WQ0038087_Modification_20230728

Initial Review
Reviewer nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
Permit Number (IR) * WQ0038087
Applicant/Permittee Terra Renewal Services, Inc
Applicant/Permittee Address P.O. Box 1746 Watkinsville, GA 30677
Is the owner in BIMS? Yes , No Is the facility in BIMS?
Owner Type
Facility Name
County
Fee Category Major
Is this a complete application?*
Yes No
Signature Authority
Signature Authority Title
Signature Authority Email
Document Type (if non -application)
Email Notifications
Organization
Terra Renewal Services Class B Residuals Program
Wilkes
Does this need review by the hydrogeologist? * Yes No
Regional Office
CO Reviewer
Admin Reviewer
Fee Amount
Complete App Date
07/28/2023
Yes No
$395
Below list any additional email address that need notification about a new project.
Email Address
Comments to be added to email notfication
Comments for Admin
Comments for RO

Comments for Reviewer
Comments for Applicant

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* David C. Coyle
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
479-747-8192
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation High -Rate Infiltration
Other Wastewater Reclaimed Water
Closed -Loop Recycle Residuals
Single -Family Residence Wastewater Other
Irrigation
Permit Number:*
WQ0038087
Has Current Existing permit number
Applicant/Permittee*
Terra Renewal Services, Inc
Applicant/Permittee Address*
P.O. Box 1746 Watkinsville, GA 30677
Facility Name*
Terra Renewal Services Class B Residuals Program
Please provide comments/notes on your current submittal below.
Attached is an application for modification of RLAP permit WQ0038087 based in Wilkes Co. The permittee is Terra Renewal Services. The main
contact is David Coyle: [e-mail] OR [e-mail]. Phone # is 479-747-8192. A check in the amount of $395
is being sent express mail via USPS and should arrive by 7/26. Please contact if any questions or complications. Thanks.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
NC_WQ0038087_RLAP_Terra Renewal_2023 Mod.pdf 14.41MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature

Submission Date 7/24/2023

TERRA
renewal
July 24, 2023
Nathaniel Thornburg; Unit Supervisor
Non -Discharge Branch
Division of Water Resources
North Carolina Department of Environmental Quality
9th Floor; Office 942W
512 N. Salisbury Street
Raleigh, NC 27604-1170
East Region Environmental Office
P.O. Box 1746
Watkinsville, GA 30677
phone [phone]
RE: APPLICATION FOR MODIFICATION OF NON -DEDICATED LAND APPLICATION PERMIT
Permit #: WQ0038087
Permittee: Terra Renewal Services, Inc
Land Site Location: Wilkes & Yadkin Counties
Dear Mr. Thornburg,
This document is intended to supply the necessary information for modification of existing Non -Dedicated
RLAP Permit # WQ0038087 for land sites in Wilkes & Yadkin Counties. The Permittee is Terra Renewal
Services, Inc of Dardanelle, Arkansas. The PDF copy of the application is "book marked" to facilitate
navigation.
This permit application was prepared and submitted by:
David C. Coyle; LSS
Senior Environmental Manager, Terra Renewal
P.O. Box 1746
Watkinsville, GA 30677
[phone]
david.covlea-terrarenewal.com
The following items are provided:
• Copy of Permit # WQ0038087
• Registered Land Application Program Form (RLAP 06-16)
• Residuals Source Certification Form (RSC 06-16)
• Operation & Maintenance Plan (NO revisions since last submittal — 2020 renewal)
• Land Application Site Certification Form (LASC 06-16)
• Landowner Agreement and Setback Waiver Forms
• Land Application Area & Setback Maps
• Soils & Agronomy Report
Supporting documentation is provided with each item where necessary to meet requirements of North
Carolina regulation 15A NCAC 02T. The O&M Plan for land application has not been modified since
issuance of the last permit modification in April 2022.

Page 2
Cover Letter
WQ0038087
2023 Mod
This modification consists of the addition of one (1) new land application site (farm fields) totaling 51.1 net
(spreadable) acres. It also includes the addition of one (1) new residuals generating facility (Tyson -
Danville, VA) and the deletion of one (1) existing residuals generating facility (Innospec Chemicals -
Salisbury, NC). Amounts of annual dry tons to be certified per source have been revised based on
calculations from current analytical data and land application records.
To ensure timely response, please send all correspondence regarding the review process to the
following:
david.covle0terrarenewal.com or P.O. Box 1746. Watkinsville. GA 30677
Your attention to the review of this application is greatly appreciated. Please contact me immediately if
you require further information or have any questions.
Sincerely,
David C. Coyle
Senior Environmental Manager

V'� .
'w
fV
TERRA
renewal
PO BOX 399 • DARDANELLE • ARKANSAS • 72834
479.747.8192
terrarenewal.com
APPLICATION FOR PERMIT MODIFICATION
Residuals Land Application Program
(RLAP - Non -Dedicated)
Permit #: WQ0038087
WILKES & YADKIN COUNTIES
July 2023
Permittee:
TERRA RENEWAL SERVICES, INC
Contact:
David C. Coyle LSS, ccA
Senior Environmental Manager
P.O. BOX 1746
WATKINSVILLE, GA 30677

SECTION 1:
COPY OF PERMIT #:
WQ0038087

ROY COOPER
Governor
MICHAEL S. PEGAN
Secretary
S. DANIEL SMITH
Director
NORTH CAROLINA
Environmental Quality
February 4, 2021
DAVID C. COYLE — ENVIRONMENTAL MANAGER
TERRA RENEWAL SERVICES, INC.
POST OFFICE BOX 1746
WATKINSVILLE, GEORGIA 30677
Subject: Permit No. WQ0038087
Terra Renewal Services RLAP
Land Application of
Class B Residuals
Wilkes County
Dear Mr. Coyle:
In accordance with your permit renewal and major modification request received August 6, 2020,
and subsequent additional information received November 18, 2020, we are forwarding herewith Permit
No. WQ0038087 dated February 4, 2021, to Terra Renewal Services, Inc. for the construction and operation
of the residuals storage structures at the Mathis-1 facility listed in Attachment A, and continued operation
of the subject residuals management program.
Modifications to the subject permit are as follows:
➢ Increase of the permitted dry tonnage per year (DT/yr) for the Hunter Farms — High Point
facility from 450 to 700 DT/yr.
➢ Due to property line changes, the acreages for certain fields have been modified to reflect the
removal of some setbacks.
➢ Fields WK-MF-23A and 23B have been combined, WK-MRF-20A and 20B have been
combined. Fields WK-YF-0513 and YK-YF-05A have been combined to become the cross -
county field WK-YK-YF-05, with the soil type becoming Fairview.
➢ Construction of the MATHIS-1 storage facility consisting of two 1,053,622 gallon sludge
storage tanks for long term residuals storage. These tanks shall be located in a
containment/berm area which provides 1,988,558 gallons of containment volume.
This permit shall be effective from the date of issuance through November 30, 2027, shall void
Permit No. WQ0038087 issued February 12, 2016, and shall be subject to the conditions and limitations as
specified therein. The Permittee shall submit a renewal application no later than June 3, 2027.
Please pay particular attention to the monitoring requirements listed in Attachment A for they may
differ from the previous permit issuance. Failure to establish an adequate system for collecting and
maintaining the required operational information shall result in future compliance problems.
D E Q North Carolina Department of Environmental Quality I Division of Water Resources
512 North Salisbury Street 1 1617 Mail Service Center I Raleigh, North Carolina 27699-1617
o.�lmm^I m ury 919.707.9000

Mr. David C. Coyle
February 4, 2021
Page 2 of 3
Please note that on September 1, 2018, North Carolina Administrative Code Title 15A Subchapter
02T — Waste not Discharged to Surface Waters was readopted. Accordingly, this permit incorporates the
requirements of these rules, therefore, please take the time to review this permit thoroughly.
The Division has removed the following permit conditions since the last permit issuance dated
February 12, 2016:
➢ Old Condition III.10. — This condition has been removed because it is covered by the new
Condition III.1O.h.
➢ Old Condition 111.11.h. — Soil pH requirements for land application have been removed.
➢ Old Condition III.13. — This condition has been removed.
➢ Old Condition VL2. — This condition has been removed because this permit is not voidable.
The following permit conditions are new since the last permit issuance dated February 12,
2016:
➢ Condition I.I. — Upon completion of construction and prior to operation of the permitted
storage sites, the Permittee shall submit an engineering certification from a North Carolina
licensed Professional Engineer certifying the facility.
➢ Condition 12. — The Permittee shall notify the Winston-Salem Regional Office at least two
business days in advance of initial operation of the constructed facilities.
➢ Condition 1.3. — Gauges to monitor waste levels in the two 1,053,622 gallon above ground
sludge storage tanks shall be installed prior to operation
➢ Condition II.8. — Setbacks have been updated to the most recent 15A NCAC 02T .1108(c)
setbacks. Setbacks for the storage tanks follow the most recent 02T . 1108(a) setbacks.
➢ Condition 111.10.1. — Residual land application may not occur if the land application sites are
located within a WS-1 watershed pursuant to 15A NCAC 02B .0212 or within the Critical Area
of a WS-II, WS-III, or WS-IV watershed.
➢ Condition 111.1I.e. — Dedicated land sites are to have public access restricted continuously
while the land is under permit and for one year afterward. Note, there are no dedicated land
sites in the current permit.
➢ Condition III.15. — Freeboard in the two 1,053,622 gallon above ground sludge storage tanks
shall not be less than two feet at any time.
➢ Condition III.16. — Gauges to monitor waste levels in the two 1,053,622 gallon above ground
sludge storage tanks shall be provided.
➢ Condition 111.17. — A protective vegetative cover shall be established and maintained on all
berms, pipe runs, erosion control areas, surface water diversions, and earthen embankments.
➢ Condition 111.18. — The Permittee shall prohibit public access to the residuals storage sites.

Mr. David C. Coyle
February 4, 2021
Page 3 of 3
➢ Condition IV.10. — Freeboard (i.e., waste level to the lowest embankment elevation) in the two
1,053,622 gallon above ground sludge storage tanks shall be measured to the nearest inch or
tenth of a foot, and recorded weekly. Weekly freeboard records shall be maintained for five
years, and shall be made available to the Division upon request.
➢ Condition IV.11. — The Permittee shall maintain records for the residuals storage sites.
➢ Condition VL6. — The Permittee shall retain a set of Division -approved plans and specifications
for the life of the facilities permitted herein.
➢ Condition VL7. — The Permittee shall maintain this permit until the proper closure of all
facilities permitted herein, or until the facilities permitted herein are permitted by another
authority.
➢ Condition VI.10. — This permit shall not be renewed if the Permittee or any affiliation has not
paid the required annual fee.
If any parts, requirements or limitations contained in this permit are unacceptable, the Permittee
has the right to request an adjudicatory hearing upon written request within 30 days following receipt of
this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North
Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service
Center, Raleigh, NC 27699-6714. Otherwise, this permit shall be final and binding.
One set of approved plans and specifications is being forwarded to you. If you need additional
information concerning this permit, please contact Erick Saunders at [phone] or
enckson. saunderskncdenr. gov.
Sincerely,
S. Daniel Smith, Director
Division of Water Resources
cc: Wilkes County Health Department (Electronic Copy)
Winston-Salem Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Brian P. Mullin, PE — Arete Engineering (Electronic Copy)
Beth Buffington — Protection and Enforcement Branch (Electronic Copy)
Laserfiche File (Electronic Copy)
Digital Permit Archive (Electronic Copy)

THIS PAGE BLANK

NORTH CAROLINA
ENVIRONMENTAL MANAGEMENT COMMISSION
DEPARTMENT OF ENVIRONMENTAL QUALITY
RALEIGH
LAND APPLICATION OF CLASS B RESIDUALS PERMIT
In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as
amended, and other applicable Laws, Rules, and Regulations
PERMISSION IS HEREBY GRANTED TO
Terra Renewal Services, Inc.
Wilkes County
FOR THE
construction and operation of residuals storage facility consisting of:
two 1,053,622 gallon synthetically lined above ground sludge storage tanks located in a containment/berm
area providing 1,988,558 gallons of containment volume; and all associated piping, valves, controls, and
appurtenances; and the
continued operation of a residuals management program for Terra Renewal Services, Inc. and consisting of
the land application of Class B residuals generated by the approved facilities listed in Attachment A to the
approved fields listed in Attachment B, with no discharge of wastes to surface waters, pursuant to the
application received August 6, 2020, subsequent additional information received November 18, 2020, and
in conformity with the Division -approved plans and specifications, and other supporting data subsequently
filed and approved by the Department of Environmental Quality and considered a part of this permit. The
disposal of residuals is regulated under Title 40 Code of Federal Regulations Part 257. This permit does
not exempt the Permittee from complying with Federal Regulation 40 CFR Part 257.
This permit shall be effective from the date of issuance through November 30, 2027, shall void Permit No.
WQ0038087 issued February 12, 2016, and shall be subject to the following conditions and limitations:
I. SCHEDULES
Upon completion of construction and prior to operation of this permitted facility, the Permittee shall
submit an engineering certification from a North Carolina licensed Professional Engineer certifying
that the permitted facility has been constructed in accordance with G.S. 143-215.1, Administrative
Code Title 15A Subchapter 02T, this permit, and the Division -approved plans and specifications. For
phased and partially certified facilities, the Permittee shall retain the responsibility to track further
construction approved under this permit, and shall provide a final engineering certification upon project
completion. Mail the Engineering Certification to the Division of Water Resources, Non -Discharge
Branch, 1617 Mail Service Center, Raleigh, NC 27699-1617, or Non-Discharge.Reports&ncdenr.gov.
[15A NCAC 02T .0116(a)]
2. The Permittee shall notify the Winston-Salem Regional Office, telephone number [phone], at
least two business days in advance of initial operation of the constructed facilities so that the Division
can conduct a startup inspection. [15A NCAC 02T .0108(b)(1)(B)]
WQ0038087 Version 2.0 Shell Version 200201 Page 1 of 15

3. Gauges to monitor waste levels in the two 1,053,622 gallon above ground sludge storage tanks shall be
installed prior to operation. Caution shall be taken not to damage the integrity of any liner (if present)
when installing a gauge. [15A NCAC 02T .0108(b)(1)(B)]
4. The Permittee shall request renewal of this permit on Division -approved forms no later than June 3,
2027. [15A NCAC 02T .0105(b), 02T .0109]
II. PERFORMANCE STANDARDS
The Permittee shall maintain and operate the subject residuals management program so there is no
discharge to surface waters, nor any contravention of groundwater or surface water standards. In the
event the residuals management program fails to perform satisfactorily, including the creation of
nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease
land applying residuals, take immediate corrective actions, and contact the Winston-Salem Regional
Office supervisor. [15A NCAC 02T .0108(b)(1)(A)]
2. This permit shall not relieve the Permittee of their responsibility for damages to groundwater or surface
water resulting from the operation of this residuals management program. [15A NCAC 02T
.0108(b)(1)(A)]
3. Only residuals generated by the facilities listed in Attachment A are approved for land application in
accordance with this permit. [15A NCAC 02T .1101]
4. Only the fields listed in Attachment B are approved for residuals land application. [G.S. 143-
215.1(a)(9)]
5. Pollutant concentrations in residuals land applied to the sites listed in Attachment B shall not exceed
the following Ceiling Concentrations or Cumulative Pollutant Loading Rates (CPLRs), on a dry
weight basis:
Parameter
Ceiling
Concentration
Cumulative Pollutant Loading Rates
(mg/kg)
(kg/ha)
(lbs/ac)
Arsenic
75
41
36
Cadmium
85
39
34
Copper
4,300
1,500
1,338
Lead
840
300
267
Mercury
57
17
15
Molybdenum
75
N/A
N/A
Nickel
420
420
374
Selenium
100
100
89
Zinc
7,500
2,800
2,498
The Permittee shall determine compliance with the CPLRs using one of the following methods:
a. By calculating the existing cumulative level of pollutants using actual analytical data from all
historical land application events of residuals, or
b. For land where residuals application has not occurred or for which the required data is incomplete,
by determining background concentrations through representative soil sampling.
[15A NCAC 02T .I105(a), 02T .I105(b)]
WQ0038087 Version 2.0 Shell Version 200201 Page 2 of 15

6. Class B biological residuals shall meet the pathogen reduction requirements in 15A NCAC 02T .1106
(b). Exemptions to this requirement shall be specified in Attachment A. [15A NCAC 02T .1106(b),
02T .I 106(d)]
7. Class B biological residuals shall meet one of the vector attraction reduction alternatives in 15A NCAC
02T .1107(a). Exemptions to this requirement shall be specified in Attachment A. [15A NCAC 02T
.1107(a), 02T .I 107(c)]
8. The facilities and sites herein were permitted per the following setbacks:
a. Setbacks for Class B land application sites are as follows (all distances in feet):
i. Each habitable residence or place of assembly
under separate ownership:
ii. Each habitable residence or places of assembly
owned by the Permittee, the owner of the land,
or the lessee or operator of the land:
In. Each property line:
iv. Public right of way:
v. Each private or public water supply source:
vi. Surface waters such as intermittent and
perennial streams, perennial waterbodies, and
wetlands:
vii. Surface water diversions such as ephemeral
streams, waterways, and ditches:
viii. Groundwater lowering ditches where the
bottom of the ditch intersects the SHWT:
ix. Subsurface groundwater lowering systems:
x. Each well with exception of monitoring wells:
xi. Bedrock outcrops:
xii. Top of slope of embankments or cuts of two
feet or more in vertical height:
xiii.Each building foundation or basement:
xiv. Each water line:
xv. Nitrification field:
Surface Irrigation Injection /
Application Surface
by Vehicle Application Incorporation
400
400
200
0
200
0
50 1,2
150 1,2
50'°2
50
50
50
100
100
100
32.8
32.8
32.8
25
25
25
25
100
25
0
100
0
100
100
100
25
25
25
15
15
15
0
15
0
0
10
0
0
20
0
' Setbacks to property lines are not applicable when the Permittee, or the entity from which the
Permittee is leasing, owns both parcels separated by the property line.
WQ0038087 Version 2.0 Shell Version 200201 Page 3 of 15

2 Per setback waivers recorded in the Wilkes and Yadkin Counties Register of Deeds, reduced
setbacks from the Class B land application site to any property line are as follows:
Field
County
Parcel No.
DB / Page
Setback
Easement
NC-WK-MF-11
Wilkes
0100606
01317 / 0055
0 feet
50 feet
NC-WK-MF-11
Wilkes
0100732
01322 / 0180
0 feet
50 feet
NC-WK-MF-11
Wilkes
0100737
01322 / 0179
0 feet
50 feet
NC-WK-MF-15
Wilkes
0100990
01317 / 0056
0 feet
50 feet
NC-WK-MF-15
Wilkes
0100991
01322 / 0181
0 feet
50 feet
NC-WK-MF-23
Wilkes
0100821
01317 / 0057
0 feet
50 feet
NC-WK-MF-23
Wilkes
0100131
01317 / 0058
0 feet
50 feet
NC-WK-MF-23
Wilkes
0100317
01322 / 0182
0 feet
50 feet
NC-WK-MF-23
Wilkes
0100266
01322 / 0183
0 feet
50 feet
NC-WK-MF-23
Wilkes
0100148
01322 / 0184
0 feet
50 feet
NC-WK-MF-23
Wilkes
0100149
01322 / 0185
0 feet
50 feet
NC-WK-RJ-02
Wilkes
0601666
01317 / 0059
0 feet
50 feet
NC-WK-RJ-05
Wilkes
0605291
01317 / 0060
0 feet
50 feet
NC-WK-YK-DM-03
NC-WK-YK-DM-07
NC-WK-YK-DM-08
Wilkes
1700289
01317 / 0054
0 feet
50 feet
NC-WK-YK-DM-07
NC-WK-YK-DM-08
Yadkin
484400359744
01304 / 0034
0 feet
50 feet
NC-WK-YK-DM-03
NC-WK-YK-DM-07
NC-WK-YK-DM-08
Yadkin
484400562719
01304 / 0036
0 feet
50 feet
[15A NCAC 02T .1108(c)]
b. The setbacks for residual storage and treatment units originally permitted or modified on or after
September 1, 2018 are as follows (all distances in feet):
I. Each habitable residence or place of assembly under separate ownership: 1001
ii. Each private or public water supply source: 100
iii. Surface waters such as intermittent and perennial streams, perennial waterbodies, 50
and wetlands:
iv. Each well with exception of monitoring wells:
v. Each property line:
100
50
' Habitable residences or places of assembly under separate ownership constructed after the
facilities herein were originally permitted or subsequently modified are exempt from this
setback.
2 Setbacks to property lines are not applicable when the Permittee, or the entity from which the
Permittee is leasing, owns both parcels separated by the property line.
[15A NCAC 02T .1108(a), 02T .1108(f), 02T .1108(g)]
10. Class B land application areas shall be clearly marked on each site prior to and during any residuals
application event. [15A NCAC 02T .0110(g)]
WQ0038087 Version 2.0 Shell Version 200201 Page 4 of 15

11. Residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance of
agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen requirements
based on the determined Realistic Yield Expectations (RYE) using any of the following methods:
a. Division's pre -approved site specific historical data for specific crop or soil types by calculating
the mean of the best three yields of the last five consecutive crop harvests for each field.
b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State
University Department of Soil Science (http://nutrients.soll.ncsu.edl /yields/index.php). A copy
shall be kept on file and reprinted every five years in accordance with Condition IV.6.
c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE
and appropriate nutrient application rates reported in any of the following documents:
i. Crop management plan as outlined by the local Cooperative Extension Office, the North
Carolina Department of Agriculture and Consumer Services, the Natural Resource
Conservation Service, or other agronomist.
ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group -Guidance
Document: Chapter 1
(http://www.ncagr.gov/SWC/tech/documents/9th Guidance Doc 100109.pdf).
In. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation
Services (MRCS). These plans must meet the USDA-NRCS 590 Nutrient Management
Standards(ftp://ftp-fc.sc.egov.usda.gov/NHQ/practice-standards/standards/590.pdf).
d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall
contact the Division to determine necessary action.
[15A NCAC 02T . I 109(a)(1)(K)]
12. When residuals are land applied to grazed pasture, hay crop realistic nitrogen rate shall be reduced by
25%. [15A NCAC 02T .0108(b)(1)(A)]
13. If residuals land application sites are to be over -seeded or double -cropped (e.g., bermuda grass in the
summer and rye grass in the winter with both crops to receive residuals), then the second crop can
receive an application of PAN at a rate not to exceed 50 pounds per acre per year (lbs/ac/yr). This
practice may be allowed as long as the second crop is to be harvested or grazed. If the second crop is
to be planted for erosion control only and is to be tilled into the soil, then no additional PAN shall be
applied. [15A NCAC 02T .0108(b)(1)(A)]
14. Prior to land application of residuals containing a sodium adsorption ratio (SAR) of 10 or higher, the
Permittee shall obtain and implement recommendations from at least one of the following: the local
Cooperative Extension Office; the Department of Agriculture and Consumer Services; the Natural
Resource Conservation Service; a North Carolina Licensed Soil Scientist; or an agronomist. The
recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a
mechanism for maintaining site integrity and conditions conducive to crop growth. The Permittee shall
maintain written records of these recommendations and details of their implementation. [15A NCAC
02T .0108(b)(1)(A)]
15. Residuals land application fields permitted on or after December 30, 1983 have a compliance boundary
that is either 250 feet from the residual land application area, or 50 feet within the property boundary,
whichever is closest to the residual land application area. Any exceedance of groundwater standards
at or beyond the compliance boundary shall require corrective action. Division -approved relocation of
the compliance boundary shall be noted in Attachment B. Multiple contiguous properties under
common ownership and permitted for use as a disposal system shall be treated as a single property with
regard to determination of a compliance boundary. [15A NCAC 02L .0106(d)(2), 02L .0107(b), 02T
.0105(h), G.S. 143-215.1(1), G.S. 143-215.1(k)]
WQ0038087 Version 2.0 Shell Version 200201 Page 5 of 15

16. The review boundary is midway between the compliance boundary and the residual land application
area. Any exceedance of groundwater standards at or beyond the review boundary shall require
preventative action. [15A NCAC 02L.0106(d)(1), 02L .0108]
17. The use of frac tanks is authorized to aid in staging of application of the injection of residuals. However,
the use of frac tanks shall not be used for the purpose of offsite storage for more than 48 hours, and
should nuisance odor problems arise as a result of the use of the frac tanks, these shall no longer be
used. Under no conditions are the frac tanks to be used for storage of residuals between the crop harvest
period and shortly before planting of crops. [15A NCAC 02T .0108(b)(1)(A)]
III. OPERATION AND MAINTENANCE REOUIREMENTS
1. The Permittee shall operate and maintain the residuals management program as anon -discharge system.
[15A NCAC 02T .1100]
2. The Permittee shall notify the Winston-Salem Regional Office, telephone number [phone], and
the appropriate local government official (i.e., county manager, city manager, or health director) at least
two business days in advance of a site's initial residuals land application event. [15A NCAC 02T
.0108(b)(1)(A)]
3. The Permittee shall notify the Winston-Salem Regional Office, telephone number [phone], at
least one business day in advance of conducting any land application activity. Notification shall include
the anticipated application date, time, and field name as listed in Attachment B. Exceptions to this
requirement shall be approved by the Winston-Salem Regional Office. [15A NCAC 02T
.0108(b)(1)(A)]
4. The Permittee shall maintain a Division -approved Operation and Maintenance Plan that shall include:
a. Description of the program, and associated facilities and equipment, in sufficient detail to show
what operations are necessary for the program to function and by whom the functions are to be
conducted;
b. Description of anticipated maintenance of facilities and equipment associated with the program;
c. Include provisions for safety measures, including restriction of access to sites and equipment;
d. Spill control provisions:
I. Response to upsets and bypasses including control, containment, and remediation; and
ii. Contact information for plant personnel, emergency responders, and regulatory agencies;
e. Detailed inspection procedures:
I. Names or titles of personnel responsible for conducting inspections;
ii. Frequency and location of inspections, and procedures to assure that the selected locations and
inspection frequency are representative of the residuals management program; and
iii. Description of record keeping and actions to be taken by the inspector in the event that
noncompliance is observed;
f Detailed sampling and monitoring procedures:
I. Names or titles of personnel responsible for conducting sampling and monitoring;
ii. Description of monitoring procedures including parameters to be monitored; and
iii. Sampling frequency and procedures to assure that representative samples are collected.
Fluctuation in temperature, flow, and other operating conditions can affect the quality of the
residuals gathered during a particular sampling event. The sampling plan shall account for any
foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to
meet pathogen and vector attraction reduction requirements.
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[15A NCAC 02T .I I I0(a)]
Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC)
classification of the residuals management program, the Permittee shall designate and employ a
certified operator in responsible charge (ORC), and one or more certified operators as back-up ORCs.
The ORC or their back-up shall visit the facilities in accordance with 15A NCAC 08G 0204 and shall
comply with all other requirement in 15A NCAC 08G 0204. [15A NCAC 02T .0117, 08G .0204]
6. The Permittee shall ensure that a copy of this permit and the Division -approved Operation and
Maintenance Plan is available when land applying residuals. [15A NCAC 02T .1110(b)]
7. The Permittee shall ensure that spill control provisions are available when transporting or land applying
residuals. [15A NCAC 02T .1110(a)(4)]
8. Class B residuals shall not be stored or staged at any land application site without prior written approval
from the Division. Class B residuals approved for storage shall be stored or staged in a manner to
prevent runoff of leachate and other wastewaters generated. [15A NCAC 02T .1110(c), 02T .1110(e)]
9. Adequate measures shall be taken to prevent wind erosion and runoff from the land application sites
listed in Attachment B. [15A NCAC 02T .0108(b)(1)(A)]
10. Class B residuals shall not be land applied under the following conditions:
a. If the residuals are likely to adversely affect a threatened or endangered species listed under section
4 of the Endangered Species Act or its designated critical habitat;
b. If the application causes nuisance conditions;
c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface
water or groundwater standards;
d. If the land is flooded, frozen, or snow-covered, or is otherwise in a condition such that runoff of
the residuals would occur;
e. Within the 100-year flood elevation, unless the residuals are injected or incorporated within a 24-
hour period following a residuals land application event;
£ During precipitation events, or within 24 hours following a rainfall event of 0.5 inches or greater
in a 24-hour period;
g. If the slope of the land is greater than 10% when liquid residuals are surface applied, or if the slope
of the land is greater than 18% when liquid residuals are injected or incorporated;
h. If the land does not have an established vegetative cover crop unless the land is a Division -approved
no -till site, or the residuals are injected, or incorporated within a 24-hour period following the
application of residuals;
i. If the vertical separation of the seasonal high water table and the depth of residuals application is
less than one foot;
j. If the vertical separation of the depth to bedrock and the depth of residuals application is less than
one foot;
k. If the application exceeds agronomic rates; or
1. If the land application sites are located within a WS-I watershed pursuant to 15A NCAC 02B .0212
or within the Critical Area of a WS-II pursuant to Sub -Item (4)(g) of Rule 15A NCAC 02B .0212,
or within the Critical Area of a WS-III or WS-IV watershed pursuant to Sub -Item (4)(h) of Rules
15A NCAC 02B .0215, and .0216.
[15A NCAC 02T .I109(a)(1)]
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11. Class B land application sites shall have the following public access restrictions:
a. Public access to public contact sites shall be restricted for one calendar year after a residuals land
application event;
b. Public access to non-public contact sites shall be restricted for 30 days after a residuals land
application event;
c. Public access to land associated with a dedicated land application site shall be restricted
continuously while the land is permitted for active use, and for one calendar year after the final
land application of residuals.
[15A NCAC 02T .1109(a)(2)]
12. Class B land application sites shall have the following harvesting and grazing restrictions:
a. Animals shall not be allowed to graze on land for 30 calendar days after any land application of
residuals;
b. Food crops, feed crops, and fiber crops shall not be harvested for 30 calendar days after any land
application of residuals;
c. Food crops with harvested parts that touch the mixture of residuals and soil and are totally above
the land surface shall not be harvested for 14 months after any land application of residuals;
d. Food crops with harvested parts below the land surface shall not be harvested for 20 months after
any land application of residuals if the residuals remain on the land surface for four months or
longer prior to incorporation into the soil;
e. Food crops with harvested parts below the land surface shall not be harvested for 38 months after
any land application of residuals if the residuals remain on the land surface for less than four months
prior to incorporation into the soil; and
f Turf grown on land where residuals are applied shall not be harvested for one calendar year after
any land application of residuals.
[15A NCAC 02T .1109(a)(3)]
13. The Permittee shall acquire from each landowner or lessee/operator a statement detailing the volume
of other nutrient sources (i.e., manufactured fertilizers, manures, or other animal waste products) that
have been applied to the site, and a copy of the most recent Nutrient Management Plan (NMP) for those
operations where a NMP is required by the US Department of Agriculture — National Resources
Conservation Service (MRCS) or other State Agencies. The Permittee shall calculate allowable nutrient
loading rates based on the provided information and use appropriate reductions.
For the purpose of this permit condition, a Crop Management Plan (CMP), Waste Utilization Plan
(WUP) or Certified Nutrient Management Plan (CNMP) shall also be considered a Nutrient
Management Plan. [15A NCAC 02T .0108(b)(1)(A), 02T .1104(c)(3)]
14. Class B residuals shall not be land applied to the fields listed in Attachment B unless the Landowner
Agreement between the Permittee and the respective field owners or lessees/operators of the land
application site is valid. The Landowner Agreements shall expire concurrent with the permit expiration
date of November 30, 2027. [15A NCAC 02T .1104(c)(4)]
15. Freeboard in the two 1,053,622 gallon above ground sludge storage tanks shall not be less than two feet
at any time. [15A NCAC 02T .0108(b)(1)(A)]
16. Gauges to monitor waste levels in the two 1,053,622 gallon above ground sludge storage tanks shall be
provided. These gauges shall have readily visible permanent markings, at inch or tenth of a foot
increments, indicating the following elevations: maximum liquid level at the top of the temporary liquid
storage volume; minimum liquid level at the bottom of the temporary liquid storage volume; and the
lowest point on top of the dam. [15A NCAC 02T .0108(b)(1)(A)]
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17. A protective vegetative cover shall be established and maintained on all berms, pipe runs, erosion
control areas, surface water diversions, and earthen embankments (i.e., outside toe of embankment to
maximum allowable temporary storage elevation on the inside of the embankment). Trees, shrubs, and
other woody vegetation shall not be allowed to grow on the earthen dikes or embankments. Earthen
embankments shall be kept mowed or otherwise controlled and accessible. [15A NCAC 02T
.0108(b)(1)(A)]
18. The Permittee shall prohibit public access to the residuals storage facilities. [15A NCAC 02T
.0108(b)(1)(A)]
IV. MONITORING AND REPORTING REQUIREMENTS
The Permittee shall conduct and report any Division required monitoring necessary to evaluate this
program's impact on groundwater and surface water. [15A NCAC 02T .0108(c)]
2. The residuals from each source generating facility shall be analyzed to demonstrate they are non-
hazardous under the Resource Conservation and Recovery Act (RCRA). Residuals that test or are
classified as a hazardous or toxic waste under 40 CFR Part 261 shall not be land applied. The analyses
(i.e., corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)) shall be
performed at the frequency specified in Attachment A, and the Permittee shall maintain these results
for five years. Any exemptions from the requirements in this condition shall be specified in Attachment
A. The TCLP analysis shall include the following parameters, and the Federal regulatory level (mg/L)
is in parentheses:
Arsenic (5.0)
1,4-Dichlorobenzene (7.5)
Nitrobenzene (2.0)
Barium (100.0)
1,2-Dichloroethane (0.5)
Pentachlorophenol (100.0)
Benzene (0.5)
I,1-Dichloroethylene (0.7)
Pyridine (5.0)
Cadmium (1.0)
2,4-Dinitrotoluene (0.13)
Selenium (1.0)
Carbon tetrachloride (0.5)
Endrin (0.02)
Silver (5.0)
Chlordane (0.03)
Heptachlor (and its epoxide)
(0.008)
Tetrachloroethylene (0.7)
Chlorobenzene (100.0)
Hexachlorobenzene (0.13)
Toxaphene (0.5)
Chloroform (6.0)
Hexachlorobutadiene (0.5)
Trichloroethylene (0.5)
Chromium (5.0)
Hexachloroethane (3.0)
2,4,5-Trichlorophenol (400.0)
m-Cresol (200.0)
Lead (5.0)
2,4,6-Trichlorophenol (2.0)
o-Cresol (200.0)
Lindane (0.4)
2,4,5-TP (Silvex) (1.0)
p-Cresol (200.0)
Mercury (0.2)
Vinyl chloride (0.2)
Cresol (200.0)
Methoxychlor (10.0)
2,4-D (10.0)
Methyl ethyl ketone (200.0)
Once the residuals have been monitored for two years at the frequency specified in Attachment A, the
Permittee may submit a permit modification request to reduce the frequency of this monitoring
requirement. In no case shall the monitoring frequency be less than once per permit cycle.
[15A NCAC 13A .0102(b), 02T. 110 1, 02T. 1105]
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3. The residuals from each source generating facility shall be analyzed at the frequency specified in
Attachment A, and the Permittee shall maintain the results for a minimum of five years. Each analysis
shall include the following parameters:
Aluminum
Mercury
Potassium
Ammonia -Nitrogen
Molybdenum
Selenium
Arsenic
Nickel
Sodium
Cadmium
Nitrate -Nitrite Nitrogen
Sodium Adsorption Ratio
(SAR)
Calcium
Percent Total Solids
TKN
Copper
pH
Zinc
Lead
Phosphorus
Magnesium
Plant Available Nitrogen
(by calculation)
[15A NCAC 02T .1101]
4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction
requirements at the frequency specified in Attachment A. The monitoring results shall specify the
stabilization process utilized, and demonstrate compliance with the Class B pathogen reduction
requirements in 15A NCAC 02T .1106(b), and one vector attraction reduction requirement in 15A
NCAC 02T .1107(a) shall be met. Any exemptions from the requirements in this condition shall be
specified in Attachment A. [15A NCAC 02T .1106(b), 02T .1107(a), 02T .1111(c)]
An annual representative soils analysis (i.e., Standard Soil Fertility Analysis) shall be conducted on
each land application site listed in Attachment B that received residuals during the calendar year. This
analysis shall be in accordance with the soil sampling guidance located in the Sampling Instructions
section of the NC Department of Agriculture & Consumer Services' website
(http://www.ncagr.gov/agronomi/pubs.htm). The Permittee shall maintain these results for a period of
no less than five years, and these results shall be made available to the Division upon request. Each
Standard Soil Fertility Analysis shall include the following parameters:
Acidity
Exchangeable Sodium Percentage
Phosphorus
Base Saturation (by calculation)
Magnesium
Potassium
Calcium
Manganese
Sodium
Cation Exchange Capacity
Percent Humic Matter
Zinc
Copper
pH
[15A NCAC 02T .0108(c), 15A NCAC 02T .1I I I(d)]
6. Representative samples of residuals that are prepared for land application shall be collected and
analyzed. [15A NCAC 02T .1111(a)]
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7. The Permittee shall maintain records for all residual land application events. These records shall
include the following:
a. Residuals source (as listed in Attachment A);
b. Date of application;
c. Location of land application (field name as listed in Attachment B);
d. Approximate acreage applied;
e. Method of application;
f. Weather conditions;
g. Dominant soil series;
h. Soil conditions;
i. Proposed crop;
j . Nitrogen Application Rate based on RYES;
k. Volume of residuals applied per acre in gallons, cubic yards, dry tons, or wet tons;
1. Volume of animal waste or other nutrient source applied per acre in gallons, cubic yards, dry tons,
or wet tons;
in. Volume of soil amendments applied per acre in gallons, cubic yards, dry tons, or wet tons; and
n. Annual and cumulative totals applied to each field for the following:
I. Class A and Class B residuals (dry tons per acre);
ii. Animal waste and other sources of nutrients (dry tons per acre);
iii. Heavy metals as specified in Condition IL3. (pounds per acre);
iv. Plant available nitrogen (pounds per acre); and
v. Phosphorus (pounds per acre).
[15A NCAC 02T .0108(c)]
8. One hard copy and one electronic copy of an annual report shall be submitted on or before March 1st
The annual report shall meet the requirements described in the Instructions for Residuals Application
Annual Reporting Forms. Instructions for reporting and annual report forms are available at
hLtp:Hdeg .nc. gov/about/divisions/water-resources/water-resources-permits/wastewater-branch/non-
discharge-permitting-unit/reporting-forms, or can be obtained by contacting the Non -Discharge Branch
directly. The annual report shall be submitted to the following address:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
[15A NCAC 02T .1I I I(d)]
9. Noncompliance Notification
The Permittee shall report to the Winston-Salem Regional Office, telephone number [phone],
within 24 hours of first knowledge of the:
a. Any process unit failure (e.g., mechanical, electrical, etc.) rendering the facility incapable of
adequate residual treatment.
b. Any failure resulting in a discharge to surface waters.
c. Any time self -monitoring indicates the program has gone out of compliance with its permit
limitations.
d. Land application of residuals abnormal in quantity or characteristic.
e. Any discharge from a vehicle or piping system transporting residuals.
Emergencies requiring reporting outside normal business hours shall call the Division's Emergency
Response personnel at telephone number [phone], [phone], or [phone]. All
noncompliance notifications shall file a written report to the Winston-Salem Regional Office within
five days of first knowledge of the occurrence, and this report shall outline the actions proposed or
taken to ensure the problem does not recur. [15A NCAC 02T .0108(b)(1)(A)]
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10. Freeboard (i.e., waste level to the lowest embankment elevation) in the two 1,053,622 gallon above
ground sludge storage tanks shall be measured to the nearest inch or tenth of a foot, and recorded
weekly. Weekly freeboard records shall be maintained for five years, and shall be made available to
the Division upon request. [15A NCAC 02T .0108(c)]
11. The Permittee shall maintain records for the residuals storage sites. These records shall include the
following:
a. Visual observations of the tanks and containment area site;
b. Residuals input source (as listed in Attachment A);
c. Date of residuals storage input;
d. Volume of residuals storage input;
e. Date of residuals storage withdrawal;
f. Volume of residuals storage withdrawal;
g. Date and estimated volume of rainfall discharges from the secondary containment; and
h. Record of preventative maintenance (e.g. changing of equipment, adjustments, testing inspections
and cleanings, etc.).
[15A NCAC 02T .0 1 08(b)(1)(A)]
V. INSPECTIONS
1. The Permittee shall perform inspections and maintenance to ensure proper operation of the Permittee's
storage, distribution, and application facilities. [15A NCAC 02T .1110(f)]
2. The Permittee shall inspect the Permittee's residuals processing, storage, transport, and application
facilities to prevent malfunctions, facility deterioration, and operator errors that may result in discharges
of wastes to the environment, threats to human health, or public nuisances. The Permittee shall maintain
an inspection log that includes the date and time of inspection, observations made, and maintenance,
repairs, or corrective actions taken. The Permittee shall maintain this inspection log for a period of five
years from the date of inspection, and this log shall be made available to the Division upon request.
[15A NCAC 02T .0108(b)(1)(A), 02T .1110(f)]
Division authorized representatives may, upon presentation of credentials, enter and inspect any
property, premises, or place related to the land application sites or facilities permitted herein at any
reasonable time for determining compliance with this permit. Division authorized representatives may
inspect or copy records maintained under the terms and conditions of this permit, and may collect
groundwater, surface water, or leachate samples. [G.S. 143-215.3(a)(2)]
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VL GENERAL CONDITIONS
1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to a
Division enforcement action. [G.S. 143-215.6A, 143-215.613, 143-215.6C]
2. This permit is effective only with respect to the nature and volume of wastes described in the permit
application, and Division -approved plans and specifications. [G.S. 143-215.1(d)]
3. Unless specifically requested and approved in this permit, there are no variances to administrative codes
or general statutes governing the construction or operation of the facilities permitted herein. [15A
NCAC 02T .0105(n)]
4. The issuance of this permit does not exempt the Permittee from complying with all statutes, rules,
regulations, or ordinances that other jurisdictional government agencies (e.g., local, state, and federal)
may require. [15A NCAC 02T .0105(c)(6)]
If the permitted residuals program change ownership, or the Permittee changes their name, the
Permittee shall submit a permit modification request on Division -approved forms. The Permittee shall
comply with all terms and conditions of this permit until the permit is transferred to the successor -
owner. [G.S.143-215.1(d3)]
6. The Permittee shall retain a set of Division -approved plans and specifications for the life of the facilities
permitted herein. [15A NCAC 02T .0105(o)]
7. The Permittee shall maintain this permit until the proper closure of all facilities permitted herein, or
until the facilities permitted herein are permitted by another authority. [15A NCAC 02T .01050)]
8. This permit is subject to revocation or modification upon 60-day notice from the Division Director, in
whole or part for:
a. violation of any terms or conditions of this permit or Administrative Code Title 15A Subchapter
02T;
b. obtaining a permit by misrepresentation or failure to disclose all relevant facts;
c. the Permittee's refusal to allow authorized Department employees upon presentation of credentials:
I. to enter the Permittee's premises where a system is located or where any records are required
to be kept;
ii. to have access to any permit required documents and records;
iii. to inspect any monitoring equipment or method as required in this permit; or
iv. to sample any pollutants;
d. the Permittee's failure to pay the annual fee for administering and compliance monitoring; or
e. a Division determination that the conditions of this permit are in conflict with North Carolina
Administrative Code or General Statutes.
[15A NCAC 02T .0110]
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9. Unless the Division Director grants a variance, expansion of the facilities permitted herein shall not
occur if any of the following apply:
a. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has been convicted of
environmental crimes under G.S. 143-215.6B, or under Federal law that would otherwise be
prosecuted under G.S. 143-215.6B, and all appeals of this conviction have been abandoned or
exhausted.
b. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has previously abandoned
a wastewater treatment facility without properly closing the facility.
c. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has not paid a civil
penalty, and all appeals of this penalty have been abandoned or exhausted.
d. The Permittee or any parent, subsidiary, or other affiliate of the Permittee is currently not compliant
with any compliance schedule in a permit, settlement agreement, or order.
e. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has not paid an annual
fee.
[15A NCAC 02T .0120(b), 02T .0120(d)]
10. This permit shall not be renewed if the Permittee or any affiliation has not paid the required annual fee.
[15A NCAC 02T .0120(c)]
Permit issued this the 4rh day of February 2021
NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
S. Daniel Smith, Director
Division of Water Resources
By Authority of the Environmental Management Commission
Permit Number WQ0038087
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Permit No. WQ0038087 Land Application of Class B Residuals
Terra Renewal Services, Inc. February 4, 2021
Terra Renewal Services RLAP Wilkes County
ENGINEERING CERTIFICATION
❑ Partial ❑ Final
I, , as a duly licensed North Carolina Professional
Engineer, having ❑ periodically / ❑ fully observed the construction of the permitted facilities, do hereby
state to the best of my abilities that the facility was constructed in compliance with G.S. 143-215.1,
Administrative Code Title 15A Subchapter 02T, this permit, and the Division -approved plans and
specifications.
Documentation of any variation to this permit, and the Division -approved plans and specifications, is in the
attached as -built drawings.
Description of variations:
Professional Engineer's Name
Firm Name
Firm No.
Address
City
State
Zip Code
Telephone
Email
Seal, Signature, and Date
THE COMPLETED ENGINEERING CERTIFICATION, INCLUDING ALL SUPPORTING
DOCUMENTATION, SHALL BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES
NON -DISCHARGE BRANCH
By U.S. Postal Service By Courier/Special DelivM
1617 MAIL SERVICE CENTER 512 N. SALISBURY ST.
RALEIGH, NORTH CAROLINA 27699-1617 RALEIGH, NORTH CAROLINA 27604
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THIS PAGE BLANK

ROY COOPER
Governor
ELIZABETH S. BISER
Secretary
RICHARD E. ROGEM, JR.
Director
NORTH CAROLINA
Environmental Quality
April 25, 2022
DAVID C. COYLE — ENVIRONMENTAL MANAGER
TERRA RENEWAL SERVICES, INC.
POST OFFICE BOX 1746
WATKINSVILLE, GEORGIA 30677
Subject: Permit No. WQ0038087
Terra Renewal Services Class B
Residuals Program
Attachments A and B
Certification
Wilkes County
Dear Mr. Coyle:
In accordance with your permit major modification request received November 19, 2021, and
subsequent additional information received March 15, 2022, we are forwarding herewith modified
Attachments A and B certified April 25, 2022, to Terra Renewal Services, Inc. for the subject residuals
management program.
Modifications to the subject Attachments are as follows:
➢ Deletion of the following residuals sources from the permit:
o The Hunter Farms, LLC — High Point, NC facility in Guilford County, totaling 700 dry
tons per year (DT/yr)
o The Brakebush Brothers Inc. — Mocksville, NC facility in Davie County, totaling 240
DT/yr.
➢ Reduction in the permitted annual dry tonnage of the Tyson Foods, Inc. — Wilkesboro, NC
facility in Wilkes County from 5,400 DT/yr to 2,000 DT/yr.
➢ Increase in the permitted annual dry tonnage of the following residuals sources:
o The AdvancePierre Foods, Inc. — Claremont, NC facility in Catawba County, increasing
from 25 DT/yr to 35 DT/yr.
o The Tyson Foods, Inc. — River Valley Ingredients — Harmony, NC facility in Iredell
County, increasing from 1,400 DT/yr to 1,700 DT/yr.
➢ Addition of the following approved residuals sources:
o The Wayne Farms LLC — Dobson Plant in Surry County, with a permitted annual dry
tonnage of 1,300 DT/yr.
D Q
�� North Carolina Department of Environmental Quality Division of Water Resources
512 North Salisbury Street 11617 Mail Service Center Raleigh, North Carolina 27699-1617
NORTH CFNOLiN�
�aw�em oe rmmmme+v� Q..IKV 919.707.9000

Mr. David C. Coyle
April 25, 2022
Page 2 of 2
o The Innospec Active Chemicals LLC — Salisbury WWTF in Rowan County with a
permitted annual dry tonnage of 1,300 DT/yr.
➢ Modification of the following existing fields to remove property line buffers due to the
inclusion of setback waivers:
o NC-WK-MRF-06, increasing from 20.4 acres to 21.0 acres
o NC-WK-MRF-12, increasing from 25.1 acres to 26.5 acres.
➢ Addition of new fields in Wilkes County totaling 153.2 acres, including:
o NC-WK-CH-02, totaling 19.3 acres.
o NC-WK-MF-17, totaling 39.5 acres
o NC-WK-MRF-13 through 15, totaling 94.4 acres.
The modified Attachments A and B shall be effective from the date of certification until November
30, 2027 (i.e., expiration date of the current permit), shall void Attachments A and B of Permit No.
WQ0038087 issued February 4, 2021, and shall be subject to the conditions and limitations as specified
therein, as well as those specified in the above -referenced permit. Please replace Attachments A and B of
Permit No. WQ0038087 that was February 4, 2021 with the modified Attachments A and B. Please note
that the Permittee shall submit a renewal application no later than June 3, 2027.
Please note that only the maps for new land application sites are attached to this letter. It is the
Permittee's responsibility to ensure that a complete permit is created by inserting these documents into the
previously issued permit.
If any parts, requirements or limitations contained in this certification are unacceptable, the
Permittee has the right to request an adjudicatory hearing upon written request within 30 days following
receipt of this permit. This request shall be in the form of a written petition, conforming to Chapter 150B
of the North Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail
Service Center, Raleigh, NC 27699-6714. Otherwise, this certification shall be final and binding.
If you need any additional information concerning this matter, please contact Erick Saunders at
[phone] or erickson.saunders&ncdenr.gov.
Sincerely,
Richard E. Rogers, Jr., Director
Division of Water Resources
cc: Rowan County Health Department (Electronic Copy)
Surry County Health Department (Electronic Copy)
Wilkes County Health Department (Electronic Copy)
Winston-Salem Regional Office, Water Quality Regional Operations Section (Electronic Copy)
Laserfiche File (Electronic Copy)
Digital Permit Archive (Electronic Copy)

ATTACHMENT A — APPROVED RESIDUAL SOURCES
Terra Renewal Services, Inc.
Certification Date: April 25, 2022
Permit Number: WQ0038087 Version: 2.1
Monitoring
Monitoring
Monitoring
Permit
Biological
Maximum
Frequency for
Frequency for
Frequency for
Approved
Owner
Facility Name
County
Number
Residuals
Dry Tons
Non -hazardous
Metals an3,5 d
Pathogen &
Mineralization
per Year'
Characteristics z
Nutrients
Vector Attraction
Rate
Reductions 1,5
Tyson Foods, Inc.
River Valley Ingredients —
Iredell
NC0005126
Yes
1,700
Annually
See Table Below
See Table Below
0.4
Harmony, NC
Wayne Farms LLC
Dobson Plant
Surry
NC0006548
Yes
1,300
Annually
See Table Below
See Table Below
0.4
Tyson Foods, Inc.
Tyson — Wilkesboro, NC
Wilkes
N/A
Yes
2,000
Annually
See Table Below
See Table Below
0.4
AdvancePierre Foods, Inc.
AdvancePierre Foods —
Catawba
N/A
Yes
35
Annually
Annually
Annually
0.4
Claremont, NC
Innospec Active Chemicals
Innospec Active Chemicals —
Rowan
WQ0001077
Yes
225
Annually
Annually
Annually
0.3
LLC
Salisbury WWTF
Mathis Properties, LLC 6
MATHIS-1 Storage Facility7
Wilkes
I WQ0038087
Yes
I N/A
I Annually
I See Table Below
See Table Below a
0.4
Total
5,260
1. Maximum Dry Tons per Year is the amount of residuals approved for land application from each permitted facility.
2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit Condition IV.2.
3. Testing of metals and nutrients as stipulated under permit Condition IV.3.
4. Analyses of pathogen and vector attraction reductions as stipulated under permit Condition IV. 4.
5. Monitoring frequencies are based on the actual dry tons applied per year using the table below, unless specified above.
Dry Tons Applied
Monitoring Frequency
Dry Tons Applied (metric tons)
(short tons per year)
(40 CFR 503 and 15A NCAC 02T
.1111 c
< 290
< 319
Once per year (Annually)
> 290 to < 1,500
> 319 to < 1,650
Once per quarter (4 x Year)
> 1,500 to < 15,000
> 1,650 to < 16,500
Once per 60 days (6 x Year)
> 15,000
> 16,500
Once per month (12 x Year)
6. An easement agreement has been provided between Mathis Properties, LLC and Terra Renewal Services, Inc. for the installation and operation of this storage facility which has been recorded on
Deed Book 01322 Page 0186 in the Wilkes County Register of Deeds. A site map for this facility can be found on Figure 32.
7. Residuals from any of the other approved residual sources may be temporarily stored in this structure. Any residuals inputted into this storage structure from another permitted source shall be
subtracted from the other source's maximum dry tonnage per year.
8. Representative samples of comingled residuals shall be conducted immediately prior to land application events to ensure that regrowth of pathogens has not exceeded the pathogen limits for Class
B biological residuals established in 15A NCAC 02T .I 106(b)(1).
WQ0038087 Version 2.1 Attachment A Page 1 of 2

ATTACHMENT A — APPROVED RESIDUAL SOURCES
Terra Renewal Services, Inc.
Certification Date: April 25, 2022
Permit Number: WQ0038087 Version: 2.1
If no land application events occur during a required sampling period (e.g., no land application occur during an entire year when annual monitoring is required), then no sampling data is
required during the period of inactivity. The annual report shall include an explanation for missing sampling data. Those required to submit the annual report to United States Environmental
Protection Agency (US EPA) may be required to make up the missed sampling. Contact the US EPA for additional information.
WQ0038087 Version 2.1 Attachment A Page 2 of 2

ATTACHMENT B — APPROVED LAND APPLICATION SITES
Terra Renewal Services Class B Residuals Program
Certification Date: April 25, 2022
Permit Number: WQ0038087 Version: 2.1
Field
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
NC-WK-CH-01
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.212417'
-80.918617'
21.8
DpC2 - Danripple
1
NC-WK-CH-02
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.217570'
-80.920074'
19.3
RyB — Ronda
33
NC-WK-CH-03
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.212656'
-80.925933'
41.6
BaB - Banister
1,36
NC-WK-CH-04
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.211892'
-80.921528'
35.8
CoA - Codorus
1
NC-WK-DF-01
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.159722'
-81.134444'
8.8
DaA - Dan River
2
NC-WK-DF-02
Pearson, William M
ASJ Mathis Farms LLC
Wilkes
36.155278'
-81.153333'
68.5
DaA - Dan River
3, 36
NC-WK-DF-03
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.151667'
-81.158889'
35.5
DaA - Dan River
4
NC-WK-DF-04
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.174444'
-81.105000'
18.5
DaA - Dan River
5
NC-WK-DS-01
Sparks, Don; Sparks, Mary
Wilkes
36.265556'
-81.975278'
53.6
FcB2 - Fairview
6
NC-WK-DS-02
Sparks, Don; Sparks, Mary
Wilkes
36.260833'
-81.968889'
42.1
FcB2 - Fairview
7
NC-WK-DS-03
Sparks, Don; Sparks, Mary
Wilkes
36.258333'
-81.973889'
33.6
FcC2 - Fairview
7
NC-WK-DS-04
Sparks, Don; Sparks, Mary
Wilkes
36.253333'
-81.003333'
28.7
FcC2 - Fairview
8
NC-WK-DS-05
Sparks, Don; Sparks, Mary
Wilkes
36.243889'
-80.999722'
16.0
FcC2 - Fairview
9
NC-WK-DS-06
Sparks, Don; Sparks, Mary
Wilkes
36.240833'
-80.980000'
16.7
DpC2 - Danripple
9
NC-WK-DS-07
Sparks, Don; Sparks, Mary
Wilkes
36.240556'
-80.976944'
23.8
Dp132 - Danripple
9
NC-WK-DS-08
Sparks, Don; Sparks, Mary
Wilkes
36.239444'
-80.974444'
41.4
PaB - Pfafftown
10
NC-WK-DS-09
Sparks, Don; Sparks, Mary
Wilkes
36.239722'
-80.968889'
41.2
FcC2 - Fairview
10
NC-WK-DS-10
Sparks, Don; Sparks, Mary
Wilkes
36.239444'
-80.964444'
6.3
FcC2 - Fairview
10
NC-WK-ED-01
Call, Isaac Jeremy
ASJ Mathis Farms LLC
Wilkes
36.178111'
-81.065492'
30.0
DpC2 - Danripple
11
NC-WK-ED-02
Call, Isaac Jeremy
ASJ Mathis Farms LLC
Wilkes
36.185558'
-81.067117'
14.8
DpC2 - Danripple
12
NC-WK-ED-03
Staley, Edward; Staley, Janet C.
ASJ Mathis Farms LLC
Wilkes
36.171331'
-81.097531'
12.1
BaB - Banister
13,36
NC-WK-ED-04
Staley, Edward; Staley, Janet C.
ASJ Mathis Farms LLC
Wilkes
36.173856'
-81.096853'
25.1
DpC2 - Danripple
13,36
NC-WK-HP-01
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.181269'
-81.003058'
15.9
FcC2 - Fairview
14
NC-WK-HP-03
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.183114'
-80.997378'
14.5
FcC2 - Fairview
14
NC-WK-MF-06
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.138617'
-80.982847'
22.5
FcC2 - Fairview
15,36
WQ0038087 Version 2.1 Attachment B Page 1 of 4

ATTACHMENT B — APPROVED LAND APPLICATION SITES
Terra Renewal Services Class B Residuals Program
Certification Date: April 25, 2022
Permit Number: WQ0038087 Version: 2.1
Field
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
NC-WK-MF-08
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.138489'
-80.980256'
12.7
FcC2 - Fairview
15,36
NC-WK-MF-09
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.151697'
-80.986713'
13.2
FcB2 - Fairview
16
NC-WK-MF-10
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.150722'
-80.983675'
19.6
FcB2 - Fairview
16
NC-WK-MF-11
Mathis Properties LLC; Mathis, John
M.; Mathis, Lisa S.; Roberts, James F.
ASJ Mathis Farms LLC
Wilkes
36.147294'
-80.983131'
22.5
FcC2 - Fairview
17. 37
NC-WK-MF-13
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.159353'
-80.979606'
33.8
FcB2 - Fairview
18
NC-WK-MF-14
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.158758'
-80.984122'
23.4
FcC2 - Fairview
18
NC-WK-MF-15
Mathis Properties LLC; Mathis, Jeffrey
B; Mathis, Dayle E.
ASJ Mathis Farms LLC
Wilkes
36.150086'
-80.994117'
13.8
FcC2 - Fairview
19,37
NC-WK-MF-17
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.164208'
-80.968621'
39.5
FcC2 - Fairview
34
NC-WK-MF-23
Mathis Properties LLC; Anderson,
Charles D; Anderson, Nina J.
ASJ Mathis Farms LLC
Wilkes
36.145864'
-80.989903'
59.2
FcB2 - Fairview
20,37
NC-WK-MU-03
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.207767'
-80.966694'
18.9
DpC2 - Danripple
21
NC-WK-NW-05
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.210517'
-80.967261'
25.3
DpB2 - Danripple
21
NC-WK-MU-06
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.209406'
-80.970353'
21.0
DpB2 - Danripple
22
NC-WK-NW-12
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.213144'
-80.969581'
26.5
PaB - Pfafftown
21
NC-WK-NW-13
Blue Ridge Conservancy
ASJ Mathis Farms LLC
Wilkes
36.210104'
-80.975250'
41.0
RyB — Ronda
35,37
NC-WK-MU-14
Blue Ridge Conservancy
ASJ Mathis Farms LLC
Wilkes
36.206196'
-80.973629'
18.5
DpC2 - Danripple
35,37
NC-WK-NW-15
Motsinger, Stephen CC.; Motsinger, Jane
ASJ Mathis Farms LLC
Wilkes
36.205112'
-80.981448'
34.9
RyB — Ronda
35,37
NC-WK-MU-20
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.199955'
-81.018875'
52.3
DaA - Dan River
23,36
NC-WK-NW-21
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.200053'
-81.012331'
27.8
DaA - Dan River
23
NC-WK-NW-22
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.187453'
-81.059136'
31.4
RyB - Ronda
12,36
NC-WK-RJ-01
Johnson, T. R.
ASJ Mathis Farms LLC
Wilkes
36.200342'
-81.025586'
20.6
DaA - Dan River
23
NC-WK-RJ-02
Barker, Kim Tharpe
Wilkes
36.216786'
-80.929053'
57.8
DaA - Dan River
24,37
NC-WK-RJ-05
Johnson, S. L.
ASJ Mathis Farms LLC
Wilkes
36.217883'
-80.924208'
45.1
DaA - Dan River
24,37
NC-WK-RJ-07
Red Oak Meadows, LLC
ASJ Mathis Farms LLC
Wilkes
36.241139'
-80.935875'
24.6
FcB2 - Fairview
25
NC-WK-SP-01
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.160979'
-81.004357'
12.7
FcC2 — Fairview
26
WQ0038087 Version 2.1 Attachment B Page 2 of 4

ATTACHMENT B — APPROVED LAND APPLICATION SITES
Terra Renewal Services Class B Residuals Program
Certification Date: April 25, 2022
Permit Number: WQ0038087 Version: 2.1
Field
Owner
Lessee
County
Latitude
Longitude
Net Acreage
Dominant Soil Series
Footnotes
NC-WK-SP-02
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.157225'
-81.004436'
26.8
FcC2 - Fairview
26,36
NC-WK-WB-01
Bell, Wayne Edward; Bell, Linda C.
ASJ Mathis Farms LLC
Wilkes
36.189444'
-81.053333'
23.2
RyB - Ronda
27,36
NC-WK-YF-07
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes
36.149351'
-80.882108'
10.3
FcB2 - Fairview
28
NC-WK-YK-DM-03
Ireland, Joel L.; Ireland, Samuel G.
ASJ Mathis Farms LLC
Wilkes
Yadkin
36.066453'
-80.881967'
11.4
FcC2 - Fairview
29
NC-WK-YK-DM-07
Ireland, Joel L.; Ireland, Samuel G.;
George F Ireland Trust
ASJ Mathis Farms LLC
Wilkes /
Yadkin
36.060197'
-80.879392'
32.6
Cc132 - Clifford
30
NC-WK-YK-DM-08
Ireland, Joel L.; Ireland, Samuel G.;
George F Ireland Trust
ASJ Mathis Farms LLC
Wilkes /
Yadkin
36.058033'
-80.880094°
26.2
Cc132 - Clifford
30
NC-WK-YK-YF-05
Mathis Properties LLC
ASJ Mathis Farms LLC
Wilkes/
Yadkin
36.149542'
-80.877026'
51.5
FcC2 - Fairview
28
NC-YK-DM-05
George F. Ireland Trust
ASJ Mathis Farms LLC
Yadkin
36.067144'
-80.874722'
21.0
Cc132 - Clifford
29
NC-YK-DM-06
George F. Ireland Trust
ASJ Mathis Farms LLC
Yadkin
36.061742'
-80.874897'
25.6
Cc132 - Clifford
30
NC-WK-TA-01
Ashley Family Properties, LLC.
ASJ Mathis Farms LLC
Yadkin
36.123889'
-80.797500'
32.3
Cc132 - Clifford
31
NC-YK-YF-01
Mathis Properties LLC
ASJ Mathis Farms LLC
Yadkin
36.147997'
-80.867922'
13.5
NaB - Nathalie
28
NC-YK-YF-03
Mathis Properties LLC
ASJ Mathis Farms LLC
Yadkin
36.148353'
-80.871856'
22.3
Cc132 - Clifford
28
NC-YK-YF-04
Mathis Properties LLC
ASJ Mathis Farms LLC
Yadkin
36.150989'
-80.872203'
23.3
Cc132 - Clifford
28
Total
1,704.2
1-35. See Figures 1-35, respectively.
36. The maximum injection depth shall be six inches below the ground surface for these fields. The Pennittee or the Pennittee's representative shall ensure an injection depth of six inches below the
ground surface complies with the terms of Permit Condition III.1O.i.
WQ0038087 Version 2.1 Attachment B Page 3 of 4

ATTACHMENT B — APPROVED LAND APPLICATION SITES Certification Date: April 25, 2022
Terra Renewal Services Class B Residuals Program Permit Number: WQ0038087 Version: 2.1
37. Per setback waivers recorded in the Wilkes and Yadkin County Register of Deeds, reduced setbacks from the Class B land application site to any property lines are as follows:
Field
County
Parcel No.
DB / Page
Setback
Easement
NC-WK-MF-11
Wilkes
0100606
01317 / 0055
0 feet
50 feet
0100732
01322 / 0180
0 feet
50 feet
0100737
01322 / 0179
0 feet
50 feet
NC-WK-MF-15
Wilkes
0100990
01317 / 0056
0 feet
50 feet
0100991
01322 / 0181
0 feet
50 feet
NC-WK-MF-23
Wilkes
0100821
01317 / 0057
0 feet
50 feet
0100131
01317 / 0058
0 feet
50 feet
0100317
01322 / 0182
0 feet
50 feet
0100266
01322 / 0183
0 feet
50 feet
0100148
01322 / 0184
0 feet
50 feet
0100149
01322 / 0185
0 feet
50 feet
NC-WK-MU-06
Wilkes
0100020
01343 / 0198
0 feet
50 feet
NC-WK-MU-12
Wilkes
0100020
01343 / 0198
0 feet
50 feet
NC-WK-NW-13
Wilkes
0100811
01343 / 0199
0 feet
50 feet
0100282
01343 / 0200
0 feet
50 feet
NC-WK-MU-14
Wilkes
0100811
01343 / 0199
0 feet
50 feet
NC-WK-NW-15
Wilkes
0100020
01343 / 0198
0 feet
50 feet
NC-WK-RJ-02
Wilkes
0601666
01317 / 0059
0 feet
50 feet
NC-WK-RJ-05
Wilkes
0605291
01317 / 0060
0 feet
50 feet
NC-WK-YK-DM-03
Wilkes
1700289
01317 / 0054
0 feet
50 feet
NC-WK-YK-DM-07
NC-WK-YK-DM-08
NC-WK-YK-DM-07
Yadkin
484400359744
01304 / 0034
0 feet
50 feet
NC-WK-YK-DM-08
NC-WK-YK-DM-03
Yadkin
484400562719
01304 / 0036
0 feet
50 feet
NC-WK-YK-DM-07
NC-WK-YK-DM-08
WQ0038087 Version 2.1 Attachment B Page 4 of 4

SECTION 2:
NON -DEDICATED RESIDUALS LAND APPLICATION PROGRAM
Form: RLAP 06-16

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM
FORM: RLAP 06-16
L APPLICANT INFORMATION:
1. Applicant's name: Terra Renewal Services, Inc
Applicant type: ❑ Individual ® Corporation ❑ General Partnership ❑ Privately -Owned Public Utility
❑ Federal ❑ State ❑ Municipal ❑ County
Signature authority's name per 15A NCAC 02T .0106: David C. Coyle Title: Senior Environmental Manager
Applicant's mailing address: P.O. Box 1746
City: Watkinsville State: GA Zip: 30677-
Telephone number: [phone] Email Address: david.coyle&terrarenewal.com
2. Consultant's name: License Number (for P.E.):
Affiliation: ❑ On Staff ❑ Retained (Firm: )
Consultant's mailing address:
City: State:
Telephone number:
3. Agronomist's name:
Affiliation: ❑ N/A ❑ On Staff
Agronomist's mailing address: _
Zip: -
Email Address:
License Number:
❑ Retained (Firm: )
City: State: Zip: -
Telephone number: (_) _- Email Address:
4. Soil Scientist's name: David C. CoyleLicense Number: 1315
Affiliation: ❑ N/A ® On Staff ❑ Retained (Firm: )
Soil Scientist's mailing address: P.O. Box 1746
City: Watkinsville State: GA Zip: 30677-
Telephone number: 4( 79) 747-8192 Email Address: david.coyle(a_terrarenewal.com
5. Fee submitted: $395.00 (See Instruction B)
IL PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ® modified, ❑ renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: WO0038087
Date of most -recently issued permit: February 4, 2021
Date of most -recently certified Attachment A (if different than the permit): February 4, 2021
Date of most -recently certified Attachment B (if different than the permit): February 4, 2021
FORM: RLAP 06-16 Page 1 of 5

III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION:
1. Residuals Processing Facility's physical address: 615 Mathis Farm Rd (Location of Office of LJC Environmental, LLC)
City: Roaring River State: NC Zip: 25669-.
Coordinates: Latitude: 36' 08' 51" Longitude: 80' 59' 09"
Datum: NAD 83 Level of accuracy: Nearest Second
Method of measurement: MAP
2. County where residuals land application program is headquartered: Wilkes
3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their
certification numbers, and their affiliations in the following table:
Designation
Name
Affiliation
Certification Number
ORC
Luke Mathis
LJC Environmental, LLC
1003524
Back -Up ORC
David Coyle
Denali Water Solutions
995723
Additional Back -Up
Will Hodges
Denali Water Solutions
997282
ORCs
Ivan Heatwole
Denali Water Solutions
1002031
if applicable)
If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the
candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school
and certification test:
4. Complete the following tables regarding management of the residuals land application program:
a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals
source -generating facilities as currently certified and proposed for certification with this application and list the results in the
following table:
Maximum amount of residuals to be certified: 5,785 dry tons per year.
PAN
Pounds of PAN per Dry Ton
(Weighted Average)
Pounds of PAN per Year
Surface
Incorporation
or Injection
Surface
Incorporation
or Injection
First -Year
36.2
46.4
209,417
268,424
Five -Year Maximum Adjusted
49.4
59.5
285,779
344,208
b. LandApplication Site Use Summary: Summarize information regarding the land application sites as currently certified and
proposed for certification with this application:
Category
Use
Acres
Comments
Crops
Forest or Plantation
Row Crops
1,755.3
Hay
Pasture
Total:
1,755.3
Methods
Surface
Incorporation or Injection
1,755.3
Total:
1,755.3
FORM: RLAP 06-16 Page 2 of 5

c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently
certified and proposed for certification assuming the scenarios listed in the following table:
Assumed
Application Rate
(lbs PAN/ac yr)
Acres Required Using
First -Year PAN Concentrations
Acres Required Using
Five -Year Maximum Adjusted PAN
Concentrations
Surface
Incorporation or
Injection
Surface
Incorporation or
Injection
50
4,188
5,368
5,716
6,884
100
2,094
2,684
2,858
3,442
150
1,396
1,789
1,905
2,295
200
1,047
1,342
1,429
1,721
6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed
residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction
practices not in place, etc.):
7. Specify type of residuals program (See Instruction F): ® Non -dedicated ❑ Dedicated
If Dedicated, specify the following (check all that apply):
❑ Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic
rates, explain;
❑ Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop
production is of secondary importance, explain;
❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation
facilities fed through a fixed supply system, explain;
IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source)
Complete and submit the following Residuals Source Certification and all associated documentation.
Residuals Source
Certification
V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site)
Complete and submit the following Land Applications Site Certification and all associated documentation.
R
Land Application Siite
Certification.doc
FORM: RLAP 06-16 Page 3 of 5

Note: Item VL Applicable to Dedicated Program with fixed irrigationystem only.
VI. DESIGN INFORMATION FOR FIXED IRRIGATION SYSTEM
1. The irrigation system is: ❑ Spray ❑ Drip
2. Disposal system is: ❑ existing ❑ proposed.
3. Minimum depth to mean seasonal high water table (SHWT) within irrigation sites(s) per Soil Scientist's Evaluation: feet
below ground surface. Rules 15A NCAC 02T .0505(p) requires at least one -foot vertical separation between SHWT and ground
surface.
4. Are there any artificial drainage or water movement structures within 200 feet of any irrigation area?
❑ Yes or ❑ No If Yes, please explain if the soil scientist report addresses artificial structures and please indicate if
structures are to be maintained or modified:
5. Loading rates recommended by the Soil Scientist Evaluation:
Soil Series
Fields within Soil Area
Recommended
Loading Rate
in/hr
Recommended
Loading Rate
in/ r
6. Design loading rates are equal or less than the loading rates recommended by Soil Scientist?
❑ Yes or ❑ No If No, explain why 15A NCAC 02T .0505(n) is not met:
7. Non -dedicated System Design (fill in the appropriate information for either a spray or drip irrigation system):
Field /Zone
Design Area
ft2
Number of
Nozzles
Maximum Application
Rate allons/hr
Design Annual Loading
Rate (gallon!/jr
Total
Spray Irrigation Design Element
Plan Sheet
Number
Specification
Pa a Number
Wetted diameter of nozzles
It
Wetted area of nozzles
ft2
Nozzle capacity
gpm
Nozzle manufacturer / model
/
Elevation of highest nozzle
It
FORM: RLAP 06-16 Page 4 of 5

Applicant's Certification (signing authority must be in compliance with 15A NCAC 02T .0106):
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper
closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
® Yes ❑ No, Explain;
I, David C. Coyle Senior Environmental Manager
(Signature Authority's Name — PLEASE PRINT) (Title)
attest that this application for Terra Renewal Services, Inc
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources
may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically
granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action,
which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water
Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed
and that if all required supporting information and attachments are not included, this application package will be returned to me as
incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false
statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to
exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature:
'��" 5-,,"
Date: 07/21 /2023
FORM: RLAP 06-16 Page 5 of 5

DENALI
February 16, 2023
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Aquifer Protection Section
1636 Mail Service Center
Raleigh, NC 27699-1636
Subject: Permitting Signature Authority
To Whom It May Concern:
3308 Bernice Avenue
Russellville, Arkansas 72802
479-498-0500
As an appropriate signing official for Denali Water Solutions, as designated by 15A NCAC 02T .0106(b), I
hereby delegate authority to sign and certify all permit applications/modifications, reports or other permit
related documents to the following staff for all permits associated with Denali Water Solutions or Terra
Renewal Services, Inc.
Position
Name
Senior Environmental Director
Jeff Retzke
Senior Environmental Manager
David Coyle
Environmental Manager
Will Hodges
Environmental Manager
Drew Epting
If you have any questions, please contact me at the following:
Permittee/Applicant name (please print): Tom Ha
Title. Executive Vice President, S.E. Division
Complete mailing address: 3308 Bernice Avenue
City: Russellville
Telephone
number:
Sincerely,
signature
479-890-6456
State: AR
Email
Address
Zip: 72802
[e-mail]

SECTION 3:
RESIDUALS SOURCE CERTIFICATION
Form: RCS 06-16

RSC 06-16
TYSON-DAVI LLE, VA

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
L RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Tyson — Danville, VA
2. Facility permit holder is: ❑ Federal, 0 State, 0 Local Government, or 0 Private.
Facility permit issued by: ❑ Div. of Water Resources, ❑ Div. of Environmental Health,
or ® Other (explain: Facility to be operated under permits issued by the VA DEQ).
3. Facility contact person and title: Mallorie Gomersall, Enviromental Manager
Complete mailing address: 1725 Cane Creek Parkway
City: Ringol State: VA Zip: 24586
Telephone number: [phone] E-mail address: mallorie.gomersallAlyson.com
4. Facility physical address: 1725 Cane Creek Parkway
City: Rmgold State: VA Zip: 24586
Coordinates: Latitude: 36' 35' 45" Longitude: 79' 18' 15"
Datum: NAD 83 Level of accuracy: Nearest Second
Method of measurement: MAP
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: = % industrial and = % domestic)
other (explain:).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: 1.0 MGD and facility average daily flow: 0.8 MGD
8. Average amount of residuals being generated at this facility 3,000 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 100% of residuals generated from solids removed from D.A.F. system
Type and volume of residuals storage (i.e., outside of residuals treatment units): One 40,000 gallon above ground storage
tank
IL RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under
40 CFR Part 503 or [jj 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
JE Biological 0 Non -Biological
FORM: RSC 06-16 Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): =
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 6/08/23 (date collected)
Passed corrosivity test: yes ?!? no. pH: s.u. (2 <pH < 12.5)
Passed ignitability test: yes Fj no. Flashpoint > 140 OF (> 140°F)
Passed reactivity test: Eyes Ono. HCN: < 50 mg/kg (<250) & HzS: < 50 mg/kg (<500)
TCLP Parameter
Limit
(mg/l)
Result
(mg/l)
TCLP Parameter
Limit
(mg/l)
Result
(mg/l)
Arsenic
5.0
< 0.15
Hexachlorobenzene
0.13
< 0.040
Barium
100.0
< 0.25
Hexachloro-1,3-Butadiene
0.5
< 0.040
Benzene
0.5
< 0.050
Hexachloroethane
3.0
< 0.040
Cadmium
1.0
< 0.050
Lead
5.0
< 0.10
Carbon Tetrachloride
0.5
< 0.10
Lindane
0.4
< 0.00040
Chlordane
0.03
< 0.0040
Mercury
0.2
< 0.0020
Chlorobenzene
100.0
< 0.050
Methoxychlor
10.0
< 0.0016
Chloroform
6.0
< 0.050
Methyl Ethyl Ketone
200.0
< 0.10
Chromium
5.0
< 0.10
Nitrobenzene
2.0
< 0.040
m-Cresol
200.0
< 0.040
Pentachlorophenol
100.0
0.20
o-Cresol
200.0
< 0.040
Pyridine
5.0
< 0.040
p-Cresol
200.0
< 0.040
Selenium
1.0
< 0.20
Cresol
200.0
< 0.040
Silver
5.0
< 0.10
2,4-D
10.0
< 0.20
Tetrachloroethylene
0.7
< 0.050
1,4-Dichlorobenzene
7.5
< 0.040
Toxaphene
0.5
< 0.0080
1,2-Dichloroethane
0.5
< 0.050
Trichloroethylene
0.5
< 0.050
1, 1 -Dichloroethylene
0.7
< 0.050
2,4,5-Trichlorophenol
400.0
< 0.040
24-Dhutrotoluene
0.13
< 0.020
2,4,6-Trichlorophenol
2.0
< 0.040
Endrin
0.02
< 0.00040
2,4,5-TP (Silvex)
1.0
< 0.0050
Heptachlor and its Hydroxide
0.008
< 0.00040
Vinyl Chloride
0.2
< 0.010
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 6/08/23 (date collected)
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(ClassA Only)
(mg1kg)
Result
(mg1kg)
Arsenic
75
41
< 5.6
Cadmium
85
39
< 1.9
Copper
4,300
1,500
56
Lead
840
300
< 3.7
Mercury
57
17
< 2.0
Molybdenum
75
n/a
< 15
Nickel
420
420
< 15
Selenium
100
100
< 7.4
Zinc
7,500
2,800
44
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: = and Date of analysis: =
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
> 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 4.01 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
nucronutnent parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 6/08/23 (date collected)
Parameter
Result
(mg1kg)
Aluminum
< 150
Ammonia -Nitrogen
4,800
Calcium
< 1,900
Magnesium
< 1,900
Nitrate -Nitrite Nitrogen
24
pH (Standard Unit)
4.4
Phosphorus
5,400
Potassium
< 1,900
Sodium
< 1,900
Total Kjeldahl Nitrogen
93,000
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 1_5
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 40 %. This
rate is a (check one): 0 default value, or 0 actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1s) Year PAN
Five -Year
Maximum Adjusted PAN
(mg1kg)
(mg/kg)
Surface
37,700
56,700
Injection/Incorporation
40,100
59,100
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
J Alternative 1 [15A NCAC 02T.1106(b)(3)(A)] -Time/Temperature Compliance.
J Alternative 2 [15A NCAC 02T.I106(b)(3)(B)] - Alkaline Treatment.
J Alternative 3 [15A NCAC 02T.I106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
J Alternative 4 [15A NCAC 02T.I106(b)(3)(D)] - No Prior Testing for Enteric Vims/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: 77 composting, � heat drying, r] heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of'Class B:
Alternative 1 [15A NCAC 02T. I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T. I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: [I aerobic digestion, I
air drying, ❑ anaerobic digestion,
❑ composting, or lime stabilization.
c. For Surface Disposal:
J Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item IL 7a. above.
J Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item IL 7b. above.
J Exempt -If Daily Cover Alternative is chosen in Item IL8. below [15A NCAC 02T.1106(a)(2)].
J Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
E] Alternative 2 [15A NCAC 02T. I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
El Alternative 3 [15A NCAC 02T. I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
El Alternative 4 [15A NCAC 02T. I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
El Alternative 5 [15A NCAC 02T. I 107(a)(5)] - 14-Day Aerobic Processes.
El Alternative 6 [15A NCAC 02T. I 107(a)(6)] - Alkaline Stabilization.
El Alternative 7 [15A NCAC 02T. I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T. I 107(a)(8)] - Drying of Unstabilized Residuals.
Alternative 9 [15A NCAC 02T. I 107(a)(9)] - Injection.
Alternative 10 [15A NCAC 02T. I 107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T. I107(b)(2)].
Q Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

RSC 06-16
ADVANCE-PIERRE FOODS-CLAREMONT, NC

DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
L RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: tdvancePierr�
2. Facility permit holder is: ❑ Federal, 0 State, 0 Local Government, or 0 Private.
Facility permit issued by: ❑ Div. of Water Resources, ❑ Div. of Environmental Health,
or a Other (explain: Facility discharges to local POTW. Residuals consist of DAF
skimmings from pretreatment).
3. Facility contact person and title: Tito: Envii alter
Complete mailing address: 3437 E. ?W St
City: Claremont State: E Zip:
Telephone number: [phone] E-mail address:
4. Facility physical address: 3437 E. Main St
City: IClaremon State: a Zip: MY -
Coordinates: Latitude: L5° 42' 43" Longitude: a° L8' 16"
Datum: NAD 83 Level of accuracy: Nearest Second
Method of measurement: MAP
5. Purpose of the facility:
treatment of municipal wastewater, ij� treatment of 100% domestic wastewater,
treatment of potable water, 0 treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: = % industrial and = % domestic)
other (explain: = ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: MGD and facility average daily flow: MGD
8. Average amount of residuals being generated at this facility E dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 100% generated from solids reed from D.A.F.
Type and volume of residuals storage (i.e., outside of residuals treatment units):
IL RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under
40 CFR Part 503 or [jj 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
JE Biological 0 Non -Biological
FORM: RSC 06-16 Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): =
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: jjjjVinalyti and Date of analysis: 12/27/2022
Passed corrosivity test: [I yes ❑ no. pH: s.u. (2 <pH < 12.5)
Passed ignitability test: E yes L] no. Flashpoint EE T (> 140°F)
Passed reactivity test: Eyes Eno. HCN: M mg/kg (<250) & HzS: < 50 mg/kg (<500)
TCLP Parameter
Limit
(mg/l)
Result
(mg/l)
TCLP Parameter
Limit
(mg/l)
Result
(mg/l)
Arsenic
5.0
< 0.15
Hexachlorobenzene
0.13
< 0.040
Barium
100.0
< 0.25
Hexachloro-1,3-Butadiene
0.5
< 0.040
Benzene
0.5
< 0.050
Hexachloroethane
3.0
< 0.040
Cadmium
1.0
< 0.050
Lead
5.0
< 0.10
Carbon Tetrachloride
0.5
< 0.050
Lindane
0.4
< 0.00040
Chlordane
0.03
< 0.0040
Mercury
0.2
< 0.0020
Chlorobenzene
100.0
< 0.050
Methoxychlor
10.0
< 0.0016
Chloroform
6.0
< 0.050
Methyl Ethyl Ketone
200.0
< 0.10
Chromium
5.0
< 0.10
Nitrobenzene
2.0
< 0.040
m-Cresol
200.0
0.11
Pentachlorophenol
100.0
< 0.20
o-Cresol
200.0
< 0.040
Pyridine
5.0
< 0.040
p-Cresol
200.0
0.11
Selenium
1.0
< 0.20
Cresol
200.0
0.11
Silver
5.0
< 0.10
2,4-D
10.0
< 0.020
Tetrachloroethylene
0.7
< 0.050
1,4-Dichlorobenzene
7.5
< 0.040
Toxaphene
0.5
< 0.0080
1,2-Dichloroethane
0.5
< 0.050
Trichloroethylene
0.5
< 0.050
1, 1 -Dichloroethylene
0.7
< 0.050
2,4,5-Trichlorophenol
400.0
< 0.040
24-Dhutrotoluene
0.13
< 0.080
2,4,6-Trichlorophenol
2.0
< 0.040
Endrin
0.02
< 0.00040
2,4,5-TP (Silvex)
1.0
< 0.0050
Heptachlor and its Hydroxide
0.008
< 0.00040
Vinyl Chloride
0.2
< 0.010
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 5/30/2023 (date sampled)
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(ClassA Only)
(mg1kg)
Result
(mg1kg)
Arsenic
75
41
< 9.4
Cadmium
85
39
< 3.1
Copper
4,300
1,500
12
Lead
840
300
< 6.3
Mercury
57
17
< 1.1
Molybdenum
75
n/a
< 25
Nickel
420
420
< 25
Selenium
100
100
< 13
Zinc
7,500
2,800
< 31
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: = and Date of analysis: =
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
> 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 6.94%.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
nucronutnent parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 5/30/2023
Parameter
Result
(mg1kg)
Aluminum
750
Ammonia -Nitrogen
170
Calcium
< 3100
Magnesium
< 3100
Nitrate -Nitrite Nitrogen
21
pH (Standard Unit)
7.1
Phosphorus
< 72
Potassium
< 3100
Sodium
9200
Total Kjeldahl Nitrogen
< 720
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 7_3
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This
rate is a (check one): 0 default value, or 0 actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1s) Year PAN
Five -Year
Maximum Adjusted PAN
(mg1kg)
(mg/kg)
Surface
350
450
Injection/Incorporation
400
550
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
J Alternative 1 [15A NCAC 02T.1106(b)(3)(A)] -Time/Temperature Compliance.
J Alternative 2 [15A NCAC 02T.I106(b)(3)(B)] - Alkaline Treatment.
J Alternative 3 [15A NCAC 02T.I106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
J Alternative 4 [15A NCAC 02T.I106(b)(3)(D)] - No Prior Testing for Enteric Vims/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: 77 composting, � heat drying, r] heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of'Class B:
Alternative 1 [15A NCAC 02T. I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T. I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: [I aerobic digestion, I
air drying, ❑ anaerobic digestion,
❑ composting, or lime stabilization.
c. For Surface Disposal:
J Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item IL 7a. above.
J Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item IL 7b. above.
J Exempt -If Daily Cover Alternative is chosen in Item IL8. below [15A NCAC 02T.1106(a)(2)].
J Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
E] Alternative 2 [15A NCAC 02T. I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
El Alternative 3 [15A NCAC 02T. I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
El Alternative 4 [15A NCAC 02T. I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
El Alternative 5 [15A NCAC 02T. I 107(a)(5)] - 14-Day Aerobic Processes.
El Alternative 6 [15A NCAC 02T. I 107(a)(6)] - Alkaline Stabilization.
El Alternative 7 [15A NCAC 02T. I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T. I 107(a)(8)] - Drying of Unstabilized Residuals.
Alternative 9 [15A NCAC 02T. I 107(a)(9)] - Injection.
Alternative 10 [15A NCAC 02T. I 107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T. I107(b)(2)].
Q Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

RSC 06-16
MATHIS-1 (STORAGE)

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
L RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name:
2. Facility permit holder is: ❑ Federal, 0 State, 0 Local Government, or ® Private.
Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health,
or ❑ Other (explain: M).
3. Facility contact person and title: �. Cale, Environmental Manager — Terra Renewal Services, Inc.
Complete mailing address: �6
City: atkinsville State: Zip: 30677-
Telephone number: (M) E-mail address: le(a_terrarenewal.com
4. Facility physical address: Mathis Mill Rd Rd
City: � State: NC Zip: WE —
Coordinates: Latitude: 36' 12' 35" Longitude: W° 58' 09"
Datum: NAD 83 Level of accuracy: Nearest Second
Method of measurement: MAP
5. Purpose of the facility:
treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
treatment of potable water, Ej treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: = % industrial and = % domestic)
other (explain: 038087).
6. Does the facility have an approved pretreatment program: 0 Yes ® No
7. Facility permitted/design flow: M MGD and facility average daily flow: M MGD
8. Average amount of residuals being generated at this facility M dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment:
T pe and volume of residuals storage (i.e., outside of residuals treatment units): MG of passive storage for residuals to
land a d under permit WO0038087
IL RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under
40 CFR Part 503 or [jj 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
JE Biological 0 Non -Biological
FORM: RSC 06-16 Page I of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): =
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: jjjjVinalyti and Date of analysis:
Passed corrosivity test: [I yes ❑ no. pH: s.u. (2 <pH < 12.5)
Passed ignitability test: E yes L] no. Flashpoint EE T (> 140°F)
Passed reactivity test: Eyes Ono. HCN: 1.0 mg/kg (<250) & HzS: M mg/kg (<500)
TCLP Parameter
Limit
(mg/l)
Result
(mg/l)
TCLP Parameter
Limit
(mg/l)
Result
(mg/l)
Arsenic
5.0
< 0.15
Hexachlorobenzene
0.13
< 0.040
Barium
100.0
< 0.25
Hexachloro-1,3-Butadiene
0.5
< 0.040
Benzene
0.5
< 0.050
Hexachloroethane
3.0
< 0.040
Cadmium
1.0
< 0.050
Lead
5.0
< 0.10
Carbon Tetrachloride
0.5
< 0.050
Lindane
0.4
< 0.00040
Chlordane
0.03
< 0.0040
Mercury
0.2
< 0.0020
Chlorobenzene
100.0
< 0.050
Methoxychlor
10.0
< 0.0016
Chloroform
6.0
< 0.050
Methyl Ethyl Ketone
200.0
< 0.050
Chromium
5.0
< 0.10
Nitrobenzene
2.0
< 0.040
m-Cresol
200.0
< 0.040
Pentachlorophenol
100.0
< 0.20
o-Cresol
200.0
< 0.040
Pyridine
5.0
< 0.040
p-Cresol
200.0
< 0.040
Selenium
1.0
< 0.20
Cresol
200.0
< 0.10
Silver
5.0
< 0.10
2,4-D
10.0
< 0.020
Tetrachloroethylene
0.7
< 0.050
1,4-Dichlorobenzene
7.5
< 0.040
Toxaphene
0.5
< 0.0080
1,2-Dichloroethane
0.5
< 0.050
Trichloroethylene
0.5
< 0.050
1, 1 -Dichloroethylene
0.7
< 0.050
2,4,5-Trichlorophenol
400.0
< 0.040
24-Dhutrotoluene
0.13
< 0.080
2,4,6-Trichlorophenol
2.0
< 0.040
Endrin
0.02
< 0.00040
2,4,5-TP (Silvex)
1.0
< 0.20
Heptachlor and its Hydroxide
0.008
< 0.00040
Vinyl Chloride
0.2
< 0.010
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 5/18/2023 (date sampled)
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(ClassA Only)
(mg1kg)
Result
(mg1kg)
Arsenic
75
41
< 6.1
Cadmium
85
39
< 2.0
Copper
4,300
1,500
27
Lead
840
300
< 4.1
Mercury
57
17
< 2.0
Molybdenum
75
n/a
< 16
Nickel
420
420
< 16
Selenium
100
100
< 8.1
Zinc
7,500
2,800
36
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: = and Date of analysis: =
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
> 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 3.64 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
nucronutnent parameters:
Laboratory: LLC. and Date of analysis:
Parameter
Result
(mg1kg)
Aluminum
300
Ammonia -Nitrogen
2400
Calcium
< 2000
Magnesium
< 2000
Nitrate -Nitrite Nitrogen
40
pH (Standard Unit)
3.6
Phosphorus
850
Potassium
< 2000
Sodium
< 2000
Total Kjeldahl Nitrogen
20000
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 1_4
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This
rate is a (check one): 0 default value, or 0 actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1s) Year PAN
Five -Year
Maximum Adjusted PAN
(mg1kg)
(mg/kg)
Surface
8,300
12,050
Injection/Incorporation
9,500
13,250
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
J Alternative 1 [15A NCAC 02T.1106(b)(3)(A)] -Time/Temperature Compliance.
J Alternative 2 [15A NCAC 02T.I106(b)(3)(B)] - Alkaline Treatment.
J Alternative 3 [15A NCAC 02T.I106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
J Alternative 4 [15A NCAC 02T.I106(b)(3)(D)] - No Prior Testing for Enteric Vims/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: 77 composting, � heat drying, r] heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of'Class B:
Alternative 1 [15A NCAC 02T. I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T. I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: [I aerobic digestion, I
air drying, ❑ anaerobic digestion,
❑ composting, or lime stabilization.
c. For Surface Disposal:
J Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item IL 7a. above.
J Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item IL 7b. above.
J Exempt -If Daily Cover Alternative is chosen in Item IL8. below [15A NCAC 02T.1106(a)(2)].
J Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
E] Alternative 2 [15A NCAC 02T. I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
El Alternative 3 [15A NCAC 02T. I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
El Alternative 4 [15A NCAC 02T. I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
El Alternative 5 [15A NCAC 02T. I 107(a)(5)] - 14-Day Aerobic Processes.
El Alternative 6 [15A NCAC 02T. I 107(a)(6)] - Alkaline Stabilization.
El Alternative 7 [15A NCAC 02T. I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T. I 107(a)(8)] - Drying of Unstabilized Residuals.
Alternative 9 [15A NCAC 02T. I 107(a)(9)] - Injection.
Alternative 10 [15A NCAC 02T. I 107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T. I107(b)(2)].
Q Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

RSC 06-16
RIVER VALLEY INGREDIENTS (RVI) - HARMONY, NC

DWR
Division of Water Resources
State of North Carolina
Department of Environmental Quality
Division of Water Resources
RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
L RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Ingredients myson Foo
2. Facility permit holder is: ❑ Federal, ❑ State, 0 Local Government, or ❑ Private.
Facility permit issued by: ® Div. of Water Resources, ❑
or ❑ Other (explain:).
3. Facility contact person and title: Kevin F�Vastewater Manager
Complete mailing address: bOI Sheffield R7
City: Harmony
Telephone number: (E) EM
4. Facility physical address: M
City: Mugu State: NC
Coordinates: Latitude: 35' 57' 15"
Datum: NAD 83
State: 0
Div. of Environmental Health,
Zip: 28634-
E-mail address: Dvin.hayneskttyson.com
Method of measurement: MAP
Zip: EU4-.
Longitude: W° 43' 17"
Level of accuracy: Nearest Second
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: = % industrial and = % domestic)
other (explain: = ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: 0 MGD and facility average daily flow: 0.23 MGD
8. Average amount of residuals being generated at this facility = dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: �Reneratec Wds removed Am D.A.F.
Type and volume of residuals storage (i.e., outside of residuals treatment units): one 5,000 gallon holding tank
IL RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under:
40 CFR Part 503 or ® 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
Biological 0 Non -Biological
Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 06-16 Page 1 of 5

3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): =
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes ® no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 12/27/2022 (date sampled)
Passed corrosivity test: yes ❑ no. pH: s.u. (2 <pH < 12.5)
Passed ignitability test: yes ❑ no. Flashpoint EE T (> 140°F)
Passed reactivity test: Eyes Eno. HCN: mg/kg (<250) & H2S: < 50 mg/kg (<500)
TCLP Parameter
Limit
(mg/l)
Result
(mg/l)
TCLP Parameter
Limit
(mg/l)
Result
(mg/l)
Arsenic
5.0
< 0.15
Hexachlorobenzene
0.13
< 0.040
Barium
100.0
< 0.25
Hexachloro-1,3-Butadiene
0.5
< 0.040
Benzene
0.5
< 0.050
Hexachloroethane
3.0
< 0.040
Cadmium
1.0
< 0.050
Lead
5.0
< 0.10
Carbon Tetrachloride
0.5
< 0.050
Lindane
0.4
< 0.00040
Chlordane
0.03
< 0.0040
Mercury
0.2
< 0.0020
Chlorobenzene
100.0
< 0.050
Methoxychlor
10.0
< 0.0016
Chloroform
6.0
< 0.050
Methyl Ethyl Ketone
200.0
< 0.10
Chromium
5.0
< 0.10
Nitrobenzene
2.0
< 0.040
m-Cresol
200.0
0.10
Pentachlorophenol
100.0
< 0.20
o-Cresol
200.0
< 0.040
Pyridine
5.0
< 0.040
p-Cresol
200.0
0.10
Selenium
1.0
< 0.20
Cresol
200.0
0.10
Silver
5.0
< 0.10
2,4-D
10.0
< 0.020
Tetrachloroethylene
0.7
< 0.050
1,4-Dichlorobenzene
7.5
< 0.040
Toxaphene
0.5
< 0.0080
1,2-Dichloroethane
0.5
< 0.050
Trichloroethylene
0.5
< 0.050
1, 1 -Dichloroethylene
0.7
< 0.050
2,4,5-Trichlorophenol
400.0
< 0.040
2,4-Dinitrotoluene
0.13
< 0.080
2,4,6-Trichlorophenol
2.0
< 0.040
Endrin
0.02
< 0.00040
2,4,5-TP (Silvex)
1.0
< 0.0050
Heptachlor and its Hydroxide
0.008
< 0.00040
Vinyl Chloride
0.2
< 0.010
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distrihution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 5/18/2023 (date sampled)
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(ClassA Only)
(mg1kg)
Result
(mg1kg)
Arsenic
75
41
< 5.2
Cadmium
85
39
< 1.7
Copper
4,300
1,500
6.6
Lead
840
300
< 3.5
Mercury
57
17
< 1.9
Molybdenum
75
n/a
< 14
Nickel
420
420
< 14
Selenium
100
100
< 6.9
Zinc
7,500
2,800
32
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: = and Date of analysis: =
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
❑ > 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 4.26 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
nucronutnent parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 5/18/2023 (date sampled)
Parameter
Result
(mg1kg)
Aluminum
4800
Ammonia -Nitrogen
19000
Calcium
23000
Magnesium
< 1700
Nitrate -Nitrite Nitrogen
59
pH (Standard Unit)
6.4
Phosphorus
7700
Potassium
2300
Sodium
3300
Total Kjeldahl Nitrogen
31000
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 1_2
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This
rate is a (check one): 0 default value, or 0 actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1s) Year PAN
Five -Year
Maximum Adjusted PAN
(mg1kg)
(mg/kg)
Surface
14,350
16,950
Injection/Incorporation
23,850
26,500
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
J Alternative 1 [15A NCAC 02T.1106(b)(3)(A)] -Time/Temperature Compliance.
J Alternative 2 [15A NCAC 02T.I106(b)(3)(B)] - Alkaline Treatment.
J Alternative 3 [15A NCAC 02T.I106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
J Alternative 4 [15A NCAC 02T.I106(b)(3)(D)] - No Prior Testing for Enteric Vims/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: 77 composting, � heat drying, r] heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of'Class B:
Alternative 1 [15A NCAC 02T. I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T. I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: [I aerobic digestion, I
air drying, ❑ anaerobic digestion,
❑ composting, or lime stabilization.
c. For Surface Disposal:
J Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item IL 7a. above.
J Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item IL 7b. above.
J Exempt -If Daily Cover Alternative is chosen in Item IL8. below [15A NCAC 02T.1106(a)(2)].
J Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
E] Alternative 2 [15A NCAC 02T. I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
El Alternative 3 [15A NCAC 02T. I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
El Alternative 4 [15A NCAC 02T. I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
El Alternative 5 [15A NCAC 02T. I 107(a)(5)] - 14-Day Aerobic Processes.
El Alternative 6 [15A NCAC 02T. I 107(a)(6)] - Alkaline Stabilization.
El Alternative 7 [15A NCAC 02T. I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T. I 107(a)(8)] - Drying of Unstabilized Residuals.
Alternative 9 [15A NCAC 02T. I 107(a)(9)] - Injection.
Alternative 10 [15A NCAC 02T. I 107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T. I107(b)(2)].
Q Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

RSC 06-16
TYSON-WILKESBORO, NC

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR FORM: RSC 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 11-15):
® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
❑ For new or renewed permits, submit a separate certification for each source facility.
® For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
❑ Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Residuals Source -Generating Facility Information:
® For each source facility, attach the following:
❑ Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for
Residuals Land Application Permits".
❑ Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated, treated, processed, and stored at the facility.
® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
❑ For each source facility, attach the following:
® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
L RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name:
2. Facility permit holder is: ❑ Federal, 0 State, L1 Local Government, or ❑ Private.
Facility permit issued by: ❑ Div. of Water Resources, ❑ Div. of Environmental Health,
or A. Other (explain: Fac discharges t4#MWl POTW; Residuals consist of DAF
ski pretreatment).
3. Facility contact person and title: �ww Wastewater Manager
Complete mailing address: 704 Fac t
City: Wilkesboro State: Zip: 28697-
Telephone number: 3( 36) 838-2171 E-mail address: james.s.brownAjyson.com
4. Facility physical address: 704 Factory Street
City: Wilkesbo State: a Zip: �-
Coordinates: Latitude: F6° 08' 42" Longitude: %- Q9' 43"
Datum: NAD 83 Level of accuracy: Nearest Second
Method of measurement: MAP
5. Purpose of the facility:
treatment of municipal wastewater, ij� treatment of 100% domestic wastewater,
treatment of potable water, 0 treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: = % industrial and = % domestic)
other (explain: = ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: I MGD and facility average daily flow: kd MGD
8. Average amount of residuals being generated at this facility 2,000 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 100% generated from solids rem from D.A.F.
Type and volume of residuals storage (i.e., outside of residuals treatment units): two 24,000 gallon holding tanks
IL RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under
40 CFR Part 503 or [jj 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
JE Biological 0 Non -Biological
FORM: RSC 06-16 Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): =
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: jjjjVinalyti and Date of analysis: 12/27/22 (date sampled)
Passed corrosivity test: [I yes ❑ no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: E yes L] no. Flashpoint EE T (> 140°F)
Passed reactivity test: Eyes Eno. HCN: M mg/kg (<250) & HzS: < 50 mg/kg (<500)
TCLP Parameter
Limit
(mg/l)
Result
(mg/l)
TCLP Parameter
Limit
(mg/l)
Result
(mg/l)
Arsenic
5.0
< 0.15
Hexachlorobenzene
0.13
< 0.040
Barium
100.0
< 0.25
Hexachloro-1,3-Butadiene
0.5
< 0.040
Benzene
0.5
< 0.050
Hexachloroethane
3.0
< 0.040
Cadmium
1.0
< 0.050
Lead
5.0
< 0.10
Carbon Tetrachloride
0.5
< 0.050
Lindane
0.4
< 0.00040
Chlordane
0.03
< 0.0040
Mercury
0.2
< 0.0020
Chlorobenzene
100.0
< 0.050
Methoxychlor
10.0
< 0.0016
Chloroform
6.0
< 0.050
Methyl Ethyl Ketone
200.0
< 0.10
Chromium
5.0
< 0.10
Nitrobenzene
2.0
< 0.040
m-Cresol
200.0
< 0.040
Pentachlorophenol
100.0
< 0.20
o-Cresol
200.0
< 0.040
Pyridine
5.0
< 0.040
p-Cresol
200.0
< 0.040
Selenium
1.0
< 0.20
Cresol
200.0
< 0.040
Silver
5.0
< 0.10
2,4-D
10.0
< 0.020
Tetrachloroethylene
0.7
< 0.050
1,4-Dichlorobenzene
7.5
< 0.040
Toxaphene
0.5
< 0.0080
1,2-Dichloroethane
0.5
< 0.050
Trichloroethylene
0.5
< 0.050
1, 1 -Dichloroethylene
0.7
< 0.050
2,4,5-Trichlorophenol
400.0
< 0.040
24-Dhutrotoluene
0.13
< 0.080
2,4,6-Trichlorophenol
2.0
< 0.040
Endrin
0.02
< 0.00040
2,4,5-TP (Silvex)
1.0
< 0.0050
Heptachlor and its Hydroxide
0.008
< 0.00040
Vinyl Chloride
0.2
< 0.010
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 05/16/2023 (date sampled)
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(ClassA Only)
(mg1kg)
Result
(mg1kg)
Arsenic
75
41
< 2.2
Cadmium
85
39
< 0.74
Copper
4,300
1,500
25
Lead
840
300
< 1.5
Mercury
57
17
< 0.82
Molybdenum
75
n/a
< 5.9
Nickel
420
420
< 5.9
Selenium
100
100
< 2.9
Zinc
7,500
2,800
33
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: = and Date of analysis: =
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
> 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 9.73 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
nucronutnent parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 05/16/2023 (date sampled)
Parameter
Result
(mg1kg)
Aluminum
260
Ammonia -Nitrogen
1600
Calcium
< 740
Magnesium
< 740
Nitrate -Nitrite Nitrogen
17
pH (Standard Unit)
4.2
Phosphorus
1400
Potassium
< 740
Sodium
< 740
Total Kjeldahl Nitrogen
15000
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 1_4
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: %. This
rate is a (check one): ❑ default value, or 0 actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1'� Year PAN
Five -Year
Maximum Adjusted PAN
(mg1kg)
(mg/kg)
Surface
6,200
9,050
Injection/Incorporation
7,000
9,850
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
J Alternative 1 [15A NCAC 02T.1106(b)(3)(A)] -Time/Temperature Compliance.
J Alternative 2 [15A NCAC 02T.I106(b)(3)(B)] - Alkaline Treatment.
J Alternative 3 [15A NCAC 02T.I106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
J Alternative 4 [15A NCAC 02T.I106(b)(3)(D)] - No Prior Testing for Enteric Vims/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: 77 composting, � heat drying, r] heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of'Class B:
Alternative 1 [15A NCAC 02T. I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T. I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: [I aerobic digestion, I
air drying, ❑ anaerobic digestion,
❑ composting, or lime stabilization.
c. For Surface Disposal:
J Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item IL 7a. above.
J Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item IL 7b. above.
J Exempt -If Daily Cover Alternative is chosen in Item IL8. below [15A NCAC 02T.1106(a)(2)].
J Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
E] Alternative 2 [15A NCAC 02T. I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
El Alternative 3 [15A NCAC 02T. I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
El Alternative 4 [15A NCAC 02T. I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
El Alternative 5 [15A NCAC 02T. I 107(a)(5)] - 14-Day Aerobic Processes.
El Alternative 6 [15A NCAC 02T. I 107(a)(6)] - Alkaline Stabilization.
El Alternative 7 [15A NCAC 02T. I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T. I 107(a)(8)] - Drying of Unstabilized Residuals.
Alternative 9 [15A NCAC 02T. I 107(a)(9)] - Injection.
Alternative 10 [15A NCAC 02T. I 107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T. I107(b)(2)].
Q Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

RSC 06-16
WAYNE FARMS-DOBSON, NC

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 06-16
L RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Facility Name: Wayne Farms — Dobson Fresh Plant
2. Facility permit holder is: Federal, 0 State, 0 Local Government, or ❑ Private.
Facility permit issued by: ® Div. of Water Resources, ❑ Div. of Environmental Health,
or ❑ Other (explain: M).
3. Facility contact person and title: Jeremy Bowfin; Complex Environmental Manager
Complete mailing address: 802 East Atkins St
City: Dobson State: NC Zip: 27017
Telephone number: [phone] E-mail address: jeremy.bowlin(dwaynefarms.com
4. Facility physical address: 802 East Atkins St
City: Dobson State: NC Zip: 27017
Coordinates: Latitude: 36' 23' 25" Longitude: 80' 42' 41"
Datum: NAD 83 Level of accuracy: Nearest Second
Method of measurement: MAP
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: = % industrial and = % domestic)
other (explain:).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: 0.70 MGD and facility average daily flow: 0.68 MGD
8. Average amount of residuals being generated at this facility 1,170 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: 100% generated from solids removed from D.A.F. (pre-treatment)
Type and volume of residuals storage (i.e., outside of residuals treatment units): 500,000 gal EQ and 3,000 gal DAF
residuals collection (dU) tank
IL RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under
40 CFR Part 503 or [jj 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
JE Biological 0 Non -Biological
FORM: RSC 06-16 Page 1 of 5

Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a. Are the residuals listed in 40 CFR §261.31-§261.33: 0 yes no.
If yes, list the number(s): =
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
261.24: 0 yes 0 no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 5/04/2023 (date collected)
Passed corrosivity test: yes ?!? no. pH: s.u. (2 <pH < 12.5)
Passed ignitability test: yes Fj no. Flashpoint > 140 OF (> 140°F)
Passed reactivity test: Eyes Ono. HCN: < 50 mg/kg (<250) & HzS: < 50 mg/kg (<500)
TCLP Parameter
Limit
(mg/l)
Result
(mg/l)
TCLP Parameter
Limit
(mg/l)
Result
(mg/l)
Arsenic
5.0
< 0.15
Hexachlorobenzene
0.13
< 0.040
Barium
100.0
0.46
Hexachloro-1,3-Butadiene
0.5
< 0.040
Benzene
0.5
< 0.050
Hexachloroethane
3.0
< 0.040
Cadmium
1.0
< 0.050
Lead
5.0
< 0.10
Carbon Tetrachloride
0.5
< 0.050
Lindane
0.4
< 0.00040
Chlordane
0.03
< 0.0040
Mercury
0.2
< 0.0020
Chlorobenzene
100.0
< 0.050
Methoxychlor
10.0
< 0.016
Chloroform
6.0
< 0.050
Methyl Ethyl Ketone
200.0
< 0.10
Chromium
5.0
< 0.10
Nitrobenzene
2.0
< 0.040
m-Cresol
200.0
0.12
Pentachlorophenol
100.0
< 0.20
o-Cresol
200.0
< 0.040
Pyridine
5.0
< 0.040
p-Cresol
200.0
0.12
Selenium
1.0
< 0.20
Cresol
200.0
0.12
Silver
5.0
< 0.10
2,4-D
10.0
< 0.020
Tetrachloroethylene
0.7
< 0.050
1,4-Dichlorobenzene
7.5
< 0.040
Toxaphene
0.5
< 0.0080
1,2-Dichloroethane
0.5
< 0.050
Trichloroethylene
0.5
< 0.050
1, 1 -Dichloroethylene
0.7
< 0.050
2,4,5-Trichlorophenol
400.0
< 0.040
24-Dhutrotoluene
0.13
< 0.080
2,4,6-Trichlorophenol
2.0
< 0.040
Endrin
0.02
< 0.00040
2,4,5-TP (Silvex)
1.0
< 0.0050
Heptachlor and its Hydroxide
0.008
< 0.00040
Vinyl Chloride
0.2
< 0.010
FORM: RSC 06-16 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 5/04/2023 (date collected)
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB)
(mglkg)
Monthly Average
Concentration Limits
(ClassA Only)
(mg1kg)
Result
(mg1kg)
Arsenic
75
41
< 0.8
Cadmium
85
39
< 27
Copper
4,300
1,500
47
Lead
840
300
< 0.54
Mercury
57
17
< 0.26
Molybdenum
75
n/a
< 2.1
Nickel
420
420
4.4
Selenium
100
100
< 1.1
Zinc
7,500
2,800
150
b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: = and Date of analysis: =
Distance from Disposal
Unit to Boundary to
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
(mg/kg)
> 0 but < 25
30
200
210
❑ > 25 but < 50
34
220
240
❑ > 50 but < 75
39
260
270
❑ > 75 but < 100
46
300
320
❑ > 100 but < 125
53
360
390
❑ > 125
62
450
420
Result (mg/kg)
FORM: RSC 06-16 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 27.7 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
nucronutnent parameters:
Laboratory: Pace Analytical Services, LLC and Date of analysis: 5/04/2023 (date collected)
Parameter
Result
(mg1kg)
Aluminum
230
Ammonia -Nitrogen
8600
Calcium
19000
Magnesium
440
Nitrate -Nitrite Nitrogen
22
pH (Standard Unit)
5.6
Phosphorus
3400
Potassium
650
Sodium
560
Total Kjeldahl Nitrogen
61000
c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 0_6
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 40 %. This
rate is a (check one): 0 default value, or 0 actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, ex lain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals:
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1s) Year PAN
Five -Year
Maximum Adjusted PAN
(mg1kg)
(mg/kg)
Surface
25,300
36,550
Injection/Incorporation
29,600
40,850
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses:
FORM: RSC 06-16 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
J Alternative 1 [15A NCAC 02T.1106(b)(3)(A)] -Time/Temperature Compliance.
J Alternative 2 [15A NCAC 02T.I106(b)(3)(B)] - Alkaline Treatment.
J Alternative 3 [15A NCAC 02T.I106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
J Alternative 4 [15A NCAC 02T.I106(b)(3)(D)] - No Prior Testing for Enteric Vims/Viable Helminth Ova.
Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: 77 composting, � heat drying, r] heat treatment,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation,
❑ gamma ray irradiation, or ❑ pasteurization.
b. For Land Application of'Class B:
Alternative 1 [15A NCAC 02T. I 106(c)(1)] - Fecal Coliform Density Demonstration.
Alternative 2 [15A NCAC 02T. I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: [I aerobic digestion, I
air drying, ❑ anaerobic digestion,
❑ composting, or lime stabilization.
c. For Surface Disposal:
J Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item IL 7a. above.
J Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item IL 7b. above.
J Exempt -If Daily Cover Alternative is chosen in Item IL8. below [15A NCAC 02T.1106(a)(2)].
J Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
E] Alternative 2 [15A NCAC 02T. I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
El Alternative 3 [15A NCAC 02T. I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
El Alternative 4 [15A NCAC 02T. I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
El Alternative 5 [15A NCAC 02T. I 107(a)(5)] - 14-Day Aerobic Processes.
El Alternative 6 [15A NCAC 02T. I 107(a)(6)] - Alkaline Stabilization.
El Alternative 7 [15A NCAC 02T. I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T. I 107(a)(8)] - Drying of Unstabilized Residuals.
Alternative 9 [15A NCAC 02T. I 107(a)(9)] - Injection.
Alternative 10 [15A NCAC 02T. I 107(a)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T. I107(b)(2)].
Q Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 06-16 Page 5 of 5

ATTACHMENT - A:
RESIDUALS SOURCE VICINTY MAP

Google Maps Danville, Virginia to 1725 Cane Creek Pkwy, Ringgold, VA 24586
Drive 6.1 miles, 11 min
Site location & directions from downtown Danville VA to Tyson Foods (Danville)
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Danville
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Take Patton St to Doctor M.L.K. Jr Mem Brg/Dr M.L.K. Jr
Mem Brg/Main St
2 min (0.4 mi)
j 1. Head southeast on S Ridge St toward Patton St
417 ft
2. Turn left at the 1 st cross street onto Patton St
0.3 mi
Take South Boston Rd to Cane Creek Pkwy
6 min (4.0 mi)
j 3. Continue straight onto Doctor M.L.K. Jr Mem
Brg/Dr M.L.K. Jr Mem Brg/Main St
0.2 mi
4. Turn right onto River St
0.6 mi
f 5. Continue onto South Boston Rd
0.9 mi
Fl 6. Keep left to stay on South Boston Rd
1.1 mi
T 7. Continue straight past Hardee's to stay on South
Boston Rd
0 Pass by Piggly Wiggly (on the right)
1.3 mi
Drive to Cane Creek Pkwy in Pittsylvania County
3 min (1.7 mi)
Fl 8. Turn left onto Cane Creek Pkwy
0.6 mi
9. Turn right to stay on Cane Creek Pkwy
1.1 mi
1725 Cane Creek Pkwy
Ringgold, VA 24586

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ATTACHMENT - B:
RESIDUALS PRODUCTION PROCESS DESCRIPTION

RESIDUALS PRODUCTION PROCESS DESCRIPTION
Tyson — Danville is a poultry processing facility (NAICS Code 311615). Wastewater is mainly generated
from the wash -down of the production equipment in the plant. The wastewater is sent to an "EQ' tank
or basin where the pH is adjusted to promote coagulation. From the EQ tank, the water travels through
a flocculation tank where polymers are added to flocculate the solids. The water then enters a dissolved
air flotation (DAF) unit where air is injected into the water column from below and the solids are forced
to the surface. The solids are skimmed off the surface by revolving rakes or blades into a hopper or
tank. From there, they are pumped or gravity flowed into holding tanks to await transfer to tanker
trucks for transport to the field. These are the residuals to be land applied.
The following flow description was provided by the Environmental Manager at the facility. A diagram
showing the components is provided on the following page.
1) Flow goes through the offal to the lift station...
2) Lift station to EQtank ...
3) EQ tank to DAF-1...
4) DAF-1 to aeration tank...
5) Aeration tank to DAF-2...
6) Sludge from DAF-2 sent to sludge thickener...
7) Sludge thickener to sludge tank located outside...
8) Water from DAF-2 sent to POTW for final treatment.
The residuals to be land applied under this permit will be collected from the "sludge tank located
outside".

EM
❑C
Customer: Tyson Foods
Location: Danville, VA
Document #: 21012026
Status: For Review
Date:1112812022
Notes:
Provide insulated ground wire in all ra
1 1 2 1 3 1 4
Customer. Tyson Foods
Location: Danville, VA
Document#: 2101202G
Status: For Review
Date: 02f 03f 2023
Notes:
Size per NEC and local regulations. 112rovide insulated ground wire in all raceways. Size per NEC and local regulations.
48DV Power
Item #
Voltage
PID Tag
# Of Conductors
Conductor Type
uctorWeight(i
Outside Diameter(inch)
Cross Section (inch^2)
From DI S T1
480VAC
BW9001A - Aeration Tank Blower "A"
3 (350kcMIL) + Ground
RHW-2 3xConduct_ + Ground
4.677
2.08
3.398
480VAC
BW9001B - Aeration Tank Blower "B"
3 (350kcMIL) + Ground
RHW-2 3xConduct_ + Ground
4.677
2.08
3.398
480VAC
BW9001C - Aeration Tank Blower "C"
3 (350kcMIL) + Ground
RHW-2 3xConduct_ + Ground
4.677
2.08
3.398
480VAC
P1002A - EQ Feed Pump "A''
3 (1AWG) + Ground
RHW-2 3xConduct_ + Ground
1.334
1.22
1.169
480VAC
P1002B - EQ Feed Pump "B''
3 (1AWG) + Ground
RHW-2 3xCanduct_ + Ground
1.334
1.22
1.169
480VAC
P1002C- EQ Feed Pump "C''
3 (1AWG) + Ground
RHW-2 3xConduct_ + Ground
1.334
1.22
1.169
480VAG
CMP9501 - AirCompressor
3 (10AWG) + Ground
RHW-2 3xConduct. + Ground
0.279
0.63
0.312
FROM MCP
1VFD
480VAC
P6002A -Aeration Feed Pump ''A''
4 (10AW G), 2 (18AWG)
OLFLEXVFD CABLE - 70071
0.354
0.798
0.500
2VFD
480VAC
P6002B -Aeration Feed Pump ''B''
4 (10AW G), 2 (18AWG)
OLFLEXVFD CABLE - 70071
0.354
0.798
0.500
3VFD
480VAC
P2001A - DAF Feed Pump "A"
4 (10AW G), 2 (18AWG)
QLFLEXVFD CABLE - 70071
0.354
0.798
0.500
4VFD
480VAC
P2001 B - DAF Feed Pump "B"
4 (10AW G), 2 (18AWG)
DLFLEXVFD CABLE - 70071
0.354
0.798
0.500
SVFD
480VAC
P9001A - DAF7001 Feed Pump "A"
4 (12AW G), 2 (18AWG)
DLFLEXVFD CABLE - 70071
0.294
0.752
0.444
6VFD
480VAC
P9001 B - DAF7001 Feed Pump "B"
4 (12AW G), 2 (18AWG)
DLFLEXVFD CABLE - 70071
0.294
0.752
0.444
7VFD
430VAC
P8004A - Sludge Transfer Pump "A"
4 (12AW G), 2 (18AWG)
XFLEXVFD CABLE - 70071
0.294
0.752
0.444
8VFD
480VAG
P8004B - Sludge Transfer Pump "B"
4 (12AW G), 2 (18AWG)
DLFLEXVFD CABLE - 70071
0.294
0.752
0.444
9VFD
480VAG
P8005 - Sludge Loadout Pump
4 (12AW G), 2 (18AWG)
DLFLEXVFD CABLE - 70071
0.294
0.752
0.444
10VFD
480VAC
P8002A - Sludge Sump Pump "A"
4 (12AW G), 2 (18AWG)
DLFLEXVFD CABLE - 70071
0.294
0.752
0.444
11VF❑
480VAC
P0002B - Sludge Sump Pump "B"
4 (12AW G), 2 (18AWG)
DLFLEXVFD CABLE - 70071
0.294
0.752
0.444
12VF❑
480VAC
SC6005- DAF6001 Skimmer Drive
4 (14AWG), 2 (18AWG)
DLFLEXVFD CABLE - 700711
0.252
0.687
0.371
13VF❑
480VAC
SC7005- DAF7001 Skimmer Drive
4 (14AWG), 2 (18AWG)
XFLEXVFD CABLE - 700711
0.252
0.687
0.371
14VFD
480VAC
SC8003 - STS003 Skimmer Drive
4 (14AW G), 2 (18AWG)
DLFLEXVFD CABLE - 700711
0.252
0.687
0.371
15VF❑
480VAC
P8001A - RASIWAS Pump "A"
4 (12AW G), 2 (18AWG)
DLFLEXVFD CABLE - 700712
0.294
0.752
0.444
16VF❑
480VAC
P8001 B - RASIWAS Pump "B"
4 (12AW G), 2 (18AWG)
OLFLEXVFD CABLE - 70071
0.294
0.752
0.444
7.110
15M
480VAC
XFA2003 - EQ Tank XTA Unit
3 (1AWG) + Ground
RHW-2 3xGonduct_ + Ground
1.334
1.22
1.169
16M
480VAC
SA2002 - EQ Tank Surface Aerator
3 (12AWG) + Ground
RHW-2 3xConduct_ + Ground
0209.
0.57
0.255
17M
480VAC
P6001A - DAF6001 Recycle Pump "A"
3 (SAW G) + Ground
RHW-2 3xConduct_ + Ground
0.356
0.7
0.305
18M
480VAC
P6001B - DAF6001 Recycle Pump "B"
3 (8AWG) + Ground
RHW-2 3xGonduct. + Ground
0.358
0.7
0.385
19M
480VAC
P7001A - DAF7001 Recycle Pump "A"
3 (8AWG) + Ground
RHW-2 3xGonduct_ + Ground
0.358
0.7
0.305
20M
480VAC
P7001B - DAF7001 Recycle Pump "B"
3 (8AWG) + Ground
RHW-2 3xGonduct_ + Ground
0.358
0.7
0.385
21M
480VAC
P4001A - Drain Sump Pump ''A''
3 (12AWG) + Ground
RHW-2 3xGonduct_ + Ground
0209.
0.57
0.255
22M
480VAC
P4001B - Drain Sump Pump ''B''
3 (12AWG) + Ground
RHW-2 3xConduct_ + Ground
0209.
0.57
0.255
23M
480VAC
AU6006 - DAF6001 Auger Drive
3 (12AWG) + Ground
RHW-2 3xConduct_ + Ground
0209.
0.57
0.255
24M
480VAC
AU7006 - DAF7001 Auger Drive
3 (12AWG) + Ground
RHW-2 3xConduct_ + Ground
0209.
0.57
0.255
3.984
REFERENCE DRAWINGS:
21012026 TYSON - DANVILLE, VA P&ID
FRC-P0.01, FRC-P0.02- PIPING DRAWINGS
FRC-M1.01 TO M1.04 - MECHANICAL DRAWINGS
FRC-E2.00 - ELECTRICAL SPEC
NOTES:
1. ALL DIMENSIONS ARE FEET AND INCHES
2. GENERAL DRAWING - FOR REFERENCE ONL'
3. CONFIRM ALL DIMENSIONS IN FIELD
4. REFER TO P&ID FOR ALL CONNECTIONS
5. SUPERSEDES FRC-E2.01 THRU E2.04 DUE TO
NUMBERING CONFLICT
1
5
It
7
480V Power
Item#
I Voltage
Conduit #(Sizel
PIDTag
Wire Numbers
#Of Conductors
ConductorType
uctorWeight(l
OutsideDiameter(inch)
Cross Sectiion(inch"2)
From Cable Tray to Field
480VAC
P4(1-114")
P1002A -EQ Feed Pump"A.
P1002A-L1,L2,L3, G
3 (1AW3)+ Grouna
RHN -2 ax Con du ct. +GrouInd
1.334
1.22
1.169
480VAC
P5(1-1A"`
P1002D -EQ Feed Pump"D
P1002B-L1,L2,L3, G
3 (1AWG)+ Ground
RHN -2 ax Con du ct. +GrouInd
1.334
1.22
1.169
480VAC
P6 (1-114"r
P1002C - EQ Feed Pump-C-
P1002C-L1,L2,L3, G
3 (1AW3)+ Ground
RHW-23xConduct. + Ground
1.334
1.22
1.169
91
Tyson
TYSON FOODS INC,
MANUFACTURING SERVICES
2200 W. DON TYSON PKWY.-P.O.BOX 2020
RKANSAS 72762
1-643-3410
G ISSUE
DESCRIPTION I #
;T RELEASE 0
� PROPRIETARY
')PECIFICATIONS HERE -ON
TYSON FOODS INC. AND
=D WITHOUT ITS PRIOR
ESE DOCUMENTS ARE
;LOSURE UNDER 5 U.S.C.
552 (B)(4)."
-NCE OF BUILDING
ohnson
ative I
RBEILT BUSINESS CENTER DRIVE
ST.. ILOUIIS, MIISSOURII 6311114
Ph 3114.419..110110
ZOW
6a
•
04
-4
1_
074
�G MAP
DANVILLE, VA
4-22
�A
F
rZ
NN VIEW
-E3.02
25.006314
0- F
Ifl
C
ic

ATTACHMENT - C:
QUANTITATIVE JUSTIFICATION for RESIDUALS PRODUCTION RATE

Quantitive Justification for Residuals Production Rate
NC DEQ RLAP Permit At WQ0038087
Permittee: Terra Renewal Services
Amount of Dry Tons to be Certified based on Historical Data
2020
(Dry Tons/Yr)
2021
(Dry Tons/Yr)
2022
(Dry Tons/Yr)
3 YR A VG
(Dry Tons/Yr)
Amount to
be Certified
(Dry Tons/Yr)
Residuals Source
Tyson -Wilkesboro
866
740
7521
803
2,000
RVI (Tyson) -Harmony
538
842
406 1
690
1,700
Tyson -Danville
N/A
N/A
N/A
N/A
1,300
Advance Pierre-Cla remont
14
14
14
14
35
Wayne Farms -Dobson
0
0
0
0
750
Mathis-1
N/A*
N/A*
N/A*
N/A*
N/A*
Total: 5,785
1) Includes dry tons placed in storage and land applied in calendar year 2022 based on percent from each generator
Weighted Average for PAN Calculations
2023 Modification
Actual PAN Concentration
Proportion Adjusted PAN Concentration
Year 1
Year 5
Year 1
Year 5
Residuals Source
Est. Volume
(Dry Tons/Yr)
Percent
NO
Surface PAN
(lbs/DT)
Inject PAN
(lbs/DT)
Surface PAN
(lbs/DT)
Inject PAN
(lbs/DT)
Surface PAN
(lbs/DT)
Inject PAN
(lbs/DT)
Surface PAN
(lbs/DT)
Inject PAN
(lbs/DT)
Tyson -Wilkesboro
2,000
35%
12.4
14.0
18.1
19.7
4.3
4.8
6.3
6.8
RVI (Tyson) -Harmony
1,700
29%
28.7
47.7
33.9
53.0
8.4
14.0
10.0
15.6
Tyson -Danville
1,300
22%
75.4
80.2
113.4
118.2
16.9
18.0
25.5
26.6
Advance Pierre-Cla remont
35
1%
0.7
0.8
0.9
1.1
0.0
0.0
0.0
0.0
Wayne Farms -Dobson
750
13%
50.6
73.1
59.2
81.7
6.6
9.5
7.7
10.6
Mathis-1
N/A*
N/A*
N/A*
N/A*
N/A*
N/A*
N/A*
N/A*
N/A*
N/A*
Total: 5,785 100%
Weighted Average: 36.2 46.4 49.4 59.5
* N/A due to pass through of storage. Residuals are comingled and not generated. Volume of residuals stored will vary from year to year. Mathis-1 is to be certified and sampled as
separate source due to change in characteristics after comingling; however, this should not change the quantity of Dry Tons generated by each facility.

Surface Application PAN
Tyson -Danville
TKN= 93000 mg/kg
NH3= 4800 mg/kg
NO3-NO2-N= 24 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO2] * 0.002
0.40 88,200 2,400 24.00
PAN= 75.41 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 88,200 35,280
PAN= 21.17 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 52,920 10,584
PAN= 9.03 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 42,336 4,516
PAN= 5.04 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 37,820 2,521
PAN= 2.74 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 37.98 Lbs/Pan/DT
Total five-year max. adjusted PAN = 113.39 Lbs/Pan/DT

Incorporation Application PAN
Tyson -Danville
TKN= 93000 mg/kg
NH3= 4800 mg/kg
NO3-NO2-N= 24 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 1.0*(NH3) + NO3-NO2] * 0.002
0.40 88,200 4,800 24.00
PAN= 80.21 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 88,200 35,280
PAN= 21.17 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 52,920 10,584
PAN= 9.03 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 42,336 4,516
PAN= 5.04 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 37,820 2,521
PAN= 2.74 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 37.98 Lbs/Pan/DT
Total five-year max. adjusted PAN = 118.19 Lbs/Pan/DT

Surface Application PAN
Advance Pierre -Claremont
TKN= 720 mg/kg
NH3= 170 mg/kg
NO3-NO2-N= 21 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO2] * 0.002
0.40 550 85 21.00
PAN= 0.65 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 550 220
PAN= 0.13 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 330 66
PAN= 0.06 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 264 28
PAN= 0.03 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 236 16
PAN= 0.02 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 0.24 Lbs/Pan/DT
Total five-year max. adjusted PAN = 0.89 Lbs/Pan/DT

Incorporation Application PAN
Advance Pierre -Claremont
TKN=
720 mg/kg
NH3=
170 mg/kg
NO3-NO2-N=
21 mg/kg
Min Rate=
0.40
PAN=
[min.rate (TKN - NH3) + 1.0*(NH3) + NO3-NO2] * 0.002
0.40 550 170 21.00
PAN=
0.82 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 550 220
PAN= 0.13 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 330 66
PAN= 0.06 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 264 28
PAN= 0.03 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 236 16
PAN= 0.02 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 0.24 Lbs/Pan/DT
Total five-year max. adjusted PAN = 1.06 Lbs/Pan/DT

Surface Application PAN
Mathis-1 Storage
TKN= 20000 mg/kg
NH3= 2400 mg/kg
NO3-NO2-N= 40 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO2] * 0.002
0.40 17,600 1,200 40.00
PAN= 16.56 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 17,600 7,040
PAN= 4.22 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 10,560 2,112
PAN= 1.80 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 8,448 901
PAN= 1.01 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 7,547 503
PAN= 0.55 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 7.58 Lbs/Pan/DT
Total five-year max. adjusted PAN = 24.14 Lbs/Pan/DT

Incorporation Application PAN
Mathis-1 Storage
TKN= 20000 mg/kg
NH3= 2400 mg/kg
NO3-NO2-N= 40 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 1.0*(NH3) + NO3-NO2] * 0.002
0.40 17,600 2,400 40.00
PAN= 18.96 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 17,600 7,040
PAN= 4.22 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 10,560 2,112
PAN= 1.80 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 8,448 901
PAN= 1.01 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 7,547 503
PAN= 0.55 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 7.58 Lbs/Pan/DT
Total five-year max. adjusted PAN = 26.54 Lbs/Pan/DT

Surface Application PAN
RVI-Harmony
TKN= 31000 mg/kg
NH3= 19000 mg/kg
NO3-NO2-N= 59 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO2] * 0.002
0.40 12,000 9,500 59.00
PAN= 28.72 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 12,000 4,800
PAN= 2.88 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 7,200 1,440
PAN= 1.23 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 5,760 614
PAN= 0.69 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 5,146 343
PAN= 0.37 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 5.17 Lbs/Pan/DT
Total five-year max. adjusted PAN = 33.89 Lbs/Pan/DT

Incorporation Application PAN
RVI-Harmony
TKN= 31000 mg/kg
NH3= 19000 mg/kg
NO3-NO2-N= 59 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 1.0*(NH3) + NO3-NO2] * 0.002
0.40 12,000 19,000 59.00
PAN= 47.72 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 12,000 4,800
PAN= 2.88 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 7,200 1,440
PAN= 1.23 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 5,760 614
PAN= 0.69 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 5,146 343
PAN= 0.37 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 5.17 Lbs/Pan/DT
Total five-year max. adjusted PAN = 52.89 Lbs/Pan/DT

Surface Application PAN
Tyson -Wilkesboro
TKN= 15000 mg/kg
NH3= 1600 mg/kg
NO3-NO2-N= 17 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO2] * 0.002
0.40 13,400 800 17.00
PAN= 12.35 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 13,400 5,360
PAN= 3.22 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 8,040 1,608
PAN= 1.37 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 6,432 686
PAN= 0.77 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 5,746 383
PAN= 0.42 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 5.77 Lbs/Pan/DT
Total five-year max. adjusted PAN = 18.12 Lbs/Pan/DT

Incorporation Application PAN
Tyson -Wilkesboro
TKN= 15000 mg/kg
NH3= 1600 mg/kg
NO3-NO2-N= 17 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 1.0*(NH3) + NO3-NO2] * 0.002
0.40 13,400 1,600 17.00
PAN= 13.95 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 13,400 5,360
PAN= 3.22 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 8,040 1,608
PAN= 1.37 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 6,432 686
PAN= 0.77 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 5,746 383
PAN= 0.42 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 5.77 Lbs/Pan/DT
Total five-year max. adjusted PAN = 19.72 Lbs/Pan/DT

Surface Application PAN
Wayne Farms -Dobson
TKN= 61000 mg/kg
NH3= 8600 mg/kg
NO3-NO2-N= 22 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 0.5 (NH3) + NO3-NO2] * 0.002
0.40 52,400 4,300 22.00
PAN= 50.56 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 52,400 20,960
PAN= 12.58 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 31,440 6,288
PAN= 5.37 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 25,152 2,683
PAN= 3.00 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 22,469 1,498
PAN= 1.63 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 22.56 Lbs/Pan/DT
Total five-year max. adjusted PAN = 73.13 Lbs/Pan/DT

Incorporation Application PAN
Wayne Farms -Dobson
TKN= 61000 mg/kg
NH3= 8600 mg/kg
NO3-NO2-N= 22 mg/kg
Min Rate= 0.40
PAN= [min.rate (TKN - NH3) + 1.0*(NH3) + NO3-NO2] * 0.002
0.40 52,400 8,600 22.00
PAN= 59.16 LBS/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of PAN/DT remaining.
2ND YEAR RESIDUAL PAN
PAN= [min.rate (1st year org. - N 2nd year min. - N] * 0.002
0.20 52,400 20,960
PAN= 12.58 LBS/DT remaining from 1 st year application
3RD YEAR RESIDUAL PAN
PAN= [min.rate (2nd year org. - N 3rd year min. - N] * 0.002
0.11 31,440 6,288
PAN= 5.37 LBS/DT remaining from 1 st year application
4TH YEAR RESIDUAL PAN
PAN= [min.rate (3rd year org. - N 4th year min. - N] * 0.002
0.07 25,152 2,683
PAN= 3.00 LBS/DT remaining from 1 st year application
5TH YEAR RESIDUAL PAN
PAN= [min.rate (4th year org. - N 5th year min. - N] * 0.002
0.04 22,469 1,498
PAN= 1.63 LBS/DT remaining from 1 st year application
Residual PAN from years 2 thru 5 after the initial application = 22.56 Lbs/Pan/DT
Total five-year max. adjusted PAN = 81.73 Lbs/Pan/DT

ATTACHMENT - D:
ANALYTICAL DATA for RESIDUALS

TYSON-DANVI LLE, VA

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: Tyson - Danville
Lot Number:YF09017
Date Completed:06/30/2023
06/30/2023 11:42 AM
Approved and released by:
Project Manager II: Lucas Odom
P RCGip0,
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TNI :
1N81 xer ava a �rcd srew Bsam
J/
ACC RE D1TED
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The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 11

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: YF09017
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18, PFAS by Isotope Dilution SOP.
Pace is a DoD/DoE and TNI accredited laboratory; however, Pace is not accredited for PFAS Direct
Aqueous Injection or Method D8421.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Non -Metals
The Phosphorus method blank for analytical batch 77735 was greater than the acceptance criteria. The
associated samples, were at concentrations greater than 1 OX the value found in the method blank;
therefore sample results are not impacted. The data has been reported.
Inorganic Metals
The following sample was classified as biosolid therefore in order to ensure proper digestion, the sample
was weighed out at 3.0 - 3.5 grams: YF09017-001. The LOQ has been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
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Page 2 of 11

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: YF09017
Sample Number Sample ID Matrix Date Sampled Date Received
001 Tyson -Danville (REP) Solid 06/08/2023 1545 06/09/2023
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 11

PACE ANALYTICAL SERVICES,
LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: YF09017
Sample
Sample ID
Matrix Parameter Method
Result Q
Units
Page
001
Tyson -Danville (REP)
Solid % Volatile Solids SM 2540G-
98
%
5
001
Tyson -Danville (REP)
Solid Ammonia - N (gas 350.1
4800
mg/kg
5
001
Tyson -Danville (REP)
Solid Flashpoint (Pensky- 1010B
>140
° F
5
001
Tyson -Danville (REP)
Solid Nitrate -Nitrite - N (soluble) 353.2
24
mg/kg
5
001
Tyson -Danville (REP)
Solid Paint Filter Test 9095B
Fail
pass/fail
5
001
Tyson -Danville (REP)
Solid Phosphorus 365.1
5400
mg/kg
5
001
Tyson -Danville (REP)
Solid TKN 351.2
93000
mg/kg
5
001
Tyson -Danville (REP)
Solid Copper 6010D
56
mg/kg
8
001
Tyson -Danville (REP)
Solid Zinc 6010D
44
mg/kg
8
(9 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 11

Client: Terra Renewal Services, Inc. Laboratory ID:YF09017-001
Description: Tyson -Danville (REP) Matrix: Solid
Date Sampled:06/08/2023 1545 % Solids: 4.01 06/20/2023 0010
Date Received:06/09/2023
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
06/15/2023 2100 CBP
77790
1 350.1
(Ammonia - N ) 350.1
10
06/13/2023 1205 CMM
77486
1
(Flashpoint () 1010B
1
06/20/2023 1942 CBP
78175
1
(Nitrate-Nitr) 353.2
1
06/22/2023 1413 C1_1_2
78426
1
(Paint Filter) 9095B
1
06/21/2023 1435 GGC
1
(Phosphorus) 365.1
5
06/13/2023 1538 BMG2
06/12/2023 2006 77469
1
(Reactive Cya) 7.3.3
1
06/21/2023 1835 NAB
06/20/2023 1942
1
(Reactive Sul) 7.3.4
1
06/21/2023 1022 CVR
06/20/2023 1205
1
(Soil pH meas) 9045D
1
06/14/2023 1235 LMM2
77276
1 351.4
(TKN) 351.2
5
06/13/2023 1226 DMA
06/12/2023 1908 77468
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
98
%
1
Ammonia - N (gas diffusion)
350.1
4800
2500
mg/kg
1
Flashpoint (Pensky-Martens Closed -Cup)
1010B
>140
140
o F
1
Nitrate -Nitrite - N (soluble)
353.2
24
5.0
mg/kg
1
Paint Filter Test
9095B
Fail
pass/fail
1
Phosphorus
7723-14-0 365.1
5400
620
mg/kg
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water @ 17.4 ° C
9045D
4.4
su
1
TKN
351.2
93000
6200
mg/kg
1
TCLP Volatiles
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B 8260D
10 06/22/2023 1530 AMR2
78340 06/12/2023 1905
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Benzene
71-43-2 8260D
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
0.10
mg/L
1
Carbon tetrachloride
56-23-5 8260D
ND
0.050
mg/L
1
Chlorobenzene
108-90-7 8260D
ND
0.050
mg/L
1
Chloroform
67-66-3 8260D
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
0.050
mg/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
0.050
mg/L
1
Tetrachloroethene
127-18-4 8260D
ND
0.050
mg/L
1
Trichloroethene
79-01-6 8260D
ND
0.050
mg/L
1
Vinyl chloride
75-01-4 8260D
ND
0.010
mg/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 11

Client: Terra Renewal Services, Inc. Laboratory ID:YF09017-001
Description: Tyson -Danville (REP) Matrix: Solid
Date Sampled:06/08/2023 1545 % Solids: 4.01 06/20/2023 0010
)ate Received:06/09/2023
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
98 70-130
1,2-Dichloroethane-d4
100 70-130
Toluene-d8
101 70-130
TCLP Semivolatiles
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8270E 1 06/20/2023 2213 JCG
06/14/2023 1623 77627 06/12/2023 1905
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
1,4-Dichlorobenzene
106-46-7 8270E
ND
0.040
mg/L
1
2,4-Dinitrotoluene
121-14-2 8270E
ND
0.080
mg/L
1
Hexachlorobenzene
118-74-1 8270E
ND
0.040
mg/L
1
Hexachlorobutadiene
87-68-3 8270E
ND
0.040
mg/L
1
Hexachloroethane
67-72-1 8270E
ND
0.040
mg/L
1
2-Methylphenol
95-48-7 8270E
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5 8270E
ND
0.040
mg/L
1
Nitrobenzene
98-95-3 8270E
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5 8270E
ND
0.20
mg/L
1
Pyridine
110-86-1 8270E
ND
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4 8270E
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2 8270E
ND
0.040
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
74 37-129
2-Fluorophenol
45 24-127
Nitrobenzene-d5
78 38-127
Phenol-d5
67 28-128
Terphenyl-d14
80 10-148
2,4,6-Tribromophenol
70 41-144
TCLP Herbicides
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date
Batch Leachate Date
1 1311/8151A
8151A 1 06/21/2023 1901 JMR 06/15/2023 1025 77706 06/12/2023 1905
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units Run
2,4-D
94-75-7 8151A ND
0.020
mg/L 1
2,4,5-TP (Silvex)
93-72-1 8151A ND
0.0050
mg/L 1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
50 50-112
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 11

Client: Terra Renewal Services, Inc. Laboratory ID:YF09017-001
Description: Tyson -Danville (REP) Matrix: Solid
Date Sampled:06/08/2023 1545 % Solids: 4.01 06/20/2023 0010
Date Received:06/09/2023
PCBs by GC
Run Prep Method Cleanup Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3550C 366013/3665A 8082A 1 06/15/2023 1102 MEZ 06/14/2023 1723 77658
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Aroclor 1016
12674-11-2
8082A
ND
420
ug/kg
1
Aroclor 1221
11104-28-2
8082A
ND
420
ug/kg
1
Aroclor 1232
11141-16-5
8082A
ND
420
ug/kg
1
Aroclor 1242
53469-21-9
8082A
ND
420
ug/kg
1
Aroclor 1248
12672-29-6
8082A
ND
420
ug/kg
1
Aroclor 1254
11097-69-1
8082A
ND
420
ug/kg
1
Aroclor 1260
11096-82-5
8082A
ND
420
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
70 41-132
Tetrachloro-m-xylene
64 35-106
TCLP Pesticides
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Leachate Date
1 1311/3520C 8081 B 1 06/20/2023 2151 SAF 06/14/2023 1044 77626 06/12/2023 1905
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
gamma-BHC (Lindane)
58-89-9
8081 B
ND
0.00040
mg/L
1
Chlordane
57-74-9
8081 B
ND
0.0040
mg/L
1
Endrin
72-20-8
8081 B
ND
0.00040
mg/L
1
Heptachlor
76-44-8
8081 B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3
8081 B
ND
0.00040
mg/L
1
Methoxychlor
72-43-5
8081 B
ND
0.0016
mg/L
1
Toxaphene
8001-35-2
8081B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
32 20-131
Tetrachloro-m-xylene
78 26-132
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 06/29/2023 1420 KAJ 06/26/2023 1401 78264
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471 B ND 2.0
mg/kg 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 11

Client: Terra Renewal Services, Inc. Laboratory ID:YF09017-001
Description: Tyson -Danville (REP) Matrix: Solid
Date Sampled:06/08/2023 1545 % Solids: 4.01 06/20/2023 0010
Date Received:06/09/2023
TCLP Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3010A
6010D
1 06/20/2023 1404 LAB
06/19/2023 2330 78042 06/12/2023 1905
1 1311/7470A
7470A
1 06/15/2023 1154 KAJ
06/14/2023 1305 77598 06/12/2023 1905
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2 6010D
ND
0.15
mg/L
1
Barium
7440-39-3 6010D
ND
0.25
mg/L
1
Cadmium
7440-43-9 601OD
ND
0.050
mg/L
1
Chromium
7440-47-3 6010D
ND
0.10
mg/L
1
Lead
7439-92-1 6010D
ND
0.10
mg/L
1
Mercury
7439-97-6 7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2 6010D
ND
0.20
mg/L
1
Silver
7440-22-4 6010D
ND
0.10
mg/L
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D
1 06/23/2023 1200 LAB
06/22/2023 1013 78266
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aluminum
7429-90-5 6010D
ND
150
mg/kg
1
Arsenic
7440-38-2 6010D
ND
5.6
mg/kg
1
Cadmium
7440-43-9 6010D
ND
1.9
mg/kg
1
Calcium
7440-70-2 6010D
ND
1900
mg/kg
1
Copper
7440-50-8 6010D
56
3.7
mg/kg
1
Lead
7439-92-1 6010D
ND
3.7
mg/kg
1
Magnesium
7439-95-4 6010D
ND
1900
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
15
mg/kg
1
Nickel
7440-02-0 6010D
ND
15
mg/kg
1
Potassium
7440-09-7 6010D
ND
1900
mg/kg
1
Selenium
7782-49-2 6010D
ND
7.4
mg/kg
1
Sodium
7440-23-5 6010D
ND
1900
mg/kg
1
Zinc
7440-66-6 6010D
44
19
mg/kg
1
Footnote(s): 'Volume Collected = 59 mL
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 11

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 11

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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 11

PACE ANALYTICAL SERVICES, LLC
DG7-Tetle: ENIV-F.4M-WOOL-028b v0J-Sample=_ lteceipt C'lccklisti.SRCl
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 11

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: Tyson - Danville
Lot Number:YF20001
Date Completed:06/22/2023
07/05/2023 10:42 AM
Approved and released by:
Project Manager II: Lucas Odom
P RCGip0,
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TNI :
1N81 xer ava a �rcd srew Bsam
J/
ACC RE D1TED
tE nocueoArmwr
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 14

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: YF20001
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18, PFAS by Isotope Dilution SOP.
Pace is a DoD/DoE and TNI accredited laboratory; however, Pace is not accredited for PFAS Direct
Aqueous Injection or Method D8421.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
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Page 2 of 14

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: YF20001
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
TyDanv F1
Solid
06/19/2023 1430
06/20/2023
002
TyDanv F2
Solid
06/19/2023 1430
06/20/2023
003
TyDanv F3
Solid
06/19/2023 1430
06/20/2023
004
TyDanv F4
Solid
06/19/2023 1430
06/20/2023
005
TyDanv F5
Solid
06/19/2023 1430
06/20/2023
006
TyDanv F6
Solid
06/19/2023 1430
06/20/2023
007
TyDanv F7
Solid
06/19/2023 1430
06/20/2023
(7 samples)
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Page 3 of 14

PACE ANALYTICAL SERVICES,
LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: YF20001
Sample
Sample ID
Matrix Parameter Method
Result Q
Units
Page
001
TyDanv F1
Solid Fecal Coliform-MF SM 9222 D-
358778
col/g
5
002
TyDanv F2
Solid Fecal Coliform-MF SM 9222 D-
503898
col/g
6
003
TyDanv F3
Solid Fecal Coliform-MF SM 9222 D-
548499
col/g
7
004
TyDanv F4
Solid Fecal Coliform-MF SM 9222 D-
462262
col/g
8
005
TyDanv F5
Solid Fecal Coliform-MF SM 9222 D-
430807
col/g
9
006
TyDanv F6
Solid Fecal Coliform-MF SM 9222 D-
493767
col/g
10
007
TyDanv F7
Solid Fecal Coliform-MF SM 9222 D-
463653
col/g
11
(7 detections)
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Page 4 of 14

Client: Terra Renewal Services, Inc. Laboratory ID:YF20001-001
Description: TyDanv F1 Matrix: Solid
Date Sampled:06/19/2023 1430 % Solids: 13.9 06/20/2023 1520
Date Received: 06/20/2023
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 06/21/2023 1535 DAT 06/20/2023 1335
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Fecal Coliform-MF
SM 9222 D-2006 358778
20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
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Page 5 of 14

Client: Terra Renewal Services, Inc. Laboratory ID:YF20001-002
Description: TyDanv F2 Matrix: Solid
Date Sampled:06/19/2023 1430 % Solids: 13.1 06/20/2023 1520
Date Received: 06/20/2023
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 06/21/2023 1535 DAT 06/20/2023 1335
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Fecal Coliform-MF SM 9222 D-2006 503898 20 col/g 1
Footnote(s): 'Fecal Coliform (MF) results estimated
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 14

Client: Terra Renewal Services, Inc. Laboratory ID:YF20001-003
Description: TyDanv F3 Matrix: Solid
Date Sampled:06/19/2023 1430 % Solids: 12.8 06/20/2023 1520
Date Received: 06/20/2023
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 06/21/2023 1535 DAT 06/20/2023 1335
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Fecal Coliform-MF SM 9222 D-2006 548499 20 col/g 1
Footnote(s): 'Fecal Coliform (MF) results estimated
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 14

Client: Terra Renewal Services, Inc. Laboratory ID:YF20001-004
Description: TyDanv F4 Matrix: Solid
Date Sampled:06/19/2023 1430 % Solids: 13.4 06/20/2023 1520
Date Received: 06/20/2023
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 06/21/2023 1535 DAT 06/20/2023 1335
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Fecal Coliform-MF SM 9222 D-2006 462262 20 col/g 1
Footnote(s): 'Fecal Coliform (MF) results estimated
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 14

Client: Terra Renewal Services, Inc. Laboratory ID:YF20001-005
Description: TyDanv F5 Matrix: Solid
Date Sampled:06/19/2023 1430 % Solids: 13.5 06/20/2023 1520
Date Received: 06/20/2023
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 06/21/2023 1535 DAT 06/20/2023 1335
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Fecal Coliform-MF
SM 9222 D-2006 430807
20 col/g 1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 14

Client: Terra Renewal Services, Inc. Laboratory ID:YF20001-006
Description: TyDanv F6 Matrix: Solid
Date Sampled:06/19/2023 1430 % Solids: 12.4 06/20/2023 1520
Date Received: 06/20/2023
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 06/21/2023 1535 DAT 06/20/2023 1335
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Fecal Coliform-MF SM 9222 D-2006 493767 20 col/g 1
Footnote(s): 'Fecal Coliform (MF) results estimated
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 14

Client: Terra Renewal Services, Inc. Laboratory ID:YF20001-007
Description: TyDanv F7 Matrix: Solid
Date Sampled:06/19/2023 1430 % Solids: 14.0 06/20/2023 1520
Date Received: 06/20/2023
Inorganic non-metals
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Fecal Colifo) SM 9222 D-2006 1 06/21/2023 1535 DAT 06/20/2023 1335
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Fecal Coliform-MF SM 9222 D-2006 463653 20 col/g 1
Footnote(s): 'Fecal Coliform (MF) results estimated
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 14

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 12 of 14

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 13 of 14

PACE ANALYTICAL SERVICES, LLC
❑U T11a: CNV-FRS'ddCOL-0296vO2_Sarnpl43Rq4;viptChGcklisA(.SRCI
iEt`feativ$ 1? ta. S12/7.07..2
Sample-:-ceipt Cheddist (SRQ
C.�iput: Terra Renrn'a] Ccoler Iltispec[ed byldatc: KSC j OC 2(Vz93a 1_ot P: Y r ,0001
[vICMIS ofr"'c;.lpt: PiiCc ,(,ChemE L-JIVSt'edi Othcu
I'es , tln I , Were ettStoa Se3L3 pt'sc11 t all r$e ei D1c'Y?
Yes I�Tu , PTA _ Cfc�i tnd seals Were eSell1. w41•U.lt. 'iDMCt ;wed u:LLjOkery?
PH Stril, ID: Odorine Snip W: NA Tested by: PTA
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Yes FJNOJ S. Did all cojitaiL ]r_bcl illfortrtaticul W. date, rime) agree wl 1i the COC?
ZYes I lNol9. Mere rests to be pubril tid listed rnl (lie COC?
QYes E:INo IQ, Did all smnples arrive ill die pi". colziiW1% Gar each (&-M mittf(W u) to �d cou�titio�t
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❑y I D ioI 41& Was the gtk�r. bundler ]isted U11 sc c��yt�iler l�beL? If yes- Q lot,!
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 14 of 14

ADVANCE PIERRE FOODS-CLAREMONT, NC

PACE ANALYTICAL SERVICES, LLC
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: SC Samples
Lot Number:YE31030
Date Completed:0611612023
Project Manager:Lucas J. Odom
AdAB
R A C R E 6 1 T E d
00D FLAP
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: YE31030
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where sampling is conducted by the client, results
relate to the accuracy of the information provided, and as the samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved The NELAC Institute (TNI)
standards, the Pace Analytical Services, LLC ("Pace") Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any
exceptions to the TNI standards, the Laboratory Quality Manual, SOPS or policies are qualified on the results page or discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI scope of accreditation: Drinking Water: VOC
(excluding BTEX, MTBE, Naphthalene, & 1,2-dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7, Boron, Calcium, Silicon, Strontium EPA 200.8,
Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320 B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200
B-2011, Fecal Coliform Colilert-18.
Pace is a DoD/DoE and TNI accredited laboratory; however, Pace is not accredited for PFAS Direct Aqueous Injection or Method D8421
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight unless flagged with a "W" qualifier
If you have any questions regarding this report, please contact the Pace Project Manager listed on the cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method recommended 15 minute holding time.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: YE31030
Sample Number Sample ID Matrix Date Sampled Date Received
001 ADVANCED CLAREMONT Solid 05/30/2023 0900 05/31/2023
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com

PACE ANALYTICAL SERVICES,
LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: YE31030
Sample
Sample ID
Matrix Parameter Method
Result Q
Units
Page
001
ADVANCED CLAREMONT
Solid % Volatile Solids SM 2540G-
91
%
5
001
ADVANCED CLAREMONT
Solid Ammonia - N (gas 350.1
170
mg/kg
5
001
ADVANCED CLAREMONT
Solid Nitrate -Nitrite - N (soluble) 353.2
21
mg/kg
5
001
ADVANCED CLAREMONT
Solid Aluminum 6010D
750
mg/kg
6
001
ADVANCED CLAREMONT
Solid Copper 6010D
12
mg/kg
6
001
ADVANCED CLAREMONT
Solid Sodium 6010D
9200
mg/kg
6
(6 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com

Client: Terra Renewal Services, Inc. Laboratory ID:YE31030-001
Description: ADVANCED CLAREMONT Matrix: Solid
Date Sampled:05/30/2023 0900 % Solids: 6.94 05/31/2023 2154
Date Received:05/31/2023
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
06/06/2023 1645 CBP
77014
1 350.1
(Ammonia - N ) 350.1
1
06/02/2023 1116 CMM
76744
1
(Nitrate-Nitr) 353.2
1
06/07/2023 1217 CLL2
77135
1
(Phosphorus) 365.1
1
06/06/2023 1219 BMG2
06/04/2023 2017 76706
1
(Soil pH meas) 9045D
1
06/01/2023 1847 CLL
76806
1 351.4
(TKN) 351.2
1
06/05/2023 1311 BMG2
06/04/2023 1948 76705
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
91
%
1
Ammonia - N (gas diffusion)
350.1
170
140
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
21
2.9
mg/kg
1
Phosphorus
7723-14-0 365.1
ND S
72
mg/kg
1
Soil pH measured in water @ 21.3 o C
9045D
7.1
su
1
TKN
351.2
ND
720
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A 8082A
1 06/06/2023 1351 SAF
06/05/2023 1520 76903
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
240
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
240
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
240
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
240
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
240
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
240
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
240
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl
62 41-132
Tetrachloro-m-xylene
57 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 06/13/2023 1315 KAJ 06/13/2023 0305 77460
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471 B ND 1.1
mg/kg 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com

Client: Terra Renewal Services, Inc. Laboratory ID:YE31030-001
Description: ADVANCED CLAREMONT Matrix: Solid
Date Sampled:05/30/2023 0900 % Solids: 6.94 05/31/2023 2154
Date Received:05/31/2023
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 06/13/2023 1627 LAB 06/12/2023 2020 77081
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
750
250
mg/kg
1
Arsenic
7440-38-2
6010D
ND
9.4
mg/kg
1
Cadmium
7440-43-9
6010D
ND
3.1
mg/kg
1
Calcium
7440-70-2
6010D
ND
3100
mg/kg
1
Copper
7440-50-8
6010D
12
6.3
mg/kg
1
Lead
7439-92-1
6010D
ND
6.3
mg/kg
1
Magnesium
7439-95-4
6010D
ND
3100
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
25
mg/kg
1
Nickel
7440-02-0
6010D
ND
25
mg/kg
1
Potassium
7440-09-7
6010D
ND
3100
mg/kg
1
Selenium
7782-49-2
6010D
ND
13
mg/kg
1
Sodium
7440-23-5
6010D
9200
3100
mg/kg
1
Zinc
7440-66-6
6010D
ND
31
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com

PACE ANALYTICAL SERVICES. LLC
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com

PACE ANALYTICAL SERVICES, LLC
X Tilde. ENV-FRM-L'COL-02A6vOT.._SaniplesfleceiptCliecklist(SRc)
Effettive Date: AP. f 702 2
Sample Receipt Cheeldist ( Fib:)
Cliche. TERRA RENEW L cooler 1jumeeted bVfdm, CM 1 3f31123 Lot*' YE310=6
ieawofrcccipt: T'fi4t ,/ Climf Ljj 1JF5 Lj l'edEx
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Sails ID, `A _ CJL cTme Strip ID: 17A _ Trstcd G}r 2
Original tewcultlrra tlpan reccipr I De llvd (C'omt)c(rd) te114ernt11rellliOB receipt #"-244 Sao aC W"'k fNA vO ?NA Stan oO MA 1�rn Uc
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PYL w2ts N Ddl-IM hj7 pliOne ? enMil O' bCt-ro-froCe CCi,-Cle One).
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7, Wos MECC firm. date & UI= listed Ontlrc C;OC aml all sm ple COiA8izcrs7
Ycs
No
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8. Did WI rcultailmrlabel h1founaliLnl (M. date, rue) a-ee wi14 [hr.COC?
,Ir
Ye4
No
9_ Were tcsrs To be liefftr&d listed on 61C COC?
I Z!IYk,4
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14_ Did all saiInples arrive illll 6C ln-O,cr-CMtainM for csc� resf �rrd'4: ill g0��+ Cu1i[lifiun
(tlnkokclL lids on, cre.)?
V Yf-',
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dialiileter) i k Ray ur 1hu VOA vials?
15. Wut MI DkohnetaMatuficul salln}IL'S T,!czived ma pH of < 27
-NO
rl
YC?
No
; V% IN.A.1
16. Jere all CrAde samples received al aI'll 9 12 it d sulfide s9nipIcs l CCClved st 3 pH > 01
�5
�AI4
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chlorj)e.
18_ Was the gimtefrumber;ist on tlLeCOnt9lllCrlabel`? �fw3_ Quoieif
Samplr 1�re-wlwdou "Must b't ComplMd krally SU4.1 �(s) inco x.etlppl,ws avert or 1;'itll headsprtce_;
sAt�le(S) 'J4 W= 1UC0 2r1 incoi'rectlypi GkLy d and vv= ad� istcd accccdi[IFl3.
hi �Illtlplc 1rVCivfn& With 12 L of circle otlt: H25 ,1J.1 Q3, HC1. NAOH jUh4 SI,, #� KA
ILLiB �,f press rttion 14A i f taorc than aye presemative is needed please l w!l ! kk it a cmurlents below.
��rlp]e(sj vrere irmived .��irh lmi:UIcs �G unnill diSllteter.
9�nlpi*S) x war ferrivcd l�ith SRC > 0,5l g(L Mrt] Is ne?) aii: wri-e
3dj-usl, acCti dii lgl�y' 1➢ 5.amp1C Rct1%,ina with 5OKUlt 11 thjo{ 1t7fitic (V aYti2 3) A I UWTIC ID, Td
C01llnlE3IL3_
Qualtrax Ib- 56360 PiBCe*AAi1&yt-1taT Servicros, 114C Page 1 Df
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: SC Samples
Lot Number:XL29028
Date Completed:01/18/2023
01/18/2023 11:49 AM
Approved and released by:
Project Manager II: Lucas Odom
P RCGip0,
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TNI :
1N81 xer ava a �rcd srew Bsam
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ACC RE D1TED
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The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 10

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: XL29028
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 10

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: XL29028
Sample Number Sample ID Matrix Date Sampled Date Received
001 Advanced Pirre Foods Solid 12/27/2022 1300 12/29/2022
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 10

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: XL29028
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 Advanced Pirre Foods Solid Flashpoint (Pensky- 1010B >140 ° F 5
001 Advanced Pirre Foods Solid 3+4-Methylphenol 8270E 0.11 mg/L 6
(2 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 10

Client: Terra Renewal Services, Inc. Laboratory ID:XL29028-001
Description: Advanced Pirre Foods Matrix: Solid
Date Sampled:12/27/2022 1300 % Solids: 13.2 01/05/2023 0109
Date Received:12/29/2022
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst Prep Date Batch
1
(Flashpoint () 1010B
1
01/13/2023 0121 CBP 64784
1
(Reactive Cya) 7.3.3
1
01/16/2023 1613 SJL 01/13/2023 1130
1
(Reactive Sul) 7.3.4
1
01/14/2023 0931 CVR 01/13/2023 1130
1
(Soil pH meas) 9045D
1
12/30/2022 1533 BMG2 63751
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Flashpoint (Pensky-Martens Closed -Cup)
1010B
>140
140
o F
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water @ 17.1 ° C
9045D
9.3
su
1
TCLP Volatiles
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B 8260D
10 01/09/20231922 CDA
64449 12/29/20221645
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Benzene
71-43-2 8260D
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
0.10
mg/L
1
Carbon tetrachloride
56-23-5 8260D
ND
0.050
mg/L
1
Chlorobenzene
108-90-7 8260D
ND
0.050
mg/L
1
Chloroform
67-66-3 8260D
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
0.050
mg/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
0.050
mg/L
1
Tetrachloroethene
127-18-4 8260D
ND
0.050
mg/L
1
Trichloroethene
79-01-6 8260D
ND
0.050
mg/L
1
Vinyl chloride
75-01-4 8260D
ND
0.010
mg/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Bromofluorobenzene
94 70-130
1,2-Dichloroethane-d4
91 70-130
Toluene-d8
95 70-130
TCLP Semivolatiles
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8270E
1 01/05/2023 1457 CMF
01/03/2023 1355 64019 12/29/2022 1649
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units Run
1,4-Dichlorobenzene
106-46-7 8270E
ND
0.040
mg/L 1
2,4-Dinitrotoluene
121-14-2 8270E
ND
0.080
mg/L 1
Hexachlorobenzene
118-74-1 8270E
ND L
0.040
mg/L 1
Hexachlorobutadiene
87-68-3 8270E
ND
0.040
mg/L 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 10

Client: Terra Renewal Services, Inc. Laboratory ID:XL29028-001
Description: Advanced Pirre Foods Matrix: Solid
Date Sampled:12/27/2022 1300 % Solids: 13.2 01/05/2023 0109
Date Received: 12/29/2022
TCLP Semivolatiles
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8270E
1 01/05/2023 1457 CMF
01/03/2023 1355 64019 12/29/2022 1649
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1 8270E
ND
0.040
mg/L
1
2-Methylphenol
95-48-7 8270E
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5 8270E
0.11
0.040
mg/L
1
Nitrobenzene
98-95-3 8270E
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5 8270E
ND
0.20
mg/L
1
Pyridine
110-86-1 8270E
ND L
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4 8270E
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2 8270E
ND
0.040
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
91 37-129
2-Fluorophenol
36 24-127
Nitrobenzene-d5
85 38-127
Phenol-d5
63 28-128
Terphenyl-d 14
103 10-148
2,4,6-Tribromophenol
117 41-144
TCLP Herbicides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/8151A
8151A
1 01/05/2023 1559 SAF
01/03/2023 2007 64037 12/29/2022 1649
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
2,4-D
94-75-7 8151A
ND
0.020
mg/L
1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
60 50-112
TCLP Pesticides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8081B
1 01/05/20231805 DAL1
01/03/20231111 63978 12/29/2022 1649
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
gamma-BHC (Lindane)
58-89-9 8081 B
ND
0.00040
mg/L
1
Chlordane
57-74-9 8081 B
ND
0.0040
mg/L
1
Endrin
72-20-8 8081 B
ND
0.00040
mg/L
1
Heptachlor
76-44-8 8081 B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3 8081 B
ND
0.00040
mg/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 10

Client: Terra Renewal Services, Inc. Laboratory ID:XL29028-001
Description: Advanced Pirre Foods Matrix: Solid
Date Sampled:12/27/2022 1300 % Solids: 13.2 01/05/2023 0109
Date Received: 12/29/2022
TCLP Pesticides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8081B
1 01/05/20231805 DAL1
01/03/20231111 63978 12/29/2022 1649
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Methoxychlor
72-43-5 8081 B
ND
0.0016
mg/L
1
Toxaphene
8001-35-2 8081B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
40 20-131
Tetrachloro-m-xylene
86 26-132
TCLP Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3010A
6010D
1 01/05/2023 2057 JMH
01/05/2023 0910
64107 12/29/2022 1649
1 1311/7470A
7470A
1 01/05/2023 1645 MRW2
01/05/2023 1150 64188 12/29/2022 1649
3 1311/3010A
6010D
1 01/11/2023 2059 JMH
01/11/2023 1118 64604 01/10/2023 1605
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2 6010D
ND
0.15
mg/L
1
Barium
7440-39-3 6010D
ND
0.25
mg/L
3
Cadmium
7440-43-9 6010D
ND
0.050
mg/L
1
Chromium
7440-47-3 6010D
ND
0.10
mg/L
1
Lead
7439-92-1 6010D
ND
0.10
mg/L
1
Mercury
7439-97-6 7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2 6010D
ND
0.20
mg/L
1
Silver
7440-22-4 6010D
ND
0.10
mg/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 10

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 10

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
[phone]
Fax [phone] www.pacelabs.com
Page 9 of 10

PACE ANALYTICAL SERVICES, LLC
Lit# Title; ENV-FRKI-V'lCOL-028gv02-.°,ampltin ecaiptCherklistySl Cj
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Sopuple I eMpt Checklist (SRC)
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 10

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 02/28/2023
Reported: 03/02/2023
For: Advance Claremont
Comments: GEOMETRIC MEAN: 223,673 MPN/g
4 STATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
230228-24-01
Fecal Coliforms
AC1
231481
MPN/g
SM92210E-2006
02/28/2023
MD
230228-24-01
Percent Solids
AC1
2.16
%
SM2540B-2011
02/28/2023
MD
230228-24-02
Fecal Coliforms
AC2
393939
MPN/g
SM92210E-2006
02/28/2023
MD
230228-24-02
Percent Solids
AC2
3.3
%
SM2540B-2011
02/28/2023
MD
230228-24-03
Fecal Coliforms
AC3
601504
MPN/g
SM92210E-2006
02/28/2023
MD
230228-24-03
Percent Solids
AC3
1.33
%
SM2540B-2011
02/28/2023
MD
230228-24-04
Fecal Coliforms
AC4
105505
MPN/g
SM92210E-2006
02/28/2023
MD
230228-24-04
Percent Solids
AC4
2.18
%
SM2540B-2011
02/28/2023
MD
230228-24-05
Fecal Coliforms
AC5
669291
MPN/g
SM92210E-2006
02/28/2023
MD
230228-24-05
Percent Solids
AC5
2.54
%
SM2540B-2011
02/28/2023
MD
230228-24-06
Fecal Coliforms
AC6
77320
MPN/g
SM92210E-2006
02/28/2023
MD
230228-24-06
Percent Solids
AC6
3.88
%
SM2540B-2011
02/28/2023
MD
230228-24-07
Fecal Coliforms
AC7
93525
MPN/g
SM92210E-2006
02/28/2023
MD
230228-24-07
Percent Solids
AC7
1.39
%
SM2540B-2011
02/28/2023
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 230228-24-01 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 230228-24-02 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 230228-24-03 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 230228-24-04 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 230228-24-05 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 230228-24-06 Temp on Arrival: 2.5
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Sample Number 230228-24-07 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4 of 4

MATHIS-1 (STORAGE)

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: SC Samples
Lot Number:YE22017
Date Completed:06/07/2023
06/07/2023 2:28 PM
Approved and released by:
Project Manager II: Lucas Odom
P RCGip0,
\%
A4W
TNI :
1N81 xer ava a �rcd srew Bsam
J/
ACC RE D1TED
tE nocueoArmwr
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 9

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: YE22017
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
Due to low percent solids, sample -001 has been analyzed using three times the method defined amount.
The LOQs have been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 9

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: YE22017
Sample Number Sample ID Matrix Date Sampled Date Received
001 MATHIS-1 Solid 05/18/20231100 05/22/2023
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 9

PACE ANALYTICAL SERVICES, LLC
Sample
Sample ID
001
MATHIS-1
001
MATHIS-1
001
MATHIS-1
001
MATHIS-1
001
MATHIS-1
001
MATHIS-1
001
MATHIS-1
001
MATHIS-1
(8 detections)
Detection Summary
Terra Renewal Services, Inc.
Lot Number: YE22017
Matrix Parameter Method Result Q Units Page
Solid
% Volatile Solids
SM 2540G-
98
% 5
Solid
Ammonia - N (gas
350.1
2400
mg/kg 5
Solid
Nitrate -Nitrite - N (soluble)
353.2
40
mg/kg 5
Solid
Phosphorus
365.1
850
mg/kg 5
Solid
TKN
351.2
20000
mg/kg 5
Solid
Aluminum
601OD
300
mg/kg 6
Solid
Copper
601OD
27
mg/kg 6
Solid
Zinc
601OD
36
mg/kg 6
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 9

Client: Terra Renewal Services, Inc. Laboratory ID:YE22017-001
Description: MATHIS-1 Matrix: Solid
Date Sampled:05/18/2023 1100 % Solids: 3.64 05/23/2023 2035
Date Received:05/22/2023
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
05/23/2023 2218 CBP
76021
1 350.1
(Ammonia - N ) 350.1
5
06/02/2023 1046 CMM
76744
1
(Nitrate-Nitr) 353.2
1
05/26/2023 1545 CLL2
76561
1
(Phosphorus) 365.1
1
05/30/2023 1729 DMA
05/24/2023 2155 76153
1
(Soil pH meas) 9045D
1
05/24/2023 2110 CLL
76327
1 351.4
(TKN) 351.2
1
05/26/2023 1520 DMA
05/25/2023 1536 76152
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
98
%
1
Ammonia - N (gas diffusion)
350.1
2400
1400
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
40
5.5
mg/kg
1
Phosphorus
7723-14-0 365.1
850
140
mg/kg
1
Soil pH measured in water @ 19.4 ° C
9045D
3.6
su
1
TKN
351.2
20000
1400
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A 8082A
1 05/31/20231630 SAF
05/23/20231741 75998
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
470
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
470
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
470
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
470
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
470
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
470
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
470
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl
69 41-132
Tetrachloro-m-xylene
64 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471B
7471B
1 06/01/20230932 KAJ 05/31/20231550 76364
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471 B ND 2.0
mg/kg 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 9

Client: Terra Renewal Services, Inc. Laboratory ID:YE22017-001
Description: MATHIS-1 Matrix: Solid
Date Sampled:05/18/2023 1100 % Solids: 3.64 05/23/2023 2035
Date Received:05/22/2023
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 06/05/2023 1550 LAB 05/31/2023 1925 76607
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
300
160
mg/kg
1
Arsenic
7440-38-2
6010D
ND
6.1
mg/kg
1
Cadmium
7440-43-9
6010D
ND
2.0
mg/kg
1
Calcium
7440-70-2
6010D
ND
2000
mg/kg
1
Copper
7440-50-8
6010D
27
4.1
mg/kg
1
Lead
7439-92-1
6010D
ND
4.1
mg/kg
1
Magnesium
7439-95-4
6010D
ND
2000
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
16
mg/kg
1
Nickel
7440-02-0
6010D
ND
16
mg/kg
1
Potassium
7440-09-7
6010D
ND
2000
mg/kg
1
Selenium
7782-49-2
6010D
ND
8.1
mg/kg
1
Sodium
7440-23-5
6010D
ND
2000
mg/kg
1
Zinc
7440-66-6
6010D
36
20
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 9
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 9

PACE ANALYTICAL SERVICES, LLC
r 1
L
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4,1 1
71
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 9

PACE ANALYTICAL SERVICES, LLC
DCV Ti tl+r_ ENS+ FRI 1 '. + C]_ 0 8G vQ „ ampler Rec�i pt Checicl ist ] RC)
prectiue Data: Z/2{2022
Sample Receipt Cheek1ist (SRC)
Clicor: TERPA RENEWAL Caokr Inspected wdaiv; c1OR 1 = 'i2, 23 Lot #: 3i E22,517
14ieans Ofr,rccipr:
Pace ¢; C; lertt UPS i Fct Ex
IL : Clain::
CS
Y {
I]. Well utstody Seals EirmiL UIl the cualce!
17C,911
INC
NA
�. 1fC113t�� 5es`sls Vwere ��11t, wele t1i IlltklCL iLLd L01lllt7lL�Jj'
):I Sl- ip ID: rLA _ Chloride Snip ID; NA Tested IVY.LrIFa
OLi@LiUd 1UR1peldLLUX LLjJD11 rt�eipr I Thrived (l :rnrcrlerl) fewrelatuir- 1j)011 vueipl 'VeSolui Sriatlr-cup 1D:-3-2,vi
1.9 fd, oC NFL /14A oC NA +rNFA uC N.1 ILIA oC
feLkd: ❑Te11rperatl>re F3laulb[, 0. ssi 13uttJc K Ghlu ID; $ _ IR Gtui Colracaan Factor; ° "C
fctaad of ct1ola8t; ❑ Wo It=. Ite FaekS '• 1) U Ice loltie
I/ es
❑Nu
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3. Were all cooler,, rccciwi nr .^.c a � { , '{ "� :t ilo- was P ee[ Kin g-t no rfkd?
FMIvas Noufwd by. plane ) chit i Lic-e-t-�-€ace (circle one),
Yes
Na
I v" NA
4, h the ccmulercial coiLnk`Spacldnr slip atrached to dns fame
y!s
f
-No
5. WeLv propel cmlydy -p?LCCIIIrn {1'cluw]llis[Le�'recervezij fl)1Lowed'
Yc5
No
6, Wele 30113ple Ms lis-cd f 1 rk , nd al i samipk connhiffr
17. Was collection drA-. & titue lEstec 011 ilw CUB' and all wuplc colltpi[Im''
IS. Did all C011(ai cr label ;11Conrlatioll pD, [late_ fime) apt=wi lLdlc C.00?
I
INO
Yes
r7Nu
rYes
Yes
Nu
9, WeTt InSfS to be pctforu1ed listed oil the COC?
oYes
❑t ;�
10_ Did ail s�mipks arrive in the pwpe^ contail>_els cacl) list aud'oa- ill repel -"I ;'.ir.::1r.
(imbrokea lidtw etc_)?
1i.1MRsskquatcsmijiir-G�I NunaaivaiisI)k?
Yc;
No
/
]'es
No
12_ Wcrc all sa[L>l;les wc6ved'Aft-All 'A fhe 11ti-ldi11 time n! 4$ Jhll}r2�_ wIhifillit-,v i :OilirS 1isrsl?
[ JI Ter
❑No
D. Werc all s�Iiuplm coutavlcrs aceaiulted for? (No rnistir.�,`r�ccc. s)
�Ye
'e
[�1ro
p
D r
14. Wise VOA. 80 l 5C arift RS - l -15 �[slglu free of l Ubbles >" pea -size , (,I. -Or 611'al) in
diaWer) hi any of B.c VOA Yinn1-0
, ".:NA
15.Werc,311DRt ImeL'�'IWunrrici2ss_rl I�l-cocivedara i1of <77
Yrs
N-4N' u
NA
16. cr{: a]I cvarudc "113 les tece led at a > 12 and sulfide saxples 1ecpiwa ar a H > 4?
❑'cs
❑No
NA
17 . IV= all n1,4Aicable �l.H�r,lYlry2uvdeF�l eat _. , (� ,53u1pof
resiLi�sal cltlariue"'
❑Yes
W]No
❑N
18_ WEE list quote lu2mher 1 i Bred ciu tLr, tcnlla to hW" if ems. [ uw—, ri
Sample
PlIeRF7'S'Aii0o CdusJ be wainplcrocd k1r ROY SAMPIC(9) iHCULWULIy IffzscIved or Mtil ke3dSi18 C.)
ample;s) ILIA were feceived incoirecflyy 11IL CI 'eel a»tl;acre adjusficd accordingly
in sample recehAng with NA utuutOrck [isle: H2504,UN03, HCl, KuOH mii.lr SR W NA
Ime of P1aqcR-atim1A If more Lira alre fluy�rc is �brricLit �Ilc�sL; uolc:rl the trtuure7l[s below_
53111]lli(S� Weiv itceivad %%ill hiibblcs J6 nim in dinfm-w(,
SJIILP�vi(s) "IA - wit mccivC7dwidi IRC } 0.5 ruq, L -t D is xru) Bi d -oxn;
adjusbA accarfUgiyia sanIPle receiving. -Ii rA sodilul ddosulfatc CN;Ia .S203)'Lvidz Uir (Lie JD- NA
coamueuts:
Qualtrex D; 563W Rau!0 Anal oirmI Services, LLC Rag-- 1 of i
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 9

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: SC Samples
Lot Number:XL29023
Date Completed:01/13/2023
01/17/2023 4:10 PM
Approved and released by:
Project Manager II: Lucas Odom
P RCGip0,
\%
A16
TNI :
1N81 xer ava a �rcd srew Bsam
J/
ACC RE D1TED
tE nocueoArmwr
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 10

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: XL29023
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 10

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: XL29023
Sample Number Sample ID Matrix Date Sampled Date Received
001 MATHIS-1 Solid 12/27/2022 0900 12/29/2022
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 10

PACE ANALYTICAL SERVICES, LLC
Sample Sample ID
001 MATHIS-1
(1 detection)
Detection Summary
Terra Renewal Services, Inc.
Lot Number: XL29023
Matrix Parameter Method Result Q Units Page
Solid Flashpoint (Pensky- 1010B >140 ° F 5
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 10

Client: Terra Renewal Services, Inc. Laboratory ID:XL29023-001
Description: MATHIS-1 Matrix: Solid
Date Sampled:12/27/2022 0900
Date Received:12/29/2022
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst Prep Date Batch
1
(Flashpoint () 1010B
1
01/12/2023 2138 CBP 64784
1
(Reactive Cya) 7.3.3
1
01/10/2023 1555 SJL 01/09/2023 1221
1
(Reactive Sul) 7.3.4
1
01/10/2023 1735 CVR 01/09/2023 1221
1
(Soil pH meas) 9045D
1
12/30/2022 1527 BMG2 63751
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Flashpoint (Pensky-Martens Closed -Cup)
1010B
>140
140
o F
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water @ 16.3 o C
9045D
4.8
su
1
TCLP Volatiles
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B 8260D
10 01/09/20231806 CDA
64449 12/29/20221645
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Benzene
71-43-2 8260D
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3 8260D
ND S
0.10
mg/L
1
Carbon tetrachloride
56-23-5 8260D
ND
0.050
mg/L
1
Chlorobenzene
108-90-7 8260D
ND
0.050
mg/L
1
Chloroform
67-66-3 8260D
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
0.050
mg/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
0.050
mg/L
1
Tetrachloroethene
127-18-4 8260D
ND
0.050
mg/L
1
Trichloroethene
79-01-6 8260D
ND
0.050
mg/L
1
Vinyl chloride
75-01-4 8260D
ND
0.010
mg/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Bromofluorobenzene
91 70-130
1,2-Dichloroethane-d4
92 70-130
Toluene-d8
96 70-130
TCLP Semivolatiles
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8270E
1 01/05/2023 1317 CMF
01/03/2023 1355 64019 12/29/2022 1649
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units Run
1,4-Dichlorobenzene
106-46-7 8270E
ND
0.040
mg/L 1
2,4-Dinitrotoluene
121-14-2 8270E
ND
0.080
mg/L 1
Hexachlorobenzene
118-74-1 8270E
ND L
0.040
mg/L 1
Hexachlorobutadiene
87-68-3 8270E
ND
0.040
mg/L 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 10

Client: Terra Renewal Services, Inc. Laboratory ID:XL29023-001
Description: MATHIS-1 Matrix: Solid
Date Sampled:12/27/2022 0900
Date Received: 12/29/2022
TCLP Semivolatiles
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8270E
1 01/05/2023 1317 CMF
01/03/2023 1355 64019 12/29/2022 1649
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1 8270E
ND
0.040
mg/L
1
2-Methylphenol
95-48-7 8270E
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5 8270E
ND
0.040
mg/L
1
Nitrobenzene
98-95-3 8270E
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5 8270E
ND
0.20
mg/L
1
Pyridine
110-86-1 8270E
ND L
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4 8270E
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2 8270E
ND
0.040
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
91 37-129
2-Fluorophenol
72 24-127
Nitrobenzene-d5
87 38-127
Phenol-d5
74 28-128
Terphenyl-d 14
96 10-148
2,4,6-Tribromophenol
ill 41-144
TCLP Herbicides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/8151A
8151A
1 01/05/2023 1427 SAF
01/03/2023 2007 64037 12/29/2022 1649
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
2,4-D
94-75-7 8151A
ND
0.020
mg/L
1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
59 50-112
TCLP Pesticides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8081B
1 01/05/20231702 DAL1
01/03/20231111 63978 12/29/2022 1649
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
gamma-BHC (Lindane)
58-89-9 8081 B
ND
0.00040
mg/L
1
Chlordane
57-74-9 8081 B
ND
0.0040
mg/L
1
Endrin
72-20-8 8081 B
ND
0.00040
mg/L
1
Heptachlor
76-44-8 8081 B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3 8081 B
ND
0.00040
mg/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 10

Client: Terra Renewal Services, Inc. Laboratory ID:XL29023-001
Description: MATHIS-1 Matrix: Solid
Date Sampled:12/27/2022 0900
Date Received: 12/29/2022
TCLP Pesticides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8081B
1 01/05/20231702 DAL1
01/03/20231111 63978 12/29/2022 1649
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Methoxychlor
72-43-5 8081 B
ND
0.0016
mg/L
1
Toxaphene
8001-35-2 8081B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
63 20-131
Tetrachloro-m-xylene
93 26-132
TCLP Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3010A
6010D
1 01/05/2023 2034 JMH
01/05/2023 0910
64107 12/29/2022 1649
1 1311/7470A
7470A
1 01/05/2023 1631 MRW2
01/05/2023 1150 64188 12/29/2022 1649
3 1311/3010A
6010D
1 01/11/2023 2047 JMH
01/11/2023 1118 64604 01/10/2023 1605
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2 6010D
ND
0.15
mg/L
1
Barium
7440-39-3 6010D
ND
0.25
mg/L
3
Cadmium
7440-43-9 6010D
ND
0.050
mg/L
1
Chromium
7440-47-3 6010D
ND
0.10
mg/L
1
Lead
7439-92-1 6010D
ND
0.10
mg/L
1
Mercury
7439-97-6 7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2 6010D
ND
0.20
mg/L
1
Silver
7440-22-4 6010D
ND
0.10
mg/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 10

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 10

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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 10

PACE ANALYTICAL SERVICES, LLC
IQC#_! itle= E14V-FFlM-WC4:l11-028G vU2-. Ssrnplas i ceipt CftieckGsr (SRC1
E#fecti,fn Date; 8J2/2022
Sample receipt Checklist (SRC)
Clien-t: � RENTEWAL Coolu hiss etrd b� ldare; K=, + : L'3P1�2 1 c►r #: XL19 1i
1"Icarls Of rloomeceipt: ?are ,e Client UPS LedEx I JlDflier
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7. Was coilectiou dmr4k time wined an the cc)c , ud all san1ple � uutriz€tcrs?
8, Did all coritiiiiwu label ii)::lfbr31l1_ipi) 0, duro, untie) agr(m with the COC-�
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 10

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 04/20/2023
Reported: 04/21 /2023
For: Mathis
Comments: GEOMETRIC MEAN: 37867 MPN/g
STATESVILLE
4 ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
230420-12-01
Fecal Coliforms
M1
46154
MPN/g
SM92210E-2006
04/20/2023
WC
230420-12-01
Percent Solids
M1
0.65
%
SM2540B-2011
04/20/2023
WC
230420-12-02
Fecal Coliforms
M2
44776
MPN/g
SM92210E-2006
04/20/2023
WC
230420-12-02
Percent Solids
M2
0.67
%
SM2540B-2011
04/20/2023
WC
230420-12-03
Fecal Coliforms
M3
16418
MPN/g
SM92210E-2006
04/20/2023
WC
230420-12-03
Percent Solids
M3
0.67
%
SM2540B-2011
04/20/2023
WC
230420-12-04
Fecal Coliforms
M4
18841
MPN/g
SM92210E-2006
04/20/2023
WC
230420-12-04
Percent Solids
M4
0.69
%
SM2540B-2011
04/20/2023
WC
230420-12-05
Fecal Coliforms
M5
33824
MPN/g
SM92210E-2006
04/20/2023
WC
230420-12-05
Percent Solids
M5
0.68
%
SM2540B-2011
04/20/2023
WC
230420-12-06
Fecal Coliforms
M6
36145
MPN/g
SM92210E-2006
04/20/2023
WC
230420-12-06
Percent Solids
M6
0.83
%
SM2540B-2011
04/20/2023
WC
230420-12-07
Fecal Coliforms
M7
142857
MPN/g
SM92210E-2006
04/20/2023
WC
230420-12-07
Percent Solids
M7
0.77
%
SM2540B-2011
04/20/2023
WC
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 230420-12-01 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 230420-12-02 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 230420-12-03 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 230420-12-04 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 230420-12-05 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 230420-12-06 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 230420-12-07 Temp on Arrival: 2.5
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4 of 4

RVI-HARMONY, NC

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: SC Samples
Lot Number:YE22018
Date Completed:06/22/2023
Revision Date: 06/16/2023
06/28/2023 2:28 PM
Approved and released by:
Project Manager II: Lucas Odom
P RCGip0,
\%
A4W
TNI :
1N81 xer ava a �rcd srew Bsam
J/
ACC RE D1TED
tE nocueoArmwr
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 9

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: YE22018
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
This report supersedes all other versions of the same lot number
Inorganic Metals
Due to low percent solids, sample -001 has been analyzed using three times the method defined amount.
The LOQs have been adjusted accordingly.
Report Revision
Per client request, the analysis of TKN and Ammonia were re -performed. The Ammonia run yielded a
similar result. The TKN value nearly doubled. Both values have been reported.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 9

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: YE22018
Sample Number Sample ID Matrix Date Sampled Date Received
001 TYHARMO Solid 05/18/20231300 05/22/2023
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 9

PACE ANALYTICAL SERVICES,
LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: YE22018
Sample
Sample ID
Matrix Parameter Method
Result Q
Units
Page
001
TYHARMO
Solid % Volatile Solids SM 2540G-
85
%
5
001
TYHARMO
Solid Nitrate -Nitrite - N (soluble) 353.2
59
mg/kg
5
001
TYHARMO
Solid Phosphorus 365.1
7700
mg/kg
5
001
TYHARMO
Solid Ammonia - N (gas 350.1
19000 H
mg/kg
5
001
TYHARMO
Solid TKN 351.2
31000 H
mg/kg
6
001
TYHARMO
Solid Aluminum 6010D
4800
mg/kg
7
001
TYHARMO
Solid Calcium 6010D
23000
mg/kg
7
001
TYHARMO
Solid Copper 6010D
6.6
mg/kg
7
001
TYHARMO
Solid Potassium 6010D
2300
mg/kg
7
001
TYHARMO
Solid Sodium 6010D
3300
mg/kg
7
001
TYHARMO
Solid Zinc 6010D
32
mg/kg
7
(11 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 9

Client: Terra Renewal Services, Inc. Laboratory ID:YE22018-001
Description: TYHARMO Matrix: Solid
Date Sampled:05/18/2023 1300 % Solids: 4.26 05/23/2023 2035
Date Received:05/22/2023
Inorganic
non-metals
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
05/23/2023 2218 CBP
76021
1
350.1
(Ammonia - N ) 350.1
25
06/02/2023 1048 CMM
76744
2
350.1
(Ammonia - N ) 350.1
25
06/19/2023 1243 CMM
77927
1
(Nitrate-Nitr) 353.2
1
05/26/2023 1547 C1_1_2
76561
1
(Phosphorus) 365.1
10
05/30/2023 1720 DMA
05/24/2023 2155 76153
1
(Soil pH meas) 9045D
1
05/24/2023 2111 CLL
76327
1
351.4
(TKN) 351.2
1
05/26/2023 1520 DMA
05/25/2023 1536 76152
2
351.4
(TKN) 351.2
2
06/20/2023 1312 BMG2
06/19/2023 2106 78040
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
85
%
1
Nitrate -Nitrite - N (soluble)
353.2
59
4.7
mg/kg
1
Ammonia - N (gas diffusion)
350.1
18000
5900
mg/kg
1
Phosphorus
7723-14-0 365.1
7700
1200
mg/kg
1
Ammonia - N (gas diffusion)
350.1
19000 H
5900
mg/kg
2
Soil pH measured in water @ 19.3 ° C
9045D
6.4
su
1
TKN
351.2
17000
1200
mg/kg
1
TKN
351.2
31000 H
2300
mg/kg
2
PCBs by GC
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 8082A
1 05/30/2023 1734 MEZ
05/26/2023 2100 76345
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
400
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
400
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
400
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
400
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
400
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
400
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
400
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl
65 41-132
Tetrachloro-m-xylene
63 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471 B
7471 B
1 06/01/2023 0935 KAJ 05/31/2023 1550 76364
Parameter
CAS Analytical
Number Method Result Q LOQ
Units Run
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 9

Client: Terra Renewal Services, Inc. Laboratory ID:YE22018-001
Description: TYHARMO Matrix: Solid
Date Sampled:05/18/2023 1300 % Solids: 4.26 05/23/2023 2035
Date Received:05/22/2023
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471B
7471B
1 06/01/20230935 KAJ
05/31/20231550 76364
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Mercury
7439-97-6 7471 B
ND
1.9
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D
1 06/05/2023 1553 LAB
05/31/2023 1925 76607
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aluminum
7429-90-5 6010D
4800
140
mg/kg
1
Arsenic
7440-38-2 6010D
ND
5.2
mg/kg
1
Cadmium
7440-43-9 6010D
ND
1.7
mg/kg
1
Calcium
7440-70-2 6010D
23000
1700
mg/kg
1
Copper
7440-50-8 6010D
6.6
3.5
mg/kg
1
Lead
7439-92-1 6010D
ND
3.5
mg/kg
1
Magnesium
7439-95-4 6010D
ND
1700
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
14
mg/kg
1
Nickel
7440-02-0 6010D
ND
14
mg/kg
1
Potassium
7440-09-7 6010D
2300
1700
mg/kg
1
Selenium
7782-49-2 6010D
ND
6.9
mg/kg
1
Sodium
7440-23-5 6010D
3300
1700
mg/kg
1
Zinc
7440-66-6 6010D
32
17
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 9
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 9

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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 9

PACE ANALYTICAL SERVICES, LLC
DC4_T'Ae: EN'J-FRrO- CGL-02&6u02_ umpl-sReceipt Che2klist(SEQ
Effective Data: 8}20+2022
Sample receipt Checklist (SRC
uner1C 1 LL464Z L4S L.L TI ally C oolu llis ectcd ?date LzA ii: I Su la
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lwictkcd: ❑Te1l�perarivc i3] u�kQ slirw; L,rllrs IR GLU ID: $ IR Gm- Coryactiou Factor: ° "C
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Yes NQ d ETA 4. I5111a c,-,annci;d ct;Luicf s ]iucking gli p atrsched to this f�to
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yes NO 7. WAS �1)11 eriffa dal: . Iilme listed Di ;ht CC ancL all soulple ca111aiuei�7
Yet Nu S. Did all c-OMAiner label Ulfbmtien CID, dam (ime) agee m1kthe CDC?
Yes I�iO 5. Were CRsls t-D be perfcnnlcd listed on the COC'�
© Yes ❑ 1:0 10. Did all saa Miles amve u1 the proper eo intrs for tacli pest amVor ila good ecitxcli[ion
(Mlbro m lids on. etc.)?
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F'.a No NA 15. Wem all DRWLnctalshmtrim sam- les received at a pH of <
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Quailrax 1D: 56360 Pa;,e11 Analytical 5ervicaa, LLC Page I of 1
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 9

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: SC Samples
Lot Number:XL29026
Date Completed:01/18/2023
01/18/2023 11:46 AM
Approved and released by:
Project Manager II: Lucas Odom
P RCGip0,
\%
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TNI :
1N81 xer ava a �rcd srew Bsam
J/
ACC RE D1TED
tE nocueoArmwr
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 10

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: XL29026
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 10

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: XL29026
Sample Number Sample ID Matrix Date Sampled Date Received
001 TYSON HARMONY Solid 12/27/2022 1130 12/29/2022
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 10

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: XL29026
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 TYSON HARMONY Solid Flashpoint (Pensky- 1010B >140 ° F 5
001 TYSON HARMONY Solid 3+4-Methylphenol 8270E 0.10 mg/L 6
(2 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 10

Client: Terra Renewal Services, Inc. Laboratory ID:XL29026-001
Description: TYSON HARMONY Matrix: Solid
Date Sampled:12/27/2022 1130 % Solids: 5.36 01/03/2023 1657
Date Received:12/29/2022
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst Prep Date Batch
1
(Flashpoint () 1010B
1
01/13/2023 0033 CBP 64784
1
(Reactive Cya) 7.3.3
1
01/16/2023 1611 SJL 01/13/2023 1130
1
(Reactive Sul) 7.3.4
1
01/14/2023 0931 CVR 01/13/2023 1130
1
(Soil pH meas) 9045D
1
12/30/2022 1530 BMG2 63751
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Flashpoint (Pensky-Martens Closed -Cup)
1010B
>140
140
o F
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water @ 16.8 o C
9045D
5.2
su
1
TCLP Volatiles
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B 8260D
10 01/09/20231857 CDA
64449 12/29/20221645
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Benzene
71-43-2 8260D
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
0.10
mg/L
1
Carbon tetrachloride
56-23-5 8260D
ND
0.050
mg/L
1
Chlorobenzene
108-90-7 8260D
ND
0.050
mg/L
1
Chloroform
67-66-3 8260D
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
0.050
mg/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
0.050
mg/L
1
Tetrachloroethene
127-18-4 8260D
ND
0.050
mg/L
1
Trichloroethene
79-01-6 8260D
ND
0.050
mg/L
1
Vinyl chloride
75-01-4 8260D
ND
0.010
mg/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Bromofluorobenzene
91 70-130
1,2-Dichloroethane-d4
90 70-130
Toluene-d8
94 70-130
TCLP Semivolatiles
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8270E
1 01/05/2023 1432 CMF
01/03/2023 1355 64019 12/29/2022 1649
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units Run
1,4-Dichlorobenzene
106-46-7 8270E
ND
0.040
mg/L 1
2,4-Dinitrotoluene
121-14-2 8270E
ND
0.080
mg/L 1
Hexachlorobenzene
118-74-1 8270E
ND L
0.040
mg/L 1
Hexachlorobutadiene
87-68-3 8270E
ND
0.040
mg/L 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 10

Client: Terra Renewal Services, Inc. Laboratory ID:XL29026-001
Description: TYSON HARMONY Matrix: Solid
Date Sampled:12/27/2022 1130 % Solids: 5.36 01/03/2023 1657
Date Received: 12/29/2022
TCLP Semivolatiles
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8270E
1 01/05/2023 1432 CMF
01/03/2023 1355 64019 12/29/2022 1649
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1 8270E
ND
0.040
mg/L
1
2-Methylphenol
95-48-7 8270E
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5 8270E
0.10
0.040
mg/L
1
Nitrobenzene
98-95-3 8270E
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5 8270E
ND
0.20
mg/L
1
Pyridine
110-86-1 8270E
ND L
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4 8270E
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2 8270E
ND
0.040
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
91 37-129
2-Fluorophenol
39 24-127
Nitrobenzene-d5
82 38-127
Phenol-d5
64 28-128
Terphenyl-d 14
102 10-148
2,4,6-Tribromophenol
118 41-144
TCLP Herbicides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/8151A
8151A
1 01/05/2023 1536 SAF
01/03/2023 2007 64037 12/29/2022 1649
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
2,4-D
94-75-7 8151A
ND
0.020
mg/L
1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
57 50-112
TCLP Pesticides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8081B
1 01/05/20231749 DAL1
01/03/20231111 63978 12/29/2022 1649
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
gamma-BHC (Lindane)
58-89-9 8081 B
ND
0.00040
mg/L
1
Chlordane
57-74-9 8081 B
ND
0.0040
mg/L
1
Endrin
72-20-8 8081 B
ND
0.00040
mg/L
1
Heptachlor
76-44-8 8081 B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3 8081 B
ND
0.00040
mg/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 10

Client: Terra Renewal Services, Inc. Laboratory ID:XL29026-001
Description: TYSON HARMONY Matrix: Solid
Date Sampled:12/27/2022 1130 % Solids: 5.36 01/03/2023 1657
Date Received: 12/29/2022
TCLP Pesticides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8081B
1 01/05/20231749 DAL1
01/03/20231111 63978 12/29/2022 1649
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Methoxychlor
72-43-5 8081 B
ND
0.0016
mg/L
1
Toxaphene
8001-35-2 8081B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
33 20-131
Tetrachloro-m-xylene
85 26-132
TCLP Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3010A
6010D
1 01/05/2023 2053 JMH
01/05/2023 0910
64107 12/29/2022 1649
1 1311/7470A
7470A
1 01/05/2023 1642 MRW2
01/05/2023 1150 64188 12/29/2022 1649
3 1311/3010A
6010D
1 01/11/2023 2055 JMH
01/11/2023 1118 64604 01/10/2023 1605
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2 6010D
ND
0.15
mg/L
1
Barium
7440-39-3 6010D
ND
0.25
mg/L
3
Cadmium
7440-43-9 6010D
ND
0.050
mg/L
1
Chromium
7440-47-3 6010D
ND
0.10
mg/L
1
Lead
7439-92-1 6010D
ND
0.10
mg/L
1
Mercury
7439-97-6 7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2 6010D
ND
0.20
mg/L
1
Silver
7440-22-4 6010D
ND
0.10
mg/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 10

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 10

PACE ANALYTICAL SERVICES, LLC
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 10

PACE ANALYTICAL SERVICES, LLC
0OL Tide: FNV-FRrv1-LW_0L-0286 vG2 5arnp1rj- Rw.;eipt is# (SRC)
ELFactive Date- M12022
Sample Receipt Cheddist (SRC)
Chem. T3-R[k,k PIE, E'cVAi Cui:lC'r T119-t.ai!d ?dale- xISKR r I'.12' 22 _906 XL
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,I Yrs 6. W samplt ws Lisred M1 rlati COC' aild all sar ple caotaiurrsl
kes N 7- 7. Was ralkdon dale & dRIP- listed fill die 00'C:md all sample cmriahwIV
Yes Na & Ll d Lill coutlliw label l nfilrrinb)ul (ID, da..e, dii=) t%! Aith the CC)C?
V Yrs Na 9. Welr [esm to be Wfclluwd listed on the CQC?
MYes ONO 10. Did all sa lcs arrive in t& proinr corltaiaers Ru cacti test S11d1oria'aod c(tlditioal
(tinbr-Ami, I S on. ere_)? _
Yes ❑ 111. W' q aL%juale sarrll)lc Volta= availalile7
Yes Na 12, -We4C all 1Aulplcs recrived wlthi3l !4 the holdhig tilllc of 48 holes, 1143iche ev curers fiSSF'?
lay ❑No 15, Wete 911 smilple_s contafWas accomltni ko Dro 3�lissib lexcess
[]Yes ❑No 01 4 14_ Wele. VOA- 8015C sal RSK-i75 &11 l rs flee oftubblrs >-pea-size" '/"ol 6ir1 i_i
ffi1R4lej1 is My of 11w VOA ViAs?
15. Wirt
16. w,�r
)leg receivcd ai a
at n PH > 12 amd
QYdS L2N0 ZNA I 1 +, 'vat. ail apprlcaair lve11 kkUNYCyajudrqahMD
1�csidual chloriaeF
LJYcs Z NolC_ I$ W-1a the gtio(c rnunber listed on the �on[ajmx
of < 2?
W s8A
,.I (4 A
If ya, Q1101-0 V.
at a 11H > 9?
Impre 1'1�s[���rtion (1w�lat tiecnmPtetad far;.uy Stu:rplP�(s} InCC1T�C.tI}' �I>'SL1V9[� �r LY3.1LL 11CAC15�8C2.�
'Nu r�ceivcd iucofrecEIyprr�;MT4and we eadjslsted
sari k rcuiving with >uI ofcirclr. obe' H S #, t 03, H�.1, NRC)H u%im� SIZ 0 K
lue ofPoservatiou ' AL . lfIMM' 117Liat one press-va0w is need, pleasC nnte in 111e 00Yo11 Mrs kJ01 v.
alllplc�,s'� NA
kvcrc received uith bubbics >61n:u ha diwue;er.
. } r��ere rec ilvrd uidl TRC > 0.5 a -a-at (Ifi#19 is np) :aud were
3ccordh181 in Salllpie r ckyiayg -Witl I S06Utl1 1111Mhte {NaISZ05} With Unique W. NA
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 10

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 04/18/2023
Reported: 04/21 /2023
For: TYHARMO
Comments: GEOMETRIC MEAN: 2499 MPN/g
STATESVILLE
4 ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
230418-37-01
Fecal Coliforms
TH1
1389
MPN/g
SM92210E-2006
04/18/2023
MD
230418-37-01
Percent Solids
TH1
1.44
%
SM2540B-2011
04/18/2023
MD
230418-37-02
Fecal Coliforms
TH2
2740
MPN/g
SM92210E-2006
04/18/2023
MD
230418-37-02
Percent Solids
TH2
1.46
%
SM2540B-2011
04/18/2023
MD
230418-37-03
Fecal Coliforms
TH3
2759
MPN/g
SM92210E-2006
04/18/2023
MD
230418-37-03
Percent Solids
TH3
1.45
%
SM2540B-2011
04/18/2023
MD
230418-37-04
Fecal Coliforms
TH4
1389
MPN/g
SM92210E-2006
04/18/2023
MD
230418-37-04
Percent Solids
TH4
1.44
%
SM2540B-2011
04/18/2023
MD
230418-37-05
Fecal Coliforms
TH5
2740
MPN/g
SM92210E-2006
04/18/2023
MD
230418-37-05
Percent Solids
TH5
1.46
%
SM2540B-2011
04/18/2023
MD
230418-37-06
Fecal Coliforms
TH6
5517
MPN/g
SM92210E-2006
04/18/2023
MD
230418-37-06
Percent Solids
TH6
1.45
%
SM2540B-2011
04/18/2023
MD
230418-37-07
Fecal Coliforms
TH7
2759
MPN/g
SM92210E-2006
04/18/2023
MD
230418-37-07
Percent Solids
TH7
1.45
%
SM2540B-2011
04/18/2023
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 230418-37-01 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 230418-37-02 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 230418-37-03 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 230418-37-04 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 230418-37-05 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 230418-37-06 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 230418-37-07 Temp on Arrival: 3.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 4

TYSON-WILKESBORO, NC

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: SC Samples
Lot Number:YE22013
Date Completed:06/07/2023
06/07/2023 2:24 PM
Approved and released by:
Project Manager II: Lucas Odom
P RCGip0,
\%
A4W
TNI :
1N81 xer ava a �rcd srew Bsam
J/
ACC RE D1TED
tE nocueoArmwr
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 9

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: YE22013
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
Due to low percent solids, sample -001 has been analyzed using three times the method defined amount.
The LOQs have been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 9

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: YE22013
Sample Number Sample ID Matrix Date Sampled Date Received
001 TYSON WILKESBORO Solid 05/16/2023 0800 05/22/2023
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 9

PACE ANALYTICAL SERVICES,
LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: YE22013
Sample
Sample ID
Matrix Parameter Method
Result Q
Units
Page
001
TYSON WILKESBORO
Solid % Volatile Solids SM 2540G-
98
%
5
001
TYSON WILKESBORO
Solid Ammonia - N (gas 350.1
1600
mg/kg
5
001
TYSON WILKESBORO
Solid Nitrate -Nitrite - N (soluble) 353.2
17
mg/kg
5
001
TYSON WILKESBORO
Solid Phosphorus 365.1
1400
mg/kg
5
001
TYSON WILKESBORO
Solid TKN 351.2
15000
mg/kg
5
001
TYSON WILKESBORO
Solid Aluminum 6010D
260
mg/kg
6
001
TYSON WILKESBORO
Solid Copper 6010D
25
mg/kg
6
001
TYSON WILKESBORO
Solid Zinc 6010D
33
mg/kg
6
(8 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 9

Client: Terra Renewal Services, Inc. Laboratory ID:YE22013-001
Description: TYSON WILKESBORO Matrix: Solid
Date Sampled:05/16/2023 0800 % Solids: 9.73 05/31/2023 2154
Date Received:05/22/2023
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
(% Volatile S) SM 254OG-1997
1
05/23/2023 2218 CBP
76021
1 350.1
(Ammonia - N ) 350.1
5
06/02/2023 1028 CMM
76744
1
(Nitrate-Nitr) 353.2
1
05/26/2023 1534 CLL2
76561
1
(Phosphorus) 365.1
5
05/30/2023 1657 DMA
05/24/2023 2155 76153
1
(Soil pH meas) 9045D
1
05/24/2023 2052 CLL
76327
1 351.4
(TKN) 351.2
2
05/26/2023 1638 DMA
05/25/2023 1536 76152
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
98
%
1
Ammonia - N (gas diffusion)
350.1
1600
510
mg/kg
1
Nitrate -Nitrite - N (soluble)
353.2
17
2.1
mg/kg
1
Phosphorus
7723-14-0 365.1
1400
260
mg/kg
1
Soil pH measured in water @ 19.5 ° C
9045D
4.2
su
1
TKN
351.2
15000
1000
mg/kg
1
PCBs by GC
Run Prep Method Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A 8082A
1 05/31/20231537 SAF
05/23/20231741 75998
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
170
ug/kg
1
Aroclor 1221
11104-28-2 8082A
ND
170
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
170
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
170
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
170
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
170
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
170
ug/kg
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Decachlorobiphenyl
69 41-132
Tetrachloro-m-xylene
62 35-106
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date Batch
1 7471B
7471B
1 06/01/20230916 KAJ 05/31/20231550 76364
CAS Analytical
Parameter
Number Method Result Q LOQ
Units Run
Mercury
7439-97-6 7471 B ND 0.82
mg/kg 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 9

Client: Terra Renewal Services, Inc. Laboratory ID:YE22013-001
Description: TYSON WILKESBORO Matrix: Solid
Date Sampled:05/16/2023 0800 % Solids: 9.73 05/31/2023 2154
Date Received:05/22/2023
ICP-AES
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3050B 6010D 1 06/05/2023 1508 LAB 05/31/2023 1925 76607
Parameter
CAS Analytical
Number Method Result Q LOQ Units Run
Aluminum
7429-90-5
6010D
260
59
mg/kg
1
Arsenic
7440-38-2
6010D
ND
2.2
mg/kg
1
Cadmium
7440-43-9
6010D
ND
0.74
mg/kg
1
Calcium
7440-70-2
6010D
ND
740
mg/kg
1
Copper
7440-50-8
6010D
25
1.5
mg/kg
1
Lead
7439-92-1
6010D
ND
1.5
mg/kg
1
Magnesium
7439-95-4
6010D
ND
740
mg/kg
1
Molybdenum
7439-98-7
6010D
ND
5.9
mg/kg
1
Nickel
7440-02-0
6010D
ND
5.9
mg/kg
1
Potassium
7440-09-7
6010D
ND
740
mg/kg
1
Selenium
7782-49-2
6010D
ND
2.9
mg/kg
1
Sodium
7440-23-5
6010D
ND
740
mg/kg
1
Zinc
7440-66-6
6010D
33
7.4
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 9
Q = Surrogate failure
L = LCS/LCSD failure
S = MS/MSD failure

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 9

PACE ANALYTICAL SERVICES, LLC
in
-3-
2LI.
4
31
,—r.' 'A
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 9

PACE ANALYTICAL SERVICES, LLC
DC# Yitfe, E W-FRM-WCOt-0286 V02—Samples Receipt Checklist (SRC)
Effocllve Date, 81212022
Sample a ipt Cheddist (SRQ
CH.,t, TIRR RE -NE AL Caatcr iLt crcd L�,widatc: Cn r 5rM 23 Lour "F22013
TAMU of receipt;
Pace
'1elicit
UPS I jFtWEx-LjC0Cr:
Yts
a
1-Wcl'eeast My su15 cszal Oil -lie C00120
Yes
i,�o , N?
2- If mswdy seals wit prestnt, weve tteviniact arxi linbrak-eiy'2
H *.`tna ID: C111canaw Stnp ID, Nf- Tinted by; r1A
Oiig.Lal 1talpejallAe flpole 1CCeip( I 1 1'IVW (CW0' Cted) timpitratue Upon dCC:11 i %i Sefid Snap-i iiji Tlx:
4.9 r4,9 aC NA f NA NA INIA vU %A rNA c?c
eUL F--j'Tc1ilpc1a1l1i.'c Ulruik Agan1bI Bolrlrs IR Gr4L ID: 3R Ctuni Correction Factor C
MC60b of coolant We fxw I I Ter lads n ay Ice mane
Yl' s
❑ No
A
3. wefe 01 CoOICI-, rCL`civcd of cff b lu%v 6-10"U. Xiju, was PigIect A-W@W 114Yd
PM was Notitit i by: phrnt ! email f (circle one},
Yes
Lj
Na
A
4. Is the -xin uercial coulkf s pactaug Slip a'taclicd t1La this f m?
v'
Yes
tlo
5. Were proper cu- twdy proccftj s (rc: Ur q"i!direceived) followed.
Yes
Nu
6, Were -swn rlc tits listed an the C OC and all smi4;jc zonlainers?
yv�j
YCs 1
71
tin
17. Was collection date &- time listeur on :lle COC .111 a ll 59W4 le cautai ICES.'
As
o
S. Did �dl container lsbelit&fjuadon (ID, date, true) ap-ce willi the 000-
,/
Yes
i~to
9 Were tL:3ts to belxe,L'fanMd listed on tie. COC`r
�Y'zs
my
1,0.Ihd ail sauiplcs ariivc na 6r. proper cmit lirfers fa¢•each test andlor ill good OC1tdLliga
(wibrok ai. lids as cm)?
[,(]Yes]
wo
) 1. Was ad1:qutlle sampI.0 whnile jvailabl0
7
�i e$
No
��- ��ere aLl Salllpl�s ]-C'vCSL'C� ��llkl?]Jl ::ti1C l101C'�L1�T C]]Ik; {�L�� 1.LLSrllS- 'A'�ll['1 LC;'ei Cfs�ll2: �11'i 'l
QYes
❑ NG
13. WtM -111 sa111pits Containers accolrnled fnu'' (�Tannssiu�l�+€teS�}
Y C
No
�l i
14. Were -110A. 5O15C nW RSi£-175�es free of ol`LAUIt4 >"PCR-Silt" C/4"or Crllill ill
dlnir tee) ill any of 111e. VOA vials`'
15.efC Ali 1]R0+[T1WCryEs alllLll2ill S15I1 'es teCL1VCd at apH 7? -
YfiS
'r es
I'No+1.1
o
,
16. Welre ali Hide 5URPlcs TCCCNr- - aC ;i pH > 12 and suffi lt• saiuples received a' a 13 > V
❑ _
❑ 1 rD
[a'k
1 , , were3 1 LCA �I;r Its+t Xw:ll 2r�J i 119I'G ,sib[}R? ( 0.5� kuUf 531LSple5 Vie. f
rl' ideal l'lAaL r-?
lqyr i
[I fro
r INA
IS. Was the quote number listed oft the MillMirrer labrl? l )7es, Io1,r 4
.9ainph PL'f9P1'3:11i0n ',N-Ti:%r he cons }feted for Any satnpie(s) Ilicorrectl V []I S£1' cd UT 11ML lLMlispavc.)
sa1uplc(s) 5;. - -- ---wuc rcccivcd incmTccfly L]I•C$ci-wd and were adjus d acxrdiugly
LPL sIIl-�)IL: 1tX V1iL wilk NA —111f. {I C c-ir lc auc: 1'I2$ , TM3, HC1- k0H 1Lsh:g SR i '4A _
j1iL" OP1ri SeFVallOn A� IL moir khan one jresCLvAtive is iiuded- pkwe nDie in die comiml.5+11C ow.
Sarnple(s) 1ver- Yee-iwd 1Arh bubWs ?C lnlll ill L'liAl=ller.
Sal;ljrles(s) VA vugc 1'Cct�.?Cd wit.11 TItc' > 0-5 11,�'L (114t 9 is no) and 'ere
adjusb!d ac"QW&O. y iu sauipte feceibrilpg {with sodium dl osrjlfak Ck$, v) with Uniga ID; NiA
001112MI�5;
Qualtrdx I D: 56360 Pace° Analytlral Services, LLC Pago 1 of 1
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 9

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: SC Samples
Lot Number:XL29024
Date Completed:01/13/2023
01/17/2023 4:11 PM
Approved and released by:
Project Manager II: Lucas Odom
P RCGip0,
\%
A16
TNI :
1N81 xer ava a �rcd srew Bsam
J/
ACC RE D1TED
tE nocueoArmwr
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 10

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: XL29024
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 10

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: XL29024
Sample Number Sample ID Matrix Date Sampled Date Received
001 TYSON WILKESBORO Solid 12/27/2022 1000 12/29/2022
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 10

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: XL29024
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 TYSON WILKESBORO Solid Flashpoint (Pensky- 1010B >140 ° F 5
(1 detection)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 10

Client: Terra Renewal Services, Inc. Laboratory ID:XL29024-001
Description: TYSON WILKESBORO Matrix: Solid
Date Sampled:12/27/2022 1000 % Solids: 3.50 01/03/2023 1657
Date Received:12/29/2022
Inorganic
non-metals
Run Prep Method
Analytical Method
Dilution
Analysis Date Analyst Prep Date Batch
1
(Flashpoint () 1010B
1
01/12/2023 2329 CBP 64784
1
(Reactive Cya) 7.3.3
1
01/06/2023 1414 SJL 01/03/2023 1236
1
(Reactive Sul) 7.3.4
1
01/10/2023 1735 CVR 01/09/2023 1221
1
(Soil pH meas) 9045D
1
12/30/2022 1528 BMG2 63751
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Flashpoint (Pensky-Martens Closed -Cup)
1010B
>140
140
o F
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water @ 16.1 ° C
9045D
3.8
su
1
TCLP Volatiles
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B 8260D
10 01/09/20231831 CDA
64449 12/29/20221645
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Benzene
71-43-2 8260D
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
0.10
mg/L
1
Carbon tetrachloride
56-23-5 8260D
ND
0.050
mg/L
1
Chlorobenzene
108-90-7 8260D
ND
0.050
mg/L
1
Chloroform
67-66-3 8260D
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
0.050
mg/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
0.050
mg/L
1
Tetrachloroethene
127-18-4 8260D
ND
0.050
mg/L
1
Trichloroethene
79-01-6 8260D
ND
0.050
mg/L
1
Vinyl chloride
75-01-4 8260D
ND
0.010
mg/L
1
Run 1 Acceptance
Surrogate Q % Recovery Limits
Bromofluorobenzene
93 70-130
1,2-Dichloroethane-d4
90 70-130
Toluene-d8
96 70-130
TCLP Semivolatiles
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8270E
1 01/05/2023 1342 CMF
01/03/2023 1355 64019 12/29/2022 1649
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units Run
1,4-Dichlorobenzene
106-46-7 8270E
ND
0.040
mg/L 1
2,4-Dinitrotoluene
121-14-2 8270E
ND
0.080
mg/L 1
Hexachlorobenzene
118-74-1 8270E
ND L
0.040
mg/L 1
Hexachlorobutadiene
87-68-3 8270E
ND
0.040
mg/L 1
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 10

Client: Terra Renewal Services, Inc. Laboratory ID:XL29024-001
Description: TYSON WILKESBORO Matrix: Solid
Date Sampled:12/27/2022 1000 % Solids: 3.50 01/03/2023 1657
Date Received: 12/29/2022
TCLP Semivolatiles
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8270E
1 01/05/2023 1342 CMF
01/03/2023 1355 64019 12/29/2022 1649
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
Hexachloroethane
67-72-1 8270E
ND
0.040
mg/L
1
2-Methylphenol
95-48-7 8270E
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5 8270E
ND
0.040
mg/L
1
Nitrobenzene
98-95-3 8270E
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5 8270E
ND
0.20
mg/L
1
Pyridine
110-86-1 8270E
ND L
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4 8270E
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2 8270E
ND
0.040
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
94 37-129
2-Fluorophenol
42 24-127
Nitrobenzene-d5
91 38-127
Phenol-d5
58 28-128
Terphenyl-d 14
104 10-148
2,4,6-Tribromophenol
115 41-144
TCLP Herbicides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/8151A
8151A
1 01/05/2023 1513 SAF
01/03/2023 2007 64037 12/29/2022 1649
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
2,4-D
94-75-7 8151A
ND
0.020
mg/L
1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
59 50-112
TCLP Pesticides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8081B
1 01/05/20231734 DAL1
01/03/20231111 63978 12/29/2022 1649
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
gamma-BHC (Lindane)
58-89-9 8081 B
ND
0.00040
mg/L
1
Chlordane
57-74-9 8081 B
ND
0.0040
mg/L
1
Endrin
72-20-8 8081 B
ND
0.00040
mg/L
1
Heptachlor
76-44-8 8081 B
ND
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3 8081 B
ND
0.00040
mg/L
1
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 10

Client: Terra Renewal Services, Inc. Laboratory ID:XL29024-001
Description: TYSON WILKESBORO Matrix: Solid
Date Sampled:12/27/2022 1000 % Solids: 3.50 01/03/2023 1657
Date Received: 12/29/2022
TCLP Pesticides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8081B
1 01/05/20231734 DAL1
01/03/20231111 63978 12/29/2022 1649
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Methoxychlor
72-43-5 8081 B
ND
0.0016
mg/L
1
Toxaphene
8001-35-2 8081B
ND
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
58 20-131
Tetrachloro-m-xylene
94 26-132
TCLP Metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3010A
6010D
1 01/05/2023 2050 JMH
01/05/2023 0910
64107 12/29/2022 1649
1 1311/7470A
7470A
1 01/05/2023 1639 MRW2
01/05/2023 1150 64188 12/29/2022 1649
3 1311/3010A
6010D
1 01/11/2023 2051 JMH
01/11/2023 1118 64604 01/10/2023 1605
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2 6010D
ND
0.15
mg/L
1
Barium
7440-39-3 6010D
ND
0.25
mg/L
3
Cadmium
7440-43-9 6010D
ND
0.050
mg/L
1
Chromium
7440-47-3 6010D
ND
0.10
mg/L
1
Lead
7439-92-1 6010D
ND
0.10
mg/L
1
Mercury
7439-97-6 7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2 6010D
ND
0.20
mg/L
1
Silver
7440-22-4 6010D
ND
0.10
mg/L
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 10

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 10

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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 10

PACE ANALYTICAL SERVICES, LLC
DC# Tn's. ENV-FRM-WCOL-0286vD2 Samples R*ceiptChecklistiSRCI
Effective Date- 91'2M22
Sample receipt Checklist ( RQ
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 10

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 05/16/2023
Reported: 05/17/2023
For: Tyson Wilkesboro
Comments: GEOMETRIC MEAN: 233,469 MPN/g
STATESVILLE
4 ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
230516-22-01
Fecal Coliforms
TW1
225166
MPN/g
SM92210E-2006
05/16/2023
MD
230516-22-01
Percent Solids
TW1
7.55
%
SM2540B-2011
MD
230516-22-02
Fecal Coliforms
TW2
264386
MPN/g
SM92210E-2006
05/16/2023
MD
230516-22-02
Percent Solids
TW2
6.43
%
SM2540B-2011
MD
230516-22-03
Fecal Coliforms
TW3
281030
MPN/g
SM92210E-2006
05/16/2023
MD
230516-22-03
Percent Solids
TW3
8.54
%
SM2540B-2011
MD
230516-22-04
Fecal Coliforms
TW4
234483
MPN/g
SM92210E-2006
05/16/2023
MD
230516-22-04
Percent Solids
TW4
7.25
%
SM2540B-2011
MD
230516-22-05
Fecal Coliforms
TW5
125786
MPN/g
SM92210E-2006
05/16/2023
MD
230516-22-05
Percent Solids
TW5
6.36
%
SM2540B-2011
MD
230516-22-06
Fecal Coliforms
TW6
417827
MPN/g
SM92210E-2006
05/16/2023
MD
230516-22-06
Percent Solids
TW6
7.18
%
SM2540B-2011
MD
230516-22-07
Fecal Coliforms
TW7
183387
MPN/g
SM92210E-2006
05/16/2023
MD
230516-22-07
Percent Solids
TW7
9.27
%
SM2540B-2011
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 230516-22-01 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 230516-22-02 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 230516-22-03 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 230516-22-04 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 230516-22-05 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 230516-22-06 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
Sample Number 230516-22-07 Temp on Arrival: 2.3
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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Page 4y4

WAYNE FARMS - DOBSON, NC

aceAnalytical
Report of Analysis
Terra Renewal Services, Inc.
PO Box 3036
Russellville, AR 72811
Attention: David Coyle
Project Name: SC Samples
Lot Number:YE08004
Date Completed:06/01/2023
06/02/2023 10:32 AM
Approved and released by:
Project Manager II: Lucas Odom
P RCGip0,
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The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 11

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terra Renewal Services, Inc.
Lot Number: YE08004
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
To follow the standard operating procedures 10ml of HNO3 was added to the sample during digestion due
to chemical fuming. The following sample(s) needed an extra 5ml to stop the fuming due to the nature of
the sample matrix: YE08004-001. The LOQ has been adjusted to reflect this change.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 11

PACE ANALYTICAL SERVICES, LLC
Sample Summary
Terra Renewal Services, Inc.
Lot Number: YE08004
Sample Number Sample ID Matrix Date Sampled Date Received
001 WAYNE FARMS DOBSON Solid 05/04/2023 0900 05/08/2023
(1 sample)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 11

PACE ANALYTICAL SERVICES, LLC
Detection Summary
Terra Renewal Services, Inc.
Lot Number: YE08004
Sample
Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
WAYNE FARMS DOBSON
Solid
% Volatile Solids
SM 2540G-
95
%
5
001
WAYNE FARMS DOBSON
Solid
Ammonia - N (gas
350.1
8600
mg/kg
5
001
WAYNE FARMS DOBSON
Solid
Flashpoint (Pensky-
1010B
>140
° F
5
001
WAYNE FARMS DOBSON
Solid
Nitrate -Nitrite - N (soluble)
353.2
22
mg/kg
5
001
WAYNE FARMS DOBSON
Solid
Phosphorus
365.1
3400
mg/kg
5
001
WAYNE FARMS DOBSON
Solid
TKN
351.2
61000
mg/kg
5
001
WAYNE FARMS DOBSON
Solid
3+4-Methylphenol
8270E
0.12
mg/L
6
001
WAYNE FARMS DOBSON
Solid
Barium
6010D
0.46
mg/L
8
001
WAYNE FARMS DOBSON
Solid
Aluminum
6010D
230
mg/kg
8
001
WAYNE FARMS DOBSON
Solid
Calcium
6010D
19000
mg/kg
8
001
WAYNE FARMS DOBSON
Solid
Copper
6010D
47
mg/kg
8
001
WAYNE FARMS DOBSON
Solid
Magnesium
6010D
440
mg/kg
8
001
WAYNE FARMS DOBSON
Solid
Nickel
6010D
4.4
mg/kg
8
001
WAYNE FARMS DOBSON
Solid
Potassium
6010D
650
mg/kg
8
001
WAYNE FARMS DOBSON
Solid
Sodium
6010D
560
mg/kg
8
001
WAYNE FARMS DOBSON
Solid
Zinc
6010D
150
mg/kg
8
(16 detections)
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 11

Client: Terra Renewal Services, Inc. Laboratory ID:YE08004-001
Description: WAYNE FARMS DOBSON Matrix: Solid
Date Sampled:05/04/2023 0900 % Solids: 27.7 05/09/2023 2312
)ate Received:05/08/2023
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 (% Volatile
S) SM 254OG-1997
1 05/11/2023 2151 CBP
75114
1 350.1
(Ammonia - N ) 350.1
100 05/10/2023 1221 CMM
74915
1
(Flashpoint () 1010B
1 05/18/2023 2022 CBP
75737
1
(Nitrate-Nitr) 353.2
1 05/12/2023 1301 C1_1_2
75283
1
(Phosphorus) 365.1
25 05/18/2023 1158 BMG2
05/14/2023 2140
75220
1
(Reactive Cya) 7.3.3
1 05/21/2023 1936 NAB
05/18/2023 1935
1
(Reactive Sul) 7.3.4
1 05/19/2023 1144 CVR
05/18/2023 1935
1
(Soil pH meas) 9045D
1 05/09/2023 1620 LMM2
74135
1 351.4
(TKN) 351.2
20 05/26/2023 1624 DMA
05/25/2023 1536
76152
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
% Volatile Solids
SM 254OG-1997
95
%
1
Ammonia - N (gas diffusion)
350.1
8600
3600
mg/kg
1
Flashpoint (Pensky-Martens
Closed -Cup)
101013
>140
140
o F
1
Nitrate -Nitrite - N (soluble)
353.2
22
0.72
mg/kg
1
Phosphorus
7723-14-0 365.1
3400
450
mg/kg
1
Reactive Cyanide
7.3.3
ND
50
mg/kg
1
Reactive Sulfide
7.3.4
ND
50
mg/kg
1
Soil pH measured in water @ 15.5 o C
9045D
5.6
su
1
TKN
351.2
61000
3600
mg/kg
1
TCLP Volatiles
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/5030B
8260D
10 05/25/2023 1559 AMR2
76239 05/15/2023 2132
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Benzene
71-43-2 8260D
ND
0.050
mg/L
1
2-Butanone (MEK)
78-93-3 8260D
ND
0.10
mg/L
1
Carbon tetrachloride
56-23-5 8260D
ND
0.050
mg/L
1
Chlorobenzene
108-90-7 8260D
ND
0.050
mg/L
1
Chloroform
67-66-3 8260D
ND
0.050
mg/L
1
1,2-Dichloroethane
107-06-2 8260D
ND
0.050
mg/L
1
1,1-Dichloroethene
75-35-4 8260D
ND
0.050
mg/L
1
Tetrachloroethene
127-18-4 8260D
ND
0.050
mg/L
1
Trichloroethene
79-01-6 8260D
ND
0.050
mg/L
1
Vinyl chloride
75-01-4 8260D
ND
0.010
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
104 70-130
1,2-Dichloroethane-d4
103 70-130
Toluene-d8
ill 70-130
LOQ = Limit of Quantitation
B = Detected in the method blank
E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above the LOQ
N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 11

Client: Terra Renewal Services, Inc. Laboratory ID:YE08004-001
Description: WAYNE FARMS DOBSON Matrix: Solid
Date Sampled:05/04/2023 0900 % Solids: 27.7 05/09/2023 2312
Date Received:05/08/2023
TCLP Semivolatiles
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8270E
1 05/19/2023 1554 JCG
05/15/2023 1519 75254 05/11/2023 2139
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
1,4-Dichlorobenzene
106-46-7 8270E
ND
0.040
mg/L
1
2,4-Dinitrotoluene
121-14-2 8270E
ND
0.080
mg/L
1
Hexachlorobenzene
118-74-1 8270E
ND
0.040
mg/L
1
Hexachlorobutadiene
87-68-3 8270E
ND
0.040
mg/L
1
Hexachloroethane
67-72-1 8270E
ND
0.040
mg/L
1
2-Methylphenol
95-48-7 8270E
ND
0.040
mg/L
1
3+4-Methylphenol
106-44-5 8270E
0.12
0.040
mg/L
1
Nitrobenzene
98-95-3 8270E
ND
0.040
mg/L
1
Pentachlorophenol
87-86-5 8270E
ND
0.20
mg/L
1
Pyridine
110-86-1 8270E
ND L
0.040
mg/L
1
2,4,5-Trichlorophenol
95-95-4 8270E
ND
0.040
mg/L
1
2,4,6-Trichlorophenol
88-06-2 8270E
ND
0.040
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
70 37-129
2-Fluorophenol
63 24-127
Nitrobenzene-d5
88 38-127
Phenol-d5
71 28-128
Terphenyl-d14
75 10-148
2,4,6-Tribromophenol
74 41-144
TCLP Herbicides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/8151A
8151A
1 05/16/2023 1151 MEZ
05/14/2023 0930 75210 05/11/2023 2139
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
2,4-D
94-75-7 8151A
ND
0.020
mg/L
1
2,4,5-TP (Silvex)
93-72-1 8151A
ND
0.0050
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
DCAA
63 50-112
PCBs by GC
Run Prep Method
Cleanup Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C
366013/3665A 8082A
1 05/15/2023 1138 MEZ
05/12/2023 1102 75136
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
Aroclor 1016
12674-11-2 8082A
ND
60
ug/kg
1
LOQ = Limit of Quantitation
B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
Q = Surrogate failure
ND = Not detected at or above
the LOQ N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
L = LCS/LCSD
failure
H = Out of holding time
W = Reported on wet weight basis
S = MS/MSD
failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 11

Client: Terra Renewal Services, Inc. Laboratory ID:YE08004-001
Description: WAYNE FARMS DOBSON Matrix: Solid
Date Sampled:05/04/2023 0900 % Solids: 27.7 05/09/2023 2312
Date Received:05/08/2023
PCBs by GC
Run Prep Method Cleanup
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3550C 366013/3665A
8082A
1 05/15/2023 1138 MEZ
05/12/2023 1102 75136
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aroclor 1221
11104-28-2 8082A
ND
60
ug/kg
1
Aroclor 1232
11141-16-5 8082A
ND
60
ug/kg
1
Aroclor 1242
53469-21-9 8082A
ND
60
ug/kg
1
Aroclor 1248
12672-29-6 8082A
ND
60
ug/kg
1
Aroclor 1254
11097-69-1 8082A
ND
60
ug/kg
1
Aroclor 1260
11096-82-5 8082A
ND
60
ug/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
82 41-132
Tetrachloro-m-xylene
78 35-106
TCLP Pesticides
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3520C
8081B
1 05/16/20231825 SAF
05/15/20231202 75248 05/11/20232139
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
gamma-BHC (Lindane)
58-89-9 8081 B
ND S
0.00040
mg/L
1
Chlordane
57-74-9 8081 B
ND
0.0040
mg/L
1
Endrin
72-20-8 8081 B
ND S
0.00040
mg/L
1
Heptachlor
76-44-8 8081 B
ND S
0.00040
mg/L
1
Heptachlor epoxide
1024-57-3 8081 B
ND S
0.00040
mg/L
1
Methoxychlor
72-43-5 8081 B
ND S
0.0016
mg/L
1
Toxaphene
8001-35-2 8081B
ND S
0.0080
mg/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Decachlorobiphenyl
53 20-131
Tetrachloro-m-xylene
115 26-132
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 05/23/2023 1105 KAJ
05/23/2023 0217 75499
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Mercury
7439-97-6 7471 B
ND
0.26
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 11

Client: Terra Renewal Services, Inc. Laboratory ID:YE08004-001
Description: WAYNE FARMS DOBSON Matrix: Solid
Date Sampled:05/04/2023 0900 % Solids: 27.7 05/09/2023 2312
Date Received:05/08/2023
TCLP Metals
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Leachate Date
1 1311/3010A
6010D 1 05/17/2023 0417 JMH
05/16/2023 2046 75316 05/11/2023 2139
1 1311/7470A
7470A 1 05/15/2023 1651 KAJ
05/15/2023 1234 75275 05/11/2023 2139
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Arsenic
7440-38-2 6010D
ND
0.15
mg/L
1
Barium
7440-39-3 6010D
0.46
0.25
mg/L
1
Cadmium
7440-43-9 601 OD
ND
0.050
mg/L
1
Chromium
7440-47-3 6010D
ND
0.10
mg/L
1
Lead
7439-92-1 6010D
ND
0.10
mg/L
1
Mercury
7439-97-6 7470A
ND
0.0020
mg/L
1
Selenium
7782-49-2 6010D
ND
0.20
mg/L
1
Silver
7440-22-4 6010D
ND
0.10
mg/L
1
ICP-AES
Run Prep Method
1 3050B
2 3050B
Analytical Method Dilution Analysis Date Analyst
601 OD 1 05/26/2023 0508 JMH
601 OD 5 05/26/2023 0515 JMH
Prep Date Batch
05/24/2023 0103 75714
05/24/2023 0103 75714
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Aluminum
7429-90-5 6010D
230
21
mg/kg
1
Arsenic
7440-38-2 6010D
ND
0.80
mg/kg
1
Cadmium
7440-43-9 6010D
ND
0.27
mg/kg
1
Calcium
7440-70-2 6010D
19000
1300
mg/kg
2
Copper
7440-50-8 6010D
47
0.54
mg/kg
1
Lead
7439-92-1 6010D
ND
0.54
mg/kg
1
Magnesium
7439-95-4 6010D
440
270
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
2.1
mg/kg
1
Nickel
7440-02-0 6010D
4.4
2.1
mg/kg
1
Potassium
7440-09-7 6010D
650
270
mg/kg
1
Selenium
7782-49-2 6010D
ND
1.1
mg/kg
1
Sodium
7440-23-5 6010D
560
270
mg/kg
1
Zinc
7440-66-6 6010D
150
2.7
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range Q = Surrogate failure
ND = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 8 of 11

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 9 of 11

PACE ANALYTICAL SERVICES, LLC
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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 10 of 11

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Qua trax ID: 563$ Pace' AnWIrtiM!s,aFvices, LLC Pap 1 ai'f
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 11 of 11

Analytical Results
Terra Renewal
PO Box 306
Yadkinville, NC 27055
Receive Date: 05/04/2023
Reported: 05/05/2023
For: Wayne Farms
Comments:
STATESVILLE
4 ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
230504-30-01
Fecal Coliforms
WFDT1
731707
MPN/g
SM92210E-2006
05/04/2023
MD
230504-30-01
Percent Solids
WFDT1
12.3
%
SM2540B-2011
05/04/2023
MD
230504-30-01
pH
WFDT1
7.11
Std. Units
SM4500HB-2011
05/04/2023
MD
230504-30-02
Fecal Coliforms
WFDT2
396826
MPN/g
SM92210E-2006
05/04/2023
MD
230504-30-02
Percent Solids
WFDT2
12.6
%
SM2540B-2011
05/04/2023
MD
230504-30-02
pH
WFDT2
7.04
Std. Units
SM4500HB-2011
05/04/2023
MD
230504-30-03
Fecal Coliforms
WFDT3
62500
MPN/g
SM92210E-2006
05/04/2023
MD
230504-30-03
Percent Solids
WFDT3
14.4
%
SM2540B-2011
05/04/2023
MD
230504-30-03
pH
WFDT3
11.9
Std. Units
SM4500HB-2011
05/04/2023
MD
230504-30-04
Fecal Coliforms
WFDT4
509554
MPN/g
SM92210E-2006
05/04/2023
MD
230504-30-04
Percent Solids
WFDT4
31.4
%
SM2540B-2011
05/04/2023
MD
230504-30-04
pH
WFDT4
7.14
Std. Units
SM4500HB-2011
05/04/2023
MD
230504-30-05
Fecal Coliforms
WFDT5
289389
MPN/g
SM92210E-2006
05/04/2023
MD
230504-30-05
Percent Solids
WFDT5
31.1
%
SM2540B-2011
05/04/2023
MD
230504-30-05
pH
WFDT5
6.94
Std. Units
SM4500HB-2011
05/04/2023
MD
230504-30-06
Fecal Coliforms
WFDT6
157895
MPN/g
SM92210E-2006
05/04/2023
MD
230504-30-06
Percent Solids
WFDT6
15.2
%
SM2540B-2011
05/04/2023
MD
230504-30-06
pH
WFDT6
9.97
Std. Units
SM4500HB-2011
05/04/2023
MD
230504-30-07
Fecal Coliforms
WFDT7
1052632
MPN/g
SM92210E-2006
05/04/2023
MD
230504-30-07
Percent Solids
WFDT7
15.2
%
SM2540B-2011
05/04/2023
MD
230504-30-07
pH
WFDT7
10.02
Std. Units
SM4500HB-2011
05/04/2023
MD
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

Condition of Receipt
Sample Number 230504-30-01 Temp on Arrival: 2.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Parameter Schedule: pH
Received on Ice
Sample Number 230504-30-02 Temp on Arrival: 2.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Parameter Schedule: pH
Received on Ice
Sample Number 230504-30-03 Temp on Arrival: 2.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Parameter Schedule: pH
Received on Ice
Sample Number 230504-30-04 Temp on Arrival: 2.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 4

Parameter Schedule: pH
Received on Ice
Sample Number 230504-30-05 Temp on Arrival: 2.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Parameter Schedule: pH
Received on Ice
Sample Number 230504-30-06 Temp on Arrival: 2.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Parameter Schedule: pH
Received on Ice
Sample Number 230504-30-07 Temp on Arrival: 2.0
Parameter Schedule: Percent Solids
Received on Ice
Parameter Schedule: Fecal Coliforms
Sodium Thiosulfate Received on Ice
Parameter Schedule: pH
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

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PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 4

ATTACHMENT - E:
OPERATION & MAINTENANCE PLAN

TERRA
renewal
PO BOX 399 • DARDANELLE • ARKANSAS • 72834
479.747.8192
terrarenewal.com
OPERATION & MAINTENANCE PLAN
Permit #: WQ0038087
(Last Revision: January 2022)
OPERATION OVERVIEW:
These operations are intended to provide residuals management for the proposed generating
facilities listed in the "Residuals Source Facility Attachment" of Form RSC 11-13 of the
corresponding permit application and Attachment -A of the finalized permit. The services include
the removal of pretreatment D.A.F. residuals that are generated on a daily basis at most of the
facilities. These residuals contain nutrients and organic matter that can be utilized as an effective
fertilizer / soil amendment for agricultural purposes. They are non -hazardous and meet the
qualifications for land application, per EPA 40 CFR 257 and North Carolina 15A NCAC 02T
regulations. Terra Renewal Services, Inc is the Permittee for the land base associated with this
permit is responsible for managing the land application of the residuals.
The residuals will be land applied on local farm sites at agronomic rates. Detailed maps and site
characterization for the sites are provided as part of the permit application. Agronomic rates are
established based on county and soil specific Realistic Yield Expectations (RYE) provided by
NCSU. The application rate of the residuals should not exceed the Realistic Nitrogen
Requirements of the crop to be grown based on the amount of Plant Available Nitrogen (PAN)
contained in the material. PAN is calculated, based on the most recent analysis, with the
following equation:
PAN = MR (TKN - NH3) + VR (NH3) + NO3 + NO2
MR = Mineralization Rate
VR = Volatilization Rate
TKN = Total Kjeldahl Nitrogen
NH3 = Ammonia - N
NO3 = Nitrate - N
NO2 = Nitrite — N
A Plant Available Nitrogen Summary is provided under Section III (Residuals Land Application
Program), Item 4 of Form: RLAP 03-15 as part of the permit application. Tables summarizing the
PAN requirements for proposed crops based on the RYE's for each field and predominant soil
series are provided in the Soils and Agronomic Evaluation section of the permit application.
Mineralization Rates & Volatilization Rates utilized for PAN calculation will be specific to the rates
certified in the permit and the type of application required based on vector attraction criteria for
each facility.
The residuals are to be applied to the fields via subsurface injection or incorporation. Residuals
will be transferred from holding tanks at the generating facility via vacuum pump onto sealed
tanker trucks for transport to the land application sites. At the land application sites, residuals
Page 1 of 6

may be transferred from the tankers directly to the application equipment or to mobile frac tanks
(b/w 18,000 and 24,000 gallon capacity) that are utilized for staging purposes. All transfers will
be conducted via 4-inch steel reinforced umbilical hoses with cam lock fittings and vacuum
pumps mounted on the tankers or the spreading equipment.
The application equipment may include an Ag-Chem Terragator with a +/- 4,000 gallon tank or a
spreader buggy with a 4,600 or 6,000 gallon tank pulled by a farm tractor. Both are mounted with
high flotation tires and vacuum / pressure pumps. A subsoil injection system may be utilized, or
the residuals may be surface applied followed by incorporation at time frames specified in the
permit. These are the methods by which Vector Attraction Reduction requirements will be met.
Application equipment will be calibrated when application rates change to ensure that agronomic
rates are met and the residuals are evenly distributed.
Mobile frac tanks may be used for staging and transfer of residuals during normal spreading
operations at active land application sites. Residuals in the frac tanks may be held at the site
during periods of inclement weather, or when land application is precluded. When land
application activities resume, the residuals in the frac tanks will be removed and land applied.
When application to a site is complete, the frac tanks will be emptied and moved to the next site.
Empty frac tanks may be stored at the land application program base of operations. Long term
storage of residuals may only be performed at permitted storage facilities. A separate O&M Plan
for the storage facilities has been developed and approved as part of the permitting process.
The residuals will be land applied in an agronomic manner based on the requirements set forth by
the NCDENR DWR and the conditions of the permit. Agronomic rates will be limited by the
nitrogen requirements of the crop to be grown based on the NCSU RYE. If crops to be grown
differ from those listed as the "proposed crops" in the permit application, then the appropriate
application rate will be set based on the NCSU RYE data for the specific site and crop to be
grown.
Soil pH will be adjusted based on site specific soil analysis with application rates based on the
recommendation of the laboratory agronomist. Liming of the fields will be performed at the
earliest convenience based on timing of application and crop rotations, but will be performed
within the calendar year when application to a field occurs. The target soil pH will be set by the
laboratory agronomist and by the conditions of the permit.
The properties proposed for land application and storage are privately owned and are not public
contact sites. Access to the sites is controlled by the landowners and operators. During active
application, access will also be controlled by Terra Renewal personnel or its contractors. The
landowners and farmers will be notified of the 30-day public access restriction prior to any land
application. Signage for public notification prior to application and for the purpose of controlling
public access to the site for 30 days after application will be posted based on the requirements of
the permit. All signage will be supplied and posted by Terra Renewal personnel or its
contractors.
Personnel involved in the application of residuals will be provided a "field book" that contains a
set of buffer maps and appropriate application rates for each field. Each individual will be briefed
on the sensitive features of each field and limits established by the ORC prior to application.
Page 2 of 6

INSPECTIONS:
Inspections will be performed by the Operator in Responsible Charge (ORC)
The Primary ORC is:
Luke Mathis; LJC Environmental
Certification # LA1003524
Contact: [phone]; Ismathisa-gmail.com
The Backup ORC is:
David C. Coyle; Senior Environmental Manager- Denali
Certification # LA995723
Contact: [phone]; david. coylea-terrarenewal.com
Ivan Heatwole; Regional Operations Manager - Denali
Certification # LA1002031
Contact: [phone]; ivan.heatwolea-denaliwater.com
Will Hodges; Environmental Manager- Denali
Certification # LA997282
Contact: [phone]; will. hodgesa-denaliwater.com
Inspections will occur as often as necessary to ensure that the land application program is
conducted properly and within the guidelines of the permit. Inspections will concentrate on fields
being actively applied as well as the most recent fields for which residuals application is
complete. Fields scheduled for application will also be inspected to determine soil and field
conditions that may prohibit operation.
Inspections will consist of on -site evaluation of the residuals application and will include, but are
not limited to, the following:
• adherence to buffers / setbacks
• active runoff or conditions that may promote runoff
• presence of nuisance conditions (odors, vectors, etc)
• uniformity of application
• presence or potential for surface ponding or saturation
• effectiveness of incorporation methods
• cleanliness of loading / unloading areas
• weather conditions
• soil conditions
• adherence to RYE - PAN application rates based on field logs and
percentage of field applied
Data will be recorded in a log based on the frequency of inspection. In the event that
noncompliance is observed, the ORC will instruct the appropriate personnel to cease operation in
the areas relative to the noncompliance and give instructions for correction. If an occurrence of
noncompliance results in an immediate hazard to public health or contamination of surface or
ground water, the ORC will mobilize sufficient resources to effectively respond to and contain the
situation. If necessary, the ORC will contact local officials and / or the regional NCDENR office to
report the occurrence. All noncompliance matters will be recorded in the inspection logs.
Page 3 of 6

SAMPLING & MONITORING:
Sampling and monitoring will be performed by qualified personnel through the direction and
assistance of the ORC and Terra Renewal Environmental Manager. Sampling procedures, for
both residuals and soils, will be performed in a manner that produces a representative sample of
the material to be analyzed.
Residuals Sampling:
Sampling and monitoring of residuals will be performed based on the amount of dry short tons of
residuals land applied in a calendar year per 15A NCAC 02T .1111. The monitoring frequency will
be as follows:
Dry Tons Applied
short tons per ear
Monitoring Frequency
Established in 40 CFR 503 and 15A NCAC 02T .1111
< 319
1 / Year
=> 319 - < 1,650
1 / Quarter 4 times per ear
=> 1,650 - < 16,500
1 / 60 Days 6 times per ear
=> 16,500
1 / Month 12 times per ear
* Monitoring frequencies are based on actual dry tons applied per year.
Agronomic rates will be adjusted accordingly based on these data.
All samples will be analyzed by a North Carolina Certified Laboratory for the following
parameters:
Metals
Arsenic
Cadmium
Copper
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
Nutrients & Other:
Aluminum
Ammonia -Nitro en
Calcium
Magnesium
Nitrate -Nitrite Nitrogen
ph
Phosphorus
Potassium
Sodium
Total Kjeldahl Nitrogen
% Total Solids
% Volatile Solids
Page 4 of 6

Samples will also be analyzed for Fecal Density to confirm that Pathogen Reduction
Requirements are being met per the conditions of the permit.
At least one sample per year will be analyzed for the following TCLP parameters to ensure that
no hazardous constituents are present. TCLP parameters will include the following:
TCLP:
H for Corrosivity
Heptachlor and its Hydroxide
Flash Point for Ignitability
Hexachlorobenzene
Sulfides & Cyanides for Reactivity
Hexachloro-1,3-Butadiene
Arsenic
Hexachloroethane
Barium
Lead
Benzene
Lindane
Cadmium
Mercury
Carbon Tetrachloride
Methox chlor
Chlordane
Methyl Ethyl Ketone
Chlorobenzene
Nitrobenzene
Chloroform
Pentachlorophenol
Chromium
Pyridine
m-Cresol
Selenium
o-Cresol
Silver
-Cresol
Tetrachloroeth lene
Cresol
Toxa hene
2,4-D
Trichloroeth lene
114-Dichlorobenzene
2,4,5-Trichloro henol
1,2-Dichloroethane
2,4,6-Trichlorophenol
1,1-Dichloroeth lene
2,4,5-TP Silvex
2,4-Dinitrotoluene
Vinyl Chloride
Endrin
Soil Sampling:
Composite soil samples will be collected for each delineated land application field in the
respective calendar year for which a land application event occurs. Soil samples will be collected
based on accepted agronomic standards and analyzed by a North Carolina Certified Laboratory
for the following parameters:
Standard Soil Fertility Analysis:
Acidity
Manganese
Calcium
% Humic Matter
CEC
pH
Copper
Phosphorus
Base Saturation
Potassium
ESP
Sodium
Magnesium
Zinc
Page 5 of 6

SPILL PREVENTION & RESPONSE:
For the purposes of this operation, a spill will be defined as: "The accidental release or discharge
of a sufficient quantity of residuals, fuel, or other foreign material that cannot be effectively
contained or removed by a single individual, with minimal effort, in a short amount of time. OR,
the release of ANY quantity of foreign material into surface waters, wetlands, ditches, drainage
areas, public rights of way, or adjacent properties." All spills and releases must be reported
immediately to the ORC and Terra Renewal supervisor. All Terra Renewal employees and sub-
contractors will be expected to understand and adhere to the following Spill Prevention &
Response Procedures:
For Spill Prevention, personnel shall take the following steps:
• Ensure truck drivers watch trailer while loading.
• Ensure hose connections and valves are properly secured while loading / unloading.
• Ensure container hatches / lids are closed and secured while transporting.
• Inspect container hatches / lids and replace as necessary.
• Ensure loading / unloading operations in the field are conducted to minimize spillage.
For Spill Response, personnel shall take the following steps:
• Identify the source of the spill / discharge and attempt to curtail or stop the flow.
• Immediately contact an ORC. Explain the situation as thoroughly as possible. This
will allow them to assess the situation and provide instructions.
• Familiarize yourself with the nearby terrain. If possible, try to contain the material or
prevent it from flowing further or entering surface waters.
• If you are able to contain the spill / discharge, attempt to vacuum up or collect the
excess material before it can be absorbed into the ground, and/or prevent additional
run-off.
• Do not allow any non -operational individuals or bystanders to contact the material,
even those offering assistance.
• If at a source facility, contact the facility personnel at the location where you were
working when the spill/discharge occurred. Do not alarm them. Be calm, exact, and
to the point when describing the incident. Ask for their assistance if necessary.
• Do not leave the area and do not remove or change any equipment. This will allow
the ORC to determine the correct cause of the incident.
• The ORC will contact the appropriate local officials and first responders if necessary.
The ORC will contact and inform the regional office of the NCDENR. The ORC will
contact any adjacent land owners onto which the spill encroached.
• The ORC, with assistance from operational supervisors, local officials, and the
NCDENR, will determine the appropriate action for containment, primary clean up,
and any necessary remediation.
• It is the responsibility of the ORC to follow up on all accidental spills / discharges. A
standard Spill Report Form must be completed and turned into a Terra Renewal
Environmental Manager.
Sufficient resources, including personnel, vacuum trucks, machinery, hay bales, powdered lime,
and hand tools, should be kept available to assist in cleaning up spills. Everyone participating in
the operation will be provided a list of emergency contacts, including the Primary ORC, the
Backup ORC, local first responders, and the regional office of the NCDENR.
SAFETY:
All Terra Renewal employees and its contractors will be expected to read, understand, and follow
the guidelines set forth in the company's "Environmental, Health, & Safety" manual which is
issued to each employee upon hiring. A copy of this manual will be provided to the supervisor of
any contractors involved in the operation. A copy can be supplied to the DWR upon request.
Page 6 of 6

SECTION 4:
LAND APPLICATION SITE CERTIFICATION
Form: LASC 06-16

LAND APPLICATION SITE CERTIFICATION
Applicant's name: Terra Renewal Services, Inc.
Land application sites currently certified: 1,704.2 net acres and Total to be certified: 1,755.3 net acres.
L LAND APPLICATION SITE INFORMATION (See Instruction B):
Status
Codes
Site/Field ID
Landowners
(�
Lessees or O s
(� perator ��
Net Acres
Count Y
s
Cro P�)
Predominant Soil
Series Nameb
Mapping Unit
or Rep. Slope°
N
NC-WK-MF-16
Mathis Properties, LLC
ASJ Mathis Farms
51.1
Wilkes
Row Crop
Fairview
FcC2
a Status Code for land application sites are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ T (Transferred) ♦ D (Deleted)
b Soil Series Name (i.e. Appling, Cecil, etc.)
° Mapping Unit must be consistent with those used in the County Soil Survey (i.e. for a 2-8% slope Cecil in Anson County the mapping unit is CeB2)
II. WATERBODY AND CLASSIFICATIONS INFORMATION (See Instruction C):
Site/Field ID
Latitude
Longitude
Location
Datum
Location Method Code
Location Accuracy
Waterbody Subbasin and
Stream Index No.
Current and Proposed
p
Class
NC-WK-MF-16
360 09' 49"
800 58' 10"
NAD 83
MAP
Nearest Second
Brier Creek 12-47 & Grays Creek 12-49-(1)
C
Note: Please keep the site information (I.) and waterbody information (11.) of the same field on the same page.
FORM: LASC 06-16 Page 1

ATTACHMENT - F:
FIELD LOCATION & TOPOGRAPHIC MAPS

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* 2.G15 Goagir.-
MF-15,23A,23B c-
ASJ MATHIS FARMS OFFICE
Imagery Date: 5J21j201 36°11'36.74" N 81°00'43.81" elev 101 ft :eye alt 11.82 mi

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TOPOGRAPHIC FIELD MAP
WILKES COUNTY, NC
FIELD: MF-16
PERMITTEE: TERRA RENEWAL SERVICES, INC
QUADRANGLE:
RONDA
Produced: 062223
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1 inch C1000feet

ATTACHMENT - G:
LANDOWNER AGREEMENT FORM

State of North Carolina
DWR
Department of Environmental Quality
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — LAND OWNER AGREEMENT
FORM: LOA 06-16
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise noted the Applicant shall submit one original and two covies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Nan-Dischar a Permitting Chit.
General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of
Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T . 1100. Do not submit
this agreement for review without a corresponding application form (FORM: RLAP 06-16).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Land Owner Agreement (FORM: LOA 06-16):
[Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) Form. Please do
not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to
the application may be made, as long as the attachments are numbered to correspond to the section and item to which they
refer.
Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the
Applicant.
[5"A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator.
AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND
The undersigned landowner or his representative hereby permits:
Applicant's name:
hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land
application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this
Agreement:
Lease Land Use or Special note
SiteJ) field ID es/no Cropping Patterns Intended Use of Crops Residuals �or�rre (no-tilllover-seed/
{y } pp' g {optional}
pasture)
hie- WK -AF-IL ySs �ona Clicp
IiN, it A 4 FGCp 9+E4 r*J
The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the
Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals.
This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and
shall be renewed each time this permit is renewed.
The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and
stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement.
FORM: LOA 06-16 Pagel of 3

I. STIPULATIONS:
L The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted
entity for the site(s) specified by this Agreement.
2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall
be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement.
3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section 11) are met.
4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1636
Mail Service Center, Raleigh, NC 27699-1636.
5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new
landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the
land application site(s).
6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program,
including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of
the equipment used by the Permittee.
7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals
land application event and a copy of the results of each soil analysis.
& If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final
soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for
the specified crop.
9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of
soil samples, and the permitted application limits.
10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of
nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s).
11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for
the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land
application events at appropriate periods.
12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or
his representative prior to and during a residuals land application event.
13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and
inspect any properly, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining
compliance with the permit; establish monitoring facilities on or near the land application sites) as required by the permit; copy any records
that must be kept under the terms and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the
term of, and 12 months after termination of, this Agreement.
II. RESTRICTIONS:
1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land
application sites) during active use and for the 12-month period following a residuals land application event. Such controls may include the
Posting of signs that indicate the activities being conducted at the land application site(s).
2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application
sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land
application events.
3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event.
4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14-
month period following a residuals land application event.
5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20-month period following a residuals land
application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil.
6. Food crops with harvested parts below the surface of the land shall not be harvested for a 3$-month period following a residuals land
application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil.
T Turf grown on land where residuals are applied shalI not be harvested for a 12-month period following a residuals land application event.
III. ALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one)
15A NCAC 02L ,0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105(h) allows the
compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance
boundary provided the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following;
❑ A re -defined compliance boundary is needed for field(s) ID:
(Please include the rationale for the requested re -location of the compliance
compliance boundary to the application package)
2' A re -defined compliance boundary is not needed for this site.
IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed)
boundary and attach a map showing the newly proposed
❑ The land application field(s) ID: is currently permitted under another
residuals land application program; Permit Number WQ: The land owner hereby acknowledge that by signing this
agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred
into the new nrogram-
(Name of the new program)
FORM: LOA 06-16 Page 2 of 3

Landowner's Certification:
I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions
regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through
a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the
deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or
agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement,
understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of
field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified
herein.
Landowner name: IVA rrs r s /rio���e� 5 LL L
Address: . f • ■ r ■ ■ / . r 4 a . ■ .. r .. ■ ■ .
City: " ASJ MATHIS FARMS LWte:
t ❑ P.7 JVIH I F11� V/NFim RD
Phone: R RING RIVER 286Ft_mail dress:
Signature: A
NORTH COUNTY
Zip:
Date: 8 I Zo I -Z
I, the undersigned Notary Public do hereby certify that -
Personally appeared before me this day and acknowledged the due execution of the forgoing instrument. ..,umrst
WITNESS my hand and official seal this the
day of
Signature and seal:
My commission expires:
Lessee's/Operator's Certification:
&Lrr ...
I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein.
Lessee/op i4W 4101Vc.: ■ A S'- MA rk's r ,tn s � �o Luker MAM i S)
Address: ASj MATI-tt-Q•
■ 615 MATHIS FARM RD +
City: : ROARING RIVEate: Zip:
Phone: " ■ * ■ ■ ■ C-mail address:
Signature:
Permittee's Certifi
Date: of zb- I-&
I certify that I have read thisAgreementand do hereby agree to abide by the stipulations and restrictions as specified herein.
Signing official name: rf 1110 Lr. 6'oy,6 MAIIAc r it- - c aura r%n-Euf.. A 1--
Signature: Date: V 1L__/ 11-I
FORM: LOA 06-16 Page 3 of 3

ATTACHMENT - H:
APPLICATION AREA & SETBACK MAP

,BUFFER
/�F- 16
c
E
PE B
MIN 25 FT MIN
... ..es......
. . . . . . . . . . . .
to
ti

ATTACHMENT - I:
SOILS & AGRONOMY REPORT

SOILS and AGRONOMY REPORT
Permit # WQ0038087 — 2023 Modification
Wilkes County
Soil Series & RYE Evaluation:
Only information and data pertaining to sites added in the 2023 modification to the above referenced
permit are provided in this report. The RYE Summary sheet was to include all new / proposed sites. No
changes were made to the soil series or crops on existing sites. RYE / PAN rate data were updated where
necessary for any changes made by the NC State Extension since the last revision.
NRCS soil maps were produced using Web Soil Survey for each field. These maps are provided as part of
this report. The NRCS soil delineations, along with site specific topographic features, were utilized to
determine the appropriate location for soil profile observations. Observations were conducted by a NC
LSS using hand auger borings, which were advanced to a minimum depth of 48 inches or 12 inches below
the depth of the seasonal high water table (shwt). Profile descriptions were recorded for each boring and
are provided as part of this report. The shallowest depth and type of restrictive horizon were recorded
for each boring. The soil profile was classified to the most closely related soil series based on the range of
characteristics. Boring locations are shown on the "Application Area & Setback Maps" provided with the
permit application.
Based on the soil profile observations and the soils mapped by the NRCS, interpretations were made as to
which soil series best represented the predominant series for a given field. The predominant soil series,
as determined by the Soil Scientist evaluation, was used to develop Realistic Yield Expectations (RYE) for
each field based on NCSU data. A summary is provided with this report that provides the field ID, net
acreage, county, predominant soil series and slope, potential crops to be grown, and the realistic yield
and nitrogen uptake of the crop.
Enclosed:
- RYE Summary Table
- NRCS Soil Data
- Soil Profile Descriptions / Evaluation Forms
- Fertility and Heavy Metals (baseline) Soil Sample Results
Soil Scientist:
��, 5��
David Coyle
NC LSS # 1315
Jr' yp C. C��

North Carolina - Realistic Yield Expectation (RYE) Summary
Permit#: WQ0038087
Permittee: Terra Renewal Services, Inc
2023
(Updated for Permit Modification)
Field ID
Net
Acres
County
Predominent Soil Series & Slope
Crop 1
PAN
(lb/ac)
RYE
Crop 2
PAN
(lb/ac)
RYE
CH-1
21.8
Wilkes
DpC2 - Danripple 8-15%
Corn (silage)
179
16.4 tons/ac
Small Grains (silage)
82
7.4 tons/ac
CH-2
19.3
Wilkes
RyB - Ronda 0-5%
Corn (silage)
162
13.7 tons/ac
Small Grains (silage)
78
6.4 tons/ac
CH-3
41.6
Wilkes
BaB - Banister 1-6%
Corn (silage)
285
26.6 tons/ac
Small Grains (silage)
113
10.5 tons/ac
CH-4
35.8
Wilkes
CoA- Codorus 0-2%
Corn (silage)
270
26.0 tons/ac
Small Grains (silage)
95
9.0 tons/ac
DF-1
8.8
Wilkes
DaA- Dan River & Comus 0-4%
Corn (silage)
237
21.8 tons/ac
Small Grains (silage)
103
9.3 tons/ac
DF-2
68.5
Wilkes
DaA- Dan River & Comus 0-4%
Corn (silage)
237
21.8 tons/ac
Small Grains (silage)
103
9.3 tons/ac
DF-3
35.5
Wilkes
DaA- Dan River & Comus 0-4%
Corn (silage)
237
21.8 tons/ac
Small Grains (silage)
103
9.3 tons/ac
DF-4
18.5
Wilkes
DaA- Dan River & Comus 0-4%
Corn (silage)
237
21.8 tons/ac
Small Grains (silage)
103
9.3 tons/ac
DM-3
11.4
Wilkes & Yadkin
FcC2- Fairview 8-15%
Corn (silage)
174
16.0 tons/ac
Small Grains (silage)
80
7.2 tons/ac
DM-5
21.0
Wilkes
CcB2-Clifford 2-6%
Corn (silage)
246
22.5 tons/ac
Small Grains (silage)
120
10.8 tons/ac
DM-6
25.6
Wilkes
CcB2-Clifford 2-6%
Corn (silage)
246
22.5 tons/ac
Small Grains (silage)
120
10.8 tons/ac
DM-7
32.6
Wilkes & Yadkin
CcB2 -Clifford 2-6%
Corn (silage)
246
22.5 tons/ac
Small Grains (silage)
120
10.8 tons/ac
DM-8
26.2
Wilkes & Yadkin
CcC2- Clifford 6-10%
Corn (silage)
231
21.2 tons/ac
Small Grains (silage)
112
10.1 tons/ac
DS-1
53.6
Wilkes
FcB2 - Fairview 2-8%
Corn (silage)
207
19.0 tons/ac
Small Grains (silage)
95
8.6 tons/ac
DS-2
42.1
Wilkes
FcB2 - Fairview 2-8%
Corn (silage)
207
19.0 tons/ac
Small Grains (silage)
95
8.6 tons/ac
DS-3
33.6
Wilkes
FcC2- Fairview 8-15%
Corn (silage)
174
16.0 tons/ac
Small Grains (silage)
80
7.2 tons/ac
DS-4
28.7
Wilkes
FcC2- Fairview 8-15%
Corn (silage)
174
16.0 tons/ac
Small Grains (silage)
80
7.2 tons/ac
DS-5
16.0
Wilkes
FcB2 - Fairview 2-8%
Corn (silage)
207
19.0 tons/ac
Small Grains (silage)
95
8.6 tons/ac
DS-6
16.7
Wilkes
DpC2 - Danripple 8-15%
Corn (silage)
179
16.4 tons/ac
Small Grains (silage)
82
7.4 tons/ac
DS-7
23.8
Wilkes
DpB2 - Danripple 2-8%
Corn (silage)
212
19.5 tons/ac
Small Grains (silage)
98
8.8 tons/ac
DS-8
41.4
Wilkes
PaB - Pfafftown 1-6%
Corn (silage)
219
20.1 tons/ac
Small Grains (silage)
101
9.1 tons/ac
DS-9
41.2
Wilkes
FcC2- Fairview 8-15%
Corn (silage)
174
16.0 tons/ac
Small Grains (silage)
80
7.2 tons/ac
DS-10
6.3
Wilkes
FcB2 - Fairview 2-8%
Corn (silage)
207
19.0 tons/ac
Small Grains (silage)
95
8.6 tons/ac
ED-1
30.0
Wilkes
DpC2 - Danripple 8-15%
Corn (silage)
179
16.4 tons/ac
Small Grains (silage)
82
7.4 tons/ac
ED-2
14.8
Wilkes
DpC2 - Danripple 8-15%
Corn (silage)
179
16.4 tons/ac
Small Grains (silage)
82
7.4 tons/ac
ED-3
12.1
Wilkes
BaB - Banister 1-6%
Corn (silage)
285
26.6 tons/ac
Small Grains (silage)
113
10.5 tons/ac
ED-4
25.1
Wilkes
DpC2 - Danripple 8-15%
Corn (silage)
179
16.4 tons/ac
Small Grains (silage)
82
7.4 tons/ac
HP-1
15.9
Wilkes
FcC2- Fairview 8-15%
Corn (silage)
174
16.0 tons/ac
Small Grains (silage)
80
7.2 tons/ac
HP-3
14.5
Wilkes
FcC2- Fairview 8-15%
Corn (silage)
174
16.0 tons/ac
Small Grains (silage)
80
7.2 tons/ac
MF-6
22.5
Wilkes
FcC2- Fairview 8-15%
Corn (silage)
174
16.0 tons/ac
Small Grains (silage)
80
7.2 tons/ac
MF-8
12.7
Wilkes
FcC2- Fairview 8-15%
Corn (silage)
174
16.0 tons/ac
Small Grains (silage)
80
7.2 tons/ac
MF-9
13.2
Wilkes
FcB2 - Fairview 2-8%
Corn (silage)
207
19.0 tons/ac
Small Grains (silage)
95
8.6 tons/ac
MF-10
19.6
Wilkes
FcB2 - Fairview 2-8%
Corn (silage)
207
19.0 tons/ac
Small Grains (silage)
95
8.6 tons/ac
MF-11
22.5
Wilkes
FcC2- Fairview 8-15%
Corn (silage)
174
16.0 tons/ac
Small Grains (silage)
80
7.2 tons/ac
MF-13
33.8
Wilkes
FcB2 - Fairview 2-8%
Corn (silage)
207
19.0 tons/ac
Small Grains (silage)
95
8.6 tons/ac
MF-14
23.4
Wilkes
FcC2- Fairview 8-15%
Corn (silage)
174
16.0 tons/ac
Small Grains (silage)
80
7.2 tons/ac
MF-15
13.8
Wilkes
FcC2- Fairview 8-15%
Corn (silage)
174
16.0 tons/ac
Small Grains (silage)
80
7.2 tons/ac
MF-16
51.1
Wilkes
FcC2- Fairview 8-15%
Corn (silage)
174
16.0 tons/ac
Small Grains (silage)
80
7.2 tons/ac
MF-17
39.5
Wilkes
FcC2- Fairview 8-15%
Corn (silage)
174
16.0 tons/ac
Small Grains (silage)
80
7.2 tons/ac
MF-23
59.2
Wilkes
FcB2 - Fairview 2-8%
Corn (silage)
207
19.0 tons/ac
Small Grains (silage)
95
8.6 tons/ac
MRF-3
18.9
Wilkes
DpC2 - Danripple 8-15%
Corn (silage)
179
16.4 tons/ac
Small Grains (silage)
82
7.4 tons/ac
MRF-5
25.3
Wilkes
DpB2 - Danripple 2-8%
Corn (silage)
212
19.5 tons/ac
Small Grains (silage)
98
8.8 tons/ac
MRF-6
21.0
Wilkes
DpB2 - Danripple 2-8%
Corn (silage)
212
19.5 tons/ac
Small Grains (silage)
98
8.8 tons/ac
MRF-12
26.5
Wilkes
PaB - Pfafftown 1-6%
Corn (silage)
219
20.1 tons/ac
Small Grains (silage)
101
9.1 tons/ac
MRF-13
41.0
Wilkes
RyB - Ronda 0-5%
Corn (silage)
162
21.8 tons/ac
Small Grains (silage)
98
9.3 tons/ac
MRF-14
18.5
Wilkes
DpC2 - Danripple 8-15%
Corn (silage)
179
16.4 tons/ac
Small Grains (silage)
82
7.4 tons/ac
MRF-15
34.9
Wilkes
RyB - Ronda 0-5%
Corn (silage)
162
21.8 tons/ac
Small Grains (silage)
98
9.3 tons/ac
MRF-20
52.3
Wilkes
DaA- Dan River & Comus 0-4%
Corn (silage)
237
21.8 tons/ac
Small Grains (silage)
103
9.3 tons/ac
MRF-21
27.8
Wilkes
DaA- Dan River & Comus 0-4%
Corn (silage)
237
21.8 tons/ac
Small Grains (silage)
103
9.3 tons/ac
MRF-22
31.4
Wilkes
RyB - Ronda 0-5%
Corn (silage)
162
13.7 tons/ac
Small Grains (silage)
78
6.4 tons/ac
RJ-1
20.6
Wilkes
DaA- Dan River & Comus 0-4%
Corn (silage)
237
21.8 tons/ac
Small Grains (silage)
103
9.3 tons/ac
RJ-2
57.8
Wilkes
DaA- Dan River & Comus 0-4%
Corn (silage)
237
21.8 tons/ac
Small Grains (silage)
103
9.3 tons/ac
RJ-5
45.1
Wilkes
DaA- Dan River & Comus 0-4%
Corn (silage)
237
21.8 tons/ac
Small Grains (silage)
103
9.3 tons/ac
RJ-7
24.6
Wilkes
FcB2 - Fairview 2-8%
Corn (silage)
207
19.0 tons/ac
Small Grains (silage)
95
8.6 tons/ac
SP-1
12.7
Wilkes
FcC2- Fairview 8-15%
Corn (silage)
174
16.0 tons/ac
Small Grains (silage)
80
7.2 tons/ac
SP-2
26.8
Wilkes
FcC2- Fairview 8-15%
Corn (silage)
174
16.0 tons/ac
Small Grains (silage)
80
7.2 tons/ac
TA-1
32.3
Yadkin
CcB2-Clifford 2-6%
Corn (silage)
246
22.5 tons/ac
Small Grains (silage)
120
10.8 tons/ac
WB-1
23.2
Wilkes
RyB - Ronda 0-5%
Corn (silage)
162
13.7 tons/ac
Small Grains (silage)
78
6.4 tons/ac
YF-1
13.5
Yadkin
NaB - Nathalie 2-6%
Corn (silage)
203
18.6 tons/ac
Small Grains (silage)
98
8.8 tons/ac
YF-3
22.3
Yadkin
CcB2-Clifford 2-6%
Corn (silage)
246
22.5 tons/ac
Small Grains (silage)
120
10.8 tons/ac
YF-4
23.3
Yadkin
CeB3 -Clifford 2-6%
Corn (silage)
246
22.5 tons/ac
Small Grains (silage)
120
10.8 tons/ac
YF-5
51.5
Wilkes & Yadkin
FcC2- Fairview 8-15%
Corn (silage)
174
16.0 tons/ac
Small Grains (silage)
80
7.2 tons/ac
YF-7
10.3
Wilkes
FcB2 - Fairview 2-89/
Corn (silage)
207
19.0 tons/ac
Small Grains (silage)
95
8.6 tons/ac
NOTES: 1755.3
RYE are based on predominant soil series forfield and data provided by NCSU at https://realisticyields.ces.ncsu.edu (adjusted rates November 2021)

501800
36o 10' 18" N
g
r
g
b5
36o 9' 41" N
501800 501900 502000 502100 502200 502300
Map Scale: 1:5,510 if printed on A portrait (8.5" x 11") sheet.
$ N 0 50 100 200 300 Meters
Feet
0 250 500 1000 1y00
Map projection: Web Mercator Conermordinates: WGS84 Edge tics: lfrM Zone 17N WGS84
usoA Natural Resources Web Soil Survey
Conservation Service National Cooperative Soil Survey
Soil Map —Wilkes County, North Carolina
(NC: Mathis_MF-16)
501900 502000 502100 502200 502300 502400
5024W 502500
5026M
36o 10' 18" N
g
r
g
b5
36o 9' 41" N
502600
7/13/2023
Page 1 of 3

MAP LEGEND
Area of Interest (AOI)
0
Area of Interest (AOI)
Soils
0
Soil Map Unit Polygons
,N
Soil Map Unit Lines
Soil Map Unit Points
Special
Point Features
Blowout
Borrow Pit
Clay Spot
Closed Depression
Gravel Pit
�i
Gravelly Spot
0
Landfill
A.
Lava Flow
Marsh or swamp
Mine or Quarry
Miscellaneous Water
Perennial Water
Rock Outcrop
Saline Spot
Sandy Spot
Severely Eroded Spot
Sinkhole
Slide or Slip
Sodic Spot
Soil Map —Wilkes County, North Carolina
(NC: Mathis_MF-16)
Spoil Area
Stony Spot
Very Stony Spot
Wet Spot
4� Other
M� Special Line Features
Water Features
Streams and Canals
Transportation
Rails
. 0 Interstate Highways
US Routes
Major Roads
Local Roads
Background
Aerial Photography
MAP INFORMATION
The soil surveys that comprise your AOI were mapped at
1:24,000.
Warning: Soil Map may not be valid at this scale.
Enlargement of maps beyond the scale of mapping can cause
misunderstanding of the detail of mapping and accuracy of soil
line placement. The maps do not show the small areas of
contrasting soils that could have been shown at a more detailed
scale.
Please rely on the bar scale on each map sheet for map
measurements.
Source of Map: Natural Resources Conservation Service
Web Soil Survey URL:
Coordinate System: Web Mercator (EPSG:3857)
Maps from the Web Soil Survey are based on the Web Mercator
projection, which preserves direction and shape but distorts
distance and area. A projection that preserves area, such as the
Albers equal-area conic projection, should be used if more
accurate calculations of distance or area are required.
This product is generated from the USDA-NRCS certified data as
of the version date(s) listed below.
Soil Survey Area: Wilkes County, North Carolina
Survey Area Data: Version 27, Sep 12, 2022
Soil map units are labeled (as space allows) for map scales
1:50,000 or larger.
Date(s) aerial images were photographed: May 18, 2019—May
21, 2019
The orthophoto or other base map on which the soil lines were
compiled and digitized probably differs from the background
imagery displayed on these maps. As a result, some minor
shifting of map unit boundaries may be evident.
usoA Natural Resources Web Soil Survey 7/13/2023
Conservation Service National Cooperative Soil Survey Page 2 of 3

Soil Map —Wilkes County, North Carolina
NC: Mathis_MF-16
Map Unit Legend
Map Unit Symbol
Map Unit Name
Acres in AOI
Percent of AOI
FaD
Fairview sandy loam, 15 to 25
2.1
2.9%
percent slopes
FcB2
Fairview sandy clay loam, 2 to
17.9
25.6%
8 percent slopes, moderately
eroded
FcC2
Fairview sandy clay loam, 8 to
50.0
71.5%
15 percent slopes,
moderately eroded
Totals for Area of Interest
69.9
100.0%
USDA Natural Resources Web Soil Survey 7/13/2023
Conservation Service National Cooperative Soil Survey Page 3 of 3

Map Unit Description ---Wilkes County, North Carolina
NC: Mathis_MF-16
Map Unit Description
The map units delineated on the detailed soil maps in a soil survey represent the
soils or miscellaneous areas in the survey area. The map unit descriptions in this
report, along with the maps, can be used to determine the composition and
properties of a unit.
A map unit delineation on a soil map represents an area dominated by one or
more major kinds of soil or miscellaneous areas. A map unit is identified and
named according to the taxonomic classification of the dominant soils. Within a
taxonomic class there are precisely defined limits for the properties of the soils.
On the landscape, however, the soils are natural phenomena, and they have the
characteristic variability of all natural phenomena. Thus, the range of some
observed properties may extend beyond the limits defined for a taxonomic class.
Areas of soils of a single taxonomic class rarely, if ever, can be mapped without
including areas of other taxonomic classes. Consequently, every map unit is
made up of the soils or miscellaneous areas for which it is named, soils that are
similar to the named components, and some minor components that differ in use
and management from the major soils.
Most of the soils similar to the major components have properties similar to those
of the dominant soil or soils in the map unit, and thus they do not affect use and
management. These are called noncontrasting, or similar, components. They
may or may not be mentioned in a particular map unit description. Some minor
components, however, have properties and behavior characteristics divergent
enough to affect use or to require different management. These are called
contrasting, or dissimilar, components. They generally are in small areas and
could not be mapped separately because of the scale used. Some small areas of
strongly contrasting soils or miscellaneous areas are identified by a special
symbol on the maps. If included in the database for a given area, the contrasting
minor components are identified in the map unit descriptions along with some
characteristics of each. A few areas of minor components may not have been
observed, and consequently they are not mentioned in the descriptions,
especially where the pattern was so complex that it was impractical to make
enough observations to identify all the soils and miscellaneous areas on the
landscape.
The presence of minor components in a map unit in no way diminishes the
usefulness or accuracy of the data. The objective of mapping is not to delineate
pure taxonomic classes but rather to separate the landscape into landforms or
landform segments that have similar use and management requirements. The
delineation of such segments on the map provides sufficient information for the
development of resource plans. If intensive use of small areas is planned,
however, onsite investigation is needed to define and locate the soils and
miscellaneous areas.
An identifying symbol precedes the map unit name in the map unit descriptions.
Each description includes general facts about the unit and gives important soil
properties and qualities.
USDA Natural Resources Web Soil Survey 7/13/2023
Conservation Service National Cooperative Soil Survey Page 1 of 6

Map Unit Description ---Wilkes County, North Carolina
NC: Mathis_MF-16
Soils that have profiles that are almost alike make up a soil series. All the soils of
a series have major horizons that are similar in composition, thickness, and
arrangement. Soils of a given series can differ in texture of the surface layer,
slope, stoniness, salinity, degree of erosion, and other characteristics that affect
their use. On the basis of such differences, a soil series is divided into soil
phases. Most of the areas shown on the detailed soil maps are phases of soil
series. The name of a soil phase commonly indicates a feature that affects use or
management. For example, Alpha silt loam, 0 to 2 percent slopes, is a phase of
the Alpha series.
Some map units are made up of two or more major soils or miscellaneous areas.
These map units are complexes, associations, or undifferentiated groups.
A complex consists of two or more soils or miscellaneous areas in such an
intricate pattern or in such small areas that they cannot be shown separately on
the maps. The pattern and proportion of the soils or miscellaneous areas are
somewhat similar in all areas. Alpha -Beta complex, 0 to 6 percent slopes, is an
example.
An association is made up of two or more geographically associated soils or
miscellaneous areas that are shown as one unit on the maps. Because of
present or anticipated uses of the map units in the survey area, it was not
considered practical or necessary to map the soils or miscellaneous areas
separately. The pattern and relative proportion of the soils or miscellaneous
areas are somewhat similar. Alpha -Beta association, 0 to 2 percent slopes, is an
example.
An undifferentiated group is made up of two or more soils or miscellaneous areas
that could be mapped individually but are mapped as one unit because similar
interpretations can be made for use and management. The pattern and
proportion of the soils or miscellaneous areas in a mapped area are not uniform.
An area can be made up of only one of the major soils or miscellaneous areas, or
it can be made up of all of them. Alpha and Beta soils, 0 to 2 percent slopes, is
an example.
Some surveys include miscellaneous areas. Such areas have little or no soil
material and support little or no vegetation. Rock outcrop is an example.
Additional information about the map units described in this report is available in
other soil reports, which give properties of the soils and the limitations,
capabilities, and potentials for many uses. Also, the narratives that accompany
the soil reports define some of the properties included in the map unit
descriptions.
Report —Map Unit Description
Wilkes County, North Carolina
FaD—Fairview sandy loam, 15 to 25 percent slopes
Map Unit Setting
National map unit symbol: 2tgdc
Elevation: 330 to 1,640 feet
USDA Natural Resources Web Soil Survey 7/13/2023
Conservation Service National Cooperative Soil Survey Page 2 of 6

Map Unit Description ---Wilkes County, North Carolina
NC: Mathis_MF-16
Mean annual precipitation: 43 to 51 inches
Mean annual air temperature: 55 to 59 degrees F
Frost -free period: 190 to 230 days
Farmland classification: Not prime farmland
Map Unit Composition
Fairview and similar soils: 87 percent
Estimates are based on observations, descriptions, and transects of
the mapunit.
Description of Fairview
Setting
Landform: Interfluves, ridges
Landform position (two-dimensional): Backslope
Landform position (three-dimensional): Interfluve
Down -slope shape: Convex
Across -slope shape: Convex
Parent material: Saprolite residuum weathered from granite and
gneiss and/or saprolite residuum weathered from schist
Typical profile
Ap - 0 to 1 inches: sandy loam
E - 1 to 6 inches: sandy loam
Btl - 6 to 20 inches: clay
Bt2 - 20 to 23 inches: sandy clay loam
BCt - 23 to 38 inches: sandy loam
C - 38 to 62 inches: sandy loam
Properties and qualities
Slope: 15 to 25 percent
Depth to restrictive feature: More than 80 inches
Drainage class: Well drained
Capacity of the most limiting layer to transmit water
(Ksat): Moderately high to high (0.57 to 1.98 in/hr)
Depth to water table: More than 80 inches
Frequency of flooding: None
Frequency of ponding: None
Available water supply, 0 to 60 inches: Moderate (about 7.8
inches)
Interpretive groups
Land capability classification (irrigated): None specified
Land capability classification (nonirrigated): 4e
Hydrologic Soil Group: B
Ecological site: F136XY320VA - Northern inner piedmont acidic
upland forest, moist
Hydric soil rating: No
USDA Natural Resources Web Soil Survey 7/13/2023
Conservation Service National Cooperative Soil Survey Page 3 of 6

Map Unit Description ---Wilkes County, North Carolina
NC: Mathis_MF-16
FcB2—Fairview sandy clay loam, 2 to 8 percent slopes,
moderately eroded
Map Unit Setting
National map unit symbol: 2tgd6
Elevation: 660 to 1,640 feet
Mean annual precipitation: 43 to 51 inches
Mean annual air temperature: 55 to 59 degrees F
Frost -free period: 190 to 230 days
Farmland classification: All areas are prime farmland
Map Unit Composition
Fairview, moderately eroded, and similar soils: 88 percent
Estimates are based on observations, descriptions, and transects of
the mapunit.
Description of Fairview, Moderately Eroded
Setting
Landform: Ridges, interfluves
Landform position (two-dimensional): Summit, shoulder
Landform position (three-dimensional): Interfluve
Down -slope shape: Convex
Across -slope shape: Convex
Parent material: Saprolite residuum weathered from granite and
gneiss and/or saprolite residuum weathered from schist
Typical profile
Apt - 0 to 4 inches: sandy clay loam
Ap2 - 4 to 9 inches: sandy clay loam
Bt - 9 to 24 inches: clay
BC - 24 to 29 inches: clay loam
C - 29 to 79 inches: loam
Properties and qualities
Slope: 2 to 8 percent
Depth to restrictive feature: More than 80 inches
Drainage class: Well drained
Capacity of the most limiting layer to transmit water
(Ksat): Moderately high to high (0.57 to 1.98 in/hr)
Depth to water table: More than 80 inches
Frequency of flooding: None
Frequency of ponding: None
Available water supply, 0 to 60 inches: Moderate (about 7.5
inches)
Interpretive groups
Land capability classification (irrigated): None specified
Land capability classification (nonirrigated): 2e
Hydrologic Soil Group: B
Ecological site: F136XY320VA - Northern inner piedmont acidic
upland forest, moist
USDA Natural Resources Web Soil Survey 7/13/2023
Conservation Service National Cooperative Soil Survey Page 4 of 6

Map Unit Description ---Wilkes County, North Carolina
NC: Mathis_MF-16
Hydric soil rating: No
FcC2—Fairview sandy clay loam, 8 to 15 percent slopes,
moderately eroded
Map Unit Setting
National map unit symbol: 2tgd7
Elevation: 660 to 1,640 feet
Mean annual precipitation: 43 to 51 inches
Mean annual air temperature: 55 to 59 degrees F
Frost -free period: 190 to 230 days
Farmland classification: Farmland of statewide importance
Map Unit Composition
Fairview, moderately eroded, and similar soils: 88 percent
Estimates are based on observations, descriptions, and transects of
the mapunit.
Description of Fairview, Moderately Eroded
Setting
Landform: Interfluves, ridges
Landform position (two-dimensional): Summit, shoulder
Landform position (three-dimensional): Interfluve
Down -slope shape: Convex
Across -slope shape: Convex
Parent material: Saprolite residuum weathered from granite and
gneiss and/or saprolite residuum weathered from schist
Typical profile
Apt - 0 to 4 inches: sandy clay loam
Ap2 - 4 to 9 inches: sandy clay loam
Bt - 9 to 24 inches: clay
BC - 24 to 29 inches: clay loam
C - 29 to 79 inches: loam
Properties and qualities
Slope: 8 to 15 percent
Depth to restrictive feature: More than 80 inches
Drainage class: Well drained
Runoff class: Low
Capacity of the most limiting layer to transmit water
(Ksat): Moderately high to high (0.57 to 1.98 in/hr)
Depth to water table: More than 80 inches
Frequency of flooding: None
Frequency of ponding: None
Available water supply, 0 to 60 inches: Moderate (about 7.5
inches)
Interpretive groups
Land capability classification (irrigated): None specified
Land capability classification (nonirrigated): 3e
Hydrologic Soil Group: C
USDA Natural Resources Web Soil Survey 7/13/2023
Conservation Service National Cooperative Soil Survey Page 5 of 6

Map Unit Description ---Wilkes County, North Carolina
NC: Mathis_MF-16
Ecological site: F136XY320VA - Northern inner piedmont acidic
upland forest, moist
Hydric soil rating: No
Data Source Information
Soil Survey Area: Wilkes County, North Carolina
Survey Area Data: Version 27, Sep 12, 2022
USDA Natural Resources Web Soil Survey 7/13/2023
Conservation Service National Cooperative Soil Survey Page 6 of 6

SOIL EVALUATION FORM
County: Wilkes
Permittee: Terra Renewal Services
Farmer: ASJ Mathis Farms
Field #: MF-16
Boring #: MF-16A
Date: 10/10/22
Evaluator: David Coyle
Land Use: Row Crop
L.P: Shoulder / Upper Backslope
Slope: 8-10%
Slope Shape: Convex
Horizon
Depth
Texture
Color
Structure
Cons.
Mottles
Ap
0-8
SCL
7.5YR 4/3
wk fn sbk
v. fr
Bt1
8-16
C
2.5 YR 4/8
mod med sbk
firm
Bt2
16-32
CL
2.5 YR 4/8
mod med sbk
fr
BC
32-42
L
2.5 YR 4/8
wk med sbk
v. fr
CB
42-48
SL
5YR 5/8
wk co sbk
v. fr
few brown and yellow mineral
C
48-52+
SL
5YR 5/8
massive
loose
common brown and yellow mineral
Additional Comments:
Depth to Seasonal Water Table:
> 52"
Type of W.T. (apparent 1 perched):
N/A
Depth To Free Water Table:
> 52"
Depth to Restrictive Horizon:
> 52"
Type of Restrictive Horizon:
N/A
Drainage Class: Well Drained
Taxonomy: Fine, kaolinitic, mesic Typic Kanhapludult
Most Closely Related Soil Series: Fairview
Variant Definition: N/A
Note: Depth to Seasonal High Water Table is defined by first indication of seasonal saturation (first 2 chroma mottles). Horizons
with < 2% (few) 2 chroma depletions were not included in determination of drainage class for soil profile.
LSS: David C. Coyle; #1315
Signature:
�P ,y;._
+��� 6N�

SOIL EVALUATION FORM
County: Wilkes
Permittee: Terra Renewal Services
Farmer: ASJ Mathis Farms
Field #: MF-16
Boring #: MF-16B
Date: 10/10/22
Evaluator: David Coyle
Land Use: Row Crop
L.P: Mid Backslope
Slope: 8-10%
Slope Shape: Linear
Horizon
Depth
Texture
Color
Structure
Cons.
Mottles
Ap
0-6
SL
7.5YR 4/3
wk fn sbk
v. fr
Bt1
6-18
C
2.5 YR 4/8
mod med sbk
fr
Bt2
18-25
CL
2.5 YR 4/8
mod med sbk
fr
BC/C
25-40
SCL
2.5 YR 5/8
wk med sbk
v. fr
few brown and yellow mineral
C
40-50+
SL
5YR 5/8
massive
loose
common brown and yellow mineral
Additional Comments:
Depth to Seasonal Water Table:
> 50"
Type of W.T. (apparent 1 perched):
N/A
Depth To Free Water Table:
> 50"
Depth to Restrictive Horizon:
> 50"
Type of Restrictive Horizon:
N/A
Drainage Class: Well Drained
Taxonomy: Fine, kaolinitic, mesic Typic Kanhapludult
Most Closely Related Soil Series: Fairview
Variant Definition: N/A
Note: Depth to Seasonal High Water Table is defined by first indication of seasonal saturation (first 2 chroma mottles). Horizons
with < 2% (few) 2 chroma depletions were not included in determination of drainage class for soil profile.
LSS: David C. Coyle; #1315
Signature:
�P ,y;._
+��� 6N�

SOIL EVALUATION FORM
County: Wilkes
Permittee: Terra Renewal Services
Farmer: ASJ Mathis Farms
Field #: MF-16
Boring #: MF-16C
Date: 10/10/22
Evaluator: David Coyle
Land Use:
Row Crop
L.P:
Toe of Broad Swale
Slope:
10-12%
Slope Shape:
Concave
Horizon
Depth
Texture
Color
Structure
Cons.
Mottles
Ap
0-6
SL
7.5YR 3/3
wk fn sbk
v. fr
E
6-16
SL
10YR 6/4
wk fn sbk
loose
Bt1
16-24
C
7.5YR 5/6
mod med sbk
firm
Bt2
24-32
CL
7.5YR 5/6
mod med sbk
fr
few med 10YR 6/4d
Bt3
32-40
CL
5YR 5/8
mod med sbk
fr
com med 10YR 6/4d; 2.5YR 4/6c
Bt4
40-52
CL
5YR 5/8
mod med sbk
fr
com med 10YR 7/3d; 2.5YR 4/6c
Additional Comments:
Depth to Seasonal Water Table:
> 52"
Type of W.T. (apparent 1 perched):
N/A
Depth To Free Water Table:
> 52"
Depth to Restrictive Horizon:
> 52"
Type of Restrictive Horizon:
N/A
Drainage Class: Well Drained
Taxonomy: Fine, mixed, semiactivemesic Typic Hapludult
Most Closely Related Soil Series: Danripple
Variant Definition: N/A
Note: Depth to Seasonal High Water Table is defined by first indication of seasonal saturation (first 2 chroma mottles). Horizons
with < 2% (few) 2 chroma depletions were not included in determination of drainage class for soil profile.
LSS: David C. Coyle; #1315
Signature:
�P ,y;._
+��� 6N�

Page 1 of 1
•
Report No: 23-006-0693 7621 Whitepine Road, Richmond, VA 23237
Account No: 08494 Waypol t - Main 8114-743-9401 °Fax $04-271-6446
ANALYTICAL www.waypointanalytical.com
Advisor: Terra Renewal Services Client: SC-1 Farm: SC-1
P O Box 399 ASJ Mathis Farms -Permit: WQ0038087
Dardanelle AR 72834
Date Received:01/06/2023
Date of Report: 01/09/2023
Lab No Field ID Sample ID Soil Class
HM% W/V pH Ac
P-1 K-1 S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I CEC BS % Ca % Mg % ESP Na
102607 MF-16 MF-16 MIN
2.0 5.4 1.6
65 56 112 63 0 0 153 153 170 5.6 72 40 26 1.3 0.1 I
I82698 NqRF 46A NqRF 46A
23
9 9 I
I92699 NqRF 46B NqRF 46B
276
9 8 I
I92646 Pvq R F 1 FA Pvq R F 1 FA
+-,
9 8 I
I9264 {bM1+F}
4-8
9 8 I
Comment
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

Waypointo
ANALYTICAL
1 /13/2023
Terra Renewal Services
P O Box 399
Dardanelle, AR, 72834
Ref: Analytical Testing
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Report Number: 23-009-0001
Project Description: ASJ Mathis Farms -Permit: WQ0038087/SC-1
Waypoint Analytical Virginia, Inc. received sample(s) on 1/9/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
&'. " -_ �' --k L, (' c --- �'
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 11

OA�
Waypoint'
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
Sample Summary Table
Report Number:
23-009-0001
Client Project Description:
ASJ Mathis Farms -Permit: WQ0038O87/SC-1
Lab No
Client Sample ID
Matrix Date Collected
Date Received
Method
Lab ID
60337
MF-16
Solids
01/09/2023
6010D
WP MTN
60337
MF-16
Solids
01/09/2023
SW-7471B
WP MTN
60338
MRF-16A
Solids
01/09/2023
SW-7471B
WP MTN
60338
MRF-16A
Solids
01/09/2023
6010D
WP MTN
60339
MRF-16B
Solids
01/09/2023
SW-7471B
WP MTN
60339
MRF-16B
Solids
01/09/2023
6010D
WP MTN
60340
MRF-17A
Solids
01/09/2023
6010D
WP MTN
60340
MRF-17A
Solids
01/09/2023
SW-7471B
WP MTN
60341
MRF-17B
Solids
01/09/2023
SW-7471B
WP MTN
60341
MRF-17B
Solids
01/09/2023
6010D
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 11

•
7621 0 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 O Fax [phone]
ANALYTICAL www.waypointanalytical.com
08494
Terra Renewal Services Project ASJ Mathis Farms -Permit:
P 0 Box 399 WQ0038087/SC-1 Report Date : 01/13/2023
Information : Received : 01/09/2023
Dardanelle , AR 72834
Brandi Watson
Report Number : 23-009-0001 REPORT OFANALYSIS
Lab No : 60337 Matrix: Solids
Sample ID : MF-16 Sampled:
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Chromium
52.1
mg/Kg
0.250
1
01/11/23 23:41
TJS
6010D
Lead
17.8
mg/Kg
0.300
1
01/11/23 23:41
TJS
6010D
Arsenic
3.47
mg/Kg
0.500
1
01/11/23 23:41
TJS
6010D
Selenium
<0.500
mg/Kg
0.500
1
01/11/23 23:41
TJS
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Molybdenum 0.439 mg/Kg 0.250 1 01/11/23 23:41 TJS 6010D
Copper
17.3
mg/Kg
0.500
1
01/11/23 23:41
TJS
6010D
Zinc
30.5
mg/Kg
1.25
1
01/11/23 23:41
TJS
6010D
Cadmium
0.215
mg/Kg
0.100
1
01/11/23 23:41
TJS
6010D
Nickel
13.7
mg/Kg
0.250
1
01/11/23 23:41
TJS
6010D
Mercury
<0.147
mg/Kg
0.147
1
01/12/2313:34
JTR
SW-7471B
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 11

Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Client: Terra Renewal Services CASE NARRATIVE
Project: ASJ Mathis Farms -Permit: WQ0038087/SC-1
Lab Report Number: 23-009-0001
Date: 1 /13/2023
Metals Analysis Method 601 OD
Sample 60340 (MRF-17A)
QC Batch No: L658190/L657757
One or more Internal Standards are outside method acceptance criteria. Re -analysis and/or sample dilutions are
required.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 52200 (#2)
Analyte: Mercury
QC Batch No: L658234/L657995
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected
Page 8 of 11

(D
WayPAoint.
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 08494
Customer Name: Terra Renewal Services
Report Number: 23-009-0001
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F-71
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
0 Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
0 Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: David Lennon Date & Time: 01/09/2023 07:34:47
Page 9 of 11

Waypoint
ANALYTICAL
O
L
SOIL SAMPLE INFORMATION SHEET
7621 Whitepine Road
Richmond, VA 23237
[phone] - Fax [phone]
www.wayp-Qjntanalytica.l.com
CUSTOMER INFORMATION GROWER INFORMATION
1�i2.�►l r�cwa�
Asp 0AT1110 fikajr %
Pa a-* -399
crni{ : W g-0,017aT]-7
A R
Sand Report to a -mail address
a ;d , ca tI t? 4-rrra r.Ln Co
Account #
08 y R y
Grower la SC__ I
Farm Ia 5 C - I
Field ID
S•nC „s S L -
x
x
Please check sam III In column providod If Herbicide or Nematode anal sis re q uested. If 1"Icide, Please indicate name of Herbicide In Add't Info box below.
a
�
Lab Number
Sample Ill
$2M - 5 cityAd11" Teats
$au bla
Addluanal
bdan dad
Intended
Altemate
Al Somata
Prw laps
i7
ii
m
S Cu Fe Mn Ns 5 Zn
lab Use Onl
i6 chars. mar
51M
53M
Salts
Texture
Np3�1
Tests
Crop Code
Grp Yield
Cro Code
Crop Yield
Cropm
+
tjff- 16h
Rr-IG6A,TA-6-
46'G/
ftf-11A
T_
-
-
_4
TIL
i I t a f
Si M - Organic Matter, Phosphorous, Potassium, Calcium, Magnesium, pH, Buffer pH
S2M - S 1 M plus any two of the following: Sodium, Sulfate -Sulfur. Boron, Zinc, Manganese, iron, Copper. Each additional
test (above two) cost $2.00.
S3M - S1M PILLs all of the follow n : Sodium. Sulfala-Sulfur- Boron, Zinc, Manganese, Iran, CapparL
ARE REQUESTED
CROP CODES TO BE USED IF FERTILIZER RECOMMENDATIONS
If the cro for wtlichyou would like recommendations is not listed, write the cropname
in the crop code bo G �_
FIELD CROPS
FORAGE CROPS
1. Barley
101. Alfalfa Hay 161. Coastal Bermuda Hay
5. Canole
103. AlfaifalCoal Season Grass Hay 162. Coastal Bermuda Pasture
TURFGRASS m
10. Com
106. Alfalfa/Warm Season Grass Hay 172. Cool Season Grass Pasture
512. Bahiagrass Lawn °=
11. ComlSoybeans Rotation
116, Bahiagrass Hay 173. Cool Season Grass Hey
613. Bahiagrass Sod Produl 3 m
12. Com - No Tid
117. Bahiagrass Pasture 181. Fescue Hay
517- Bentgrass Green 2 =
13. Cam Silage
121. Common Bermuda May 182, Fescue Pasture
521. Bermudagrass Athledc 9
20. Cotton
122. Common Bermuda Pasture 183, FescuelLegume }lay
522. Bermudagrass Fairway
21, Cotton - No Till
123. Common BermudalLegume Hay 184. FescuelLegume Pasture
523. Bermudagrass Green
25. Grain Sorghum
124_ Common BermudalLe ume Pasture 237, R e rass
524. Bermudagrass Lawn
30, Oats
INDICATE TYPE OF GRASS ANDIOR LEGUME
525. Bermudagrass Sod Pr[
32- Peanuts
626. Bermudegrass Tee a
34, Popoom
297. OTHER HAY
533. Bluegrass Lavin ° r
35. Rapeseed
» .. m .. ....... --
534. Bluegrass Sod Product n
36. Rice
298.
39- Rye
.... ............ ....._...-..,..............__........._._........_..............._...............-...........-.._.._............................_....
547. Centipede Sod Product !■
45, Soybeans
299. CRP
561. Fescue Athletic Field g
VEGETABLE CROPS
FRUIT & NUT CROPS
46, Soybeans - No Till
563. Fescue Lawn Q oa N
51. Sugarcane - Plant
307. Beans - Lima 381. Spinach
400, Apples
564. Fescue Sod Production W on
52, Sugarcane - Stubble
309. Beans - Snap 382. Squash
410. Blueberries
576. St. Augustine Lawn
62. Tobacco - Burley
320. Cabbage 383. Sweet Cam
420. Citrus
577. St. Augustine Sod Prod o
63. Tobacco - Dark
322. Cantaloupe 384. Sweet Potatoitonj
430. Grapes
583. Zoysiagrass Lawn _
84. Tobacco - Flue Cured
33D. Cucumbers 391. Sweet Potato(bu)
470. Peaches
584. Zoysiagrass Sod Produ
75. Wheat
340, Garden 385. Tomatoes
475, Pecans
78. Wheat SiiagelCom Silage
369. Peppers 398. Watermelons
490. Strawberries
92. Wheat/Beans Double Crop
Additional Tests or Other Information
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Submittal of information sheet to Waypoint Anaiytical, Inc. is acceptance of our terms and conditions. All prices are subjeol to change without notice.
Additional fees may be charged to client if sample requires additional preparation procedures.
Page 10 of 11

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NC — Soil Sample Permitting Parameters:
Fertility:
Metals:
Acidity
Base Saturation
Calcium
Cation Exchange Capacity
Copper
Exchangeable Sodium Percentage
Magnesium
Manganese
Percentage Humic Matter
pH
Phosphorus
Potassium
Sodium
Zinc
Arsenic
Cadmium
Copper
Chromium
Lead
Mercury
Molybdenum
Nickel
Selenium
Zinc
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Page 11 of 11