NCG150056_2023 DMR_20230721

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG150000
Airports
Click here for instructions
Complete,sign,scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report(DMR)Upload form within
30 days of receiving sampling results. Mail the original,signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Mailed in DMRs must contain an original wet signature. Electronic signatures will not be accepted for mailed in DMRs.This is a
requirement until the permittee has registered for eDMR for reporting.
Certificate of Coverage No. NCG15 0056 Person Collecting Samples:Deontae Watson
Facility Name: Fayetteville Regional Airport Laboratory Name: Microbac Laboratories, Inc.-Fayetteville
Facility County: Cumberland Laboratory Cert. No.: ii (certification is attached)
Discharge during this period:®Yes ❑ No (if no,skip to signature and date)
Has your facility implemented mandatory Tier response actions for any benchmark exceedances?❑Yes ® No
If so,which Tier(I,II,or III)?
A copy of this DMR has been uploaded electronically via https://edocs.deq.nc.gov/Forms/SW-DMR ®Yes ❑ No
Date Uploaded:
Part A:Analytical Monitoring Requirements for Outfalls with Industrial Activities—Benchmarks in (Red)
Parameter Parameter Outfall Outfall Outfall Outfall Outfall
Code
N/A Receiving Stream Class C C C C C
N/A Date Sample Collected MM/DD/YYYY 6/20/23 6/20/23 6/20/23 6/20/23 6/20/23
46529 24-Hour Rainfall in inches 0.38in 0.38in 0.38in 0.38in 0.38in
00400 pH(Freshwater:6-9,Saltwater:6.8-
8.5) 9.4 8.8 9.4 9.2 8.5
C0530 TSS in mg/L(100 or 50*) <2.55 19.1 7.98 4.34 <2.50
01027 Conductivity in µohms/cm 0.00166 0.00171 0.00078 0.0037 0.00185
C0034 Chemical Oxygen Demand(COD)in
mg/L(120) <20 <20 <20 <20 <20
Non-Polar Oil&Grease in mg/L(15)
00552 for drainage areas that use>55
gal/mo of new hydraulic oil on avg. <5.0 <5.2 <5.0 <5.0 <5.0
NCOIL Estimated New Motor/Hydraulic Oil
Usage in gal/month N/A N/A N/A N/A N/A
* Outfalls to Outstanding Resource Waters(ORW),High Quality Waters(HQW),Trout Waters(Tr)and Primary Nursery Areas(PNA)
have a benchmark TSS limit of 50 mg/L.All other water classifications have a benchmark of 100 mg/L.
Notes(optional):
"I certify by my signature below, under penalty of law,that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for
gathering the information,the information submitted is,to the best of my knowledge and belief,true, accurate, and complete. I am
aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for
knowing viol tions."
,497VSID 'liCtibj __ 7/21/2023
Signature of Permittee or Delegated Authorized Individual Date

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Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K3B0233
Project Description
Stormwater
For:
Deontae Watson
Fayetteville Regional Airport, NC
400 Airport Road Suite 1
Fayetteville, NC 28306
Customer Relationship Associate
Samantha Oakes
Friday,July 7, 2023
Please find enclosed the analytical results for the samples you submitted to Microbac Laboratories. Review and compilation of
your report was completed by Microbac Laboratories, Inc.-Fayetteville. If you have any questions,comments,or require further
assistance regarding this report, please contact your service representative listed above.
I certify that all test results meet all of the requirements of the accrediting authority listed within this report.Analytical results are
reported on a'as received'basis unless specified otherwise.Analytical results for solids with units ending in(dry)are reported
on a dry weight basis. A statement of uncertainty for each analysis is available upon request.This laboratory report shall not be
reproduced, except in full,without the written approval of Microbac Laboratories.The reported results are related only to the
samples analyzed as received.
1
Microbac Laboratories, Inc.
2592 Hope Mills Rd I Fayetteville,NC 28306 1910.864.1920 p I www.microbac.com
Page 1 of 8

( MICROBAC"
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K3B0233
Fayetteville Regional Airport,NC Project Name: Stormwater
Deontae Watson Project/PO Number: N/A
400 Airport Road Suite 1 Received: 06/20/2023
Fayetteville, NC 28306 Reported: 07/07/2023
Sample Summary Report
Sample Name Laboratory ID Client Matrix Sample Type Sample Begin Sample Taken Lab Received
Outfall 1 K3B0233-01 Stormwater Grab 06/20/23 08:45 06/20/23 12:45
Outfall 2 K3B0233-02 Stormwater Grab 06/20/23 08:50 06/20/23 12:45
Outfall 3 K3B0233-03 Stormwater Grab 06/20/23 09:14 06/20/23 12:45
Outfall 4 K3B0233-04 Stormwater Grab 06/20/23 09:06 06/20/23 12:45
Outfall 5 K3B0233-05 Stormwater Grab 06/20/23 09:26 06/20/23 12:45
Page 2 of 8

< MICROBAC
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K3B0233
Analytical Testing Parameters
Client Sample ID: Outfall 1
Sample Matrix: Stormwater Collected By: Client
Lab Sample ID: K3B0233-01 Collection Date: 06/20/2023 8:45
Inorganics Total Result MDL RL Units DF Note Prepared Analyzed Analyst
Method: Chemical Oxygen Demand Preparation/SM 5220 D-2011
Chemical Oxygen Demand(COD) <20.0 6.89 20.0 mg/L 1 06/27/23 1130 07/05/23 1515 JRB
Method: EPA 1664B
Oil&Grease(HEM) <5.0 2.2 5.0 mg/L 1 07/06/23 1147 07/07/23 1147 BNS
Method:SM 2540 D-2015
Total Suspended Solids(TSS) <2.55 2.55 2.55 mg/L 1 D8 06/22/23 1218 CJB
Client Sample ID: Outfall 2
Sample Matrix: Stormwater Collected By: Client
Lab Sample ID: K3B0233-02 Collection Date: 06/20/2023 8:50
Inorganics Total Result MDL RL Units DF Note Prepared Analyzed Analyst
Method:Chemical Oxygen Demand Preparation/SM 5220 D-2011
Chemical Oxygen Demand(COD) <20.0 6.89 20.0 mg/L 1 06/27/23 1130 07/05/23 1515 JRB
Method:EPA 1664B
Oil&Grease(HEM) <5.2 2.3 5.2 mg/L 1 07/06/23 1147 07/07/23 1147 BNS
Method:SM 2540 D-2015
Total Suspended Solids(TSS) 19.1 2.50 2.50 mg/L 1 06/22/23 1218 CJB
Client Sample ID: Outfall 3
Sample Matrix: Stormwater Collected By: Client
Lab Sample ID: K3B0233-03 Collection Date: 06/20/2023 9:14
Inorganic_s Total Result MDL RL Units DF Note Prepared Analyzed Analyst
Method:Chemical Oxygen Demand Preparation/SM 5220 D-2011
Chemical Oxygen Demand(COD) <20.0 6.89 20.0 mg/L 1 06/27/23 1130 07/05/23 1515 JRB
Method:EPA 1664B
Oil&Grease(HEM) <5.0 2.1 5.0 mg/L 1 07/06/23 1147 07/07/23 1147 BNS
Method:SM 2540 D-2015
Total Suspended Solids(TSS) 7.98 2.53 2.53 mg/L 1 06/22/23 1218 CJB
Microbac Laboratories, Inc. - Fayetteville
2592 Hope Mills Rd I Fayetteville,NC 28306 1910.864.1920 p I www.microbac.com Page 3 of 8 J

(5) MICROBACR
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K3B0233
Client Sample ID: Outfall 4
Sample Matrix: Stormwater Collected By: Client
Lab Sample ID: K3B0233-04 Collection Date: 06/20/2023 9:06
Inorganics Total Result MDL RL Units DF Note Prepared Analyzed Analyst
Method:Chemical Oxygen Demand Preparation/SM 5220 D-2011
Chemical Oxygen Demand(COD) <20.0 6.89 20.0 mg/L 1 06/27/23 1130 07/05/23 1515 JRB
Method: EPA 1664B
Oil&Grease(HEM) <5.0 2.2 5.0 mg/L 1 07/06/23 1147 07/07/23 1147 BNS
Method:SM 2540 D-2015
Total Suspended Solids(TSS) 4.34 2.53 2.53 mg/L 1 06/22/23 1218 CJB
Client Sample ID: Outfall 5
Sample Matrix: Stormwater Collected By: Client
Lab Sample ID: K3B0233-05 Collection Date: 06/20/2023 9:26
Inorganics Total Result MDL RL Units DF Note Prepared Analyzed Analyst
Method:Chemical Oxygen Demand Preparation/SM 5220 D-2011
Chemical Oxygen Demand(COD) <20.0 6.89 20.0 mg/L 1 06/27/23 1130 07/05/23 1515 JRB
Method:EPA 1664B
Oil&Grease(HEM) <5.0 2.1 5.0 mg/L 1 07/06/23 1147 07/07/23 1147 BNS
Method:SM 2540 D-2015
Total Suspended Solids(TSS) <2.50 2.50 2.50 mg/L 1 06/22/23 1218 CJB
Microbac Laboratories, Inc. - Fayetteville
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 4 of 8

( MICROBAC
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K3B0233
Batch Log Summary
Method Batch Laboratory ID Client/Source ID
SM 2540 D-2015 KF32116 KF32116-BLK2
K3B0233-05 Outfall 5
KF32116-BLK1
KF32116-DUP1 K3F0127-01
KF32116-DUP2 K3F0127-02
KF32116-BS1
KF32116-BS2
K3B0233-01 Outfall 1
K3B0233-02 Outfall 2
K3B0233-03 Outfall 3
K3B0233-04 Outfall 4
Method Batch Laboratory ID Client I Source ID
SM 5220 D-2011 KF32243 KF32243-MS1 K3F0298-02
KF32243-CCV4
KF32243-CCB1
KF32243-CCB2
KF32243-CCB3
KF32243-CCV1
KF32243-CCV2
KF32243-CCV3
KF32243-BLK1
K3B0233-05 Outfall 5
KF32243-BS1
KF32243-MRL1
K3B0233-01 Outfall 1
K3B0233-02 Outfall 2
K3B0233-03 Outfall 3
K3B0233-04 Outfall 4
KF32243-DUP1 K3F0298-02
Method Batch Laboratory ID Client/Source ID
EPA 1664B KG30004 KG30004-DUP1 K3F0174-01
KG30004-BS1
KG30004-MS1 K3F0174-02
K3B0233-01 Outfall 1
K3B0233-02 Outfall 2
K3B0233-03 Outfall 3
K3B0233-05 Outfall 5
KG30004-BLK1
Microbac Laboratories, Inc. - Fayetteville
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 5 of 8

(9MICROBAC'°
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K3B0233
EPA 1664B KG30004 K3B0233-04 Outfall 4
Batch Quality Control Summary: Microbac Laboratories, Inc.-Fayetteville
Spike Source %REC RPD
Inorganics Total Result RL Units Level Result %REC Limits RPD Limit Notes
Batch KF32116-Wet Chem Aqueous-SM 2540 D-2015
PBW01 (KF32116-BLK1) Prepared&Analyzed:06/22/2023 12:18
Total Suspended Solids(TSS) <83.3 83.3 mg/L
PBWO2(KF32116-BLK2) Prepared&Analyzed:06/22/2023 12:18
Total Suspended Solids(TSS) <83.3 83.3 mg/L
LCSW01 (KF32116-BS1) Prepared&Analyzed:06/22/2023 12:18
Total Suspended Solids(TSS) 96.8 2.50 mg/L 99.8 97 95-105
LCSW02(KF32116-BS2) Prepared&Analyzed:06/22/202312:18
Total Suspended Solids(TSS) 95.9 2.50 mg/L 100 96 95-105
Influent,CompositeD(KF32116-DUP1) Source:K3F0127-01 Prepared&Analyzed:06/22/2023 12:18 S1
Total Suspended Solids(TSS) 248 41.7 mg/L 88.3 95 10
Influent,CompositeD(KF32116-DUP2) Source: K3F0127-02 Prepared&Analyzed:06/22/2023 12:18 S1
Total Suspended Solids(TSS) 7.80 5.00 mg/L ND 10
Batch KF32243-COD_Prep-SM 5220 D-2011
PBW01 (KF32243-BLK1) Prepared:06/27/2023 11:30 Analyzed:07/05/2023 15:15
Chemical Oxygen Demand(COD) <20.0 20.0 mg/L
LCSW01 (KF32243-BS1) Prepared:06/27/2023 11:30 Analyzed:07/05/2023 15:15
Chemical Oxygen Demand(COD) 76.5 mg/L 75.0 102 90-110
002D(KF32243-DUP1) Source:K3F0298-02 Prepared:06/27/2023 11:30 Analyzed:07/05/2023 15:15
Chemical Oxygen Demand(COD) <20.0 20.0 mg/L ND 10
002S(KF32243-MS1) Source: K3F0298-02 Prepared:06/27/2023 11:30 Analyzed:07/05/2023 15:15
Chemical Oxygen Demand(COD) 95.1 20.0 mg/L 75.0 ND 127 80-120 Al2
Batch KG30004-Wet Chem Aqueous-EPA 1664B
Blank(KG30004-BLK1) Prepared:07/06/202311:47 Analyzed:07/07/2023 11:47
Oil&Grease(HEM) <5.0 5.0 mg/L
LCS(KG30004-BS1) Prepared:07/06/2023 11:47 Analyzed:07/07/2023 11:47
Oil&Grease(HEM) 39.6 5.0 mg/L 40.0 99 78-114
Duplicate(KG30004-DUP1) Source:K3F0174.01 Prepared:07/06/2023 11:47 Analyzed:07/07/2023 11:47
i
Oil&Grease(HEM) <5.0 5.0 mg/L ND 18
Matrix Spike(KG30004-MS1) Source:K3F0174-02 Prepared:07/06/2023 11:47 Analyzed:07/07/2023 11:47
Oil&Grease(HEM) 40.7 5.2 mg/L 40.0 ND 102 78-114
Microbac Laboratories, Inc. - Fayetteville
2592 Hope Mills Rd I Fayetteville,NC 28306 1910.864.1920 p I www.microbac.com Page 6 of 8

OMICROBAC`P
Microbac Laboratories, Inc. - Fayetteville
CERTIFICATE OF ANALYSIS
K3B0233
Definitions
Al2: MS/MSD fail recovery,but the LCS passes criteria.
D8: Sample yielded<2.5 mg dried residue with<1 L volume analyzed.
mg/L: Milligrams per Liter
RL: Reporting Limit
RPD: Relative Percent Difference
S1: Relative Percent Difference(RPD)outside accepted recovery limits
Cooler Receipt Log
Cooler ID: Default Cooler Temp: 14.3°C
Cooler Inspection Checklist
Ice Present or not required? Yes Shipping containers sealed or not required? Yes
Custody seals intact or not required? Yes Chain of Custody(COC)Present? Yes
COC includes customer information? Yes Relinquished and received signature on COC? Yes
Sample collector identified on COC? Yes Sample type identified on COC? Yes
Correct type of Containers Received Yes Correct number of containers listed on COC? Yes
Containers Intact? Yes COC includes requested analyses? Yes
Enough sample volume for indicated tests received? Yes Sample labels match COC(Name,Date&Time?) Yes
Samples arrived within hold time? Yes Correct preservatives on COC or not required? Yes
Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes
VOA vials have zero headspace,or not recd.? Yes
Project Requested Certification(s)
Microbac Laboratories, Inc.-Fayetteville
11 North Carolina Department of the Environment and Natural Resources
Report Comments Reviewed and Approved By:
Samples were received in proper condition and the reported results conform to
applicable accreditation standard unless otherwise noted. kAANa•-$COALje
The data and information on this,and other accompanying documents,represents only the
sample(s)analyzed. This report is incomplete unless all pages indicated in the footnote are Samantha Oakes
present and an authorized signature is included. The services were provided under and Customer Relationship Associate
subject to Microbac's standard terms and conditions which can be located and Reported: 07/07/2023 16:00
reviewed at<https://www.microbac.com/standard-terms-conditions>.
Microbac Laboratories, Inc. - Fayetteville
2592 Hope Mills Rd I Fayetteville, NC 28306 1910.864.1920 p I www.microbac.com Page 7 of 8

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