ,5 pg/L
3/12/2 2
1.1- i hloro th n
SW e-4 method 82 Ost5 30B
< .5 pg/L
3/12/2 2
M-Dichloroethene
SW846method 826O 150338
< ,5pg/L
3/12/2 2
1,1-Dichloropropene
SW 846 method 82 OB154'30
< ,5 pg/L
3/12/2 2
1,2,3-Trichlorobenzene
SW846method 8 8O /5030B
< ,5p /L03/412/2020
12,3- ri hloroprop r
Ste{ 846 method 8260B,5030B
< ,5 pg/L
3/12/2 2
12, -Tri hl rob ?
Sty 846 method 8260t5030
< .5 /L
03/12/2020
1,2,4-Trimethylbenzene
SUS 846 method 826OB15 30
.5 pg/L
3/12/2 2
1.2- ibr m m3- hl ropr p ne
SW 846 method 82 cBtu 0
< .5 pg/L
3/12/2 2
1,2-Dibromoethane
SW 846 method 82 B/503 B
< ,5 /L
/1 / 2
.2-Dichlorobenzene
Sri 846 method 826OB/5 3
< .5 pg/L03,112/2020
12- i hlor th n
SW 846 method 826OB/5030B
< .5 pg/L03/12/2020
1,2-Dichloroproparte
SW 88#44 i method 828OB/5030
<0 5 pg/L
3/12/2 2
1,3,5- rir othylb o
W 846 method 82 OBi5030
< ,5 pg/L.
3/1 /2
1,3-Dichlorobenzene
SW 646 method8260B/5030
< ,5pg/L
03/1 / 2
1,3-Dichloropropane
SW 846 mete 2 Bt5c30
< ,5 pg/L
03/12/2020
1, ffi s l lorob r
� 84 method 8 6OB/5030B
� ,5 pg/L
3/1 /2 2
2- i hior prop
SW 846 melhoo 826OB/5030B<
,5 pg/L
3/12/2 2
Report :: 2820- 4002 rage 4 of

ANALYTICAL & CONSULTING CHEMSTS
Environmental Chemists, Inc.
6602 Windmill V ,T, ;'m�ngton, TC' 4 )5 e 9-10,391022311ab 0 910,292,4424 Fax
710 o� serto- n Road, Manteo, NC 27994 o 252,473 '," 1 1 / c�ax
255 A it ngton High, av, Jacksonville, - C 28;40 a 91E .3 7,5843 Lab,_ Fax
Fca a envi ronment a 1c h re sts co
Wood -EC-AMEC
Date of Report, Mar 2, 2020
5710 Oleander Drive , Suite 110
Customer PO #:
WilmingtOn NC 28405
Customer : 110170019
It tl ; Ben Moors
Report : 2020-04002
Project g Hexion CLRS
2-Chlorotoluene
SW 846 €teen£ d 826OB15030B
,5 g/L
3/12/2 2
hl r t 11
SW 846 !method 826OB15030B
,5 g/L
3/12/2020
Benzene
SW 846 method 826131 03
g ,5 ug/L
3112/2 2
romobe zen
S 1846 method 82608/5030
< ,5 g/L
3/12/2 2
Bromochloromethane
SW 846 method 82 0B,'503
<:,5 g/L
03/12/2020
Bromodichloromethane
SW 846 method 8260B1503 3
<0,5 g1L
03/12/2020
Bromoform
SW 846 met -nod 8260 /5030B
< ,5 g/L
3/1 /2 2
Bromomethane
SW 846 method 826OB15030B
< ,5 g/L03/12/2020
Carbon tetrachloride
SW 846 method 826O 15ou B
,5 g/L
3/1 1202
Chlorobenzene
SW 846 method 82 0 /503 B
< ,5 g/L
3/1 /2 2
Chloroethane
SW 846 method 828O 15Q30B
< ,5 leg/L
3/12,2 2
, ,,
kl r-fora
SW 846 method 826 Ei5d3 €3
< ,5 g/L
3112/2 22
hl l` r th
SW 846 meted 8286515030S
< ,5 g/L
3/1 /2 2
cis-126Do hlor th n
SW 846 method 8266 5830
< .5 g/L
03/12/2020
cis-1,3-Dichloropropene
SW BA6 method 82 0B/5G 4B
< ,5 g/L
3/12/2 2
Dibromochloromethane
SW 646 method 826 B/5 30B
< ,5 Isg1L
3/1 /2 2{
Di r mom t£ Fame
Sol 846 Method 826OB15030B
< ,5 leg/L
03/12/2 2
€chlor d flilC7€'C3m th n
SW 846 method 8260B/5030B
< ,5 g/L
3/1 /2 2
Ethylbenzene
SW 846 method 826OB15030B
< .5 leg/
3/12/2 2
Hexachlorobutadiene
SW 845 method 826OB15030B
< , g/L
3/1 /2 /2
1sopropylbenzene
SW 846 method 826OB15030B
< .5 g/L
3/ 121202
M+P Xylene
SW 846 method 826OB1503
<1 .O 3grL
3/12/2 2
Methylene h pride
SW 846 method 826 B150 0B
<:,5 g/L
3/12/2 2
Naphthalene
SW 846 method 826 t315030
< ,5 g/L
3/ 1 /2 21
n-Butylbenzene
SAI 8A6 method 82 0B/503'8
< ,5 g/L03/12/2020
n-Propylbenzene
SW 846 method 8266B158388
< ,5 pg1L
3/12/2 2
ortho-Xylene
SW 848 method 8260B15030B
< ,5 g/L
03/12/ 2
p lsopropyltol <
�,r-1 �ii�1@ 1.6�3� "aiii$d�l #
SW 846 me hod 26 E1 030B
on ,in-/i
_ � is
03/12/202
sec-Butylbenzene
SW 8A6 method 8260B,1503013
< ,5 g/L
3112/2 2
Styrene
SW 846 method 8260-R,5030B
<0 5 PgAL
3i1212 20
eprrt :: 2 a20-04882
Page 6 of 6

Environmental Chemists, Inc.
6602 jL?indmi' !V , WiiniingtO NC "}8405 * 9 ;.3 ' 0 23 Lab 0 910 392.44241 ax
10 ovN se `own Road, Nl.1I=wo, NC 2.19q1 o 292,4'-1,570'. Lab/Fax
255 -: Wilming�,ton Highway, Tac sonv ilia', NC 28540 o 910 .242,284? r ab/Tax
ANALYTICAL & CONSULTING CHIENSTS
Toluene
SOU 346 method 82 0I ,/5030B
<: g/L
03/12/2 2
ran -1 ,2® l l?I r o then
W 846 method 82 GB115030B
<3,5 pg/L3/1212
2
``r rt a1,3- t hC' r
Sita46 me'nod 826086030B<M
pg/
3/1 /2 2
Trichloroethene
SW 846 method 6263 /503 B
< . pg/L
3/12/2 2
Trichlorofluoromethane
SW BA6 method 82608.5030E
<0,5 pgiL
3/12/2 2
Vinyl chloride
SW 846 method 8 60B/5030
<0, /L
03/12,12020
Formaldehyde
84€ 6315A
<50 pg/L3/13/2
2
Nitrate Nitrogen 1
Nitrite Nitrogen
EPA 353.2
0,03 r g/
3/1 /2 2
itr t +Nitrit - Itr g n
EPA 353,2
29,5 mg/L
3,1 12 2
Re or` #: 2326- 4002 Page 6 of 6

Wood- A - ec QC - M2 -04002
LCS
'rue 1''
Result esult
% Recovery
Limits
Parameter
rt2gt
agar
%
Ammonia
5.0
5.0
100
90-1 10 �
02
0.60
0,61
102
90-110
NO3 & NCB`?
1.00
0,93
93
90-110
Sulfate
50,0 �
6,7
93
90-1 !0
T
-------------------
600
5b6
94
90- 1 10
TOC
10,0
10.9
109
90-1 10
TP
1 1,60
1.57
98
90-110
MS/MSD
�
%
True ''aloe
Recovery
%
Limits %
T imits %
Parameter
Rey overt/
mg, L
mg1L
Dykrence
Recovery �
Diff�rence
Ammonia
5.0
4,9/4= 8
98/96
2
80-120
<20
%02
0.50
0.5110,52
10"r 10
2
80-120
< 20
NO3 & NO2
0.50
0.51 /0.49
; 1021/98
4
80-120
< 20
Sulfate
10,0
9.019.0
90190
0
1 80-120
<20
TDS
N/A
N/A
NIA
N/A
80_ 120
< 20
TOCMe
10.9
109
f A
N/A
< 20
T
1,60
7W 1.76
i
106;` 110
4
80=120
< 20

Ammonia
N/A
NA
/A
<10
N 027
N/A
/A
N/A
< i o
O3 & NO'-)
/A
1A
N/A
< 20
Sulfate
N/A
N A
/A
<10
TICS
1150.00
1166,00
1
< 10
TOC
4,9
4
<10
TP
N/A
N/A i
N/A
<10
BLANK
Results
Limit
Parameter
Ammonia
<0.1
0.1
NO2
<0.01
0.01
Sulfate 2
1 5
2.5
TICS
<2.5
2.5
T C
<0.25
0.25
TP
<0.02
0.02

Analytical Environmental Services, Inc
Client: Environmental Chemists, Inc.
ProjectName: 20-097614HORMIJINGIUM
Lab ID: 2003D35-001
analyses Result
Formaldehyde by SW8315A
Formaldehyde 120
f, ..Hfiem Vatze exceeds m—ifnam contamicant eevzt
EitL Belo,, epo ung lirak
H r ci ding times .`or preparation or -slys s exceeded
ti Anahvte-,t NELAC ,enTfiied
B inaiyte dereco,d in rite as=_eiated method Mark
Greater tha€r Resat v.tl-
date; 18-t ar-20
Client Sample ID: 20-09761 �
Collection Bate: 3/10/2020 9:45:00 M
Matrix: Aqueous
Reporting €fiDilution
Limit nal [`nits €tatcbli) DateAnalyzed Analyst
Factor
56 ug(L 293865 i 03113f2020 19,13 HL
E Est; na€ed (hive ab.,e q-nnutio. range)
S Spke Recovery outside €smits due to 3aatsix
4arr See case narratme
F ,'Anaiyzen in the No wh;,-.h
I—, ;han Rmit valve
EFnnnat ci -1u-- detested belccu Re; ;€ ng €.tmot

Analytical Environmental Services, Inc
Client- Environmental Chemists, Inc.
Project Name: . r `20-09778 �. _,-
Lab ID: 2003D-15-002
Analyses Result
Formaldehyde by SW8315A
Formaldehyde BRL
QuaiiCees: Value sxceeds ma—num comarti Want level
BRL t3alosv rep.rtmg ' ;nit
H i-loidilty times f<,r f reparation or maiys,s exceeded
N gals-te t VELA(c tiistd
E3 =,na'.titz deterred in the asE-3-ted medwd blank_
C-_:aeu &'ml R_SVit'aide
Irate: l 8-Mar-20
Client Sample ID: 20-09778
Collection hate: s/ 10i2020 9:30:00 AM [
Matrix: aqueous
Reporting Dilution
Limit mit Qua[ Units l3afchlD `actor l�ate.tmtalyzed Analyst
50 uv3 293865 1 03/13.%2020 2°:27 HL
E E.,wii Yed (,td- abo,e Gaantitat= €.,nge)
S Spike Rt,co-, outside limits due to ,-znx
Nary See case narrative
Les, thar R=es,jk value
Estimated value detected bel— Reporting L_trait

Environmental chemist, Inc., Wilmington, NC Lab #94
602 Windmill Way
Wilmington, NC 28405
.2.22
F% V11 1E A
2L,
-ReportClient:
Date-
—0-- Number -
Receipt sample:UPS
_. s
Delivered 13 •
f• ^ . - - • .
- b
- -
.
r # • #
# # a
III Jill I
- #
•• t
TOC/Volatiles are PH checked
l3acteina samples are checked
at time of analysis and recorded on the benchsheet,
for
Chlorine at time of analysis # recorded on the benchsheet
'Sample ' #
• - ' i •
• - •
be co
Sami LL ctly preserved
...•i
•
fs were adjusted accordingly
by
.'s„..

ENVIRONMENTAL CHEMISTS,
6602 Windmill Way Wilmington, INC 28406
INC OFFICE: 910-392-0223 FAX [phone]
NCDENW 0WQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info @environmentalchemists.corn
Analytical & Consuffing Chemists
COLLECTION AND CHAIN OF CUSTODY1.
Client: a
PROJECT NAME:
REPORT NO:
c
ADDRESS: k 'I
CONTACT NAME:
PO NO: o
y
: 4
REPORT TO �"
..... . . . ...
PHONE/FAX
Viv,ce.
COPY TO:
email:
Sampled �I ped B
SAMPLE TYW I Influent, E Effluent W Well, ST = Stream, SO Soil, SL Sludge, Other:
PRESERVATION
Identification
Sa e dentificat on
Sample
lo z E (D C j CL —W
a 'C �6' CD
E 8 a z
X 0 ANALYSIS REQUESTED
-0 0
<2
E 0 C 'r 0
=)
z z
z < 4
x z
Date
Time Temp
C P
G.,
C
G
C P
=7
C P
'G-
C �\
G
Jt'
G
P
C
C P
G G
Transfer
Relinquished By- Dateiiirne
Received By: Date[Time
P
Temper8ture when Received ,:; 7
*C:—L- —Accepted: —Rejected:
Resample Requested:
Delivered
Date: ---- Time :
Comments:
TURNAROUND:

ENVIRONMENTAL CHEMISTS, INC
6602 ndmill Way Wil, NC 28405
ingtonX
OFFICE:Wi910-392-0223 FmA
910-392-4424
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: US CERTIFICATION # 37729
[e-mail]
Analytical & Consulting Chemists
COLLECTION AND CHAIN OF CUSTODY
2, U) - 6 va
Client: u" U"), 0
PROJECT NAME: Ike`„ ........ . . .. ....
REPORT NO:
ADDRESS:
CONTACT NAME:
PO NO:
REPORT TO:
PHONE1FAX:
")A
T 0:
email: 9
JCOPY
By:
SAMPIfE I Influen E Effluent, W Well, ST = Stream, SO Soil, SL Sludge, Other:
TYPE:Sampled
Collection
PRESERVATION
Sample Identification
a 0 e UJ
0 2 z 0
=02.06-
0 W ANALYSIS REQUESTED
E a C 0
0 0 a� = J D 0 z
1-:-, z z
Date
Time
Te
0
`7 I �777
C P
—0�
.
. ......... .
..........
G
P
n kv,
C P
C
,:5
Z�
J 14
G
C P
G
------TT1-TT
c P ---
I
F --- Fl-­--�
G G
Transfer Relinquished B­ Date/Time
P
Temperature when Received OC:_2_iAccepted: -Rejected:
Delivered B
y ------Received By:
Comments,
Date/Tirne
77-7-
Resample Requested:_
.Date: Time:
TURNAR*UND: �

(sri;
ANALYTICAL & CONSULTING CHEMISTS
1117 0
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab o 910.392.44424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252,473,5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 o 910.347.5843 Lab/Fax
[e-mail]
Wood -AMEC Date of Report: Apr 06, 2021
5710 Oleander Drive, Suite 110 Customer PO #:
Wilmington NC 28406 Customer ID: 11070019
Attention: Report #: 2021-04441
Project ID: Hexion CLRS
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
21-10940 Site: WWMW-2 3/17/2021 10:00 AM Water Ben Moore
Test Method Results Date Analyzed
Sulfate
EPA 300.0
516 mg/L
03/17/2021
Total Dissolved Solids (TDS)
SM 2640 c
950 mg/L
03/18/2021
Total Phosphorus
SM 450D P F
0.08 mg/L
03/25/2021
Total Organic Carbon (TOC)
SM 5310 B
6.2 mg/L
03122/2021
1, 1, 1,2-Tetrachtoroethane
SW 646 method 8260815030B
<0.5pg/L
03/18/2021
1, 1, 1 -Trichloroethane
SW 846 methodB26OB15030B
<0.5pg/L
03116/2021
1,1,2,2-Tetrachloroethane
SW 846 method 826OB15030B
<0.5pg/L
03/18/2021
1,1,2-Trichloroethane
SW 846 method 8260815030E
<0.5 pg/L
03/18/2021
1, 1 -Dichloroethane
SW 846 method 826OB15030B
<0,5 pg1L
03/18/2021
1,1-Dichloroethene
SW 846 method 82608150308
<0.5 pg/L
03/18/2021
1,1-Dichloropropane
SW 646 method 82BOB16030B
<0.5 pg/L
03/18/2021
1,2,3-Trlchlorobenzene
SW 846 method 82608/60308
<0.5 pg/L
03/18/2021
1,2,3-Trichooropropane
SW 848 method 82608150308
<0.5 pg/L
03/18/2021
1,2,4-Trichlorobenzene
SW 846 method 8280B15030B
<0.5 pg/L
03/1812021
1,2,4-Trimethylbenzene
SW 846 method 82608160308
<0.5 pg/L
03/18/2021
1,2-Dibromo-3-Chloropropane
SW 846 method 0260815030B
<0.5 pg/L
03/18/2021
1,2-Dibromoethane
SW 846 method 8260131503013
<Q,5 pg/L
03/18/2021
1,2-Dichlorobenzene
SW 846 method 8266131503013
<0.5 pg/L
03/18/2021
1,2-Dichloroethane
SW 846 method 82BOB15030B
<0.5 pg/L
03/18/2021
1,2-Dichloropropane
SW 846 method 826OB16030B
<0,5 pg/L
03/18/2021
1,3,5-Trimethylbenzene
SW 846 method 8260131503013
<0,5 pg/L
03/18/2021
1,3-Dichlorobenzene
SW 846 method 826OB15030B
<0.5 pg/L
03/18/2021
1,3-Dichloropropane
SW 846 method 82608150308
<0.5 pg/L
03/18/2021
1,4-Dichlorobenzene
SW 846 method 8260131603013
<0.5 pg/L
03/18/2021
2,2-Dichloropropane
SW 846 method 82608150308
<Q,5 pg/L
03/18/2021
2-Chlorotoluene
SW 846 method 82000160308
<0,5 pg/L
03/18/2021
Report #:: 2021-04441 Page i of 7

(sly
ANALYTICAL & CONSULTING CHEMISTS
Environmentale
6602 Windmill Way, Wilmington, NC 28405 ® 910.392.0223 Lab a 910.392.4424 Fax
710 Bowseztown Road, Manteo, NC 27954 9 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 m 910.347.5843 Lab/Fax
inI'o@enviran men talchernists.con-1
Wood -AMEC
Date of Report: Apr 06, 2021
5710 Oleander Drive, Suite 110
Customer PO M
Wilmington NC 28405
Customer ID: 11070019
Attention:
Report #: 2021-04441
Project ID: Hexion CLRS
2-Hexanone
SW 846 method 826OB15030B
<2.5 pg/L
03/18/2021
4-Chlorotoluene
SW 846 method 8260815030E
<0.5 pg/L
03/18/2021
Acetone
SW 846 method 8280615030E
<2.5 pg/L
03118/2021
Acrolein
SW 846 method 826OB15030B
<5 pg/L
03/18/2021
Acrylonitrlle
SW 846 method 82608/5030B
<5 pg/L
03/18/2021
Benzene
SW 846 method 8260E15030B
<0.5 pg/L
03/1812021
Bromobenzene
SW 846 method 82609/5030B
<0.5 pg/L
03/18/2021
Bromochloromethane
SW 846 method 826OB160308
<0,5 pg/L
03/18/2021
Bromodichloromethane
SW 846 method 020UB/5030B
<0.5 pg/L
03/18/2021
Bromoform
SW 846 method 626081503013
<0.5 pg/L
03/18/2021
Bromomethane
SW 846 method 8260815030E
<0.5 pg/L
03/18/2021
Carbon Disulfide
SW 846 method 826OB15030B
<0.5 pg/L
03/18/2021
Carbon tetrachloride
SW 846 method 8260815030E
<0.5 pg/L
03/18/2021
Chlorobenzene
SW 846 method 826OB15030B
<0.5 pg/L
03/18/2021
Chloroethane
SW 846 method 82608150308
<0,5 pg/L
03/18/2021
Chloroform
SW 846 method 826OB16030D
<0,5pg/L
03/18/2021
Chloromethane
SW 846 method 820OB150309
<0.5 pg/L
03/18/2021
C15-1,2-Dichloroethene
SW 846 method 826ont6o3oo
<0.5 pg/L
03/18/2021
cis-1,3-Dichloropropene
SW 846 method 826OB15030B
<0.5 pg/L
03/18/2021
Dibromochloromethane
SW 846 method 8260B15030B
<0.5 pg/L
03/18/2021
Dibromomethane
SW 846 method 826OB150308
<0.5 pg/L
0311812021
Dichlorodifluoromethane
SW 846 method 826013I503013
<0.5 pg1L
03/18/2021
Ethylbenzene
SW 846 method 82BOB/5030B
<0.5 pg/L
03/18/2021
Hexachlorobutadiene
SW 846 method 82BOB15030B
<0 5 pg/L
03/18/2021
IPE
SW 846 method 826OB15030B
<0.6 pg/L
03/18/2021
lsopropyl benzene
SW 846 method 8260B150308
<0.6 pg/L
03/18/2021
M+P Xylene
SW 846 method 8260815030E
<1.0 pg/L
03/18/2021
MEK
SW 846 method 826013/503013
<2.5 pg/L
03/18/2021
Methylene chloride
SW 846 method 8260015030E
<0.5 pg/L
03/18/2021
MiBK
SW 846 method 8260BI5030B
<2.5 pg/L
03/18/2021
Report fl:: 2021-04441 Page 2 of 7

ANALYTICAL & CONSULTING CHEMISTS
Environmental Inc.
6602 Windmill Way, Wilmington, NC 28405 d 910.392,0223 Lab ° 910-392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 O 252.473.5702 Lab/Fax
255-A WiIniington Highway, Jacksonville, NC 28540 9 910.347.5843 Lab/Fax
info(u-environmentalchcmists.con3
Wood -AMEC
Date of Report: Apr 06, 2021
5710 Oleander Drive , Suite 110
Customer PO #:
Wilmington NC 28405
Customer 1D: 11070019
Attention:
Report #: 2021-04441
Project ID: Hexion CLRS
MTBE
SW 848 method 826OB15030B
<0.5 pg/L
03118/2021
Naphthalene
SW 846 method 8260815030E
<0.5 pg/L
03/18/2021
n-Butylbenzene
SW B46 method 8260815030B
<0.5 pg/L
03/18/2021
n-Propylbenzene
SW 846 method 8260815030E
<0,5 pg/L
03/18/2021
ortho-Xylene
SW 846 method 826OB150308
<0.5 pg/L
03/18/2021
p-Isopropyltoluene
SW 846 method 0260E150308
<0,5 pg/L
03/18/2021
sec-Butylbenzene
SW 846 method 8260815030E
G0.5 pg/L
03/18/2021
Styrene
SW 846 method 8260015030E
C0,5 pg/L
03/18/2021
tent-Butylbenzene
SW 846 method 82608/50308
<0.5 pg/L
03/18/2021
Tetrachloroethene
SW 846 method 8260t3150308
<0.5 pg/L
03/18/2021
Toluene
SW 646 method 826013150308
a0 5 pg/L
03/18/2021
Trans-1,2-Dichloroethene
SW 846 method 026013150308
<0.5 pg/L
03/18/2021
Trans-1,3-dichloropropene
SW 848 method 82BOB16030B
<0.5 pg/L
03/18/2021
Trichloroethene
SW B46 method 82BOB15030B
<0.5 pg/L
03/18/2021
Trichlorofluoromethane
SW 846 method 82601315030E
<0,5 pg/L
03/18/2021
Vinyl chloride
SW 846 method B25081503GB
<0.5 pg/L
03/18/2021
Formaldehyde
SW8468315A
160.0pg/L
03/19/2021
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2
0.03 mg/L
03/18/2021
Nitrate+Nitrite-Nitrogen
EPA363.2
72.6mg/L
03/19/2021
Nitrate Nitrogen
Subtraction Method
72,6mg/L
04/01/2021
Total Nitrogen (Cale)
Total Nitrogen
Total Nitrogen
303 mg/L
04/06/2021
Lab ID Sample ID:
Collect DatelTime
Matrix Sampled by
21-10940A Site: WWMW-2
3/17/2021 10:00 AM
Water Ben Moore
Test
Method
Results Date Analyzed
Ammonia Nitrogen
sM 450u NH3 c
45.4 mg1L
04/05/2021
Total Kjeldahl Nitrogen (TKN)
SM4500orgB
230mg/L
04/05/2021
Report 1l.: 2021-04441 Page 3 of 7

Wood -AMEC Date of Report: Apr 06, 2021
5710 Oleander Drive, Suite 110 Customer PO #:
Wilmington I IC 28405 Customer ID: 11070019
Attention: Report #: 2021-04441
Project ID: Hexion CLRS
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-10941 Site: WWMW-1 3/17/2021 10:15 AM Water Ben Moore
Test
Method
Results
Date Analyzed
Sulfate
EPA 300.0
761 mg/L
03/17/2021
Total Dissolved Solids (TDS)
SM 2540 c
1840 mg/L
03/1812021
Total phosphorus
SM 4500 P F
1.63 rng1L
03/25/2021
Total Organic Carbon (TOC)
SM 5310 B
147 mg/L
0312212021
1,1,1,2-Tetrachloroethane
SW 846 method8280B15030B
<2 pg/L
03/19/2021
1,1,1-Trtchloroethane
SW 846 method8280B15030B
<2pg/L
03/19/2021
1,1,2,2-Tetrachloroethane
SW 846 method 82608150306
<2 pg/L
03/19/2021
1,1,2-Trichloroethane
SW 846 method 82601315030E
<2 pg/L
03/19/2021
1,1-Dichloroethane
SW 848 method 6260015030B
<2 pg/L
0311912021
1,1-Dich[oroethene
SW 846 method 8280SI5030B
<2 pg/L
03/19/2021
1,1-Dich[oropropane
SW 846 method 8260BI5030B
<2 pg/L
03/19/2021
1,2,3-Trichlorobenzene
SW 846 method 8260B15030B
<2 pg/L
03/19/2021
1,2,3-Trichloropropane
SW 846 method 8260BI5030B
<2 pg/L
03/19/2021
1,2,4-Trichlorobenzene
SW 846 method 8280B150308
<2 pg/L
03/19/2021
1,2,4-Trimethylbenzene
SW 846 method 8200BI5030B
<2 pg/L
03/19/2021
1,2-Dibromo-3-Chloropropane
SW 846 method 826OB150308
<2 pg/L
03/19/2021
1,2-Dibromoethane
SW 846 method 8280815030E
<2 pg/L
03/19/2021
1,2-Dichlorobenzene
SW 846 method 82608/50306
<2 pg/L
03/19/2021
1,2-Dichloroethane
SW 846 method 8280BI50308
<2 pg/L
03/19/2021
1,2-Dichloropropane
SW 848 method 8260815030E
<2 pg/L
0311912021
1,3,5-Trimethylbenzene
SW 646 method 8200815030E
<2 pg/L
03/19/2021
1,3-Dichlorobenzene
SW 846 method 8280815030E
<2 pg/L
03/19/2021
1,3-Dichloropropane
SW 646 method 82608160308
<2 pg/L
03/19/2021
1,4-Dichlorobenzene
SW 846 method 0260BI5030B
<2 pg/L
03/19/2021
2,2-Dichloropropane
SW 846 method 8280E/5030B
<2 pg/L
0311912021
2-Chlorotoluene
SW 846 method 82808/50308
<2 pg/L
03/19/2021
Report #:: 2021-04441 Page 4 of 7

Wood -AMEC
Date of Report: Apr 06, 2021
5710 Oleander Drive, Suite 110
Customer PO M
Wilmington NC 28405
Customer ID: 11070019
Attention:
Report M 2021-04441
Project ID: Hexion CLRS
2-Hexanone
SW 646 method 82608I5030B
<10 pg/L
03/19/2021
4-Chlorotoluene
SW 846 method 6260815030D
<2 pg/L
03/19/2021
Acetone
SW 846 method 8260B160300
43.4 pg/L
03/1912021
Acrolein
SW 846 method 826OB160308
<20 pg/L
03/19/2021
Acrylonitrile
SW 846 method 8260815030B
<20 pg/L
03/19/2021
Benzene
SW 846 method 8260B15030B
<2 pgIL
03/19/2021
Bromobenzene
SW 846 method 8260BI5030B
<2 pg/L
03/19/2021
Bromochloromethane
SW 846 method 826oBI6030B
<2 pg/L
03/19/2021
Bromodichloromethane
SW 846 method 8260315030B
<2 pg/L
03/19/2021
Bromoform
SW 846 method 82608150308
<2 pg/L
03/19/2021
Bromomethane
SW 046 method 8260815030B
<2 pg/L
03/19/2021
Carbon Disulfide
SW 846 method 826OB15030B
1950 pg/L
0311912021
Carbon tetrachloride
SW 846 method 826OB15030B
<2 pg/L
03/19/2021
Chlorobenzene
SW 846 method 82608/5030B
<2 pg/L
03/19/2021
Chloroethane
SW 846 method 826OB15030B
<2 pg/L
03/19/2021
Chloroform
SW 846 method B260BI5030B
<2 pg/L
03/19/2021
Chloromethane
SW 846 method 826OB15030B
<2 pg/L
03/19/2021
cis- 1,2-Dichloroethene
SW 846 method 82608I50308
<2 pg/L
03/19/2021
cis-1,3-Dichloropropene
SW 646 method 82608160308
<2 pg/L
03/19/2021
Dibromochloromethane
SW 646 method 8260815030E
<2 pg/L
03/19/2021
Dibromomethane
SW 846 method 820UB/5030B
<2 pg/L
03/19/2021
Dichlorodifluoromethane
SW 845 method 6260BI5030B
<2 pg/L
03/19/2021
Ethylbenzene
SW 846 method 826OB15030B
<2 pg/L
03/19/2021
Hexachlorobutadiene
SW 846 method 826OB15030B
<2 pg/L
03/19/2021
IPE
SW 846 method 8260B15030B
<2 pg/L
03/19/2021
1 sopropyl benzene
SW 846 method 82BOB150308
<2 pg/L
03/1912021
M+P Xylene
SW 846 method 826OB150308
<4 pg/L
03/19/2021
MEK
SW 846 method 0200BI5030B
15.3 pg/L
03/19/2021
Methylene chloride
SW 646 method 8260815030E
<2 pg/L
03/19/2021
Ml BK
SW 846 method 8260BIBD30B
<10 pg/L
03/19/2021
Report #:: 2021-04441
Page 5 of 7

{ `Environmental Chemists, Inc.
! ¢ 6602 Windmill Way, Wilmington, NC 28405 0 910.392.0223 Lab 4 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 s 252.473.5702 Lab/Fax
255-,rA Wilmington Highway, Jacksonville, NC 28540 6 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS illfo@eiiviraninent,-tichcniists.com
eiiviraninentalchemists.com
Wood -AMEC
Date of Report: Apr 06, 2021
5710 Oleander Drive , Suite 110
Customer PO #:
Wilmington NC 28405
Customer ID: 11070019
Attention:
Report #: 2021-04441
Project ID: Flexion CLRS
MTBE
SW 846 method 6260615030B
<2 pg/L
03/1912021
Naphthalene
SW 646 method 826OB15030B
<2 pg/L
03/19/2021
n-Butylbenzene
SW 846 method 8260815030E
<2 pg/L
03/19/2021
n-Propylbenzene
SW 846 method 8260815030E
<2 pg/L
03/19/2021
ortho-Xylene
SW 846 method 82BOB15030B
<2 pg/L
03/19/2021
p-Isopropyltoluene
SW 846 method 8260815030E
<2 pg/L
03/19/2021
sec-Butylbenzene
SW 846 method 82601315030B
<2 pg/L
03/19/2021
Styrene
SW 846 method 6260815030E
<2 pg/L
03/19/2021
tert-Butylbenzene
SW 846 method 82608150308
<2 pg/L
03/1912021
Tetrachloroethene
SW 846 method 826013150308
<2 pg/L
03/19/2021
Toluene
SW 646 method 82608/5030B
<2 pg/L
03/19/2021
Trans-1,2-Dichloroethene
SW 846 method 82601376030E
<2 pg/L
03/19/2021
Trans- 1,3-dichloropropene
SW 846 method 82608150308
<2 pg/L
03/1912021
Trichloroethene
SW 846 method 626081603013
<2 pg/L
03/19/2021
Trichlorotluoromethane
SW 846 method 82608150308
<2 pg/L
03/19/2021
Vinyl chloride
SW 846 method 826OB160308
<2 pg/L
03/19/2021
Formaldehyde
SW846 8315A
7800.0 pg/L
03/22/2021
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353.2
0.04 mg/L
03118/2021
Nitrate+Nitrite-Nitrogen
EPA353.2
0.40mg/L
03/19/2021
Nitrate Nitrogen
Subtraction Method
0.36mg/L
04/01/2021
Total Nitrogen (Cale)
Total Nitrogen
Total Nitrogen
831 mg/L
04/06/2021
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
21-10941A Site: WWMW-1
3/17/2021 10:15 AM
Water Ben Moore
Test
Method
Results Date Analyzed
Ammonia Nitrogen
SM 4500 NH3 C
748 mg1L
03/2212021
Total Kjeldahl Nitrogen (TKN)
SM 4500 Org 8
831 mg/L
03/2212021
Report #;: 2021-04441 Page 6 of 7

ANALYTICAL & CONSULTING CHEMISTS
Wood -AMEC
5710 Oleander Drive , Suite 110
Wilmington NC 28405
Attention:
6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab e 910.392.4424 Fax
710 Bowsertown road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 e 910,347,5843 Lab/Fax
info cr environmentalchemists.com
Date of Report: Apr 06, 2021
Customer PO #:
Customer lD: 11070019
Report #: 2021-04441
Project ID: Hexion CLRS
Comment: Sample # 21-10941-SW 846 method 826OB15030B -reporting limit elevated due to matrix
interference.
Reviewed by:
Report #;; 2021-04441 Page 7 of 7

ANALYTICAL & CONSULTING CHEMISTS
LCS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab e 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
info(a)environmentalchemists.com
Wood -Ames QC - 2021-04441
Parameter
True Value
M91L
Result
mglL
% Recovery
Linfits
Ammonia
5.0
4.9
98
90-110
Ammonia
5.0
5.0
100
90-110
NO2
0.60
0.61
102
90-1 10
NO3 & NO2
1.00
1.00
100
90-110
Sulfate
50.0
47.2
94
90-110
TDS
600
600
100
90-110
TOC
10.0
10.2
102
90-110
TKN
0.5
0.5
102
90- 11 0
TKN
4.0
3.8
95
90-110
TP
1.60
1.60
100
90-110
MS/MSD
Parameter
True Value
mg/L
Recovery
inglL
/
Recover y
%
Difference
Limits %
Recovery
Limits %
Difference
Ammonia
4.0
4.1/4.1
1021102
0
80-120
520
Ammonia
10.0
10.0/9.4
100/94
6
80-120
<20
NO2
0,50
0.55/0.53
110/106
4
80-120
<20
NO3 & NO2
0.50
0.5110.51
102/ 102
a
80-120
< 20
Sulfate
10.0
10.3/9.8
103/98
5
80-120
< 26
TDS
N/A
N/A
N/A
N/A
80-120
<20
TOC
10.0
9.7
97
N/A
N/A
<20
TKN
10.0
9.7/9.7
97/97
0
N/A
< 20
TKN
4.0
3.9/3.9
98/98
0
N/A
< 20
TP
2.00
1.83/1.83
92/92
0
80/120
<20

C"
f
ANALYTICAL & CONSULTING CHEMISTS
DUPLICATE SAMPLES
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab 4 910.392.4424 Fax
710 Bowsertown .Road, Manteo, NC 27954 0 252,5473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax
iiifo a eirvironmentalobcmists.eom
Parameter
Results
inglL
% Difference
Limits %
Ammonia
N/A
N/A
N/A
< 10
Ammonia
N/A
N/A
N/A
N/A
NO2
N/A
N/A
N/A
< 10
NO3 & NO2
N/A
N/A
N/A
< 20
Sulfate
<15
<15
0
< 10
TDS
1860
1830
2
510
TOC
8.0
8.0
0
<10
TKN
NIA
N/A
N/A
<10
TKN
NIA
N/A
N/A
<10
TP
N/A
N/A
N/A
510
BLANK
Parameter,
Results
mg/L
Limit
ing/L
Ammonia
<0.1
0.1
Ammonia
<0,1
0.1
NO2
<0.0 l
0.01
NO3 & NO2
<0.01
0.01
Sulfate
<2.5
2.5
TDS
<2.5
2.5
TOC
<0.25
0.25
TKN
<0.25
0.25
TKN
<0.25
0.25
TP
<0.02
0.02

LABORATORY CONTROL SAMPLE #1
Report#2021-4441 Page t of
Spike Compounds
Method
Blank
Result
Spike
Added
Blank Spike
QC Lirrrits
(Mandatory)
% Recovery Range
Result
Recovery
Dichlorodifluorom ethane
<0.5
10
10.32
103
33.3 -150
Chloromethane
<0.5
10
10.58
106
61.2 --128
Vinyl chloride
<0.5
10
10.54
105
54.3 -134
Bromomethane
<0.5
10
10.73
107
64.6 -143
Chloroethane
<0.5
10
10.75
108
55.8 --153
TrichIorofluoromethane
<0.5
10
10.62
106
52.9 -153
1, 1 -Dichloroethene
<0.5
10
11.15
112
59.1 -145
Acetone
<2.5
50
55.01
110
50.3 -155
Methylene chloride
<0.5
10
10.92
109
52.0 -141
trans-1,2-Dichloroethene
<0.5
10
11
Ito
58.3 -145
MTBE
<0.5
10
10.86
109
58.3 -145
1,1-Diehl oroethane.._.__.._
<0.5
10
10.98
110
66.1 -140
1PE
<0.5
10
10.95
1 1 a
52.5 --147
2,2-Dichloropropane
<0.5
10
10,47
105
59.9 --137
cis-1,2-Dichloroethene
<0.5
10
10.91
109
57.4 --139
MEK
<2.5
50
54.83
Ito
58.9 -135
Bromochloromethane
<0.5
10
10.8
108
63.5 -130
Chloroform
<0.5
10
10.99
Ito
54.2 -153
1,1,1-Trichooroethane
<0.5
10
10.9
110
60.6 -130
Carbon tetrachloride
<0.5
10
10.9
110
51.7 -147
1,1-Dichloropropane
<0.5
10
10.5
105
53.6 -134
Benzene
<0.5
10
10.79
108
63.3 --133
1,2-Dichloroethane
<0.5
10
10.85
109
62.6 -150
Trichloroethene
<0.5
10
1098
Ito
73.1-138
1,2-Dichloropropane
<0.5
10
10.85
109
61.8 -138
Dibromomethane
<0.5
10
10.88
109
56.4 -136

LABORATORY CONTROL SAMPLE #1
Renort#2021-4441 Page 2 of
Spike Com ounds
P P
Method
Blank
Result
Spike
Added
Blank Spike
QC Limits
Mcnadator
(Mandatory)
% Recovery Range
Result
Recovery
Bromodiehlorornethane
<0.5
10
€ 0 97
110
74.3 -143
cis-1,3-Dichloropropene
<0.5
10
10.55
106
63.9 - 135
M1BK
<2.5
50
54.81
1 110
58.7 -145
Toluene
<0.5
10
10.89
109
62.3 -143
trans-1,3-Dichloropropene
<0.5
10
10.74
107
71.3 -143
1,1,2-Trichloroethane
<0.5
10
11.03
1 110
57.7--147
Tetrachloroethene
<0.5
10
10.83
108
58.1-139
1,3-Dichloropropane
<0.5
10
10.83
108
61.5 --147
2-Hexanone
<2.5
50
54.92
Ito
59.6 -- 148
DibromochIoromethane
<0.5
10
10.89
109
69.5 -147
1,2-Dibromoethane
<0.5
10
10.93
109
69.2 --133
Chlorobenzene
<0.5
10
10.87
109
76.5 -117
Ethyl benzene
<0.5
10
10.99
110
629 -143
1, 1, 1,2-Tetrachloroethane
<0.5
10
10.91
109
69.4-137
M+P Xylene
<1
20
22.05
110
62.5 -134
O-Xylene
<0.5
10
11.12
111
62.3 -140
Styrene
<0.5
10
10.54
105
66,8 -131
Bromoforrn
<0.5
10
10.68
107
61.6 -..141
Isopropylbenzene
<0.5
10
10.8
108
68.1-130
Bromobenzene
<0.5
10
11.45
115
64.9 -125
1,1,2,2-Tetrachloroethane
<0.5
10
€1.4 €
114
65.7 --146
n-Piopylbenzene
<0.5
10
11.04
110
54.2 -149
1,2,3-Trichloropropane
<0.5
10
11.48
115
68.5 -145
2-Chlorotoluene
<0.5
10
11,37
114
56.8 -147
1,3,5-Trimethylbenzene
<0.5
10
11.58
116
63.8 -137

LABORATORY CONTROL SAMPLE #1
RewiI82021-4441 Paue 3 of 3
Spike Compounds
Method
Blank
Result
S pike
Added
Added
Blank Spike
QC Limits
(Mandatory)
% Recovery Range
Result
Recovery
4-Chlorotoluene
<0.5
10
11.26
113
62.6 -145
tert-Butyl benzene
<0.5
10
11,86
119
63.0 -128
1,2,4-Trimethylbenzene
<0.5
10
11.92
119
63.8 -138
sec-Butylbenzene
<0.5
10
11.74
117
71.0 - 143
1,3-Dichlorobenzene
<0.5
10
11.99
120
70.5 -- 127
4-Isopropyltoluene
<0.5
10
11.83
118
58.9 -132
1,4-Dichlorobenzene
<0.5
10
11.88
119
78.8 -122
n-Butylbenzene
<0.5
10
11.68
117
55.5 -136
1,2-Dichlorobenzene
<0.5
10
12.07
121
78.6 - 121
1,2-Dibromo-3 -chi oropropane
<0.5
10
12.56
126
65.5 - 139
1,2,4-Trichlorobenzene
<0.5
10
12.33
123
60.5 -137
Hexachlorobutadiene
<0.5
10
12.3
123
37.0 -131
Naphthalene
<0.5
10
12.7
127
54.9 - 138
1,2,3-Trichlorobenzene
<0.5
i0
12.74
127
62.5 -132
Acrolein
<5
100
35.1
35.1
24.65 - 167
Acrylonitrile
<5
25
28.39
114
68.6 --132

Analytical Environmental Services, Inc
Date: 23-Mar-21
Client: Environmental Chemists, Inc, Client Sample ID: 410940
Project Name: 21-4441 Collection Date: 3/17/2021 10:00:00 AM
Lnb ID: 2I031,56-001 Matrix: Aqueous
tteporting Dilution
Analyses Result Qual Units DatchlD Date Analyzed Analyst
Limit Factor
Formaldehyde by SW8315A
Formaldehyde 160 50 ug[L, 312211 € 03/191202120:38 1iF
Qualifiers: • value exceeds maximum conlammam level
13RL Below reporting limit
H Holding limes for preparation or analysis exceeded
N Analyte not NELAC certified
n Ana€yte delecled in the associated method blank
> Greater than Result value
E Ltimated(value above quanthatimi mnPe)
S Spike Recovery outside liatitsdue tomatrix
Narr Seeclsttwnlive
F Analyzed in the lab which is a deviation from the mobod
C Less dvin Result Y.W.
3 Estimated value detected below Reporting Limit
Page 3 of 8
i _ (---)U- 041

Analytical Environmental Services, Inc
Date: 23-Mar-21
Client;
Environmental Chemists, Inc.
Client Sample ID;
#10941
Project Name:
21-4441
Collection Date:
3/17/2021 10:15:00 AM
Lab ID:
21031,56-002
Matrix:
Aqueous
Anal ses Result Reporting Dilution
y Limit Qual Units I3atchlD factor Date Analyzed Analyst
Formaldehyde by SW8315A
Formaldehyde 7800 500 ug/L 312211 €0 031221202107:18 RP
Qualaien: • Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation oraaalysls exceeded
N Analytenot NELACcertified
B Analyte detected in the associated method blank
> Csreater than Result value
E Esiimared(vatue above quantitatron range)
S Spike Recovery outside limits due to matrix
Narr See case narmot,
f Analyzed in the lab wktch is a deviation from the method
e Less than Result value
J Estimated value deteetedbelow RepurtingLimit
Pagel 4 of 8

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client Obr-) Date: Report Number:.s ) ---0 ` q q
Receipt of sample: ECHEM Pickup ❑ Client Delive UPS ❑ FedEx ❑ Other ❑
YES
JEJ
NO
N/A
1. Were custody seals present on the cooler?
YES
111.
NO IV
N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt aC
1❑
How temperature taken: ❑ Temperature Blank Against Bottles
111 Gun ID: Thomas Traceable S/N 192511657 1R Gun Correction Factor'C: 0.0
❑ YES
10
NO
3. If temperature of cooler exceeded 6`C, was Project Mgr./QA notified?
YES
❑
NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑
NO
5. Were sample ID's listed on the COC?
YES
❑
NO 1
6. Were samples ID's listed on sample containers?
YES
❑
NO
7. Were collection date and time listed on the COC?
YES
❑
NO
8. Were tests to be performed listed on the COC?
YES
ID
NO
9. Did samples arrive in proper containers for each test?
YES
10
NO
10. Did samples arrive in good condition for each test?
YES
❑
NO 11. Was adequate sample volume availableT
,j
YES 10
NO 12. Were samples received within proper holding time for requested tests?
YES 10
NO 13. Were acid preserved samples received at a pH of <2?
Cl YES
❑
NO 14. Were cyanide samples received at a pH >12?
❑ YES
C
NO 15. Were sulfide samples received at a pH >9?
COMMENTS:
DOC. QA.002 Rev 1

Analytical
ENVIRONMENTAL
CHEMISTS, INC
6602 Windmill Way Wilmington, NC 28405
& Consulting Chemists
NCDENR: DWQ CERTIFICATION # 94 NCDHHs: DLL CERTIFICATION # 37729
aFF 3
tsCom2-4¢24
i
Client:
COLLECTION AND C
AIN OF CUSTODY
info@Ta ny ranm �ta�hemi
/� Z`--
ADDRESS: � � � �j�
AROJECT Ni4Ml=:
� �
�jfl'1 �WLf {i IZ, REPORT NO: T
CONTACT NAME:
REPORT TO:
Y,
+ � 7
COPY TO:
PHONEIFAX:
Sampled By.
SAMPLE; TYp>r: 1 frtfluent
email:
E =
. Ywtr�° i,,
Caller#ion d Efflutant, W Well, ST =Stream, SO = Soil, 5L = Sludge, Other:
Sample Identification
a a
o �� ��
PRESERVATION
o n
©ate
c c o f
Time Temp c
m m e
x z ° ` ¢ x ut s
ANALYSIS REQUESTED
�s 17,2
C P
sx z s a z E o
G
bw
C P
OL
C P
1
SAM
010
Q
1110
61�
G G
NOTICE-DECKORINATION: samples for Ammonla, TKN, Cyanide, Phenal and Bacteria must be dechlorinated (G
Transfer Relinquished 6y;
�. DatelTin
2_
Temperature whenTill
Received °
Accep
Deliver By:ted: .j�
Comments:_ Received By:_
NO _
or less] in the field at the time of collection. See reverse for Instructions
Received Bv:
a
ate:p Time:
TURNAROUND: .�

ENVIRONMENTAL CHEMISTS, INC 6602 Windmill Way Wilmington, NC 28405
OFFICE: 91 0-392-0223 FAX [phone]
NCDENR: DWO CERTIFICATION # 94 NCbHHS: DL5 CERTIFICATION * 37729 [e-mail]
COLLECTION AN CHAIN OF CUSTODYy
PROJECT NAME: �
0 V { REPORT NO:
CONTACT NAME: v% PO No: �D ! q 7�
REPORT TO: U 1-i
COPY TO:
`� PHONEIFAX:
on
eFrlaii: � �, . YhE6�v�f
SAMPLE TYPE: I ; Influent, E = Effluent. W ; Well, ST = Stream, SO = Soil, SL W Sludge, Other:
a
a �
w PRESERVATION
a — M
m w v [�
E o a a s = o c 2 _j p x C, w cc
Time Temp U) y �' o = 1CL ANALYSIS REQUESTED
C P
C
n
tp FOY M"' cf1 P
P �U ( (�
G
P
NOTICE - DECHLORINATION: Samples for Amimnnia, TKN Cyanide, Phenol and Bacteria mus be dechiorinatod 10,5 p m or Ie
'Transfer Relinquishes! By P ssI in the held at the time of c
i]atelTime allectlon. Sea reverse for Instructions
2. 3 } V Received By: pal
�d l
Temperature when Received °C:
Delivered BY: Accepted:
Re Comments: Received By: "�� sampie Requested:
Dater . 1 Z me:}i
TURNAR0UND:

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Into
6602 Windnnill Way, Wilmington, NC 28405 o 910.392.0223 Lab D 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 o 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 n 910.347.5843 Lab/Fax
[e-mail]
Wood -AMEC
Date of Report: Nov 20, 2019
5710 Oleander Drive, Suite 110
Customer PO #: 6480199024
Wilmington NC 28405
Customer ID: 11070019
Attention: Ben Moore
Report #: 2019-18641
Project ID: Hexion CLRS
Lab ID Sample ID,
Collect Date/Time Matrix Sampled by
19-47446 Site: WWMW-1
11/6/2019
9:00 AM Water Ben Moore
Test
Method
Results
Date Analyzed
Sulfate
EPA300.0
416mg/L
11/11/2019
Ammonia Nitrogen
EPA350.1
517 mg/L
1111212019
Total Dissolved Solids (TDS)
SM 2540 C
582 mg/L
11/07/2019
Total Phosphorus
SM 4500 P r
0.91 mg/L
11/13/2019
Total Organic Carbon (TOC)
SM 6310 B
64,6 mg/L
11/07/2019
1, 1, 1,2-Tetrachloroethane
SW 846 method a260B15034B
<2 pg/L
11/06/2019
1, 1, 1 -Trichloroethane
SW 846 method 8260815030B
<2 pg/L
11/06/2019
1,1,2,2-Tetrachloroethane
SW 646 method 826OB15030B
<2 pg/L
11/06/2019
1,1,2-Trichloroethane
SW 846 method 82601315030E
<2 pg/L
11/06/2019
1,1-Dichloroethane
SW 846 method 8260815030E
<2 pg/L
11/06/2019
1,1-Dichloroethene
SW 846 method 8260815030E
<2 pg/L
11/06/2019
1,1-Dichloropropane
SW 846 method 8260815030E
<2 pg/L
11/06/2019
1,2,3-Ticchoorobenzene
SW 846 method 826OB15030B
<2 pg/L
11/06/2019
1,2,3-Trichloropropane
SW 846 method 826OB15030B
<2 pg/L
11/06/2019
1,2,4-Trichlorobenzene
SW 846 method 8260Bf5030B
<2 pg/L
11/06/2019
1,2,4-Trimethylbenzene
SW 848 method 826OB15030B
e2 pg/L
11/06/2019
1,2-Dibromo-3-Chloropropane
SW 846 method $260B/60308
<2 pg/L
11/06/2019
1,2-Dibromoethane
SW 846 method 8260$15030B
<2 pg/L
11/06/2019
1,2-Dichlorobe nzene
SW 646 method 6260815030E
<2 pg/L
11/0612019
1,2-Dichloroethane
SW 846 method 8260BI5030B
<2 pg/L
11/06/2019
1,2-Dichloropropane
SW 846 method 8260B15030B
<2 pg/L
11/06/2019
1,3,6-Trimethylbenzene
SW 846 method 8260B150308
<2 pg/L
11/06/2019
1, 3-Dichlorobenzene
SW 846 method 826OB15030B
<2 pg/L
11/06/2019
1,3-Dichloropropane
SW 846 method 8260815030B
<2 pg/L
11/06/2019
1,4-Dichlorobenzene
SW 846 method 82BOBI5030B
<2 pg/L
11/0612019
2,2-Dich loropro pane
SW 846 method 826OB15030B
<2 pg/L
11/0612019
Report #:: 2019-18641
Page 1 of 6

Environmental Chemists, Inc®
6602 Windinill Way, Wilmington, NC 28405 o 910.392.0223 Lab o 910.392.4424 Fax
710 Bowsertown Read, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 9 910.347.5843 Lab/Fax
info{ricnvironnicntalche►nists.coiik
Wood -AMEC
Date of Report: Nov 20, 2019
5710 Oleander Drive, Suite 110
Customer PO #: 6480199024
Wilmington NC 28405
Customer ID: 11070019
Attention: Ben Moore
Report #: 2019-18641
Project ID: Hexion CLRS
2-Chlorotoluene
SW 846 method 8260B15030B
<2 pg/L
11/06/2019
4-Chlorotoluene
SW 846 method 8260BI50308
<2 pglL
11/06/2019
Benzene
SW 646 method 8260815030B
<2 pg/L
11/06/2019
Bromobenzene
SW 846 method 82606I5030B
<2 pg/L
11/06/2019
Bromochloromethane
SW 846 method 6200615030E
<2 pg/L
11/06/2019
Bromodichloromethane
SW 846 method 82606/5030B
<2 pg/L
11/06/2019
Bromoform
SW 846 method 8260B16030B
<2 pg/L
11/06/2019
Bromomethane
SW 846 method 8260W50306
<2 pg/L
11/06/2019
Carbon tetrachloride
SW 846 method 8260816030B
<2 pg/L
11/06/2019
Chlorobenzene
SW 846 method 8260815030B
<2 pg/L
11/06/2019
Chloroethane
SW 846 method 826oB150306
<2 pg/L
11/06/2019
Chloroform
SW 846 method 8260B15030B
<2 pg/L
11/06/2019
Chloromethane
SW 846 method 82608150308
<2 pg/L
11/06/2019
Cis-1,2-Dichloroethene
SW 846 method 8260615030B
<2 pg/L
11/06/2019
cis-1,3-Dichloropropene
SW 846 method 8260815030B
<2 pg/L
11/06/2019
Dibromochloromethane
SW 846 method 8260B/6030B
<2 pg/L
11/06/2019
Dibromomethane
SW 848 method 8280B15030B
<2 pg/L
11/0612019
Dich lorodifl uorom ethane
SW 846 method 8260B/50308
<2 pg/L
11/06/2019
Ethylbenzene
SW 846 method 8260B150306
<2 pg/L
11/06/2019
Hexachlorobutadiene
SW 846 method 8260t3150306
<2 pg/L
11/06/2019
Isopropylbenzene
SW 846 method 8280615030E
<2 pg/L
11/06/2019
M+P Xylene
SW 846 method 8260815030B
<4 pg/L
11/06/2019
Methylene chloride
SW 846 method 82BOB15030B
<2 pg/L
11106/2019
Naphthalene
SW 846 method 8260BI5030B
<2 pg/L
11/06/2019
n-Butylbenzene
SW 846 method 826OB150308
<2 pg/L
11/06/2019
n-Propylbenzene
SW 846 method 8260B15030B
<2 pg/L
11/06/2019
ortho-Xylene
SW 846 method 826OB150308
<2 pg/L
11/06/2019
p-Isopropyltoluene
SW 846 method 8260B150308
<2 pg/L
11/06/2019
sec-Butylbenzene
SW 846 method 82608/5030S
<2 pg/L
11/06/2019
Styrene
SW 846 method 82&0B15030B
<2 pg/L
11/06/2019
Report k; 2019-18641
Page 2 or 6

Wood -AMEC
Date of Report: Nov 20, 2019
5710 Oleander Drive, Suite 110
Customer PO #: 6480199024
Wilmington NC 28405
Customer ID: 11070019
Attention: Ben Moore
Report #: 2019-18641
Project ID: Hexion CLRS
tort-Butylbenzene
SW 846 method 826OB15030B
<2 pg/L
11/06/2019
Tetrachloroethene
SW 846 method 8260B/5030B
<2 pg/L
1 1/0612019
Toluene
SW 846 method 826OB15030B
<2 pg/L
11/06/2019
Trans-1 ,2-Dichloroethene
SW 846 method 8260B/5030B
<2 pg/L
11/06/2019
Trans-1,3-dichloroprope ne
5W 846 method 826GS150308
<2 pg/L
11/06/2019
Trichloroethene
SW 846 method 8260615030E
<2 pg/L
1 1106/2019
Trichlorofluoromethane
SW 846 method 8260815030B
<2 pg/L
11/06/2019
Vinyl chloride
SW 846 method 8260B/5030B
<2 pgIL
11/06/2019
Formaldehyde
SW846 8315A
150.0 pg/L
11/08/2019
Nitrate Nitrogen (Cale)
Nitrite Nitrogen EPA353.2 0.03mg/L 11/0812019
Nitrate+Nitrite-Nitrogen EPA353.2 <0.02rnglL 11/16/2019
Nitrate Nitrogen Subtraction Method <0.02 mg/L 11/2012019
Report H:: 2019-18641 Page 3 of 0

Wood -AMEC
Date of Report: Nov 20, 2019
5710 Oleander Drive, Suite 110
Customer PO #: 6480199024
Wilmington NC 28405
Customer ID: 11070019
Attention: Ben Moore
Report #: 2019-18641
Project ID: Hexion CLRS
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
19-47448 Site: WWMW-2
11/6/2019
9:30 AM Water Ben Moore
Test
Method
Results
Date Analyzed
Sulfate
EmPA300.0
109mg/L
11/11/2019
Ammonia Nitrogen
EPA 350.1
39.4 mg/L
11/11/2019
Total Dissolved Solids (TDS)
SM 2540 c
248 mg/L
11/07/2019
Total Phosphorus
SM 4500 P F
0.46 mg/L
11/1312019
Total Organic Carbon (TOG)
SM 5310 B
4.9 mg/L
11/07/2019
1,1,1,2-Tetrachloroethane
SW 846 method8260815030B
<0,5pg/L
1110612019
1, 1, 1 -Trichloroethane
SW 846 method 826ot3150308
<0.5 pg/L
11106/2019
1,1,2,2-Tetrachloroethane
SW 846 method8260B15030B
<0.5pg/L
11/06/2019
1,1,2-Trichloroethane
SW 846 method 8260B15030B
<0.5 pg/L
11/06/2019
1,1-Dichloroethane
SW 846 method 82608/5030B
<0.5 pg/L
11/06/2019
1, 1 -Dichloroethene
SW 846 method 826OB15030B
<0.5 pg/L
11106/2019
1,1-Dichloropropene
SW 846 method8260B15030B
<0.5 pg/L
11/06/2019
1,2,3-Trichlorobenzene
SW 846 method 8260B15030B
<0.5 pglL
11/06/2019
1,2,3-Trichloropropane
SW 846 method 826OB16030B
<0.5 pg/L
11/06/2019
1,2,4-Trichlorobenzene
SW 846 method 82608150308
<0.5 pg/L
11/06/2019
1,2,4-Trimethylbenzene
SW 846 method 826015030B
<0,5 pg/L
11106/2019
1,2-Dibromo-3-Chloropropane
SW 846 method 6260815030B
<0.5 pg/L
11/06/2019
1,2-Dibromoethane
SW 846 method 826OB15030B
<0.6 pg/L
11/06/2019
1,2-Dichlorobenzene
SW 846 method 82608150SOB
<0.5 pg/L
11/06/2019
1,2-Dichloroethane
SW 846 method 8260815030E
<0.5 pg/L
11/06/2019
1,2-Dichloropropane
SW 846 method828OB15030B
<0.5 pg/L
11/06/2019
1,3,5-Trimethylbenzene
SW 846 method 82601315030B
<0.5 pg/L
11/06/2019
1,3-Dichlorobenzene
SW 846 method 8260815030E
<0.5 pg/L
11/06/2019
1,3-Dichloropropane
SW 846 method 826OB15030B
<0.5 pg/L
11/06/2019
1,4-Dichlorobenzene
SW 846 method 826OB160308
<0.5 pg/L
11/06/2019
2,2-D ich loro propane
SW 846 method 826OB15030B
<0.5 pg/L
11/06/2019
Report #:: 2019-18641
Page 4 of 6

ANALYTICAL & CONSULTING CHEMISTS
y r ne t .l Chemists, Inc.
6602 Windmill 4Vay, Wilmington, NC 28405 o 910.392.0223 Lab 9 910.392.4424 Fax
A 0 Bowsertown Road, N4anteo, NC 27954 ® 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 s 910.347.5843 Lab/Fax
info,elivironrirex)taleliertiists.coni
Wood -AMEC
Date of Report: Nov 20, 2019
5710 Oleander Drive, Suite 110
Customer PO #: 6480199024
Wilmington NC 28405
Customer ID: 11070019
Attention: Ben Moore
Report #: 2019-18641
Project 10; Hexion CLRS
2-Chlorotoluene
SW 846 method 82801315030B
<0.5 pg/L
11/06/2019
4-Chlorotoluene
SW 846 method 826OB15030B
<0.5 pg/L
11/06/2019
Benzene
SW 846 method 826013150306
<0.5 pg/L
11/0612019
Bromobenzene
SW 846 method 8260B/5030B
<0,5 pg/L
11/0612019
Bromochloromethane
SW 846 method 8260B15030B
<0.5 pg/L
11/06/2019
Bromodichloromethane
SW 846 method 82BOB15030B
<0,5 pg/L
1 1106/2019
Bromoform
SW 846 method 82606/5030B
<0.5 pg/L
11/06/2019
Bromomethane
SW 846 method 8260B15030B
<0.5 pg/L
11/06/2019
Carbon tetrachloride
SW 846 method 626OB15030B
<0.5 pg/L
11/06/2019
Chlorobenzene
SW 846 method 826OB15030B
<0.5 pg/L
11/0612019
Chloroethane
SW 846 method 8260815030E
<0.5 pg/L
11/06/2019
Chloroform
SW 846 method 8260B150308
<0,5 pg/L
11/06/2019
Chloromethane
SW 846 method 8280815030E
<0.5 pg/L
11/06/2019
cis-1,2-Dichloroethene
SW 846 method 8260815030B
<0.5 pg/L
11/06/2019
cis-1,3-Dichloropropene
SW 846 method 8260815030B
<0.5 pg/L
11/06/2019
Dibromochloromethane
SW 846 method 8260815030E
<0,5 pg/L
11/06/2019
Dibromomethane
SW 846 method 8260615030E
<0.5 pg/L
11/06/2019
Dichlorodifluoromethane
SW 846 method 8260815030B
<0.5 pg/L
11/06/2019
Ethylbenzene
SW 846 method 826OB15030B
<0.5 pg/L
11/06/2019
Hexachlorobutadiene
SW 846 method 8260B150308
<0,5 pg/L
11/06/2019
Isopropylbenzene
SW 846 method 82608/5030B
<0,5 pg/L
11/06/2019
M+P Xylene
SW 846 method 8260B150308
<1.0 pg/L
11/06/2019
Methylene chloride
SW 846 method 82608160306
<0,5 pg/L
11/06/2019
Naphthalene
SW 84B method 82601315030B
<0.5 pg/L
11/06/2019
n-Butylbenzene
SW 846 method 82608/5030B
<0,5 pg/L
11/06/2019
n-Propylbenzene
SW 846 method 826OB15030B
<0.5 pg/L
11/06/2019
ortho-Xylene
SW 846 method 8260B1503W
<0.5 pg/L
11/06/2019
p-Isopropyltoluene
SW 846 method 8260615030B
<0.5 pg/L
11106/2019
sec-Butylbenzene
SW 846 method 82608160308
<0,5 pg/L
11/06/2019
Styrene
SW 846 method 82606160308
<0.5 pg/L
11/06/2019
Report #:: 2019-18641
Page 5 of 6

ANALYTICAL & CONSULTING CHEMISTS
I in
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 O 910.392.0223 Lab ® 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252,473.5702 Lab/Fax
255-A Wiltnington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
info@envirot�metrt��lchetnists.com
Wood -AMEC
Date of Report: Nov 20, 2019
5710 Oleander Drive , Suite 110
Customer PO #: 6480199024
Wilmington NC 28405
Customer ID: 11070019
Attention: Ben Moore
Report #: 2019-18641
Project ID: Hexion CLRS
tert-B utyl benzene
SW 846 method 8264B15030B
<0.5 pg/L
11/06/2019
Tetrachloroethene
SW 846 method B26OB15030B
<0.5 pg/L
11/06/2019
Toluene
SW 846 method 8260B/5030B
<0.5 pg/L
11/06/2019
Trans- 1,2-Dichloroethene
SW 846 method 82606/503013
<0.5 pg/L
11/06/2019
Trans-1,3-dichloropropene
SW 846 method 826013/50308
<0.5 pg/L
11/06/2019
Trlch loroethelle
SW 846 method 8260815030E
<0.5 pg/L
11106/2019
Trichlorofluoro methane
SW 846 method 826013/50308
<0.5 pg/L
11/06/2019
Vinyl chloride
SW 846 method 8260B/5030B
<0.5 pg/L
11/06/2019
Formaldehyde
SW046 8315A
<50 pg/L
11/08/2019
Nitrate Nitrogen (Cale)
Nitrite Nitrogen
EPA 353,2
0.03 mg/L
11/08/2019
Nitrate+Nitrite-Nitrogen
EPA 353.2
29.7 mg1L
11/1812019
Nitrate Nitrogen
Subtraction Method
29.7mg/L
11/20/2019
Comment: Sample # 19-47446-Method
SW 846 Method 8260B-
Reporting limit elevated due to matrix
interference.
Reviewed by:
r
Report #:: 2019-18641 Page 6 of 6

LABORATORY CONTROL SAMPLE #1
Repot t##2019-18641 Page 1 of 3
Spike Compounds
Alethod
Blank
Result
Spike
Added
Blank Spike
QC Limits
(Mandatory)
% Recovery Range
Result
Recovery
Dichlorodifluoromethane
<0.5
20
14.14
70.7
33.3 -150
Chloromethane
<0.5
20
15.91
79.6
61.2 -128
Vinyl chloride
<0.5
20
16.22
81.1
54.3 -134
Bromomethane
<0.5
20
17.68
88.4
64.6 -143
ChIoroethane
<0.5
20
18.82
94.1
55.8 --153
Trichlorofluoromethane
<0.5
20
18.5
92.5
52.9 ---153
1, 1 -Dichloroethene
<0.5
20
20.64
103
59.1 - 145
Methylene chloride
<0.5
20
18.89
94.5
52.0 -141
trans-1,2-Dichloroethene
<0.5
20
19.03
95.2
58.3 -145
1,I-Dichloroethene
<0.5
20
20.49
102
66.1-140
2,2-Dichloropropane
<0.5
20
20.28
101
59.9 -137
cis-1,2-Dichloroethene
<0.5
20
20.02
100
57.4 ---139
Bromochloromethane
<0.5
20
19.2
96
63.5 -130
Chloroform
<0.5
20
19.96
99.8
54.2 -153
1, 1, 1 -Trichloroethane
<0.5
20
19.34
96.7
60.6 -130
Carbon tetrachloride
<0.5
20
19.12
95.6
51.7 --147
I, I-Dichloropropene
<0.5
20
18.77
93.9
53.6 -134
Benzene
<0.5
20
19.25
96.3
63.3 - 133
1,2-Dichloroethane
<0.5
20
19.6
98
62.6 -150
Trichloroethene
<0.5
20
19.24
96.2
73.1-138
1,2-Dichloropropane
<0.5
20
19.08
95.4
61.8 -138
Dibromomethane
<0.5
20
19.95
99.8
56.4 -136

LABORATORY CONTROL SAMPLE #1
Report#2019-18641 Page 2 of 3
Spike Compounds
Method
Blank
Result
Spike
p
Added
Blank Spike
QC Limits
(Mandatory)
Recovery Range
Result
Recovery
BromodichIoromethane
<0.5
20
19.69
98.5
74.3 -143
cis- 1,3 -Diehl oropropene
<0.5
20
20.83
104
63.9 --135
Toluene
<0.5
20
19.57
97.9
62.3 -143
trans-1,3-Dichloropropene
<0.5
20
20.11
101
71.3 -143
1,1,2-Trichloroethane
<0.5
20
20.41
102
57.7 -147
Tetrachloroethane
<0.5
20
19.25
96.3
58.1-139
1,3-Dichloropropane
<0.5
20
20.01
100
61.5 ---147
Dibromochloromethane
<0.5
20
20.38
102
69.5 -147
1,2-Dibromoethane
<0.5
20
19.96
99.8
69.2 -133
Chlorobenzene
<0.5
20
19.2
96
76.5 -117
Ethylbenzene
<0.5
20
19,31
96.6
62.9 -143
1, 1, 1,2-Tetrachloroethane
<0.5
20
19.45
97.3
69.4 --137
M+P Xylene
<1
40
38.03
95.1
62.5 --134
O-Xylene
<0.5
20
19.36
96.8
62.3 -140
Styrene
<0.5
20
19.37
96.9
66.8 -131
Bromoform
<0.5
20
19.2
96
61.6 -141
Isopropylbenzene
<0.5
20
19.32
96.6
68.1--130
Bromobenzene
<0.5
20
20.38
102
64.9 --125
1,1,2,2-Tetrachloroethane
<0.5
20
19.74
98.7
65.7 --146
n-Propylbenzene
<0.5
20
20.18
101
54.2 --149
1,2,3-Trichloropropane
<0.5
20
21.07
105
68.5 -145
2-Chlorotoluene
<0.5
20
20.19
101
56.8 -147
1,3,5-Trimethylbenzene
<0.5
20
20.08
100
63.8 - 137

LABORATORY CONTROL SAMPLE #1
Report#2019-18641 Page 3 of 3
Spike Compounds
Method
Blank
Result
Spike
p
Added
Blank Spike
QC Limits
(Mandatory)
% Recovery Range
Result
Recovery
4-Chlorotoluene
<0.5
20
20.72
104
62.6 -145
test-Butylbenzene
<0.5
20
20.46
102
63.0 ---128
1,2,4-Trimethylbenzenc
<0.5
20
20.34
102
63.8 -138
sec-Butylbenzene
<0.5
20
20.55
71.0-143
1,3-Dichlorobenzene
<0.5
20
19.89
P10q3
70.5-127
4-lsopropyltoluene
<0.5
20
20.58
58.9 -132
1,4-Dichlorobenzene
<0.5
20
20.52
103
78.8 ---122
n-Butylbenzene
<0.5
20
20.24
101
55.5 -136
1,2-Dichlorobenzene
<0.5
20
20.66
103
78.6 -121
1,2-Dibromo-3-ehloropropane
<0.5
20
20.62
103
65.5 -139
1,2,4-Trichlorobenzene
<0.5
20
20.17
101
60.5 -137
Hexachlorobutadiene
<0.5
20
21.36
107
37.0 -131
Naphthalene
<0.5
20
22.32
112
54.9 -138
1,2,3-Trichlorobenzene
<0.5
20
21.13
106
62.5 -13

ANALYTICAL & CONSULTING CHEMISTS
LCS
Environmental efists, Inc.
6602 Windmill Way, Wilmington, NC 28405 o 910.392.0223 Lab s 910.392.4424 Fax
710 Bowsertotvn Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax
iiifo c@ienvironmen(alchemists.com
Wood-Amee QC - 2019-18641
Parameter
True Value
mk/L
Result
mg/L
% Recovery
Limits
%
Ammonia
5.0
5.0
100
90-110
Ammonia
5.0
5.0
100
90-110
NO2
0.60
0.56
93
90-110
NO3 & NO2
1.00
0.90
90
90-110
Sulfate
50.0
47.0
94
90-110
TDS
600
600
100
90-110
TOC
10.0
10.3
103
90-1 10
TP
1.60
1.59
99
90-1 10
MS/MSD
Parameter
True Value
mg/1-
Recovery
tytg/L
%
RecovelT
%
Difference
Limits %
Recovery
Limits %
Difference
Ammonia
5.0
5.2/5.2
104/104
0
80-120
520
Ammonia
5.0
5.1/5.1
102/102
0
80-120
520
NO2
0.50
0.53
106
N/A
80-120
<20
NO3 &NO2
0.50
0.45/0.43
90/86
4
80-120
<20
Sulfate
10.0
10.1/10.1
101/101
0
80-120
520
TDS
N/A
N/A
N/A
N/A
80-120
<20
TOC
10.0
9.7
97
N/A
N/A
< 20
TP
1.60
1.31 /1.46
82/91
10
80/ 120
< 20

ANALYTICAL & CONSULTING CHEMISTS
DUPLICATE SAMPLES
rinvironmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 e 910.392.0223 Lab o, 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 s 910.347.5843 Lab/Fax
inFo{c7r_eaiviroizmentalchemists.com
ResultsParameter
rng/L
% Difference
Limits %
Ammonia
N/A
N/A
NIA
< 10
Ammonia
N/A
NIA
NIA
< 10
NO2
<0.02
<0.02
0
< 10
NO3 & NO2
NIA
N/A
N/A
520
Sulfate
<15
<15
0
< 10
TDS
348.00
328.00
6
< 10
TOC
1.6
1.6
0
<10
TP
NIA
N/A
N/A
<10
BLANK
Parameter
Results
mg/L
Limit
n?g/L
Ammonia
<0.1
0.1
Ammonia
<0.1
0.1
NO2
<0.01
0.01
NO3 & NO2
<0.01
0.01
Sulfate
<2.5
2.5
TDS
<2.5
2.5
TOC
<0.25
0.25
TP
<0-02
0.02

Analytical Environmental Services, Inc bate: 15Nov-19
Client: )environmental Chemists, Inc. Client Sample ID: #47433
Project Name: Formaldehyde Collection Date: 11/5/2019 2:06:00 PM
Lab ID: 1911622-004 Matrix: Aqueous
Reporting Dilution
Analyses Result Limit Qual Units i3atchlD Factor Date Analyzed Analyst
Formaldebyde by SW8315A
Formaldehyde 180 50 uglL 287695 1 11/08/201918:40 HL
Quallfietst •
Value exceeds maxim= wntaminaat level
BRL Below reporting limit
$
Holding times for preparation or analysis acceded
N
Aaalyle not NEW certified
B
Aualyte detected in the associated method blank
?
(treater than Result value
B Estimated (value above quantitation sense)
S Spike Recovery outside limits due to matrix
Nary See case nartative
NC Notconrnmed
c Leas ffim Result value
3 EstirmtW value detected below Reporting Limit
Page 7 of 16

Analytical Environmental Services, Inc Date: 15-Nov-19
Client: Environmental Chemists, Inc. Client Sample ID: #47446
Project Name: Formaldehyde Collection hate: 11/612019 9:00:00 AM
Lab Ill: 1911622-001 Matrix: Aqueous
Analyses Result xepornng Dilution
Limit Qual Units BatchID Factor Date Analyzed Analyst
Formaldehyde by SW8315A
Formaldehyde 150 50 ugJL 297695 1 11/081201917:59 HL
Qaaliren: 0 Value Woods maximum coatarnineat Icvel
BRL Below reporting limit
* [folding times far preparation or analysis exceeded
N Ana" not NELAC certified
€s Aaelyto detected in the auociatad method blank
> Grftter than Result value
E Ntimated (vatuo above quantitatien range)
S spike Recovery outside fimits due to matrix
Naff See rave narrative
NC Notconfirmed
< Less than Rtanit Value
J P-stimatedvaluedetected WnwReporting Limit
Page 4 of 16

Analytical Environmental Services, Inc
Date: 15-NOV-19
Client: Environmental Chemists, Inc. Client Sample ID: #47448
Project Name: Formaldehyde Collection Bate: 11/6/2019 9:30:00 AM
Lab ID: 1911622-002 Matriss Aqueous
Analyses Result rce ornnLimit Quai Units RatehID Dflutton Date Analyzed Analyst
Factor
Formaldehyde by SW8315A
Formaldehyde BRL 50 ug/L 287695 1 111081201918:13 HL
Quatirren: • Valutexceedamaximumcontaminantlovet
BRL Below reporting trout
H Hp€ding timed For preperntion or antlysis exceeded
N Awlyte. not NELAC certified
a Analyse detected in the U104a1ed medtod blank
> Greater then Result va€uo
8 Esfimatcd (value above. quaatilation angel
S Spike Recovery ouW4 €units due to matrix
Nary See case narretivo
NC Notcouflrmed
< Loss than Result value
7 Estimated value dclmcd below Reporting Limis
Page 5 of 16

ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
info 0 environmentalchemists.com
-2-
Client. f
PROJECT NAME: ULA
/
REPORT NO: — p
ADDRESS: -T 1'D Lf
CONTACT NAME:
PO N0: ` • Z
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REPORT TO: , v\ vvk, ' v
PHONE/FAX: `j � q 27
s 'j Zvi t j
COPY TO:
email: bc %r�, n r w z ) G G 041`
Sampled By: SAMPLE TYPE: I = Influent. E = Effluent. W = Well. ST = Strum_ SO = Soil_ SL = Sludge_ Other:
Sample Identification
Collection
a
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a c E
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PRESERVATION
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Delivered By: P Received By: _Date: —.0�_ Time: I I IQ
Comments: TUF1NAROUND• 4

NC 284
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ENVIRONMENTAL. CHEMISTS, INC 6602 ICE. 910-3 2s-223IFAX 910 392-442405
Analytical & Consulting Chemists NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 infoGenvironmentalchemists.com
!'_f11 I Pr Tif M AWN f%UAIM r%0 ru so-rnnv
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PROJECT NAME: o'nZ''�
REPORT NO:
ADDRESS:
CONTACT NAME:
REPORT TO:
PO NO: LCJ�
PHONEIFAX:
COPY TO:
email-
san' weci ev: CAaAw P -rvn=. i _ fr.31.. .,+ r _ =ui.. %a, _ iA■_.. -- -.__.-
Sample Identification
Collection
a
m
a
a o
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w
a
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"
m
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PRESERVATION
ANALYSIS REQUESTED
Date
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S1

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Wood -AMEC
5710 Oleander Drive , Suite 110
Wilmington NC 28405
Attention: Ben Moore
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report:
Dec 10, 2020
Customer PO M
6480200031
Customer ID:
11070019
Report M
2020-19982
Project ID: Hexion CLRS
Lab ID Sample ID:
20-50870 Site: WWMW-1
Test
Collect Date/Time
11/24/2020 9:15 AM
Method
Matrix Sampled by
Water Client
Results Date Analyzed
Sulfate
EPA 300.0
772 mg/L
11/24/2020
Ammonia Nitrogen
EPA 350.1
610 mg/L
12/04/2020
Total Dissolved Solids (TDS)
SM 2540 C
1380 mg/L
11/24/2020
Total Phosphorus
SM 4500 P F
1.43 mg/L
12/07/2020
Total Organic Carbon (TOC)
SM 5310 B
81.2 mg/L
11/24/2020
1, 1, 1,2-Tetrachloroethane
SW 846 method 826013/50308
< 0.50 pg/L
12/5/2020
1, 1, 1 -Trichloroethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
1,1,2,2-Tetrachloroethane
SW 846 method 82608/503013
< 0.50 pg/L
12/5/2020
1,1,2-Trichloroethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
1,1-Dichloroethane
SW 846 method 826013/5030B
< 0.50 pg/L
12/5/2020
1, 1 -Dichloroethene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
1,1-Dichloropropene
SW 846 method 826013/50306
< 0.50 pg/L
12/5/2020
1,2,3-Trichlorobenzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
1,2,3-Trichloropropane
SW 846 method 82608/50306
< 0.50 pg/L
12/5/2020
1,2,4-Trichlorobenzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
1,2,4-Trimethyl benzene
SW 846 method 82608/503013
< 0.50 pg/L
12/5/2020
1,2-Dibromo-3-Chloropropane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
1,2-Dibromoethane
SW 846 method 826013/5030B
< 0.50 pg/L
12/5/2020
1,2-Dichlorobenzene
SW 846 method 826OB15030B
< 0.50 pg/L
12/5/2020
1,2-Dichloroethane
SW 846 method 826013/5030B
< 0.50 pg/L
12/5/2020
1,2-Dichloropropane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
1,3,5-Trimethylbenzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
1,3-Dichlorobenzene
SW 846 method 8260B15030B
< 0.50 pg/L
12/5/2020
1,3-Dichloropropane
SW 846 method 826013/5030B
< 0.50 pg/L
12/5/2020
1,4-Dichlorobenzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
2,2-Dichloropropane
SW 846 method 826013/5030B
< 0.50 pg/L
12/5/2020
Report #:: 2020-19982 Page 1 of 6

F""W' -- —, -4"7 Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab • 910.392.4424 Fax
5M, 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
Qs ' 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Wood -AMEC
5710 Oleander Drive, Suite 110
Wilmington NC 28405
Attention: Ben Moore
Date of Report: Dec 10, 2020
Customer PO #: 6480200031
Customer ID: 11070019
Report #: 2020-19982
Project ID: Hexion CLRS
2-Chlorotoluene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
4-Chlorotoluene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Benzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Bromobenzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Bromochloromethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Bromodichloromethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Bromoform
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Bromomethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Carbon tetrachloride
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Chlorobenzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Chloroethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Chloroform
SW 846 method 82606/5030B
< 0.50 pg/L
12/5/2020
Chloromethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
cis-1,2-Dichloroethene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
cis- 1,3-Dichloropropene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Dibromochloromethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Dibromomethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Dichlorodifluoromethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Ethylbenzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Hexachlorobutadiene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Isopropylbenzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
M+P Xylene
SW 846 method 8260B/5030B
< 1.00 pg/L
12/5/2020
Methylene chloride
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Naphthalene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
n-Butylbenzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
n-Propylbenzene
SW 846 method 82606/5030B
< 0.50 pg/L
12/5/2020
ortho-Xylene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
p-Isopropyltoluene
SW 846 method 82608/5030B
< 0.50 pg/L
12/5/2020
sec -Butyl benzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Styrene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Report # 2020-19982
Page 2 of 6

r7-71 Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
Am255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Wood -AMEC
5710 Oleander Drive, Suite 110
Wilmington NC 28405
Attention: Ben Moore
Date of Report: Dec 10, 2020
Customer PO #: 6480200031
Customer ID: 11070019
Report #: 2020-19982
Project ID: Hexion CLRS
tert-B utyl benzene
SW 846 method 82608/503013
< 0.50 pg/L
12/5/2020
Tetrachloroethene
SW 846 method 82606/5030B
< 0.50 pg/L
12/5/2020
Toluene
SW 846 method 826013/5030B
< 0.50 pg/L
12/5/2020
Trans-1,2-Dichloroethene
SW 846 method 82606/50308
< 0.50 pg/L
12/5/2020
Trans-1,3-dichloropropene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Trichloroethene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Trichlorofluoromethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Vinyl chloride
SW 846 method 826013/5030B
< 0.50 pg/L
12/5/2020
Formaldehyde
SW846 8315A
380.0 pg/L
11 /27/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2
< 0.02 mg/L
11/25/2020
Nitrate+Nitrite-Nitrogen EPA 353.2
0.07 mg/L
11/30/2020
Nitrate Nitrogen Subtraction Method
0.07 mg/L
12/05/2020
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN) EPA 351.2
562 mg/L
12/09/2020
Total Nitrogen Total Nitrogen
562 mg/L
12/10/2020
Report C 2020-19982 Page 3 of 6

r777 Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
srn' 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Wood -AMEC
Date of Report: Dec 10, 2020
5710 Oleander Drive, Suite 110
Customer PO #: 6480200031
Wilmington NC 28405
Customer ID: 11070019
Attention: Ben Moore
Report M 2020-19982
Project ID: Hexion CLRS
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
20-50871 Site: WWMW-2
11/24/2020
9:00 AM Water Client
Test
Method
Results
Date Analyzed
Sulfate
EPA 300.0
327 mg/L
11/24/2020
Ammonia Nitrogen
EPA 350.1
28.5 mg/L
12/02/2020
Total Dissolved Solids (TDS)
SM 2540 c
679 mg/L
11/24/2020
Total Phosphorus
SM 4500 P F
0.12 mg/L
12/07/2020
Total Organic Carbon (TOC)
SM 5310 B
5.9 mg/L
11/24/2020
1, 1, 1,2-Tetrachloroethane
SW 846 method 826013/50308
< 0.50 pg/L
12/5/2020
1, 1, 1 -Trichloroethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
1,1,2,2-Tetrachloroethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
1,1,2-Trichloroethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
1,1-Dichloroethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
1,1-Dichloroethene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
1,1-Dichloropropene
SW 846 method 826013/5030B
< 0.50 pg/L
12/5/2020
1,2,3-Trichlorobenzene
SW 846 method 82606/5030B
< 0.50 pg/L
12/5/2020
1,2,3-Trichloropropane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
1,2,4-Trichlorobenzene
SW 846 method 82608/503013
< 0.50 pg/L
12/5/2020
1,2,4-Trimethylbenzene
SW 846 method 82606/5030B
< 0.50 pg/L
12/5/2020
1,2-Dibromo-3-Chloropropane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
1,2-Dibromoethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
1,2-Dichlorobenzene
SW 846 method 82606/5030B
< 0.50 pg/L
12/5/2020
1,2-Dichloroethane
SW 846 method 826013/50306
< 0.50 pg/L
12/5/2020
1,2-Dichloropropane
SW 846 method 82608/503013
< 0.50 pg/L
12/5/2020
1,3,5-Trimethylbenzene
SW 846 method 826OB15030B
< 0.50 pg/L
12/5/2020
1,3-Dichlorobenzene
SW 846 method 826013/50308
< 0.50 pg/L
12/5/2020
1,3-Dichloropropane
SW 846 method 82606/5030B
< 0.50 pg/L
12/5/2020
1,4-Dichlorobenzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
2,2-Dichloropropane
SW 846 method 82608/503013
< 0.50 pg/L
12/5/2020
Report #:: 2020-19982
Page 4 of 6

Environmental Chemists, Inc.
envirochem
ANALYTICAL & CONSULTING CHEMISTS
Wood -AMEC
5710 Oleander Drive, Suite 110
Wilmington NC 28405
Attention: Ben Moore
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Dec 10, 2020
Customer PO #: 6480200031
Customer ID: 11070019
Report #: 2020-19982
Project ID: Hexion CLRS
2-Chlorotoluene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
4-Chlorotoluene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Benzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Bromobenzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Bromochloromethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Bromodichloromethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Bromoform
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Bromomethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Carbon tetrachloride
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Chlorobenzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Chloroethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Chloroform
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Chloromethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
cis-1,2-Dichloroethene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
cis- 1,3-Dichloropropene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Dibromochloromethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Dibromomethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Dichlorodifluoromethane
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Ethylbenzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Hexachlorobutadiene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Isopropylbenzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
M+P Xylene
SW 846 method 8260B/5030B
< 1.00 pg/L
12/5/2020
Methylene chloride
SW 846 method B260B/5030B
< 0.50 pg/L
12/5/2020
Naphthalene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
n-Butylbenzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
n-Propylbenzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
ortho-Xylene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
p-Isopropyltoluene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
sec-B utyl benzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Styrene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Report # . 2020-19982
Page 5 of 6

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
's;,', 255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Wood -AMEC
5710 Oleander Drive, Suite 110
Wilmington NC 28405
Attention: Ben Moore
Date of Report: Dec 10, 2020
Customer PO #: 6480200031
Customer ID: 11070019
Report #: 2020-19982
Project ID: Hexion CLRS
tert-B utyl benzene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Tetrachloroethene
SW 846 method 82608/503013
< 0.50 pg/L
12/5/2020
Toluene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Trans- 1,2-Dichloroethene
SW 846 method 826013/503013
< 0.50 pg/L
12/5/2020
Trans-1,3-dichloropropene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Trichloroethene
SW 846 method 8260B/5030B
< 0.50 pg/L
12/5/2020
Trichlorofluoromethane
SW 846 method 826013/503013
< 0.50 pg/L
12/5/2020
Vinyl chloride
SW 846 method 826013/5030B
< 0.50 pg/L
12/5/2020
Formaldehyde
SW846 8315A
330.0 pg/L
11/27/2020
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 3532
0.03mg/L
11/25/2020
Nitrate+Nitrite-Nitrogen EPA 353.2
43.9 mg/L
11/30/2020
Nitrate Nitrogen Subtraction Method
48.9 mg/L
12/05/2020
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN) EPA 351 2
18.6 mg/L
12/02/2020
Total Nitrogen Total Nitrogen
62.4 mg/L
12/08/2020
Comment:
Reviewed by:
Report #.: 2020-19982 Page 6 of 6

Environmental Chemists, Inc.
envirochem
ANALYTICAL & CONSULTING CHEMISTS
LCS
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
[e-mail]
Wood-Amec QC - 2020-19982
Parameter
True Value
mg/L
Result
mg1L
% Recovery
Limits
%
Ammonia
5.0
5.1
102
90-110
Ammonia
5.0
5.0
100
90-110
NO2
0.60
0.63
105
90-110
NO3 & NO2
1.00
0.92
92
90-110
Sulfate
50.0
47.2
94
90-110
TDS
600
602
100
90-110
TOC
10.0
10.3
103
90- 110
TKN
4.0
3.8
95
90-110
TKN
4.0
3.8
95
90-110
TP
1.60
1.50
94
90-110
MS/MSD
Parameter
True Value
mg1L
Recovery
mg1L
%
Recovery
%
Difference
Limits %
Recovery
Limits %
Difference
Ammonia
4.0
4.0/3.8
100/95
5
80-120
<20
Ammonia
4.0
4.2/4.2
1051105
0
80-120
<20
NO2
0.50
0.56/0.55
112/ 110
2
80-120
<20
NO3 & NO2
0.50
0.49/0.50
98/100
2
80-120
520
Sulfate
10.0
8.0/8.0
80/80
0
80-120
<20
TDS
75.0
83.0
111
N/A
80-120
<20
TOC
10.0
9.5
95
N/A
N/A
<20
TKN
4.0
3.7/3.8
92/95
3
N/A
<20
TKN
4.0
3.8/4.0
951100
5
N/A
<20
TP
2.00
1.99/1.85
99/93
6
80/120
<20

DUPLICATE SAMPLES
Parameter
Results/L
g
% Difference
Limits
Ammonia
N/A
N/A
N/A
< 10
Ammonia
N/A
N/A
N/A
N/A
NO2
N/A
N/A
N/A
< 10
NO3 & NO2
N/A
N/A
N/A
< 20
Sulfate
7.0
7.0
0
< 10
TDS
1408
1355
4
< 10
TOC
9.7
9.4
3
<10
TKN
N/A
N/A
N/A
<10
TKN
N/A
N/A
N/A
510
TP
N/A
N/A I
N/A
:510
BLANK
Parameter
Results
mg1L
Limit
mg/L
Ammonia
<0.1
0.1
Ammonia
<0.1
0.1
NO2
<0.01
0.01
NO3 & NO2
<0.01
0.01
Sulfate
<2.5
2.5
TDS
<2.5
2.5
TOC
<0.25
0.25
TKN
<0.25
0.25
TKN
<0.25
0.25
TP
<0.02
0.02

Analytical Environmental Services, Inc
Date: 2-Dec-20
Client:
Environmental Chemists, Inc.
Client Sample ID:
#50870
Project Name:
50870-58071
Collection Date:
11/24/2020 9:15:00 AM
Lab ID:
2011T12-001
Matrix:
Aqueous
Analyses Result xepornng Dilution
Limit Qual Units BatchID Factor Date Analyzed Analyst
Formaldehyde by SW8315A
Formaldehyde 380 50 ug/L 306544 1 l 1/27/2020 16 23 HL
Qualifiers: • Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limn
Page 3 of 8

Analytical Environmental Services, Inc
Date: 2-Dec-20
Client:
Environmental Chemists, Inc.
Client Sample ID:
#50871
Project Name:
50870-58071
Collection Date:
11/24/2020 9:00:00 AM
Lab ID:
2011T12-002
Matrix:
Aqueous
Analyses Result nepornn
Limit
Qual Units BatchlD Factor Dilution Date Analyzed Analyst
Formaldehyde by SW8315A
Formaldehyde 330 50 ug/L 306544 1 11/27/202016:37 HL
Qualifiers: ' Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Grmter than Result value
E Estimated (value above quantization range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit
Page 4 of 8

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client:_Woo ib Date: t Report Number:.O--
Receipt of sample:
ECHEM Pickup ❑ Client Delivery I
JUPS ❑ FedEx ❑ Other ❑
❑ YES
❑
NO
0 N/A
11. Were custody seals present on the cooler?
❑ YES
❑
NO
tq N/A 12.
If custody seals were present, were they intact/unbroken?
Original temperature upon receipt —3. 3—°C Corrected temperature upon receipt
How temperature taken:
❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES
❑
NO
1 3. If temperature of cooler exceeded VC, was Project Mgr./QA notified?
YES
10
NO
1 4. Were proper custody procedures (relinquished/received) followed?
YES
10
NO
1 5. Were sample ID's listed on the COC?
YES
10
NO
1 6. Were samples ID's listed on sample containers?
YES
10
NO
1 7. Were collection date and time listed on the COC?
JIg YES
10
NO
1 8. Were tests to be performed listed on the COC?
R YES
10
NO
1 9. Did samples arrive in proper containers for each test?
IX YES
I0
NO
110. Did samples arrive in good condition for each test?
YES
10
NO
111. Was adequate sample volume availableT
YES
10
NO
112. Were samples received within proper holding time for requested tests?
YES
10
NO
113. Were acid preserved samples received at a pH of <2?
❑ YES
10
NO
114. Were cyanide samples received at a pH >12?
❑ YES
❑
NO
115. Were sulfide samples received at a pH >9?
YES
❑
NO
116. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
YES
10
NO 117.
Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
10
NO 118.
Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1
'C

ENVIRONMENTAL CHEMISTS, INC
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: Vi 6M
PROJECT NAME: V /dGmz
REPORT NO: ZO_
ADDRESS: 5-7) b (OU r e
CONTACT NAME: r r u l -Gb y-r
PO NO: woz'o 6d3 7
IT q
REPORT TO: 04 Mr{
PHONE/FAX:
COPY TO:
email: -bev,, mbzy-P WDts'p IC_ , C
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
a
HN
E
N
N
c c
"
_
C 0
c°
" a
C=
t E
N
p
o
a
W
0°co
g Z
PRESERVATION
ANALYSIS REQUESTED
Date
Time
Temp
Z
Z
v
N
==
o
o
Z~
G
LU
w=
LL
o
On-
lJ
o1�
,6
�S
P
bo�71
�2 0 Z �
§
C
P
I
To L
4-
0
A
C
P
F�II
4, cj V,
C
P
©
G.
c
G
G
IN
C
�S
G
f o Uf7
I,
y
Y'
520d �ti^,04 i� �&j et a �
I G
G
C
P
h
N �� e h rn�St� Spun 0'1 c her 1�
G
G
NOTICE - DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacteria must be dechlorinated (0.5 ppm or less) in the field at the time of collection. See reverse for instructions
Transfer
Relinquished By:
Date/Time
Received By:
Date/Time
1.
AAI
L ?rJ j 26
2.
Temperature when Received °C: ---S . J Accepted: Iff r d: Resarr�gI Req ested:
Delivered By: �, Received By: Date;;tComments: �_TURNAROUND: CV-' c."'

[env7irroche]m
ANALYTICAL & CONSULTING CHEMISTS
Wood -AM EC
5710 Oleander Drive, Suite 110
Wilmington NC 28405
Attention: Ben Moore
Lab ID Sample ID:
21-49902 Site: WWMW-1
Test
Sulfate
Ammonia Nitrogen
Total Dissolved Solids (TDS)
Total Phosphorus
Total Organic Carbon (TOC)
1, 1, 1,2-Tetrachloroethane
1, 1, 1 -Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report:
Nov 22, 2021
Customer PO #:
6480210006
Customer ID:
11070019
Report #:
2021-19942
Project ID: Hexion CLRS
Collect Date/Time Matrix
11/10/2021 9:40 AM Water
Method
EPA 300.0, Rev. 2.1, 1993
EPA 350.1, Rev. 2.0, 1993
SM 2540 C-2015
SM 4500 P (F-H)-2011
SM 5310 B-2014
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
Results
Sampled by
Client
Date Analyzed
1590 mg/L
11 /15/2021
760mg/L
11/16/2021
2410 mg/L
11/10/2021
1.56 mg/L
11/19/2021
90.4 mg/L
11/11/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
<1 pg/L
11/14/2021
Report #:: 2021-19942 Page 1 of 6

F"00- -- —, -"q7 Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
4 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Wood -AMEC
Date of Report: Nov 22, 2021
5710 Oleander Drive, Suite 110
Customer PO #: 6480210006
Wilmington NC 28405
Customer ID: 11070019
Attention: Ben Moore
Report #: 2021-19942
Project ID: Hexion CLRS
2-Chlorotoluene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
4-Chlorotoluene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Benzene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Bromobenzene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Bromochloromethane
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Bromodichloromethane
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Bromoform
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Bromomethane
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Carbon tetrachloride
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Chlorobenzene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Chloroethane
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Chloroform
SW 846 Method 8260D15030B
<1 pg/L
11/14/2021
Chloromethane
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
cis- 1,2-Dichloroethene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
cis-1,3-Dichloropropene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Dibromochloromethane
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Dibromomethane
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Dichlorodifluoromethane
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Ethylbenzene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Isopropylbenzene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
M+P Xylene
SW 846 Method 8260D/5030B
<2 pg/L
11/14/2021
Methylene chloride
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Naphthalene
SW 846 Method 8260D/5030B
3.10 pg/L
11/14/2021
n-Butylbenzene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
n-Propylbenzene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
ortho-Xylene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
sec -Butyl benzene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Styrene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Report #. 2021-19942 Page 2 of 6

gnZvirochem]
ANALYTICAL & CONSULTING CHEMISTS
Wood -AMEC
5710 Oleander Drive, Suite 110
Wilmington NC 28405
Attention: Ben Moore
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report:
Nov 22, 2021
Customer PO #:
6480210006
Customer ID:
11070019
Report #:
2021-19942
Project ID: Hexion CLRS
tert-Butyl benzene
SW 846 Method 826013/503013
<1 pg/L
11/14/2021
Tetrachloroethene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Toluene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Trans-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Trans- 1,3-dichloropropene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Trichloroethene
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Vinyl chloride
SW 846 Method 8260D/5030B
<1 pg/L
11/14/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA353.2, Rev. 2.0,1993
0.02 mg/L
11/11/2021
Nitrate Nitrogen
Subtraction Method
0.05 mg/L
11/18/2021
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev. 2.0, 1993
774 mg/L
11/17/2021
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0,1993
0.07mg/L
11/11/2021
Total Nitrogen
Total Nitrogen
774 mg/L
11/18/2021
Report #:: 2021-19942 Page 3 of 6

[envirroehem]
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
[e-mail]
Wood -AMEC Date of Report: Nov 22, 2021
5710 Oleander Drive, Suite 110 Customer PO #: 6480210006
Wilmington NC 28405 Customer ID: 11070019
Attention: Ben Moore Report #: 2021-19942
Project ID: Hexion CLRS
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
21-49903 Site: WWMW-2 11/10/2021 9:20 AM Water Client
Test Method Results Date Analyzed
Sulfate
EPA 300.0, Rev. 2.1,1993
261 mg/L
11/15/2021
Ammonia Nitrogen
EPA 350.1, Rev. 2.0,1993
64.2 mg/L
11/15/2021
Total Dissolved Solids (TDS)
SM 2540 C-2015
513 mg/L
11 /10/2021
Total Phosphorus
SM 4500 P (F-H)-2011
0.11 mg/L
11 /19/2021
Total Organic Carbon (TOC)
SM 5310 B-2014
6.0 mg/L
11/12/2021
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1, 1, 1 -Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1,1,2-Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1,1-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1,1-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1,1-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1,2,3-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1,2,3-Trichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1,2,4-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1,2,4-Trimethyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1,2-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1,2-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Report #:: 2021-19942 Page 4 of 6

Eenviroclhftem
ANALYTICAL & CONSULTING CHEMISTS
Wood -AMEC
5710 Oleander Drive , Suite 110
Wilmington NC 28405
Attention: Ben Moore
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report:
Nov 22, 2021
Customer PO #:
6480210006
Customer ID:
11070019
Report #:
2021-19942
Project ID: Hexion CLRS
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Chloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
cis- 1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
cis-1,3-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Dibromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Dibromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Dichlorodifluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Ethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Isopropylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
11/14/2021
Methylene chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
sec-B utyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Styrene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Report #:: 2021-19942
Page 5 of 6

F--71 Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
sM 710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Wood -AMEC
Date of Report: Nov 22, 2021
5710 Oleander Drive, Suite 110
Customer PO #: 6480210006
Wilmington NC 28405
Customer ID: 11070019
Attention: Ben Moore
Report #: 2021-19942
Project ID: Hexion CLRS
tert-B utyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Tetrachloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Toluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Trans- 1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Trans- 1,3-dichloropropene
SW 846 Method 8260D/6030B
<0.5 pg/L
11/14/2021
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/14/2021
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA353.2, Rev. 2.0,1993
0.15 mg/L
11/11/2021
Nitrate Nitrogen
Subtraction Method
5.09 mg/L
11/18/2021
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev. 2.0,1993
48.2 mg/L
11/17/2021
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0,1993
5.24 mg/L
11/12/2021
Total Nitrogen
Total Nitrogen
53.4 mg/L
11/18/2021
Comment: Sample # 2149902-Method 8260D-Reporting limit elevated due to matrix interference
Reviewed by:
Report #:: 2021-19942 Page 6 of 6

F7 7 W 7
gnZviroche]m]
ANALYTICAL & CONSULTING CHEMISTS
LCS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
[e-mail]
Wood-Amec QC - 2021-19942
Parameter
True Value
mg'L
Result
mg1L
% Recovery
Limits
%
Ammonia
5.0
5.0
100
90-110
Ammonia
5.0
4.9
98
90-110
NO2
0.60
0.55
92
90-110
NO3 & NO2
1.00
1.09
109
90-110
Sulfate
50.0
46.6
93
90-110
TDS
600
599
100
90-110
TOC
10.0
9.7
97
90-110
TOC
10.0
8.9
89
90- 110
TKN
4.0
4.1
102
90-110
TP j
1.60 j
1.66 1
104 j
90-110
I"YMT11
Parameter
True Value
mg1L
Recovery
mg/L
%
Recovery
%
Difference
Limits %
Recovery
Limits %
Difference
Ammonia
2.0
2.0/2.1
1001105
5
80-120
<20
Ammonia
2.0
2.1/2.1
1051105
0
80-120
<20
NO2
0.50
0.50/0.52
100/104
4
80-120
<20
NO3 & NO2
0.50
0.47/0.49
94/98
4
80-120
< 20
Sulfate
10.0
8.5/8.4
85/84
1
80-120
<20
TDS
N A
N/A
N/A
N/A
80-120
<20
TOC
10.0
10.6
106
N/A
N/A
< 20
TOC
10.0
10.4
104
N/A
N/A
< 20
TKN
4.0
4.0/4.1
100/ 102
2
N/A
< 20
TP
2.50
2.56/2.51 j
102/ 100 j
2 j
80./ 120 j
< 20

Environmental Chemists, Inc.
nnvirochem
ANALYTICAL & CONSULTING CHEMISTS
DUPLICATE SAMPLES
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Parameter
Results
mg L
% Difference
Limits °o
Ammonia
N/A
N/A
N A
< 10
Ammonia
NIA
N/A
N/A
N/A
NO2
N/A
N/A
N/A
< 10
NO3 & NO2
N/A
N/A
N/A
< 20
Sulfate
<15
<15
0
<_ 10
TDS
985
1005
2
< 10
TOC
<1
<1
0
<10
TOC
<1
<1
0
<10
TKN
N/A
N/A
N/A
<10
TP j
N/A
N/A i
N/A
<10
BLANK
Parameter
Results
mg/L
Limit
M91L
Ammonia
<0.1
0.1
Ammonia
<0.1
0.1
NO2
<0.01
0.01
NO3 & NO2
<0.01
0.01
Sulfate
<2.5
2.5
TDS
<2.5
2.5
TOC
<0.25
0.25
TOC
<0.25
0.25
TKN
<0.25
0.25
TP
<0.02
0.02

Analytical Environmental Services, Inc
Date: 16-Nov-21
Client:
Environmental Chemists, Inc.
Client Sample ID:
21-49902
Project Name:
2021-19942
Collection Date:
11/10/2021 9:40:00 AM
Lab ID:
2111D82-001
Matrix:
Aqueous
Reporting Dilution
Analyses Result Qual Units BatchlD Date Analyzed Analyst
Limit Factor
Formaldehyde by SW8315A
Formaldehyde
Qualifiers: • Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
710 250 ug/L 325646 1 11/12/2021 14:18 DS
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
1 Estimated value detected below Reporting Limit
^ ��� '�-Z Page 3of8

Analytical Environmental Services, Inc
Date: 16-Nov-21
Client:
Environmental Chemists, Inc.
Client Sample ID:
21-49903
Project Name:
2021-19942
Collection Date:
11/10/2021 9:40:00 AM
Lab ID:
2111D82-002
Matrix:
Aqueous
Keporting Dilution
Analyses Result Qua[ Units BatchID Date Analyzed Analyst
Limit Factor
Formaldehyde by SW8315A
Formaldehyde 79 50 ug/L 325646 1 11/12/202114:29 DS
Qualifiers: ' Value exceeds maximum contaminant level
BRL Below reporting limn
H Holding times for preparation or analysts exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantiration range)
S Spike Recovery outside limits due to matrix
Nair See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limn
Page 4 of 8

Environmental Chemist, Inc., Wilmington, NIC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client:\Iqml) Date( � � �� Report Number: _ 02
Receipt of sample: ECHEM Pickup ❑ Client Delivery A
JUPS ❑ FeclEx ❑ Other ❑
❑ YES
❑ NO
N/A
1. Were custody seals present on the cooler?
❑ YES
ID NO
N/A
12. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt 1 01 °C Ct Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES
I ❑ NO
1 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
JW YES I0
NO
14. Were proper custody procedures (relinquished/received) followed?
YES 10
NO
5. Were sample ID's listed on the COC?
YES 10
NO
6. Were samples ID's listed on sample containers?
YES 10
NO
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive in proper containers for each test?
YES
❑ NO 110.
Did samples arrive in good condition for each test?
tz ES ❑ IN 11
ii. VVas adequate sample volume availableT
PQ YES ❑ NO 112.
Were samples received within proper holding time for requested tests?
YES I ❑ NO 113.
Were acid preserved samples received at a pH of <2?
❑ YES I0 NO
14. Were cyanide samples received at a pH >12?
❑ YES ❑ NO
vrc I In Rin
15. Were sulfide samples received at a pH >9?
,- ,.. _ ,_.__. —
COMMENTS:
DOC_ OA nn7 Rav 1

Analytical & Consulting Chemists
Client: w
ADDRESS:
?'\ ') �
Sampled B
Sample Identification
WWMW- roI
W
IN
NOTICE - DECHLORINATION:
Transfer
Coll
Date I Tim
ENVIRONMENTAL CHEMISTS, IN C OFFICE: 910-392-02 36602 Windmill Way FAX910 Wilmington,3NC 92-4424 5
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
PROJECT NAME: l�� AI' 1v� C�-'Z S REPORT NO: p� j — 9 Va—
1 CONTACT NAME: y` PO NO: b� 21 Q1
REPORT TO: h�� PHONE/FAX: I J S
COPY TO:
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
on a d a
PRESERVATION
0 A C f.7 c` 0 e W 0
E o c` o a_ r E `o a Im z -j o o p o� W ANALYSIS REQUESTED
p U J O O U fn z x W x
e Temp y " " a z z x= x i i.-
_j o
W G P �R4 ZCO Ll, / ' ' �—
C P
C P
G G <. Z
C P
II is 2 G G t�C
C P
G G
C P
G G
C P _
G G ` •.
pies for Ammonia, TKN, Cyanide, Phenol and Bacteria must be dechlorinated (0.5 ppm or Ii
Relinquished B Date/Time
1. kl,
2.
Temperature when Received °C: Accepted: I
Delivered By: Received By:
Comments:
� P63S 1ro„us� I�wtr�,oHif,
926v zu, Tvc�
-ros, SvIf I
�J %W��n�G NI w�cr,C4s N
in the field at the time of collection. See reverse for Instructions
Received By: I Date/Time
Resam4�I Re uested:
Date: D Time:
TURNARO ND:
ro�t�,

Environmental Chemists, Inc.
envirochem
ANALYTICAL & CONSULTING CHEMISTS
Wood - WSP USA E&I Inc
5710 Oleander Drive. Suite 110
Wilmington NC 28405
Attention:
Lab ID Sample ID:
23-11559 Site: WWMW-01
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab + 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
infbf4environmentalchemisls.com
Date of Report:
Mar 27, 2023
Customer PO #:
6228232003
Customer ID:
11070019
Report #:
2023-04647
Project ID: Bakelite Acme CLRS
Collect Date/Time Matrix Sampled by
3/8/2023 9:20 AM Water Client
Test
Method
Results
Date Analyzed
Iron
EPA 200 7. Rev. 4.4 ' 994 (Dissolved)
5.58 mg/L
03/14/2023
Manganese
EPA 200 7 Rev 4 4 1994 (Dissolved;
0.520 mg/L
03/14/2023
Sulfate
EPA 300 0 Rev 2 1 1993
1020 mg/L
03/09/2023
Ammonia Nitrogen
EPA 3501 Rev 2 0 1993
490 mg/L
03/16/2023
Total Dissolved Solids (TDS)
SM 2640 c-2015
1310 mg/L
03/08/2023
Total Phosphorus
SM 4600 P (F.-H, .2011
0.16 mg/L
03/15/2023
Sulfide
SM 4500 S D-2011
3.94 mg/L
03/13/2023
Total Organic Carbon (TOC)
SM 5310 B-2014
26.6 mg/L
03/13/2023
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D150308
< 0.50 pg/L
3/21/2023
1, 1, 1 -Trichloroethane
SW 846 Method 82BOD15030B
< 0.50 pg/L
3/21/2023
1,1,2,2-Tetrachloroethane
SW 8" Method 8260D15030B
< 0.50 pg/L
3/21/2023
1,1,2-Trichloroethane
SW 846 Method 8260D1503013
< 0.50 pg/L
3/21/2023
1,1-Dichloroethane
SW 80 Method 8260D15030B
< 0.50 pg/L
3/21/2023
1,1-Dichloroethene
SW MO Method 82BOD15030B
< 0.50 pg/L
3/21/2023
1,1-Dichloropropene
SW US Method 8260D/5030B
< 0.50 pg/L
3/21/2023
1, 2, 3-Trichlorobenzene
SW $46 Method 82SOD15030B
< 0,50 pg/L
3/21/2023
1,2,3-Trichloropropane
SW 846 Method 8260DIS030B
< 0.50 pg/L
3/21/2023
1,2,4-Trichlorobenzene
SW $46 Method 82BOD/5030B
< 0.50 pg/L
3/21/2023
1,2,4-Trimethylbenzene
SW 846 Method 82BODIS030B
< 0.50 pg/L
3/21/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 826OD16030B
< 0.50 pg/L
3/21/2023
1,2-Dibromoethane
SW 846 Method 828OD150308
< 0.50 pg/L
3/21/2023
1,2-Dichlorobenzene
SW Me Method 82GOD15030B
< 0.50 pg/L
3/21/2023
1,2-Dichloroethane
SW 846 Method 8260D150308
< 0.50 pg/L
3121 /2023
1,2-Dichloropropane
SW 846 Method 8260D15030B
< 0.50 pg/L
3/21/2023
1, 3,5-Trimethylbenzene
SW $46 Method 82BOD15030B
< 0.50 pg/L
3/21/2023
1,3-Dichlorobenzene
SW 846 Method 826OD15030B
< 0.50 pg/L
3/21/2023
Report # 2023-04647 Page 1 of 9

Environmental Chemists, Inc.
envirochem
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
info(r7;environmentalchemists.com
Wood - WSP USA E$I Inc
Date of Report: Mar 27, 2023
5710 Oleander Drive, Suite 110
Customer PO #: 6228232003
Wilmington NC 28405
Customer ID: 11070019
Attention:
Report #: 2023-04647
Project ID: Bakelite Acme CLRS
1, 3-Dichloropropane
SW 846 Method 8260DIS030B
< 0.50 pg/L
3/21/2023
1,4-Dichlorobenzene
SW 846 Method 826OD15030B
< 0.50 pg/L
3/21/2023
2,2-Dichloropropane
SW 846 Method 826OD15030B
< 0.50 pg/L
3/21/2023
2-Chlorotoluene
SW 846 Method 8250DI5030B
< 0.50 pg/L
3/21/2023
2-Hexanone
SW 846 Method 8250DIS0308
< 2.50 pg/L
3/21/2023
4-Chlorotoluene
SW a46Method 8260DI50309
< 0.50 pg/L
3/21/2023
Acetone
SW 846 Method 8260M5030B
6.26 pg/L
3/21/2023
Acrolein
SW 846 Method 826OD15030B
< 5.00 pg/L
3/21/2023
Acrylonitrile
SW 846 Method 826OD150308
< 5.00 pg/L
3/21/2023
Benzene
SW 846 Method 8260D150308
< 0.60 pg/L
3/21/2023
Bromobenzene
SW "S Method 826OD15030B
< 0.50 pg/L
3/21/2023
Bromochloromethane
SW 846 Method 8280015030B
< 0.50 pg/L
3/21/2023
Bromodlchloromethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
3/21/2023
Bromoform
SW 846 Method 826OD15030B
< 0.50 pg/L
3/21/2023
Bromomethane
SW 846 Method 8280D15030B
< 0.50 pg/L
3/21/2023
Carbon Disulfide
SW 846 Method 826OD16030B
380 pg/L
03/21/2023
Carbon tetrachloride
SW 846 Method 826OD15030B
< 0.50 pg/L
3/21/2023
Chlorobenzene
SW 848 Method 82BOD150308
< 0.50 pg/L
3/21/2023
Chloroethane
SW 846 Method 8260DI5030B
< 0.50 pglL
3/21/2023
Chloroform
SW 846 Method 82BODI5030B
< 0.50 pg/L
3/21/2023
Chloromethane
SW so Method 826OD150308
< 0.50 pg/L
3/21/2023
cis-1,2-Dichloroethene
SW 846 Method 82BOD160308
< 0.50 pg/L
3/21/2023
cis-1,3-Dichloropropene
SW 846 Method 82BOD15030B
< 0.50 pg/L
3/21/2023
Dibromochloromethane
SW 846 Method 8260DI5030B
< 0.50 pg/L
3/21/2023
Dibromomethane
SW 846 Method 8260DI5030B
< 0.50 pg/L
3121 /2023
Dichlorodifluoromethane
SW 846 Method 8280D/50013
< 0.50 pg/L
3/21/2023
Ethylbenzene
SW 846 Method 8260D15030B
< 0.50 pg/L
3/21/2023
Hexachlorobutadiene
SW 846 Method 82SOD15030B
< 0.50 pg/L
3/21/2023
I PE
SW 646 Method 8260D15030B
< 0.50 pg/L
3/21/2023
Isopropylbenzene
SW 846 Method 8260D15030B
< 0.50 pg/L
3/21/2023
Report* 2023-04647
Page 2 of 9

ANALYTICAL & CONSULTING CHEMISTS
Wood - WSP USA E&I Inc
5710 Oleander Drive, Suite 110
Wilmington NC 28405
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab * 910.392.4424 Fax
710 $owsertown Road, Manteo, NC 27954 • 252.4735702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 + 910.347.5843 Lab/Fax
infoC§ environmentalchemists.com
Date of Report:
Mar 27, 2023
Customer PO #:
6228232003
Customer ID:
11070019
Report #:
2023-04647
Project ID: Bakelite Acme CLRS
M+P Xylene
SW 846 Method 82ND15030B
< 1.00 µg/L
3/21/2023
MEK
SW 848 Method 8260DIS0308
< 2.50 µg/L
3/21/2023
Methylene chloride
SW 846 Method 8260D15030B
< 0.50 µg/L
3/21/2023
MIBK
SW 846 Method MOD15030B
< 2.50 µg/L
3/21/2023
MTBE
SW 846 Method 826013/503013
< 0.50 µg/L
3121 /2023
Naphthalene
SW 846 Method 8280DIS030B
< 0.50 pg/L
3/21/2023
n-Butylbenzene
SW 046 Method 826OD15030B
< 0.50 pg/L
3/21/2023
n-Propylbenzene
SW 846 Method 8260DIS030B
< 0.50 µg/L
3/21/2023
ortho-Xylene
SW 80 Method 8260DIS0308
< 0.50 µg/L
3/21/2023
p-isopropyltoluene
SW 846 Method 82BOD15030B
< 0.50 µg/L
3/21/2023
sec-Butylbenzene
SW 846 Method 826OD15030B
< 0,50 µg/L
3/21/2023
Styrene
SW 846 Method 8260D15030B
< 0.50 µg/L
3/21/2023
tent-Butylbenzene
SW 846 Method 8260D15030B
< 0.50 µg/L
3121 /2023
Tetrachloroethene
SW 846 Method 8260DIS030B
< 0.50 µglL
3/21/2023
Toluene
SW W Method 8260015030E
< 0.50 µg/L
3/21/2023
Trans-1,2-Dichloroethene
SW 846 Method 8200D150308
< 0.50 µg/L
3/21/2023
Trans-1,3-dichloropropene
SW 846 Method 8260D15030B
< 0.50 µg/L
3/21/2023
Trichloroethene
SW 846 Method 8260Dl5030B
< 0.50 µg1L
3121 /2023
Trichlorofluoromethane
SW 846 Method 826OD15030B
< 0.50 µg/L
3/21/2023
Vinyl chloride
SW 846 Method 826OD15030B
< 0.50 µg/L
3/21/2023
Formaldehyde
SW848 8315A
<50 µg/L
03/13/2023
Nitrate Nitrogen (Caic)
Nitrite Nitrogen
EPA 353.2, Rev 2.0. 1993
< 0.02 mg1L
03/09/2023
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev 2.0. 1993
0.04 mg/L
03/13/2023
Nitrate Nitrogen
Subtraction Method
0.04 mg/L
03/15/2023
Total Nitrogen (Caic)
Total Kjeldahl Nitrogen (TKN)
EPA3512 Rev 2 0, 1993
501 mg/L
03/15/2023
Total Nitrogen
Total Nitrogen
501 mg/L
03/20/2023
Report* 2023.04647
Page 3 of 9

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Wood - WSP USA E81 Inc
5710 Oleander Drive, Suite 110
Wilmington NC 28405
Attention:
Lab ID Sample ID:
23-11560 Site: WWMW-02
Test
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab, Fax
Method
info;a:-environmentalchemists.com
Date of Report:
Mar 27, 2023
Customer PO #:
6228232003
Customer ID:
11070019
Report #:
2023-04647
Project ID: Bakelite Acme CLRS
7011e0a-telnme — Matrix
Sampled by
3/8/2023 9:30 AM Water
Client
Results Date Analyzed
Iron
EPA 200 7, Rev. 4.4, 1994 (D.ssolved)
0.019 mg/L
03/14/2023
Manganese
EPA 200 7, Rev 4.4, 1994 (Dissolved]
0.469 mg/L
03/14/2023
Sulfate
EPA 300 0, Rev 2 1. 1993
264 mg/L
03/09/2023
Ammonia Nitrogen
EPA 3501. Rev 2 0.1993
8.8 mg/L
03/16/2023
Total Dissolved Solids (TDS)
SM 2540 C-2015
534 mg/L
03/08/2023
Total Phosphorus
SM 4500 P (F-H)-2011
< 0.04 mg/L
03/15/2023
Sulfide
SM 4500 S D-2011
<0.05 mg/L
03/13/2023
Total Organic Carbon (TOC)
SM 5310 8-2014
4.9 mg/L
03/13/2023
1, 1, 1,2-Tetrachloroethane
SW 846 Method 82BOD15030B
< 0.50 pg/L
3/21/2023
1,1,1-Trichloroethane
SW 846 Method 8260D15030B
< 0.50 pg/L
3/21/2023
1,1,2,2-Tetrachloroethane
SW 846 Method 8260015030B
< 0.50 pglL
3/21/2023
1,1,2-Trichloroethane
SW 846 Method 826OD15030B
< 0.50 pglL
3121 /2023
1,1-Dichloroethane
SW 80 Method 8260D150308
< 0.50 pglL
3/21/2023
1,1-Dichloroethene
SW 846 Method 8260015030E
< 0.50 pg/L
3/21/2023
1,1-Dichloropropene
SW 846 Method 8260D150308
< 0.50 pg/L
3/21/2023
1,2,3-Trichiorobenzene
SW 846 Method 826OD/50308
< 0.50 pg/L
3/21/2023
1,2,3-Trichloropropane
SW 646 Method 826OD15030B
< 0.50 pg/L
3/21/2023
1,2,4-Trichlorobenzene
SW 846 Method 82BOD15030B
< 0.50 pg/L
3/21/2023
1,2,4-Trimethylbenzene
SW 846 Method 8280015030E
< 0.50 pg/L
3/21/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 82601)15030B
< 0.50 pglL
3/21/2023
1,2-Dibromoethane
SW 848 Method 8260D150308
< 0.50 pg/L
3/21/2023
1,2-Dichlorobenzene
SW 848 Method 8260D1503013
< 0.50 pg/L
3/21/2023
1,2-Dichloroethane
SW 846 Method 826OD15030B
< 0.50 pglL
3/21/2023
1,2-Dichloropropane
SW 846 Method 82GOD15030B
< 0.50 pglL
3/21/2023
1,3,5-Trimethylbenzene
SW 846 Method 826OD150308
< 0.50 pglL
3/21/2023
1,3-Dichlorobenzene
SW s48 Method 028aD15030B
< 0.50 pglL
3/21/2023
Report #:. 2023-04647
Page 4 of 9

F7- Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
Ran 255-A Wilmington Highway, Jacksonville, NC 28540 r 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info; environmentalchemists.com
Wood - WSP USA E&I Inc
Date of Report: Mar 27, 2023
5710 Oleander Drive, Suite 110
Customer PO #: 6228232003
Wilmington NC 28405
Customer 10: 11070019
Attention:
Report #: 2023-04647
Project ID: Bakelite Acme CLRS
1,3-Dichloropropane
SW 846 Method 82BOD15030B
< 0.50 pg/L
3/21/2023
1,4-Dichlorobenzene
SW 846 Method 826OD160308
< 0.50 pg/L
3/21/2023
2,2-Dichloropropane
SW 846 Method 826OD150308
< 0.50 pg/L
3/21/2023
2-Chlorotoluene
SW 846 Method 826OD160308
< 0.50 pg/L
3/21/2023
2-Hexanone
SW 846 Method 82BOD15030B
< 2.50 pg/L
3/21/2023
4-Chlorotoluene
SW 846 Method 826OD150308
< 0.50 pg/L
3/21/2023
Acetone
SW 846 Method 826OD16030B
7.89 pg/L
3/21/2023
Acrolein
SW 846 Method 8260D15030B
< 5.00 pg/L
3/21/2023
Acrylonitrile
SW 840 Method 826OD15030B
< 5.00 pg/L
3/21/2023
Benzene
SW s46 Method 82BOD15030B
< 0.50 pg/L
3/21/2023
Bromobenzene
SW 846 Method 8260015030E
< 0.50 pg/L
3/21/2023
Bromochloromethane
SW 848 Method 82BOD1503DB
< 0.50 pg/L
3/21/2023
Bromodichloromethane
SW W Method BMD15030B
< 0.50 pg/L
3121 /2023
Bromoform
SW 848 Method 82BOD15030B
< 0.50 pg/L
3121 /2023
Bromomethane
SW 8" Method 8260D15030B
< 0.50 pg/L
3/21/2023
Carbon Disulfide
SW 846 Method 826DD1503DB
<0.5 pg/L
03/21 /2023
Carbon tetrachloride
SW 846 Method 82ODD15030B
< 0.50 pg/L
3/21/2023
Chlorobenzene
SW 8" Method 826DD15030B
< 0.50 pg/L
3/21/2023
Chloroethane
SW 8" Method 826OD15030B
< 0.50 pg/L
3/21/2023
Chloroform
SW 846 Method 8260D150308
< 0.50 pg/L
3/21/2023
Chloromethane
SW 846 Method 8260D150308
< 0.50 pg/L
3/21/2023
cis-1, 2-Dichloroethene
SW 846 Method 826OD15030B
< 0.50 pg/L
3/21/2023
cis- 1,3-Dich loropropene
SW 846 Method 826OD15030B
< 0.50 pg/L
3/21/2023
Dibromochloromethane
SW 846 Method 82BOD15030B
< 0.50 pg/L
3/21/2023
Dibromomethane
SW 846 Method 82SOD15030B
< 0.50 pg/L
3/21/2023
Dichlorodifluoromethane
SW 846 Method 8280DI5030B
< 0.50 pg/L
3/21/2023
Ethylbenzene
SW 846 Method 8280D15030B
< 0.50 pg1L
3/21/2023
Hexachlorobutadiene
SW 846 Method 626OD150306
< 0.50 pg/L
3121 /2023
IPE
SW 8" Method 8260D15030B
< 0.50 pg/L
3/21/2023
Isopropylbenzene
SW US Method 82ODD15030B
< 0.50 pg/L
3/21/2023
Report *: 2D23-04647
Page 5 of 9

[envirochem
ANALYTICAL & CONSULTING CHEMISTS
Wood - WSP USA B&I Inc
5710 Oleander Drive , Suite 110
Wilmington NC 28405
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.3475843 Lab i Fax
info(kenvironmenta Ichemists.com
Date of Report:
Mar 27, 2023
Customer PO #:
6228232003
Customer ID:
11070019
Report #:
2023-04647
Project ID: Bakelite Acme CLRS
M+P Xylene
SW 846 Method 82BODI5030B
< 1.00 pg/L
3/21/2023
MEK
SW 846 Method 82BOD/5030B
< 2.50 pg/L
3/21/2023
Methylene chloride
SW 846 Method 82BOD15030B
< 0.50 pg/L
3/21/2023
MIBK
SW 846 Method 826OD15030B
< 2.50 pg/L
3/21/2023
MTBE
SW 846 Method 82BOD/5030B
< 0.50 pg/L
3/21/2023
Naphthalene
SW 846 Method 826ODI5030B
< 0.50 pg1L
3/21/2023
n-Butylbenzene
SW 848 Method 8260Dr50308
< 0.50 pg/L
3/21/2023
n-Propylbenzene
SW 846 Method 82BOD/5030B
< 0.50 pg/L
3/21/2023
ortho-Xylene
SW 846 Method 828013I503013
< 0.50 pg/L
3/21/2023
p-Isopropyltoluene
SW 846 Method 82SOD15030B
< 0.50 pg/L
3/21/2023
sec -Butyl benzene
SW 846 Method 82BOD15030B
< 0.50 pg/L
3/21/2023
Styrene
SW 846 Method 82BOD/5030B
< 0.50 pg/L
3/21/2023
tert-Butylbenzene
SW 846 Method 8260DI503013
< 0.50 pg/L
3/21/2023
Tetrachloroethene
SW 846 Method 82BOD/5030B
< 0.50 pg/L
3/21/2023
Toluene
SW 846 Method 82BOD/5030B
< 0.50 pg/L
3/21/2023
Trans-1 ,2-Dichloroethene
SW 8" Method 826OD15030B
< 0.50 pg/L
3/21/2023
Trans-1,3-dichloropropene
SW 846 Method 8260131503013
< 0.50 pg/L
3/21/2023
Trichloroethene
SW 846 Method 826OD/5030s
< 0.50 pg/L
3/21/2023
Trichlorofluoromethane
SW 846 Method 82ND15030B
< 0.50 pg/L
3/21/2023
Vinyl chloride
SW 846 Method 8260Df5030B
< 0.50 pg/L
3/21/2023
Formaldehyde
SW846 8315A
<50 pg/L
03/13/2023
Nitrate Nitrogen (Cafc)
Nitrite Nitrogen
EPA 353.2. Rev 2 0. 1003
0.05 mg/L
03/09/2023
Nitrate+Nitrite-Nitrogen
EPA 353 2. Rev 2 0,1993
12.6 mg/L
03/13/2023
Nitrate Nitrogen
Subtraction Method
12.6 mg/L
03/15/2023
Total Nitrogen (Cafc)
Total Kjeldahl Nitrogen (TKN)
EPA351 2, Rev 20, 1993
10.8 mg/L
03/15/2023
Total Nitrogen
Total iv"en
23.4 mg/L
03/27/2023
Report #.: 2023.04647 Page 6 of 19

Environmental Chemists, Inc.
envirochem
ANALYTICAL & CONSULTING CHEMISTS
Wood - WSP USA E&I Inc
5710 Oleander Drive , Suite 110
Wilmington NC 28405
Attention:
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info(a environmentaichemists.com
Date of Report:
Mar 27, 2023
Customer PO #:
6228232003
Customer ID:
11070019
Report #:
2023-04647
Project ID: Bakelite Acme CLRS
Lab ID Sample ID:
23-11561 Site: WWMW-03
Test
Collect Date[Time
3/8/2023 9:45 AM
Method
Matrix Sampled by
Water Client
Results Date Analyzed
Iron
EPA 200.7, Rev 4.4, 1994 (Dissolved)
2.35 mg/L
03/14/2023
Manganese
EPA200.7. Rev 4.4. 1994 (DiwoW
0.088 mg/L
03/14/2023
Sulfate
EPA 300.0. Rev 2.1. 1993
56 mg/L
03/09/2023
Ammonia Nitrogen
EPA 350.1, Rev 2.0, 1993
120 mg/L
03/16/2023
Total Dissolved Solids (TDS)
SM 2640 C-2016
404 mg/L
03/08/2023
Total Phosphorus
SM 4500 P (F-H)-2011
< 0.04 mg/L
03/15/2023
Sulfide
SM 4500 S D-2011
0.15 mg/L
03/13/2023
Total Organic Carbon (TOC)
SM 5310 0-2014
15.8 mg/L
03/13/2023
1,1,1,2-Tetrachloroethane
SW 846 Method 8260D/5030B
< 0.50 pg/L
3/21/2023
1,1,1-Trcchloroethane
SW 846 Method 8260DI5030B
< 0.50 pg/L
3121 /2023
1, 1,2,2-Tetrach loroethane
SW 846 Method 8260015030B
< 0.50 pg/L
3/21/2023
1,1,2-Trichooroethane
SW 846 Method 8280DIS030B
< 0.50 NgIL
3/21/2023
1,1-Dichloroethane
SW 846 Method 826OD160308
< 0.50 pg/L
3/21/2023
1, 1 -Dichloroethene
SW 846 Method 6260DIS030B
< 0.50 pg/L
3/21/2023
1, 1 -Dichloropropene
SW 846 Method 826DDIS030B
< 0.50 pg/L
3/21/2023
1,2,3-Trichlorobenzene
SW 846 Method 8260DIS0308
< 0.50 pg/L
3/21/2023
1,2,3-Trichloropropane
SW 846 Method 826OD160308
< 0.50 pg/L
3/21/2023
1,2,4 Trichlorobenzene
SW 848 Method 826OD160308
< 0.50 pg/L
3/21/2023
1,2,4-Trimethylbenzene
SW 846 Method 826OD15030B
< 0.50 pg/L
31z1/2023
1,2-Dibromo-3-Chloropropane
SW 846 Method 826OD15030B
< 0.50 pg/L
3/21/2023
1,2-Dibromoethane
SW 846 Method 8260D15030B
< 0.50 pg/L
3/21/2023
1,2-Dichlorobenzene
SW 846 Method 8260D15030B
< 0.50 pg/L
3/21/2023
1,2-Dichloroethane
SW B46 Method 828OD15030B
< 0.50 pg/L
3/21/2023
1,2-Dichloropropane
SW 646 Method 8260D15030B
< 0.50 pg/L
3/21/2023
1,3,5-Trimethylbenzene
SW 846 Method SMD16030B
< 0.50 pg/L
3/2112023
1,3-Dichlorobenzene
SW 846 Method 8260DIS03GB
< 0.50 pg/L
3/21/2023
Report #*.: 2023-04647 Page 7 of 9

77 Environmental Chemists, Inc.
1 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
'' 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infora:environmentalchemists.com
Wood - WSP USA E&I Inc
Date of Report: Mar 27, 2023
5710 Oleander Drive, Suite 110
Customer PO #: 6228232003
Wilmington NC 28405
Customer ID: 11070019
Attention:
Report #: 2023-04647
Project ID: Bakelite Acme CLRS
1,3-Dichloropropane
SW a46 Method 8260D 5030E
< 0.50 pg/L
3121 /2023
1,4-Dichlorobenzene
SW 846 Method 82800 5030E
< 0.50 pg/L
3/21/2023
2,2-Dichloropropane
SW 846 Method 8280D 5030B
< 0.50 pg/L
3/21/2023
2-Chlorotoluene
SW 846 Method 8260D 5030B
< 0.50 pg/L
3/21/2023
2-Hexanone
SW 846 Method 82BOD15030B
< 2.50 pg/L
3/21/2023
4-Chlorotoluene
SW 846 Method 826OD15030B
< 0.50 pg/L
3/21/2023
Acetone
SW 846 Method 8260D.5030B
10.3 pg/L
3/21/2023
Acrolein
SW 846 Method 8280D:5030B
< 5.00 pg/L
3121 /2023
Acrylonitrile
SW 846 Method 8260D5030B
< 5.00 pg/L
3/21/2023
Benzene
SW 8" Method 8260D5030B
< 0.50 pg/L
3/21/2023
Bromobenzene
SW "6 Method 8260D5030B
< 0.50 pg/L
3/21/2023
Bromochloromethane
SW 8" Method 8280D5030B
< 0.50 pg/L
3/21/2023
Bromodichloromethane
SW 846 Method 8260D,5030B
< 0.50 pg/L
3/21/2023
Bromoform
SW a46 Method 82800,50308
< 0.50 pg/L
3/21/2023
Bromomethane
SW 846 Method 826OD15030B
< 0.50 pg/L
3/21/2023
Carbon Disulfide
SW $46 Method 826OD15030B
<0.5 pg/L
03/21/2023
Carbon tetrachloride
SW 8" Method 8260D+50308
< 0.50 pg/L
3/21/2023
Chlorobenzene
SW 846 Method 8260Dr5030B
< 0.50 pg/L
3/21/2023
Chloroethane
SW 846 Method 8260Dr5030B
< 0.50 pg/L
3/21/2023
Chloroform
SW 846 Method 8260D. 5030E
< 0.50 pg/L
3/21/2023
Chloromethane
SW 846 Method 8260D,15030B
< 0.50 pg/L
3/21/2023
cis-1,2-Dichloroethene
SW 846 Method 82800.-5030B
< 0.50 pg/L
3/21/2023
cis-1,3-Dichloropropene
SW 846 Method 8280D5030B
< 0.50 pg/L
3/21/2023
Dibromochloromethane
SW 848 Method 8260D5030B
< 0.50 pg/L
3/21/2023
Dibromomethane
SW 848 Method 826OD160308
< 0.50 pg/L
3/21/2023
Dichlorodifluoromethane
SW 848 Method 8260D150308
< 0.50 pg/L
3/21/2023
Ethylbenzene
SW 846 Method 828OD150308
0.74 pg/L
3/21/2023
Hexachlorobutadiene
SW 846 Method 8260DI60308
< 0.50 pg/L
3/21/2023
I PE
SW 846 Method 826OD150308
< 0.50 pg/L
3/21/2023
lsopropylbenzene
SW 846Method 8280D15030B
< 0.50 pg/L
3/21/2023
Report #.. 2023-04647
Page 8 of 9

F"00-- 77 Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info[u;environmentalchemists.com
Wood - WSP USA E&I Inc
Date of Report: Mar 27, 2023
5710 Oleander Drive, Suite 110
Customer PO #: 6228232003
Wilmington NC 28405
Customer ID: 11070019
Attention.
Report #: 2023-04647
Project ID: Bakelite Acme CLRS
M+P Xylene
SW 846 Method 0260DI50308
< 1.00 pg/L
3/21/2023
MEK
SW 846 Method 8260DIS030B
< 2,50 pg/L
3/21/2023
Methylene chloride
SW 846 Method 8260D1503013
< 0.50 pg1L
3/21/2023
MIBK
SW 846 Method 826DD/50306
< 2.50 pg/L
3/21/2023
MTBE
SW 846 Method 826OD15030B
< 0.50 pg/L
3/21/2023
Naphthalene
SW 846 Method 826OD15030B
< 0.50 pg/L
3121 /2023
n-Butylbenzene
SW 846 Method 8260D15030B
< 0.50 pg/L
3/21/2023
n-Propylbenzene
SW 846 Method BMD15030B
< 0.50 pg/L
3/21/2023
ortho-Xylene
SW 846 Method 8280DI5030B
< 0.50 pg/L
3/21/2023
p-Isopropyltoluene
SW 80 Method 826OD1503DB
< 0.50 pg/L
3/21/2023
sec-Butylbenzene
SW 846 Method 82BOD1503GB
< 0.50 pg/L
3/21/2023
Styrene
SW 846 Method 8260DI50308
< 0.50 pg/L
3/21/2023
tert-Butylbenzene
SW 846 Method 8260D150308
< 0.50 pg/L
3/21/2023
Tetrachloroethene
SW 846 Method 8260DIS0308
< 0.50 pg/L
3/21/2023
Toluene
SW 846 Method 826OD150308
< 0.50 pg/L
3/21/2023
Trans-1 ,2-Dickloroethene
SW 846 Method a2600150306
< 0.50 pg/L
3/21/2023
Trans-1,3-dichloropropene
SW 846 Method 8260DIS030B
< 0.50 pg/L
3/21/2023
Tnchloroethene
SW 846 Method 826OD15030B
< 0.50 pg/L
3/21/2023
Tnchlorofluoromethane
SW 846 Method 826OD15030B
< 0.50 pg/L
3/21/2023
Vinyl chloride
SW 846 Method 8260DIS030B
< 0.50 pg/L
3/21/2023
Formaldehyde
SW846 8315A
<50 pg/L
03/13/2023
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2, Rev 2.0, 1993 < 0.02 mg/L 03/09/2023
Nitrate+Nitrite-Nitrogen EPA 353.2, Rev 2.0,1993 0.10 mg/L 03/13/2023
Nitrate Nitrogen Subtraction Method 0.10 mg/L 03/27/2023
Total Nitrogen (Cale)
Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0, 1993 131 mg/L 03/15/2023
Total Nitrogen Total Nitrogen 131 mg/L 03/20/2023
Comment: �}
Reviewed by:
Report #:: 2023-04647 Page 9 of 9

Analytical Environmental Services, Inc
Date: 17-Mar-23
Client:
Environmental Chemists, Inc.
Client Sample ID:
23-11559
Project Name:
23-11559-11561
Collection Date:
3 8 2023 9:20:00 AM
Lab ID:
2303D10-001
Matrix:
Aqueous
Reporting Dilution
Analyses Result Limit Qual Units Batch[D Factor Date Anal Analyst
Formaldehyde b% SW8315A
FimnaldelivdE
Oug"n: 4lue etceedn utatmtnn] conrnnta:utt let cl
HRL Belau rcpomng luau
I I I lolding tines for prcparaaon or anal•sis acceded
1 Ana1)4nli NLLACcertnled
B Anahie doccicd in the associated inelhod blank
Greater than Result taluc
BRL S:l -.111 352519 1 03 13 2023 11 12 DS
E h ttntaled italuc abot a gtwnutation mngo
S Spike Recocen oulside luuiu due 10 11121FIX
Nary Sce case nartautc
F Anal+zed in the lab which is a deviation hone the method
Less than Resuh value
J Esunuted chic dctcocd b0o%% Rcpooing Limit
?age 4 of 10
► 1 559

Analytical Environmental Services, Inc
Date: 17-Mar-23
Client:
Environmental Chemists, Inc.
Client Sample ID:
23-11560
Project Name:
23-11559-11561
Collection Date:
3'8.2023 9:30:00AM
Lab ID:
2303D10-002
Matrix:
Aqueous
Analyses Result Reporting Qual Units BatchlD Dilution DateAnahzed Anal)st
Limit Factor
Formaldehyde by SW8315A
Formaldehyde
Qrallirwrs: %slur exceeds tnatmtum eontanagant le+cl
BRL Belo. rnponing limit
I I I loldinv owes for preparation or anal} sis cu ceded
X Anal% to not NUAC rentticd
B Axialtw deteetad in the associaled method blank
Grcala than Result %attic
I�RI. ,:i - 1 352519 1 03 13 2023 11 34 DS
L hstmtaled lutue abotc quantilanon rangel
S Spike Reca%en outside horns dux to rnalnx
\arc See case narratne
F Anahzed in the tab ahich is a dcx iauon from the nirthod
Les> than Result whic
J hslumatcd taluc dcteetad Mloa Repamng Limit
l 1 h I,,(-)
Page 5 of 10

Analytical Environmental Services, Inc
Date: 17-Mar-23
Client:
Environmental Chemists, Inc-
Client Sample 1D:
23-11561
Project Name:
23-11559-11561
Collection Date:
3 8 2023 9A5:00 AM
Lab ID:
2303D10-003
Matrix:
Aqueous
Reporting Dilution
Analyses Result Qual Units BatchlD Date Analyzed Analyst
Limit Factor
Formaldeh3de by S"'8315A
Formaldehy& BRL I 352519 1 03'13`202311.45 DS
Qualifiers: %clue ctccod> masttnom wntarntnant level E Esun:atad I valuc abuse quantnauon range;
8RL Betuu reporting limit S Spakc Recuven outride lints due to mains
I lidding trines for preparation or anal}su es.ecded .\arr Sec case nanatn c
C Anal}w nut \'hL W serniled E Anah zed in the lab %shach is a des iauon Frain the method
B anahtr dcteeteJ m the .unaaatsd methnJ blank - Less than Re,uh s alue
Greater than R;sult sale. J Esunaated value detected betou Reporting Limn
Page 6 of 10

Environmental Chemists, Inc.
envirochem
ANALYTICAL & CONSULTING CHEMISTS
LCS
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab - 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 - 252.473.3702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
info l,ctie nvironmentalchemists.com
Wood QC - 2023-4647
Parameter
True Value
m lL
Result
M91L
% Recovery
Limits
%
Ammonia
5.0
90-110
Iron
2.00
1.99
100
90-110
Manganese
1.00
1.00
100
90-110
NO2
0.60
0.65
108
90-110
NO3 & NO2
1.00
0.95
95
90-110
Sulfate
50.0
48.0
96
90-110
TDS
600
606
101
90-110
Sulfide
0.50
0.47
94
90-I10
TO C
10.0
10.3
103
TKN
4.0
4.2
105
90-110
TP
1.60
1.52
95
90-1 10
MS/MSD
Parameter
True Value
m . L
Recovery
m iL
00
Recovery
°o
Difference
Limits %
Recover
Limits %
Difference
Ammonia
4.0
80-120
<20
Iron
1.00
0.9911.00
99,1100
1
80-120
5 20
Manganese
0.100
0,10310,103
1031I 03
0
80-120
< 20
NO2
0.50
0.5310.53
106l106
0
80-120
!S20
NO3 & NO2
0.50
0.46f'0.48
92/96
4
80-120
:520
Sulfate
10.0
9.6.19.6
96'96
0
80-120
<_ 20
TDS
NIA
NIA
NA
N A
80-120
<20
Sulfide
0.50
0.39-0.42
78*..,84
6
70-130
530
TOC
10.0
9.6
96
N A
80-120
<20
TKN
5.0
4.7 4.5
94M
4
80-120
<20
TP
2.00
2.00 1.90
100/95
5
80-120
< 20
* Batch accepted based on all other passing QC's

DUPLICATE SAMPLES
Parameter
Results
mg L
% Difference
Limits %
Ammonia
N. A
NIA
N/A
< 10
Iron
N/A
NIA
N/A
NIA
Manganese
N/A
NIA
N;'A
NIA
NO2
MA
N)A
N!A
< 10
NO3 & NO2
NIA
WA
NIA
520
Sulfate
48.0
48.0
0
< 10
TDS
977
977
0
510
Sulfide
NIA
N A
NIA
NIA
TOC
<0.5
°.0.5
0
<_10
TKN
NIA
N, A
N!A
510
TP
N A
NA
N/A
<10
BLANK
Parameter
Results
mg1L
Limit
mgiL
Ammonia
<0.1
0.1
Iron
<0.005
0.005
Manganese
<0.005
0.005
NO2
<o.01
0.01
NO3 & NO2
<0.01
0.01
Sulfate
<2.5
2.5
TDS
<2.5
2.5
Sulfide
<0.025
0.025
TOC
<0.25
0.25
TKN
<0.25
0.25
TP
<0.02
0.02

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
Date. � 8
6602 Windr-nill Way
Wilmington, NC 28405
910 392.0223
Cl en,:
��
Report Number: _ 2023- Q -Y(67-7
Receipt of sample:
ECHEM Pickup ❑ 0.ent Del very UPS ❑ FedEx ❑ Omer ❑
❑
YES
❑
NO
Z
N/A
1./ere custody seals present on the cooler?
❑
YES
❑
NO
N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt C Corrected temperature upon receipt =C
How temperatu-e taken:
❑ Temperature Blank � Against Bottles
IR Gun ID:
Thomas Traceable S/N 210886869 lR Gun Correction Factor -C: 0.0
YES
❑
NO
3
if temperature of cooler exceeded 6-C, vas Project Mgr./QA notified?
YES
❑
NO
4.
Were proper custod/ procedure; (rel,nqu shed/received) follov ed?
YES
❑
NO
5.
Were sample .D s listed on the COC?
`(ES
❑
NO
6
Were samples ID's listed on sample conta' iers?
YES
❑
NO
7
Were co',ection date and time listed on the COC?
YES
❑
NO
8
'.ere tests to be performed listed on the COC?
YrS
❑
NO
9
D•d samp!Es a-r:vE in proper conta:-iers fo- each test?
YES
❑
10.
samples arr'•:e i-I goad cond tio-1 fo• each Cest?
'' t5
❑
rrN^O
F•�O
lD,ld
adeq Ja.� ;�-np'e vo!: -ne a la lab'e-V
f ES
❑
tJ0
12,
VIer samples rGC� pro3--r n•o'd n"' t nie 0- re ?
�d ;trl i 0 f �q�es!ed t � s?
vES
❑
NO
13.
Mere ac d p-eserved sanzo'es rece ed a: a pH of <2? *
❑
YES
❑
�`:0
1='.
V" _ cya:,:d sa-rsa'_. r4ce. cd a: a p-1 >12'
YES
❑
NO
1S.
s a's7l�jT? 5?"Tip`e"s received a! a p-I >9?
YES
❑
I'v'O
1�
+V,'ere
y'1��r� i�.�JII `. `r+�n=1i�� rC"[ei`.�d a. C �fl�.^1''"i� re ]•�.1 or <1 ] Fii/i_�
=5
❑
P.'�
17.
t`. ""� S:,";dslC; u_ r___ = res daa' o <0 S n+/
❑
YES
❑
�r�
I 1
k`: ti'c O`t-, 0,— � : ip'�s +, .: i I'1 . _ d
._.. 7 i i... ..._.
Sample Preservation; t ,'�s."cz^
C' :e - = u = .r` :� C T M..
COMMENTS:
D-3C QA 002 R_a 1

- 1�3
ENVIRONMENTAL CHEMISTS, INC 6602Wiin9 011Way Wilmington,
FAX C284 5
OFFICEAnalytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: h PROJECT NAME: ; + �►,� REPORT NO: Z 3
ADDRESS: S D f IJr [ r SITE: PO NO: ., 2Z°�� { jj a3 �' "}XXx,
I I C F? REPORT TO: PHONEIFAX:�3J+
f
Sample Identification
J_
Transfer
COPY TO:
I email:
.r,. r noo LaS P, haw—
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Collection
d
d
d
PRESERVATION
a
- (7
c
C J
O
a W
m
o
O
E
a
t E
o
Z
J l
p
0
0
u�a
ANALYSIS REQUESTED
Date
Time
Temp.
rn
U
V
U
a.
Z
Z
T
f 2
=
z
�_
p
LLr
.
1.
�J -
--P;-1
11:5,CA
1�
]
milli
0 IN ---
IN
Date/Time Received By: Date/Time
2. 04
Temperature when Received °C: Accepted- Rejected: Resample Requested:
Delivered By: Received By: T Date: Tire:
Comments: — TURNAROUND:
�Zg Z 3 XD 3 , 4*+ ,M! , k2-3 , 573 OV�

- ENVIRONMENTAL 602 Windmill Way Wilmington, NC 28405
CHEMISTS, INC� N C OFFICE: 910-392-0223 FAX 91 a-392-4424
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DL5 CERTIFICATION # 37729 [e-mail]
✓1 COLLECTION AND C IN OF CUSTODY
Client: Si PROJECT NAME: REPORT NO: 3ADDRESS: $ 10 o(2 i SITE; PO NO: -�
L �114
N Z I REPORT TO: PHONE/FAX: )0 G S
COPY TO: email: bels•, . nxerw Avas 4. C &*k—
Sampled By: SAMPLE TYPE I = I fl -
Sample Identification
�
mWrn^ M_
I
Collection
Date
Time
Temp
n uent, E - Effluent, vv = Weil, ST = Stream, SO = Soil, SL = Sludge, Other:
CL
PRESERVATION
IT
a
0
9 w
G
°
c a°
r E
02
o
m 2
3z
Z
0 a
0°
w ANALYSIS REQUESTED
N
�°
�`"
Q
ZI2
=
z F j
o
� 11111��
�ryIg,1111
Transfer Relinquished By: Date/Time Received By: DatelTime
�.
2. :
Temperature when Received °C: Accepted: Rejected: Resample Requested:
Delivered By: Received By: Date: Time:
Comments: G
TURNAROUND:

Windml Way
• - ENVIRONMENTAL CHEMISTS, INC OFFICE: 910i392-0223'FAX9t1Q392-44245
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY ?
Client: PROJECT NAME: 4 , (h4, Lf j REPORT NO: J — O W
ADDRESS: ' d G4 W SITE: L W-A, PO NO: 4,71aZ
1�. REPORT TO: PHONE/FAX.-
COPY TO: email: r, . hA
Sampled By: SAMPLE TYPE: I = Influent, E Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Collection a N PRESERVATION
H w m 06 (D c a W G
Sample Identification a s 9 0 0 0� � m M z o o p � o � ,mu ANALYSIS REQUESTED
w
v a v E a g z Z = y = z
Date Time Tam
VY� � I C P
1 � P
VO
c
14
Transfer Relinquished By: Date/Time Received By: Daterrime
1. --— ��= a 74 �
2. 3
Temperature when Received °C: Accepted: _ _Rejected: Resample Requested:
Delivered By: Received By:_. Date: Time:
Comments:
- TURNAROUND:

Environmental Chemists, Inc.
sM'
ANALYTICAL & CONSULTING CHEMISTS
Wood - WSP USA E&I Inc
5710 Oleander Drive, Suite 110
Wilmington NC 28405
Attention:
6602 Windmill Way, Wilmington, NC 28405 + 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Nov 15, 2022
Customer PO #:
Customer ID: 11070019
Report #: 2022-21778
Project ID: Bakelite Acme CLRS
Lab ID Sample ID:
22-53379 Site: WWMW-01
Test
Collect Date/Time
11/2/2022 9:30 AM
Method
Matrix Sampled by
Water Client
Results Date Analyzed
Iron
EPA200.7, Rev. 4.4, 1994 (Dissolved)
0.648 mg/L
11/08/2022
Manganese
EPA 200.7, Rev. 4.4,1994 (Dissolved)
0.186 mg/L
11/08/2022
Sulfate
EPA 300.0, Rev. 2.1, 1993
730 mg/L
11/07/2022
Ammonia Nitrogen
EPA 350.1, Rev. 2.0,1993
540 mg/L
11/04/2022
Total Dissolved Solids (TDS)
SM 2540 C-2015
744 mg/L
11/03/2022
Total Phosphorus
SM 4500 P (F-H)-2011
2.46 mg/L
11 /09/2022
Sulfide
SM 4500 S D-2011
12.4 mg/L
11/07/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
38.1 mg/L
11/02/2022
1, 1, 1,2-Tetrachloroethane
SW 846 Method 826013/50308
<0.5 pg/L
11/08/2022
1, 1, 1 -Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,1,2-Trichloroethane
SW 846 Method 8260D/50306
<0.5 pg/L
11/08/2022
1, 1 -Dichloroethane
SW 846 Method 8260D/50306
<0.5 pg/L
11/08/2022
1,1-Dichloroethene
SW 846 Method 8260D/503013
<0.5 pg/L
11/08/2022
1,1-Dichloropropene
SW 846 Method 8260D/50306
<0.5 pg/L
11/08/2022
1,2,3-Trichlorobenzene
SW 846 Method 826013/503013
<0.5 pg/L
11/08/2022
1,2,3-Trichloropropane
SW 846 Method 8260D/503013
<0.5 pg/L
11/08/2022
1,2,4-Trichlorobenzene
SW 846 Method 8260D/50306
0.62 pg/L
11/08/2022
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2-Dibromoethane
SW 846 Method 8260D/50306
<0.5 pg/L
11/08/2022
1,2-Dichlorobenzene
SW 846 Method 8260D/503013
<0.5 pg/L
11/08/2022
1,2-Dichloroethane
SW 846 Method 8260D/50306
<0.5 pg/L
11/08/2022
1,2-Dichloropropane
SW 846 Method 826013/503013
<0.5 pg/L
11/08/2022
1,3,5-Trimethylbenzene
SW 846 Method 8260D/503013
<0.5 pg/L
11/08/2022
1,3-Dichlorobenzene
SW 846 Method 8260D/50306
0.67 pg/L
11/08/2022
Report #.: 2022-21778 Page 1 of 9

SM
ANALYTICAL & CONSULTING CHEMISTS
row"'W7 q1
Wood - WSP USA E&I Inc
5710 Oleander Drive, Suite 110
Wilmington NC 28405
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Nov 15, 2022
Customer PO #:
Customer ID: 11070019
Report #: 2022-21778
Project ID: Bakelite Acme CLRS
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Chloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
cis- 1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
cis- 1,3-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Dibromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Dibromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Dichlorodifluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Ethylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
11/08/2022
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Isopropylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
11/08/2022
Methylene chloride
SW 846 Method 8260D/50308
<0.5 pg/L
11/08/2022
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
n-Butylbenzene
SW 846 Method 8260D/5030B
0.98 pg/L
11/08/2022
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Report #:: 2022-21778
Page 2 of 9

71 Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
SM
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS infoCenvironmentalchemists.com
Wood - WSP USA E&I Inc
5710 Oleander Drive , Suite 110
Wilmington NC 28405
Attention:
Date of Report: Nov 15, 2022
Customer PO #:
Customer ID: 11070019
Report #: 2022-21778
Project ID: Bakelite Acme CLRS
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
sec -Butyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Styrene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
tert-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Tetrachloroethene
SW 846 Method 826013/503013
<0.5 pg/L
11/08/2022
Toluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Trans-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Trans- 1,3-dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Trichloroethene
SW 846 Method 826013/50306
<0.5 pg/L
11/08/2022
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Vinyl chloride
SW 846 Method 8260D15030B
<0.5 pg/L
11/08/2022
Formaldehyde
SW846 8315A
110 pg/L
11 /04/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev 2 0, 1993
0.06 mg/L
11/03/2022
Nitrate+Nitrite-Nitrogen
EPA353.2, Rev. 2.0,1993
< 0.02 mg/L
11/03/2022
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
11/15/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev. 2.0,1993
579 mg/L
11/09/2022
Total Nitrogen
Total Nitrogen
579 mg/L
11/15/2022
Report #:: 2022-21778 Page 3 of 9

ro""W' -- -:"q"l
;SM
ANALYTICAL & CONSULTING CHEMISTS
Wood - WSP USA E&I Inc
5710 Oleander Drive, Suite 110
Wilmington NC 28405
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Nov 15, 2022
Customer PO #:
Customer ID: 11070019
Report #: 2022-21778
Project ID: Bakelite Acme CLRS
Lab ID Sample ID:
22-53382 Site: WWMW-02
Test
Collect Date/Time
11/2/2022 9:45 AM
Method
Matrix Sampled by
Water Client
Results Date Analyzed
Iron
EPA 200.7, Rev. 4.4, 1994 (Dissolved)
<0.06 mg/L
11/08/2022
Manganese
EPA 200.7, Rev. 4.4, 1994 (Dissolved)
0.839 mg/L
11/08/2022
Sulfate
EPA 300.0, Rev. 2.1, 1993
210 mg/L
11/07/2022
Ammonia Nitrogen
EPA 350.1, Rev. 2.0,1993
45.6 mg/L
11/04/2022
Total Dissolved Solids (TDS)
SM 2540 C-2015
713 mg/L
11/03/2022
Total Phosphorus
SM 4500 P (F-H)-2011
0.12 mg/L
11/09/2022
Sulfide
SM 4500 S D-2011
<0.05 mg/L
11/07/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
6.8 mg/L
11/02/2022
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D/503013
<0.5 pg/L
11/08/2022
1, 1, 1 -Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,1,2-Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,1-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1, 1 -Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,1-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2,3-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2,3-Trichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2,4-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,3,5-Trimethylbenzene
SW 846 Method 8260D/503013
<0.5 pg/L
11/08/2022
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Report #:: 2022-21778 Page 4 of 9

envirochem
SM�
ANALYTICAL & CONSULTING CHEMISTS
F0057- q1
Wood - WSP USA E&I Inc
5710 Oleander Drive, Suite 110
Wilmington NC 28405
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 e 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Nov 15, 2022
Customer PO #:
Customer ID: 11070019
Report #: 2022-21778
Project ID: Bakelite Acme CLRS
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,4-Dichlorobenzene
SW 846 Method 826013/50308
<0.5 pg/L
11/08/2022
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Chloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
cis-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
cis- 1,3-Dichloropropene
SW 846 Method 82600/5030B
<0.5 pg/L
11/08/2022
Dibromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Dibromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Dichlorodifluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Ethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Isopropylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
11/08/2022
Methylene chloride
SW 846 Method 8260D15030B
<0.5 pg/L
11/08/2022
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
ortho-Xylene
SW 846 Method 8260D/50308
<0.5 pg/L
11/08/2022
Report #:: 2022-21778
Page 5 of 9

F- 7`1
aM
ANALYTICAL & CONSULTING CHEMISTS
Wood - WSP USA E&I Inc
5710 Oleander Drive , Suite 110
Wilmington NC 28405
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Nov 15, 2022
Customer PO #:
Customer ID: 11070019
Report #: 2022-21778
Project ID: Bakelite Acme CLRS
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
sec-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Styrene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
tert-B utyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Tetrachloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Toluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Trans-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Trans- 1,3-dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Formaldehyde
SW846 8315A
<50 pg/L
11 /04/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.23 mg/L
11/03/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0,1993
55.8 mg/L
11/03/2022
Nitrate Nitrogen
Subtraction Method
55.6mg/L
11/15/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev. 2.0,1993
19.2 mg/L
11/09/2022
Total Nitrogen
Total Nitrogen
75.0 mg/L
11/15/2022
Report #:: 2022-21778 Page 6 of 9

41 Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
s.M 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Wood - WSP USA E&I Inc
5710 Oleander Drive, Suite 110
Wilmington NC 28405
Attention:
Date of Report: Nov 15, 2022
Customer PO #:
Customer ID: 11070019
Report #: 2022-21778
Project ID: Bakelite Acme CLRS
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-53383 Site: WWMW-03
11/2/2022 10:00 AM Water Client
Test
Method
Results Date Analyzed
Iron
EPA200.7, Rev.4.4, 1994 (Dissolved)
0.108 mg/L
11/08/2022
Manganese
EPA 200.7, Rev. 4.4, 1994 (Dissolved)
0.079 mg/L
11/08/2022
Sulfate
EPA300.0, Rev.2.1, 1993
38 mg/L
11/07/2022
Ammonia Nitrogen
EPA 350.1, Rev. 2.0, 1993
160 mg/L
11/04/2022
Total Dissolved Solids (TDS)
SM 2540 C-2015
400 mg/L
11/03/2022
Total Phosphorus
SM 4500 P (F-H)-2011
< 0.04 mg/L
11/11/2022
Sulfide
SM 4500 S D-2011
<0.05 mg/L
11/07/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
19.9 mg/L
11/02/2022
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/08/2022
1, 1, 1 -Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,1,2-Trichloroethane
SW 846 Method 8260D/503013
<0.5 pg/L
11/08/2022
1,1-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1, 1 -Dichloroethene
SW 846 Method 8260D/503013
<0.5 pg/L
11/08/2022
1,1-Dichloropropene
SW 846 Method 8260D/50306
<0.5 pg/L
11/08/2022
1,2,3-Trichlorobenzene
SW 846 Method 8260D/503013
<0.5 pg/L
11/08/2022
1,2,3-Trichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2,4-Trichlorobenzene
SW 846 Method 8260D/503013
<0.5 pg/L
11/08/2022
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/503013
<0.5 pg/L
11/08/2022
1,2-Dibromoethane
SW 846 Method 8260D/503013
<0.5 pg/L
11/08/2022
1,2-Dichlorobenzene
SW 846 Method 8260D/50306
<0.5 pg/L
11/08/2022
1,2-Dichloroethane
SW 846 Method 8260D/503013
<0.5 pg/L
11/08/2022
1,2-Dichloropropane
SW 846 Method 8260D/503013
<0.5 pg/L
11/08/2022
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Report #:: 2022-21778 Page 7 of 9

Environmental Chemists, Inc.
GSM
ANALYTICAL & CONSULTING CHEMISTS
Wood - WSP USA E&I Inc
5710 Oleander Drive, Suite 110
Wilmington NC 28405
Attention:
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Nov 15, 2022
Customer PO #:
Customer ID: 11070019
Report #: 2022-21778
Project ID: Bakelite Acme CLRS
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Chloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
cis- 1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
cis- 1,3-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Dibromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Dibromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Dichlorodifluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Ethylbenzene
SW 846 Method 8260D/5030B
2.30 pg/L
11/08/2022
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 Ng/L
11/08/2022
lsopropylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
M+P Xylene
SW 846 Method 8260D150308
<1.0 pg/L
11/08/2022
Methylene chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
n-Butylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/08/2022
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Report #:: 2022-21778
Page 8 of 9

SM'
ANALYTICAL & CONSULTING CHEMISTS
Wood - WSP USA E&I Inc
5710 Oleander Drive , Suite 110
Wilmington NC 28405
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Nov 15, 2022
Customer PO #:
Customer ID: 11070019
Report #: 2022-21778
Project ID: Bakelite Acme CLRS
p-Isopropyltoluene
SW 846 Method 8260D/5030B
21.2 pg/L
11/08/2022
sec -Butyl benzene
SW 846 Method 826013/503013
<0.5 pg/L
11/08/2022
Styrene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
tert-B utyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Tetrachloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Toluene
SW 846 Method 8260D/5030B
1.52 pg/L
11/08/2022
Trans- 1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Trans-1,3-dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Formaldehyde
SW846 8315A
<50 pg/L
11 /04/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353 2, Rev. 2.0, 1993
0.02 mg/L
11/03/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2,Rev- 2.0,1993
0.14mg/L
11/03/2022
Nitrate Nitrogen
Subtraction Method
0.12 mg/L
11/15/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev, 2.0,1993
148 mg/L
11/09/2022
Total Nitrogen
Total Nitrogen
148 mg/L
11/15/2022
Comment:
7C
Z::�'
Reviewed by:
Report #:: 2022-21778 Page 9 of 9

LABORATORY CONTROL SAMPLE #1
Report#2022-21778 Page 1 of 3
Spike Compounds
p p
Method
Blank
Result
Spike
Added
Blank Spike
QC Limits
Mandator
(Mandatory)
°o Recovery Range
Result
Recovery
Dichlorodifluoromethane
<0.5
10
11.34
113
80-120
Chloromethane
<0.5
10
10.66
107
80-120
Vinyl chloride
<0.5
10
11.7
117
80-120
Bromomethane
<0.5
10
12.14
121
80-120
Chloroethane
<0.5
10
11.58
116
80-120
Trichlorofluoromethane
<0.5
10
10.98
110
80-120
1, 1 -Dichloroethene
<0.5
10
10.61
106
80-120
Methylene chloride
<0.5
10
10.51
105
80-120
trans-1,2-Dichloroethene
<0.5
10
10.99
110
80-120
1, 1 -Dichloroethane
<0.5
10
10.71
107
80-120
2,2-Dichloropropane
<0.5
10
10.48
105
80-120
cis-1,2-Dichloroethene
<0.5
10
10.83
108
80-120
Bromochloromethane
<0.5
10
10.85
109
80-120
Chloroform
<0.5
10
10.74
107
80-120
1, 1, 1 -Trichloroethane
<0.5
10
10.75
108
80-120
Carbon tetrachloride
<0.5
10
10.71
107
80-120
1, 1 -Dichloropropene
<0.5
10
10.7
107
80-120
Benzene
<0.5
10
10.83
108
80-120
1,2-Dichloroethane
<0.5
10
10.66
107
80-120
Trichloroethene
<0.5
10
10.78
108
80-120
1,2-Dichloropropane
<0.5
10
10.9
109
80-120
Dibromomethane
<0.5
10
10 81
108
80-120

LABORATORY CONTROL SAMPLE #1
Report#2022-21778 Page 2 of 3
Spike Compounds
p p
Method
Blank
Result
Spike
Added
Blank Spike
QC Limits
Mandator
(Mandatory)
Recovery Range
Result
Recovery
Bromodichloromethane
<0.5
10
10.75
108
80-120
cis-1,3-Dichloropropene
<0.5
10
10.5
105
80-120
Toluene
<0.5
10
10.86
109
80-120
trans-1,3-Dichloropropene
<0.5
10
10.52
105
80-120
1,1,2-Trichloroethane
<0.5
10
10.91
109
80-120
Tetrachloroethene
<0.5
10
10.8
108
80-120
1,3-Dichloropropene
<0.5
10
10.81
108
80-120
Dibromochloromethane
<0.5
10
10.92
109
80-120
1,2-Dibromoethane
<0.5
10
10.8
108
80-120
Chlorobenzene
<0.5
10
10.69
107
80-120
Ethyl benzene
<0.5
10
10.92
109
80-120
1, 1, 1,2-Tetrachloroethane
<0.5
10
10.92
109
80-120
M+P Xylene
<1
20
22.18
111
80-120
O-Xylene
<0.5
10
10.7
107
80-120
Styrene
<0.5
10
10.93
109
80-120
Bromoform
<0.5
10
10.79
108
80-120
Isopropylbenzene
<0.5
10
10.95
110
80-120
Bromobenzene
<0.5
10
1 1 01
110
80-120
1,1,2,2-Tetrachloroethane
<0.5
10
10.75
108
80-120
n-Propylbenzene
<0.5
10
11.01
110
80-120
1,2,3-Trichloropropane
<0.5
10
11.1
111
80-120
2-Chlorotoluene
<0.5
10
11
110
80-120
1,3,5-Trimethylbenzene
<0.5
10
11.14
111
80-120

LABORATORY CONTROL SAMPLE #1
Report42022-21778 Page 3 of 3
Spike Compounds
p p
Method
Blank
Result
Spike
Added
Blank Spike
QC Limits
Mandator
(Mandatory)
% Recovery Range
Result
Recovery
4-Chlorotoluene
<0.5
10
11.03
110
80-120
tert-Butylbenzene
<0.5
10
11.06
111
80-120
1,2,4-Trimethylbenzene
<0.5
10
10.79
108
80-120
sec-Butylbenzene
<0.5
10
1 1 11
111
80-120
1,3-Dichlorobenzene
<0.5
10
10.9
109
80-120
4-Isopropyltoluene
<0.5
10
10.95
110
80-120
1,4-Dichlorobenzene
<0.5
10
10.92
109
80-120
n-Butylbenzene
<0.5
10
11.06
111
80-120
1,2-Dichlorobenzene
<0.5
10
10.68
107
80-120
1,2-Dibromo-3-chloropropane
<0.5
10
10.64
106
80-120
1,2,4-Trichlorobenzene
<0.5
10
1111
111
80-120
Hexachlorobutadiene
<0.5
10
11.53
115
80-120
Naphthalene
<0.5
10
11.63
116
80-120
1,2,3-Trichlorobenzene
<0.5
10
1118
112
80-120

LABORATORY CONTROL SAMPLE 92
Report#2022-21778 Page 1 of 3
Spike Compounds
p p
Method
Blank
Result
Spike
Added
Blank Spike
QC Limits
Mandator
(Mandatory)
Recovery Range
Result
Recovery
Dichlorodifluoromethane
<0.5
15
17.34
116
80-120
Chloromethane
<0.5
15
15.67
104
80-120
Vinyl chloride
<0.5
15
16.98
113
80-120
Bromomethane
<0.5
15
16.35
109
80-120
Chloroethane
<0.5
15
17.81
119
80-120
Trichlorofluoromethane
<0.5
15
16.27
108
80-120
1, 1 -Dichloroethene
<0.5
15
16.04
107
80-120
Methylene chloride
<0.5
15
16.31
109
80-120
trans-1,2-Dichloroethene
<0.5
15
16.45
110
80-120
1, 1 -Dichloroethane
<0.5
15
16.2
108
80-120
2,2-Dichloropropane
<0.5
15
17.4
116
80-120
cis-1,2-Dichloroethene
<0.5
15
16.54
110
80-120
Bromochloromethane
<0.5
15
16.33
109
80-120
Chloroform
<0.5
15
16.3
109
80-120
1, 1, 1 -Trichloroethane
<0.5
15
16.08
107
80-120
Carbon tetrachloride
<0.5
15
16.04
107
80-120
1, 1 -Dichloropropene
<0.5
15
15.84
106
80-120
Benzene
<0.5
15
16.43
110
80-120
1,2-Dichloroethane
<0.5
15
16
107
80-120
Trichloroethene
<0.5
15
16.15
108
80-120
1,2-Dichloropropane
<0.5
15
16.78
112
80-120
Dibromomethane
<0.5
15
16.24
108
80-120

LABORATORY CONTROL SAMPLE #2
Report#2022-21778 Page 2 of 3
Spike Compounds
p p
Method
Blank
Result
Spike
Added
Blank Spike
QC Limits
Mandator
(Mandatory)
Recovery Range
Result
Recovery
Bromodichloromethane
<0.5
15
16.17
108
80-120
cis-1,3-Dichloropropene
<0.5
15
15.71
105
80-120
Toluene
<0.5
15
16.22
108
80-120
trans-1,3-Dichloropropene
<0.5
15
15.48
103
80-120
1,1,2-Trichloroethane
<0.5
15
16.38
109
80-120
Tetrachloroethee
<0.5
15
16.2
108
80-120
1,3-Dichloropropane
<0.5
15
16.15
108
80-120
Dibromochloromethane
<0.5
15
15.9
106
80-120
1,2-Dibromoethane
<0.5
15
15.98
107
80-120
Chlorobenzene
<0.5
15
16.38
109
80-120
Ethyl benzene
<0.5
15
16.38
109
80-120
1, 1, 1,2-Tetrachloroethane
<0.5
15
16.33
109
80-120
M+P Xylene
<1
30
33.1
110
80-120
O-Xylene
<0.5
15
16.21
108
80-120
Styrene
<0.5
15
16.57
110
80-120
Bromofonn
<0.5
15
15.61
104
80-120
Isopropylbenzene
<0.5
15
16.71
1 1 1
80-120
Bromobenzene
<0.5
15
16.23
108
80-120
1,1,2,2-Tetrachloroethane
<0.5
15
1622
108
80-120
n-Propylbenzene
<0.5
15
16.49
110
80-120
1,2,3-Trichloropropane
<0.5
15
16.29
109
80-120
2-Chlorotoluene
<0.5
15
16.59
111
80-120
1,3,5-Trimethylbenzene
<0.5
15
16.75
112
80-120

LABORATORY CONTROL SAMPLE #2
Report#2022-21778 Page 3 of 3
Spike Compounds
p p
Method
Blank
Result
Spike
Added
Blank Spike
QC Limits
Mandator
(Mandatory)
Recovery Range
Result
Recovery
4-Chlorotoluene
<0.5
15
16.53
110
80-120
tert-Butylbenzene
<0.5
15
16.64
1 1 1
80-120
1,2,4-Trimethylbenzene
<0.5
15
16.55
110
80-120
sec-Butylbenzene
<0.5
15
16.67
111
80-120
1,3-Dichlorobenzene
<0.5
15
16.35
109
80-120
4-Isopropyltoluene
<0.5
15
16.76
112
80-120
1,4-Dichlorobenzene
<0.5
15
16.29
109
80-120
n-Butylbenzene
<0.5
15
17.09
114
80-120
1,2-Dichlorobenzene
<0.5
15
15.95
106
80-120
1,2-Dibromo-3-chloropropane
<0.5
15
15.02
100
80-120
1,2,4-Trichlorobenzene
<0.5
15
15.95
106
80-120
Hexachlorobutadiene
<0.5
15
17.18
115
80-120
Naphthalene
<0.5
15
15.86
106
80-120
1,2,3-Trichlorobenzene
<0.5
15
15.78
105
80-120

Environmental Chemists, Inc.
Cnviroehem
ANALYTICAL & CONSULTING CHEMISTS
LCS
6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
Wood QC - 2022-21778
Parameter
True Value
mg'L
Result
mg1L
% Recovery
Limits
Ammonia
5.0
5.2
104
90-110
Iron
2.00
1.95
98
90-110
Manganese
1.00
1.01
101
90-110
NO2
0.60
0.62
103
90-110
NO3 & NO2
1.00
0.97
97
90-110
Sulfate
50.0
46.6
93
90-110
TDS
600
600
100
90-110
Sulfide
0.50
0.46
92
90-110
TOC
10.0
10.3
103
90-110
TKN
4.0
3.9
98
90-110
TP
1.60
1.58
99
90-110
TP
1.60
1.57
98
90-110
MS/MSD
Parameter
True Value
mg/L
Recovery
mg/L
Recovery
%
Difference
Limits %
Recovery
Limits
Difference
Ammonia
4.0
3.7/3.7
92/92
0
80-120
<20
Iron
1.00
1.03/1.00
103/100
3
80-120
<20
Manganese
0.100
0.100/0.100
100/100
0
80-120
<20
NO2
0.50
0.45/0.48
90/96
6
80-120
<20
NO3 & NO2
0.50
0.5510.56
110/112
2
80-120
<20
Sulfate
10.0
8.8/8.8
88/88
0
80-120
<20
TDS
N/A
N/A
N/A
N/A
80-120
<20
Sulfide
0.50
0.40/0.39
80/78
2
70-130
<30
TOC
10.0
10.2
102
N/A
80-120
<20
TKN
5.0
4.7/5.1
94/ 102
8
80-120
<20
TP
2.00
1.91 /2.00
96/ 100
4
80-120
<20
TP
2.00
1.99/1.99
99.5/99.5
0
80-120
520

DUPLICATE SAMPLES
Parameter
Results
mg 1L
% Difference
Limits %
Ammonia
N/A
N/A
N/A
<10
Iron
N/A
N/A
N/A
N/A
Manganese
N/A
N/A
N/A
N/A
NO2
N/A
N/A
N/A
< 10
NO3 & NO2
N/A
N/A
N/A
< 20
Sulfate
<15
<15
0
< 10
TDS
744
766
3
< 10
Sulfide
0.120
0.128
6
<10
TOC
1.4
1.3
7
<l 0
TKN
N/A
N/A
N/A
<10
TP
N/A
N/A
N/A
510
TP
N/A
N/A
N/A
<10
BLANK
Parameter
Results
mg/L
Limit
mg1L
Ammonia
<0.1
0.1
Iron
<0.005
0.005
Manganese
<0.005
0.005
NO2
<0.01
0.01
NO3 & NO2
<0.01
0.01
Sulfate
<2.5
2.5
TDS
<2.5
2.5
Sulfide
<0.025
0.025
TOC
<0.25
0.25
TKN
<0.25
0.25
TP
<0.02
0.02
TP
<0.02
0.02

Analytical Environmental Services, Inc
Date: I I-Nov-22
Client:
Environmental Chemists, Inc.
Client Sample ID:
22-53379
Project Name:
2022-21778
Collection Date:
11/2/2022 9:30:00 AM
Lab ID:
2211360-001
Matrix:
Aqueous
xeporting Dilution
Analyses Result Qual Units BatchID Date Analyzed Analyst
Limit Factor
Formaldehyde by SW8315A
Formaldehyde 110 100 ug/L 345847 l l 1/04/2022 14 49 CM
Qualifiers: • Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit
Page 3 of 9
-- ) --) ---) I `-1 --1 X

Analytical Environmental Services, Inc
Date: I I -Nov-22
Client:
Environmental Chemists, Inc.
Client Sample ID:
22-53382
Project Name:
2022-21778
Collection Date:
11/2/2022 9:45:00 AM
Lab ID:
2211360-002
Matrix:
Aqueous
xepornng Dilution
Analyses Result Qual Units BatchID Date Analyzed Analyst
Limit Factor
Formaldehyde by SW8315A
Formaldehyde
Qualifiers: • Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
BRL 50 ug/L 345847 1 11/04/202214.59 CM
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit
Page 4 of 9

Analytical Environmental Services, Inc
Date: I I-Nov-22
Client:
Environmental Chemists, Inc.
Client Sample ID:
22-53383
Project Name:
2022-21778
Collection Date:
11/2/2022 10:00:00 AM
Lab ID:
2211360-003
Matrix:
Aqueous
tceportmg Dilution
Analyses Result Qual Units BatchlD Date Analyzed Analyst
Limit Factor
Formaldehyde by SW8315A
Formaldehyde BRL 50 ug/L 345847 1 11/04/2022 15 21 CM
Qualifien: • Value exceeds maximum contaminant level
BRL Belowreportmg limit
H Holding times for preparation or analysts exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantitation range)
S Spike Recovery outside limos due to matrix
Nary See case narrative
F Analyzed in the lab which is a deviation from the method
< Less than Result value
J Estimated value detected below Reporting Limit
Page 5 of 9

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client: /,cJUu Date: // (1- 1 c'� a, Report Number: 2022- o�— J7 �k
Receipt of sample: ECHEM Pickup ❑ Client Delivery ET--
UPS ❑ FedFx ❑ Other ❑
❑ YES
❑ NO
V N/A
11. Were custody seals present on the cooler?
❑ YES
ID NO
14 N/A
12. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank M Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor 'C: 0.0
IR YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
R YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
12 YES
❑ NO
5. Were sample ID's listed on the COC?
6a YES
❑ NO
6. Were samples ID's listed on sample containers?
YES
❑ NO
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
[� YES
❑ NO
9. Did samples arrive in proper containers for each test?
tZ YES
❑ NO
10. Did samples arrive in good condition for each test?
YES 113
NO
❑ NO 112.
11. Was adequate sample volume availableT
Were samples received within proper holding time for requested tests?
IR YES
YES
❑ NO 113.
Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
YES
❑ NO
1.5. Were sulfide samples received at a pH >9?
YES
❑ NO
16. Were NH3/TI<N/Phenol received at a chlorine residual of <0.5 it y"
YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES Ill
NO 118.
Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. OA.nn? Rav 1

pr
ENVIRONMENTAL CHEMISTS INC 6602WindmillWayWilmington,NC28405
OFFICE: 910-392-0223 FAX [phone]
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
Client: ,��}} PROJECT IN,,,,A IME: i L, REPORT NO: oZv a a- 2 17 7-9-
ADDRESS: 5� C� ov) t,� SITE: Kk 4 tjL PO NO: bULZ
REPORT TO: PHONE/FAX:
COPY TO:
Sampled By: SAMPLE
CollectionCD a m
a M v—
Sample Identification o 6 `"
CL
E c o o a°
Date Time Temp Cn " "
TYPE: I = Influent,
email: h , iMZS
E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
PRESERVATION
t=_ W o
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Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
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COLLECTION AND CHAIN OF CUSTODY
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F"I�' -- Environmental Chemists, Inc.
enyirochem 6602 Windmill Way, Wilmington, NC 28405 ■ 910.392.0223 Lab • 910.392.4424 Fax
srn 710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Wood -AMEC
5710 Oleander Drive , Suite 110
Wilmington NC 28405
Attention: Ben Moore
Date of Report: Jul 29, 2022
Customer PO M
Customer ID: 11070019
Report M 2022-13097
Project ID: Hexion CLRS
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-31844 Site: WWMW-01
7/13/2022 9:45
AM Water Client
Test
Method
Results
Date Analyzed
Iron
EPA 200.7, Rev. 4.4, 1994 (Dissolved)
0.175 mg/L
07/19/2022
Manganese
EPA 200.7, Rev. 4.4,1994 (Dissolved)
0.158 mg/L
07/19/2022
Sulfate
EPA 300.0, Rev. 2.1, 1993
442 mg/L
07/20/2022
Ammonia Nitrogen
EPA 350.1, Rev. 2.0, 1993
390 mg/L
07/20/2022
Total Dissolved Solids (TDS)
SM 2540 C-2015
1130 mg/L
07/14/2022
Total Phosphorus
SM 4500 P (F-H)-2011
5.73 mg/L
07/21 /2022
Sulfide
SM 4500 S D-2011
22.5 mg/L
07/22/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
38.3 mg/L
07/13/2022
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1, 1, 1 -Trichloroethane
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,1,2-Trichloroethane
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,1-Dichloroethane
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,1-Dichloroethene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,1-Dichloropropene
SW 846 Method 8260D/50306
<1 pg/L
07/18/2022
1,2,3-Trichlorobenzene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,2,3-Trichloropropane
SW 846 Method 826013/50306
<1 pg/L
07/18/2022
1,2,4-Trichlorobenzene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,2-Dichlorobenzene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,2-Dichloroethane
SW 846 Method 8260D/50306
<1 pg/L
07/18/2022
1,2-Dichloropropane
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
Report #:: 2022-13097 Page 1 of 9

[en7—,iocohrem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Wood -AMEC
Date of Report: Jul 29, 2022
5710 Oleander Drive , Suite 110
Customer PO M
Wilmington NC 28405
Customer ID: 11070019
Attention: Ben Moore
Report #: 2022-13097
Project ID: Hexion CLRS
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
sec-Butylbenzene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
Styrene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
tert-Butylbenzene
SW 846 Method 826013/503013
<1 pg/L
07/18/2022
Tetrachloroethene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
Toluene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
Trans-1,2-Dichloroethene
SW 846 Method 8260D/6030B
<1 pg/L
07/18/2022
Trans-1,3-dichloropropene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
Trichloroethene
SW 846 Method 8260D/503013
<1 pg/L
07/18/2022
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
Vinyl chloride
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
Formaldehyde
SW846 8315A
52.0 pg/L
07/15/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.05 mg/L
07/14/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.14 mg/L
07/19/2022
Nitrate Nitrogen
Subtraction Method
0.09 mg/L
07/27/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev. 2.0, 1993
414 mg/L
07/21/2022
Total Nitrogen
Total Nitrogen
414 mg/L
07/27/2022
Report #:: 2022-13097 Page 3 of 9

[enyiroche]m]
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Wood -AMEC Date of Report: Jul 29, 2022
5710 Oleander Drive, Suite 110 Customer PO #:
Wilmington NC 28405 Customer ID: 11070019
Attention: Ben Moore Report #: 2022-13097
Project ID: Hexion CLRS
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-31845 Site: WWMW-02 7/13/2022 10:00 AM Water Client
Test Method Results Date Analyzed
Iron
EPA 200.7, Rev. 4.4, 1994 (Dissolved)
0.031 mg/L
07/19/2022
Manganese
EPA 200.7, Rev. 4.4,1994 (Dissolved)
0.342 mg/L
07/19/2022
Sulfate
EPA 300.0, Rev. 2.1, 1993
190 mg/L
07/19/2022
Ammonia Nitrogen
EPA 350.1, Rev. 2.0, 1993
78.3 mg/L
07/20/2022
Total Dissolved Solids (TDS)
SM 2540 c-2015
367 mg/L
07/14/2022
Total Phosphorus
SM 4500 P (F-H)-2011
1.40 mg/L
07/21 /2022
Sulfide
SM 4500 S D-2011
<0.05 mg/L
07/22/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
7.5 mg/L
07/13/2022
1, 1, 1,2-Tetrach loroethane
SW 846 Method 8260D/50306
<0.5 pg/L
07/18/2022
1, 1, 1 -Trichloroethane
SW 846 Method 8260D/503013
<0.5 pg/L
07/18/2022
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
1,1,2-Trichloroethane
SW 846 Method 8260D/503013
<0.5 pg/L
07/18/2022
1, 1 -Dichloroethane
SW 846 Method 8260D/503013
<0.5 pg/L
07/18/2022
1,1-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
1,1-Dichloropropene
SW 846 Method 8260D/503013
<0.5 pg/L
07/18/2022
1,2,3-Trichlorobenzene
SW 846 Method 826013/5030B
<0.5 pg/L
07/18/2022
1,2,3-Trichloropropane
SW 846 Method 8280D15030B
<0.5 pg/L
07/18/2022
1,2,4-Trichlorobenzene
SW 846 Method 8260D/50306
<0.5 pg/L
07/18/2022
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/503013
<0.5 pg/L
07/18/2022
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
1,2-Dichlorobenzene
SW 846 Method 8260D/50306
<0.5 pg/L
07/18/2022
1,2-Dichloroethane
SW 846 Method 8260D/503013
<0.5 pg/L
07/18/2022
1,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
1,3,5-Trimethylbenzene
SW 846 Method 8260D/503013
<0.5 pg/L
07/18/2022
1,3-Dichlorobenzene
SW 846 Method 8260D/50306
<0.5 pg/L
07/18/2022
Report #:: 2022-13097 Page 4 of 9

envirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
[e-mail]
Wood -AMEC Date of Report: Jul 29, 2022
5710 Oleander Drive, Suite 110 Customer PO #:
Wilmington NC 28405 Customer ID: 11070019
Attention: Ben Moore Report #: 2022-13097
Project ID: Hexion CLRS
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
2,2-Dich loropro pane
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Bromomethane
SW 846 Method 8260D/6030B
<0.5 pg/L
07/18/2022
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Chloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
cis-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
cis-1,3-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Dibromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Dibromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Dichlorodifluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Ethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Isopropyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
07/18/2022
Methylene chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Report #:: 2022-13097
Page 5 of 9

Environmental Chemists, Inc.
iLL enyirochem 6602 Windmill Way, Wilmington, NC 28405 + 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Wood -AMEC
5710 Oleander Drive , Suite 110
Wilmington NC 28405
Attention: Ben Moore
Date of Report: Jul 29, 2022
Customer PO M
Customer ID: 11070019
Report #: 2022-13097
Project ID: Hexion CLRS
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
sec-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Styrene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
tert-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Tetrachloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Toluene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Trans-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Trans-1,3-dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
07/18/2022
Formaldehyde
SW846 8315A
<50 pg/L
07/15/2022
Nitrate Nitrogen (Caic)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.51 mg/L
07/14/2022
Nitrate+Nitrite-Nitrogen
EPA353.2, Rev. 2.0,1993
20.1 mg/L
07/19/2022
Nitrate Nitrogen
Subtraction Method
19.5 mg/L
07/27/2022
Total Nitrogen (Caic)
Total Kjeldahl Nitrogen (TKN)
EPA351.2, Rev. 2.0,1993
77.8 mg/L
07/21/2022
Total Nitrogen
Total Nitrogen
97.9 mg/L
07/27/2022
Reportk: 2022-13097 Page 6 of 9

Environmental Chemists, Inc.
enyirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Wood -AMEC Date of Report: Jul 29, 2022
5710 Oleander Drive , Suite 110 Customer PO #:
Wilmington NC 28405 Customer ID: 11070019
Attention: Ben Moore Report #: 2022-13097
Project ID: Hexion CLRS
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-31846 Site: WWMW-03 7/13/2022 10:15 AM Water Client
Test Method Results Date Analyzed
Iron
EPA 200.7, Rev. 4.4, 1994 (Dissolved)
1.08 mg/L
07/19/2022
Manganese
EPA 200.7, Rev. 4.4, 1994 (Dissolved)
0.127 mg/L
07/19/2022
Sulfate
EPA 300.0, Rev. 2.1, 1993
40 mg/L
07/20/2022
Ammonia Nitrogen
EPA 350.1, Rev. 2.0,1993
130 mg/L
07/20/2022
Total Dissolved Solids (TDS)
SM 2540 c-2015
459 mg/L
07/14/2022
Total Phosphorus
SM 4500 P (F-H)-2011
9.48 mg/L
07/21 /2022
Sulfide
SM 4500 S D-2011
0.19 mg/L
07/22/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
37.6 mg/L
07/13/2022
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1, 1, 1 -Trichloroethane
SW 846 Method 8260D/503013
<1 pg/L
07/18/2022
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,1,2-Trichloroethane
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,1-Dichloroethane
SW 846 Method 8260D/503013
<1 pg/L
07/18/2022
1,1-Dichloroethene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1, 1 -Dichloropropene
SW 846 Method 8260D/50308
<1 pg/L
07/18/2022
1,2,3-Trichlorobenzene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,2,3-Trichloropropane
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,2,4-Trichlorobenzene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,2-Dichlorobenzene
SW 846 Method 8260D/50308
<1 pg/L
07/18/2022
1,2-Dichloroethane
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,2-Dichloropropane
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
Report #:: 2022-13097 Page 7 of 9

Cnyirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab ■ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ■ 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ■ 910.347.5843 Lab/Fax
[e-mail]
Wood -AMEC
Date of Report: Jul 29, 2022
5710 Oleander Drive, Suite 110
Customer PO #:
Wilmington NC 28405
Customer ID: 11070019
Attention: Ben Moore
Report #: 2022-13097
Project ID: Hexion CLRS
p-Isopropyltoluene
SW 846 Method 8260D/5030B
327 pg/L
07/18/2022
sec-Butylbenzene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
Styrene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
tert-Butyl benzene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
Tetrachloroethene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
Toluene
SW 846 Method 8260D/5030B
1.08 pg/L
07/18/2022
Trans-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
Trans-1,3-dichloropropene
SW 846 Method 826OD15030B
<1 pg/L
07/18/2022
Trichloroethene
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
Trichlorofluoromethane
SW 846 Method 8260D/50308
<1 pg/L
07/18/2022
Vinyl chloride
SW 846 Method 8260D/5030B
<1 pg/L
07/18/2022
Formaldehyde
SW846 8315A
59.0 pg/L
07/15/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2, Rev. 2.0, 1993 < 0.02 mg/L 07/14/2022
Nitrate+Nitrite-Nitrogen EPA 353.2, Rev. 2.0, 1993 0.12 mg/L 07/19/2022
Nitrate Nitrogen Subtraction Method 0.12 mg/L 07/27/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN) EPA 351.2, Rev. 2.0, 1993 175 mg/L 07/21/2022
Total Nitrogen Total Nitrogen 175 mg/L 07/27/2022
Comment: Sample # 22-31844 and 22-31846- Method 8260D reporting limit elevated due to matrix
interference.
Reviewed by:
Report #:: 2022-13097 Page 9 of 9

Analytical Environmental Services, Inc
Date: 21-Jul-22
Client:
Environmental Chemists, Inc.
Client Sample ID:
22-31844
Project Name
2022-13097
Collection Date:
7/13/2022 9:45:00 AD1
Lab ID:
2207F13-001
Matrix:
Aqueous
Reporting Dilutio
Analyses Result Limit Qual Units [3atchlD n Date Analyzed Analyst
Formaldehyde by SW8315A
Formaldehyde 52 50 ug(L 339642 1 07/15/2022 14 31 CM
Qualifiers: ' Value exceeds maximum contaminant level
BRL Below reporting limn
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
E Estimated (value above quantitation range)
S Spike Recovery outside limns due to matrix
Narr Seecasemrrauve
F Analyzed in the lab which is a deviation from the method
Less than Result value
J Estimated value detected below Reporting Limn
Page 3 of 9

Analytical Environmental Services, Inc
Date: 21-Jul-22
Client:
Environmental Chemists, Inc.
Client Sample ID:
22-31845
Project Name
2022-13097
Collection Date:
7/13/2022 10:00:00 AM
Lab ID:
2207F13-002
Matrix:
Aqueous
Reporting Dilutio
Analyses Result Limit Qual Units BatchlD n DateAnal}zed Analyst
Formaldehyde by SW8315A
Formaldehyde
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limn
H Holding times for preparation or analysis exceeded
N Amlyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
13RL 50 u@/L 339642 1 07/15/2022 18 03 CM
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
F Analyzed in the lab which is a deviation from the method
Less than Result value
1 Estimated value detected below Reporting Limit
Page 4 of 9

Analytical Environmental Services, Inc
Date: 21-Jul-22
Client:
Environmental Chemists, Inc.
Client Sample ID:
22-31846
Project tame
2022-13097
Collection Date:
7/13/2022 10:15:00 AM
Lab ID:
22071`13-003
Matrix:
Aqueous
Reporting Dilutio
Analyses Result Limit Qual Units BatchlD InDatcAnalyzed Analyst
Formaldehyde by SW8315A
Formaldehyde
Qualifiers: value exceeds maximum contaminant level
BRL Below repotting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Ana4te detected in the associated method blank
> Greater than Result value
59 50 ug/L 339642 1 07/15/20221813 CM
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Nary Seecasenarratne
F Analyzed in the lab which is a deviation from the method
Less than Result value
1 Estimated value detected below Reporting Limn
Page 5 of 9

Environmental Chemist, Inc., Wilmington, NC Lab #94
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
Client:W 0C) l — [\/M Q_ Date: " / ' aa ReportNumber. o-a -° 0/-7
Receipt of sample: ECHEM Pickup ❑ Client Delivery
JUPS ❑ Fed Ex ❑ Other ❑
❑ YES
❑ NO
q N/A
11. Were custody seals present on the cooler?
❑ YES
10 NO
JR N/A
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt ir - °C „( C,Q Corrected temperature upon receipt °C
How temperature taken: ❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES
❑ NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
k1 YES
❑ NO
4. Were proper custody procedures (relinquished/received) followed?
ffirl YES
❑ NO
5. Were sample ID's listed on the COC?
YES
❑ NO
6. Were samples ID's listed on sample containers?
YES
❑ NO
7. Were collection date and time listed on the COC?
YES
❑ NO
8. Were tests to be performed listed on the COC?
YES
❑ NO
9. Did samples arrive in proper containers for each test?
YES
YES
❑ NO
10. Did samples arrive in good condition for each test?
11. Was adequate sample volume available?'
❑ NO
5Z YES
❑ NO 112.
Were samples received within proper holding time for requested tests?
YES
❑ NO
13. Were acid preserved samples received at a pH of <2?
❑ YES
❑ NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑ NO
15. Were sulfide samples received at a pH >9?
YES
❑ NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
❑ YES
❑ NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑ NO 118.
Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation: If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

-
"
ENVIRONMENTAL
MENTAL CHEMISTS
L S
mir
INC
Analytical & Consulting Chemists
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
OFFICE 910- 2-0223
ionfo@ nv ronmentalchem
COLLECTION AND CHAIN OF CUSTODY
Client: Wood-AMEC
ADDRESS: 1 ��
PROJECT NAME: Hexion Acmr CLRS
�rr
REPORT NO:
v N
�'1� CONTACT NAME: Ben Moore
PO NO: Z� l�'
REPORT TO: Ben Moore
573A
PHONE FAX: [phone]
COPY TO:
Sampled By:
email: ben.moore@wood Ic.cc
SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Slud
Collection
Sample Identification
a A. PRESERVATION
~ o ° _ 0 _ ; o o W
m
n a m
E o 0 0 �L c E `o a z o
Date Time Temp co
� " " " a J z Z _ =
W
0 o a w ANALYSIS RE
z
i
o
C P
G 'G �� 17 ti
C P
Formaldehyde (8315
3
C P
EPA 8260 Low -Level
G G (
C
TOC
G
C P
NO3, NHL, TP
C� G
-Sulfate
C
G !
C P
TDS
G
C
1.
Transfer Relinquished By:
Date/Time Received
_
2.
Temperature when Rived 'C; o r Acce ted:
p Rejected -
Delivered
Resample Re ue
Delivered By: Received By: j� Comments: Date: Time:l,Lo7s
URNAROUND:

ENVIRONMENTAL CHEMISTS, INC 6602WindmillWayWilmir
OFFICE: 910-392-0223 FA)
Analytical &Consulting Chemists
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@ nv ronmentalchemi
COLLECTION AND CHAIN OF CUSTODY
Client: Wood-AMEC PROJECT NAME: Hexion Actnr CLRS
REPORT NO:
ADDRESS: 1 ib Sv�� CONTACT NAME: Ben Moore PO NO: 677194Z 7r '
e 2 REPORT TO: Ben Moore PHONE/FAX: [phone]
COPY TO: email: [e-mail]
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W =Well, ST =Stream, SO = Soil, SL = Slud
Collection PRESERVATION
Sample Identification 0 . W c
CL c o a° c E `o a 2 z -' o o p o Ui w ANALYSIS RE
Date Time Temp N " "_ U a J Z Z=_= z-1 o
�I 13 a tni LL
Transfer
Relin uished By:
Date/Time
Received By:
Zo�3
57.E za'sz5

Analytical & Consulting Chemists
Client: Wood-AMEC
ADDRESS: 131 n O
Sampled Bv:
ENVIRONMENTAL CHEMISTS INC OFFICE: 910-392-022311E it 3 3
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 info@environmentalchemi
COLLECTION AND CHAIN OF CUSTODY
PROJECT NAME: Hexion Acmr CLRS I REPORT NO:
U'Y� U,`t-� I t U CONTACT NAME: Ben Moore
-zz REPORT TO: Ben Moore
COPY TO:
PHONE/FAX: 910.452.118 5
email: ben.moore(a_)woodplc.cc
RAMPI F TVPG• I = 1nfh—f C — Cffl.. —6 UU — lei a cT _ c••-__� e.� _
Sample Identification
Collection
n
F
d
c
N
M
m 2
a o
E
V o
r-
-0o
U a
—_
c`
ab
t E
V
_ __________,
p
2
o
a
_
Ow
co ou
Q
J z
_..._�..-,
PRESERVATION
-- ......,
v. vim. •..a...,
vv — ...v, VL VIY4
ANALYSIS RE
Date
Time
Temp
w
z
z
-'
o
=
0
=
=
0
z
0
~
G
w
o
�
LL
w
O
•,�ww�w : c�3
03
TZ
1015
c
P
�
i
Formaldehyde (8315)
G
G
C
P
EPA 8260 Low -Level
C
P
I
TOC
G
C
NO3, NH3, TP
G
G
C
r
I
ISulfate
G
C
`
1
IT.S
G
C
bSrs�l� '—C�-my
G
tt
G
G
V
Transfer Relinquished By: Date/Time Received By: C
1. r z
2.
cnINUIOLUIC ru %1: 1, /L'-� Hcceptea: - Rejected: Resample Requested:
Delivered By: -^- Received By: Date: 47i 2 Z Time:,LZ5
Comments: TURNAROUND:

Comprehensive Site Assessment —Bakelite Acme
Appendix D Groundwater elevation data for WWMW-1 through
WWMW-3 (Since RI)
EHS Support LLC

Appendix D - Groundwater elevation data for WWMW-1 through WWMW-3 (Since RI)
Location
WWMW-1
WWMW-2
WWMW-3
Northing
211953.2745
211852.5798
211736.6509
Easting
2240745.256
2240665.828
2240736.922
Top of Casing Elevation
24.08
16.74
18.12
Date Measured
Groundwater Elevation (ft amsl)
2016 (RI)
13.73
9.84
NA
July 24, 2019
14.62
9.99
NA
November 20, 2019
14.17
9.91
NA
March 10, 2020
13.57
8.92
NA
July 16, 2020
13.49
9.28
NA
November 24, 2020
13.65
10.56
NA
March 17, 2021
13.29
9.46
NA
July 8, 2021
13.16
8.39
NA
November 10, 2021
12.75
7.13
NA
March 9, 2022
12.44
7.59
NA
July 12, 2022
13.30
7.92
11.54
August 10, 2022
13.43
8.07
11.59
November 2, 2022
13.38
8.39
11.54
March 8, 2023
13.81
9.39
12.02
ft amsl = feet above mean sea level
NA = not applicable (WWMW-3 was installed in July 2022)
RI = remedial investigation

Comprehensive Site Assessment —Bakelite Acme
Lbj.Fj--01-q
Appendix E BIOSCREEN and BIOCHLOR Input Parameters and
Model Outputs
EHS Support LLC

APPENDIX E — BIOCHLOR AND BIOSCREEN INPUT PARAMETERS AND MODEL OUTPUTS
Client Name:
Site Location:
Project No.
Bakelite Synthetics
Acme, NC
LLC.03536.2021
TDS —Calibration Input Parameters
810SCREEN Natural Attenuation Decision Support System 6akelrre l7ala !opal lnsWctivns:
a rr Force Center rar Enarranmenlai Excedenm
Vece- 1.4 TDS Y23 115 1. Enter value tldedlV..--or
Aun Nanse,,,,, lT -' 2 Calwlate by7ionedgrey
OGEE
1. HYDROGEOLOGY
N.-...... ... .... ..
5 GENERAL Oat -ii (Tu restore
va-rf Vs
Seepage
2w0..��..��,
�(fii
1lcmisec)
W Van Data use�ow
Modeled Are Length 450 (ft) } L form ! hd bull be! w}
200
H draulic Conduct 1C
Si ula4o Tme'dth"
1.0E-03 r9 r by model
Hydra Gradient f
OA47 ftJft
r }
.... "" 1�nvalwlated
.... .... „ a T enfer any" ...... ,
Pomsullc
'I[y n
0.25 (-J
G. SOURCE DATA
2..........DISPERS...I..O..N ...
knm„1��Plln2d LokePlmCmSchan
,,sn,cZonc,d ICvncenGoSWrdlhs
rt
-d
Longitudinal Dipersvyaf
Wid ConZv
TransversDispesmty" fpyx
15 (ftj
n 0
Vertical Disparspr y= alpha,
0 0 (Sf}
u 0
or
'_ T or
19 1? 10 - e•. e•. e•. r. m m m m m m
Estimated Plume Length LP
350 (ft)
I I
3. ADSORPTION
Source Halfl ite (see
Factor'rdation
(}
- N) brew of Plume Looking Doom
- lost
ist Orde[
5ollaBulk Demly dw
17 (111 Solub
eM�ass Infinite (fCg} Observed Centerlirre ConcehheriaRs at Mondowig Wefls'-
ParffonCoelficimt Koc
14.3 (Ul In
Source N.APL Soil IF No Data Leave Dlapk or Fnler'0"
FractionOrganicCarhun foc
I I.IIE-3 (-J
_.
7. FIELD DATA FOR COMPARISON
Concentration (mgfL) 1310.0 0 534.0 0 0 0 11 0 C 0
...........................................................................................................-
4. BIODEGRADATIDN
Dist Crum Source j1t)
1st Order Decay Coe1T' 1."n
6.9E-7 (peryr)
or
=T er
1. CHOOSE TYPE OF OUTPUT TO SEE:
Solute HalfLLlFe I -half
(year]
Recalculate This
RUN Help
or lnafantaneoua Reaction Model
Sheet
RUN ARRAY
Delta oxygen' DO
(mg7L)
CENTERLINE
Delta Nitrate` N09
(I -I
Paste Example Dtasat
Observed Ferrous Iron' Fe2+
(MIL)
E6(mg,
P Reslate FormulasFr4
View Out tlt Vtew outputDelta
Sulfate` SO4
(mgvL}
Dispersivrl'es, R, lamhda, vUrer
tOhserved
Methane' CH4
-
TDS —Calibration Output
DISSOL'<'EDRYDROCARRON CONCENTR.gTTON ALONGPLL-W CE,I'1ERL1i (tngi at Z=O)
D; meal n, Se— (R)
TYPEOFMODEL
0 '..
45 DID
135 180 225 27D 315 '.. 3e) 405 '.. 45O
Na D.gradatian
1310.000
748:708 530.490 390 103 266 7.27 157 9.71 .7.7..0.3.7 '.. 29.858 '.. 8.978 2 061 0.357
1st OrderD
1310DOD
7497D8 E30490 39D 103 266727 157971 77037 29858 9975 2D6t 0357
Inst. Reaction
_Freld
131 D DDD
742 427 521 768 379 810 255 D54 145 D82 63242 15535 0 DOD 0 000 0 000
__..
Oatafmm Sde
1310DOD
534 DDO
—0­1sf Order Decay Reacfreo _NO Degradation m Field DaFafrom Sde
1400.000
1200.000
oT000.000
�0.000
oo&0aa
v .000
L .r
GJ 400.000
700.000
0.000
0 50
100 150
200 250 300 350 400 450 500
Distance Frmm Source tft)
3ime;
Calculate
1 Years
Return to Recalculate This
Animation Input Sheet
EHS Support LLC

Client Name:
Site Location:
Project No.
:I
Bakelite Synthetics
Acme, NC
LLC.03536.2021
TDS— Plume Extent Input Parameters
BIOSCREEN Natural Attenuation Decision
Support System Ba erne Data hput astructiortsr
Arr Force Center for Envuonineniar Erecilo,—
Va stun 1.4 TDS 323 115 _ 1. Enter tcdlue direetry....or
Run Name _Tor 2 C.leulateby Allinglnprey
1. HYDROGEOLOGY
___
5. GENERAL 0 c0s below (T s tore
02
Seepage Velocdy' Vs
210.0 (R/yr)
Modeled Area Length' L alas nit button below)
51E (RJ j �
or
o () V� noble' Data useddirec0 in model
r '',t Modeled Area Wdth' 200 v
y du
GZdie'tl
i -03 m/sec )
•,,,
atil4 caleulaterbmodel
�) 1 y
y'd'�Fad Gradient I
n
0 047
r
•• • • • • • • • flue
pol—tflc
Porostyc
g0
25 6' SOURGE DATA
Smmtce 7luckrress m Sat Zone• 10 (R) Vertical Plane Soun:er Look at Plume CrossSeetron
R. DISPERSION
Source Zones and Input Concentrations & ffdths
LorgR.diud DrspersW alphas
i5 2 (R)
Width Co -to !L' far Zones i, 2, and 3
Transverse Disperslvily' alp'ey
1.5 (R)
O 0
Vertrcal DispersivW aiply
DO(R)
O 0
or
19 1310 0 o a o a �0 0 0 0 0
Estimated Plume Lengtin LP
1 t
3. AO SORPTION
Source Halflite (see Help(:
Retardation Factor` R
1
001
r) Viewo Plume LoNmng Dow
or
he
•'�•'
(RgrD
•l�b •ass InfnO�e (Kg) observed Ceetedine C—otre Wefts
OOr
if No Data Leave Bta�nsatte,"Oorinq
�(LzI m'S Nor Enter'O'
FractioSO
9 eoi Garbon fmc
LDNAp ASoO
T. FIEG�•DAT••F• 11 C...
10Ea OMPARISON
Gcncentratlon (mg1L) 13100 0 534.0 0 0 0 0 1 0 0 0
4. 810DEGRADATION
❑ist from Source R
()
1st Order Decay ac lambda
&.9E-7 (peryr)
or
8. CHOOSE TYPE OF OUTPUT TO SEE:
Salute Half-Lde t-half
orinsbnbneous Reaetron Model
Delta oxygen' Do
1 OOE+O& (year)
s5 (mgrL)
Re-l-We This
P Sheet
CENTERLINE RUN ARRAY Help
Delta Ndrate' NO3
O.7 (mg/L)
Paste Example Dataset
Observed Ferrous Iron' Fe2>
Delta Suhte' SO4
16.6 (mg2)
22.4 (mg2)
i/I@W Output VIEW output
P p Restore Formulas for Vs,
Oh—cl Methane' CH4
66 (mg&)
Disporsivuies, R, lambda, other
TDS — Plume Extent Output
➢ISSOLITDDYDROCARDO\ CO\CF-SMU7I01 ALONGPLLAM CE\'PERLLoE (mg1L ¢t Z=O)
Dismxce from 8--"
TYPE OF MODEL 1 0
52 103
155 2O6 258 31 O 361 413 464 516
No Degradation
1310 000
722.399 534.415
443 139 386 764 347.526 318.147 294.938 275.691 258 792 242.801
1st Order Deeay
1310000
722399 534415
443139 I 386763 341528 318146 294938 275691 258791 242801
Inst. Reaction
1310000
715824 525.737
433440 976434 336760 307049 283.591 264.119 247030 230.961
Field D.I. roan 54e
1310 O00
534 O00
�7st Order Decey �tnstantaneous Rea-- —No Degrada5- o hod Gala k—Side
7400.000
1200.11011
07000.000
$D0.000
00 000
C
U 400000
200.000
0.000
0
Igo
200 300 400 500 600
Distance From Source (f )
Tim
Calculate
4 Years Return to Recalculate This
Animation
Input Sheet
EHS Support LLC

Client Name:
Site Location:
Project No.
Bakelite Synthetics
Acme, NC
LLC.03536.2021
Sulfate —Calibration Input Parameters
BIOSCREEN Natural Attenuation Decision
Support System Baxelrie natd mpurrnstnicill
A,r Force CeNer For EnvrmnmenYal E—Vence
9.a SvlYate 323 115 f. Cuter value ddechY....dr
ty n rey
filing5.
DRODEOL ....
OGY
.........
GENERALTo restore
..(iY) L
s..
seepage Velocity" V.
210.1)...... (R40
Modeled Area Length 450 for h n beo
!gr bu[to
or
..
_ ? w� -Data d OY n del....
MWet d n
[dth" 200 fry + Yartable�,,,������..Value
Hyctir K
P.r..............
nA
�/ c rakrNdwlfec...
IY J � by -
id �4 3
Hydraulic Grradientyl
J
,,,, „ I ,,,,
Porosity n
6. SOURCE DAT�����������,,,,,,,,,,,,,,,,,,,,,���������������������,,,,,,,,,,,,,,,,,
075 (( A
������ llli����,,,,,,,,,,,,,,,,,,,,�����������������11111,,,,,,,,,,,,,,,,,,,,���������������������,,,,,,,,,,,,,,,,,,,,���������������������................ ......,,,,,,,,,,,Source,
l; h,K,kn,ess,f „Sat,Zon,e` 10 (nJ Vertical Plane Source.- Lookat Plume Gross -Section
Y. DISPERSION
Source Zones and Input Concentrations & Widros
Longitudinal Disperstm ' alphas
i5 2 (Rf
_�
Wrdth Conc.l1 ` _ nes 1. 2, and 3
Transverse DlspersNity` alpha y
i.5 I'M
0 0
Vertical DispersNity' alpha a
0 o (R}
0 0
or
T w
19 1026 ' a e e e e ± a a e a 0
Estimated Plume Length LP
_
sw(RJ
r r
ADSORPTR)N
Source
Halfrife (see Help(:
Retardation Factor` R
1 tl If fYr} VleWorPlume Looking Down
or
_ w i InEt
A t_ 1si Order'
Soil Bulk Density rho
17 (rrgAJ 5
I ul M ss Infinite (Kg) 00.rervetl Centerline Concentrations at Mvnitonng YVe!!s
Partition Coefficlent Koc
14.3 (Vkg) In aomce NAPL Soil IINa Data Leave Hlanlf or Enler'0'
FractionOrganlcCarbon rtw
1.0E-3 (-J 7.
FIELD DATA FOR COMPARISON
ConCenlrat[on (mg1L) 1020.0 0 264-0 0 0 0 0 0 0 0 0
4. BIUDEGRADATIDN
Dist from Source (fl)
1st Order Bell Coett ambaa
1.3E+0 (P-A
or
w 6. CHOOSE TYPE OF OUTPUT TO SEE:
So Me Hatt LAe t-halr
_'h
0.55 tyeaq
RUN Help Recalculate This
orMstantaneousAeactionModel
Delta Oxygen ^
(mg2J I
RUN ARRAY
CENTERLINE
0
Delta Ndrale" NO3
7
0.7 (mgRJ
paste Exam le Dataset
p
Observed Ferrous Ir Fe2+
Delta Suffate' SO4
Observetl Methane' CH4
16 6 (mg2J
22.4 (mg&)
66 (mg/L)
View Dut ut View output
p p Restore Formulas Tor Vs,
Dispersivilies, R, lambda, other
_
Sulfate —Calibration Output
DISSOLVED HYDROCARBON CONCENTRATION ALONG PLII CENTERLLVE (mg7L at Z=O)
nis�c f aa. S,—,e"
TYPE OF MODEL
0
45 0135
180 225 210 315 360 405 450
No Degradation
-
1020.000
582.963 413 053 303.744 207 681 1 3.001 59.983 ?3.'43 6.991 1.604 0 273
- - - - - -
list Order Decay
1620.00D
460.686 261.979 159.669
94.162 49.977 22.532 8.258 2.396 0.531 0.09D
Inst. Reaction
............ ...............
1 D20 ODD
................
576 663 404 331 293 452 i 196 0DB 110 ill 46 190 8.925 0.000 D D00 0 000
.................. .. e...... ........... .............. ........... ............. ............... ........................
Field Data from Site
1 D20.00D
264 DDO
It Order Decay —P—fnstantaneoas Reaction —No Degradaaon 0 Field Data from Site
1200.000
1000.000
4
Soo .000
�0.000
c 400.000
U
T00.000
0.000
0 50
100 150
200 250 300 350 400 450 500
Distance From So— (ft)
Calculate
Srme
9 Years Returnto Recalculate This
Animation
Input Sheet
EHS Support LLC

Client Name:
Site Location:
Project No.
Bakelite Synthetics
Acme, NC
LLC.03536.2021
Sulfate — Plume Extent Input Parameters
BIOSCREEN Natural Attenuation Decision
Support System Eake ire ?Tara RrlputbistrueHons.,
Arr Face Genre, fa E-ro —Nat Edc0e—
Versmn 1.4 lsulfar, 3,23 115 -I_ Eh[er Value ltrecgy___.or
2
E~
.
1. OL OGY
................
5 GENERAL p02 cells below To restore
See Velocity'
page Velocity' Vs
516 (ftJ to~�
210.0 Mr) Modeled Area Length famrulas hR bT J
,
Modeled200 (ftr Vanab�'Hate ed,�I an motley,.......
1-DE-03
tlranik Conduclfv K
IN tY
ec Slmnlaor t
Tlme'Areartlth'
f 1 (Y J + _ -yai0euseGfote Dy nrgtlel,
Gratlient
P
n
""
"""'10
mashy n
0.25 H a, SOURCE DATA
............................................................................
...........�
ass In Sat Zone' (ftJ Vertical Pfane Source: Look as P eY��X
���������������,,,,,,,,,,,,,,�������������� Cross -Section
4. DISPERSION
Source Zonand 1npu1 Goncentrarrons a IMdfhs
Longitutlhnal DlspersMty' alplsar
152 (fCJ
Wltlth ft Conc !L' _ - nes 1, 2, and3
Transverse Dispersivity' alpha y
1 5 (rc)
0 0
Vertical Dlsperslvily` alpha z
fl fl (ftJ
9 fl
or
_q`ar _
19 102fl V. a a 9 9 a a a a n
Estimated Plume Length LP
®(IF)
r
r r
TIDN
Source Halfrife (see Help):
Retartlalion Factor` R
1 fl (-j - - {yr1 View of Plume Looking Down
(
Centerline Concentrationsat MonitoringNleflslr
1YeMPARISON
ParTillon Goeffitenl Koc
.3 In
Pl.�E-3
Source PIAPL oo i No Oafs Leave Wank or Enter "C"
FractlonOrgamCarbw too
()
7.StFELDtDATA FOR COt(Kg)Observed
............ ...............
..............
Concentration (rrlglL) 1020.0 0 264.0 0 0 0 0 0 0 0 0
4, B100EGRADATION
Dist. from Source (it)
1s1 Order Decay Coen" amdua
1.3E+0 (peryr)
or
111 or S. CHOOSE TYPE OF OUTPUT TO SEE:
Solute Halt-Ll t halt
0.55 (year)
RUN Help Recalculate This
or Instantaneous Reaction Model
RUN ARRAY
Delia Oxygen" DO
1.65 (mg/L)
CENTERLINE
Della Nitrate" NO3
0.7 (mglL)
Paste Example Dalaset
Observed Ferrous Iron' Fe2+
16.6 (mg/L)
View Output Yfew Output
PRestore Formulas for Vs,
Della Sulfate' SO4
22 4 (mg/L)
UlspersivNes, R, lambda, other
ObseNetl Methane' Cy4
66 (mg/L)
MM
Sulfate — Plume Extent Output
OLSS011uY➢ROCAR➢O\ CONCEN IRUTIO\ ALO\GPLLl1E CE\'1'ERLL\'E (mg/L at Z�)
D—ft— S.— W
TYPE OF MODEL 0
52 103
155 20B 258 310 381 413 464 516
No Degradation
-_-
1020.000
562.478 416 109
345.039 d71 144 270.596 247 717 229.647 214.661 201.502 189.051 _-
--96108---64914
1s11 Order Decry
-_-
1020 ODD
422761 236067-
146503,_. 44679 31.159 21941 15562_- 11004
Inst. Reaction
............... .............
1020.000
............
555.904 407.432-
............ . ..............
335340 290814--259826 236620 218289 203.088 189.740.., 177.111_-
..... ........... ............... ............. . ............... .............................
Field Data from Sit.
1020.000
264000
Misr order Decay Reacrron —No Degadahnn a Fiend Data rrdm 5Re
1200.000
1000.000
q
° 800.000
V 110.000
c 400.000
0
200.000
0.000
0
200
100 300 400 500 600
Distance Fmm So— (ft)
Calculate
lime:
q years
Animation Return to Recalculate This
EHS Support LLC

Client Name:
Site Location:
Project No.
:I
Bakelite Synthetics
Acme, NC
LLC.03536.2021
Ammonia —Calibration Input Parameters
BIOSCREEN Natural Attenuation Decision Support System Ba,<elee Dara input tnsvucdons:
A✓Porte
Veraron 7.4 Arrmoma 312.. 115 t. Enter valve dnec[fy__or ".
Ran Rome o- 2. Calculate by Rini
prey '..
VeGl
__.
(Tin
Seepage
oc4itflGY Vs
�210.0---t(fl/yf} ModeEed Area WLe dhh' 200 Va6ahle` u�l dd
Hydraulic Conductmt K
VNat�a al madet�
1 OE-03 fcmkec) Simulation Time 1 r ® y
��+
Hydraulic Gradient i
0047 (ttAtJ
(Don't enter any. data)
porosity rt
..,
0.25 (-J G. SOHRCE BATA
Source Thiclmesa in SatZone' 10 (RJ Ver8ca1 plane Source_ Look at plume Cross -Section
4. DISPERSION
Snurce Zones Input Cancentra6bns 8, Widths
Longlludinal Dlspusoty' elptrex
15.� (ftJ
��oand
Width` if ant L' i 2 and3
Transverse Dispersmty` alphay
1.5 (f1)
0 0
Vertical Disperamty" Monad
0.0 (h)
or
_ -•
19 490 e m e
Estimated Plume Length Lp
® (ftJ
r f
7. A�RPTI�N,,,���,,,,���,,,,���,,,���,,,,���,,,,���,,,,��,,,,���,,,,���,,,,���,,,���,,,,���,,,,���
OS
„
Sorce Halllile u(see HeIpI:
Retardation Factor' R
1.0 (-) - - (yr) View of Plume Loafong Down
or
_ Inst
Re lst artleri
Soil Sulk Density rho
1.7 (kg,1J Soluble Mass Infinite (KgJ Observed Cen[edrne Concenbafions at Monrl Wells
Partition Gaalficient Kac
l43 (Lxkg) In
Source NAPL, Sol tf Ab Data Leave Blank or 1"0"
FractlonOrganlcCarbon roc
1 ♦)E-3 (-) 7 FIELD DATA FOR COMPARISON
concentratian ir*LJ 4sos 0 e e 0 s s s s o 0 s
4. BIODEGRADATION
Gist. tram Source {ftJ
1st Order Decay Coe1f' e-1—
12E+1 (peryrJ
or
ltr` a 8. CHOOSE TYPE OF OUTPUT TO SEE:
Solute Half-Lde t-half
w Instantaneous Reacton Mode?
Delta Oxygen' DO
Delta Nitrate" NO3
0.06 (year}
RUN RUN ARRAY Help Renlurlate
t66 fmg2) CENTERLIN
0 7 (mg/C} Paste Example Dalai
Observed Fenaus Iran' Fe2+
16.6 ftk)
view Output View Output Restore Formuias for Vs,
Delta Sulfate' SO4
22.4 (Mg/L}
Disperaivitiea, R lambda, other
Observed Methane` C?i4
fi.6 fn+9R)
Ammonia — Calibration Output
DISSOLVED HYDROCARBON COISCEA'TRAni ALONG PLUME CETTERLTT'E (mglL at 2rD)
Dfstaace frnxr Scarce U)
TYPE OF MODEL
0 -
45 -_ 90
135 180 226 270 315 360 405 450
Na Degradation
490 000 290051 198 427 145 218 99 788 59 089 28 815 11 188 3 259 0 771 0.133
--- -- •-- -_--- • --_-❑ • --_-
1 st Order Decay
---1nst.
490.DDO 57 427 8.594
-
1 436 0 252 D 045 OD8 0001 O-ODD 0.000 0.000
•-- ----46199 •---15020 • ---0
Reaction
490000-- 273771 199.706 135rN
-
88-095ODD 0.000 OOOO DODO
•--_--- • --_- • ---- __-- • --_- ---- -
Field Data from Site
490 DOD--
8 800-
_1st Order Decay Read- —Mo Degradation o Field Data from Site
600.000
500.000
e
a 400.000
� J
1.000
a
_
z00.000
V
100.000
0.000
0 50
ran 150
200 250 300 350 400 450 sou
Distance From Source fft)
Tuae:
CalculateA
Animation
Years
Return to Recalculate This
EHS Support LLC

Client Name:
Site Location:
Project No.
:I
Bakelite Synthetics
Acme, NC
LLC.03536.2021
Ammonia — Plume Extent Input Parameters
BIOSCREEN Natural Attenuation
Decision
Support System Rakerre flab mpue mstn G ons:
A, Force Cea[er for EnvrronmenlaV EYCellence
Versma 93 Ammonra323 115 Y, Enter value d—dv
in qrey
Run Name,,,,, T ^ 2 Calculate bVTo
OGY
RY
.Se
..
"' - • ...
m
S. GENERAL o02 cells below (To restore
�E
pa9 VS
or
e1rO D (fvyd
Modeled A ea Leng h* 516 t� } fo mul hn bu ton be ow)
Modeled Area Wldth* 2DO (f1) W es} Vanabk: Gate used dir-yym model
Hydreulic Conduct K
Nly
10E-03 }
(cm/sec
Simulation Tlme` 4 (yr) + ® Value rslculated bymodel
Hydreulic Gradient
P—m V n
025 O
5. SOURCEDATA
Source Thrcknessln Sat Zane10 (R) Vedfcei Plane Suurcer Look at Plume Cro-5-t-
..
2. DISPERSION
Source Zones and Input Concentrahons&widths
Lo g tudlnal D spe svW alpha r
1o5.2 (ft)
Wldth* ft Gunc IL' for— 1, 2, and 3
ran
Tsverse Dispersvily` alpha y
1.5 (R)
0 0
Vertical D!,p, lvty` alpha z
0 0 (ft)
D 0 \
o 0 0
Estimated Plume Length LP
®(ftr
t r
3. ADSORPTION
Source Halflife (see Help):
Retardation Factor" R
10 U
(yr) Vew.fPlume L-Kog down
or
) or
lrfst Reed. 15t OR1er
SA Bulk Density rho
17 (Irg/1)
Soluble Mass Infirnle (Kg) Observed Centedine Concentrations et Morrill Wells
Part@on Coefficient Koc
143 (U1fg)
]n Source NAPL ENI If No Data Leave Rlenkor Enter"O"
F—tonOrganicCarbon fnc
1.17E-3 (-)
7, FIELD DATA FOR COMPARISON
Cancentratlon (mg(L) ""' 0 8.8 0 0 0 0 0 0 0 0
4. BIODEGRADATION
Dist. from Source (ft)
1st Order Decay Ceeff` lamtwa
1.0E+1 (peryrJ
or
I
8. CHOOSE TYPE OF OUTPUT TO SEE:
Solute HalLifet-half
orinsfammeous Reaction Model
Dena Oxygen* Do
0.06 New)
_
Recalculate
RUN RUN ARRAY Help This Sheet
CENTERLINEDelta
Nllmle' NO3
(mgA)
Pasfe Fxrrple Dall
Observed Ferrous Iron` Fee+
M(mgA)
(M91W
View Output View Output Restore Formulas farVs,
Dena Sulfate` SO4
(mgA-)Observed
❑isperslvities, f{ lambda, other
Methane' CN4
(mgA)
Ammonia —Plume Extent Output
DISSOLVED HYDROCARBON CONCENTRATION ALONG PLI:IME CENTERLINE (mgiL at Z=0)
niawnrel om source 0t)
TYPE OF MODEL 0
52 103
155 2W 258 310 361 413 464 516 '
No Degradation
490 ODD
27021D 199896
165754 ''. 144667 ''. 1299132 ''. 119 DO 110.32D 1D3.121 96 WD ''. 90819
1st Order Decay
490 ODD
42 937 5 047
0 665 D OW 0 013 D OW D 000 0 ODD 0 ODD D ODD
Inet. Reaction
4900110
263636 191218
156055 134337 119223 107904 98963 91549 85038 78878
Reta Oat. from Srte
490 000
0800
—1S Drder Oeray —No Oegradebou o Field Data6om Site
600.000
500.000
C
r 400.000
G .00
c 100.000
U
100.000
0.000
0
I00
200 300 400 500 600
Distance From Source (ft)
Calculate
ztime_
Animation
4 years
Return to Recalculate This
EHS Support LLC

Client Name: Site Location: Project No. -a
Bakelite Synthetics Acme, NC LLC.03536.2021
Nitrate -Calibration Input Parameters, where PCE represents ammonia and TICE represents nitrate
BtOCNLORNatural Attenuation Decision Support System EakalRe J Oafs Input Insttue ions:
Versou 22 AmmoniaNibintn 3123 115 1_Enta IV ,deadly-_nr
O.Q.C.. M .... L w—� "' cr 2 CalrLlaie by Mln9 rn 91aY
4. .... ..... . p S GENERAL ee CC
R N
lYPE OFCHLOlkINATEO SOLVENT p02 celb Press Enter. then C�
[To resrnre lormulac,hr"Resrore Formulas"Eugonl
ADVECTION odeledA ea W�dlh' a0 R VBnebn Data used directly in mode[
Seepage V bitty` Vs 21 g 0 (IUyr Modeled Area L h 45D R Test !
or A Z 1 L g[h . IR} r— Rwlrar�s7ormaG natural nttenuatian
Hyd r Contlu dlvily K 1flE N3 [omiseol Z n 2 Length p (ry} ton 2 IS i7crLrrN Scn:ening Pmroc6l
Hydra M1 Grecq,rn D 047 Ilrlf[] - yenc�al Plaue Efle.3— Determme SoV rce Wall
pT- Rh rF% .... g 025 [) fi SODNCE DATA Tl PE Fit ti uo j L.-i and Inpul S.Ii Coneenbalyens
2. DlSPFRSION -- - Single Planer 1
Alpha % 152 (ft) Calc. Source OpN
{Alpha y}I (Alpha x}' g.1 (} Source Thickness n Set. Zo ' 10 (it)
(Alpha }I{Wphe z}' 1.E-02 (� Y1 -
']. "MRPTION_. _. -. _. I., Wdffi-(tt)-
Retard.ti,n Factor'
Conc.
Sod Bulk Derrslty, rho 17 (kglL} =PCE 49D.6 11
Fraction OrganicCarbon, foc 1.DE-3 l-] I =_TCE 04 P VleW of PIUme Looking DOWn
Padltlan Coefielent Koe al DCE P
PCE t4 fLrAg} I,1R (-} VC 6 Cbser,W Centerline Cone at MDQAfing lilpl]g
TCE T4 (Lily} 1,10 (-] ETH
DCE T4 fL i, 1,10 (-)
VIC t4 fUrff IID l-} T FIELD DATA FOR COMPARISON
ETH
Comynen A
!nz TCE A
T2E OCE 4
F1PE VC ETH #
a
PCET[ESCE VC #
I. (-7 PcEcunc.{mg27
1. TCE C— (my-)
yC-Iffi eni T C IDCECone.:Mpew
half-life r�l "IeI VCCgne (mg2)
3.50 ETH Conn- (mg'L}
D,D2 100 Dslance from' ' R)
lD0 ❑ate Dpte Cnllr�M 2023
100 0. CIIWSE TYPE OF 9IITPD7 TO SEE
IF r-] Help
R�1ore
1EE RUN CENTERLINE RUN ARRAY
5'EE OUIPIfT I Paste LMprplect
���AAA00000
t10tIAtI�tIAtIAtIAtIAtIOtIAtIOtIA
tl�tl�tl�tl�tl�tl�tl�tlOtl�tIOtIA
m��00000000
a®mtl®tl®tl®tl®tl®tl®®�
EHS Support LLC 7

Client Name:
Site Location:
Project No.
:I
Bakelite Synthetics
Acme, NC
LLC.03536.2021
Nitrate - Calibration Output, where PCE represents ammonia
DISSOLVED CHLORNATED SOLVENT CONCENTRATIONS ALONG PLUME CENTERLINE JmgtLi at Z-D
Distance from Source (ft)
PCE
0 1 45
9❑ 135 1&0 225
270 315 360
405
459
No DefiFadat-1
490.0DD I 2M22333
194.018 137.598 91.E-81 53.229
25.E-81 9.754 2.9D2
0.656
0.105
131,11 f-ation
489.9998 57.031
9.108 1.264 0.207 0.035
0.0% 0.001 0.000
0.000
0.909
Monitoring Well Locations{fti
0 50 90 155 200 250 300 WO 450
500
Field gala Fram Sile 490.000 0.000 8.800 o-. UGG O.o-o-0 0.000 0.000 o.GG a.aua 0.0a
0.000
ENO D�ad�bNAotl cn -Sequ td 1s ONer Decay o Fp Det f- Sip
7000.000
_
See PCE
J 100.000 -- -
7 g
see TCE
10.000 -5
`a so
1A00 5
See DCE
�r 0.100 45D
acc
See VC
0.010
L7
0.001
0 100 200 300 40C Wo 600
See ETH
Distance From SoUme (fk)
Time_
}0 years
�Inpotm
Prepare An imatlon TO All TO
UShe
Array
Lo
Nitrate - Plume Calibration Output, where TCE represents nitrate
D[S SOLVED CHLORINATED SOLVENT CONCENTRATIONS ALONG PLUME CENTERLINE img1Q at Z-1)
Distance from Source {fti
TCE 0 1 45 90 135 130 225 270 315 360 405
450
No Degrad.ti-1
0.010 1 0.023 1 0.016 0.011 0.007
0.004
O.0D2
0.091
❑.CDo
0.000
0.000
B.A.naTarmativn
0.11404 86.213 14.220 2.266 0.17a
0.063
0.011
0.002
❑.0UG
D.o-o-a
D.DUu
Monitoring
D 50 90 155 200
Well Locations(ft)
250 30D 354 40D 450
500
F101 Data from Site 0.040 0190 12.600 0.000 0.09G
0.000 0.o-0o- O.o-oo- 0.000
�No f>�s�bNProd�r �Se9uerRiel lstDNer moray o EJd De�tmm Sip
g❑.0❑❑
J
See PCE
m 10.000
See TCE
1 000
ASee
DCE
31 0.100
See VC
� 0.010
U
0 001
0 100 200 300 400 500 60D
See ETH
Distance From Source (k)
Time:
ReWmto
1�
Prepare Animation uv.tect iv All
InPul
iv Array
Lo Sheet
EHS Support LLC

Client Name: Site Location: Project No.
Bakelite Synthetics Acme, NC LLC.03536.2021
Nitrate — Plume Extent Output, where PCE represents ammonia and TCE represents nitrate
BIOCHLOR Natural Attenuation Decision Support System I Bakelite I Dala InPlIt IFT13trUCti011 St
Ammonia -> Nitrate 3?23 115 1. Enter value direody or
Egoel 2444 2. CalculaSe by filling in gray
TYPE OF CHLORINATE❑ 5f]LtlEAfr: LL� Et.GENERAL M nes 152 cells. Press Enter, then
............. E h.a..n.e..s ............... :Simulation Time' yr) i hit
[ModeledZea Width' riabi-e' Data used direct) in model.
Seepage Velocity' Vs Modeled Area Length' Teg if Natural Att-nuatnn
2o,, I Length' jotans!ormarV Scneninq Pmw�?
Hydraulic Co 2 Length' Zzn� 2- iB
"cluoduity K I—) L I s D.urrinq
Hydraulic Gradient i .04
, ft) . . . . . . . . . .. . . . . . . . . . . . . . . . . .. . . . . . . . . . ... Vertical Plane S-2 Source IM41
.......................................Effective Porosity .. .......... ...... 6. SOURCE DATA TYPE: Continuous
Loulim and Input SalYem Ca"nenimtom
2- DISPERSIONS.— Options N Single Planar
Alpha
[Alpha Alpha Source Thickness in Sat. Zone' (Ft)
(Alpha
1E-02
yl
(Ft,
Retardation F-W,— - R k.'
or r
Cone. (mgk)' Cl ILL-
SDU Sulk Density, rho (kglL) PCE 480.0 0
Fra ction Organ ioCarb on. foe TCE 0 View of Plume Looking Down
Partition Coefficient Koo i DCE 0
PCE 0 Obseerued Centerline Conc. at Monitoring Wells
.ETH
TCE
DCE �L�kkgg� 1 1.10 1 H
VC �,fl L 1 1.10 '7- FIELD DATA V66 COMPARI N
ETH
1a
(L
I , 1.10
H
. PCE Conc. (mg?L)
Co— R (used in r—dell
j TCE Conc. (mg?L)
C BIOTRANSFORMATICI,t
Order 0—.,C.cfficic.t
DCE Conc. (mg?L)
zon<=
L (Vqr)
YieldJJL
VC Conc. (mg?L)
PCE TCE
'0
06 3.60
ETH Con.. (mg7!-)
TCE DCE
3a.654
E
0.02
1.00[Distance
from Source (ft)
rit-,E
VC
0.000
C-
E
1.00 :Date Data Collected 2423
ETH
0.000
1.00 8- CHOOSE TYPE OF OUTPUT TO -SEE-
Zone�
i (119r)
'--
0 Help
Restore
RESET
PLE
T---E
TCE
DCE
k,270 10
RUN CENTERLINE RUN ARRAY
Fa"ulas
L,CE
VC
F-c—,"-1 C-
SEE OUTPUT
p -'o Un,&.A
ETH
1 0.000
EHS Support LLC 9

Client Name: Site Location: Project No. -a
Bakelite Synthetics Acme, NC WLLC.03536.2021
Nitrate — Plume Extent Output, where PCE represents ammonia
DISSOLVED CHLORINATED SOLVENT CONCENTRATIONS ALONG PLUME CENTERLINE (mglL) at Z-D
PCE
............................... Na Degradatiai
.. ............. .
BiotrenaFormatioi
I.ttSFITS-7<Tl.T.'iY�RT^fr: li
����
r r
r r
rrr
r rrr
r rrr
r rrr
r r
—Na oeyraaao.Nrr.a.�mn—sey.ea�it�om.rDe�ay � F��rtn�rram s�
000.000
See PCE
a100.000 — S16
? See TCE
e
10.000
0
1.000 See UCE
u0.100 See VC
p 0.010
[.1 See ETH
0 001
9 109 200 31I0 400 500 600
Distance From Source (ft.)
Tlm
Prere Anlmadon J u9+-4-0✓Years Un prated Re[um to To All To Arra
Sheel Input
Nitrate — Plume Extent Output Parameters, where TCE represents nitrate
TICE
No Deg retlatiar
i BwtransFormatiar
DISSOLVED CHLORINATED SOLVERT CONC ENTRATIONS ALONG PLUME CLNTERLgtE {rngfL) at Z—D
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