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HomeMy WebLinkAboutWQ0016376_Monitoring - 04-2023_20230724Monitoring Report Submittal Permit Number#* WQ0016376 Name of Facility:* S&J VILLARI LIVESTOCK PROCESSING FACILITY - WARSAW Month: * April Year: * 2023 Report Information Type* Upload Document* NDMR, NDAR-1, NDAR-2, NDMLR WWT April 2023.pdf 7.49MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address: * gerald.m@vfgmail.com Name of Submitter: * Gerald Matthews Signature: Date of submittal: 7/24/2023 This will be filled in automatically Initial Review Reviewer: Wanda.Gerald Is the project number correct?* W00016376 Is the monitoring report accepted?* Yes NO Regional Office* Wilmington Reviewer: _anonymous Review Date: 7/25/2023 FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page % of f-, Permit No.: WQ0016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: April Year: 2023 Did irrigation Field Name: 1 Field Name: 2 Field Name: 3 Field Name: 4 occur Area (acres): 0.65 Area (acres): 1.16 Area (acres): 1.12 Area (acres): 1.07 at this facility? Cover Crop:Coastal Bermuda Cover Crop: p: Coastal Bermuda Cover Crop: p: Coastal Bermuda Cover Crop: p: Coastal Bermuda 1-1 YES F'J NO Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Weather Freeboard Field Irrigated? ❑ YES NO Field Irrigated? - YES -= No Field Irrigated? ❑ YES No Field Irrigated? [ YES 7 No p>. N 'D V N 4-7 �' d y N�' CL C 2 wO •a C N o ar N m M Na F- N -O Q 'a E • m J E a) 7 x 41 E2 o > Q -❑ E 7 E x d a E.2 oQ 7 --O N E =Q7 E X O E 11 . o CL J Q --yQ E .' E J E omC16 oo JN °F in in in gal min in in gal min in in gal min in in gal min in in 1 C 60 156 2 C 3 C 4 CL 5 CL 6 CL 7 CL 8 R 2.5 o C 10 G 11 C� _ -- 92 r - r ! • 13^ C;L -+ -- 15 C I 16 17 CL ( -� 7,299 23 0.41 0.41 13,027 42 0.41 0.41 1 12,577 40 0.41 0.41 11 12.016 39 0-41 0.41 18 G - 7,492 23 0.42 0.42 13.370 42 0.42 0.42 i2,909 40 0.42 0.42 12.333 39 0.42 0.42 19 C 7,251 23 0.41 0.41 12.941 42 0.41 0.41 12:495 1 40 0.41 0.41 11.937 39 ! 0.41 1 0.41 120 C 7,484 23 0.42 0.42 13.356 42 0.42 0.42 1 12,895 40 0.42 0.42 12.320 39 i 0.42 21 CL - 7,342 23 0.42 0.42 13.103 42 0.42 0.42 12,651 ! 40 ! 0.42 0.42 I 12.086 39 0.42 0 42 ���iii 22 R 0 05 I ��- . 23 241 C R i! 02 148 -- I 1 25 C27 28 29 30 R R R 90 I I 0.1 o w 31 a Monthly L.oading:l 36868 2.09 6_ .797 2.09 ! 63,527 2.09 I r0,692. 2.09 12 Niantri Floating Total (in).l EL2268 22.68 99.68 22.68• FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page Z of (,-' Permit No.: W00016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: April Year: 2023 Did irrigation occur Field Name: 5 Field Name: 6 Field Name: 7 Field Name: 8 Area (acres): 1.19 Area (acres): 1.17 Area (acres): 1.05 Area (acres): 1.25 at this facility? Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda YES =1 No Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Weather Freeboard Field Irrigated? ❑ YES "i NO Field Irrigated? YES No Field Irrigated? ❑ YES [I No Field Irrigated? - YES NO v - E � o •-o E EJa) m'0 m -ao > ac > Ej mo EE.o E .d o o E ' _ E Tz E n ~ = oo mi°= o rn = oMQ= o > Q >Q J7 Q oc > J J m r- n- °F in in in gal min in in gal min in in gal min in in gal min in in 1 C 60 156 2 C 3 C 4 CL 5 CL 6 CL 7 CL 8 R 2.5 9 C 10 C 13 C - -- -- ---- j 14 CL 15 C _ 16 C 17 CL _ 13,363 43 0.41 0.41 13.139 42 0.41 0.41 11,791 38 0.41 0.41 14,037 1 45 0.41 0.41 18 C 13,716 43 OA2 0.42 13.485 42 0.42 0.42 12,102 38 j 0.42 0.42 14,407 45 0.42 0.42 19 C --- -- 20 C 21 CL - _ - - 13,442 43 0,42 0.42 13.216 42 0.42 0.42 11,860 38 0.42 ! 0.42 14,120 I 45 0.422 j-0.42 22 R 0.05 _ - - 23 C --- - - 24 P. - 0.02 126 27 R 0.5 28 R 0 5- 29 R 0.1 30 R 0.01 90 148 Monthly t.oading�l 67,498 2.09 I 66.364 2.09 59,556 209 70'�01 2.09 r 12 Month Float;n ;ota1 �;�n : 22.68 l 22.68 22.68 22,68 13,276 43 0.41 0.41 13.053 42 0 41 0.41 11,714 38 0.41 0.41 ! 13,945 I 45 � 0.41 13,701 43 0.42 0.42 13.471 42 0.42 0.42 j 12,089 � 38 0.42 0.42 14.392 45 0.42 �0.411 0.42 FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page 3 of Permit No.: WQ0016376 Facility Name: S&J Milan Livestock Processing Facility -Warsaw County: Duplin Month: April Year: 2023 Field Name: 9 Field Name: 10 Field Name: 11 Field Name: 12 Did irrigation occur Area (acres): 1 Area (acres): 1.46 Area (acres): 1.43 Area (acres): 1.23 at this facility? Cover Crop:Coastal Bermuda Cover Crop: P� Coastal Bermuda Cover Crop: P� Coastal Bermuda Cover Crop: P� Coastal Bermuda YES No Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 u Annual Rate (in): 41.96 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Annual Rate (in): 41.96 Weather Freeboard Field Irrigated? ' J YFs =1 No Field Irrigated? ❑ YES NO Field Irrigated? ❑ YES No Field Irrigated? F. __ YES [ No >, O N a � YUm L Om m O J A ,-0� C � E 7 E '_ o J E <A ?' C O 0 N '13 EN a o a Q rn _L C �o m o J E LA C E v •O o% 6/ E N o a E = m Q1 m o E m C E O v 0 d a E O Q o a � Q 'D N y i LP T C o E LA 7 C E =>` woCl oE °F in in in gal min in in gal min in in gal min in in gal min in in 1 C 60 156 2 C 3 C 4 CL 5 CL 6 CL 7 CL 8 R 2.5 9 0 C 1C 1 Cr 12 C ---- 131 C -- --- 14 CL 15 C C I j -{ F16 17 CL _ 11,230 36 0.41 0.41 16,395 53 0.41 0.41 1 16,059 51 0.41 0.41 13.813 44 0.4 i j 0.41 18 C 11,526 1 36 0.42 0.42 16.828 53 0.42 0.42 16,482 51 I 0.42 0.42 14,177 44 0.42 0.42 191 C 11,156 36 0.41 0.41 16,288 53 0.41 0.41 15,953 51 0.41 0.41 j 13.722 44 ( 0.41 i 0.41 20 C _ 11,514 36 0.42 0.42 16,810 53 0.42 0.42 16,464 51 0.42 0.42 14,16� 0.42 0.42 121 CL 11,296 36 0.42 0.42 16.492 53 0.42 0.42 16,153 51 0.42 0.42 13.894 44 0.42 0.42 22 R 0.05 ' i 123 C 24 R - 002 i C C R 0.5 0 r R R R 0 0.0'I - 90 1 nn i I� 1- -� i i j i ------ ---- - ... - Monthly t.uadm13 g: i 56,722 2.09 82,813 2.09 �; 81, i 11 2.09 Fy, 768 2.09 - �2 Month Floating Total (++t): 22.68 22.68 22.68 22.6e FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page -/- of k Permit No.: WQ0016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: April Year: 2023 Did irrigation occur Field Name: 13 Field Name: 14E Field Name: 14W Field Name: 15 this facility? Area (acres): 2.16 Area (acres): 13.73 Area (acres): 7.7 Area (acres): 0.73 at Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda YES NO Hourly Rate (in): 0-6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Hourly Rate (in): 0.6 Annual Rate (in): 41.96 Annual Rate (in): 31.6 Annual Rate (in): 24.21 Annual Rate (in): 30.44 Weather Freeboard Field Irrigated? ❑ YES ❑ No Field Irrigated? ` YES NO Field Irrigated? ❑ YES ❑ NO Field Irrigated? ^ YES NO W m M c •0 a0 C a) ° _j rn r I`ip N •d CL > Q -m01 E Q X o m _ 0 Em >Q 'O a c roX0 � E x a)- E o E J a) -pO .o o EO - J E 'cU am Ea m= oE J °F in in in gal min in in gal min in in gal min in in gal min in in 1 C 60 156 2 C 3 I5 C 4 CL 128.214 384 0.34 0.05 71,905 216 0.34 0.10 CL 1 127,746 384 0.34 005 71,642 216 0.34 0.10 6 CL 1 127,567 384 0.34 0.05 71,541 216 0.34 0.10 7 CL 8 R 2.5 9 C 10 C 11 C 128.209 384 0.34 0.05 71,901 216 0.34 0.10 121 C 119.874 384 0.32 0.05 67,227 216 0.32 0.09 141 CL 15 C 16 C 17 CL _ 24,256 78 0.41 0.32 --. l 8.198 26 0.41 0.41 18 C i 24,896 78 0,42 0.33 8.414 26 1 0.42 0.42 19 C .i 24,097 78 0,41 0.32 8,144 26 0.41 0-41 20 C 24,869 78 0.42 0.33 I 8.405 26 0.42 0.42 21 CL - 24,399 78 0.42 0.32 _ 8.246 26 0-42 0.42 22 R 0.05 --- - 23-. 24 R I 0.02 - - 25 C 26 C r - ----- - 27 R O.S 28 P. 0.5 -- I I 1 R 0.1 ' I-- -� --�- - r3-C - R - 0.01 _ 90 -- i48 --.- - - i __.. _..__ ._... __ ._.... Monthly goading: , 122.517 209 631,610 i.69 3541216 1.69 4 40., 2 r:'4i ✓f 12 Month Floating Total (i a 22.68 21 33 21.33 FORM' NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page ') of C Permit No.: WQ0016376 Facility Name: S&J Villari Livestock Processing Facility -Warsaw County: Duplin Month: April Year: 2023 Did irrigation occur Field Name: 16 Field Name: 17 Field Name: Field Name: this facility? Area (acres): 1.25 Area (acres): 0.82 Area (acres): Area (acres): at Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Cover Crop: YES NO Hourly Rate (in): 0.6 Hourly Rate (in): 0.5 Hourly Rate (in): Hourly Rate (in): Annual Rate (in): 13.83 Annual Rate (in): 16.95 Annual Rate (in): Annual Rate (in): Weather Freeboard Field Irrigated? YES ❑ NO Field Irrigated? �1 YES _ NO Field Irrigated? ❑YES NO Field Irrigated? - YES _ NO >1 m W 3: c °o Ui o o m-o E a >< E ~ E rn x � 0 CLE L — o ET c E oE E m a °' — o J E D E ° m o _CD-o E .2 0 Q m°� o J E ? crn E�� oo J °F in in in gal min in in gal I min in in gal min in in gal min in in 1 C 60 156 2 C 3 C 4 CL 5 CL 12,126 181 0.36 0.12 7.954 119 0.36 0.18 6 CL 7 CL 8 R 2.5 19 C ; 10 C -- 12 C — - 113 C 14 15 CL C --�— _. i6 C 17 CL 11,599 181 0.34 0.11 7.609 119 0.34 0.17 1 18 C i9 C 20 C — — - 21 -�--.-_�- 22 R - 0.05 23 C -- 24 R 0.02 25 26 ---- 27 28 29 -C R - R _ 05 0.1- 30 R Monthly Loading: - - -- 23,725 0.70 5 563 0.70 0 0.00 0 -" o 0c 12 Month floating Tot (in). 7.04 --- 7.04 FORM: NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of 16 Did the application rates exceed the limits in Attachment B of your permit? Q Compliant ❑ Non -Compliant Were adequate measures taken to prevent effluent ponding in or runoff from the sites? P] Compliant ❑ Non -Compliant Was a suitable vegetative cover maintained on all sites as specified in your permit? ❑ Compliant ❑ Non -Compliant Were all setbacks listed in your permit maintained for every application to each permitted site? E Compliant ❑ Non -Compliant Were all freeboards maintained in accordance with the specified freeboard heights in your permit? 21 Compliant ❑ Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Gerald Lamar Matthews Permittee: Sam Villari Certification No.: 993131 Signing Official: Grade: SI Phone Number: 910-289-7500 Signing Official's Title: Owner Has the ORC changed since the previous NDAR-1? ❑ Yes C No Phone Number: 910-2.93-2157 Permit Exp.: 11/302025 L _ O2 ? Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel property gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the systern, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of water Quality Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page I of --4- Permit No.: WQ0016376 Facility Name: S&J Villari Livestock Processing Facility-Warsa County: Duplin Month: April Year: 2023 PPI: 001 Flow Measuring Point: ❑ influent Effluent ` No flow generated Parameter Monitoring Point: _ InfluentJ, Effluent _Groundwater Lowering ,Surface Water Parameter Code -► 50050 00310 00940 50060 31616 00610 00625 00620 00600 00400 00665 70300 00530 CU Q j E - o f= i U o ° L N c N O ° E m-Fz° . U o a G L Z C + z a C f O a -0 o °O -n o V) U) o a)E m° c-0 a o (n n cn 'o 24-hr hrs GPD mg/L mg/L mg/L #1100 mL mg/L mg/L mg/L mg/L su mg/L mg/L mg/L 1 OTOO 8 20,000 2 11:00 4 50,000 3 r5 07:00 10 78,910 4 07:00 10 79,100 07:00 10 77,200 6 1 07:00 10 73,400 <0.1 7.4 7 07:00 10 75,100 8 07:00 7 20,000 9 09:00 3 50,000 10 07:00 10 80,100 11 07:00 10 77,200 12 07:00 10 78,900 13 07:00 10 77,800 <0.10 7.3 _ 141 07:00 10 79,200 151 08:00 6 20,000 - 161 OT00 4 50,000 - -- - 17 07:00 10 79,100 18 07:00 10 74,480 - ----- ---- - --^-- _---� ^---- - 19 07:00 10 71,016 --- - 20 07:00 1n 72,830 <.10 I 6.3 ----.. 21 07:00 10 78,560 - 22 07:00 - 8 70,850 -- -t- - - - -- 23 07:00 5 50,000 _ 24 07:00 10 10,000- 25 261 127 07:00 07:00 07:00 _ 10 10 10 78,150------ 78,210 74,660 38 52 <0.1 17300 46-3 62.2 0.08 62.8 7.13 5,13 --- 316 56.5 -- -- ' ----- 28 07:00 10 75,690 29 07:00 7 80,610 1 30 15:00 5 10,000 _ _ I 31 -- Average: 63,036 38.00 52.00 0.00 17,300.00 46.30 62.20 0.08 62,80 5.13 31600 56.50 Daily Maximum: 80,610 38.00 52.00 0.10 17,300.00 46.30 62.20 0.08 62.80 7.40 1 5.13 316.00_1 56.50 I Daily Mtntmum: 10,000 38.00 52.00 0.10 17,300.00 46.30 62.20 008 62.80 6.3o7 5.13 I 316.00 56.50 I Sampling Type: Recorder Grab Grab Grab Grab Grab Grab Grab Grab Grab I Grab Grab Grab -- j -- _ Monthly Avg Limit, 100,260 I - ----- --• --------•-Daily limit: -- ---- I - I I .. _ - --- - - - ...--------- Sample Frequency: Recorder Montniy I Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly __- FORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page of 4 Permit No.: W00016376 Facility Name: S&J Villari Livestock Processing Facility-Warsa County: Duplin Month: April Year: 2023 PPI: 002 Flow Measuring Point: �] Influent lu] Effluent No now generated Parameter Monitoring Point: ^ Influent :` Effluent _Groundwater Lowering Surface water Parameter Code —► 50050 00625 00610 00620 00665 31616 00600 p _F0 : ` U E- � O O m E 2 ~ O 3 LL a m rn Y o Y Z 0 E o E Q O io Z w � r a E._ Zn t a E m o u- 0 U m� o ir Z 24-hr hrs GPD mg/L mg/L mg/L mg/L #/100 mL mg/L 1 07:00 8 20,000 2 11:00 4 50,000 3 07:00 10 78,910 4 07:00 10 79,100 5 07:00 10 77,200 6 07:00 10 73,400 7 07:00 10 75,100 8 07:00 7 20,000 9 09:00 3 50,000 10 07:00 10 80,100 11 07:00 10 77,200 12 07:00 10 78,900 13 07:00 10 77,800 _ 14 07:00 10 79,200 15 08:00 6 20,000 _ 16 07:00 4 50,000 17 07:00 10 79,100 -- -"" 18 07:00 10 74,480 —v-- ---- -- -------- 191 07:00 10 71,016 - - 20 07:00 10 72,830 21 07:00 10t70,850 78,560 22 07:00 8 23 07:00 5 50,000 24 07:00 10 10,000 25 07:00 10 78,150- 26 07:00 10 78,210 27 07:00 10 74,660 06 <0.2 <0.02 <0.04 19 2.4 28 07:00 10 75.690 29 07:00 7 80,610 30 15:00 _ _ 5 10,000 311, Average: Daily Maximum: 63,036 0.60 0.00 0.00 0.00 19.00 2.40 i �— 1 80,610 0.60 0.20 0.02 0.04 I 19.00 2A0 � _ I r Dailv Minimum: 10,000 060 0.20 0.02 0.04 19.00 I 2.40 Samplitig Type: Recorder Grab Grab Grab Grab Grab Monthly Avg. Lunit: Daily Lirnit: I - --------- I Sample Frequency: Recorder Monthly Monthly Montnly Monthly I Monrhiy - I ORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page •.:� of l lo.: WQ0016376 Facility Name: S&J Villari Livestock Processing Facility-Warsa County: Duplin Month: April Year: 2023 003 Flow Measuring Point: Influent Effluent _,i No flow generated Parameter Monitoring Point: — Influent :_j Effluent _^ Groundwater Lowering _ Surface Water rCode 0 50050 00625 00610 00620 00665 31616 00600 C O a)u E a; F O 3 U_ •C � C m cm Y ro Z M o E QE +� Z N 3 m r N 0 iE o U .R lL .O U C - 'O O Z tr hrs GPD mg/L mg/L mg/L mg/L #/100 mL mg/L 10 8 20,000 10 4 50,000 10 10 78,910 )0 10 79,100 )0 10 77,200 )0 10 73,400 )0 10 75,100 )0 7 20,000 )0 3 50,000 )0 10 80,100 )0 10 77,200 )0 10 78,900 )0 10 77,800 )0 10 79,200 )0 6 20,000 - -- )0 4 50,000 — -- - - )0 10 74,480 --- )0 10 71,016 — I --- -- --- )0 1 10 72,830 )C 10 78,560 - -- I )0 8 70,850 _ I )0 )0 5 10 50,000 10,000 1 0.08 0.05 1600 3.7 - — — i 1 -- I )— )0 )0 )0 10 10 10 10 78,150 78,210- 74,660 75,690 1.7 )C 7 80.610 -- — - - Average: 63,036 1 70 1.00 0.08 0.05 1,600.00 3.70 i ily Maximum: 80,610 1.70 1.00 0.08 0.05 1,600.00 3.70 lily Minimum: 10,000 1.70 1.00 0.08 0.05 1,600.00 3.70 impling Type: Recorder Grab I Grab Grab Grab Grab t Daily Limit I --- le- .requency_ - - Recorder Monthy Monthly Monthly I Monthly Monthly I i — -- - ----- �— —__ — 1------ - ... _ . FORM: NDMR 03-12 NON -DISCHARGE MONITORING REPORT (NDMR) Page __q_ of Sampling Person(s) Name: GERALD LAMAR MATTHEWS Name Certified Laboratories Name: Environmentat Chemists INC. Name: Water Agricultural Laboratories )es all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? ❑� Compliant ❑ Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification RC: GERALD LAMAR MATTHEWS Permittee: SAM VILLARI ertification No.: 993131 Signing Official: rade: SI Phone Number: 910-289-7500 Signing Official's Title: OWNER as the ORC changed since the previous NDMR? E/1 Yes ❑ No Phone Number: 910-293-2157 Permit Expiration: 11/30/2025 l Sra26 �d27 ��-- _ ZE-Lv23 Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penally of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete I arm aware that there are significant penalties for submitting false information, including the possibility of tines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Quality Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page_ of Permit No.: WQ0016376 Facility Name: SU Villari Livestock Processing Facility -Warsaw County: Duplin Month: April Year: 2023 Field Name: Zone 1 Field Name: Zone 2 Field Name: Zone 3 Field Name: Zone 4 Field Name: Zone 5 Area (acres): 0.65 Area (acres): 1.16 Area (acres): 1.12 Area (acres): 1.07 Area (acres): 1.19 Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermude Cover Crop: Coastal Bermude Cover Crop: Coastal Bermude Cover Crop: Coastal Bermuda Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Field Loaded? E, YES I __ NO Field Loaded? L ; YES j J No - Field Loaded? '- YES No Field Loaded? YES ❑ No Field Loaded? 0 YES {. NO Z Z ZZ O Z Z ZZ O D ZO2 Z 0) a a n 0 0. sa :o d o aa > n. IL ¢ - m 'CD ❑ 0)E U N f0 _I Z N d Z CU U _j Z Nd Z+ C c C 7 O a j O a ; L) O > C O a ) Oj 7 UO a > > L) > > > Month gal 54,845 mg/L Ibs/ac Ibs/ac gal mg/L lbs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac gal mg/L Ibslac Ibslac May 38A 26.8 26.8 97,880 38.1 26.8 26.8 94,485 38.1 26.8 26.8 90,286 38.1 26.8 26.8 100,412 38.1 26.8 26.8 June 31.774 35.8 14.6 41.4 56,706 35.8 14.6 41.4 54,750 35.8 14.6 41.4 522305 35.8 14.6 41.4 58,171 35.8 14.6 41.4 July 23.200 47.5 14.1 55.5 39,401 47.5 13.5 54.9 39,973 47.5 14.1 55.5 38,189 47.5 14.1 55.5 42,472 47.5 14.1 55.5 August 80,508 39.8 41.1 96.7 143,676 39.8 41.1 96.0 138,721 39.8 41.1 96,.7 132,827 39.8 41.2 96.8 147,392 39.8 41.1 96.7 September 32.740 55.8 23.4 120.1 58,429 55.8 23.4 119.4 56,413 55.8 23.4 120.1 53,895 55.8 23.4 120.2 59,939 55.8 23.4 120.1 October 0 36.7 0.0 120.1 0 36.7 0.0 119.4 0 36.7 0.0 120.1 0 36.7 0.0 120.2 0 36.7 0.0 120.1 November 30,888 50.6 20.1 140.2 55,122 50.6 20.1 139.5 53,222 50.6 20.1 140.1 50,846 50.6 20.1 140.2 56,548 50.6 20.1 140.2 December 15,799 25.6 5.2 145.3 28,196 25.6 5.2 144.7 27,223 25.6 5.2 145.3 26,608 25.6 5.3 145.6 28,325 25.3 5.0 145.2 January 33,163 36.2 15.4 160.7 59,182 36.2 15.4 160.1 57,142 36.2 15.4 160.7 54,590 36.2 15.4 161.0 60.712 36.2 15.4 j 160.6 February 0 31.8 0.0 160.7 0 31.8 0.0 160.1463t7l 31.8 0.0 160.7 0 31.8 0.0 161.0 0 31.8 0.0 160.6 March 60,397 41 31.8 192.5 107,787 41 31.8 191.8 41 31.8 192.5 99,425 41 31.8 192.7 110,575 41 31.8 192.4 April 36,868 28.6 13.5 206.0 65,797 28.6 13.5 205.4 28.6 13.5 206.0 60,692 28.6 13.5 206.3 67,498 28.6 13.5 205.9 12 Month Floating PAN Load (Ibslac/yr): 206.0 205.4 206.0 206.3 205.9 Annual PAN Load Limit (Ibs/ac/yr): 350 350.00 350.00 350.00 350.00 FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page Z of S7- Permit No.: WQ0016376 Facility Name: SU Villari Livestock Processing Facility -Warsaw County: Duplin Month: April Year: 2023 Field Name: Zone 6 Field Name: Zone 7 Field Name: Zone 8 Field Name: Zone 9 Field Name: Zone 10 Area (acres): 1.17 Area (acres): 1.05 Area (acres): 1.25 Area (acres): 1 Area (acres): 1.46 Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Field Loaded? � YES F_? NO Field Loaded? I'I YES ;-j No Field Loaded? u YEs No Field Loaded? YEs ❑ NO Field Loaded? '' YEs - No 2)Z C Z D Z C Z N z C Z d z C Z N C Q d ` m cam Q Q 4 ` �_j Q roJ > J ary m > c°v ° r @_j a)- ma > m ° f9,°j d °� �ro °u (D > Z CD c 7 a c p � a ar j£ a, � ;° aa V V o 2 o aV 2 U o Qj v' °o v°, ao v > > L) > > > Month gal 98,724 mg/L Ibs/ac Ibslac gal mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac gal m /L g Ibs/ac Ibslac gal mg/L Ibslac Ibslac May 38.1 26.8 26.8 88,599 38.1 26.8 26.8 105,474 38.1 26.8 26.8 84,378 38.1 26.8 26.8 123,193 38.1 26.8 26.8 June 57;194 35.8 14.6 41.4 51,327 35.8 14.6 41.4 61,105 35.8 14.6 41.4 48,884 35.8 14.6 41.4 71,370 35.8 14.6 41.4 July 41.759 47.5 14.1 55.5 37,475 47.5 14.1 55.5 44,614 47.5 14.1 55.5 35,691 47.5 14.1 55.5 52,109 47.5 14.1 55.5 August 144,915 39.8 41.1 96.7 130,051 39.8 41.1 96.7 154,822 39.8 41.1 96.7 123,858 39.8 41.1 96.7 180,832 39.8 41.1 96.7 September 58,931 55.8 23.4 120.1 52,888 55.8 23.4 120.1 62.962 55.8 23.4 120.1 50,370 55.8 23.4 120.1 73,539 55.8 23.4 120.1 October 0 36.7 0.0 120.1 0 36.7 0.0 1201 0 36.7 0.0 120.1 0 36.7 0.0 120.1 0 36.7 0.0 120.1 November 55,598 50.6 20.1 140.2 49,896 50.6 20.1 140.2 59.399 50.6 20.1 140.2 47,519 50.6 20.1 140.2 69,380 50.6 20.1 140.2 December 28,438 25.6 5.2 145.3 25,522 25.6 5.2 145.3 30,384 25.6 5.2 145.3 24,306 25.6 5.2 145.3 35,488 25.6 5.2 145.3 January 59,691 36.2 15.4 160.7 53,571 36.2 15.4 160.7 63,773 36.2 15.4 160.7 51,019 36.2 15.4 160.7 74,489 36.2 15.4 160.7 February 0 31.8 0.0 160.7 0 31.8 0.0 160.7 0 31.8 0.0 160.7 0 31.8 &0 160.7 0 31.8 0.0 160.7 March 108,717 41 31.8 192.5 97,567 41 31.8 192.5 116,151 41 31.8 192.5 92,920 41 31.8 192.5 135,664 41 31.8 192.5 April 66,364 28.6 13.5 206.0 59,556 28.6 13.5 206.0 70,901 28.6 13.5 206.0 56,722 28.6 13.5 206.,0 82,813 28.6 13.5 206.0 12 Month Floating PAN Load (Ibs/ac/yr): 206.0 206.0 ��' 206.0 206.0 .. 206.0 �a< Annual PAN Load Limit 77 µ (Ibs/ac/yr): 350 350.00 350.00 350.00 111 u 350.00 FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page -3 of Permit No.: WQ0016376 Facility Name: SU Villari Livestock Processing Facility -Warsaw County: Duplin Month: April Year: 2023 Field Name: Zone 11 Field Name: Zone 12 Field Name: Zone 13 Field Name: Zone 14E Field Name: Zone 14W Area (acres): 1.43 Area (acres): 1.23 Area (acres): 2.16 Area (acres): 13.73 Area (acres): 7.7 Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Cover Crop: Coastal Bermuda Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Field Loaded? = YES --NO Field Loaded? i._] YES ❑ NO Field Loaded? .J YES 7 NO Field Loaded? [Z, YES [-, NO Field Loaded? YES NO v a' Z o a z y >-EL � 2 Z o z v v 2 z o z a w z o z ¢ m 'p z o ¢' z > n m n¢ a a v a :' m J a a m o¢. ' m J ° a io > ¢ m IV C A d = 0 r+ j J Z 0 C d ,4, J Z ¢ m C 2 N T a-=+ J 7 Z ¢ � C f`V d T � o J Z ¢ � +`-� N N ?. R J � Z c _j o = ¢ c = a. E c = ¢ E y " = E ¢ E ° aL.� -°.I = E ¢ 0 > > o ¢ c� o > > o ¢ ° c� o > 0 > ¢ 0 ° U a 2 > = U o ' a. L) > > ° 0 ° g 3 a. U V j U 0 ¢ ; ¢ Month gal 120,663 mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibslac gal mg/L Ibslac Ibs/ac gal mg/L Ibslac Ibslac May 38.1 26.8 26.8 103,787 38.1 26.8 26.8 182,259 38.1 26.8 26.8 1.271,672 38.1 29A 29.4 713,224 38.1 29.4 29.4 June 69,904 35.8 14.6 41.4 60.126 35.8 14.6 41 A 105,590 35.8 14.6 41.4 1.232,318 35.8 26.8 56.2 691.103 35.8 26.8 56.2 July 51,039 47.5 14.1 55.5 43,900 47.5 14.1 55.5 77,092 47.5 14.1 55.5 373,498 47.5 10.8 67.0 209.462 47.5 10.8 67.0 August 177,117 39.8 41.1 96.7 152,072 39.8 41.0 96.6 267,534 39.8 41.1 96.7 1,301,064 39.8 31.5 98.5 729.657 39.8 31.5 98.5 September 72,028 55.8 23.4 120.1 61,953 55.8 23.4 120.0 108,797 55.8 23.4 120.1 568,929 55.8 19.3 117.7 319.063 55.8 19.3 117.7 October 0 36.7 0.0 120.1 0 367 00 120.0 0 36.7 0.0 120.1 0 36.7 0.0 117.7 0 36.7 0.0 117.7 November 67,953 50.6 20.1 140.2 58,449 50.6 20.1 140.1 102,643 50.6 20.1 140.2 898,247 50.6 27.6 145.4 503,749 50.6 27.6 145.4 December 34,759 25.6 5.2 145.3 29,697 25.6 5.2 145.2 52,502 25.6 5.2 145.3 191,560 25.6 3.0 148.3 107,430 25.6 3.0 148.3 January 72,957 36.2 15.4 160.7 1 62,753 36.2 15.4 160.6 110,202 36.2 15.4 160.7 546,990 36.2 12.0 160.4 306,760 36.2 12.0 160.4 February 0 31.8 0.0 160.7 0 31 8 0.0 160.6 0 31.8 0.0 160.7 246,807 31.8 4.8 165.1 138,414 31.8 4.8 165.1 March 132,877 41 31.8 192.5 114,293 41 318 192.4 200,711 41 31.8 192.5 689,966 41 17.2 182.3 386,943 41 17.2 182.3 April 81,111 28.6 13.5 206.0 69,768 28.6 13.5 205.9 122,517 28.6 13.5 206.0 631,610 28.6 11.0 193.3 354,216 28.6 11.0 193.3 12 Month Floating PAN Load 206.0 (Ibslac/yr); �'� 205.9 206.0 193 3 193.3 Annual PAN Load Limit 350 350.00 350.00 350.00 350.00 (Ibslac/yr): ��w FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page V of S^ Permit No.: W00016376 Facility Name: SU Villari Livestock Processing Facility -Warsaw County: Duplin Month: April Year: 2023 Field Name: Zone 15 Field Name: Zone 16 Field Name: Zone 17 Field Name: Field Name: Area (acres): 0.73 Area (acres): 1.25 Area (acres): 0.82 Area (acres): Area (acres): Cover Crop: Norfolk Cover Crop: Coastal Bermud Cover Crop: Coastal BermudE Cover Crop: Cover Crop: Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Field Loaded? YES No Field Loaded? YES I_ II No Field Loaded? `' YES J: No Field Loaded ❑ Yrs .� No Field Loaded? �_ YES NO d a z Q O z Q >� m z a o z a ;' z Q° z Q ;� ,Q z Q O z Q d z Q° z Q m� a �� Q a �a °0 Q a a� ;� �° ° ° ° ° �° ° a� a° @o 0 E d u c J �0 E E °� '� v � J E E @ m c J �� z Q �� R rm J J E Z J � z O C ° Q 7 n- 7 C ° 7 Q > CD U C O E 3 > C c 7 E C : 7 > a U g 0 > a U g a > a g a U a O R U O > a O a U ; ; ; Month gal 61.597 mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibslac gal mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac gal mg/L Ibs/ac Ibs/ac May 38.1 26.8 26.8 24,814 38.1 6.3 6.3 16,278 38.1 6.3 6.3 June 35,685 35.8 14.6 41.4 23,098 35.8 5.5 11.8 15,153 35.8 5.5 11.8 July 26,054 47.5 14.1 55.5 24,142 47.5 7.7 19.5 15,838 47.5 7.7 19.5 August 90,417 39.8 41.1 96.7 24,232 39.8 6.4 25.9 15.896 39.8 6.4 25.9 September 36,770 1 55.8 23.4 120.1 22,826 55.8 8.5 34.4 14,974 55.8 8.5 34.4 October 0 36.7 0.0 120.1 0 36.7 0.0 34.4 0 36.7 0.0 34.4 November 34.689 50.6 20.1 140.2 24,072 50.6 8.1 42.5 15,791 50.6 8.1 42.5 December 17,744 25.6 5.2 145.3 24,662 25.6 4.2 46.7 16,178 25.6 4.2 46.7 January 37.243 36.2 15.4 160.7 11,612 36.2 2.8 49.6 7,618 36.2 2.8 49.6 February 0 31.8 0.0 160.7 11,783 31.8 2.5 52.1 7,730 31.8 2.5 52.1 March 67,833 41 31.8 192.5 24,159 41 6.6 58.7 15,849 41 6.6 58.7 April 67.833 1 41 31.8 224.3 24,159 41 6.6 65.3 15,849 41 6.6 65.3 12 Month Floating PAN Load (Ibs/ac/yr): 224.3 65.3 65.3 0.0 0.0 Annual PAN Load 350 350.00 350.00 0.00 i 0.00 FORM: NDMLR 10-13 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page �- of S Did the mass loading rates exceed the limits in Attachment B of your permit? ❑� Compliant ❑ Non -compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification II Permittee Certification ORC: Gerald Lamar Matthews Permittee: SAM VILLARI Certification Number: 993131 Signing Official: Grade: SI Phone Number: 910-289-7500 Signing Official's Title: OWNER Has the ORC changed since the previous NDMLR? ❑ Yes 21 No Phone No.: 910-293-2157 Permit Exp.: 11/30/25 Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab a 910.392.4424 Fax 7I0 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info(r%environmentalchemists.com The Pork Company Date of Report; May 10, 2023 892 Penny Branch Road Customer PO #: Warsaw NC 28398 Customer ID: 08100099 Attention: Report #: 2023-08345 Project ID: WWTF Eff - Mthly Lab ID Sample ID: Collect DatelTime Matrix Sampled by 23-21061 Site: Effluent Grab 4/27/2023 8:30 AM Water Gerald Matthews Test Method Results Date Analyzed PAN Calculation 28.6 mg1L 05/10/2023 Used 30% Mineralization Rate.. Total Dissolved Solids (TDS) SM 2540 C-2015 316 mglL 04/27/2023 Residue Suspended (TSS) SM 2640 D-2015 56.5 mg/L 04/28/2023 Arnmonia Nitrogen SM 4500 NH3 C-2011 46.3 mg/L 04/28/2023 Total Kjeldahl Nitrogen (TKN) SM 4500 Norg B-2011 62.2 mg/L 04/28/2023 Total Phosphorus SM 4500 P (F-H,-2011 5.13 mg/L 05/05/2023 BOJ Sample estimated Gid not meet quality SM 5210 B-2016 >61 mg/L 04/27/2023 control requirements, Blank=0.39mglL, above acceptable limit of 0.2-mg/L and GGA=123%. above acceptable limits of (85-115%) and DO dep:etion not met Fecal Coliform Chloride Nitrate Nitrogen (Cale) Nitrite Nitrogen Nitrate Nitrogen Total Nitrogen (Cale) Nitrate+N itrite-Nitrogen Total Nitrogen Lab ID Sample ID: 23-21061A Site: Effluent Grab Tesr BOD Reanalyzed outside of hold time. SM 92238-Mw SM4500 0 E-2011 17300 MPN/100mi 04/27/2023 52 mg/L 05/01/2023 EPA 353 2. Rev, 2 0, 1993 0.08 mg1L 04/28/2023 Subtraction Method 0.56 mg/L 05/10/2023 EPA 353 2. Rev 2 0, 1993 0.64 mg/L 05/01 /2023 Total Nitrogen 62.8mg/L 05/10/2023 Method SM 5210 B-2016 Collect Date/Time Matrix Sampled by 4/27/2023 8:30 AM Water Gerald Matthews Results 38 mg/L Date Analyzed 05/04/2023 Report 0 2023-08345 Page 1 of 2 — : - 77 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab o 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 s 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info," envi ron men talchemists.com The Pork Company Date of Report: May 10, 2023 892 Penny Branch Road Customer PO #: Warsaw NC 28398 Customer ID: 08100099 Attention: Report #: 2023-08345 Project ID: WWTF Eff - Mthly Lab ID �..« Sample ID: Collect Date/Time Matrix .._�.�. Sampled by .�_.. 23-21062 Site: PPI-002 Upstream 4/27/2023 9:00 AM Water Gerald Matthews Test Ammonia Nitrogen Total Phosphorus Fecal Coliform Nitrate Nitrogen (Cale) Nitrite Nitrogen Nitrate Nitrogen Total Nitrogen (Cale) Total Kieldahl Nitrogen (TKN) Nitrate+Nitrite-Nitrogen Total Nitrogen Method EPA 350 1 Rev 2 0, 1993 SM 4500 P (F-H)-2011 SM 9222 0-2015 MF EPA 353 2 Rev 2 0, 1993 Subtraction Method EPA 351 2 Rev 2 0, 1993 EPA 353 2 Rev 2 0- 1993 Total Nitrogen Results Date Analyzed Lab ID Sample ID: Collect Date/Time Matrix 23-21063 Site: PPI-003 Downstream 4/27/2023 8:50 AM Water < 0.2 mg/L 05/03/2023 < 0.04 mg/L 05/05/2023 19 Colonies1100ml- 04/27/2023 < 0.02 mg/L 04/28/2023 1.75 mg/L 05/10/2023 0.6 mg/L 05/04/2023 1.75 mg/L 05/01/2023 2.4 mg/L 05/10/2023 Sampled by Gerald Matthews Test Method Results Date Analyzed Ammonia Nitrogen EPA 350 1, Rev 20, 1993 1.0 mg/1- 05/03/2023 Total Phosphorus SM 4500 P F,F-H�-2011 0.05 mg/L 05/05/2023 Fecal Coliform SM 9222 D-2015 MF 1600 Colonies1100mL 04/27/2023 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353 2, Rev 2 0 1993 0.08 mg/L 04/28/2023 Nitrate Nitrogen Subtraction Method 1.89 mg/L 05/10/2023 Total Nitrogen (Cale) Total Kieldahl Nitrogen (TKN) EPA 3512 Rev 20 1993 1.7 mg/L 05/04/2023 Nitrate+Nitrite-Nitrogen EPA 3532.Rev. 20.1993 1.97mg/L 05/01/2023 Total Nitrogen Total Nitrogen 3.7 mg/L 05/ 1012023 Comment: Reviewed by: � y„� W Report N 2023-08345 Page 2 of 2 Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way Wilmington, NC 28405 Sample Receipt Checklist 910.392.0223 Client: ll_Date: AA4 eport Number:- 2023- Qd� Receipt of sample: YES ❑ NO ECHEM Pickup Client Cie ver ❑pS ❑ — Y FedEx O Other Ei- ® NIA © YES ❑ NO 1. Were custody seals present on the Gooier? Originsl temperature upon N/A 2. If custody seals were present, were they intact/unbroken? receipt °C Corrected temperature upon receipt How temperature taken: ❑ Temperature Blank 2 Against Bottles l Gun ID: Thomas Traceable S/N 210886869 IR Gun Correction factor °C: 0.0 1�9 YES l YES ❑ ❑ i40 NO 3. If temperature of cooler exceeded 6'C, was Project Mgr./QA notified? [t YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? 12 YES 5. Were sample ID's listed on the COC? ❑ NO Ll Were samples 10's fisted on sample containers? YES ❑ NO 7. Were collection date and time listed on the it YES 0 NO 8. Were tests to be performed listed on the COC? YES YES ❑ ❑ NO 9. Did samples arrive in proper containers for each test? YES NO 10. Did samples arrive in good condition for each test? —` ® NO 11. Was adequate sample volume available?' -- !� YES ❑ NO 12. Were samples received within proper holding time for requested tests? YES ❑ YES 17 ❑ NO 13, Were acid preserved samples received at a pH of <2? ❑ NO 14. Were cyanide samples received at a pH >12? YES ❑ NO 15. Were sulfide samples received at a pH >9? YES 0 YES ❑ ❑ NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 rn/L?# - YES ❑ NO NO 17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 rnJL? 18. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/Voiatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. ample ?reservation:: (Must be completed for any sample(sj incorrect) or ample(s) y preserved with headspace) were received incorrectly preserved and were adjusted accordingly y adding (circle one): H2504 HNO3 HCi NaOH ime of preservation: If more than one preservative is needed, notate in comments below cte: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or rtify the state lab if directed to analyzed by the customer. who was notified, date and time: olatiies Sample{s) were received with headspace COMMENTS: DOC. Q4.002 Rev 1 6602 Windmill Way mington ENVIRONMENTAL CHEMISTS, INC OFFICE: 910302-02231FAX910-392-44245 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS• DLS CERTIFICATION # 37729 info@environmentaichemists.com COLLECTION AND CHAIN OF CUSTODY CLIENT: The Pork Company PROJECT NAME: WWTF Effluent REPORT NO: ADDRESS: 1012 US Hwy 117 CONTACT NAME: PO NO: Warsaw, NC 28398 REPORT TO: Gerald Matthews, ORC PHONE/FAX: Permit Number: W00016376 email: Sampled B SAMPLE TYPE: I = Influent, E - Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification PPI-001 Effluent-1 PPI-001 (Effluent-1 S t) March, July, November PPI-001 (Effl-Triannuah PPI-002 PPI-002 due 1/month Collection PRESERVATION = a , TX1 E o �. u E 3 ANALYSIS REQUESTED Date Time Tem �, a z = _ = C X G G 80D,TSS,NO2 C P G G X Z' , NO3, NH3, TKN'Total P, PAN, Total NL C P�..__ X v Fecal Coliform G G �_ I I I ITDS, Chloride X X I (Fecal Cnlifnrm' X j lFecal Coliform Total P, Total N Total P, Total N i ransrer Relin fished Date/Time Rec d B : Date/Time 2. Temperature when Received °C:- `Accepted: Rejected: example Requested: Delivered By: Received By: t iDate: f� -„ �„ lime: comments TURNAROUND: