July 2023_Mod Major CAMA TJ Land Development

July 10, 2023

Mr. Curt Weychert, Assistant Major Permit Coordinator
North Carolina Division of Coastal Management
400 Commerce Avenue
Morehead City, NC 28557

Dear Mr. Weychert:

The purpose of this letter is to request that the Major CAMA/Dredge and Fill application for TJ
Land Development LLC be taken off hold and the enclosed modified project design be recirculated
to the applicable Department of Environmental Quality agencies. This application package
incorporates design changes because of the May 22, 2023, comment letter from the NC Division
of Marine Fisheries Habitat Specialist Mr. Jimmy Harrison and the May 30, 2023, comment letter
from the NC Wildlife Resource Commission Coastal Habitat Coordinator, Ms. Maria Dunn. Both
agencies had concerns over the excavation in Battalina Creek referring to the proposed excavation
as “new excavation in a PNA”. The concerns presented by the NCDMF May 22, 2023, letter was
unexpected because NCDMF did not object nor raise any concerns over adverse impacts to fishery
habitats in the original proposal that proposed twice the square footage of excavation in Battalina
Creek. Nevertheless, this modified project proposal removes all excavation within and adjacent
to Battalina Creek, all proposed docks and bulkhead construction. The proposed location of the
marine pumpout and fueling slip has moved to Baker Creek in the vicinity of slips 11 and 12. The
fuel storage tank location is now adjacent to the proposed parking lot outside the buffer. At the
request of the Division of Water Resources (DWR) enclosed with this modified application
package are the results of the spoil sediment sampling analysis from Boat Harbor Canal and Baker
Creek as well as an explanation of the hydrological conditions in the wetland situated between
Tract A and Tract C as it relates to potential impacts from construction of a retaining wall. Per
DWR the plan view plat shows a slip numbering system. Also, enclosed with this narrative cover
letter is revised Major CAMA Dredge and Fill DCM application forms, MP-1, MP-2, MP-3, and
MP-4 and a revised plan view plat. The adjacent riparian property owners have been renotified
and the letters and certified mail receipts are a part of the resubmittal. The applicant has submitted
separately to the DWR a response to DWR’s “More Information Request” dated May 23, 2023
and June 19, 2023 for the applicant requested Buffer Authorization and 401 Water Quality
Certification respectively.

The applicant hired Terracon Consultants Inc. to conduct the DWR requested bottom sediment
sampling for contaminants in the spoil material derived from the proposed maintenance excavation
in Boat Harbor Canal. A total of 5 samples were taken from BHC under the DWR approved
sampling plan. As a proactive measure Terracon took three samples from Baker Creek. A
reference site was taken for naturally occurring background levels in Battalina Creek. The report
presenting the test results is enclosed. Based upon the findings the level of contaminants, many of
which were below laboratory detectable limits, did not warrant special spoil handling and final
deposition under existing state and federal guidelines. Handling of the spoil material and the final
deposition of the material will not change from the original proposal described in the narrative
cover letter and application package submitted on June 28, 2022.

Mr. Curt Weychert, Assistant Major Permit Coordinator
North Carolina Division of Coastal Management
July 10, 2023
Page Two

The revised DWR “Request for More Information” letter dated June 19, 2023 raised a concern
over the proposed retaining wall and the potential to negatively impact the wetland hydrology in
the adjacent wetland. The Section 404 wetland comprising most of Tract B and situated between
Tract A and Tract C is an emergent estuarine wetland dominated by herbaceous growth, a
homogeneous stand of the invasive common reed (Phragmites australis) indicative of the prior
disturbances resulting from the excavation and filling activities that created the adjacent uplands.
Archived aerial imagery from 1964 submitted as part of the Major CAMA/Dredge and Fill
application shows a large expanse of black needlerush (Juncus roemerianus) marsh that was filled
by excavation of Battalina Creek and a canal system, Baker Creek, and Boat Harbor Canal. This
same marsh was excavated creating the Sargent Canal and the adjacent upland spoil bank.

The emergent estuarine wetlands in the Albemarle-Pamlico Peninsula because of the flat
topography, derive most of their wetland hydrology from the adjacent surface waters and the
seasonal climatic conditions that irregularly flood these wetlands. Surface water levels in this
region also influence/impact groundwater levels in these lower coastal areas. The topographic
gradient is flat and the associated drainage patterns, both surface and subsurface, in this region are
influenced by water levels in the adjacent surface water body. The construction of a retaining wall
along the upland wetland/wetland interface will not impact the drainage patterns because of the
flat topography and will not impede the seasonal flooding of the wetland from wind borne tidal
flooding.

There has been increasing concern and resultant DEQ scoping meetings and permit applications
from the agricultural community in this region because of the inability to gravity flow existing
man-made drainage features with outlets to surfaces waters of the state forcing agriculture
operations to build dikes, block ditches and install mechanical pumps to lower ground water levels
and to block saltwater intrusion from rising sea levels. The Town of Belhaven is no stranger to
the impacts of rising water levels and the negative impacts to drainage and has been actively
pursuing a project design that will incorporate dikes, water control structures and pumps. The
density and vigorous growth of common reed and the associated buildup of organics will help to
maintain the elevation of this wetland over time in the face of rising sea levels. Retaining walls
along the Coastal Wetland/upland interface are a common authorized development activity in the
coastal area. The applicant’s 2018 project across from the current project site (DWR Project No.
20181108v1) included the construction of 612’ of retaining wall along the upland/wetland line.
DWR staff did not raise any concerns over potential impacts to wetland hydrology during the
review of this application. The wall will be constructed with the equipment used to drive the vinyl
sheets operating from uplands resulting in no wetland impacts and or disturbance during
construction activities. Equipment access to Tract C was described in the original narrative project
cover letter dated June 28, 2022. The degradation of this wetland at the current project site
occurred during the excavation and filling that occurred during the late sixties. The invasive
common reed has choked out the native coastal wetland species. While still maintaining some

Mr. Curt Weychert, Assistant Major Permit Coordinator
North Carolina Division of Coastal Management
July 10, 2023
Page Three

important wetland functions, the dense stand of common reed has diminished other functions
especially the habitat value of this wetland.

Thank you for your time spent reviewing and processing this modified/amended Major
CAMA/Dredge and Fill permit application. Please do not hesitate to contact me with any questions
or concerns related to this resubmittal by email or cell: [e-mail] or (252) 402-
4015.

Sincerely,

Steve Trowell
Agent for TJ Land Development LLC

Enclosures

Cc: Kelly Spivey, District Manager, NCDCM Washington Regional Office-EC
Raleigh Bland, Project Manager, USACE Washington Regulatory Field Office-EC
Maria Dunn, Coastal Habitat Coordinator, NCWRC, Washington Regional Office-EC
James Harrison, Fishery Habitat Specialist, NCDMF, Washington Regional Office-EC
Shelton Sullivan, Environmental Specialist II, NCDWR 401 & Buffer Permitting Branch
Raleigh Office
Holley Snider, Environmental Specialist II, NCDWR 401 & Buffer Permitting Branch-EC

252-808-2808 :: 1-888-4RCOAST :: www.nccoastalmanagement.net
DCM MP-1
APPLICATION for
Major Development Permit
(last revised 12/27/06)
North Carolina DIVISION OF COASTAL MANAGEMENT

1. Primary Applicant/ Landowner Information
Business Name
Tj Land Development Llc
Project Name (if applicable)
TJ's Transient Marina
Applicant 1: First Name
Tobin
MI
J.
Last Name
Tetterton
Applicant 2: First Name

MI

Last Name

If additional applicants, please attach an additional page(s) with names listed.
Mailing Address

PO Box
125
City
Pantego
State
NC
ZIP
27860
Country
US
Phone No.
252 - 943 - 3333 ext.
FAX No.
- -
Street Address (if different from above)

City

State

ZIP
-
Email
[e-mail]

2. Agent/Contractor Information
Business Name
N/A
Agent/ Contractor 1: First Name
Steve
MI
J
Last Name
Trowell
Agent/ Contractor 2: First Name

MI

Last Name

Mailing Address
102 East Watson Street
PO Box

City
Windsor
State
NC
ZIP
27983 Phone No. 1
252 – 402-4015 - ext.
Phone No. 2
- - ext.
FAX No.

Contractor #

Street Address (if different from above)

City

State

ZIP
-
Email
[e-mail]

<Form continues on back>

Form DCM MP-1 (Page 2 of 4) APPLICATION for
Major Development Permit
252-808-2808 :: 1-888-4RCOAST :: www.nccoastalmanagement.net
3. Project Location
County (can be multiple)
Beaufort County
Street Address
975 Pantego Street
State Rd. #
Off HWY 264
Subdivision Name
N/A
City
Belhaven
State
NC
Zip
27810 -
Phone No.
(252) – 943- - 3333 ext.
Lot No.(s) (if many, attach additional page with list)
Tract A, B, C, , , ,
a. In which NC river basin is the project located?
Tar Pamlico
b. Name of body of water nearest to proposed project
Battillina Creek, Baker Creek and Boat Harbor Canal
c. Is the water body identified in (b) above, natural or manmade?
Natural Manmade Unknown
d. Name the closest major water body to the proposed project site.
Pungo River
e. Is proposed work within city limits or planning jurisdiction?
Yes No
f. If applicable, list the planning jurisdiction or city limit the proposed
work falls within.
N/A

4. Site Description
a. Total length of shoreline on the tract (ft.)
Approx. 1,715'
b. Size of entire tract (sq.ft.)
4.117 acres or 179,336 ft²
c. Size of individual lot(s)
2.5, 0.4, 1.3,
(If many lot sizes, please attach additional page with a list)
d. Approximate elevation of tract above NHW (normal high water) or
NWL (normal water level)
3.0' NHW or NWL
e. Vegetation on tract
Tract A is vegetated with maintained lawn grasses and a sparse amount of loblolly pines growing on canal bank edge. Tract
B is a 404 wetland vegetated with Phragmites. Tract C includes some of the same wetland feature on Tract B and includes
an upland spoil bank vegetated with mixed hardwoods and shrubs.
f. Man-made features and uses now on tract
A canal system that serves as a base of operation and habor of refuge for the mooring of commercial fishing vessels.
Gravel drive way, loading area and open area used for the storage of boat trailers, crab pots and other associated
commercial fishing gear. The site also serves as a base of operation for a marine construction buisness.
g. Identify and describe the existing land uses adjacent to the proposed project site.
Mixed adjacent land uses include residential, commercial fishing dockage and 2 different boat maintenance yards.
h. How does local government zone the tract?
Marine Industrial

i. Is the proposed project consistent with the applicable zoning?
(Attach zoning compliance certificate, if applicable)
Yes No NA
j. Is the proposed activity part of an urban waterfront redevelopment proposal? Yes No
k. Has a professional archaeological assessment been done for the tract? If yes, attach a copy.

If yes, by whom?
Yes No NA

l. Is the proposed project located in a National Registered Historic District or does it involve a
National Register listed or eligible property?
Yes No NA

<Form continues on next page>
Form DCM MP-1 (Page 3 of 4) APPLICATION for
Major Development Permit
252-808-2808 :: 1-888-4RCOAST :: www.nccoastalmanagement.net
m. (i) Are there wetlands on the site?

(ii) Are there coastal wetlands on the site?

(iii) If yes to either (i) or (ii) above, has a delineation been conducted?
(Attach documentation, if available)
Yes No

Yes No

Yes No
n. Describe existing wastewater treatment facilities.
Town of Belhaven Sewer
o. Describe existing drinking water supply source.
Town of Belhaven
p. Describe existing storm water management or treatment systems.
None

5. Activities and Impacts
a. Will the project be for commercial, public, or private use? Commercial Public/Government
Private/Community
b. Give a brief description of purpose, use, and daily operations of the project when complete.
The purpose of this project is to provide a marina facility for transient boats traveling the Intercoastal Waterway. Amenities
will include a building housing a bathhouse, laundry room and ships store. Fueling services and a marine pumpout will also
be provided. There will be no live aboard dockage provided. Site visit duration will be limited to 30 days.
c. Describe the proposed construction methodology, types of construction equipment to be used during construction, the number of each type
of equipment and where it is to be stored.
Long reach excavator, excavator, dump trucks, tractor, skidsteer loader, equipment barge
d. List all development activities you propose.
Excavation of uplands to create boat mooring and improve navigation, bulkhead and dock construction. Construction of
commercial building.
e. Are the proposed activities maintenance of an existing project, new work, or both? New
f. What is the approximate total disturbed land area resulting from the proposed project? 3.1 acres Sq.Ft or Acres

g. Will the proposed project encroach on any public easement, public accessway or other area
that the public has established use of?
Yes No NA
h. Describe location and type of existing and proposed discharges to waters of the state.
Surface runoff.
i. Will wastewater or stormwater be discharged into a wetland?

If yes, will this discharged water be of the same salinity as the receiving water?
Yes No NA

Yes No NA
j. Is there any mitigation proposed?
If yes, attach a mitigation proposal.
Yes No NA

<Form continues on back>
Form DCM MP-1 (Page 4 of 4) APPLICATION for
Major Development Permit
252-808-2808 :: 1-888-4RCOAST :: www.nccoastalmanagement.net
6. Additional Information
In addition to this completed application form, (MP-1) the following items below, if applicable, must be submitted in order for the application
package to be complete. Items (a) – (f) are always applicable to any major development application. Please consult the application
instruction booklet on how to properly prepare the required items below.
a. A project narrative.
b. An accurate, dated work plat (including plan view and cross-sectional drawings) drawn to scale. Please give the present status of the
proposed project. Is any portion already complete? If previously authorized work, clearly indicate on maps, plats, drawings to distinguish
between work completed and proposed.
c. A site or location map that is sufficiently detailed to guide agency personnel unfamiliar with the area to the site.
d. A copy of the deed (with state application only) or other instrument under which the applicant claims title to the affected properties.
e. The appropriate application fee. Check or money order made payable to DENR.
f. A list of the names and complete addresses of the adjacent waterfront (riparian) landowners and signed return receipts as proof that such
owners have received a copy of the application and plats by certified mail. Such landowners must be advised that they have 30 days in
which to submit comments on the proposed project to the Division of Coastal Management.
Name William Axson Smith, Jr. Phone No.
Address P.O. Box 295, Belhaven, NC 27810
Name Sargent Investment Group LLC Phone No.
Address 2811 Deerfield Land N, Wilson, NC 27896
Name Phone No.
Address

g. A list of previous state or federal permits issued for work on the project tract. Include permit numbers, permittee, and issuing dates.

h. Signed consultant or agent authorization form, if applicable.
i. Wetland delineation, if necessary.
j. A signed AEC hazard notice for projects in oceanfront and inlet areas. (Must be signed by property owner)
k. A statement of compliance with the N.C. Environmental Policy Act (N.C.G.S. 113A 1-10), if necessary. If the project involves expenditure
of public funds or use of public lands, attach a statement documenting compliance with the North Carolina Environmental Policy Act.

7. Certification and Permission to Enter on Land
I understand that any permit issued in response to this application will allow only the development described in the application.
The project will be subject to the conditions and restrictions contained in the permit.
I certify that I am authorized to grant, and do in fact grant permission to representatives of state and federal review agencies to
enter on the aforementioned lands in connection with evaluating information related to this permit application and follow-up
monitoring of the project.
I further certify that the information provided in this application is truthful to the best of my knowledge.
Date __June 26, 2023_________________________ Print Name _TJ Land Development LLC C/O Toby Tetterton, Agent
Steve Trowell__________________________

Signature ___________________________

Please indicate application attachments pertaining to your proposed project.
DCM MP-2 Excavation and Fill Information DCM MP-5 Bridges and Culverts
DCM MP-3 Upland Development
DCM MP-4 Structures Information

252-808-2808 :: 1-888-4RCOAST :: www.nccoastalmanagement.net revised: 12/26/06
Form DCM MP-2
EXCAVATION and FILL
(Except for bridges and culverts)
Attach this form to Joint Application for CAMA Major Permit, Form DCM MP-1. Be sure to complete all other sections of the Joint
Application that relate to this proposed project. Please include all supplemental information.
Describe below the purpose of proposed excavation and/or fill activities. All values should be given in feet.

Access
Channel
(NLW or
NWL)
Canal Boat Basin Boat Ramp Rock Groin Rock
Breakwater
Other
(excluding
shoreline
stabilization)
Length
Width
Avg. Existing
Depth NA NA
Final Project
Depth NA NA
1. EXCAVATION This section not applicable
a. Amount of material to be excavated from below NHW or NWL in
cubic yards.
b. Type of material to be excavated.

c. (i) Does the area to be excavated include coastal wetlands/marsh
(CW), submerged aquatic vegetation (SAV), shell bottom (SB),
or other wetlands (WL)? If any boxes are checked, provide the
number of square feet affected.
CW SAV SB
WL None
(ii) Describe the purpose of the excavation in these areas:
d. High-ground excavation in cubic yards.

2. DISPOSAL OF EXCAVATED MATERIAL This section not applicable
a. Location of disposal area.

b. Dimensions of disposal area.

c. (i) Do you claim title to disposal area?
Yes No NA
(ii) If no, attach a letter granting permission from the owner.
d. (i) Will a disposal area be available for future maintenance?
Yes No NA
(ii) If yes, where?
e. (i) Does the disposal area include any coastal wetlands/marsh
(CW), submerged aquatic vegetation (SAV), shell bottom (SB),
or other wetlands (WL)? If any boxes are checked, provide the
number of square feet affected.
CW SAV SB
WL None
(ii) Describe the purpose of disposal in these areas:
f. (i) Does the disposal include any area in the water?
Yes No NA
(ii) If yes, how much water area is affected?
Clay loam
27159 US 264 East 240' x 680'
-3.5'
420'
12'
-2.0'
-6.0'
Upland ExcavationSargent below NWL
Baker Creekand Boat Harbor, below NWL
450' and 525'395', 490',420'
varies 20' to 48'21.5' av., 16.5'av,10'
+2', +2',+4'
-6.0', -5.0' BHC -8.0', -7.0',-10.0'
2,583 cubic yards calculated using survey data
7,573 cubic yards calculated using survey data
Form DCM MP-2 (Excavation and Fill, Page 2 of 2))))
252-808-2808 :: 1-888-4RCOAST :: www.nccoastalmanagement.net revised: 12/26/06
3. SHORELINE STABILIZATION This section not applicable
(If development is a wood groin, use MP-4 – Structures)
a. Type of shoreline stabilization:
Bulkhead Riprap Breakwater/Sill Other:
b. Length:
Width:
c. Average distance waterward of NHW or NWL:

d. Maximum distance waterward of NHW or NWL:

e. Type of stabilization material:

f. (i) Has there been shoreline erosion during preceding 12
months?
Yes No NA
(ii) If yes, state amount of erosion and source of erosion amount
information.

g. Number of square feet of fill to be placed below water level.
Bulkhead backfill Riprap
Breakwater/Sill Other
h. Type of fill material.

i. Source of fill material.

4. OTHER FILL ACTIVITIES This section not applicable
(Excluding Shoreline Stabilization)
a. (i) Will fill material be brought to the site? Yes No NA
If yes,
(ii) Amount of material to be placed in the water
(iii) Dimensions of fill area
(iv) Purpose of fill

b. (i) Will fill material be placed in coastal wetlands/marsh (CW),
submerged aquatic vegetation (SAV), shell bottom (SB), or
other wetlands (WL)? If any boxes are checked, provide the
number of square feet affected.
CW SAV SB
WL None
(ii) Describe the purpose of the fill in these areas:

5. GENERAL
a. How will excavated or fill material be kept on site and erosion
controlled?

b. What type of construction equipment will be used (e.g., dragline,
backhoe, or hydraulic dredge)?

c. (i) Will navigational aids be required as a result of the project?
Yes No NA
(ii) If yes, explain what type and how they will be implemented.

d. (i) Will wetlands be crossed in transporting equipment to project
site? Yes No NA
(ii) If yes, explain steps that will be taken to avoid or minimize
environmental impacts.

Date

Project Name

Applicant Name

Applicant Signature

1'
0 12'
Vinyl Sheets
N/A
900 ft²
Local permitted borrow pit
Sandy clay
Upland excavation to be undertaken as much as possible in the "dry".The bulkhead will be constructed before the excavation activities began.Spoil material will be sloped, graded and seed with appropriate seasonal mix.
Already permitted and installed.
TJ's Transient Marina
The shortest practical route for upland to upland crossing will be chosen.Wooden equipment mats will be placed on wetland for equipment to travel on.Trucks will not be loaded fully to reduce overall weight. Mats will be removedupon completion of work.
TJ Land Development ,Toby Tetterton, Agent Steve Trowell
1,248'
Long reach excavator, dump truck, equipment barge and bulldozer.
June 26, 2023
252-808-28082 :: 1-888-4RCOAST :: www.nccoastalmanagement.net revised: 12/26/06
Form DCM MP-3
UPLAND DEVELOPMENT
(Construction and/or land disturbing activities)
Attach this form to Joint Application for CAMA Major Permit, Form DCM MP-1. Be sure to complete all other sections of the Joint
Application that relate to this proposed project. Please include all supplemental information.
GENERAL UPLAND DEVELOPMENT
a. Type and number of buildings, facilities, units or structures
proposed.

b. Number of lots or parcels.

c. Density (give the number of residential units and the units per
acre).

d. Size of area to be graded, filled, or disturbed including roads,
ditches, etc.

e. If the proposed project will disturb more than one acre of land, the
Division of Land Resources must receive an erosion and
sedimentation control plan at least 30 days before land-disturbing
activity begins.
(i) If applicable, has a sedimentation and erosion control plan been
submitted to the Division of Land Resources?
Yes No NA
(ii) If yes, list the date submitted:

f. List the materials (such as marl, paver stone, asphalt, or concrete)
to be used for impervious surfaces.

g. Give the percentage of the tract within the coastal shoreline AEC to
be covered by impervious and/or built-upon surfaces, such as
pavement, building, rooftops, or to be used for vehicular driveways
or parking.

i. Give the percentage of the entire tract to be covered by impervious
and/or built-upon surfaces, such as pavement, building, rooftops,
or to be used for vehicular driveways or parking.

h. Projects that require a CAMA Major Development Permit may also
require a Stormwater Certification.
(i) Has a site development plan been submitted to the Division of
Water Quality for review?
Yes No NA
(ii) If yes, list the date submitted: _____________
j. Describe proposed method of sewage disposal.

k. Have the facilities described in Item (i) received state or local
approval?
Yes No NA
If yes, attach appropriate documentation.
l. Describe location and type of proposed discharges to waters of the
state (e.g., surface runoff, sanitary wastewater, industrial/
commercial effluent, “wash down” and residential discharges).

m. Does the proposed project include an innovative stormwater
design?
Yes No NA
If yes, attach appropriate documentation.
One building, 40' x 240'Three parcels: Tract A -2.45 acres, Tract B - 0.369 acresTract C - 1.294 acres
1 building per 4.1 Acres
To be submitted under seperatecover.
18,000 ft² or 14%
15.1%
Town of Belhaven Sewer
Surface runoff.
Gravel for driveways and parking.
2.9 acres
(2)-retaining walls, 350 linear feet Tract "A" and 406' Tract "C"
Form DCM MP-3 (Upland Development, Page 2 of 2))))
252-808-2808 :: 1-888-4RCOAST :: www.nccoastalmanagement.net revised: 12/26/06
m. Describe proposed drinking water supply source (e.g., well,
community, public system, etc.)

n. (i) Will water be impounded?Yes No NA
(ii) If yes, how many acres?
o. When was the lot(s) platted and recorded?

p. If proposed development is a subdivision, will additional utilities be
installed for this upland development?
Yes No NA

Date

Project Name

Applicant Name
Applicant Signature
Town of Belhaven
TJ Transient Marina
June 26, 2023
Tract "A" and "B" prior to August 2000Tract "C" June 2022
TJ Land Development LLC, Toby Tetterton, Agent Steve Trowell
252-808-2808 :: 1-888-4RCOAST :: www.nccoastalmanagement.net revised: 12/27/06
Form DCM MP-4
STRUCTURES
(Construction within Public Trust Areas)
Attach this form to Joint Application for CAMA Major Permit, Form DCM MP-1. Be sure to complete all other sections of the Joint
Application that relate to this proposed project. Please include all supplemental information.
1. DOCKING FACILITY/MARINA CHARACTERISTICS This section not applicable
a. (i) Is the docking facility/marina:
Commercial Public/Government Private/Community
b. (i) Will the facility be open to the general public?
Yes No
c. (i) Dock(s) and/or pier(s)
(ii) Number
(iii) Length
(iv) Width
(v) Floating Yes No
d. (i) Are Finger Piers included?Yes No
If yes:
(ii) Number
(iii) Length
(iv) Width
(v) Floating Yes No
e. (i) Are Platforms included?Yes No
If yes:
(ii) Number
(iii) Length
(iv) Width
(v) Floating Yes No
Note: Roofed areas are calculated from dripline dimensions.
f. (i) Are Boatlifts included?Yes No
If yes:
(ii) Number
(iii) Length
(iv) Width
g. (i) Number of slips proposed

(ii) Number of slips existing

h. Check all the types of services to be provided.
Full service, including travel lift and/or rail, repair or
maintenance service
Dockage, fuel, and marine supplies
Dockage (“wet slips”) only, number of slips:
Dry storage; number of boats:
Boat ramp(s); number of boat ramps:
Other, please describe:
i. Check the proposed type of siting:
Land cut and access channel
Open water; dredging for basin and/or channel
Open water; no dredging required
Other; please describe:
j. Describe the typical boats to be served (e.g., open runabout,
charter boats, sail boats, mixed types).

k.Typical boat length:
m. (i) Will the facility have tie pilings?
Yes No
(ii) If yes number of tie pilings?
l. (i) Will the facility be open to the general public?
Yes No
3- Docks, 1 - Pier
1
24'
16'
Transient mixed sailboats and power boats 26' and greater
35'
Boat harbor Canal is currently used to moor commercial vessels.Baker Creek has been used over the years as well. As many as 5 vessels at any time.
Dock "A" 985', Dock "B" 168, Dock "C" 420', Pier "A" 70'
Dock "A" 6', Dock"B" 8', Dock "C" 6', Pier "A" 6''
38
Form DCM MP-4 (Structures, Page 2 of 4))))
252-808-2808 :: 1-888-4RCOAST :: www.nccoastalmanagement.net revised: 12/27/06

2. DOCKING FACILITY/MARINA OPERATIONS This section not applicable
a. Check each of the following sanitary facilities that will be included in the proposed project.
Office Toilets
Toilets for patrons; Number: ; Location:

Showers
Boatholding tank pumpout; Give type and location:

b. Describe treatment type and disposal location for all sanitary wastewater.

c. Describe the disposal of solid waste, fish offal and trash.

d. How will overboard discharge of sewage from boats be controlled?

e. (i) Give the location and number of “No Sewage Discharge” signs proposed.

(ii) Give the location and number of “Pumpout Available” signs proposed.

f. Describe the special design, if applicable, for containing industrial type pollutants, such as paint, sandblasting waste and petroleum products.

g. Where will residue from vessel maintenance be disposed of?

h. Give the number of channel markers and “No Wake” signs proposed.
i. Give the location of fuel-handling facilities, and describe the safety measures planned to protect area water quality.

j. What will be the marina policy on overnight and live-aboard dockage?

k. Describe design measures that promote boat basin flushing?

l. If this project is an expansion of an existing marina, what types of services are currently provided?

Fixed standpipe on Pier "A" connected to Town of Belhaven Sewer.
Town Sewer.
Trash service provided by the Town of Belhaven.
At the entrance points to each dock.
"No Sewage Discharge" and "Pumpout Available" combined on each of 5 different sign locations.
N/A
Overnight dockage will be allowed but no live-aboard.
The existing canal system will be widened with the most significant width expansion at the entrance.The design is a continous surface water expansion maintaining a water depth no deeper than the depthin the existing marked channel leading to this canal system.
Bathrooms, showers and laundry located in the 40' x 240' marina building.
Site has served as commercial fishing staging area and harbor of refuge for mooring of commercial fishing vessels.
Fuel handling facilities are located and limited to Pier "A" and portion of Dock "C". Proposed fuel tank will be above 100 floodand comply with industry standards with a double wall design. Spill prevention and response described in project narrative.
There will be an marina operation policy banning boats from discharging sewage and those thatviolate the policy will be expelled. Signage will be placed at the entrance to each dock.
TBD
40' x 240 building
There will be no maintenance activities that will generate industrial type pollutants. The shipstore willsell only biodegradable soap for washing vessels.
N/A
Form DCM MP-4 (Structures, Page 3 of 4))))
252-808-2808 :: 1-888-4RCOAST :: www.nccoastalmanagement.net revised: 12/27/06
m. Is the marina/docking facility proposed within a primary or secondary nursery area?
Yes No
n. Is the marina/docking facility proposed within or adjacent to any shellfish harvesting area?
Yes No
o. Is the marina/docking facility proposed within or adjacent to coastal wetlands/marsh (CW), submerged aquatic vegetation (SAV), shell bottom
(SB), or other wetlands (WL)? If any boxes are checked, provide the number of square feet affected.
CW SAV SB
WL None

p. Is the proposed marina/docking facility located within or within close proximity to any shellfish leases? Yes No
If yes, give the name and address of the leaseholder(s), and give the proximity to the lease.

3. BOATHOUSE (including covered lifts) This section not applicable
a. (i) Is the boathouse structure(s):
Commercial Public/Government Private/Community
(ii) Number
(iii) Length
(iv) Width
Note: Roofed areas are calculated from dripline dimensions.

4. GROIN (e.g., wood, sheetpile, etc. If a rock groin, use MP-2, Excavation and Fill.) This section not applicable
a. (i) Number
(ii) Length
(iii) Width

5. BREAKWATER (e.g., wood, sheetpile, etc.) This section not applicable
a. Length b. Average distance from NHW, NWL, or wetlands

c. Maximum distance beyond NHW, NWL or wetlands

6. MOORING PILINGS and BUOYS This section not applicable
a. Is the structure(s):
Commercial Public/Government Private/Community
b. Number
c. Distance to be placed beyond shoreline
Note: This should be measured from marsh edge, if present.
d. Description of buoy (color, inscription, size, anchor, etc.)

e. Arc of the swing

N/A
Form DCM MP-4 (Structures, Page 4 of 4))))
252-808-2808 :: 1-888-4RCOAST :: www.nccoastalmanagement.net revised: 12/27/06
7. GENERAL
a. Proximity of structure(s) to adjacent riparian property lines

Note: For buoy or mooring piling, use arc of swing including length
of vessel.
b. Proximity of structure(s) to adjacent docking facilities.

c. Width of water body

d. Water depth at waterward end of structure at NLW or NWL

e. (i) Will navigational aids be required as a result of the project?
Yes No NA
(ii) If yes, explain what type and how they will be implemented.

8. OTHER This section not applicable
a. Give complete description:

Date

Project Name

Applicant Name
Applicant Signature
6'
Already authorized
48' Sargent Canal, 80' Boat Harbor Canal 82' Sargent Canal, 80' Boat Harbor Canal, 100' Baker Creek
An 8' x 114' boardwalk over 404 wetlands(8' x 78') and uplands (8' x 36") from Tract "A" to accessdock "C" on Tract "C".
June 26, 2023
TJ's Transient Marina
80' to 175'
TJ Land Development LLC, Toby Tetterton, Agent Steve Trowell
Terracon Consultants, Inc. 314 Beacon Drive Greenville, NC 28590
P [phone] F [phone] terracon.com Registered NC F-0869
July 6, 2023
TJ’s Land Development LLC
987 East Pantego Street
Belhaven, North Carolina 27810
Attn: Mr. Toby Tetterton
P: [phone]
E: [e-mail]
Re: Report of Sediment Sampling
Proposed TJ’s Transient Marina
727 Pantego Street
Belhaven, Beaufort County, North Carolina
Terracon Project No. 72237064
Dear Mr. Tetterton,
Terracon Consultants, Inc. (Terracon) has completed the sediment sampling services for TJ’s
Land Development (client) at the above-referenced site. The work was performed in general
accordance with our proposal P72237064, dated June 19, 2023. The purpose of this sampling
was to evaluate the presence of metals and other contaminants in the channel bottom sediment
prior to dredging. Dredged soils/sediment with elevated metal levels or contamination would
require handling differently than non-impacted soils.
Terracon appreciates this opportunity to provide environmental services on this project. Should
you have any questions or require additional information, please do not hesitate to contact our
office at [phone].
Sincerely,
Terracon Consultants, Inc.
Carl F. Bonner, PE Neal McElveen, PE
Principal / Office Manager Principal / Senior Engineer
Attachments
Report of Sediment Sampling Services
Proposed TJ’s Transient Marina ■ Belhaven, NC
July 6, 2023 ■Terracon Report No. 72237064
Responsive ■Resourceful ■Reliable 1
PROJECT INFORMATION
We understand that a marina for transient boats is planned for the site in Belhaven, NC. The
site is currently undeveloped and is a thinly wooded peninsula bordered by Baker’s Canal,
Baker’s Creek and Boat Harbor Canal. Both Boat Harbor Canal and Baker’s Canal are man-
made waterways. These waterways have silted in and will require dredging in order to allow
for adequate draft for boats to access the marina and haul-out yard.
Across Baker’s Canal, to the west of the site, is TJ’s Marina and Boat Yard that has several
docks and a travel lift for removing boats for servicing. Boat maintenance is currently
performed onsite.
Across Boat Harbor Canal, to the south of the site, is an existing boat maintenance facility
named River Forest Shipyard. Boat maintenance is performed at River Forest Shipyard and
this facility has been operational for many years. We understand that River Forest Shipyard
floods several times a year and sediment and metals of concern wash into Boat Harbor Canal.
The purpose of the sediment sampling in Boat Harbor Canal and Baker’s Creek prior to
dredging was to evaluate metals concentrations and other contaminants from the adjacent
boat works to determine if special handling is warranted.
SCOPE OF SERVICES
Our scope of services was in response to the identified concerns outlined in the Project
Information.
Sediment Sampling
In order to obtain representative samples of the existing soils/sediment in the basins that are
to be dredged, we performed the following:
Mobilized to the site with sediment samplers, laboratory prepared containers and the
appropriate PPE.
Used a boat provided by the client, traveled to the locations marked on the attached
drawing.
Anchored the boat at the sample location.
Obtained a sample of the upper 3 feet of sediment at each location.
Mixed the sample using stainless steel spoons and gloved hands. The mixing bowls
and spoons were cleaned before sampling and between each sampling point.
Samples were placed in laboratory prepared jars and then stored on ice.
Shipped the samples on ice overnight to Pace Analytical Lab in Huntersville, NC.
Report of Sediment Sampling Services
Proposed TJ’s Transient Marina ■ Belhaven, NC
July 6, 2023 ■Terracon Report No. 72237064
Responsive ■Resourceful ■Reliable 2
Analyzed the samples obtained for Metals using EPA Method 6010, Mercury using
EPA Method 7470A, PCBs using EPA Method 8082 Low Level and PAHs using EPA
Method 8270C, Hexavalent Chromium using EPA Method 7196A and Hexavalent
Chromium using EPA 7196A Leachate (SPLP).
Additionally, as suggested by NCDEQ, the samples were using SW-846 Test Method
1311 Toxicity Characteristic Leaching Procedure (TCLP) for disposal purposes.
Issued this written report summarizing our field activities and the analytical results.
2.1 Standard of Care
Terracon’s services were performed in a manner consistent with generally accepted practices
of the profession undertaken in similar studies in the same geographical area during the same
time. Terracon makes no warranties, either expressed or implied, regarding the findings,
conclusions, or recommendations. Please note that Terracon does not warrant the work of
laboratories, regulatory agencies, or other third parties supplying information used in the
preparation of the report. These services were performed in accordance with the scope of
work agreed with you, our client, as reflected in our proposal and were not restricted by or
intended to be in conformance with ASTM E1903-11.
2.2 Additional Scope Limitations
Findings, conclusions and recommendations resulting from these services are based upon
information derived from the on-site activities and other services performed under this scope
of work; such information is subject to change over time. Certain indicators of the presence of
hazardous substances, petroleum products, or other constituents may have been latent,
inaccessible, unobservable, non-detectable, or not present during these services; thus, we
cannot represent that the site is free of hazardous substances, toxic materials, petroleum
products, or other latent conditions beyond those identified during this assessment.
Subsurface conditions may vary from those encountered at specific borings or wells or during
other surveys, tests, assessments, investigations, or exploratory services. The data,
interpretations, findings and our recommendations are based solely upon data obtained at the
time and within the scope of these services.
2.3 Reliance
This report was prepared for the exclusive use and reliance of TJ’s Marine Construction, LLC
(client). Reliance by any other party is prohibited without the written authorization of the client
and Terracon. Reliance on the Sediment Sampling Report by the client and all authorized
parties will be subject to the terms, conditions, and limitations stated in the Agreement for
Services sections of this proposal incorporated herein, the Reliance Agreement, and the
Report of Sediment Sampling Services
Proposed TJ’s Transient Marina ■ Belhaven, NC
July 6, 2023 ■Terracon Report No. 72237064
Responsive ■Resourceful ■Reliable 3
report. The defined contractual limitation of liability is the aggregate limit of Terracon’s liability
to the client and all relying parties.
FINDINGS
Sampling was performed on June 21, 2023. Samples S-1 through S-8 were located in the
areas to be dredged. Sample S-9 was a background sample. Please see the attached
Exhibits 1 and 2 for the sediment sample locations.
Based on electronic mail correspondence with representatives of the North Carolina
Department of Environmental Quality (NCDEQ), the sediment sample results are compared
to the NCDEQ Preliminary Soil Remediation Goals (PSRGs), dated January 2023.
Metals were tested using both the EPA Method 6010 and the SW-846 Test Method 1311
Toxicity Characteristic Leaching Procedure (TCLP).
Cadmium (except for background sample S-9), selenium, and silver were below laboratory
reporting limits. Arsenic concentrations ranged from below reporting limits to 9.5 milligrams
per kilogram [mg/kg] (S-1). Total chromium was identified in all the sediment samples ranging
from concentrations of 3.3 mg/kg (S-8) to 14.8 mg/kg (S-1). Copper concentrations ranged
from below reporting limits to 78.4 mg/kg (S-4). Total lead was identified in all the sediment
samples ranging from concentrations of 3.4 mg/kg (S-8) to 17.8 mg/kg (S-6). Zinc
concentrations ranged from below reporting limits to 51.5 mg/kg (S-4).
TCLP and SPLP (Hexavalent Chromium) were below laboratory reporting limits for all analytes
except zinc in S-4 that indicated a concentration of 0.34 milligrams per liter (mg/l). Please note
that Zinc does not have an established TCLP limit. The analytical results of our sampling are
summarized in Tables 1 and 2 below. The complete analytical test data reports are attached
with this report.
Report of Sediment Sampling Services
Proposed TJ’s Transient Marina ■ Belhaven, NC
July 6, 2023 ■Terracon Report No. 72237064
Responsive ■Resourceful ■Reliable 4
Metals – EPA 6010
The metals analysis indicated in the following table.
Table 1 – Total Metals - EPA 6010 Soil Sampling Analytical Summary
Sample ID
Co
n
t
a
m
i
na
n
t

o
f
Co
n
c
e
r
n
(Q
u
a
n
t
i
t
ie
s
Re
p
o
r
t
e
d
i
n
mg
/
k
g
)
An
a
l
y
z
e
d
b
y
EP
A
Me
t
h
o
d
60
1
0
Ar
s
e
n
i
c
Ca
d
m
i
u
m
Ch
r
o
m
i
u
m
Co
p
p
e
r
Le
a
d
Ni
c
k
e
l
Se
l
e
n
i
u
m
Si
l
v
e
r
Zi
n
c
S-1 9.5 ND 14.8 ND 8.7 2.9 ND ND 5.5
S-2 ND ND 6.5 ND 6.1 2.6 ND ND 5.2
S-3 ND ND 5.1 ND 4.3 ND ND ND 4.5
S-4 ND ND 5.5 78.4 8.3 3.0 ND ND 51.5
S-5 ND ND 14.2 ND 10.5 4.1 ND ND 8.5
S-6 ND ND 7.5 7.4 17.8 5.8 ND ND 20.7
S-7 6.3 ND 9.9 8.9 8.0 ND ND ND 10.6
S-8 ND ND 3.3 ND 3.4 ND ND ND ND
S-9 Background 4.4 2.0 4.6 ND 4.4 ND ND ND ND
Residential
Health Based
PSRG (mg/kg)
0.68 1.4 0.31 630 400 310 78 78 4700
Industrial/Com
mercial Health
Based PSRG
(mg/kg)
3.0 20 6.5 9300 800 4700 1200 1200 70000
Protection of
Groundwater
PSRG (mg/kg)
5.8 3 3.8 700 250 130 2.1 3.4 1200
USGS Eastern
Concentrations
(mg/kg)
0.1-73
(mean
= 4.8)
NE
1-1000
(mean
33)
1-700
(mean
13)
10-300
(mean
= 14)
5-700
(mean
11)
0.1-3.9
(mean
0.3
NE
5-2900
(mean
40)
Constituents shaded are above NCDEQs Industrial/Commercial Health Based PSRGs. Quantities are reported in mg/kg (parts
per million); ND = Non-Detect (constituent was analyzed to be below the laboratory’s reporting limit); NE = Not Established
United States Geological Survey (USGS) Eastern Concentrations are from USGS Paper 1270 “Element Concentrations in Soils
and Other Surficial Materials of the Conterminous United States, published in 1984.
Report of Sediment Sampling Services
Proposed TJ’s Transient Marina ■ Belhaven, NC
July 6, 2023 ■Terracon Report No. 72237064
Responsive ■Resourceful ■Reliable 5
Table 2 – TCLP Metals - TCLP Soil Sampling Analytical Summary
Sample ID
Contaminant of Concern (Quantities Reported in mg/L) Analyzed by EPA Method 6010D
except for Chromium (SPLP) and Mercury (7470) - Toxicity Characteristic Leaching
Procedure TCLP
Ar
s
e
n
i
c
Ca
d
m
i
u
m
Ch
r
o
m
i
u
m
Co
p
p
e
r
Le
a
d
Ni
c
k
e
l
Se
l
e
n
i
u
m
Si
l
v
e
r
Zi
n
c
S-1 ND ND ND ND ND ND ND ND ND
S-2 ND ND ND ND ND ND ND ND ND
S-3 ND ND ND ND ND ND ND ND ND
S-4 ND ND ND ND ND ND ND ND 0.34
S-5 ND ND ND ND ND ND ND ND ND
S-6 ND ND ND ND ND ND ND ND ND
S-7 ND ND ND ND ND ND ND ND ND
S-8 ND ND ND ND ND ND ND ND ND
S-9 Background ND ND ND ND ND ND ND ND ND
TCLP
Regulatory
Limits (mg/L)
5.0 1.0 5.0 N/A 5.0 N/A 1.0 5.0 N/A
Quantities are reported in mg/L; ND = Non-Detect (constituent was analyzed to be below the laboratory’s reporting limit); Copper,
Nickel and Zinc do not have TCLP regulatory limits.
Mercury – EPA 7470 TCLP
Non-detect in the samples analyzed.
Mercury – EPA 7471
Non-detect in the samples analyzed.
Polychlorinated Biphenyls (PCB) - EPA 8082 Low Level
Non-detect in the samples analyzed.
Polycyclic Aromatic Hydrocarbons (PAH) - EPA 8082 Low Level
Non-detect in the samples analyzed.
Report of Sediment Sampling Services
Proposed TJ’s Transient Marina ■ Belhaven, NC
July 6, 2023 ■Terracon Report No. 72237064
Responsive ■Resourceful ■Reliable 6
Hexavalent Chromium - EPA 7196 SPLP
Non-detect in the samples analyzed.
CONCLUSIONS
Based on our sampling and the analytical laboratory results, the proposed dredge soils do not
appear to be impacted and will not require special treatment for disposal.
As noted in Table 1, arsenic and chromium were detected at levels above the NCDEQ
Industrial/Commercial PSRGs, however the levels are deemed to be naturally occurring.
Terracon compared the results to the United States Geological Survey (USGS) Eastern
Concentrations from USGS Paper 1270 “Element Concentrations in Soils and Other Surficial
Materials of the Conterminous United States, published 1984, and as depicted in Table 1, the
detected metals concentrations for the dredge samples and the background sample at the
site are within the average range of concentrations expected for naturally occurring elements
within soils in North Carolina.
In addition, the results of the TCLP analysis for the metals, including Mercury and Hexavalent
Chromium, were non-detect, therefore further supporting the assertion of naturally occurring
levels.
Report of Sediment Sampling Services
Proposed TJ’s Transient Marina | Belhaven, NC
July 6, 2023 | Terracon Project No. 72237064
Note to Preparer: This is a large table with outside borders. Just click inside the table
above this text box, then paste your GIS Toolbox image.
When paragraph markers are turned on you may notice a line of hidden text above
and outside the table – please leave that alone. Limit editing to inside the table.
Exhibit 1 – Site Location
DIAGRAM IS FOR GENERAL LOCATION ONLY, AND IS NOT INTENDED FOR CONSTRUCTION PURPOSES MAP PROVIDED BY MICROSOFT BING MAPS
Report of Sediment Sampling Services
Proposed TJ’s Transient Marina | Belhaven, NC
July 6, 2023 | Terracon Project No. 72237064
Note to Preparer: This is a large table with outside borders. Just click inside the table
above this text box, then paste your GIS Toolbox image.
When paragraph markers are turned on you may notice a line of hidden text above
and outside the table – please leave that alone. Limit editing to inside the table.
Exhibit 2 – Sample Locations
DIAGRAM IS FOR GENERAL LOCATION ONLY, AND IS NOT INTENDED FOR CONSTRUCTION PURPOSES MAP PROVIDED BY MICROSOFT BING MAPS
SITE PLAN PROVIDED BY CLIENT
#=CL#
July 03, 2023
LIMS USE: FR - CARL BONNER
LIMS OBJECT ID: 92674134
92674134
Project:
Pace Project No.:
RE:
Carl Bonner
Terracon
314 Beacon Drive
Winterville, NC 28590
TJs TRANSIENT MARINA
Dear Carl Bonner:
Enclosed are the analytical results for sample(s) received by the laboratory on June 22, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 43
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
North Carolina Certification #: 381
South Carolina Certification #: 98011001
Virginia Certification #: 460204
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 43
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Lab ID Sample ID Matrix Date Collected Date Received
92674134001 S-1 Solid 06/21/23 08:40 06/22/23 09:35
92674134002 S-2 Solid 06/21/23 08:52 06/22/23 09:35
92674134003 S-3 Solid 06/21/23 09:02 06/22/23 09:35
92674134004 S-4 Solid 06/21/23 09:12 06/22/23 09:35
92674134005 S-5 Solid 06/21/23 09:26 06/22/23 09:35
92674134006 S-6 Solid 06/21/23 09:38 06/22/23 09:35
92674134007 S-7 Solid 06/21/23 09:59 06/22/23 09:35
92674134008 S-8 Solid 06/21/23 10:18 06/22/23 09:35
92674134009 S-9 Solid 06/21/23 10:34 06/22/23 09:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 43
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92674134001 S-1 EPA 8082A 8 PASI-CSEM
EPA 6010D 9 PASI-GAMS
EPA 6010D 9 PASI-GAMS
EPA 7470A 1 PASI-GAVB
EPA 7471B 1 PASI-GAVB
EPA 8270E 21 PASI-CSEM
SW-846 1 PASI-CKDF
EPA 7196A 1 PASI-AMDW
EPA 7196A 1 PASI-AMDW
92674134002 S-2 EPA 8082A 8 PASI-CSEM
EPA 6010D 9 PASI-GAMS
EPA 6010D 9 PASI-GAMS
EPA 7470A 1 PASI-GAVB
EPA 7471B 1 PASI-GAVB
EPA 8270E 21 PASI-CSEM
SW-846 1 PASI-CKDF
EPA 7196A 1 PASI-AMDW
EPA 7196A 1 PASI-AMDW
92674134003 S-3 EPA 8082A 8 PASI-CSEM
EPA 6010D 9 PASI-GAMS
EPA 6010D 9 PASI-GAMS
EPA 7470A 1 PASI-GAVB
EPA 7471B 1 PASI-GAVB
EPA 8270E 21 PASI-CSEM
SW-846 1 PASI-CKDF
EPA 7196A 1 PASI-AMDW
EPA 7196A 1 PASI-AMDW
92674134004 S-4 EPA 8082A 8 PASI-CSEM
EPA 6010D 9 PASI-GAMS
EPA 6010D 9 PASI-GAMS
EPA 7470A 1 PASI-GAVB
EPA 7471B 1 PASI-GAVB
EPA 8270E 21 PASI-CSEM
SW-846 1 PASI-CKDF
EPA 7196A 1 PASI-AMDW
EPA 7196A 1 PASI-AMDW
92674134005 S-5 EPA 8082A 8 PASI-CSEM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 43
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 6010D 9 PASI-GAMS
EPA 6010D 9 PASI-GAMS
EPA 7470A 1 PASI-GAVB
EPA 7471B 1 PASI-GAVB
EPA 8270E 21 PASI-CSEM
SW-846 1 PASI-CKDF
EPA 7196A 1 PASI-AMDW
EPA 7196A 1 PASI-AMDW
92674134006 S-6 EPA 8082A 8 PASI-CSEM
EPA 6010D 9 PASI-GAMS
EPA 6010D 9 PASI-GAMS
EPA 7470A 1 PASI-GAVB
EPA 7471B 1 PASI-GAVB
EPA 8270E 21 PASI-CSEM
SW-846 1 PASI-CKDF
EPA 7196A 1 PASI-AMDW
EPA 7196A 1 PASI-AMDW
92674134007 S-7 EPA 8082A 8 PASI-CSEM
EPA 6010D 9 PASI-GAMS
EPA 6010D 9 PASI-GAMS
EPA 7470A 1 PASI-GAVB
EPA 7471B 1 PASI-GAVB
EPA 8270E 21 PASI-CSEM
SW-846 1 PASI-CKDF
EPA 7196A 1 PASI-AMDW
EPA 7196A 1 PASI-AMDW
92674134008 S-8 EPA 8082A 8 PASI-CBAJ
EPA 6010D 9 PASI-GAMS
EPA 6010D 9 PASI-GAMS
EPA 7470A 1 PASI-GAVB
EPA 7471B 1 PASI-GAVB
EPA 8270E 21 PASI-CSEM
SW-846 1 PASI-CKDF
EPA 7196A 1 PASI-AMDW
EPA 7196A 1 PASI-AMDW
92674134009 S-9 EPA 8082A 8 PASI-CBAJ
EPA 6010D 9 PASI-GAMS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 43
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 6010D 9 PASI-GAMS
EPA 7470A 1 PASI-GAVB
EPA 7471B 1 PASI-GAVB
EPA 8270E 21 PASI-CSEM
SW-846 1 PASI-CKDF
EPA 7196A 1 PASI-AMDW
EPA 7196A 1 PASI-AMDW
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Sample:S-1 Lab ID:92674134001 Collected:06/21/23 08:40 Received:06/22/23 09:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 06/28/23 12:33 12674-11-206/24/23 17:1542.6 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/28/23 12:33 11104-28-206/24/23 17:1542.6 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/28/23 12:33 11141-16-506/24/23 17:1542.6 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/28/23 12:33 53469-21-906/24/23 17:1542.6 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/28/23 12:33 12672-29-606/24/23 17:1542.6 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/28/23 12:33 11097-69-106/24/23 17:1542.6 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/28/23 12:33 11096-82-506/24/23 17:1542.6 1
Surrogates
Decachlorobiphenyl (S)56 %06/28/23 12:33 2051-24-306/24/23 17:1510-174 1
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic 9.5 mg/kg 06/28/23 22:47 7440-38-206/24/23 12:203.9 1
Cadmium ND mg/kg 06/28/23 22:47 7440-43-906/24/23 12:201.3 1
Chromium 14.8 mg/kg 06/28/23 22:47 7440-47-306/24/23 12:201.3 1
Copper ND mg/kg 06/28/23 22:47 7440-50-806/24/23 12:205.2 1
Lead 8.7 mg/kg 06/28/23 22:47 7439-92-106/24/23 12:203.2 1
Nickel 2.9 mg/kg 06/28/23 22:47 7440-02-006/24/23 12:202.6 1
Selenium ND mg/kg 06/28/23 22:51 7782-49-2 D306/24/23 12:2032.3 5
Silver ND mg/kg 06/28/23 22:47 7440-22-406/24/23 12:201.3 1
Zinc 5.5 mg/kg 06/28/23 22:47 7440-66-606/24/23 12:203.9 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 06/29/23 17:43 Initial pH: 9.36; Final pH: 5.43
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP, TCLP
Arsenic ND mg/L 07/01/23 06:50 7440-38-206/30/23 13:250.30 1
Cadmium ND mg/L 07/01/23 06:50 7440-43-906/30/23 13:250.10 1
Chromium ND mg/L 07/01/23 06:50 7440-47-306/30/23 13:250.10 1
Copper ND mg/L 07/01/23 06:50 7440-50-806/30/23 13:250.20 1
Lead ND mg/L 07/01/23 06:50 7439-92-106/30/23 13:250.25 1
Nickel ND mg/L 07/01/23 06:50 7440-02-006/30/23 13:250.20 1
Selenium ND mg/L 07/01/23 06:50 7782-49-206/30/23 13:250.40 1
Silver ND mg/L 07/01/23 06:50 7440-22-406/30/23 13:250.10 1
Zinc ND mg/L 07/01/23 06:50 7440-66-606/30/23 13:250.20 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 06/29/23 17:43 Initial pH: 9.36; Final pH: 5.43
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury, TCLP
Mercury ND mg/L 07/03/23 11:57 7439-97-607/03/23 07:200.0050 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury ND mg/kg 06/30/23 11:51 7439-97-606/30/23 08:000.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Sample:S-1 Lab ID:92674134001 Collected:06/21/23 08:40 Received:06/22/23 09:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV MW PAH by SIM
Acenaphthene ND ug/kg 06/30/23 06:53 83-32-906/27/23 21:1213.1 1
Acenaphthylene ND ug/kg 06/30/23 06:53 208-96-806/27/23 21:1213.1 1
Anthracene ND ug/kg 06/30/23 06:53 120-12-706/27/23 21:1213.1 1
Benzo(a)anthracene ND ug/kg 06/30/23 06:53 56-55-306/27/23 21:1213.1 1
Benzo(a)pyrene ND ug/kg 06/30/23 06:53 50-32-806/27/23 21:1213.1 1
Benzo(b)fluoranthene ND ug/kg 06/30/23 06:53 205-99-206/27/23 21:1213.1 1
Benzo(g,h,i)perylene ND ug/kg 06/30/23 06:53 191-24-206/27/23 21:1213.1 1
Benzo(k)fluoranthene ND ug/kg 06/30/23 06:53 207-08-906/27/23 21:1213.1 1
Chrysene ND ug/kg 06/30/23 06:53 218-01-906/27/23 21:1213.1 1
Dibenz(a,h)anthracene ND ug/kg 06/30/23 06:53 53-70-306/27/23 21:1213.1 1
Fluoranthene ND ug/kg 06/30/23 06:53 206-44-006/27/23 21:1213.1 1
Fluorene ND ug/kg 06/30/23 06:53 86-73-706/27/23 21:1213.1 1
Indeno(1,2,3-cd)pyrene ND ug/kg 06/30/23 06:53 193-39-506/27/23 21:1213.1 1
1-Methylnaphthalene ND ug/kg 06/30/23 06:53 90-12-0 L206/27/23 21:1213.1 1
2-Methylnaphthalene ND ug/kg 06/30/23 06:53 91-57-606/27/23 21:1213.1 1
Naphthalene ND ug/kg 06/30/23 06:53 91-20-306/27/23 21:1213.1 1
Phenanthrene ND ug/kg 06/30/23 06:53 85-01-806/27/23 21:1213.1 1
Pyrene ND ug/kg 06/30/23 06:53 129-00-006/27/23 21:1213.1 1
Surrogates
2-Fluorobiphenyl (S)27 %06/30/23 06:53 321-60-806/27/23 21:1210-130 1
Nitrobenzene-d5 (S)41 %06/30/23 06:53 4165-60-006/27/23 21:1210-150 1
Terphenyl-d14 (S)49 %06/30/23 06:53 1718-51-006/27/23 21:1210-162 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.6 %06/22/23 17:41 N20.10 1
Analytical Method: EPA 7196A Preparation Method: EPA 7196A Modified
Pace Analytical Services - Asheville
7196 Chromium, Hexavalent
Chromium, Hexavalent ND mg/kg 06/27/23 21:23 18540-29-906/27/23 18:545.9 1
Analytical Method: EPA 7196A Leachate Method/Date: EPA 1312; 06/26/23 15:37
Pace Analytical Services - Asheville
7196 Chromium, Hex, SPLP
Chromium, Hexavalent ND mg/L 06/28/23 22:51 18540-29-9 H10.010 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Sample:S-2 Lab ID:92674134002 Collected:06/21/23 08:52 Received:06/22/23 09:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 06/28/23 12:46 12674-11-206/24/23 17:1540.9 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/28/23 12:46 11104-28-206/24/23 17:1540.9 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/28/23 12:46 11141-16-506/24/23 17:1540.9 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/28/23 12:46 53469-21-906/24/23 17:1540.9 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/28/23 12:46 12672-29-606/24/23 17:1540.9 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/28/23 12:46 11097-69-106/24/23 17:1540.9 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/28/23 12:46 11096-82-506/24/23 17:1540.9 1
Surrogates
Decachlorobiphenyl (S)48 %06/28/23 12:46 2051-24-306/24/23 17:1510-174 1
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 06/28/23 22:56 7440-38-206/24/23 12:203.5 1
Cadmium ND mg/kg 06/28/23 22:56 7440-43-906/24/23 12:201.2 1
Chromium 6.5 mg/kg 06/28/23 22:56 7440-47-306/24/23 12:201.2 1
Copper ND mg/kg 06/28/23 22:56 7440-50-806/24/23 12:204.6 1
Lead 6.1 mg/kg 06/28/23 22:56 7439-92-106/24/23 12:202.9 1
Nickel 2.6 mg/kg 06/28/23 22:56 7440-02-006/24/23 12:202.3 1
Selenium ND mg/kg 06/28/23 23:01 7782-49-2 D306/24/23 12:2028.9 5
Silver ND mg/kg 06/28/23 22:56 7440-22-406/24/23 12:201.2 1
Zinc 5.2 mg/kg 06/28/23 22:56 7440-66-606/24/23 12:203.5 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 06/29/23 17:43 Initial pH: 9.67; Final pH: 5.55
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP, TCLP
Arsenic ND mg/L 07/01/23 07:10 7440-38-206/30/23 13:250.30 1
Cadmium ND mg/L 07/01/23 07:10 7440-43-906/30/23 13:250.10 1
Chromium ND mg/L 07/01/23 07:10 7440-47-306/30/23 13:250.10 1
Copper ND mg/L 07/01/23 07:10 7440-50-806/30/23 13:250.20 1
Lead ND mg/L 07/01/23 07:10 7439-92-106/30/23 13:250.25 1
Nickel ND mg/L 07/01/23 07:10 7440-02-006/30/23 13:250.20 1
Selenium ND mg/L 07/01/23 07:10 7782-49-206/30/23 13:250.40 1
Silver ND mg/L 07/01/23 07:10 7440-22-406/30/23 13:250.10 1
Zinc ND mg/L 07/01/23 07:10 7440-66-606/30/23 13:250.20 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 06/29/23 17:43 Initial pH: 9.67; Final pH: 5.55
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury, TCLP
Mercury ND mg/L 07/03/23 12:07 7439-97-607/03/23 07:200.0050 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury ND mg/kg 06/30/23 12:04 7439-97-606/30/23 08:000.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Sample:S-2 Lab ID:92674134002 Collected:06/21/23 08:52 Received:06/22/23 09:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV MW PAH by SIM
Acenaphthene ND ug/kg 06/30/23 07:32 83-32-906/27/23 21:1212.4 1
Acenaphthylene ND ug/kg 06/30/23 07:32 208-96-806/27/23 21:1212.4 1
Anthracene ND ug/kg 06/30/23 07:32 120-12-706/27/23 21:1212.4 1
Benzo(a)anthracene ND ug/kg 06/30/23 07:32 56-55-306/27/23 21:1212.4 1
Benzo(a)pyrene ND ug/kg 06/30/23 07:32 50-32-806/27/23 21:1212.4 1
Benzo(b)fluoranthene ND ug/kg 06/30/23 07:32 205-99-206/27/23 21:1212.4 1
Benzo(g,h,i)perylene ND ug/kg 06/30/23 07:32 191-24-206/27/23 21:1212.4 1
Benzo(k)fluoranthene ND ug/kg 06/30/23 07:32 207-08-906/27/23 21:1212.4 1
Chrysene ND ug/kg 06/30/23 07:32 218-01-906/27/23 21:1212.4 1
Dibenz(a,h)anthracene ND ug/kg 06/30/23 07:32 53-70-306/27/23 21:1212.4 1
Fluoranthene ND ug/kg 06/30/23 07:32 206-44-006/27/23 21:1212.4 1
Fluorene ND ug/kg 06/30/23 07:32 86-73-706/27/23 21:1212.4 1
Indeno(1,2,3-cd)pyrene ND ug/kg 06/30/23 07:32 193-39-506/27/23 21:1212.4 1
1-Methylnaphthalene ND ug/kg 06/30/23 07:32 90-12-0 L206/27/23 21:1212.4 1
2-Methylnaphthalene ND ug/kg 06/30/23 07:32 91-57-606/27/23 21:1212.4 1
Naphthalene ND ug/kg 06/30/23 07:32 91-20-306/27/23 21:1212.4 1
Phenanthrene ND ug/kg 06/30/23 07:32 85-01-806/27/23 21:1212.4 1
Pyrene ND ug/kg 06/30/23 07:32 129-00-006/27/23 21:1212.4 1
Surrogates
2-Fluorobiphenyl (S)29 %06/30/23 07:32 321-60-806/27/23 21:1210-130 1
Nitrobenzene-d5 (S)45 %06/30/23 07:32 4165-60-006/27/23 21:1210-150 1
Terphenyl-d14 (S)48 %06/30/23 07:32 1718-51-006/27/23 21:1210-162 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.5 %06/22/23 17:41 N20.10 1
Analytical Method: EPA 7196A Preparation Method: EPA 7196A Modified
Pace Analytical Services - Asheville
7196 Chromium, Hexavalent
Chromium, Hexavalent ND mg/kg 06/27/23 21:23 18540-29-906/27/23 18:546.0 1
Analytical Method: EPA 7196A Leachate Method/Date: EPA 1312; 06/26/23 15:37
Pace Analytical Services - Asheville
7196 Chromium, Hex, SPLP
Chromium, Hexavalent ND mg/L 06/28/23 22:52 18540-29-9 H10.010 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Sample:S-3 Lab ID:92674134003 Collected:06/21/23 09:02 Received:06/22/23 09:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 06/28/23 13:00 12674-11-206/24/23 17:1542.0 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/28/23 13:00 11104-28-206/24/23 17:1542.0 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/28/23 13:00 11141-16-506/24/23 17:1542.0 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/28/23 13:00 53469-21-906/24/23 17:1542.0 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/28/23 13:00 12672-29-606/24/23 17:1542.0 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/28/23 13:00 11097-69-106/24/23 17:1542.0 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/28/23 13:00 11096-82-506/24/23 17:1542.0 1
Surrogates
Decachlorobiphenyl (S)51 %06/28/23 13:00 2051-24-306/24/23 17:1510-174 1
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 06/28/23 23:06 7440-38-206/24/23 12:203.6 1
Cadmium ND mg/kg 06/28/23 23:06 7440-43-906/24/23 12:201.2 1
Chromium 5.1 mg/kg 06/28/23 23:06 7440-47-306/24/23 12:201.2 1
Copper ND mg/kg 06/28/23 23:06 7440-50-806/24/23 12:204.8 1
Lead 4.3 mg/kg 06/28/23 23:06 7439-92-106/24/23 12:203.0 1
Nickel ND mg/kg 06/28/23 23:06 7440-02-006/24/23 12:202.4 1
Selenium ND mg/kg 06/28/23 23:06 7782-49-206/24/23 12:206.0 1
Silver ND mg/kg 06/28/23 23:06 7440-22-406/24/23 12:201.2 1
Zinc 4.5 mg/kg 06/28/23 23:06 7440-66-606/24/23 12:203.6 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 06/29/23 17:43 Initial pH: 9.48; Final pH: 5.41
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP, TCLP
Arsenic ND mg/L 07/01/23 07:15 7440-38-206/30/23 13:250.30 1
Cadmium ND mg/L 07/01/23 07:15 7440-43-906/30/23 13:250.10 1
Chromium ND mg/L 07/01/23 07:15 7440-47-306/30/23 13:250.10 1
Copper ND mg/L 07/01/23 07:15 7440-50-806/30/23 13:250.20 1
Lead ND mg/L 07/01/23 07:15 7439-92-106/30/23 13:250.25 1
Nickel ND mg/L 07/01/23 07:15 7440-02-006/30/23 13:250.20 1
Selenium ND mg/L 07/01/23 07:15 7782-49-206/30/23 13:250.40 1
Silver ND mg/L 07/01/23 07:15 7440-22-406/30/23 13:250.10 1
Zinc ND mg/L 07/01/23 07:15 7440-66-606/30/23 13:250.20 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 06/29/23 17:43 Initial pH: 9.48; Final pH: 5.41
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury, TCLP
Mercury ND mg/L 07/03/23 12:10 7439-97-607/03/23 07:200.0050 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury ND mg/kg 06/30/23 12:07 7439-97-606/30/23 08:000.30 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Sample:S-3 Lab ID:92674134003 Collected:06/21/23 09:02 Received:06/22/23 09:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV MW PAH by SIM
Acenaphthene ND ug/kg 06/30/23 07:51 83-32-906/27/23 21:1212.4 1
Acenaphthylene ND ug/kg 06/30/23 07:51 208-96-806/27/23 21:1212.4 1
Anthracene ND ug/kg 06/30/23 07:51 120-12-706/27/23 21:1212.4 1
Benzo(a)anthracene ND ug/kg 06/30/23 07:51 56-55-306/27/23 21:1212.4 1
Benzo(a)pyrene ND ug/kg 06/30/23 07:51 50-32-806/27/23 21:1212.4 1
Benzo(b)fluoranthene ND ug/kg 06/30/23 07:51 205-99-206/27/23 21:1212.4 1
Benzo(g,h,i)perylene ND ug/kg 06/30/23 07:51 191-24-206/27/23 21:1212.4 1
Benzo(k)fluoranthene ND ug/kg 06/30/23 07:51 207-08-906/27/23 21:1212.4 1
Chrysene ND ug/kg 06/30/23 07:51 218-01-906/27/23 21:1212.4 1
Dibenz(a,h)anthracene ND ug/kg 06/30/23 07:51 53-70-306/27/23 21:1212.4 1
Fluoranthene ND ug/kg 06/30/23 07:51 206-44-006/27/23 21:1212.4 1
Fluorene ND ug/kg 06/30/23 07:51 86-73-706/27/23 21:1212.4 1
Indeno(1,2,3-cd)pyrene ND ug/kg 06/30/23 07:51 193-39-506/27/23 21:1212.4 1
1-Methylnaphthalene ND ug/kg 06/30/23 07:51 90-12-0 L206/27/23 21:1212.4 1
2-Methylnaphthalene ND ug/kg 06/30/23 07:51 91-57-606/27/23 21:1212.4 1
Naphthalene ND ug/kg 06/30/23 07:51 91-20-306/27/23 21:1212.4 1
Phenanthrene ND ug/kg 06/30/23 07:51 85-01-806/27/23 21:1212.4 1
Pyrene ND ug/kg 06/30/23 07:51 129-00-006/27/23 21:1212.4 1
Surrogates
2-Fluorobiphenyl (S)24 %06/30/23 07:51 321-60-806/27/23 21:1210-130 1
Nitrobenzene-d5 (S)44 %06/30/23 07:51 4165-60-006/27/23 21:1210-150 1
Terphenyl-d14 (S)43 %06/30/23 07:51 1718-51-006/27/23 21:1210-162 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.2 %06/22/23 17:41 N20.10 1
Analytical Method: EPA 7196A Preparation Method: EPA 7196A Modified
Pace Analytical Services - Asheville
7196 Chromium, Hexavalent
Chromium, Hexavalent ND mg/kg 06/27/23 21:23 18540-29-906/27/23 18:546.0 1
Analytical Method: EPA 7196A Leachate Method/Date: EPA 1312; 06/26/23 15:37
Pace Analytical Services - Asheville
7196 Chromium, Hex, SPLP
Chromium, Hexavalent ND mg/L 06/28/23 22:52 18540-29-9 H10.010 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Sample:S-4 Lab ID:92674134004 Collected:06/21/23 09:12 Received:06/22/23 09:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 06/28/23 13:13 12674-11-206/24/23 17:1552.4 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/28/23 13:13 11104-28-206/24/23 17:1552.4 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/28/23 13:13 11141-16-506/24/23 17:1552.4 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/28/23 13:13 53469-21-906/24/23 17:1552.4 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/28/23 13:13 12672-29-606/24/23 17:1552.4 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/28/23 13:13 11097-69-106/24/23 17:1552.4 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/28/23 13:13 11096-82-506/24/23 17:1552.4 1
Surrogates
Decachlorobiphenyl (S)56 %06/28/23 13:13 2051-24-306/24/23 17:1510-174 1
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 06/28/23 23:25 7440-38-206/24/23 12:204.4 1
Cadmium ND mg/kg 06/28/23 23:25 7440-43-906/24/23 12:201.5 1
Chromium 5.5 mg/kg 06/28/23 23:25 7440-47-306/24/23 12:201.5 1
Copper 78.4 mg/kg 06/28/23 23:25 7440-50-806/24/23 12:205.9 1
Lead 8.3 mg/kg 06/28/23 23:25 7439-92-106/24/23 12:203.7 1
Nickel 3.0 mg/kg 06/28/23 23:25 7440-02-006/24/23 12:203.0 1
Selenium ND mg/kg 06/28/23 23:25 7782-49-206/24/23 12:207.4 1
Silver ND mg/kg 06/28/23 23:25 7440-22-406/24/23 12:201.5 1
Zinc 51.5 mg/kg 06/28/23 23:25 7440-66-606/24/23 12:204.4 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 06/29/23 17:43 Initial pH: 9.27; Final pH: 5.37
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP, TCLP
Arsenic ND mg/L 07/01/23 07:29 7440-38-206/30/23 13:250.30 1
Cadmium ND mg/L 07/01/23 07:29 7440-43-906/30/23 13:250.10 1
Chromium ND mg/L 07/01/23 07:29 7440-47-306/30/23 13:250.10 1
Copper ND mg/L 07/01/23 07:29 7440-50-806/30/23 13:250.20 1
Lead ND mg/L 07/01/23 07:29 7439-92-106/30/23 13:250.25 1
Nickel ND mg/L 07/01/23 07:29 7440-02-006/30/23 13:250.20 1
Selenium ND mg/L 07/01/23 07:29 7782-49-206/30/23 13:250.40 1
Silver ND mg/L 07/01/23 07:29 7440-22-406/30/23 13:250.10 1
Zinc 0.34 mg/L 07/01/23 07:29 7440-66-606/30/23 13:250.20 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 06/29/23 17:43 Initial pH: 9.27; Final pH: 5.37
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury, TCLP
Mercury ND mg/L 07/03/23 12:13 7439-97-607/03/23 07:200.0050 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury ND mg/kg 06/30/23 12:09 7439-97-606/30/23 08:000.38 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Sample:S-4 Lab ID:92674134004 Collected:06/21/23 09:12 Received:06/22/23 09:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV MW PAH by SIM
Acenaphthene ND ug/kg 06/30/23 08:10 83-32-906/27/23 21:1216.0 1
Acenaphthylene ND ug/kg 06/30/23 08:10 208-96-806/27/23 21:1216.0 1
Anthracene ND ug/kg 06/30/23 08:10 120-12-706/27/23 21:1216.0 1
Benzo(a)anthracene ND ug/kg 06/30/23 08:10 56-55-306/27/23 21:1216.0 1
Benzo(a)pyrene ND ug/kg 06/30/23 08:10 50-32-806/27/23 21:1216.0 1
Benzo(b)fluoranthene ND ug/kg 06/30/23 08:10 205-99-206/27/23 21:1216.0 1
Benzo(g,h,i)perylene ND ug/kg 06/30/23 08:10 191-24-206/27/23 21:1216.0 1
Benzo(k)fluoranthene ND ug/kg 06/30/23 08:10 207-08-906/27/23 21:1216.0 1
Chrysene ND ug/kg 06/30/23 08:10 218-01-906/27/23 21:1216.0 1
Dibenz(a,h)anthracene ND ug/kg 06/30/23 08:10 53-70-306/27/23 21:1216.0 1
Fluoranthene ND ug/kg 06/30/23 08:10 206-44-006/27/23 21:1216.0 1
Fluorene ND ug/kg 06/30/23 08:10 86-73-706/27/23 21:1216.0 1
Indeno(1,2,3-cd)pyrene ND ug/kg 06/30/23 08:10 193-39-506/27/23 21:1216.0 1
1-Methylnaphthalene ND ug/kg 06/30/23 08:10 90-12-0 L206/27/23 21:1216.0 1
2-Methylnaphthalene ND ug/kg 06/30/23 08:10 91-57-606/27/23 21:1216.0 1
Naphthalene ND ug/kg 06/30/23 08:10 91-20-306/27/23 21:1216.0 1
Phenanthrene ND ug/kg 06/30/23 08:10 85-01-806/27/23 21:1216.0 1
Pyrene ND ug/kg 06/30/23 08:10 129-00-006/27/23 21:1216.0 1
Surrogates
2-Fluorobiphenyl (S)46 %06/30/23 08:10 321-60-806/27/23 21:1210-130 1
Nitrobenzene-d5 (S)60 %06/30/23 08:10 4165-60-006/27/23 21:1210-150 1
Terphenyl-d14 (S)45 %06/30/23 08:10 1718-51-006/27/23 21:1210-162 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 37.3 %06/23/23 13:43 N20.10 1
Analytical Method: EPA 7196A Preparation Method: EPA 7196A Modified
Pace Analytical Services - Asheville
7196 Chromium, Hexavalent
Chromium, Hexavalent ND mg/kg 06/27/23 21:24 18540-29-906/27/23 18:547.5 1
Analytical Method: EPA 7196A Leachate Method/Date: EPA 1312; 06/26/23 15:37
Pace Analytical Services - Asheville
7196 Chromium, Hex, SPLP
Chromium, Hexavalent ND mg/L 06/28/23 22:53 18540-29-9 H10.010 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Sample:S-5 Lab ID:92674134005 Collected:06/21/23 09:26 Received:06/22/23 09:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 06/28/23 13:26 12674-11-206/24/23 17:1543.1 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/28/23 13:26 11104-28-206/24/23 17:1543.1 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/28/23 13:26 11141-16-506/24/23 17:1543.1 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/28/23 13:26 53469-21-906/24/23 17:1543.1 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/28/23 13:26 12672-29-606/24/23 17:1543.1 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/28/23 13:26 11097-69-106/24/23 17:1543.1 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/28/23 13:26 11096-82-506/24/23 17:1543.1 1
Surrogates
Decachlorobiphenyl (S)58 %06/28/23 13:26 2051-24-306/24/23 17:1510-174 1
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 06/28/23 23:35 7440-38-206/24/23 12:203.5 1
Cadmium ND mg/kg 06/28/23 23:35 7440-43-906/24/23 12:201.2 1
Chromium 14.2 mg/kg 06/28/23 23:35 7440-47-306/24/23 12:201.2 1
Copper ND mg/kg 06/28/23 23:35 7440-50-806/24/23 12:204.7 1
Lead 10.5 mg/kg 06/28/23 23:35 7439-92-106/24/23 12:202.9 1
Nickel 4.1 mg/kg 06/28/23 23:35 7440-02-006/24/23 12:202.3 1
Selenium ND mg/kg 06/28/23 23:40 7782-49-2 D306/24/23 12:2029.3 5
Silver ND mg/kg 06/28/23 23:35 7440-22-406/24/23 12:201.2 1
Zinc 8.5 mg/kg 06/28/23 23:35 7440-66-606/24/23 12:203.5 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 06/29/23 17:43 Initial pH: 9.36; Final pH: 5.38
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP, TCLP
Arsenic ND mg/L 07/01/23 07:34 7440-38-206/30/23 13:250.30 1
Cadmium ND mg/L 07/01/23 07:34 7440-43-906/30/23 13:250.10 1
Chromium ND mg/L 07/01/23 07:34 7440-47-306/30/23 13:250.10 1
Copper ND mg/L 07/01/23 07:34 7440-50-806/30/23 13:250.20 1
Lead ND mg/L 07/01/23 07:34 7439-92-106/30/23 13:250.25 1
Nickel ND mg/L 07/01/23 07:34 7440-02-006/30/23 13:250.20 1
Selenium ND mg/L 07/01/23 07:34 7782-49-206/30/23 13:250.40 1
Silver ND mg/L 07/01/23 07:34 7440-22-406/30/23 13:250.10 1
Zinc ND mg/L 07/01/23 07:34 7440-66-606/30/23 13:250.20 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 06/29/23 17:43 Initial pH: 9.36; Final pH: 5.38
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury, TCLP
Mercury ND mg/L 07/03/23 12:42 7439-97-607/03/23 07:200.0050 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury ND mg/kg 06/30/23 12:17 7439-97-606/30/23 08:000.29 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Sample:S-5 Lab ID:92674134005 Collected:06/21/23 09:26 Received:06/22/23 09:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV MW PAH by SIM
Acenaphthene ND ug/kg 06/30/23 08:30 83-32-906/27/23 21:1213.0 1
Acenaphthylene ND ug/kg 06/30/23 08:30 208-96-806/27/23 21:1213.0 1
Anthracene ND ug/kg 06/30/23 08:30 120-12-706/27/23 21:1213.0 1
Benzo(a)anthracene ND ug/kg 06/30/23 08:30 56-55-306/27/23 21:1213.0 1
Benzo(a)pyrene ND ug/kg 06/30/23 08:30 50-32-806/27/23 21:1213.0 1
Benzo(b)fluoranthene ND ug/kg 06/30/23 08:30 205-99-206/27/23 21:1213.0 1
Benzo(g,h,i)perylene ND ug/kg 06/30/23 08:30 191-24-206/27/23 21:1213.0 1
Benzo(k)fluoranthene ND ug/kg 06/30/23 08:30 207-08-906/27/23 21:1213.0 1
Chrysene ND ug/kg 06/30/23 08:30 218-01-906/27/23 21:1213.0 1
Dibenz(a,h)anthracene ND ug/kg 06/30/23 08:30 53-70-306/27/23 21:1213.0 1
Fluoranthene ND ug/kg 06/30/23 08:30 206-44-006/27/23 21:1213.0 1
Fluorene ND ug/kg 06/30/23 08:30 86-73-706/27/23 21:1213.0 1
Indeno(1,2,3-cd)pyrene ND ug/kg 06/30/23 08:30 193-39-506/27/23 21:1213.0 1
1-Methylnaphthalene ND ug/kg 06/30/23 08:30 90-12-0 L206/27/23 21:1213.0 1
2-Methylnaphthalene ND ug/kg 06/30/23 08:30 91-57-606/27/23 21:1213.0 1
Naphthalene ND ug/kg 06/30/23 08:30 91-20-306/27/23 21:1213.0 1
Phenanthrene ND ug/kg 06/30/23 08:30 85-01-806/27/23 21:1213.0 1
Pyrene ND ug/kg 06/30/23 08:30 129-00-006/27/23 21:1213.0 1
Surrogates
2-Fluorobiphenyl (S)51 %06/30/23 08:30 321-60-806/27/23 21:1210-130 1
Nitrobenzene-d5 (S)61 %06/30/23 08:30 4165-60-006/27/23 21:1210-150 1
Terphenyl-d14 (S)64 %06/30/23 08:30 1718-51-006/27/23 21:1210-162 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.5 %06/23/23 13:43 N20.10 1
Analytical Method: EPA 7196A Preparation Method: EPA 7196A Modified
Pace Analytical Services - Asheville
7196 Chromium, Hexavalent
Chromium, Hexavalent ND mg/kg 06/27/23 21:24 18540-29-906/27/23 18:546.0 1
Analytical Method: EPA 7196A Leachate Method/Date: EPA 1312; 06/26/23 15:37
Pace Analytical Services - Asheville
7196 Chromium, Hex, SPLP
Chromium, Hexavalent ND mg/L 06/28/23 22:53 18540-29-9 H10.010 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Sample:S-6 Lab ID:92674134006 Collected:06/21/23 09:38 Received:06/22/23 09:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 06/28/23 13:40 12674-11-206/24/23 17:1539.5 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/28/23 13:40 11104-28-206/24/23 17:1539.5 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/28/23 13:40 11141-16-506/24/23 17:1539.5 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/28/23 13:40 53469-21-906/24/23 17:1539.5 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/28/23 13:40 12672-29-606/24/23 17:1539.5 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/28/23 13:40 11097-69-106/24/23 17:1539.5 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/28/23 13:40 11096-82-506/24/23 17:1539.5 1
Surrogates
Decachlorobiphenyl (S)60 %06/28/23 13:40 2051-24-306/24/23 17:1510-174 1
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 06/28/23 23:44 7440-38-206/24/23 12:203.6 1
Cadmium ND mg/kg 06/28/23 23:44 7440-43-906/24/23 12:201.2 1
Chromium 7.5 mg/kg 06/28/23 23:44 7440-47-306/24/23 12:201.2 1
Copper 7.4 mg/kg 06/28/23 23:44 7440-50-806/24/23 12:204.8 1
Lead 17.8 mg/kg 06/28/23 23:44 7439-92-106/24/23 12:203.0 1
Nickel 5.8 mg/kg 06/28/23 23:44 7440-02-006/24/23 12:202.4 1
Selenium ND mg/kg 06/28/23 23:44 7782-49-206/24/23 12:206.0 1
Silver ND mg/kg 06/28/23 23:44 7440-22-406/24/23 12:201.2 1
Zinc 20.7 mg/kg 06/28/23 23:44 7440-66-606/24/23 12:203.6 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 06/29/23 17:43 Initial pH: 9.52; Final pH: 5.61
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP, TCLP
Arsenic ND mg/L 07/01/23 07:39 7440-38-206/30/23 13:250.30 1
Cadmium ND mg/L 07/01/23 07:39 7440-43-906/30/23 13:250.10 1
Chromium ND mg/L 07/01/23 07:39 7440-47-306/30/23 13:250.10 1
Copper ND mg/L 07/01/23 07:39 7440-50-806/30/23 13:250.20 1
Lead ND mg/L 07/01/23 07:39 7439-92-106/30/23 13:250.25 1
Nickel ND mg/L 07/01/23 07:39 7440-02-006/30/23 13:250.20 1
Selenium ND mg/L 07/01/23 07:39 7782-49-206/30/23 13:250.40 1
Silver ND mg/L 07/01/23 07:39 7440-22-406/30/23 13:250.10 1
Zinc ND mg/L 07/01/23 07:39 7440-66-606/30/23 13:250.20 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 06/29/23 17:43 Initial pH: 9.52; Final pH: 5.61
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury, TCLP
Mercury ND mg/L 07/03/23 12:44 7439-97-607/03/23 07:200.0050 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury ND mg/kg 06/30/23 12:20 7439-97-606/30/23 08:000.28 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Sample:S-6 Lab ID:92674134006 Collected:06/21/23 09:38 Received:06/22/23 09:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV MW PAH by SIM
Acenaphthene ND ug/kg 06/30/23 08:49 83-32-906/27/23 21:1212.2 1
Acenaphthylene ND ug/kg 06/30/23 08:49 208-96-806/27/23 21:1212.2 1
Anthracene ND ug/kg 06/30/23 08:49 120-12-706/27/23 21:1212.2 1
Benzo(a)anthracene ND ug/kg 06/30/23 08:49 56-55-306/27/23 21:1212.2 1
Benzo(a)pyrene ND ug/kg 06/30/23 08:49 50-32-806/27/23 21:1212.2 1
Benzo(b)fluoranthene ND ug/kg 06/30/23 08:49 205-99-206/27/23 21:1212.2 1
Benzo(g,h,i)perylene ND ug/kg 06/30/23 08:49 191-24-206/27/23 21:1212.2 1
Benzo(k)fluoranthene ND ug/kg 06/30/23 08:49 207-08-906/27/23 21:1212.2 1
Chrysene ND ug/kg 06/30/23 08:49 218-01-906/27/23 21:1212.2 1
Dibenz(a,h)anthracene ND ug/kg 06/30/23 08:49 53-70-306/27/23 21:1212.2 1
Fluoranthene ND ug/kg 06/30/23 08:49 206-44-006/27/23 21:1212.2 1
Fluorene ND ug/kg 06/30/23 08:49 86-73-706/27/23 21:1212.2 1
Indeno(1,2,3-cd)pyrene ND ug/kg 06/30/23 08:49 193-39-506/27/23 21:1212.2 1
1-Methylnaphthalene ND ug/kg 06/30/23 08:49 90-12-0 L206/27/23 21:1212.2 1
2-Methylnaphthalene ND ug/kg 06/30/23 08:49 91-57-606/27/23 21:1212.2 1
Naphthalene ND ug/kg 06/30/23 08:49 91-20-306/27/23 21:1212.2 1
Phenanthrene ND ug/kg 06/30/23 08:49 85-01-806/27/23 21:1212.2 1
Pyrene ND ug/kg 06/30/23 08:49 129-00-006/27/23 21:1212.2 1
Surrogates
2-Fluorobiphenyl (S)40 %06/30/23 08:49 321-60-806/27/23 21:1210-130 1
Nitrobenzene-d5 (S)50 %06/30/23 08:49 4165-60-006/27/23 21:1210-150 1
Terphenyl-d14 (S)52 %06/30/23 08:49 1718-51-006/27/23 21:1210-162 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.2 %06/23/23 13:43 N20.10 1
Analytical Method: EPA 7196A Preparation Method: EPA 7196A Modified
Pace Analytical Services - Asheville
7196 Chromium, Hexavalent
Chromium, Hexavalent ND mg/kg 06/27/23 21:27 18540-29-906/27/23 18:545.7 1
Analytical Method: EPA 7196A Leachate Method/Date: EPA 1312; 06/26/23 15:37
Pace Analytical Services - Asheville
7196 Chromium, Hex, SPLP
Chromium, Hexavalent ND mg/L 06/28/23 22:53 18540-29-9 H10.010 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Sample:S-7 Lab ID:92674134007 Collected:06/21/23 09:59 Received:06/22/23 09:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 06/28/23 13:53 12674-11-206/24/23 17:1546.4 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/28/23 13:53 11104-28-206/24/23 17:1546.4 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/28/23 13:53 11141-16-506/24/23 17:1546.4 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/28/23 13:53 53469-21-906/24/23 17:1546.4 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/28/23 13:53 12672-29-606/24/23 17:1546.4 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/28/23 13:53 11097-69-106/24/23 17:1546.4 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/28/23 13:53 11096-82-506/24/23 17:1546.4 1
Surrogates
Decachlorobiphenyl (S)60 %06/28/23 13:53 2051-24-306/24/23 17:1510-174 1
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic 6.3 mg/kg 06/28/23 23:54 7440-38-206/24/23 12:204.0 1
Cadmium ND mg/kg 06/28/23 23:54 7440-43-906/24/23 12:201.3 1
Chromium 9.9 mg/kg 06/28/23 23:54 7440-47-306/24/23 12:201.3 1
Copper 8.9 mg/kg 06/28/23 23:54 7440-50-806/24/23 12:205.3 1
Lead 8.0 mg/kg 06/28/23 23:54 7439-92-106/24/23 12:203.3 1
Nickel ND mg/kg 06/28/23 23:54 7440-02-006/24/23 12:202.7 1
Selenium ND mg/kg 06/28/23 23:59 7782-49-2 D306/24/23 12:2033.4 5
Silver ND mg/kg 06/28/23 23:54 7440-22-406/24/23 12:201.3 1
Zinc 10.6 mg/kg 06/28/23 23:54 7440-66-606/24/23 12:204.0 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 06/29/23 17:43 Initial pH: 9.4; Final pH: 5.32
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP, TCLP
Arsenic ND mg/L 07/01/23 07:44 7440-38-206/30/23 13:250.30 1
Cadmium ND mg/L 07/01/23 07:44 7440-43-906/30/23 13:250.10 1
Chromium ND mg/L 07/01/23 07:44 7440-47-306/30/23 13:250.10 1
Copper ND mg/L 07/01/23 07:44 7440-50-806/30/23 13:250.20 1
Lead ND mg/L 07/01/23 07:44 7439-92-106/30/23 13:250.25 1
Nickel ND mg/L 07/01/23 07:44 7440-02-006/30/23 13:250.20 1
Selenium ND mg/L 07/01/23 07:44 7782-49-206/30/23 13:250.40 1
Silver ND mg/L 07/01/23 07:44 7440-22-406/30/23 13:250.10 1
Zinc ND mg/L 07/01/23 07:44 7440-66-606/30/23 13:250.20 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 06/29/23 17:43 Initial pH: 9.4; Final pH: 5.32
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury, TCLP
Mercury ND mg/L 07/03/23 12:47 7439-97-607/03/23 07:200.0050 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury ND mg/kg 06/30/23 12:22 7439-97-606/30/23 08:000.32 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Sample:S-7 Lab ID:92674134007 Collected:06/21/23 09:59 Received:06/22/23 09:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV MW PAH by SIM
Acenaphthene ND ug/kg 06/30/23 09:08 83-32-906/27/23 21:1214.0 1
Acenaphthylene ND ug/kg 06/30/23 09:08 208-96-806/27/23 21:1214.0 1
Anthracene ND ug/kg 06/30/23 09:08 120-12-706/27/23 21:1214.0 1
Benzo(a)anthracene ND ug/kg 06/30/23 09:08 56-55-306/27/23 21:1214.0 1
Benzo(a)pyrene ND ug/kg 06/30/23 09:08 50-32-806/27/23 21:1214.0 1
Benzo(b)fluoranthene ND ug/kg 06/30/23 09:08 205-99-206/27/23 21:1214.0 1
Benzo(g,h,i)perylene ND ug/kg 06/30/23 09:08 191-24-206/27/23 21:1214.0 1
Benzo(k)fluoranthene ND ug/kg 06/30/23 09:08 207-08-906/27/23 21:1214.0 1
Chrysene ND ug/kg 06/30/23 09:08 218-01-906/27/23 21:1214.0 1
Dibenz(a,h)anthracene ND ug/kg 06/30/23 09:08 53-70-306/27/23 21:1214.0 1
Fluoranthene ND ug/kg 06/30/23 09:08 206-44-006/27/23 21:1214.0 1
Fluorene ND ug/kg 06/30/23 09:08 86-73-706/27/23 21:1214.0 1
Indeno(1,2,3-cd)pyrene ND ug/kg 06/30/23 09:08 193-39-506/27/23 21:1214.0 1
1-Methylnaphthalene ND ug/kg 06/30/23 09:08 90-12-0 L206/27/23 21:1214.0 1
2-Methylnaphthalene ND ug/kg 06/30/23 09:08 91-57-606/27/23 21:1214.0 1
Naphthalene ND ug/kg 06/30/23 09:08 91-20-306/27/23 21:1214.0 1
Phenanthrene ND ug/kg 06/30/23 09:08 85-01-806/27/23 21:1214.0 1
Pyrene ND ug/kg 06/30/23 09:08 129-00-006/27/23 21:1214.0 1
Surrogates
2-Fluorobiphenyl (S)46 %06/30/23 09:08 321-60-806/27/23 21:1210-130 1
Nitrobenzene-d5 (S)56 %06/30/23 09:08 4165-60-006/27/23 21:1210-150 1
Terphenyl-d14 (S)56 %06/30/23 09:08 1718-51-006/27/23 21:1210-162 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 29.3 %06/23/23 13:43 N20.10 1
Analytical Method: EPA 7196A Preparation Method: EPA 7196A Modified
Pace Analytical Services - Asheville
7196 Chromium, Hexavalent
Chromium, Hexavalent ND mg/kg 06/27/23 21:28 18540-29-906/27/23 18:546.0 1
Analytical Method: EPA 7196A Leachate Method/Date: EPA 1312; 06/26/23 15:37
Pace Analytical Services - Asheville
7196 Chromium, Hex, SPLP
Chromium, Hexavalent ND mg/L 06/28/23 22:57 18540-29-9 H10.010 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Sample:S-8 Lab ID:92674134008 Collected:06/21/23 10:18 Received:06/22/23 09:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 06/26/23 21:22 12674-11-206/26/23 10:1342.2 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/26/23 21:22 11104-28-206/26/23 10:1342.2 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/26/23 21:22 11141-16-506/26/23 10:1342.2 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/26/23 21:22 53469-21-906/26/23 10:1342.2 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/26/23 21:22 12672-29-606/26/23 10:1342.2 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/26/23 21:22 11097-69-106/26/23 10:1342.2 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/26/23 21:22 11096-82-506/26/23 10:1342.2 1
Surrogates
Decachlorobiphenyl (S)24 %06/26/23 21:22 2051-24-306/26/23 10:1310-174 1
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic ND mg/kg 06/29/23 00:04 7440-38-206/24/23 12:203.5 1
Cadmium ND mg/kg 06/29/23 00:04 7440-43-906/24/23 12:201.2 1
Chromium 3.3 mg/kg 06/29/23 00:04 7440-47-306/24/23 12:201.2 1
Copper ND mg/kg 06/29/23 00:04 7440-50-806/24/23 12:204.6 1
Lead 3.4 mg/kg 06/29/23 00:04 7439-92-106/24/23 12:202.9 1
Nickel ND mg/kg 06/29/23 00:04 7440-02-006/24/23 12:202.3 1
Selenium ND mg/kg 06/29/23 00:04 7782-49-206/24/23 12:205.8 1
Silver ND mg/kg 06/29/23 00:04 7440-22-406/24/23 12:201.2 1
Zinc ND mg/kg 06/29/23 00:04 7440-66-606/24/23 12:203.5 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 06/29/23 17:43 Initial pH: 9.32; Final pH: 5.44
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP, TCLP
Arsenic ND mg/L 07/01/23 07:49 7440-38-206/30/23 13:250.30 1
Cadmium ND mg/L 07/01/23 07:49 7440-43-906/30/23 13:250.10 1
Chromium ND mg/L 07/01/23 07:49 7440-47-306/30/23 13:250.10 1
Copper ND mg/L 07/01/23 07:49 7440-50-806/30/23 13:250.20 1
Lead ND mg/L 07/01/23 07:49 7439-92-106/30/23 13:250.25 1
Nickel ND mg/L 07/01/23 07:49 7440-02-006/30/23 13:250.20 1
Selenium ND mg/L 07/01/23 07:49 7782-49-206/30/23 13:250.40 1
Silver ND mg/L 07/01/23 07:49 7440-22-406/30/23 13:250.10 1
Zinc ND mg/L 07/01/23 07:49 7440-66-606/30/23 13:250.20 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 06/29/23 17:43 Initial pH: 9.32; Final pH: 5.44
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury, TCLP
Mercury ND mg/L 07/03/23 12:50 7439-97-607/03/23 07:200.0050 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury ND mg/kg 06/30/23 12:25 7439-97-606/30/23 08:000.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Sample:S-8 Lab ID:92674134008 Collected:06/21/23 10:18 Received:06/22/23 09:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV MW PAH by SIM
Acenaphthene ND ug/kg 06/30/23 09:28 83-32-906/27/23 21:1212.6 1
Acenaphthylene ND ug/kg 06/30/23 09:28 208-96-806/27/23 21:1212.6 1
Anthracene ND ug/kg 06/30/23 09:28 120-12-706/27/23 21:1212.6 1
Benzo(a)anthracene ND ug/kg 06/30/23 09:28 56-55-306/27/23 21:1212.6 1
Benzo(a)pyrene ND ug/kg 06/30/23 09:28 50-32-806/27/23 21:1212.6 1
Benzo(b)fluoranthene ND ug/kg 06/30/23 09:28 205-99-206/27/23 21:1212.6 1
Benzo(g,h,i)perylene ND ug/kg 06/30/23 09:28 191-24-206/27/23 21:1212.6 1
Benzo(k)fluoranthene ND ug/kg 06/30/23 09:28 207-08-906/27/23 21:1212.6 1
Chrysene ND ug/kg 06/30/23 09:28 218-01-906/27/23 21:1212.6 1
Dibenz(a,h)anthracene ND ug/kg 06/30/23 09:28 53-70-306/27/23 21:1212.6 1
Fluoranthene ND ug/kg 06/30/23 09:28 206-44-006/27/23 21:1212.6 1
Fluorene ND ug/kg 06/30/23 09:28 86-73-706/27/23 21:1212.6 1
Indeno(1,2,3-cd)pyrene ND ug/kg 06/30/23 09:28 193-39-506/27/23 21:1212.6 1
1-Methylnaphthalene ND ug/kg 06/30/23 09:28 90-12-0 L206/27/23 21:1212.6 1
2-Methylnaphthalene ND ug/kg 06/30/23 09:28 91-57-606/27/23 21:1212.6 1
Naphthalene ND ug/kg 06/30/23 09:28 91-20-306/27/23 21:1212.6 1
Phenanthrene ND ug/kg 06/30/23 09:28 85-01-806/27/23 21:1212.6 1
Pyrene ND ug/kg 06/30/23 09:28 129-00-006/27/23 21:1212.6 1
Surrogates
2-Fluorobiphenyl (S)46 %06/30/23 09:28 321-60-806/27/23 21:1210-130 1
Nitrobenzene-d5 (S)57 %06/30/23 09:28 4165-60-006/27/23 21:1210-150 1
Terphenyl-d14 (S)49 %06/30/23 09:28 1718-51-006/27/23 21:1210-162 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.2 %06/23/23 13:43 N20.10 1
Analytical Method: EPA 7196A Preparation Method: EPA 7196A Modified
Pace Analytical Services - Asheville
7196 Chromium, Hexavalent
Chromium, Hexavalent ND mg/kg 06/27/23 21:28 18540-29-906/27/23 18:545.2 1
Analytical Method: EPA 7196A Leachate Method/Date: EPA 1312; 06/26/23 15:37
Pace Analytical Services - Asheville
7196 Chromium, Hex, SPLP
Chromium, Hexavalent ND mg/L 06/28/23 22:57 18540-29-9 H10.010 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Sample:S-9 Lab ID:92674134009 Collected:06/21/23 10:34 Received:06/22/23 09:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8082A Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8082 GCS PCB
PCB-1016 (Aroclor 1016)ND ug/kg 06/26/23 21:44 12674-11-206/26/23 10:1339.7 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/26/23 21:44 11104-28-206/26/23 10:1339.7 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/26/23 21:44 11141-16-506/26/23 10:1339.7 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/26/23 21:44 53469-21-906/26/23 10:1339.7 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/26/23 21:44 12672-29-606/26/23 10:1339.7 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/26/23 21:44 11097-69-106/26/23 10:1339.7 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/26/23 21:44 11096-82-506/26/23 10:1339.7 1
Surrogates
Decachlorobiphenyl (S)56 %06/26/23 21:44 2051-24-306/26/23 10:1310-174 1
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP
Arsenic 4.4 mg/kg 06/29/23 00:23 7440-38-206/24/23 12:203.3 1
Cadmium ND mg/kg 06/29/23 00:23 7440-43-906/24/23 12:201.1 1
Chromium 4.6 mg/kg 06/29/23 00:23 7440-47-306/24/23 12:201.1 1
Copper ND mg/kg 06/29/23 00:23 7440-50-806/24/23 12:204.4 1
Lead 4.4 mg/kg 06/29/23 00:23 7439-92-106/24/23 12:202.8 1
Nickel ND mg/kg 06/29/23 00:23 7440-02-006/24/23 12:202.2 1
Selenium ND mg/kg 06/29/23 00:23 7782-49-206/24/23 12:205.5 1
Silver ND mg/kg 06/29/23 00:23 7440-22-406/24/23 12:201.1 1
Zinc ND mg/kg 06/29/23 00:23 7440-66-606/24/23 12:203.3 1
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Leachate Method/Date: EPA 1311; 06/29/23 17:43 Initial pH: 9.77; Final pH: 5.45
Pace Analytical Services - Peachtree Corners, GA
6010D ATL ICP, TCLP
Arsenic ND mg/L 07/01/23 07:54 7440-38-206/30/23 13:250.30 1
Cadmium ND mg/L 07/01/23 07:54 7440-43-906/30/23 13:250.10 1
Chromium ND mg/L 07/01/23 07:54 7440-47-306/30/23 13:250.10 1
Copper ND mg/L 07/01/23 07:54 7440-50-806/30/23 13:250.20 1
Lead ND mg/L 07/01/23 07:54 7439-92-106/30/23 13:250.25 1
Nickel ND mg/L 07/01/23 07:54 7440-02-006/30/23 13:250.20 1
Selenium ND mg/L 07/01/23 07:54 7782-49-206/30/23 13:250.40 1
Silver ND mg/L 07/01/23 07:54 7440-22-406/30/23 13:250.10 1
Zinc ND mg/L 07/01/23 07:54 7440-66-606/30/23 13:250.20 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Leachate Method/Date: EPA 1311; 06/29/23 17:43 Initial pH: 9.77; Final pH: 5.45
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury, TCLP
Mercury ND mg/L 07/03/23 12:52 7439-97-607/03/23 07:200.0050 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Peachtree Corners, GA
7471 Mercury
Mercury ND mg/kg 06/30/23 12:28 7439-97-606/30/23 08:000.29 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 43
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Sample:S-9 Lab ID:92674134009 Collected:06/21/23 10:34 Received:06/22/23 09:35 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV MW PAH by SIM
Acenaphthene ND ug/kg 06/30/23 09:47 83-32-906/27/23 21:1211.9 1
Acenaphthylene ND ug/kg 06/30/23 09:47 208-96-806/27/23 21:1211.9 1
Anthracene ND ug/kg 06/30/23 09:47 120-12-706/27/23 21:1211.9 1
Benzo(a)anthracene ND ug/kg 06/30/23 09:47 56-55-306/27/23 21:1211.9 1
Benzo(a)pyrene ND ug/kg 06/30/23 09:47 50-32-806/27/23 21:1211.9 1
Benzo(b)fluoranthene ND ug/kg 06/30/23 09:47 205-99-206/27/23 21:1211.9 1
Benzo(g,h,i)perylene ND ug/kg 06/30/23 09:47 191-24-206/27/23 21:1211.9 1
Benzo(k)fluoranthene ND ug/kg 06/30/23 09:47 207-08-906/27/23 21:1211.9 1
Chrysene ND ug/kg 06/30/23 09:47 218-01-906/27/23 21:1211.9 1
Dibenz(a,h)anthracene ND ug/kg 06/30/23 09:47 53-70-306/27/23 21:1211.9 1
Fluoranthene ND ug/kg 06/30/23 09:47 206-44-006/27/23 21:1211.9 1
Fluorene ND ug/kg 06/30/23 09:47 86-73-706/27/23 21:1211.9 1
Indeno(1,2,3-cd)pyrene ND ug/kg 06/30/23 09:47 193-39-506/27/23 21:1211.9 1
1-Methylnaphthalene ND ug/kg 06/30/23 09:47 90-12-0 L206/27/23 21:1211.9 1
2-Methylnaphthalene ND ug/kg 06/30/23 09:47 91-57-606/27/23 21:1211.9 1
Naphthalene ND ug/kg 06/30/23 09:47 91-20-306/27/23 21:1211.9 1
Phenanthrene ND ug/kg 06/30/23 09:47 85-01-806/27/23 21:1211.9 1
Pyrene ND ug/kg 06/30/23 09:47 129-00-006/27/23 21:1211.9 1
Surrogates
2-Fluorobiphenyl (S)40 %06/30/23 09:47 321-60-806/27/23 21:1210-130 1
Nitrobenzene-d5 (S)54 %06/30/23 09:47 4165-60-006/27/23 21:1210-150 1
Terphenyl-d14 (S)53 %06/30/23 09:47 1718-51-006/27/23 21:1210-162 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.7 %06/23/23 13:43 N20.10 1
Analytical Method: EPA 7196A Preparation Method: EPA 7196A Modified
Pace Analytical Services - Asheville
7196 Chromium, Hexavalent
Chromium, Hexavalent ND mg/kg 06/27/23 21:28 18540-29-906/27/23 18:544.9 1
Analytical Method: EPA 7196A Leachate Method/Date: EPA 1312; 06/26/23 15:37
Pace Analytical Services - Asheville
7196 Chromium, Hex, SPLP
Chromium, Hexavalent ND mg/L 06/28/23 22:57 18540-29-9 H10.010 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
782815
EPA 3050B
EPA 6010D
6010D ATL
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples:92674134001, 92674134002, 92674134003, 92674134004, 92674134005, 92674134006, 92674134007,
92674134008, 92674134009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4060727
Associated Lab Samples:92674134001, 92674134002, 92674134003, 92674134004, 92674134005, 92674134006, 92674134007,
92674134008, 92674134009
Matrix:Solid
Analyzed
Arsenic mg/kg ND 2.8 06/28/23 20:55
Cadmium mg/kg ND 0.93 06/28/23 20:55
Chromium mg/kg ND 0.93 06/28/23 20:55
Copper mg/kg ND 3.7 06/28/23 20:55
Lead mg/kg ND 2.3 06/28/23 20:55
Nickel mg/kg ND 1.9 06/28/23 20:55
Selenium mg/kg ND 4.6 06/28/23 20:55
Silver mg/kg ND 0.93 06/28/23 20:55
Zinc mg/kg ND 2.8 06/28/23 20:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4060728LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 96.596.2 100 80-120
Cadmium mg/kg 95.396.2 99 80-120
Chromium mg/kg 97.896.2 102 80-120
Copper mg/kg 98.396.2 102 80-120
Lead mg/kg 95.996.2 100 80-120
Nickel mg/kg 98.296.2 102 80-120
Selenium mg/kg 92.596.2 96 80-120
Silver mg/kg 94.296.2 98 80-120
Zinc mg/kg 97.796.2 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4060729MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92673801001
4060730
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 115 94 75-125102 10 20117ND110122
Cadmium mg/kg 115 95 75-125101 8 20117ND110119
Chromium mg/kg 115 96 75-125107 12 201177.3 118 133
Copper mg/kg 115 101 75-125110 11 20117ND118132
Lead mg/kg 115 100 75-125114 13 2011727.9 143 162
Nickel mg/kg 115 99 75-125109 12 201173.3 117 132
Selenium mg/kg 115 83 75-12579 3 20117ND95.2 92.8
Silver mg/kg 115 95 75-125104 12 20117ND109122
Zinc mg/kg 115 95 75-125104 9 2011716.9 127 139
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
784181
EPA 3010A
EPA 6010D
6010D ATL TCLP
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples:92674134001, 92674134002, 92674134003, 92674134004, 92674134005, 92674134006, 92674134007,
92674134008, 92674134009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4065770
Associated Lab Samples:92674134001, 92674134002, 92674134003, 92674134004, 92674134005, 92674134006, 92674134007,
92674134008, 92674134009
Matrix:Water
Analyzed
Arsenic mg/L ND 0.30 07/01/23 06:40
Cadmium mg/L ND 0.10 07/01/23 06:40
Chromium mg/L ND 0.10 07/01/23 06:40
Copper mg/L ND 0.20 07/01/23 06:40
Lead mg/L ND 0.25 07/01/23 06:40
Nickel mg/L ND 0.20 07/01/23 06:40
Selenium mg/L ND 0.40 07/01/23 06:40
Silver mg/L ND 0.10 07/01/23 06:40
Zinc mg/L ND 0.20 07/01/23 06:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4067019LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/L 10.210 102 80-120
Cadmium mg/L 9.610 96 80-120
Chromium mg/L 9.810 98 80-120
Copper mg/L 10.210 102 80-120
Lead mg/L 9.410 94 80-120
Nickel mg/L 10.110 101 80-120
Selenium mg/L 10.810 108 80-120
Silver mg/L 1010 100 80-120
Zinc mg/L 9.510 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4067017MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674134001
4067018
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/L 10 104 75-125100 3 2010ND10.4 10.0
Cadmium mg/L 10 97 75-12594 3 2010ND9.7 9.4
Chromium mg/L 10 100 75-12597 3 2010ND109.7
Copper mg/L 10 103 75-125100 3 2010ND10.3 10.1
Lead mg/L 10 95 75-12592 3 2010ND9.5 9.2
Nickel mg/L 10 103 75-125100 4 2010ND10.3 10
Selenium mg/L 10 110 75-125108 2 2010ND11.0 10.8
Silver mg/L 10 103 75-12599 4 2010ND10.3 9.9
Zinc mg/L 10 96 75-12593 3 2010ND9.7 9.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
784185
EPA 7470A
EPA 7470A
7470 Mercury TCLP, ATL
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples:92674134001, 92674134002, 92674134003, 92674134004, 92674134005, 92674134006, 92674134007,
92674134008, 92674134009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4065770
Associated Lab Samples:92674134001, 92674134002, 92674134003, 92674134004, 92674134005, 92674134006, 92674134007,
92674134008, 92674134009
Matrix:Water
Analyzed
Mercury mg/L ND 0.0050 07/03/23 11:50
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4067040LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/L 0.0160.017 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4067038MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674134001
4067039
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/L 0.017 88 75-12597 10 200.017ND 0.015 0.016
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
783941
EPA 7471B
EPA 7471B
7471 Mercury
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples:92674134001, 92674134002, 92674134003, 92674134004, 92674134005, 92674134006, 92674134007,
92674134008, 92674134009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4065816
Associated Lab Samples:92674134001, 92674134002, 92674134003, 92674134004, 92674134005, 92674134006, 92674134007,
92674134008, 92674134009
Matrix:Solid
Analyzed
Mercury mg/kg ND 0.24 06/30/23 11:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4065817LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.320.33 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4065818MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674134001
4065819
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.4 109 75-125108 1 200.4ND 0.45 0.45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
782847
EPA 3546
EPA 8082A
8082 GCS PCB
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92674134001, 92674134002, 92674134003, 92674134004, 92674134005, 92674134006, 92674134007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4060833
Associated Lab Samples:92674134001, 92674134002, 92674134003, 92674134004, 92674134005, 92674134006, 92674134007
Matrix:Solid
Analyzed
PCB-1016 (Aroclor 1016)ug/kg ND 32.5 06/28/23 15:27
PCB-1221 (Aroclor 1221)ug/kg ND 32.5 06/28/23 15:27
PCB-1232 (Aroclor 1232)ug/kg ND 32.5 06/28/23 15:27
PCB-1242 (Aroclor 1242)ug/kg ND 32.5 06/28/23 15:27
PCB-1248 (Aroclor 1248)ug/kg ND 32.5 06/28/23 15:27
PCB-1254 (Aroclor 1254)ug/kg ND 32.5 06/28/23 15:27
PCB-1260 (Aroclor 1260)ug/kg ND 32.5 06/28/23 15:27
Decachlorobiphenyl (S)%88 10-174 06/28/23 15:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4060834LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/kg 98.0169 58 36-130
PCB-1260 (Aroclor 1260)ug/kg 128169 76 38-133
Decachlorobiphenyl (S)%81 10-174
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4060838MATRIX SPIKE SAMPLE:
MSSpike
Result
92674164001
PCB-1016 (Aroclor 1016)ug/kg 109171 64 10-144ND
PCB-1260 (Aroclor 1260)ug/kg 116171 68 10-141ND
Decachlorobiphenyl (S)%65 10-174
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92674141006
4060839SAMPLE DUPLICATE:
PCB-1016 (Aroclor 1016)ug/kg ND 30ND
PCB-1221 (Aroclor 1221)ug/kg ND 30ND
PCB-1232 (Aroclor 1232)ug/kg ND 30ND
PCB-1242 (Aroclor 1242)ug/kg ND 30ND
PCB-1248 (Aroclor 1248)ug/kg ND 30ND
PCB-1254 (Aroclor 1254)ug/kg ND 30ND
PCB-1260 (Aroclor 1260)ug/kg ND 30ND
Decachlorobiphenyl (S)%6758
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
782958
EPA 3546
EPA 8082A
8082 GCS PCB
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92674134008, 92674134009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4061046
Associated Lab Samples:92674134008, 92674134009
Matrix:Solid
Analyzed
PCB-1016 (Aroclor 1016)ug/kg ND 32.6 06/26/23 22:05
PCB-1221 (Aroclor 1221)ug/kg ND 32.6 06/26/23 22:05
PCB-1232 (Aroclor 1232)ug/kg ND 32.6 06/26/23 22:05
PCB-1242 (Aroclor 1242)ug/kg ND 32.6 06/26/23 22:05
PCB-1248 (Aroclor 1248)ug/kg ND 32.6 06/26/23 22:05
PCB-1254 (Aroclor 1254)ug/kg ND 32.6 06/26/23 22:05
PCB-1260 (Aroclor 1260)ug/kg ND 32.6 06/26/23 22:05
Decachlorobiphenyl (S)%80 10-174 06/26/23 22:05
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4061047LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/kg 133166 80 36-130
PCB-1260 (Aroclor 1260)ug/kg 157166 95 38-133
Decachlorobiphenyl (S)%92 10-174
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4061048MATRIX SPIKE SAMPLE:
MSSpike
Result
92672963041
PCB-1016 (Aroclor 1016)ug/kg 117249 47 10-144ND
PCB-1260 (Aroclor 1260)ug/kg 64.1249 26 10-141ND
Decachlorobiphenyl (S)%29 10-174
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92673900001
4061049SAMPLE DUPLICATE:
PCB-1016 (Aroclor 1016)ug/kg ND 30ND
PCB-1221 (Aroclor 1221)ug/kg ND 30ND
PCB-1232 (Aroclor 1232)ug/kg ND 30ND
PCB-1242 (Aroclor 1242)ug/kg ND 30ND
PCB-1248 (Aroclor 1248)ug/kg ND 30ND
PCB-1254 (Aroclor 1254)ug/kg ND 30ND
PCB-1260 (Aroclor 1260)ug/kg ND 30ND
Decachlorobiphenyl (S)%4119
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
783392
EPA 3546
EPA 8270E
8270E MSSV PAH by SIM
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92674134001, 92674134002, 92674134003, 92674134004, 92674134005, 92674134006, 92674134007,
92674134008, 92674134009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4063157
Associated Lab Samples:92674134001, 92674134002, 92674134003, 92674134004, 92674134005, 92674134006, 92674134007,
92674134008, 92674134009
Matrix:Solid
Analyzed
1-Methylnaphthalene ug/kg ND 10.1 06/30/23 06:15
2-Methylnaphthalene ug/kg ND 10.1 06/30/23 06:15
Acenaphthene ug/kg ND 10.1 06/30/23 06:15
Acenaphthylene ug/kg ND 10.1 06/30/23 06:15
Anthracene ug/kg ND 10.1 06/30/23 06:15
Benzo(a)anthracene ug/kg ND 10.1 06/30/23 06:15
Benzo(a)pyrene ug/kg ND 10.1 06/30/23 06:15
Benzo(b)fluoranthene ug/kg ND 10.1 06/30/23 06:15
Benzo(g,h,i)perylene ug/kg ND 10.1 06/30/23 06:15
Benzo(k)fluoranthene ug/kg ND 10.1 06/30/23 06:15
Chrysene ug/kg ND 10.1 06/30/23 06:15
Dibenz(a,h)anthracene ug/kg ND 10.1 06/30/23 06:15
Fluoranthene ug/kg ND 10.1 06/30/23 06:15
Fluorene ug/kg ND 10.1 06/30/23 06:15
Indeno(1,2,3-cd)pyrene ug/kg ND 10.1 06/30/23 06:15
Naphthalene ug/kg ND 10.1 06/30/23 06:15
Phenanthrene ug/kg ND 10.1 06/30/23 06:15
Pyrene ug/kg ND 10.1 06/30/23 06:15
2-Fluorobiphenyl (S)%56 10-130 06/30/23 06:15
Nitrobenzene-d5 (S)%62 10-150 06/30/23 06:15
Terphenyl-d14 (S)%61 10-162 06/30/23 06:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4063158LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/kg 15.0 L233.6 45 49-130
2-Methylnaphthalene ug/kg 18.033.6 54 50-130
Acenaphthene ug/kg 17.333.6 51 46-130
Acenaphthylene ug/kg 17.533.6 52 47-130
Anthracene ug/kg 18.733.6 56 48-130
Benzo(a)anthracene ug/kg 20.833.6 62 50-130
Benzo(a)pyrene ug/kg 16.933.6 50 37-130
Benzo(b)fluoranthene ug/kg 20.733.6 62 47-130
Benzo(g,h,i)perylene ug/kg 18.633.6 55 49-130
Benzo(k)fluoranthene ug/kg 19.333.6 58 47-130
Chrysene ug/kg 18.033.6 54 44-130
Dibenz(a,h)anthracene ug/kg 18.633.6 56 53-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4063158LABORATORY CONTROL SAMPLE:
LCSSpike
Fluoranthene ug/kg 22.233.6 66 50-130
Fluorene ug/kg 17.933.6 53 48-130
Indeno(1,2,3-cd)pyrene ug/kg 19.033.6 57 52-130
Naphthalene ug/kg 17.433.6 52 49-130
Phenanthrene ug/kg 17.233.6 51 45-130
Pyrene ug/kg 22.333.6 66 51-130
2-Fluorobiphenyl (S)%64 10-130
Nitrobenzene-d5 (S)%68 10-150
Terphenyl-d14 (S)%73 10-162
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4063159MATRIX SPIKE SAMPLE:
MSSpike
Result
92674134001
1-Methylnaphthalene ug/kg 23.842.9 55 14-130ND
2-Methylnaphthalene ug/kg 23.442.9 54 15-130ND
Acenaphthene ug/kg 22.242.9 52 19-130ND
Acenaphthylene ug/kg 22.742.9 53 25-130ND
Anthracene ug/kg 26.142.9 61 22-130ND
Benzo(a)anthracene ug/kg 26.542.9 62 14-130ND
Benzo(a)pyrene ug/kg 25.042.9 58 10-130ND
Benzo(b)fluoranthene ug/kg 24.842.9 58 10-130ND
Benzo(g,h,i)perylene ug/kg 21.442.9 50 10-130ND
Benzo(k)fluoranthene ug/kg 23.642.9 55 10-130ND
Chrysene ug/kg 22.442.9 52 10-130ND
Dibenz(a,h)anthracene ug/kg 21.542.9 50 10-130ND
Fluoranthene ug/kg 32.142.9 75 10-130ND
Fluorene ug/kg 23.442.9 55 21-130ND
Indeno(1,2,3-cd)pyrene ug/kg 21.842.9 51 10-130ND
Naphthalene ug/kg 22.442.9 52 22-130ND
Phenanthrene ug/kg 25.142.9 59 10-130ND
Pyrene ug/kg 31.442.9 73 10-130ND
2-Fluorobiphenyl (S)%37 10-130
Nitrobenzene-d5 (S)%50 10-150
Terphenyl-d14 (S)%67 10-162
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92674342001
4063160SAMPLE DUPLICATE:
1-Methylnaphthalene ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92674342001
4063160SAMPLE DUPLICATE:
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Pyrene ug/kg ND 30ND
2-Fluorobiphenyl (S)%4748
Nitrobenzene-d5 (S)%5255
Terphenyl-d14 (S)%5453
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
782429
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92674134001, 92674134002, 92674134003
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92673801006
4058770SAMPLE DUPLICATE:
Percent Moisture %14.4 N232514.9
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92674134003
4059180SAMPLE DUPLICATE:
Percent Moisture %19.9 N212520.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
782683
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92674134004, 92674134005, 92674134006, 92674134007, 92674134008, 92674134009
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92674208001
4059974SAMPLE DUPLICATE:
Percent Moisture %27.9 N222528.6
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92674141005
4059975SAMPLE DUPLICATE:
Percent Moisture %22.3 N262523.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
783389
EPA 7196A Modified
EPA 7196A
7196 Chromium, Hexavalent
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92674134001, 92674134002, 92674134003, 92674134004, 92674134005, 92674134006, 92674134007,
92674134008, 92674134009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4063145
Associated Lab Samples:92674134001, 92674134002, 92674134003, 92674134004, 92674134005, 92674134006, 92674134007,
92674134008, 92674134009
Matrix:Solid
Analyzed
Chromium, Hexavalent mg/kg ND 4.4 06/27/23 21:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4063146LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 23.923.6 101 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4063147MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92673273004
4063148
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg M11337375-12573 3 20128ND96.8 93.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 43
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
783388
EPA 7196A
EPA 7196A
7196 Chromium, Hexavalent
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92674134001, 92674134002, 92674134003, 92674134004, 92674134005, 92674134006, 92674134007,
92674134008, 92674134009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4061116
Associated Lab Samples:92674134001, 92674134002, 92674134003, 92674134004, 92674134005, 92674134006, 92674134007,
92674134008, 92674134009
Matrix:Water
Analyzed
Chromium, Hexavalent mg/L ND 0.010 06/28/23 22:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4063142LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/L 0.250.25 102 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4063143MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92674134001
4063144
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/L H10.25 99 75-125100 1 200.25ND 0.25 0.25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 43
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Analysis conducted outside the EPA method holding time.H1
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 43
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92674134001 782847 783508S-1 EPA 3546 EPA 8082A
92674134002 782847 783508S-2 EPA 3546 EPA 8082A
92674134003 782847 783508S-3 EPA 3546 EPA 8082A
92674134004 782847 783508S-4 EPA 3546 EPA 8082A
92674134005 782847 783508S-5 EPA 3546 EPA 8082A
92674134006 782847 783508S-6 EPA 3546 EPA 8082A
92674134007 782847 783508S-7 EPA 3546 EPA 8082A
92674134008 782958 783192S-8 EPA 3546 EPA 8082A
92674134009 782958 783192S-9 EPA 3546 EPA 8082A
92674134001 782815 782843S-1 EPA 3050B EPA 6010D
92674134002 782815 782843S-2 EPA 3050B EPA 6010D
92674134003 782815 782843S-3 EPA 3050B EPA 6010D
92674134004 782815 782843S-4 EPA 3050B EPA 6010D
92674134005 782815 782843S-5 EPA 3050B EPA 6010D
92674134006 782815 782843S-6 EPA 3050B EPA 6010D
92674134007 782815 782843S-7 EPA 3050B EPA 6010D
92674134008 782815 782843S-8 EPA 3050B EPA 6010D
92674134009 782815 782843S-9 EPA 3050B EPA 6010D
92674134001 784181 784224S-1 EPA 3010A EPA 6010D
92674134002 784181 784224S-2 EPA 3010A EPA 6010D
92674134003 784181 784224S-3 EPA 3010A EPA 6010D
92674134004 784181 784224S-4 EPA 3010A EPA 6010D
92674134005 784181 784224S-5 EPA 3010A EPA 6010D
92674134006 784181 784224S-6 EPA 3010A EPA 6010D
92674134007 784181 784224S-7 EPA 3010A EPA 6010D
92674134008 784181 784224S-8 EPA 3010A EPA 6010D
92674134009 784181 784224S-9 EPA 3010A EPA 6010D
92674134001 784185 784425S-1 EPA 7470A EPA 7470A
92674134002 784185 784425S-2 EPA 7470A EPA 7470A
92674134003 784185 784425S-3 EPA 7470A EPA 7470A
92674134004 784185 784425S-4 EPA 7470A EPA 7470A
92674134005 784185 784425S-5 EPA 7470A EPA 7470A
92674134006 784185 784425S-6 EPA 7470A EPA 7470A
92674134007 784185 784425S-7 EPA 7470A EPA 7470A
92674134008 784185 784425S-8 EPA 7470A EPA 7470A
92674134009 784185 784425S-9 EPA 7470A EPA 7470A
92674134001 783941 784082S-1 EPA 7471B EPA 7471B
92674134002 783941 784082S-2 EPA 7471B EPA 7471B
92674134003 783941 784082S-3 EPA 7471B EPA 7471B
92674134004 783941 784082S-4 EPA 7471B EPA 7471B
92674134005 783941 784082S-5 EPA 7471B EPA 7471B
92674134006 783941 784082S-6 EPA 7471B EPA 7471B
92674134007 783941 784082S-7 EPA 7471B EPA 7471B
92674134008 783941 784082S-8 EPA 7471B EPA 7471B
92674134009 783941 784082S-9 EPA 7471B EPA 7471B
92674134001 783392 784068S-1 EPA 3546 EPA 8270E
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 43
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92674134
TJs TRANSIENT MARINA
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92674134002 783392 784068S-2 EPA 3546 EPA 8270E
92674134003 783392 784068S-3 EPA 3546 EPA 8270E
92674134004 783392 784068S-4 EPA 3546 EPA 8270E
92674134005 783392 784068S-5 EPA 3546 EPA 8270E
92674134006 783392 784068S-6 EPA 3546 EPA 8270E
92674134007 783392 784068S-7 EPA 3546 EPA 8270E
92674134008 783392 784068S-8 EPA 3546 EPA 8270E
92674134009 783392 784068S-9 EPA 3546 EPA 8270E
92674134001 782429S-1 SW-846
92674134002 782429S-2 SW-846
92674134003 782429S-3 SW-846
92674134004 782683S-4 SW-846
92674134005 782683S-5 SW-846
92674134006 782683S-6 SW-846
92674134007 782683S-7 SW-846
92674134008 782683S-8 SW-846
92674134009 782683S-9 SW-846
92674134001 783389 783398S-1 EPA 7196A Modified EPA 7196A
92674134002 783389 783398S-2 EPA 7196A Modified EPA 7196A
92674134003 783389 783398S-3 EPA 7196A Modified EPA 7196A
92674134004 783389 783398S-4 EPA 7196A Modified EPA 7196A
92674134005 783389 783398S-5 EPA 7196A Modified EPA 7196A
92674134006 783389 783398S-6 EPA 7196A Modified EPA 7196A
92674134007 783389 783398S-7 EPA 7196A Modified EPA 7196A
92674134008 783389 783398S-8 EPA 7196A Modified EPA 7196A
92674134009 783389 783398S-9 EPA 7196A Modified EPA 7196A
92674134001 783388S-1 EPA 7196A
92674134002 783388S-2 EPA 7196A
92674134003 783388S-3 EPA 7196A
92674134004 783388S-4 EPA 7196A
92674134005 783388S-5 EPA 7196A
92674134006 783388S-6 EPA 7196A
92674134007 783388S-7 EPA 7196A
92674134008 783388S-8 EPA 7196A
92674134009 783388S-9 EPA 7196A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/03/2023 04:22 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 43
Page 41 of 43
Page 42 of 43
Page 43 of 43